Philadelphia, PA 19145 Certificate of Analysis...Grooms , Mr. Larry Gould , Ms. Jessica Mason , Mr. Dan McKenna , Mr. Chin So This page is included as part of the Analytical Report

Report ID: 2219776 - 4/13/2017 Page 1 of 36

Mr. Jeffrey HamPhiladelphia Gas Works (PGW)3100 West Passyunk AvenuePhiladelphia, PA 19145

April 13, 2017

Dear Mr. Ham:

Certificate of AnalysisProject Name:Purchase Order:

Soils Workorder:Workorder ID:

2219776PGW001|Passyunk LP Tank Area S

CC: Ms. Amy Brown , Mr. Eric Hendrickson , Jobi Cherian , Mr. KevinGrooms , Mr. Larry Gould , Ms. Jessica Mason , Mr. Dan McKenna ,Mr. Chin SoThis page is included as part of the Analytical Report andmust be retained as a permanent record thereof. Project Coordinator

Mrs. Vanessa N Badman

Enclosed are the analytical results for samples received by the laboratory on Tuesday, April 4, 2017.

The ALS Environmental laboratory in Middletown, Pennsylvania is a National Environmental LaboratoryAccreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet therequirements of NELAP.

If you have any questions regarding this certificate of analysis, please contact Mrs. Vanessa N Badman (ProjectCoordinator) at (717) 944-5541.

Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and anyapplicable state requirements. The test results meet requirements of the current NELAP standards or staterequirements, where applicable. For a specific list of accredited analytes, refer to the certifications section of theALS website at www.alsglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads.

This laboratory report may not be reproduced, except in full, without the written approval of ALS Environmental.

ALS Spring City: 10 Riverside Drive, Spring City, PA 19475 610-948-4903

NELAP Certifications: NJ PA010 , NY 11759 , PA 22-293 DoD ELAP: A2LA 0818.01State Certifications: DE ID 11 , MA PA0102 , MD 128 , VA 460157 , WV 343

DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 2 of 36

Workorder: 2219776 PGW001|Passyunk LP Tank Area S

SAMPLE SUMMARY

Lab ID Sample ID Matrix Date Collected Date Received Collected By

2219776001 04032017-01 Solid 4/3/2017 13:25 4/4/2017 20:00 Ms. Jessica Mason









DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 3 of 36


SAMPLE SUMMARY

Standard Acronyms/Flags

Notes

-- All Waste Water analyses comply with methodology requirements of 40 CFR Part 136.-- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141.-- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis.-- The Chain of Custody document is included as part of this report.

Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyteIndicates that the analyte was Not Detected (ND)

Method Detection LimitPractical Quantitation Limit

JU

MDLPQL

Reporting Detection LimitNot Detected - indicates that the analyte was Not Detected at the RDLAnalysis was performed using this containerRegulatory Limit

RDLNDCntr

RegLmtLaboratory Control SampleMatrix Spike

LCSMS

Matrix Spike DuplicateSample DuplicatePercent Recovery

MSDDUP

%RecRelative Percent DifferenceRPD

-- Samples collected by ALS personnel are done so in accordance with the procedures set forth in the ALS Field Sampling Plan (20 - Field Services Sampling Plan).

N Indicates presumptive evidence of the presence of a compound

-- All Library Search analytes should be regarded as tentative identifications based on the presumptive evidence of the mass spectra. Concentrations reported are estimated values. -- Parameters identified as "analyze immediately" require analysis within 15 minutes of collection. Any "analyze immediately" parameters not listed under the header "Field Parameters" are preformed in the laboratory and are therefore analyzed out of hold time.

LOD DoD Limit of DetectionLOQ DoD Limit of QuantitationDL DoD Detection Limit

-- Method references listed on this report beginning with the prefix “S” followed by a method number (such as S2310B-97) refer to methods from “Standard Methods for the Examination of Water and Wastewater”.

I Indicates reported value is greater than or equal to the Method Detection Limit (MDL) but less than the Report Detection Limit (RDL)(S) Surrogate CompoundNC Not Calculated* Result outside of QC limits

-- For microbiological analyses, the "Prepared" value is the date/time into the incurbator and the "Analyzed" value is the date/time out the incubator.


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 4 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-01

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

4/3/2017 13:25

CntrMethod

SEMIVOLATILESAcenaphthene 2380 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DAcenaphthylene 6840 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DAcetophenone 174 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DAnthracene 7730 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DAtrazine ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DBenzaldehyde 277 ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DBenzo(a)anthracene 26600 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DBenzo(a)pyrene 29000 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DBenzo(b)fluoranthene 32800 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DBenzo(g,h,i)perylene 19600 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DBenzo(k)fluoranthene 11200 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DBiphenyl 619 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Bromophenyl-phenylether ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DButylbenzylphthalate ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DCaprolactam ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DCarbazole 531 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Chloro-3-methylphenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Chloroaniline ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Chloronaphthalene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Chlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Chlorophenyl-phenylether ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DChrysene 34700 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270Dmp-Cresol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270Do-Cresol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDi-n-Butylphthalate ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDi-n-Octylphthalate 387 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDibenzo(a,h)anthracene 5440 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDibenzofuran 610 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D3,3-Dichlorobenzidine ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,4-Dichlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDiethylphthalate ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,4-Dimethylphenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DDimethylphthalate ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,4-Dinitrophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 5 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-01

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776001


Date Collected:

Date Received:

