2016-01-18
6
Title: Microwave-assisted stereoselective
alpha-2-deoxyglycosylation of hex-1-en-3-uloses Author(s): Lin HC,
Wu HH, Lin ZP, et al. Source: TETRAHEDRON LETTERS Volume: 50 Issue:
52 Pages: 7327-7329 Published: DEC 30 2009
Title: Microwave-assisted McMurry polymerization utilizing
low-valent titanium for the synthesis of poly
2,6-[1,5-bis(dodecyloxy)naphthylene vinylene] (PNV) Author(s):
Thomas H, Stuhr-Hansen N, Westerlund F, et al. Source: TETRAHEDRON
LETTERS Volume: 50 Issue: 52 Pages: 7374-7378 Published: DEC 30
2009
Title: Microwave-Assisted, Rapid, Solvent-Free Aza-Michael
Reaction by Perchloric Acid Impregnated on Silica Gel Author(s):
Singh SP, Kumar TV, Chandrasekharam M, et al. Source: SYNTHETIC
COMMUNICATIONS Volume: 39 Issue: 22 Pages: 3982-3989 Published:
2009
Title: Novel One-Pot Synthesis of 3-Phenylnaphtho[2,3-b]furan
and 3-Phenylbenzofurans Under Microwave Irradiation and
Solvent-Free Conditions Author(s): Wang ZX, Gu JZ, Jing HW, et al.
Source: SYNTHETIC COMMUNICATIONS Volume: 39 Issue: 22 Pages:
4079-4087 Published: 2009
Title: Synthesis and characterization of Eu-doped hydroxyapatite
through a microwave assisted microemulsion process Author(s): Yang
C, Yang PP, Wang WX, et al. Source: SOLID STATE SCIENCES Volume: 11
Issue: 11 Pages: 1923-1928 Published: NOV 2009
Title: Synthesis, Spectral and Biological Evaluation of Some
Mesoporphyrinic Zn(II) Complexes Author(s): Boscencu R, Socoteanu
R, Ilie M, et al. Source: REVISTA DE CHIMIE Volume: 60 Issue: 10
Pages: 1006-1011 Published: OCT 2009
Title: Synthesis and Antimicrobial Activity of New Aromatic
Esters of Potential Interest in Supramolecular Chemistry Author(s):
Balan AM, Zbancioc G, Bentea E, et al. Source: REVISTA DE CHIMIE
Volume: 60 Issue: 10 Pages: 1021-1024 Published: OCT 2009
Title: Synthesis of Novel Flower-Like Zn(OH)F via a
Microwave-Assisted Ionic Liquid Route and Transformation into
Nanoporous ZnO by Heat Treatment Author(s): Song JK, Zheng MB, Yang
ZJ, et al. Source: NANOSCALE RESEARCH LETTERS Volume: 4 Issue: 12
Pages: 1512-1516 Published: DEC 2009
Title: Microwave-assisted solid-phase peptide synthesis at 60
degrees C: alternative conditions with low enantiomerization
Author(s): Loffredo C, Assuncao NA, Gerhardt J, et al. Source:
JOURNAL OF PEPTIDE SCIENCE Volume: 15 Issue: 12 Pages: 808-817
Published: DEC 2009
Title: Microwave-assisted synthesis of ZnO micro-javelins
Author(s): Padmanabhan SC, Ledwith D, Pillai SC, et al. Source:
JOURNAL OF MATERIALS CHEMISTRY Volume: 19 Issue: 48 Pages:
9250-9259 Published: 2009
brak
rozpuszczalnika
selektywno
ciecze jonowe
nonik stay **
nonik stay *
1.
Microwave-Assisted Bleaching of Wool Fabrics
By: Abou El-Kheir, Amira; Haggag, Karima; Mowafi, Salwa I.; et
al.
JOURNAL OF NATURAL FIBERS Volume: 12 Issue: 2 Pages: 97-107
Published: MAR 4 2015
2.
Microwave-assisted synthesis of graphene-Ni composites with
enhanced microwave absorption properties in Ku-band
By: Zhu, Zetao; Sun, Xin; Li, Guoxian; et al.
