Poly(vinyl alcohol) / Cellulose Barrier FilmsShweta Paralikar John SimonsenWood Science & EngineeringOregon State UniversityJohn LombardiVentana Research Corp.

OUTLINE

Introduction

Materials

Results and Discussion

Conclusions

Acknowledgements

Introduction Barrier Films?

Designed to reduce/retard gas migration

Widely used in the food and biomedical industries

Another application is as a barrier to toxic chemicals

Chemical Vapor Barrier To prevent the diffusion of toxic chemical vapors, while allowing water vapor to pass through

Hydrophilic barriers to protect from hydrophobic toxins

Should be tough and flexible

Useful in protective clothing

Materials Poly(vinyl alcohol) = PVOH

Nontoxic, good barrier for oxygen, aroma, oil and solvents Prepared by partial or complete hydrolysis of poly(vinyl acetate)

Structure:

PVOH Water Stability

PVOH films have poor resistance to water

Crosslinking agent reduces water sorption and the crosslinks also act as a barrier to diffusion

Poly(acrylic acid)-PAA

Poly(acrylic acid) PAA:

Crosslinking reactionSource: Sanli, O., et al. Journal of applied polymer science, 91( 2003) Heat treatment forms ester linkages

Cellulose Nanocrystals-(CNXLs)CNXLs were prepared by acid hydrolysis of cellulose obtained from cottonCrystalline regionsAmorphous regionAcid hydrolysisIndividual nanocrystalsIndividual cellulose polymerNative cellulose

Proposed structurePVOHPAA

ObjectivesPrepare chemical barrier films with PVOH/ PAA/ CNXL system

To understand the chemistry and physics of this system

Select optimum time and temperature for heat treatment

Find combination which allows moisture to pass through but restricts diffusion of toxic chemical vapors

Surface modify CNXLs to improve interaction with matrix

MethodsFilm Preparation

Testing methodsWater solubility - Optimize heat treatmentFourier Transform Infrared Spectroscopy - Bond analysisPolarized Optical Microscopy - DispersionWater Vapor Transmission Rate (WVTR)Universal Testing Machine - Mechanical propertiesDifferential Thermogravimetric Analysis - Thermal degradationChemical Vapor Transmission Rate (CVTR)

Preparation of the Blends5 wt % solution of PVOH and PAA1 wt % solution of dispersed CNXLs in DI waterRemaining composition of the film consists of PVOH

Film Preparation

Compositions were mixed, sonicated and then air dried for 40 hours

The thickness of the film was controlled by the concentration (%solids) of the dispersion before drying

Heat treatment optimization

Evaluate via water solubility test At 125 C/1 hr films were completely soluble in water after a dayAt 185 C/1hr color of the films changed to brownAt 150 C and 170 C/45 min films were clear and had good water resistance

% Solubility =Lower = BetterTotal % Solubility after 72 hours of soaking time

Fourier Transform Infrared SpectroscopyPVOHPAAAbsorbanceRed: Heat treated film Blue: Non heat treated film

Absorbance

1500 cm-1

2500 cm-1

3500 cm-1

FTIR of 10% CNXL/10% PAA/80% PVOHWavenumbers (cm-1)AbsorbanceRed: Heat treated film Blue: Non heat treated film

Polarized Optical MicroscopyDispersion of CNXLsa) 5% CNXL/ 10%PAA b) 10% CNXL/ 10% PAA c) 15% CNXL/ 10% PAA

Water Permeability Water Vapor Transmission Rate

Test were conducted at 30C and 30% relative humidity

D

WVTR

Chart1

33.18453570190.65347319570.6534731957

21.38169381750.52693328680.5269332868

12.69711707420.79209441860.7920944186

9.80029155870.15813767560.1581376756

11.82078008710.36795373990.3679537399

18.17283291290.77521295570.7752129557

15.12102237550.3503925610.350392561

10.39149975320.49500681740.4950068174

12.97466301480.71238951710.7123895171

Composition

Flux g/m2 day

Sheet1

gm/mmhr

170

FilmAreawt loss/hrgm/mt^2*hrgm/mt^2*hrgm/mt^2*hrgm/mt^2*daystddev

100 PVOH100 PVOH875.910.1090.029066666733.184535701934.1432.89796.4288568460.6534731957100PVOH

10PAA/0CNXL0CNXL/10PAA760.77540.0610.016266666721.381693817522.01620.97513.16065161940.526933286810%cncc/90pvoh

0PAA/10CNXL10CNXL/0PAA588.060.0280.007466666712.697117074211.89211.113304.73080978130.792094418615%cncc/85pvoh

10PAA/10CNXL10CNXL/10PAA799.97620.02940.007849.80029155879.5919.901235.20699740820.158137675620%cncc/80pvoh

10PAA/20CNXL20CNXL/10PAA789.570.0350.009333333311.820780087111.28611.9912283.69872208920.3679537399

20PAA/0CNXL0CNXL/20PAA719.0220.0490.013066666718.172832912918.37219.604436.14798990850.7752129557

0PAA/20CNXL20CNXL/0PAA864.13910.0490.013066666715.121022375514.94315.619362.90453701260.350392561

20PAA/10CNXL10CNXL/20PAA769.860.030.00810.39149975329.89210.882249.39599407680.4950068174

20PAA/20CNXL20CNXL/20PAA842.6680.0410.010933333312.974663014811.56112.114311.39191235460.7123895171

15CNXL/0PAA835.910.040.010666666712.760544396712.2112.09306.25306552140.3575679238

15CNXL/10PAA840.10.0320.008533333310.1575209310.219.93243.78050232120.1488398616

gm/mt^2*hrstddev

100PVOH84033.1834.1432.890.6542425646

10%C.CNXL/0%PAA84012.1112.0111.590.2759226945

15%C.CNXL/0%PAA84011.7811.9411.620.16

20%C.CNXL/0%PAA84014.2314.9814.050.4932544982

10%C.CNXL/10%PAA8409.359.599.820.2350177298

15%C.CNXL/10%PAA8409.139.319.610.2424871131

20%C.CNXL/10%PAA84010.2310.3110.590.1890326251

100PVOH10%CNXL/0%PAA15%CNXL/0%PAA20%CNXL/0%PAA10%CNXL/10%PAA15%CNXL/10%PAA20%CNXL/10%PAA

C.CNXL33.1812.1111.7814.239.359.1310.23

0.650.790.3570.350.1580.1480.367

CNXL33.1812.6912.7615.129.810.1511.82

0.650.270.160.490.2350.2420.189

0,20268.666250.0930.00350943413.0624295469

0,10268.666250.1380.005207547219.3829599729

10,20268.666250.05730.00216226428.0481420757

20,0268.666250.08820.003328301912.3882396348

20,20268.666250.08080.003049056611.3488635203

10,0268.666250.08950.003377358512.570832736

Sheet1

0.650.650.650.65

0.270.270.790.79

0.160.160.3570.357

0.490.490.350.35

0.2350.2350.1580.158

0.2420.2420.1480.148

0.1890.1890.3670.367

C.CNXL

CNXL

Composition

Flux

Sheet2

116.960.5200.60.0250.025

116.96116.460.8530.50.6688524590.0278688525

116.96115.610.58210.66285714290.0276190476

116.96115.031.27

116.96113.76113.76

Sheet3

Mechanical tensile testing

27 micron thick films were cut into a dogbone shape

Strain rate: 1 mm/min

Span: 20 mm Stress, MPa

Chart30

0.3317734

1.1124172

3.1616068

5.503538

7.3380506

8.0015978

7.8649852

7.4551474

7.435631

7.5332118

7.5136954

7.7088566

7.7674044

7.5136954

7.8259532

7.8845014

7.825953

8.0406302

8.2943392

8.2162748

8.3528874

8.6261128

8.7041772

8.5675646

8.9188542

9.094499

9.0944994

9.270144

9.309176

9.484821

9.504337

9.484821

9.543369

9.8556266

10.0898194

10.0703036

9.9922394

10.245948

10.5777224

10.753367

10.8899794

10.8899796

11.2022368

11.1241722

11.5144948

11.3459464545

11.3725593636

11.425785

11.5233653636

11.2927209091

11.4523979091

11.2838496364

11.1064307273

11.0532049091

10.7338505455

10.4144961818

10.3257871818

10.3790127273

10.2282068182

10.0774003636

9.917723

9.8378844545

9.5894980909

9.5628854545

9.4919177273

9.3854660909

9.1370797273

9.0661120909

8.9241767273

8.8265962727

8.6314354545

8.6048224545

8.6225643636

8.2233715455

8.3919196364

7.9040173636

7.620147

7.2298251818

7.0878897273

6.8040192727

6.71531

6.4580525455

6.208557

Strain, mm/mm

Stress vs Strain Curve

sintech data1names

AAAnumberNCCPAA

11520

c21520

c31510

c41520

c51010

c61020

c7520

c8020

c9010

10020

11520

AAA#11

11520

2010

3510

41010

51510

62010

700

850

9100

10150

11100

12200

sintech data1format

EXTENSION (mm)"LOAD (N)