4/3/2017 13:25

CntrMethod

2,4-Dinitrotoluene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,6-Dinitrotoluene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D1,4-Dioxane ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DFluoranthene 28600 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DFluorene 2510 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DHexachlorobenzene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DHexachlorobutadiene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DHexachlorocyclopentadiene ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DHexachloroethane ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DIndeno(1,2,3-cd)pyrene 19400 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DIsophorone ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Methylnaphthalene 4710 ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DNaphthalene 6800 ug/kg 56.9 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Nitroaniline ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D3-Nitroaniline ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Nitroaniline ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DNitrobenzene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Nitrophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D4-Nitrophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DN-Nitrosodiphenylamine ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DPentachlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DPhenanthrene 28300 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DPhenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DPyrene 49700 ug/kg 1140 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 114 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,4,5-Trichlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2,4,6-Trichlorophenol ND ug/kg 228 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4,6-Tribromophenol (S) 90.2 % 19 - 132 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270D2,4,6-Tribromophenol (S) 87.8 % 19 - 132 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Fluorobiphenyl (S) 81.5 % 40 - 110 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270D2-Fluorobiphenyl (S) 76.4 % 40 - 110 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Fluorophenol (S) 66.1 % 26 - 116 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D2-Fluorophenol (S) 65.6 % 26 - 116 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 6 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-01

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776001


Date Collected:

Date Received:

4/3/2017 13:25

CntrMethod

Nitrobenzene-d5 (S) 72.3 % 38 - 112 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DNitrobenzene-d5 (S) 78.8 % 38 - 112 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DPhenol-d5 (S) 72.8 % 35 - 111 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DPhenol-d5 (S) 73.9 % 35 - 111 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270DTerphenyl-d14 (S) 87.7 % 45 - 126 4/8/17 00:10 CMA 4/13/17 03:32 GEC ASW846 8270DTerphenyl-d14 (S) 84 % 45 - 126 4/8/17 00:10 CMA 4/10/17 16:48 GEC ASW846 8270D

WET CHEMISTRYMoisture 12.1 % 0.1 4/7/17 11:54 VKBS2540G-11Total Solids 87.9 % 0.1 4/7/17 11:54 VKBS2540G-11

METALSAluminum, Total 5880 mg/kg 11.4 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CAntimony, Total ND mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CArsenic, Total 41.8 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CBarium, Total 58.2 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CBeryllium, Total ND mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CCadmium, Total ND mg/kg 0.57 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CCalcium, Total 4270 mg/kg 11.4 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CChromium, Total 30.5 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CCobalt, Total 5.2 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CCopper, Total 70.8 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CIron, Total 17100 mg/kg 11.4 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CLead, Total 223 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CMagnesium, Total 2840 mg/kg 11.4 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CManganese, Total 340 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CMercury, Total 0.23 mg/kg 0.048 4/5/17 03:30 AXC 4/5/17 07:44 AXC A2SW846 7471BNickel, Total 18.9 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CPotassium, Total 400 mg/kg 56.9 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CSelenium, Total ND mg/kg 5.7 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CSilver, Total ND mg/kg 0.57 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CSodium, Total 105 mg/kg 56.9 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CThallium, Total ND mg/kg 3.4 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CVanadium, Total 24.4 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010CZinc, Total 443 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:04 TSS A1SW846 6010C


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 7 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-01

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776001


Date Collected:

Date Received:

4/3/2017 13:25

CntrMethod

Project CoordinatorMrs. Vanessa N Badman


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 8 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-02

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776002


Date Collected:

Date Received:

4/3/2017 13:31

CntrMethod

VOLATILE ORGANICSAcetone ND ug/kg 9.0 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BBenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BBromochloromethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BBromodichloromethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BBromoform ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BBromomethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B2-Butanone ND ug/kg 9.0 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BCarbon Disulfide ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BCarbon Tetrachloride ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BChlorobenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BChlorodibromomethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BChloroethane ND ug/kg 4.5 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BChloroform ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BChloromethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BCyclohexane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2-Dibromo-3-chloropropane

ND ug/kg 4.5 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B

1,2-Dibromoethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2-Dichlorobenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,3-Dichlorobenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,4-Dichlorobenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BDichlorodifluoromethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,1-Dichloroethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2-Dichloroethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,1-Dichloroethene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Bcis-1,2-Dichloroethene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Btrans-1,2-Dichloroethene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2-Dichloropropane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Bcis-1,3-Dichloropropene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Btrans-1,3-Dichloropropene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,4-Dioxane ND ug/kg 67.5 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BEthylbenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BFreon 113 ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B2-Hexanone ND ug/kg 9.0 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BIsopropylbenzene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BMethyl acetate ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BMethyl cyclohexane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 9 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-02

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776002


Date Collected:

Date Received:

4/3/2017 13:31

CntrMethod

Methyl t-Butyl Ether ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B4-Methyl-2-Pentanone(MIBK)


Methylene Chloride ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BStyrene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,1,2,2-Tetrachloroethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BTetrachloroethene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BToluene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BTotal Xylenes ND ug/kg 5.4 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2,3-Trichlorobenzene ND ug/kg 4.5 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,2,4-Trichlorobenzene ND ug/kg 4.5 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,1,1-Trichloroethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B1,1,2-Trichloroethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BTrichloroethene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BTrichlorofluoromethane ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BVinyl Chloride ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Bo-Xylene ND ug/kg 1.8 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260Bmp-Xylene ND ug/kg 3.6 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B


1,2-Dichloroethane-d4 (S) 82.9 % 56 - 124 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B4-Bromofluorobenzene (S) 104 % 51 - 128 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BDibromofluoromethane (S) 92.6 % 62 - 123 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260BToluene-d8 (S) 98.3 % 59 - 131 4/4/17 23:51 SYB 4/5/17 07:23 SYB BSW846 8260B