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS Volume: 377 Pages:
95-103 Published: MAR 1 2015
3.
Single-crystalline AgIn(MoO4)(2) nanosheets grafted Ag/AgBr
composites with enhanced plasmonic photocatalytic activity for
degradation of tetracycline under visible light
By: Yan, Xu; Wang, Xiyou; Gu, Wei; et al.
APPLIED CATALYSIS B-ENVIRONMENTAL Volume: 164 Pages: 297-304
Published: MAR 2015
4.
Inhibition of photocorrosion and photoactivity enhancement for
ZnO via specific hollow ZnO core/ZnS shell structure
By: Yu, Linhui; Chen, Wei; Li, Danzhen; et al.
APPLIED CATALYSIS B-ENVIRONMENTAL Volume: 164 Pages: 453-461
Published: MAR 2015
5.
Preparation, characterisation and physicochemical properties of
the phosphate modified peanut protein obtained from
Arachin Conarachin L.
By: Yu, Lina; Yang, Weiqiang; Sun, Jie; et al.
FOOD CHEMISTRY Volume: 170 Pages: 169-179 Published: MAR 1
2015
6.
Optimisation and validation of the microwave-assisted extraction
of phenolic compounds from rice grains
By: Setyaningsih, W.; Saputro, I. E.; Palma, M.; et al.
FOOD CHEMISTRY Volume: 169 Pages: 141-149 Published: FEB 15
2015
7.
Negative pressure cavitation-microwave assisted preparation of
extract of Pyrola incarnata Fisch. rich in hyperin, 2 '-O-
galloylhyperin and chimaphilin and evaluation of its antioxidant
activity
By: Yao, Xiao-Hui; Zhang, Dong-Yang; Luo, Meng; et al.
FOOD CHEMISTRY Volume: 169 Pages: 270-276 Published: FEB 15
2015
http://www.uni-graz.at/~kappeco/index.htm
Enhanced Deprotection, Coupling, and Cleavage Reactions
Galanin Synthesis
Reaction Reagents Time Max Temp.
(C)
Deprotection 20% Piperidine / DMF 3 min 21=A, 75=B
Coupling HBTU/HOBt/DIEA 0.9/1/1 ,
x10 excess
4 min 21=A, 75=B
Cleavage Reagent K
18 min 38=A and B
GWTLNSAGYLLGPQQFFGLM-NH2 Conditions
Scale: 0.10mmol w/ MBHA Rink Amide Resin, 0.59meq/g.
(Novabiochem)
A= Conventional
B= Microwave
GWTLNSAGYLLGPQQFFGLM-NH2
Conventional
(Purity = < 10 %)
Microwave
(Purity = 84.8%)
Efekty nietermiczne?
czy rnice w:
szybkoci
wydajnoci
selektywnoci
to tylko wynik szybkiego, rwnomiernego
ogrzania reagentw?
czy w ogle s rnice?
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2016-01-18
7
ania
olejowa
reaktor
mikrofalowy
Img_8960.jpg
Natalia Wisowska, 2006.
Termostat Obserwacja Palladium Catalyzed Aminocarbonylation of
Aryl
Halides
Carbonylation reactions those which incorporate CO
into a molecule often pose experimental challenges
due to the difficulties which accompany the use of
carbon monoxide gas at elevated pressure. In situ
generation of CO gas from reaction of potassium tert-
butoxide and dimethylformamide provides a safe and
convenient route for carbonylation reactions. The
microwave assisted, palladium catalyzed
aminocarbonylation of aryl halides with in situ
generated carbon monoxide has been reported.2 With
the Discover SP camera, both color change and
continued generation of carbon monoxide gas can be
observed throughout the reaction, assisting with rapid
reaction optimization.
1) Leadbeater, N. E.; McGowan, C. C. Clean, Fast Organic
Chemistry; CEM Publishing, 2006.
(2) Wan, Y.; Alterman, M.; Larhed, M.; Hallberg, A. J. Org.
Chem. 2002, 67, 6232.