-0.0188240.390266

-0.0188240.682966

-0.0162840

-0.0086640.487833

-0.0035840.682966

0.0065761.073232

0.0116561.463498

0.0218161.658631

0.0268962.048897

0.0370561.951331

0.0446762.439164

0.0522963.512396

0.0624564.292928

0.0700764.097795

0.0802365.561293

0.0878565.658859

0.0954766.049126

0.1005566.829658

0.1107166.536958

0.1157967.122358

0.1259567.219924

0.1310368.098023

0.1411967.90289

0.1488168.585856

0.1589768.390723

0.1665969.171255

0.1767569.268822

0.1843769.756655

0.1919969.268822

0.2021569.659088

0.2097769.561521

0.2173969.659088

0.2224769.659088

0.2300969.854221

0.24025610.14692

0.24787610.049354

0.2529569.756655

0.26311610.14692

0.2707369.756655

0.2808969.659088

0.28851610.244487

0.29613610.244487

0.30375610.14692

0.3139169.659088

0.3215369.756655

0.3291569.756655

0.33931610.244487

0.34693610.14692

0.35709610.537187

0.3647169.659088

0.37233610.049354

0.3774169.659088

0.3875769.756655

0.3951969.756655

0.40535610.14692

0.4129769.659088

0.4231369.951788

0.43075610.537187

0.4383769.463955

0.44853610.342054

0.45361610.14692

0.4637769.854221

0.47139610.342054

0.48155610.14692

0.4891769.854221

0.49933610.537187

0.50441610.049354

0.5145769.854221

0.5221969.756655

0.52981610.14692

0.53743610.14692

0.54759610.14692

0.55521610.537187

0.56283610.439621

0.57045610.439621

0.58061610.439621

0.58823610.439621

0.59839610.342054

0.6060169.854221

0.61363610.244487

0.62379610.14692

0.6288769.951788

0.63903610.634753

0.64665610.634753

0.6542769.951788

0.66189610.14692

0.67205610.634753

0.6771369.951788

0.68729610.049354

0.69491610.049354

0.70507610.342054

0.71269610.829886

0.72031610.537187

0.73047610.634753

0.73809610.439621

0.7457169.951788

0.75333610.342054

0.76095610.049354

0.76857610.73232

0.77873610.927454

0.78635610.537187

0.79397610.244487

0.8015969.951788

0.81175610.244487

0.81937610.537187

0.82699610.342054

0.83715610.537187

0.84477610.439621

0.85493610.927454

0.86255611.02502

0.87017610.244487

0.87779610.634753

0.88541610.439621

0.89303610.927454

0.90319610.537187

0.91081610.244487

0.92097610.439621

0.92859610.439621

0.93621610.14692

0.94383610.927454

0.95399610.927454

0.96161610.829886

0.96923610.73232

0.97685610.634753

0.98955611.02502

0.99971610.927454

1.00987610.829886

1.01749610.537187

1.02765611.220153

1.03273610.244487

1.04035610.634753

1.04797610.829886

1.05559610.439621

1.06575610.829886

1.07337611.220153

1.08099610.927454

1.09115611.02502

1.09877610.634753

1.10893610.829886

1.11655611.122586

1.12417610.927454

1.13433610.537187

1.14195610.829886

1.14957611.317719

1.15719610.73232

1.16735611.415286

1.17497610.634753

1.18259611.220153

1.19275610.634753

1.20037610.73232

1.20799610.927454

1.21561610.537187

1.22323610.829886

1.23339610.537187

1.24101610.634753

1.25117610.927454

1.25879610.829886

1.26641610.73232

1.2765767.61019

1.2841968.585856

1.2943569.463955

1.30197610.14692

1.31213610.244487

1.31975610.439621

1.32737610.342054

1.33753610.73232

1.34515610.244487

1.35531610.927454

1.36293610.927454

1.37055610.049354

1.37817610.927454

1.38579610.049354

1.39595610.14692

1.40357610.73232

1.41119610.634753

1.41627610.14692

1.42897610.537187

1.43405610.439621

1.44421610.049354

1.45183610.049354

1.4619969.659088

1.46961610.342054

1.47977610.14692

1.48739610.342054

1.49501610.634753

1.50771610.537187

1.51279610.244487

1.52295610.244487

1.53057610.927454

1.53819610.439621

1.54581610.439621

1.55343610.634753

1.56105610.439621

1.56867610.342054

1.57629610.829886

1.58645610.342054

1.59407610.829886

1.60169610.244487

1.60931610.537187

1.61693610.439621

1.62709610.14692

1.63217610.14692

1.64233610.14692

1.64995610.537187

1.65757610.14692

1.66519610.342054

1.67535610.244487

1.68297610.049354

1.69059610.634753

1.70075610.049354

1.7109169.951788

1.71853610.342054

1.72615610.537187

1.7337769.951788

1.74393610.537187

1.75155610.14692

1.75917610.439621

1.76933610.439621

1.7744169.561521

1.78457610.14692

1.7921969.854221

1.79981610.342054

1.8074369.561521

1.81759610.342054

1.8252169.659088

1.8353769.756655

1.8404569.854221

1.85061610.244487

1.85823610.244487

1.8709369.659088

1.87855610.342054

1.88617610.244487

1.8937969.659088

1.9039569.854221

1.91157610.342054

1.9217369.756655

1.92935610.244487

1.9395169.854221

1.9471369.854221

1.9547569.366389

1.9623769.756655

1.9725369.561521

1.9801569.659088

1.9903169.561521

1.9979369.561521

2.0055569.659088

2.0131769.561521

2.0207969.951788

2.0309569.366389

2.03603610.049354

2.0512769.561521

2.0588969.951788

2.0639769.854221

2.07159610.14692

2.0817569.659088

2.0893769.561521

2.09953610.049354

2.1071569.756655

2.1173169.756655

2.12493610.049354

2.13255610.049354

2.1401769.366389

2.1477969.366389

2.1579569.366389

2.1655769.659088

2.1731969.951788

2.1808169.756655

2.1884369.268822

2.1960569.951788

2.2062169.463955

2.2112969.366389

2.2214569.951788

2.2290769.756655

2.2392369.366389

2.2468569.756655

2.2570169.951788

2.2646369.659088

2.2722569.659088

2.2798769.659088

2.2874969.463955

2.2925769.756655

2.3027369.561521

2.3103569.561521

2.3179769.463955

2.3255969.268822

2.3357569.659088

2.3433769.854221

2.3509969.366389

2.3611569.366389

2.3687769.561521

2.3763969.268822

2.3865569.854221

2.3941769.463955

2.4043369.951788

2.4119569.463955

2.4195769.463955

2.4271969.561521

2.4348169.854221

2.4449769.073689

2.4525969.463955

2.4602169.268822

2.4703769.756655

2.4754569.463955

2.4830769.366389

2.4906969.366389

2.5008569.366389

2.5084769.854221

2.5160969.463955

2.5237169.951788

2.5338769.366389

2.5414969.951788

2.55165610.049354

2.5592769.756655

2.5668969.171255

2.5770569.659088

2.5821369.463955

2.5922969.951788

2.5999169.268822

2.6100769.854221

2.6151569.463955

2.6253169.463955

2.6329369.561521

2.6405569.756655

2.6481769.366389

2.6583369.366389

2.6659569.854221

2.6761169.854221

2.6837369.951788

2.6913569.366389

2.6989769.366389

2.7065969.659088

2.71421610.049354

2.72183610.14692

2.73199610.049354

2.73961610.439621

2.74723610.049354

2.75485610.342054

2.76501610.14692

2.77263610.342054

2.78025610.244487

2.7904169.854221

2.79803610.537187

2.8056569.756655

2.81327610.14692

2.8208969.951788

2.82851610.244487

2.83613610.439621

2.84375610.244487

2.85391610.342054

2.86153610.537187

2.87169610.14692

2.87931610.244487

2.8894769.951788

2.89709610.73232

2.90471610.049354

2.91487610.049354

2.92249610.829886

2.93011610.73232

2.94027610.73232

2.94789610.537187

2.95805610.342054

2.96567610.829886

2.97075610.342054

2.98091610.244487

2.98599610.537187

2.99615610.73232

3.00377610.927454

3.01393610.829886

3.02155610.634753

3.02917610.244487

3.03933610.634753

3.04695610.537187

3.05457610.537187

3.06473610.927454

3.07235610.342054

3.07997610.73232

3.09013610.634753

3.09775610.342054

3.10791610.927454

3.11299610.537187

3.12315611.122586

3.13077610.829886

3.14093610.342054

3.14855611.122586

3.15617610.634753

3.16379610.342054

3.17395610.927454

3.18157610.634753

3.19173610.829886

3.19681610.342054

3.20697610.73232

3.21459610.829886

3.22475610.73232

3.23237610.634753

3.23999610.927454

3.25015610.537187

3.25523610.537187

3.26539611.122586

3.27301610.73232

3.27809610.537187

3.28825610.73232

3.29587610.342054

3.30349610.829886

3.31365610.634753

3.32127610.342054

3.32889610.439621

3.33651610.14692

3.34667610.829886

3.35429610.537187

3.36191611.02502

3.37207610.244487

3.37969610.634753

3.38731610.829886

3.39493610.439621

3.40255610.439621

3.41271610.73232

3.42033610.73232

3.4279569.854221

3.43557610.439621

3.4431969.951788

3.45081610.73232

3.46097610.049354

3.46859610.342054

3.47875610.049354

3.48383610.73232

3.49653610.634753

3.50161610.439621

3.50923610.14692

3.51939610.049354

3.5244769.659088

3.53209610.342054

3.54225610.14692

3.54987610.244487

3.55749610.537187

3.56511610.634753

3.57527610.049354

3.5828969.756655

3.59051610.049354

3.6006769.756655

3.6082969.951788

3.61591610.049354

3.6235369.366389

3.6336969.951788

3.6413169.756655

3.6489369.756655

3.6565569.073689

3.6667169.171255

3.6743369.268822

3.6844969.659088

3.6895769.268822

3.6997369.073689

3.7073569.561521

3.7175169.463955

3.7251368.878556

3.7327569.463955

3.7403768.878556

3.7505368.683423

3.7581569.171255

3.7657768.976122

3.7759368.683423

3.7835569.366389

3.7911768.390723

3.7987968.878556

3.8064168.585856

3.8140368.976122

3.8241968.000457

3.8318168.488289

3.8419768.488289

3.8470568.390723

3.8572168.390723

3.8648368.488289

3.8749968.098023

3.8826168.000457

3.8927768.488289

3.9003968.000457

3.9080168.19559

3.9181767.61019

3.9257967.512624

3.9334167.219924

3.9410367.512624

3.9486567.805324

3.9562768.000457

3.9664367.707757

3.9715167.61019

3.9842167.219924

3.9892967.512624

3.9994567.707757

4.0070767.512624

4.0146977.61019

4.0248567.61019

4.0324767.61019

4.0400967.122358

4.0502567.122358

4.0578777.317491

4.0680367.317491

4.0756567.317491

4.0832767.61019

4.0908977.317491

4.0959767.61019

4.1086767.122358

4.1239167.317491

4.1315367.024791

4.1391567.024791

4.1493166.927225

4.1569367.415058

4.1670966.634525

4.1747166.634525

4.1823367.024791

4.1899567.219924

4.2001167.024791

4.2051967.122358

4.2153566.927225

4.2229766.536958

4.2305966.146692

4.2407566.439392

4.2483766.244259

4.2585366.634525

4.2661566.146692

4.2737766.536958

4.2839366.536958

4.2915566.341826

4.3017165.951559

4.3093365.853993

4.3194966.049126

4.3271166.049126

4.3347366.341826

4.3448965.853993

4.3499765.951559

4.3601366.146692

4.3652165.853993

4.3753766.146692

4.3829965.561293

4.3906166.341826

4.4007765.951559

4.4083965.951559

4.4185565.561293

4.4261766.244259

4.4337965.658859

4.4439565.853993

4.4490375.658859

4.4591965.36616

4.4693565.463727

4.4769766.146692

4.4845965.756426

4.4922175.658859

4.4998365.463727

4.5074565.463727

4.5150766.146692

4.5252375.951559

4.5328565.36616

4.5379365.853993

4.5480965.853993

4.5557165.756426

4.5633365.756426

4.5734965.658859

4.5811165.756426

4.5887365.268593

4.5988965.658859

4.6065165.658859

4.6141365.171027

4.6242965.853993

4.6293765.561293

4.6395364.878327

4.6496965.07346

4.6547765.463727

4.6623965.36616

4.6700164.780761

4.6776365.36616

4.6852565.07346

4.6928765.07346

4.7055764.975894

4.7081164.975894

4.7182765.463727

4.7258964.780761

4.7335164.878327

4.7436764.780761

4.7512965.07346

4.7589164.780761

4.7665365.07346

4.7741565.171027

4.7817765.171027

4.7919364.585628

4.7970164.878327

4.8097164.878327

4.8147964.683194

4.8249564.390495

4.8325764.195362

4.8427364.000228

4.8503574.000228

4.8579764.097795

4.8681364.000228

4.8732164.488061

4.8833774.000228

4.8909963.902662

4.8986163.902662

4.9087764.390495

4.9163964.292928

4.9214763.512396

4.9316364.390495

4.9392564.000228

4.9494164.195362

4.9570364.488061

4.9646564.585628

4.9748164.292928

4.9824364.390495

4.9925964.000228

5.0002164.390495

5.0078364.585628

5.0154563.902662

5.0256164.097795

5.0332364.488061

5.0433963.902662

5.0510164.390495

5.0586364.390495

5.0662564.292928

5.0764164.390495

5.0814963.902662

5.0941963.707529

5.0992764.292928

5.1094364.097795

5.1170563.609962

5.1246763.707529

5.1322964.292928

5.1424564.292928

5.1500763.902662

5.1602363.609962

5.1678563.902662

5.1754764.000228

5.1856364.195362

5.1907164.000228

5.2008763.707529

5.2059563.512396

5.2161163.512396

5.2237363.902662

5.2338964.292928

5.2415173.122129

5.2491364.000228

5.2592963.609962

5.2669163.707529

5.2745373.609962

5.2821563.414829

5.2923163.707529

5.2999363.512396

5.3075563.707529

5.3151763.707529

5.3253363.219696

5.3329563.707529

5.3405763.317262

5.3507363.902662

5.3583564.000228

5.3659763.805095

5.3735963.512396

5.3812163.512396

5.3913763.512396

5.3989963.902662

5.4066163.609962

5.4142363.219696

5.4243963.122129

5.4320163.317262

5.4421763.512396

5.4497963.122129

5.4574163.024563

5.4675762.926996

5.4726563.219696

5.4853563.414829

5.4904363.707529

5.5005963.414829

5.5082162.731863

5.5158362.926996

5.5234562.926996

5.5336162.82943

5.5412362.731863

5.5513963.122129

5.5564772.53673

5.5691763.024563

5.5742562.926996

5.5844162.731863

5.5920363.122129

5.5996572.82943

5.6098163.122129

5.6174362.82943

5.6275962.731863

5.6352162.926996

5.6428362.82943

5.6504563.122129

5.6580762.53673

5.6656962.731863

5.6758572.24403

5.6834762.341597

5.6936361.951331

5.6987161.853764

5.7088772.146464

5.7164962.439164

5.7241162.341597

5.7342762.146464

5.7418962.048897

5.7495161.756198

5.7596762.439164

5.7672961.658631

5.7749161.951331

5.7825361.951331

5.7926961.951331

5.8003161.268365

5.8053961.365932

5.8155561.951331

5.8231761.073232

5.8333361.365932

5.8409561.561065

5.8511161.756198

5.8587361.561065

5.8663561.268365

5.8739761.268365

5.8841361.463498

5.8917560.682966

5.9019160.780532

5.9095361.073232

5.9171560.975665

5.9273160.487833

5.9323961.365932

5.9425560.878099

5.9476370.975665

5.9577961.365932

5.9679560.975665

5.9755760.878099

5.9831960.975665

5.9933560.975665

6.0009761.073232

6.0085960.780532

6.0162160.780532

6.0263760.487833

6.0339970.780532

6.0441560.878099

6.0517760.682966

6.0593960.878099

6.0695560.487833

6.0771760.682966

6.0873360.585399

6.0949560.585399

6.1051160.487833

6.1127360.390266

6.1228960.390266

6.1330560.2927

6.1381360.682966

6.1482960.682966

6.1559160.682966

6.1609960.487833

6.1711560.682966

6.1787760.487833

6.1889360.585399

6.1965560.097567

6.2067160.682966

6.2143360.195133

6.2219560.878099

6.2295770.390266

6.2371960.390266

6.2473560.487833

6.2549760.780532

6.2651360.682966

6.2651360.585399

Test Method"CM

Sample I. D."A

Specimen Numbe

EXTENSION (mm)"LOAD (N)