SEMIVOLATILESAcenaphthene 541 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DAcenaphthylene 1980 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DAcetophenone ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DAnthracene 1790 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DAtrazine ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DBenzaldehyde ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DBenzo(a)anthracene 5240 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DBenzo(a)pyrene 8600 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DBenzo(b)fluoranthene 10100 ug/kg 225 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270DBenzo(g,h,i)perylene 9780 ug/kg 225 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270DBenzo(k)fluoranthene 3500 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DBiphenyl 308 ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Bromophenyl-phenylether ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DButylbenzylphthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 10 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-02

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776002


Date Collected:

Date Received:

4/3/2017 13:31

CntrMethod

Caprolactam ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DCarbazole 251 ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Chloro-3-methylphenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Chloroaniline ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Chloronaphthalene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Chlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Chlorophenyl-phenylether ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DChrysene 7320 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Dmp-Cresol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Do-Cresol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDi-n-Butylphthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDi-n-Octylphthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDibenzo(a,h)anthracene 2300 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDibenzofuran 259 ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D3,3-Dichlorobenzidine ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4-Dichlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDiethylphthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4-Dimethylphenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DDimethylphthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4-Dinitrophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4-Dinitrotoluene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,6-Dinitrotoluene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D1,4-Dioxane ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DFluoranthene 5860 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DFluorene 451 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DHexachlorobenzene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DHexachlorobutadiene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DHexachlorocyclopentadiene ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DHexachloroethane ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DIndeno(1,2,3-cd)pyrene 7780 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DIsophorone ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Methylnaphthalene 2170 ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DNaphthalene 4450 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 11 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-02

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776002


Date Collected:

Date Received:

4/3/2017 13:31

CntrMethod

2-Nitroaniline ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D3-Nitroaniline ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Nitroaniline ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DNitrobenzene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Nitrophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D4-Nitrophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DN-Nitrosodiphenylamine ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPentachlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPhenanthrene 4790 ug/kg 56.3 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPhenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPyrene 9940 ug/kg 225 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 113 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4,5-Trichlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2,4,6-Trichlorophenol ND ug/kg 225 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D


2,4,6-Tribromophenol (S) 92.5 % 19 - 132 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270D2,4,6-Tribromophenol (S) 84.9 % 19 - 132 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Fluorobiphenyl (S) 81.2 % 40 - 110 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270D2-Fluorobiphenyl (S) 73.5 % 40 - 110 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D2-Fluorophenol (S) 68.7 % 26 - 116 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270D2-Fluorophenol (S) 65.7 % 26 - 116 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DNitrobenzene-d5 (S) 77.1 % 38 - 112 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270DNitrobenzene-d5 (S) 69.7 % 38 - 112 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPhenol-d5 (S) 71.8 % 35 - 111 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270DPhenol-d5 (S) 69.8 % 35 - 111 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270DTerphenyl-d14 (S) 87.2 % 45 - 126 4/8/17 00:10 CMA 4/13/17 03:57 GEC DSW846 8270DTerphenyl-d14 (S) 86.7 % 45 - 126 4/8/17 00:10 CMA 4/10/17 17:13 GEC DSW846 8270D


METALSAluminum, Total 8320 mg/kg 10.7 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CAntimony, Total 2.2 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CArsenic, Total 87.5 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CBarium, Total 84.8 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010C


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 12 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-02

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776002


Date Collected:

Date Received:

4/3/2017 13:31

CntrMethod

Beryllium, Total ND mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CCadmium, Total ND mg/kg 0.53 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CCalcium, Total 30400 mg/kg 10.7 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CChromium, Total 20.9 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CCobalt, Total 14.1 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CCopper, Total 30.4 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CIron, Total 17300 mg/kg 10.7 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CLead, Total 177 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CMagnesium, Total 18700 mg/kg 10.7 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CManganese, Total 559 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CMercury, Total 0.40 mg/kg 0.052 4/5/17 03:30 AXC 4/5/17 07:45 AXC D2SW846 7471BNickel, Total 20.9 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CPotassium, Total 2270 mg/kg 53.5 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CSelenium, Total ND mg/kg 5.3 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CSilver, Total ND mg/kg 0.53 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CSodium, Total 492 mg/kg 53.5 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CThallium, Total ND mg/kg 3.2 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CVanadium, Total 30.6 mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010CZinc, Total 120 mg/kg 2.1 4/5/17 02:45 LXC 4/6/17 04:07 TSS D1SW846 6010C



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 13 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-03

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776003


Date Collected:

Date Received:

4/3/2017 13:43

CntrMethod

SEMIVOLATILESAcenaphthene 400 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DAcenaphthylene 955 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DAcetophenone 624 ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DAnthracene 1010 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DAtrazine ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzaldehyde 348 ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzo(a)anthracene 2660 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzo(a)pyrene 5300 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzo(b)fluoranthene 7280 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzo(g,h,i)perylene 6810 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBenzo(k)fluoranthene 2240 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DBiphenyl 407 ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Bromophenyl-phenylether ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DButylbenzylphthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DCaprolactam ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DCarbazole 186 ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Chloro-3-methylphenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Chloroaniline ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Chloronaphthalene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Chlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Chlorophenyl-phenylether ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DChrysene 4320 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Dmp-Cresol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Do-Cresol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDi-n-Butylphthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDi-n-Octylphthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDibenzo(a,h)anthracene 1740 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDibenzofuran 247 ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D3,3-Dichlorobenzidine ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,4-Dichlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDiethylphthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,4-Dimethylphenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DDimethylphthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,4-Dinitrophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 14 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-03

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776003


Date Collected:

Date Received:

4/3/2017 13:43

CntrMethod

2,4-Dinitrotoluene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,6-Dinitrotoluene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D1,4-Dioxane ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DFluoranthene 3420 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DFluorene 260 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DHexachlorobenzene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DHexachlorobutadiene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DHexachlorocyclopentadiene ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DHexachloroethane ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DIndeno(1,2,3-cd)pyrene 5740 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DIsophorone ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Methylnaphthalene 3380 ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DNaphthalene 6340 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Nitroaniline ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D3-Nitroaniline ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Nitroaniline ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DNitrobenzene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Nitrophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D4-Nitrophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DN-Nitrosodiphenylamine ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DPentachlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DPhenanthrene 3180 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DPhenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DPyrene 5590 ug/kg 52.7 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 105 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,4,5-Trichlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2,4,6-Trichlorophenol ND ug/kg 211 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D


2,4,6-Tribromophenol (S) 78.1 % 19 - 132 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Fluorobiphenyl (S) 70.6 % 40 - 110 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D2-Fluorophenol (S) 56 % 26 - 116 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DNitrobenzene-d5 (S) 67.4 % 38 - 112 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DPhenol-d5 (S) 63.9 % 35 - 111 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270DTerphenyl-d14 (S) 82.3 % 45 - 126 4/8/17 00:10 CMA 4/10/17 17:38 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 15 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-03

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776003


Date Collected:

Date Received:

4/3/2017 13:43

CntrMethod


METALSAluminum, Total 11500 mg/kg 197 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CAntimony, Total ND mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CArsenic, Total 57.0 mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CBarium, Total 315 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CBeryllium, Total 31.7 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CCadmium, Total ND mg/kg 9.9 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CCalcium, Total 35100 mg/kg 197 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CChromium, Total 35.5 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CCobalt, Total 57.6 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CCopper, Total 3580 mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CIron, Total 74400 mg/kg 197 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CLead, Total 1830 mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CMagnesium, Total 15900 mg/kg 197 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CManganese, Total 1350 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CMercury, Total 0.76 mg/kg 0.053 4/7/17 04:00 AXC 4/10/17 02:19 AXC A2SW846 7471BNickel, Total 421 mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CPotassium, Total ND mg/kg 986 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CSelenium, Total ND mg/kg 98.6 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CSilver, Total ND mg/kg 9.9 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CSodium, Total 2180 mg/kg 986 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CThallium, Total ND mg/kg 59.1 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CVanadium, Total 32.9 mg/kg 19.7 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010CZinc, Total 13000 mg/kg 39.4 4/5/17 02:45 LXC 4/6/17 04:52 TSS A1SW846 6010C



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 16 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-04

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776004


Date Collected:

Date Received:

4/3/2017 13:46

CntrMethod

VOLATILE ORGANICSAcetone ND ug/kg 10.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BBenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BBromochloromethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BBromodichloromethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BBromoform ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BBromomethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B2-Butanone ND ug/kg 10.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BCarbon Disulfide ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BCarbon Tetrachloride ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BChlorobenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BChlorodibromomethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BChloroethane ND ug/kg 5.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BChloroform ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BChloromethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BCyclohexane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2-Dibromo-3-chloropropane

ND ug/kg 5.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B

1,2-Dibromoethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2-Dichlorobenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,3-Dichlorobenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,4-Dichlorobenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BDichlorodifluoromethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,1-Dichloroethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2-Dichloroethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,1-Dichloroethene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Bcis-1,2-Dichloroethene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Btrans-1,2-Dichloroethene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2-Dichloropropane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Bcis-1,3-Dichloropropene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Btrans-1,3-Dichloropropene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,4-Dioxane ND ug/kg 75.2 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BEthylbenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BFreon 113 ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B2-Hexanone ND ug/kg 10.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BIsopropylbenzene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BMethyl acetate ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BMethyl cyclohexane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 17 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-04

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776004


Date Collected:

Date Received:

4/3/2017 13:46

CntrMethod

Methyl t-Butyl Ether ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B4-Methyl-2-Pentanone(MIBK)

ND ug/kg 10.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B

Methylene Chloride 5.4 ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BStyrene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,1,2,2-Tetrachloroethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BTetrachloroethene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BToluene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BTotal Xylenes ND ug/kg 6.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2,3-Trichlorobenzene ND ug/kg 5.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,2,4-Trichlorobenzene ND ug/kg 5.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,1,1-Trichloroethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B1,1,2-Trichloroethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BTrichloroethene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BTrichlorofluoromethane ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BVinyl Chloride ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Bo-Xylene ND ug/kg 2.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260Bmp-Xylene ND ug/kg 4.0 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B


1,2-Dichloroethane-d4 (S) 88.6 % 56 - 124 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B4-Bromofluorobenzene (S) 105 % 51 - 128 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BDibromofluoromethane (S) 96.7 % 62 - 123 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260BToluene-d8 (S) 97.8 % 59 - 131 4/4/17 23:54 SYB 4/6/17 03:19 SYB CSW846 8260B

SEMIVOLATILESAcenaphthene 541 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DAcenaphthylene 1680 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DAcetophenone 649 ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DAnthracene 1900 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DAtrazine ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DBenzaldehyde 725 ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DBenzo(a)anthracene 5530 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DBenzo(a)pyrene 10400 ug/kg 229 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DBenzo(b)fluoranthene 12600 ug/kg 229 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DBenzo(g,h,i)perylene 14300 ug/kg 229 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DBenzo(k)fluoranthene 3680 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DBiphenyl 680 ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D4-Bromophenyl-phenylether ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DButylbenzylphthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 18 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-04

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776004


Date Collected:

Date Received:

4/3/2017 13:46

CntrMethod

Caprolactam ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DCarbazole 272 ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D4-Chloro-3-methylphenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D4-Chloroaniline ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Chloronaphthalene ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Chlorophenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D4-Chlorophenyl-phenylether ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DChrysene 7820 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Dmp-Cresol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Do-Cresol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDi-n-Butylphthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDi-n-Octylphthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDibenzo(a,h)anthracene 2480 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDibenzofuran 396 ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D3,3-Dichlorobenzidine ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2,4-Dichlorophenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDiethylphthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2,4-Dimethylphenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DDimethylphthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2,4-Dinitrophenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2,4-Dinitrotoluene ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2,6-Dinitrotoluene ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D1,4-Dioxane ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DFluoranthene 7530 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DFluorene 417 ug/kg 57.3 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DHexachlorobenzene ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DHexachlorobutadiene ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DHexachlorocyclopentadiene ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DHexachloroethane ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DIndeno(1,2,3-cd)pyrene 11600 ug/kg 229 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DIsophorone ND ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 229 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Methylnaphthalene 5900 ug/kg 115 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DNaphthalene 13300 ug/kg 229 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 19 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-04

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776004


Date Collected:

Date Received:

4/3/2017 13:46

CntrMethod



2,4,6-Tribromophenol (S) 93.7 % 19 - 132 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270D2,4,6-Tribromophenol (S) 81.4 % 19 - 132 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Fluorobiphenyl (S) 84.4 % 40 - 110 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270D2-Fluorobiphenyl (S) 74.9 % 40 - 110 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270D2-Fluorophenol (S) 69.1 % 26 - 116 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270D2-Fluorophenol (S) 60.3 % 26 - 116 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DNitrobenzene-d5 (S) 77.3 % 38 - 112 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DNitrobenzene-d5 (S) 82.9 % 38 - 112 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DPhenol-d5 (S) 69 % 35 - 111 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DPhenol-d5 (S) 76.6 % 35 - 111 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270DTerphenyl-d14 (S) 84.6 % 45 - 126 4/8/17 00:10 CMA 4/10/17 18:03 GEC DSW846 8270DTerphenyl-d14 (S) 91.4 % 45 - 126 4/8/17 00:10 CMA 4/13/17 04:21 GEC DSW846 8270D


METALSAluminum, Total 6130 mg/kg 11.7 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CAntimony, Total ND mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CArsenic, Total 67.8 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CBarium, Total 146 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010C


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 20 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-04

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776004


Date Collected:

Date Received:

4/3/2017 13:46

CntrMethod

Beryllium, Total 2.3 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CCadmium, Total ND mg/kg 0.58 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CCalcium, Total 25000 mg/kg 11.7 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CChromium, Total 13.9 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CCobalt, Total 12.0 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CCopper, Total 204 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CIron, Total 22200 mg/kg 11.7 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CLead, Total 282 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CMagnesium, Total 9470 mg/kg 11.7 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CManganese, Total 813 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CMercury, Total 0.65 mg/kg 0.057 4/7/17 04:00 AXC 4/10/17 02:22 AXC D2SW846 7471BNickel, Total 52.1 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CPotassium, Total 747 mg/kg 58.4 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CSelenium, Total ND mg/kg 5.8 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CSilver, Total ND mg/kg 0.58 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CSodium, Total 301 mg/kg 58.4 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CThallium, Total ND mg/kg 3.5 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CVanadium, Total 32.4 mg/kg 1.2 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010CZinc, Total 963 mg/kg 2.3 4/5/17 02:45 LXC 4/6/17 04:14 TSS D1SW846 6010C



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 21 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-05

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776005


Date Collected:

Date Received:

4/3/2017 14:10

CntrMethod

SEMIVOLATILESAcenaphthene 71.4 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DAcenaphthylene 148 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DAcetophenone ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DAnthracene 161 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DAtrazine ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzaldehyde ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzo(a)anthracene 735 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzo(a)pyrene 1240 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzo(b)fluoranthene 1520 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzo(g,h,i)perylene 1200 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBenzo(k)fluoranthene 509 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DBiphenyl ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Bromophenyl-phenylether ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DButylbenzylphthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DCaprolactam ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DCarbazole ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Chloro-3-methylphenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Chloroaniline ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Chloronaphthalene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Chlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Chlorophenyl-phenylether ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DChrysene 1130 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Dmp-Cresol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Do-Cresol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDi-n-Butylphthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDi-n-Octylphthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDibenzo(a,h)anthracene 343 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDibenzofuran ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D3,3-Dichlorobenzidine ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,4-Dichlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDiethylphthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,4-Dimethylphenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DDimethylphthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,4-Dinitrophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 22 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-05

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776005


Date Collected:

Date Received:

4/3/2017 14:10

CntrMethod

2,4-Dinitrotoluene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,6-Dinitrotoluene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D1,4-Dioxane ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DFluoranthene 945 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DFluorene ND ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DHexachlorobenzene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DHexachlorobutadiene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DHexachlorocyclopentadiene ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DHexachloroethane ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DIndeno(1,2,3-cd)pyrene 1050 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DIsophorone ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Methylnaphthalene 142 ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DNaphthalene 297 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Nitroaniline ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D3-Nitroaniline ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Nitroaniline ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DNitrobenzene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Nitrophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D4-Nitrophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DN-Nitrosodiphenylamine ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DPentachlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DPhenanthrene 758 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DPhenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DPyrene 1390 ug/kg 53.0 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 106 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,4,5-Trichlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2,4,6-Trichlorophenol ND ug/kg 212 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D


2,4,6-Tribromophenol (S) 105 % 19 - 132 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Fluorobiphenyl (S) 79.7 % 40 - 110 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D2-Fluorophenol (S) 71.9 % 26 - 116 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DNitrobenzene-d5 (S) 76.9 % 38 - 112 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DPhenol-d5 (S) 73.9 % 35 - 111 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270DTerphenyl-d14 (S) 89.6 % 45 - 126 4/8/17 00:10 CMA 4/10/17 18:28 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 23 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-05