-0.0188240.390266

-0.0188240.682966

-0.0162840

-0.0086640.487833

-0.0035840.682966

0.0065761.073232

0.0116561.463498

0.0218161.658631

0.0268962.048897

0.0370561.951331

0.0446762.439164

0.0522963.512396

0.0624564.292928

0.0700764.097795

0.0802365.561293

0.0878565.658859

0.0954766.049126

0.1005566.829658

0.1107166.536958

0.1157967.122358

0.1259567.219924

0.1310368.098023

0.1411967.90289

0.1488168.585856

0.1589768.390723

0.1665969.171255

0.1767569.268822

0.1843769.756655

0.1919969.268822

0.2021569.659088

0.2097769.561521

0.2173969.659088

0.2224769.659088

0.2300969.854221

0.24025610.14692

0.24787610.049354

0.2529569.756655

0.26311610.14692

0.2707369.756655

0.2808969.659088

0.28851610.244487

0.29613610.244487

0.30375610.14692

0.3139169.659088

0.3215369.756655

0.3291569.756655

0.33931610.244487

0.34693610.14692

0.35709610.537187

0.3647169.659088

0.37233610.049354

0.3774169.659088

0.3875769.756655

0.3951969.756655

0.40535610.14692

0.4129769.659088

0.4231369.951788

0.43075610.537187

0.4383769.463955

0.44853610.342054

0.45361610.14692

0.4637769.854221

0.47139610.342054

0.48155610.14692

0.4891769.854221

0.49933610.537187

0.50441610.049354

0.5145769.854221

0.5221969.756655

0.52981610.14692

0.53743610.14692

0.54759610.14692

0.55521610.537187

0.56283610.439621

0.57045610.439621

0.58061610.439621

0.58823610.439621

0.59839610.342054

0.6060169.854221

0.61363610.244487

0.62379610.14692

0.6288769.951788

0.63903610.634753

0.64665610.634753

0.6542769.951788

0.66189610.14692

0.67205610.634753

0.6771369.951788

0.68729610.049354

0.69491610.049354

0.70507610.342054

0.71269610.829886

0.72031610.537187

0.73047610.634753

0.73809610.439621

0.7457169.951788

0.75333610.342054

0.76095610.049354

0.76857610.73232

0.77873610.927454

0.78635610.537187

0.79397610.244487

0.8015969.951788

0.81175610.244487

0.81937610.537187

0.82699610.342054

0.83715610.537187

0.84477610.439621

0.85493610.927454

0.86255611.02502

0.87017610.244487

0.87779610.634753

0.88541610.439621

0.89303610.927454

0.90319610.537187

0.91081610.244487

0.92097610.439621

0.92859610.439621

0.93621610.14692

0.94383610.927454

0.95399610.927454

0.96161610.829886

0.96923610.73232

0.97685610.634753

0.98955611.02502

0.99971610.927454

1.00987610.829886

1.01749610.537187

1.02765611.220153

1.03273610.244487

1.04035610.634753

1.04797610.829886

1.05559610.439621

1.06575610.829886

1.07337611.220153

1.08099610.927454

1.09115611.02502

1.09877610.634753

1.10893610.829886

1.11655611.122586

1.12417610.927454

1.13433610.537187

1.14195610.829886

1.14957611.317719

1.15719610.73232

1.16735611.415286

1.17497610.634753

1.18259611.220153

1.19275610.634753

1.20037610.73232

1.20799610.927454

1.21561610.537187

1.22323610.829886

1.23339610.537187

1.24101610.634753

1.25117610.927454

1.25879610.829886

1.26641610.73232

1.2765767.61019

1.2841968.585856

1.2943569.463955

1.30197610.14692

1.31213610.244487

1.31975610.439621

1.32737610.342054

1.33753610.73232

1.34515610.244487

1.35531610.927454

1.36293610.927454

1.37055610.049354

1.37817610.927454

1.38579610.049354

1.39595610.14692

1.40357610.73232

1.41119610.634753

1.41627610.14692

1.42897610.537187

1.43405610.439621

1.44421610.049354

1.45183610.049354

1.4619969.659088

1.46961610.342054

1.47977610.14692

1.48739610.342054

1.49501610.634753

1.50771610.537187

1.51279610.244487

1.52295610.244487

1.53057610.927454

1.53819610.439621

1.54581610.439621

1.55343610.634753

1.56105610.439621

1.56867610.342054

1.57629610.829886

1.58645610.342054

1.59407610.829886

1.60169610.244487

1.60931610.537187

1.61693610.439621

1.62709610.14692

1.63217610.14692

1.64233610.14692

1.64995610.537187

1.65757610.14692

1.66519610.342054

1.67535610.244487

1.68297610.049354

1.69059610.634753

1.70075610.049354

1.7109169.951788

1.71853610.342054

1.72615610.537187

1.7337769.951788

1.74393610.537187

1.75155610.14692

1.75917610.439621

1.76933610.439621

1.7744169.561521

1.78457610.14692

1.7921969.854221

1.79981610.342054

1.8074369.561521

1.81759610.342054

1.8252169.659088

1.8353769.756655

1.8404569.854221

1.85061610.244487

1.85823610.244487

1.8709369.659088

1.87855610.342054

1.88617610.244487

1.8937969.659088

1.9039569.854221

1.91157610.342054

1.9217369.756655

1.92935610.244487

1.9395169.854221

1.9471369.854221

1.9547569.366389

1.9623769.756655

1.9725369.561521

1.9801569.659088

1.9903169.561521

1.9979369.561521

2.0055569.659088

2.0131769.561521

2.0207969.951788

2.0309569.366389

2.03603610.049354

2.0512769.561521

2.0588969.951788

2.0639769.854221

2.07159610.14692

2.0817569.659088

2.0893769.561521

2.09953610.049354

2.1071569.756655

2.1173169.756655

2.12493610.049354

2.13255610.049354

2.1401769.366389

2.1477969.366389

2.1579569.366389

2.1655769.659088

2.1731969.951788

2.1808169.756655

2.1884369.268822

2.1960569.951788

2.2062169.463955

2.2112969.366389

2.2214569.951788

2.2290769.756655

2.2392369.366389

2.2468569.756655

2.2570169.951788

2.2646369.659088

2.2722569.659088

2.2798769.659088

2.2874969.463955

2.2925769.756655

2.3027369.561521

2.3103569.561521

2.3179769.463955

2.3255969.268822

2.3357569.659088

2.3433769.854221

2.3509969.366389

2.3611569.366389

2.3687769.561521

2.3763969.268822

2.3865569.854221

2.3941769.463955

2.4043369.951788

2.4119569.463955

2.4195769.463955

2.4271969.561521

2.4348169.854221

2.4449769.073689

2.4525969.463955

2.4602169.268822

2.4703769.756655

2.4754569.463955

2.4830769.366389

2.4906969.366389

2.5008569.366389

2.5084769.854221

2.5160969.463955

2.5237169.951788

2.5338769.366389

2.5414969.951788

2.55165610.049354

2.5592769.756655

2.5668969.171255

2.5770569.659088

2.5821369.463955

2.5922969.951788

2.5999169.268822

2.6100769.854221

2.6151569.463955

2.6253169.463955

2.6329369.561521

2.6405569.756655

2.6481769.366389

2.6583369.366389

2.6659569.854221

2.6761169.854221

2.6837369.951788

2.6913569.366389

2.6989769.366389

2.7065969.659088

2.71421610.049354

2.72183610.14692

2.73199610.049354

2.73961610.439621

2.74723610.049354

2.75485610.342054

2.76501610.14692

2.77263610.342054

2.78025610.244487

2.7904169.854221

2.79803610.537187

2.8056569.756655

2.81327610.14692

2.8208969.951788

2.82851610.244487

2.83613610.439621

2.84375610.244487

2.85391610.342054

2.86153610.537187

2.87169610.14692

2.87931610.244487

2.8894769.951788

2.89709610.73232

2.90471610.049354

2.91487610.049354

2.92249610.829886

2.93011610.73232

2.94027610.73232

2.94789610.537187

2.95805610.342054

2.96567610.829886

2.97075610.342054

2.98091610.244487

2.98599610.537187

2.99615610.73232

3.00377610.927454

3.01393610.829886

3.02155610.634753

3.02917610.244487

3.03933610.634753

3.04695610.537187

3.05457610.537187

3.06473610.927454

3.07235610.342054

3.07997610.73232

3.09013610.634753

3.09775610.342054

3.10791610.927454

3.11299610.537187

3.12315611.122586

3.13077610.829886

3.14093610.342054

3.14855611.122586

3.15617610.634753

3.16379610.342054

3.17395610.927454

3.18157610.634753

3.19173610.829886

3.19681610.342054

3.20697610.73232

3.21459610.829886

3.22475610.73232

3.23237610.634753

3.23999610.927454

3.25015610.537187

3.25523610.537187

3.26539611.122586

3.27301610.73232

3.27809610.537187

3.28825610.73232

3.29587610.342054

3.30349610.829886

3.31365610.634753

3.32127610.342054

3.32889610.439621

3.33651610.14692

3.34667610.829886

3.35429610.537187

3.36191611.02502

3.37207610.244487

3.37969610.634753

3.38731610.829886

3.39493610.439621

3.40255610.439621

3.41271610.73232

3.42033610.73232

3.4279569.854221

3.43557610.439621

3.4431969.951788

3.45081610.73232

3.46097610.049354

3.46859610.342054

3.47875610.049354

3.48383610.73232

3.49653610.634753

3.50161610.439621

3.50923610.14692

3.51939610.049354

3.5244769.659088

3.53209610.342054

3.54225610.14692

3.54987610.244487

3.55749610.537187

3.56511610.634753

3.57527610.049354

3.5828969.756655

3.59051610.049354

3.6006769.756655

3.6082969.951788

3.61591610.049354

3.6235369.366389

3.6336969.951788

3.6413169.756655

3.6489369.756655

3.6565569.073689

3.6667169.171255

3.6743369.268822

3.6844969.659088

3.6895769.268822

3.6997369.073689

3.7073569.561521

3.7175169.463955

3.7251368.878556

3.7327569.463955

3.7403768.878556

3.7505368.683423

3.7581569.171255

3.7657768.976122

3.7759368.683423

3.7835569.366389

3.7911768.390723

3.7987968.878556

3.8064168.585856

3.8140368.976122

3.8241968.000457

3.8318168.488289

3.8419768.488289

3.8470568.390723

3.8572168.390723

3.8648368.488289

3.8749968.098023

3.8826168.000457

3.8927768.488289

3.9003968.000457

3.9080168.19559

3.9181767.61019

3.9257967.512624

3.9334167.219924

3.9410367.512624

3.9486567.805324

3.9562768.000457

3.9664367.707757

3.9715167.61019

3.9842167.219924

3.9892967.512624

3.9994567.707757

4.0070767.512624

4.0146977.61019

4.0248567.61019

4.0324767.61019

4.0400967.122358

4.0502567.122358

4.0578777.317491

4.0680367.317491

4.0756567.317491

4.0832767.61019

4.0908977.317491

4.0959767.61019

4.1086767.122358

4.1239167.317491

4.1315367.024791

4.1391567.024791

4.1493166.927225

4.1569367.415058

4.1670966.634525

4.1747166.634525

4.1823367.024791

4.1899567.219924

4.2001167.024791

4.2051967.122358

4.2153566.927225

4.2229766.536958

4.2305966.146692

4.2407566.439392

4.2483766.244259

4.2585366.634525

4.2661566.146692

4.2737766.536958

4.2839366.536958

4.2915566.341826

4.3017165.951559

4.3093365.853993

4.3194966.049126

4.3271166.049126

4.3347366.341826

4.3448965.853993

4.3499765.951559

4.3601366.146692

4.3652165.853993

4.3753766.146692

4.3829965.561293

4.3906166.341826

4.4007765.951559

4.4083965.951559

4.4185565.561293

4.4261766.244259

4.4337965.658859

4.4439565.853993

4.4490375.658859

4.4591965.36616

4.4693565.463727

4.4769766.146692

4.4845965.756426

4.4922175.658859

4.4998365.463727

4.5074565.463727

4.5150766.146692

4.5252375.951559

4.5328565.36616

4.5379365.853993

4.5480965.853993

4.5557165.756426

4.5633365.756426

4.5734965.658859

4.5811165.756426

4.5887365.268593

4.5988965.658859

4.6065165.658859

4.6141365.171027

4.6242965.853993

4.6293765.561293

4.6395364.878327

4.6496965.07346

4.6547765.463727

4.6623965.36616

4.6700164.780761

4.6776365.36616

4.6852565.07346

4.6928765.07346

4.7055764.975894

4.7081164.975894

4.7182765.463727

4.7258964.780761

4.7335164.878327

4.7436764.780761

4.7512965.07346

4.7589164.780761

4.7665365.07346

4.7741565.171027

4.7817765.171027

4.7919364.585628

4.7970164.878327

4.8097164.878327

4.8147964.683194

4.8249564.390495

4.8325764.195362

4.8427364.000228

4.8503574.000228

4.8579764.097795

4.8681364.000228

4.8732164.488061

4.8833774.000228

4.8909963.902662

4.8986163.902662

4.9087764.390495

4.9163964.292928

4.9214763.512396

4.9316364.390495

4.9392564.000228

4.9494164.195362

4.9570364.488061

4.9646564.585628

4.9748164.292928

4.9824364.390495

4.9925964.000228

5.0002164.390495

5.0078364.585628

5.0154563.902662

5.0256164.097795

5.0332364.488061

5.0433963.902662

5.0510164.390495

5.0586364.390495

5.0662564.292928

5.0764164.390495

5.0814963.902662

5.0941963.707529

5.0992764.292928

5.1094364.097795

5.1170563.609962

5.1246763.707529

5.1322964.292928

5.1424564.292928

5.1500763.902662

5.1602363.609962

5.1678563.902662

5.1754764.000228

5.1856364.195362

5.1907164.000228

5.2008763.707529

5.2059563.512396

5.2161163.512396

5.2237363.902662

5.2338964.292928

5.2415173.122129

5.2491364.000228

5.2592963.609962

5.2669163.707529

5.2745373.609962

5.2821563.414829

5.2923163.707529

5.2999363.512396

5.3075563.707529

5.3151763.707529

5.3253363.219696

5.3329563.707529

5.3405763.317262

5.3507363.902662

5.3583564.000228

5.3659763.805095

5.3735963.512396

5.3812163.512396

5.3913763.512396

5.3989963.902662

5.4066163.609962

5.4142363.219696

5.4243963.122129

5.4320163.317262

5.4421763.512396

5.4497963.122129

5.4574163.024563

5.4675762.926996

5.4726563.219696

5.4853563.414829

5.4904363.707529

5.5005963.414829

5.5082162.731863

5.5158362.926996

5.5234562.926996

5.5336162.82943

5.5412362.731863

5.5513963.122129

5.5564772.53673

5.5691763.024563

5.5742562.926996

5.5844162.731863

5.5920363.122129

5.5996572.82943

5.6098163.122129

5.6174362.82943

5.6275962.731863

5.6352162.926996

5.6428362.82943

5.6504563.122129

5.6580762.53673

5.6656962.731863

5.6758572.24403

5.6834762.341597

5.6936361.951331

5.6987161.853764

5.7088772.146464

5.7164962.439164

5.7241162.341597

5.7342762.146464

5.7418962.048897

5.7495161.756198

5.7596762.439164

5.7672961.658631

5.7749161.951331

5.7825361.951331

5.7926961.951331

5.8003161.268365

5.8053961.365932

5.8155561.951331

5.8231761.073232

5.8333361.365932

5.8409561.561065

5.8511161.756198

5.8587361.561065

5.8663561.268365

5.8739761.268365

5.8841361.463498

5.8917560.682966

5.9019160.780532

5.9095361.073232

5.9171560.975665

5.9273160.487833

5.9323961.365932

5.9425560.878099

5.9476370.975665

5.9577961.365932

5.9679560.975665

5.9755760.878099

5.9831960.975665

5.9933560.975665

6.0009761.073232

6.0085960.780532

6.0162160.780532

6.0263760.487833

6.0339970.780532

6.0441560.878099

6.0517760.682966

6.0593960.878099

6.0695560.487833

6.0771760.682966

6.0873360.585399

6.0949560.585399

6.1051160.487833

6.1127360.390266

6.1228960.390266

6.1330560.2927

6.1381360.682966

6.1482960.682966

6.1559160.682966

6.1609960.487833

6.1711560.682966

6.1787760.487833

6.1889360.585399

6.1965560.097567

6.2067160.682966

6.2143360.195133

6.2219560.878099

6.2295770.390266

6.2371960.390266

6.2473560.487833

6.2549760.780532

6.2651360.682966

6.2651360.585399

Test Method"CM

Sample I. D."A

Specimen Numbe

EXTENSION (mm)"LOAD (N)