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776005


Date Collected:

Date Received:

4/3/2017 14:10

CntrMethod


METALSAluminum, Total 4900 mg/kg 52.0 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CAntimony, Total ND mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CArsenic, Total 15.8 mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CBarium, Total 38.8 mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CBeryllium, Total ND mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CCadmium, Total ND mg/kg 2.6 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CCalcium, Total 74700 mg/kg 52.0 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CChromium, Total 20.4 mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CCobalt, Total ND mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CCopper, Total 32.5 mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CIron, Total 12100 mg/kg 52.0 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CLead, Total 97.2 mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CMagnesium, Total 42900 mg/kg 52.0 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CManganese, Total 152 mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CMercury, Total 0.19 mg/kg 0.048 4/7/17 04:00 AXC 4/10/17 02:23 AXC A2SW846 7471BNickel, Total 16.0 mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CPotassium, Total 520 mg/kg 260 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CSelenium, Total ND mg/kg 26.0 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CSilver, Total ND mg/kg 2.6 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CSodium, Total ND mg/kg 260 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CThallium, Total ND mg/kg 15.6 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CVanadium, Total 19.7 mg/kg 5.2 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010CZinc, Total 112 mg/kg 10.4 4/5/17 02:45 LXC 4/6/17 04:55 TSS A1SW846 6010C



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 24 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-06

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776006


Date Collected:

Date Received:

4/3/2017 14:17

CntrMethod

SEMIVOLATILESAcenaphthene 413 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DAcenaphthylene 1990 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DAcetophenone 387 ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DAnthracene 1080 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DAtrazine ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzaldehyde ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzo(a)anthracene 3530 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzo(a)pyrene 6110 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzo(b)fluoranthene 7530 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzo(g,h,i)perylene 7100 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBenzo(k)fluoranthene 2230 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DBiphenyl ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Bromophenyl-phenylether ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DButylbenzylphthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DCaprolactam ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DCarbazole 130 ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Chloro-3-methylphenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Chloroaniline ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Chloronaphthalene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Chlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Chlorophenyl-phenylether ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DChrysene 5330 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Dmp-Cresol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Do-Cresol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDi-n-Butylphthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDi-n-Octylphthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDibenzo(a,h)anthracene 1860 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDibenzofuran 121 ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D3,3-Dichlorobenzidine ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,4-Dichlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDiethylphthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,4-Dimethylphenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DDimethylphthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,4-Dinitrophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 25 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-06

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776006


Date Collected:

Date Received:

4/3/2017 14:17

CntrMethod

2,4-Dinitrotoluene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,6-Dinitrotoluene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D1,4-Dioxane ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DFluoranthene 4150 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DFluorene 396 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DHexachlorobenzene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DHexachlorobutadiene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DHexachlorocyclopentadiene ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DHexachloroethane ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DIndeno(1,2,3-cd)pyrene 6040 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DIsophorone ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Methylnaphthalene 645 ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DNaphthalene 1380 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Nitroaniline ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D3-Nitroaniline ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Nitroaniline ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DNitrobenzene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Nitrophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D4-Nitrophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DN-Nitrosodiphenylamine ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DPentachlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DPhenanthrene 4090 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DPhenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DPyrene 7170 ug/kg 60.2 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 120 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,4,5-Trichlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2,4,6-Trichlorophenol ND ug/kg 241 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D


2,4,6-Tribromophenol (S) 98.7 % 19 - 132 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Fluorobiphenyl (S) 75.9 % 40 - 110 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D2-Fluorophenol (S) 68 % 26 - 116 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DNitrobenzene-d5 (S) 80.4 % 38 - 112 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DPhenol-d5 (S) 74.2 % 35 - 111 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270DTerphenyl-d14 (S) 87.5 % 45 - 126 4/8/17 00:10 CMA 4/10/17 18:53 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 26 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-06

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776006


Date Collected:

Date Received:

4/3/2017 14:17

CntrMethod


METALSAluminum, Total 4070 mg/kg 21.9 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CAntimony, Total ND mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CArsenic, Total 18.4 mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CBarium, Total 59.2 mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CBeryllium, Total ND mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CCadmium, Total ND mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CCalcium, Total 60400 mg/kg 21.9 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CChromium, Total 13.0 mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CCobalt, Total 10.8 mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CCopper, Total 254 mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CIron, Total 15500 mg/kg 21.9 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CLead, Total 293 mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CMagnesium, Total 33500 mg/kg 21.9 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CManganese, Total 231 mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CMercury, Total 0.34 mg/kg 0.053 4/12/17 02:00 AXC 4/12/17 05:16 AXC A2SW846 7471BNickel, Total 54.1 mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CPotassium, Total 416 mg/kg 109 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CSelenium, Total ND mg/kg 10.9 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CSilver, Total ND mg/kg 1.1 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CSodium, Total 169 mg/kg 109 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CThallium, Total ND mg/kg 6.6 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CVanadium, Total 18.1 mg/kg 2.2 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010CZinc, Total 1510 mg/kg 4.4 4/5/17 02:45 LXC 4/6/17 05:05 TSS A1SW846 6010C



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 27 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-07

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776007


Date Collected:

Date Received:

4/3/2017 14:39

CntrMethod

SEMIVOLATILESAcenaphthene 270 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DAcenaphthylene 433 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DAcetophenone ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DAnthracene 1070 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DAtrazine ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DBenzaldehyde ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DBenzo(a)anthracene 5190 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DBenzo(a)pyrene 13900 ug/kg 271 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DBenzo(b)fluoranthene 15400 ug/kg 271 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DBenzo(g,h,i)perylene 14300 ug/kg 271 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DBenzo(k)fluoranthene 4830 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DBiphenyl 138 ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Bromophenyl-phenylether ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DButylbenzylphthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DCaprolactam ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DCarbazole 325 ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Chloro-3-methylphenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Chloroaniline ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Chloronaphthalene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Chlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Chlorophenyl-phenylether ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DChrysene 10200 ug/kg 271 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270Dmp-Cresol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270Do-Cresol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDi-n-Butylphthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDi-n-Octylphthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDibenzo(a,h)anthracene 4330 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDibenzofuran 143 ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D3,3-Dichlorobenzidine ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4-Dichlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDiethylphthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4-Dimethylphenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DDimethylphthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4-Dinitrophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 28 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-07

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776007


Date Collected:

Date Received:

4/3/2017 14:39

CntrMethod

2,4-Dinitrotoluene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,6-Dinitrotoluene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D1,4-Dioxane ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DFluoranthene 3590 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DFluorene 249 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DHexachlorobenzene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DHexachlorobutadiene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DHexachlorocyclopentadiene ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DHexachloroethane ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DIndeno(1,2,3-cd)pyrene 11100 ug/kg 271 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DIsophorone ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Methylnaphthalene 716 ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DNaphthalene 1650 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Nitroaniline ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D3-Nitroaniline ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Nitroaniline ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DNitrobenzene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Nitrophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D4-Nitrophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DN-Nitroso-di-n-propylamine ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DN-Nitrosodiphenylamine ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DPentachlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DPhenanthrene 2140 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DPhenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DPyrene 7440 ug/kg 54.1 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D1,2,4,5-Tetrachlorobenzene ND ug/kg 108 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,3,4,6-Tetrachlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4,5-Trichlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4,6-Trichlorophenol ND ug/kg 216 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D


2,4,6-Tribromophenol (S) 89.3 % 19 - 132 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2,4,6-Tribromophenol (S) 90.7 % 19 - 132 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270D2-Fluorobiphenyl (S) 78.6 % 40 - 110 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Fluorobiphenyl (S) 77.6 % 40 - 110 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270D2-Fluorophenol (S) 69.2 % 26 - 116 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270D2-Fluorophenol (S) 69.9 % 26 - 116 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 29 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-07

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776007


Date Collected:

Date Received:

4/3/2017 14:39

CntrMethod

Nitrobenzene-d5 (S) 74.4 % 38 - 112 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DNitrobenzene-d5 (S) 76 % 38 - 112 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DPhenol-d5 (S) 75.5 % 35 - 111 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DPhenol-d5 (S) 73.8 % 35 - 111 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270DTerphenyl-d14 (S) 90.6 % 45 - 126 4/8/17 00:10 CMA 4/10/17 19:18 GEC ASW846 8270DTerphenyl-d14 (S) 90.4 % 45 - 126 4/8/17 00:10 CMA 4/13/17 04:46 GEC ASW846 8270D


METALSAluminum, Total 8400 mg/kg 216 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CAntimony, Total 71.6 mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CArsenic, Total ND mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CBarium, Total 210 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CBeryllium, Total 28.1 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CCadmium, Total ND mg/kg 10.8 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CCalcium, Total 49800 mg/kg 216 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CChromium, Total 29.7 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CCobalt, Total 31.2 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CCopper, Total 1140 mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CIron, Total 35900 mg/kg 216 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CLead, Total 616 mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CMagnesium, Total 21400 mg/kg 216 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CManganese, Total 739 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CMercury, Total 0.19 mg/kg 0.054 4/12/17 02:00 AXC 4/12/17 05:19 AXC A2SW846 7471BNickel, Total 188 mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CPotassium, Total ND mg/kg 1080 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CSelenium, Total ND mg/kg 108 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CSilver, Total ND mg/kg 10.8 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CSodium, Total ND mg/kg 1080 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CThallium, Total ND mg/kg 64.9 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CVanadium, Total 31.6 mg/kg 21.6 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010CZinc, Total 5300 mg/kg 43.3 4/5/17 02:45 LXC 4/6/17 05:08 TSS A1SW846 6010C


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 30 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-07

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776007


Date Collected:

Date Received:

4/3/2017 14:39

CntrMethod



DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 31 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-08

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776008


Date Collected:

Date Received:

4/3/2017 14:44

CntrMethod

VOLATILE ORGANICSAcetone ND ug/kg 9.7 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BBenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BBromochloromethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BBromodichloromethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BBromoform ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BBromomethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B2-Butanone ND ug/kg 9.7 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BCarbon Disulfide ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BCarbon Tetrachloride ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BChlorobenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BChlorodibromomethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BChloroethane ND ug/kg 4.8 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BChloroform ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BChloromethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BCyclohexane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2-Dibromo-3-chloropropane


1,2-Dibromoethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2-Dichlorobenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,3-Dichlorobenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,4-Dichlorobenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BDichlorodifluoromethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,1-Dichloroethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2-Dichloroethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,1-Dichloroethene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Bcis-1,2-Dichloroethene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Btrans-1,2-Dichloroethene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2-Dichloropropane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Bcis-1,3-Dichloropropene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Btrans-1,3-Dichloropropene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,4-Dioxane ND ug/kg 72.5 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BEthylbenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BFreon 113 ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B2-Hexanone ND ug/kg 9.7 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BIsopropylbenzene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BMethyl acetate ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BMethyl cyclohexane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 32 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-08

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776008


Date Collected:

Date Received:

4/3/2017 14:44

CntrMethod

Methyl t-Butyl Ether ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B4-Methyl-2-Pentanone(MIBK)