-0.060338-0.1953

-0.0603380

-0.060338-0.585901

-0.060338-0.3906

-0.060338-0.488251

-0.060338-0.09765

-0.0552580.1953

-0.050178-0.09765

-0.045098-0.09765

-0.0425580

-0.037478-0.3906

-0.0323980

-0.0273180.29295

-0.0273180.1953

-0.0196980.488251

-0.0171580.1953

-0.0120780.878851

-0.0095380.683551

-0.0044580.683551

0.0031621.660052

0.0057021.562402

0.0107822.050652

0.0158621.953002

0.0184022.343603

0.0234823.320104

0.0285623.515404

0.0311024.198954

0.0361824.589555

0.0412624.394255

0.0463424.784855

0.0488825.273105

0.0539625.370756

0.0590425.956657

0.0641226.542557

0.0641226.151956

0.0717426.933157

0.0742827.421408

0.0793627.226107

0.0819027.128458

0.0869827.323758

0.0895227.909658

0.0946027.519058

0.0996827.909658

0.1022227.421408

0.1073027.909658

0.1098427.812008

0.1174628.300258

0.1174628.690859

0.1250828.495559

0.1276228.495559

0.1327028.495559

0.1352429.37441

0.1403229.66736

0.1454029.86266

0.1479429.66736

0.1530229.96031

0.15810210.253261

0.16318210.155611

0.1657229.96031

0.17080210.643861

0.17334210.057961

0.17842211.034462

0.18350211.034462

0.18604210.936812

0.18858210.839161

0.19620211.327412

0.20128211.522712

0.20382211.620362

0.20890211.620362

0.21398211.620362

0.21906212.010962

0.22160211.913313

0.22414211.522712

0.22922211.718013

0.23176212.010962

0.23938212.303913

0.24192211.815663

0.24700211.522712

0.25208211.425062

0.25462211.229761

0.25716211.522712

0.26224211.327412

0.26732211.034462

0.27240211.132112

0.27494210.546211

0.27748210.44856

0.28510210.839161

0.28764210.643861

0.29272210.253261

0.29272210.44856

0.30034210.350911

0.30288210.546211

0.3079629.86266

0.31050210.253261

0.3155829.96031

0.32066210.253261

0.32828210.546211

0.3308229.56971

0.3359029.56971

0.33844210.155611

0.34352210.155611

0.34606210.155611

0.3511429.37441

0.3562229.56971

0.3587629.47206

0.3638429.47206

0.3663829.76501

0.3714629.47206

0.3765429.86266

0.3816229.86266

0.3841629.86266

0.3892429.47206

0.3943229.37441

0.3968629.86266

0.3994029.37441

0.4070229.66736

0.4095629.27676

0.4146429.86266

0.4171829.081459

0.4222629.86266

0.4273429.96031

0.4324229.27676

0.4349629.96031

0.4375029.56971

0.4451229.86266

0.45020210.155611

0.4527429.76501

0.4552829.66736

0.4603629.86266

0.4629029.27676

0.4705229.47206

0.4705229.47206

0.4781429.66736

0.4806829.37441

0.4857629.27676

0.4883029.66736

0.4933829.76501

0.4984629.47206

0.5035429.081459

0.5060829.081459

0.5111629.17911

0.5162428.98381

0.5187829.37441

0.5238629.37441

0.5264029.47206

0.5314829.17911

0.5365629.56971

0.5416429.27676

0.5416429.17911

0.5492629.47206

0.5543428.593209

0.5594229.27676

0.5619629.27676

0.5670429.17911

0.5721228.886159

0.5746628.788509

0.5772028.788509

0.5822829.17911

0.5873628.886159

0.5924428.788509

0.5949829.081459

0.6026029.081459

0.6051428.788509

0.6102229.27676

0.6153028.98381

0.6203828.690859

0.6229228.98381

0.6280028.98381

0.6305428.886159

0.6356228.495559

0.6381628.788509

0.6432428.495559

0.6457828.788509

0.6508628.690859

0.6559428.98381

0.6610228.788509

0.6635628.788509

0.6686428.202609

0.6737228.495559

0.6788028.397909

0.6813428.104959

0.6864228.495559

0.6889628.202609

0.6940428.300258

0.6991228.202609

0.7016627.812008

0.7092828.007308

0.7118228.300258

0.7169028.788509

0.7194428.202609

0.7245227.812008

0.7296028.007308

0.7346828.593209

0.7372227.714358

0.7423028.104959

0.7448427.909658

0.7499228.007308

0.7524628.007308

0.7575428.690859

0.7626228.202609

0.7677028.007308

0.7702428.495559

0.7753228.495559

0.7804028.690859

0.7854828.202609

0.7880227.812008

0.7931028.397909

0.7981828.007308

0.8032628.397909

0.8058028.202609

0.8083428.593209

0.8134227.909658

0.8185028.397909

0.8235828.690859

0.8261228.202609

0.8312028.007308

0.8337428.593209

0.8388228.593209

0.8413628.593209

0.8489828.690859

0.8515228.397909

0.8566028.593209

0.8591428.593209

0.8642228.593209

0.8667628.495559

0.8718428.202609

0.8769228.886159

0.8769228.104959

0.8845428.690859

0.8870828.104959

0.8921628.300258

0.8947028.593209

0.9023228.495559

0.9048628.788509

0.9099428.104959

0.9124828.007308

0.9175628.593209

0.9226427.812008

0.9251828.788509

0.9302628.104959

0.9328028.300258

0.9378828.007308

0.9429628.300258

0.9480428.104959

0.9505827.812008

0.9556627.812008

0.9582028.300258

0.9632828.495559

0.9658227.909658

0.9734428.007308

0.9785228.397909

0.9810627.812008

0.9861427.812008

0.9912228.495559

0.9937627.616708

1.0013827.714358

1.0039227.909658

1.0090027.909658

1.0115427.909658

1.0166227.616708

1.0191628.104959

1.0267827.909658

1.0293227.714358

1.0344027.714358

1.0369427.519058

1.0420227.616708

1.0471027.909658

1.0521827.812008

1.0547227.812008

1.0598027.421408

1.0623427.714358

1.0699627.812008

1.0699627.421408

1.0775827.909658

1.0801227.616708

1.0877427.616708

1.0902827.128458

1.0928227.616708

1.0979027.616708

1.1004427.226107

1.1055227.519058

1.1106027.519058

1.1156827.421408

1.1182227.812008

1.1233027.323758

1.1258427.519058

1.1309227.909658

1.1360027.812008

1.1410827.519058

1.1436227.616708

1.1487027.519058

1.1512427.812008

1.1563227.421408

1.1588627.421408

1.1639427.323758

1.1690227.714358

1.1715627.714358

1.1766427.714358

1.1791827.421408

1.1842627.616708

1.1893427.519058

1.1944227.616708

1.1969627.030808

1.2020427.128458

1.2071227.226107

1.2122027.323758

1.2122027.616708

1.2172827.909658

1.2223627.812008

1.2249027.421408

1.2299827.323758

1.2325227.616708

1.2376027.421408

1.2426827.421408

1.2477627.226107

1.2477626.933157

1.2553827.128458

1.2604627.128458

1.2630027.519058

1.2655427.030808

1.2731627.226107

1.2757027.519058

1.2807827.128458

1.2833227.812008

1.2884027.226107

1.2934827.421408

1.2985627.714358

1.3011027.909658

1.3036427.128458

1.3112627.421408

1.3163428.007308

1.3188827.714358

1.3214227.421408

1.3265027.323758

1.3315827.714358

1.3366627.519058

1.3392027.812008

1.3442828.104959

1.3468228.104959

1.3519027.909658

1.3544427.519058

1.3595227.616708

1.3646028.007308

1.3696827.909658

1.3722227.909658

1.3773028.104959

1.3798427.909658

1.3849228.104959

1.3874628.007308

1.3925428.007308

1.3976228.495559

1.4027028.007308

1.4052428.495559

1.4077828.495559

1.4154028.300258

1.4204828.300258

1.4230227.909658

1.4255627.909658

1.4331828.495559

1.4357227.812008

1.4408028.007308

1.4433428.104959

1.4484227.812008

1.4535027.714358

1.4585828.007308

1.4611228.300258

1.4662028.397909

1.4687428.104959

1.4763628.690859

1.4789028.300258

1.4839828.397909

1.4865228.397909

1.4916028.495559

1.4941428.593209

1.4992228.690859

1.5043028.397909

1.5068428.397909

1.5119228.104959

1.5144628.495559

1.5195427.909658

1.5246228.007308

1.5297028.397909

1.5297028.202609

1.5373228.593209

1.5398628.007308

1.5474828.397909

1.5474828.300258

1.5525628.300258

1.5551028.202609

1.5601828.397909

1.5652628.593209

1.5678027.909658

1.5728828.397909

1.5754228.104959

1.5805028.397909

1.5830428.104959

1.5881228.690859

1.5932027.909658

1.5982828.495559

1.6008228.593209

1.6059027.812008

1.6084428.397909

1.6135228.007308

1.6186028.593209

1.6211428.202609

1.6262228.202609

1.6287627.909658

1.6338428.300258

1.6363828.007308

1.6440028.397909

1.6465428.397909

1.6516227.909658

1.6541627.616708

1.6592428.007308

1.6643228.397909

1.6694028.202609

1.6719428.397909

1.6744827.714358

1.6795628.300258

1.6846428.007308

1.6897228.202609

1.6922627.909658

1.6973428.202609

1.6998828.007308

1.7075027.812008

1.7075028.300258

1.7151228.397909

1.7176628.104959

1.7252828.593209

1.7278228.007308

1.7329028.300258

1.7354428.397909

1.7405227.714358

1.7430628.397909

1.7481428.300258

1.7506827.909658

1.7557628.495559

1.7583028.007308

1.7633827.714358

1.7684628.397909

1.7735428.300258

1.7786228.202609

1.7786228.104959

1.7862427.714358

1.7887828.202609

1.7938627.812008

1.7964028.007308

1.8014828.202609

1.8040228.397909

1.8116427.616708

1.8141827.519058

1.8192627.519058

1.8218027.616708

1.8294228.397909

1.8319627.323758

1.8370427.714358

1.8395827.812008

1.8421228.104959

1.8472028.007308

1.8497428.007308

1.8573627.812008

1.8599027.909658

1.8649827.714358

1.8675227.421408

1.8751427.323758

1.8776828.104959

1.8827627.714358

1.8853027.812008

1.8903827.421408

1.8954627.714358

1.9005428.202609

1.9005428.007308

1.9056227.714358

1.9107027.519058

1.9157828.202609

1.9183228.007308

1.9234027.714358

1.9284828.007308

1.9310228.007308

1.9361027.421408

1.9386427.128458

1.9437227.226107

1.9488027.812008

1.9538827.030808

1.9538827.421408

1.9615027.323758

1.9640427.714358

1.9691227.812008

1.9716627.812008

1.9767427.323758

1.9818227.128458

1.9843624.980155

1.9894425.273105

1.9919825.566056

1.9970625.663706

2.0021425.859006

2.0072226.347257

2.0072226.054306

2.0148427.128458

2.0173826.640207

2.0250026.933157

2.0300826.737857

2.0351626.542557

2.0377026.444907

2.0427827.323758

2.0453227.226107

2.0504026.835507

2.0554827.421408

2.0605626.542557

2.0605626.542557

2.0681827.030808

2.0707224.394255

2.0758024.589555

2.0783425.370756

2.0834225.468406

2.0859625.663706

2.0935825.663706

2.0961226.249607

2.1012026.737857

2.1037426.151956

2.1088226.249607

2.1113626.542557

2.1164427.030808

2.1215226.542557

2.1240626.542557

2.1291427.030808

2.1316826.444907

2.1367626.737857

2.1393026.835507

2.1443826.640207

2.1494625.468406

2.1520023.906004

2.1570824.784855

2.1621624.980155

2.1672425.273105

2.1697825.859006

2.1748625.761356

2.1799425.566056

2.1824826.054306

2.1850225.566056

2.1901026.542557

2.1951825.956657

2.2002626.835507

2.2028026.054306

2.2078826.249607

2.2129626.347257

2.2180427.030808

2.2205824.687205

2.2256624.589555

2.2282024.589555

2.2332824.882505

2.2358225.566056

2.2434425.077805

2.2459825.468406

2.2510625.566056

2.2536025.956657

2.2586826.054306

2.2637626.054306

2.2688426.444907

2.2713826.249607

2.2739226.347257

2.2815426.444907

2.2840826.151956

2.2891626.249607

2.2917026.151956

2.2967826.444907

2.3018626.444907

2.3069426.640207

2.3069425.956657

2.3120226.737857

2.3171026.542557

2.3221826.542557

2.3247226.347257

2.3272626.249607

2.3323426.640207

2.3374226.640207

2.3425026.640207

2.3450426.249607

2.3501226.835507

2.3552026.151956

2.3602825.956657

2.3602826.835507

2.3679026.640207

2.3704426.444907

2.3755226.054306

2.3780626.347257

2.3831426.347257

2.3856826.347257

2.3907626.542557

2.3958426.347257

2.3983825.859006

2.4034626.151956

2.4085426.542557

2.4136226.835507

2.4136226.054306

2.4187026.151956

2.4237826.737857

2.4288626.444907

2.4314024.394255

2.4364824.491905

2.4390225.077805

2.4441025.370756

2.4491825.077805

2.4517225.663706

2.4568025.859006

2.4618825.663706

2.4669625.761356

2.4695025.859006

2.4745826.151956

2.4771226.151956

2.4822025.663706

2.4847426.054306

2.4898226.444907

2.4923626.151956

2.4974425.663706

2.4999825.956657

2.5050626.249607

2.5101425.468406

2.5152226.151956

2.5203025.663706

2.5228425.663706

2.5279225.566056

2.5330025.468406

2.5380826.151956

2.5380825.273105

2.5431625.370756

2.5482425.566056

2.5533225.761356

2.5558625.956657

2.5609425.956657

2.5634825.761356

2.5711025.468406

2.5736426.054306

2.5787226.151956

2.5812625.761356

2.5888825.859006

2.5914225.761356

2.5939625.468406

2.5990425.663706

2.6015825.566056

2.6066625.761356

2.6117425.566056

2.6168225.175456

2.6219025.370756

2.6244425.175456

2.6269825.273105

2.6346025.566056

2.6371425.468406

2.6422225.468406

2.6447625.566056

2.6498425.663706

2.6549225.273105

2.6600025.370756

2.6625425.663706

2.6676225.370756

2.6701624.980155

2.6752425.566056

2.6777824.882505

2.6828625.273105

2.6879425.468406

2.6904825.956657

2.6955625.175456

2.6981025.468406

2.7031825.370756

2.7082625.175456

2.7133424.980155

2.7133424.980155

2.7209625.566056

2.7235025.175456

2.7285825.663706

2.7311224.980155

2.7362025.566056

2.7412825.566056

2.7463625.077805

2.7489025.077805

2.7514424.980155

2.7590624.980155

2.7616024.980155

2.7666825.566056

2.7666825.273105

2.7743025.370756

2.7768424.980155

2.7819225.370756

2.7844624.589555

2.7870024.882505

2.7946225.566056

2.7997025.273105

2.8022424.980155

2.8047825.273105

2.8098624.980155

2.8149425.468406

2.8200225.370756

2.8200225.077805

2.8251024.003654

2.8301824.101304

2.8327224.784855

2.8378024.491905

2.8403424.784855

2.8454224.980155

2.8505024.589555

2.8530424.784855

2.8581224.589555

2.8632024.882505

2.8682824.882505

2.8708224.589555

2.8759024.980155

2.8784424.687205

2.8835225.077805

2.8911425.468406

2.8911424.687205

2.8987624.784855

2.9038425.077805

2.9089222.831853

2.9114623.906004

2.9165423.613054

2.9216224.394255

2.9267024.589555

2.9292423.906004

2.9343224.589555

2.9368623.906004

2.9419424.687205

2.9444824.491905

2.9521024.491905

2.9546424.784855

2.9597224.394255

2.9622624.394255

2.9673424.491905

2.9698824.394255

2.9749624.491905

2.9800424.687205

2.9825824.589555

2.9876624.980155

2.9927424.687205

2.9952824.101304

2.9978224.784855

3.0029024.491905

3.0079824.882505

3.0130624.394255

3.0156024.784855

3.0206824.882505

3.0232224.394255

3.0283024.296605

3.0333824.296605

3.0359224.394255

3.0410024.980155

3.0460824.394255

3.0486224.394255

3.0537024.882505

3.0587824.980155

3.0613224.394255

3.0664024.687205

3.0689424.296605

3.0765624.296605

3.0791024.882505

3.0841824.394255

3.0867224.491905

3.0918024.296605

3.0943424.491905

3.0994224.394255

3.1045024.589555

3.1095824.589555

3.1121224.101304

3.1146624.589555

3.1197424.784855

3.1248224.491905

3.1299024.980155

3.1324424.198954

3.1375224.491905

3.1400624.296605

3.1451424.296605

3.1502224.882505

3.1553024.784855

3.1553024.003654

3.1629224.687205

3.1654624.003654

3.1705424.687205

3.1730824.101304

3.1781624.101304

3.1832424.394255

3.1857824.198954

3.1908624.101304

3.1934023.906004

3.1959424.589555

3.2010224.589555

3.2061024.003654

3.2086424.003654

3.2137224.784855

3.2162623.906004

3.2238824.101304

3.2238824.003654

3.2289624.101304

3.2340423.808354

3.2391224.394255

3.2416624.198954

3.2467424.198954

3.2518224.687205

3.2543624.101304

3.2594423.906004

3.2619824.003654

3.2670624.589555

3.2721424.101304

3.2772224.198954

3.2797623.906004

3.2848424.491905

3.2873824.101304

3.2924624.687205

3.2950024.296605

3.3026224.003654

3.3051624.394255

3.3102424.101304

3.3127824.491905

3.3178624.589555

3.3229423.808354

3.3254824.003654

3.3305624.491905

3.3356424.491905

3.3381824.101304

3.3432623.906004

3.3483424.198954

3.3483424.198954

3.3559623.808354

3.3585023.710704

3.3635823.906004

3.3661224.198954

3.3737424.198954

3.3788224.003654

3.3813624.198954

3.3839024.296605

3.3915223.613054

3.3940623.515404

3.3991423.613054

3.4016822.831853

3.4067623.515404

3.4118423.027153

3.4169223.710704

3.4194623.906004

3.4220023.906004

3.4270823.710704

3.4321624.296605

3.4347024.198954

3.4372424.394255

3.4448624.296605

3.4474024.101304

3.4524824.198954

3.4550224.198954

3.4601023.613054

3.4626423.710704

3.4677223.613054

3.4728023.906004

3.4778823.124803

3.4804222.929503

3.4855023.027153

3.4880423.124803

3.4931223.417754

3.4982023.320104

3.5032824.101304

3.5058224.198954

3.5083624.003654

3.5159823.808354

3.5185224.296605

3.5236023.710704

3.5261424.101304

3.5312223.515404

3.5363023.710704

3.5413822.636553

3.5439223.027153

3.5490023.222453

3.5540823.027153

3.5591623.710704

3.5617023.613054

3.5667824.003654

3.5693223.906004

3.5744023.417754

3.5769423.906004

3.5820223.710704

3.5871023.515404

3.5896423.613054

3.5947224.296605

3.5998024.101304

3.6023423.808354

3.6074223.613054

3.6125023.515404

3.6150423.613054

3.6201223.515404

3.6226624.296605

3.6277423.515404

3.6302824.003654

3.6353623.320104

3.6404424.101304

3.6455223.906004

3.6480623.710704

3.6506023.613054

3.6556823.710704

3.6607623.417754

3.6658424.101304

3.6683823.710704

3.6734622.734203

3.6760023.320104

3.6836223.124803

3.6836223.417754

3.6912423.515404

3.6937823.710704

3.6963223.417754

3.7014024.003654

3.7064824.003654

3.7115623.710704

3.7141023.222453

3.7191823.710704

3.7217224.101304

3.7268023.808354

3.7318822.441253

3.7369623.124803

3.7395022.831853

3.7445823.124803

3.7471223.222453

3.7522023.710704

3.7547422.929503

3.7598223.613054

3.7649024.003654

3.7699823.710704

3.7725223.320104

3.7776023.222453

3.7826823.710704

3.7877623.613054

3.7903023.320104

3.7953822.929503

3.7979223.515404

3.8030023.613054

3.8055423.515404

3.8080823.222453

3.8131623.417754

3.8182423.710704

3.8233223.417754

3.8258623.027153

3.8309423.808354

3.8334823.417754

3.8385623.417754

3.8436423.710704

3.8487223.124803

3.8512623.027153

3.8563423.710704

3.8588823.027153

3.8614223.320104

3.8690423.222453

3.8715822.929503

3.8766623.417754

3.8766622.929503

3.8817422.636553

3.8868223.320104

3.8919022.831853

3.8944423.320104

3.8969822.343603

3.9046023.222453

3.9071422.148302

3.9122222.343603

3.9147622.245952

3.9198422.636553

3.9249222.148302

3.9274622.636553

Test Method"CM

Sample I. D."A

Specimen Numbe

EXTENSION (mm)"LOAD (N)