Methylene Chloride ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BStyrene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,1,2,2-Tetrachloroethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BTetrachloroethene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BToluene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BTotal Xylenes ND ug/kg 5.8 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2,3-Trichlorobenzene ND ug/kg 4.8 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,2,4-Trichlorobenzene ND ug/kg 4.8 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,1,1-Trichloroethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B1,1,2-Trichloroethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BTrichloroethene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BTrichlorofluoromethane ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BVinyl Chloride ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Bo-Xylene ND ug/kg 1.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260Bmp-Xylene ND ug/kg 3.9 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B


1,2-Dichloroethane-d4 (S) 84.5 % 56 - 124 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B4-Bromofluorobenzene (S) 105 % 51 - 128 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BDibromofluoromethane (S) 95.2 % 62 - 123 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260BToluene-d8 (S) 99 % 59 - 131 4/4/17 23:55 SYB 4/5/17 08:10 SYB BSW846 8260B

SEMIVOLATILESAcenaphthene 771 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DAcenaphthylene 251 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DAcetophenone ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DAnthracene 1610 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DAtrazine ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DBenzaldehyde ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DBenzo(a)anthracene 5350 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DBenzo(a)pyrene 11800 ug/kg 219 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DBenzo(b)fluoranthene 12500 ug/kg 219 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DBenzo(g,h,i)perylene 12900 ug/kg 219 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DBenzo(k)fluoranthene 3740 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DBiphenyl ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D4-Bromophenyl-phenylether ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DButylbenzylphthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 33 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-08

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776008


Date Collected:

Date Received:

4/3/2017 14:44

CntrMethod

Caprolactam ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DCarbazole 185 ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D4-Chloro-3-methylphenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D4-Chloroaniline ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Dbis(2-Chloroethoxy)methane ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Dbis(2-Chloroethyl)ether ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Dbis(2-Chloroisopropyl)ether ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Chloronaphthalene ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Chlorophenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D4-Chlorophenyl-phenylether ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DChrysene 8360 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Dmp-Cresol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Do-Cresol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDi-n-Butylphthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDi-n-Octylphthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDibenzo(a,h)anthracene 3060 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDibenzofuran ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D3,3-Dichlorobenzidine ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2,4-Dichlorophenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDiethylphthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2,4-Dimethylphenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DDimethylphthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2,4-Dinitrophenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2,4-Dinitrotoluene ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2,6-Dinitrotoluene ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D1,4-Dioxane ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270Dbis(2-Ethylhexyl)phthalate ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DFluoranthene 6690 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DFluorene 500 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DHexachlorobenzene ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DHexachlorobutadiene ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DHexachlorocyclopentadiene ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DHexachloroethane ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DIndeno(1,2,3-cd)pyrene 10500 ug/kg 219 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DIsophorone ND ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Methyl-4,6-dinitrophenol ND ug/kg 219 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Methylnaphthalene 473 ug/kg 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DNaphthalene 717 ug/kg 54.8 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 34 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-08

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776008


Date Collected:

Date Received:

4/3/2017 14:44

CntrMethod



2,4,6-Tribromophenol (S) 95.7 % 19 - 132 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270D2,4,6-Tribromophenol (S) 88.2 % 19 - 132 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Fluorobiphenyl (S) 81.1 % 40 - 110 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270D2-Fluorobiphenyl (S) 73.8 % 40 - 110 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D2-Fluorophenol (S) 72.5 % 26 - 116 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270D2-Fluorophenol (S) 67.4 % 26 - 116 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DNitrobenzene-d5 (S) 80.7 % 38 - 112 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DNitrobenzene-d5 (S) 75.3 % 38 - 112 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DPhenol-d5 (S) 74.1 % 35 - 111 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270DPhenol-d5 (S) 75.2 % 35 - 111 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DTerphenyl-d14 (S) 90 % 45 - 126 4/8/17 00:10 CMA 4/13/17 05:11 GEC DSW846 8270DTerphenyl-d14 (S) 86 % 45 - 126 4/8/17 00:10 CMA 4/10/17 19:43 GEC DSW846 8270D


METALSAluminum, Total 3180 mg/kg 9.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CAntimony, Total ND mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CArsenic, Total 12.7 mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CBarium, Total 46.1 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010C


DL ID - 47901, QC - 0

Report ID: 2219776 - 4/13/2017 Page 35 of 36


ANALYTICAL RESULTS

4/4/2017 20:0004032017-08

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2219776008


Date Collected:

Date Received:

4/3/2017 14:44

CntrMethod

Beryllium, Total 1.7 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CCadmium, Total 1.1 mg/kg 0.49 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CCalcium, Total 5390 mg/kg 9.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CChromium, Total 19.3 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CCobalt, Total 5.6 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CCopper, Total 155 mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CIron, Total 13400 mg/kg 9.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CLead, Total 271 mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CMagnesium, Total 3110 mg/kg 9.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CManganese, Total 113 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CMercury, Total 0.16 mg/kg 0.051 4/12/17 02:00 AXC 4/12/17 05:20 AXC D2SW846 7471BNickel, Total 32.9 mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CPotassium, Total 331 mg/kg 48.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CSelenium, Total ND mg/kg 4.9 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CSilver, Total ND mg/kg 0.49 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CSodium, Total 109 mg/kg 48.8 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CThallium, Total ND mg/kg 2.9 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CVanadium, Total 12.7 mg/kg 0.98 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010CZinc, Total 633 mg/kg 2.0 4/5/17 02:45 LXC 4/6/17 04:27 TSS D1SW846 6010C



DL ID - 47901, QC - 0

Page 36 of 36

Thursday, April 13, 2017 2:59:32 PM

Documents

Philadelphia, PA 19145 Certificate of Analysis...Grooms , Mr. Larry Gould , Ms. Jessica Mason , Mr. Dan McKenna , Mr. Chin So This page is included as part of the Analytical Report