-0.110573-0.097567

-0.110573-0.2927

-0.1105730.390266

-0.1105730.195133

-0.1105730

-0.1105730.2927

-0.1105730

-0.1105730

-0.1105730.195133

-0.110573-0.097567

-0.1105730.390266

-0.1105730.585399

-0.110573-0.097567

-0.1105730.097567

-0.1105730.195133

-0.1105730.390266

-0.1080330

-0.1080330.390266

-0.108033-0.097567

-0.1080330.2927

-0.1080330.585399

-0.1080330

-0.108033-0.195133

-0.108033-0.195133

-0.1080330.2927

-0.1054930.585399

-0.1054930

-0.105493-0.2927

-0.105493-0.097567

-0.105493-0.195133

-0.1054930.487833

-0.102953-0.195133

-0.1029530.2927

-0.1029530

-0.1029530.2927

-0.102953-0.195133

-0.102953-0.195133

-0.1004130.195133

-0.1004130.390266

-0.1004130.390266

-0.1004130

-0.0978730.585399

-0.097873-0.195133

-0.097873-0.097567

-0.0978730.195133

-0.0953330.2927

-0.0953330.097567

-0.095333-0.2927

-0.0953330.2927

-0.095333-0.097567

-0.0953330.585399

-0.0927930.195133

-0.0927930.097567

-0.092793-0.097567

-0.0927930.390266

-0.0927930.195133

-0.0927930.390266

-0.0927930.487833

-0.0927930.780532

-0.0902530

-0.0902530.2927

-0.087713-0.195133

-0.0877130.487833

-0.0877130.2927

-0.0877130.2927

-0.0851730

-0.0851730.585399

-0.0851730.487833

-0.085173-0.097567

-0.0851730.097567

-0.0851730.487833

-0.082633-0.195133

-0.082633-0.097567

-0.082633-0.2927

-0.082633-0.2927

-0.0800930.585399

-0.0800930.585399

-0.0800930.2927

-0.0800930.195133

-0.080093-0.195133

-0.077553-0.097567

-0.0775530.487833

-0.0775530.780532

-0.0775530.2927

-0.0750130.097567

-0.0750130.097567

-0.0750130

-0.0750130

-0.0750130.390266

-0.075013-0.097567

-0.0750130.585399

-0.0750130.682966

-0.075013-0.097567

-0.0724730.097567

-0.0724730.585399

-0.0724730.097567

-0.0699330.2927

-0.0699330.097567

-0.0699330.487833

-0.0699330.195133

-0.0699330.2927

-0.0673930.390266

-0.0673930

-0.0673930.195133

-0.0673930.585399

-0.0673930.097567

-0.0673930.195133

-0.0648530.585399

-0.064853-0.195133

-0.0648530.390266

-0.0648530.585399

-0.0623130.097567

-0.0623130.487833

-0.0623130.390266

-0.0623130.585399

-0.059773-0.097567

-0.0597730.390266

-0.059773-0.097567

-0.0597730.2927

-0.0572330.585399

-0.0572330.682966

-0.0572330.195133

-0.0572330

-0.0572330.780532

-0.0572330.390266

-0.0572330.195133

-0.0572330.390266

-0.057233-0.195133

-0.0546930.195133

-0.0546930.682966

-0.0546930.390266

-0.0521530

-0.0521530.195133

-0.0521530.195133

-0.049613-0.097567

-0.0496130.195133

-0.0496130.2927

-0.0496130.487833

-0.049613-0.097567

-0.0496130

-0.0470730.585399

-0.0470730.097567

-0.0470730.585399

-0.0470730.097567

-0.0445330

-0.0445330.097567

-0.0445330.487833

-0.041993-0.097567

-0.0419930.682966

-0.0419930.390266

-0.0419930.682966

-0.0419930.2927

-0.0394530.097567

-0.0394530.487833

-0.0394530.195133

-0.0394530.390266

-0.0394530

-0.0394530.195133

-0.0394530.2927

-0.0369130.487833

-0.0369130.585399

-0.0369130.195133

-0.0343730.2927

-0.0343730.195133

-0.0343730.682966

-0.0343730.585399

-0.0318330.487833

-0.0318330.487833

-0.0318330.195133

-0.0318330.487833

-0.0318330.097567

-0.0318330.097567

-0.0292930.585399

-0.0292930.682966

-0.0292930

-0.0292930.195133

-0.0292930.682966

-0.0267530.487833

-0.0267530.2927

-0.0267530.682966

-0.0267530.487833

-0.0242130.195133

-0.0242130.487833

-0.0242130.682966

-0.0242130.195133

-0.0242130.097567

-0.0216730.682966

-0.0216730.2927

-0.0216730.097567

-0.0216730.878099

-0.0216730.2927

-0.0216730.390266

-0.021673-0.097567

-0.0216730.585399

-0.0191330.487833

-0.0191330.585399

-0.0191330.585399

-0.0191330.2927

-0.0165930.195133

-0.0165930.487833

-0.0165930.195133

-0.0165930

-0.0140530.682966

-0.0140530.682966

-0.0140530.195133

-0.0140530.878099

-0.0140530.682966

-0.0140530.195133

-0.0115130.2927

-0.0115130.780532

-0.0115130.682966

-0.0115130.585399

-0.0089730.878099

-0.0089730.2927

-0.0089730.682966

-0.0089730.682966

-0.0064330.878099

-0.0064330.195133

-0.0064330.390266

-0.0064330.195133

-0.0064331.073232

-0.0064330.390266

-0.0064330.878099

-0.0038930.097567

-0.0038930.195133

-0.0038930.975665

-0.0038930.780532

-0.0038930.2927

-0.0038930.195133

-0.0038930.585399

-0.0038930.878099

-0.0013530.682966

-0.0013530.390266

0.0011870.780532

0.0011870.390266

0.0011870.2927

0.0037270.390266

0.0037271.170799

0.0037270.780532

0.0037270.390266

0.0037270.585399

0.0037270.585399

0.0037271.268365

0.0062671.170799

0.0062671.170799

0.0062671.170799

0.0062670.780532

0.0088070.682966

0.0088070.878099

0.0088071.073232

0.0113470.878099

0.0113471.268365

0.0113471.561065

0.0113471.170799

0.0113470.878099

0.0138871.170799

0.0138871.073232

0.0138871.463498

0.0138871.658631

0.0138871.170799

0.0138871.073232

0.0138871.170799

0.0138871.658631

0.0138870.878099

0.0164271.268365

0.0164271.268365

0.0164271.853764

0.0189671.951331

0.0189671.268365

0.0189671.365932

0.0215071.268365

0.0215071.951331

0.0215072.24403

0.0215072.439164

0.0215072.24403

0.0215071.658631

0.0215072.341597

0.0240472.24403

0.0240471.951331

0.0240471.853764

0.0240472.24403

0.0265872.82943

0.0265872.24403

0.0265872.53673

0.0265872.731863

0.0291272.82943

0.0291272.53673

0.0291272.439164

0.0291273.219696

0.0291273.219696

0.0316673.024563

0.0316672.439164

0.0316672.926996

0.0316672.731863

0.0316672.439164

0.0316672.82943

0.0316672.731863

0.0316673.219696

0.0316673.122129

0.0342072.926996

0.0342073.024563

0.0342073.122129

0.0367473.609962

0.0367473.219696

0.0367473.707529

0.0367474.292928

0.0392873.609962

0.0392874.097795

0.0392873.902662

0.0392873.512396

0.0392874.292928

0.0392874.488061

0.0418274.097795

0.0418274.292928

0.0418274.390495

0.0418274.683194

0.0443674.585628

0.0443674.488061

0.0443674.488061

0.0443674.585628

0.0469074.975894

0.0469075.171027

0.0469075.561293

0.0469074.878327

0.0469075.07346

0.0469075.658859

0.0494475.36616

0.0494475.658859

0.0494474.975894

0.0494475.463727

0.0494475.268593

0.0494475.268593

0.0494475.36616

0.0519875.951559

0.0519875.36616

0.0519875.561293

0.0545275.756426

0.0545276.049126

0.0545275.853993

0.0545276.536958

0.0570675.951559

0.0570676.146692

0.0570676.439392

0.0570675.853993

0.0570676.146692

0.0570676.634525

0.0570676.829658

0.0596076.244259

0.0596076.927225

0.0596076.341826

0.0621476.927225

0.0621476.927225

0.0621477.024791

0.0621476.634525

0.0646877.219924

0.0646877.024791

0.0646876.927225

0.0646877.219924

0.0646877.219924

0.0646877.317491

0.0646877.61019

0.0672276.927225

0.0672276.927225

0.0672277.317491

0.0672277.415058

0.0672277.122358

0.0672277.024791

0.0672277.317491

0.0697677.122358

0.0697677.415058

0.0697677.317491

0.0723078.098023

0.0723078.293157

0.0723077.61019

0.0748478.488289

0.0748478.390723

0.0748478.098023

0.0748478.19559

0.0748478.293157

0.0748478.683423

0.0748478.390723

0.0773878.19559

0.0773877.90289

0.0773878.000457

0.0773878.683423

0.0799278.683423

0.0799278.293157

0.0799278.390723

0.0799278.976122

0.0824678.780989

0.0824678.488289

0.0824678.976122

0.0824679.073689

0.0824679.268822

0.0824678.976122

0.0824678.683423

0.0824679.171255

0.0850079.073689

0.0850078.976122

0.0850078.878556

0.0850078.780989

0.0850078.488289

0.0850078.976122

0.0875479.171255

0.0875478.780989

0.0875478.780989

0.0900879.756655

0.0900879.073689

0.0900879.268822

0.0926279.756655

0.0926279.756655

0.0926279.171255

0.0926279.659088

0.0926279.951788

0.0926279.366389

0.0951679.659088

0.0951679.366389

0.09516710.14692

0.0977079.659088

0.09770710.14692

0.0977079.756655

0.09770710.14692

0.1002479.756655

0.1002479.951788

0.1002479.951788

0.10024710.14692

0.10024710.634753

0.10024710.634753

0.10278710.049354

0.1027879.951788

0.10278710.244487

0.10278710.049354

0.10278710.049354

0.10278710.049354

0.10532710.14692

0.10532710.634753

0.10532710.634753

0.10786710.73232

0.10786711.02502

0.10786710.73232

0.10786710.927454

0.11040710.634753

0.11040711.02502

0.11040710.829886

0.11040710.634753

0.11040711.220153

0.11294711.122586

0.11294710.927454

0.11294710.829886

0.11294710.634753

0.11294711.02502

0.11548711.317719

0.11548711.220153

0.11548711.122586

0.11548710.927454

0.11802710.829886

0.11802711.220153

0.11802711.903119

0.11802711.805552

0.11802711.415286

0.11802711.317719

0.11802711.707986

0.12056711.512852

0.12056711.122586

0.12056711.415286

0.12056711.512852

0.12056711.220153

0.11802711.317719

0.11802711.707986

0.11802711.415286

0.12056711.903119

0.12056712.098251

0.12056712.000685

0.12310711.903119

0.12310711.707986

0.12310712.195818

0.12564712.293384

0.12564712.195818

0.12564712.293384

0.12564711.903119

0.12564711.805552

0.12564712.195818

0.12818711.805552

0.12818712.390952

0.12818711.903119

0.12818712.293384

0.13072712.000685

0.13072712.195818

0.13072712.098251

0.13072712.390952

0.13326712.586084

0.13326712.488518

0.13326712.878784

0.13326712.781217

0.13326712.683651

0.13326712.195818

0.13326712.976351

0.13580712.878784

0.13580712.488518

0.13580712.293384

0.13580712.878784

0.13580712.586084

0.13580712.390952

0.13834712.488518

0.13834712.586084

0.14088713.366617

0.14088712.976351

0.14088713.464183

0.14342713.366617

0.14342712.878784

0.14342713.171484

0.14342713.26905

0.14342713.561749

0.14342712.878784

0.14596713.366617

0.14596713.659317

0.14596713.756883

0.14596713.659317

0.14596713.073917

0.14850713.952016

0.14850713.659317

0.14850713.366617

0.15104713.561749

0.15104713.366617

0.15104713.756883

0.15104713.85445

0.15104714.342283

0.15358713.85445

0.15358714.244715

0.15358713.756883

0.15358714.147149

0.15358713.85445

0.15358713.85445

0.15358714.049582

0.15612713.756883

0.15612714.439849

0.15612714.049582

0.15612714.342283

0.15866714.147149

0.15866714.634982

0.15866714.244715

0.15866714.244715

0.15866714.439849

0.16120714.049582

0.16120714.244715

0.16120714.732548

0.16120714.147149

0.16120714.634982

0.16120714.927681

0.16374714.342283

0.16374714.732548

0.16374715.025248

0.16374714.342283

0.16628715.025248

0.16628714.537415

0.16628715.122815

0.16628715.317948

0.16882715.025248

0.16882715.025248

0.16882715.317948

0.16882714.927681

0.16882715.025248

0.16882714.634982

0.17136715.122815

0.17136715.025248

0.17136714.927681

0.17136715.122815

0.17136714.927681

0.17136714.732548

0.17390714.537415

0.17390714.927681

0.17390715.220381

0.17390715.317948

0.17644714.927681

0.17644715.51308

0.17644715.220381

0.17644715.708214

0.17644715.317948

0.17898715.220381

0.17898715.903347

0.17898715.415514

0.17898715.903347

0.17898716.000913

0.17898715.903347

0.18152715.805781

0.18152715.805781

0.18152715.805781

0.18406715.903347

0.18406715.415514

0.18406716.09848

0.18406715.610648

0.18406715.415514

0.18660715.415514

0.18660716.000913

0.18660716.488746

0.18914715.805781

0.18914716.09848

0.18914715.610648

0.18914715.805781

0.18914715.708214

0.18914715.805781

0.18914716.09848

0.18914716.000913

0.19168716.09848

0.19168716.000913

0.19168715.805781

0.19422716.293614

0.19422716.39118

0.19422716.293614

0.19422716.586313

0.19676716.683879

0.19676716.781446

0.19676716.683879

0.19676716.39118

0.19676716.586313

0.19676716.293614

0.19676716.781446

0.19930716.196046

0.19930716.488746

0.19930716.09848

0.19930716.196046

0.20184716.39118

0.20184716.683879

0.20184716.586313

0.20438717.269279

0.20438716.683879

0.20438716.683879

0.20438717.171712

0.20692717.269279

0.20692716.879012

0.20692716.488746

0.20692716.586313

0.20692716.683879

0.20692716.781446

0.20692716.586313

0.20692717.269279

0.20946716.586313

0.20946716.781446

0.20946716.683879

0.21200716.879012

0.21200717.464411

0.21200716.879012

0.21200717.074146

0.21454716.879012

0.21454717.464411

0.21454717.269279

0.21454716.683879

0.21454717.269279

0.21454716.781446

0.21454716.781446

0.21708717.464411

0.21708717.464411

0.21708717.659545

0.21708717.269279

0.21962717.269279

0.21962717.561978

0.21962716.879012

0.22216717.561978

0.22216717.561978

0.22216717.854678

0.22216717.659545

0.22216717.757112

0.22470717.464411

0.22470717.757112

0.22470716.976578

0.22470717.269279

0.22470717.171712

0.22470717.561978

0.22470717.171712

0.22724717.366845

0.22724717.366845

0.22724717.269279

0.22978717.854678

0.22978718.147377

0.22978717.464411

0.22978717.659545

0.23232717.269279

0.23232717.952244

0.23232718.244945

0.23232717.952244

0.23232717.464411

0.23232717.854678

0.23486717.464411

0.23486717.952244

0.23486718.244945

0.23486718.049811

0.23486718.049811

0.23740718.147377

0.23740718.342511

0.23740718.732777

0.23740718.440077

0.23994718.244945

0.23994718.927909

0.23994719.22061

0.23994719.025477

0.23994718.732777

0.23994718.63521

0.24248719.22061

0.24248718.63521

0.24248718.927909

0.24248719.025477

0.24248718.440077

0.24248719.025477

0.24248718.732777

0.24248718.732777

0.24502718.732777

0.24502718.732777

0.24502718.830343

0.24756719.22061

0.24756719.123043

0.24756719.318176

0.24756719.806008

0.25010719.513309

0.25010719.610876

0.25010718.537644

0.25010717.757112

0.25010716.781446

Test Method"CM

Sample I. D."A

Specimen Numbe

EXTENSION (mm)"LOAD (N)

-0.104523-0.292971

-0.1045230

-0.104523-0.195314

-0.104523-0.585942

-0.104523-0.292971

-0.1070630

-0.1299230

-0.129923-0.488285

-0.1299230.097657

-0.1299230.097657

-0.129923-0.097657

-0.129923-0.390628

-0.1299230

-0.129923-0.195314

-0.1299230.097657

-0.1299230.195314

-0.1299230.195314

-0.1299230.195314

-0.129923-0.292971

-0.129923-0.195314

-0.129923-0.292971

-0.1299230.195314

-0.129923-0.488285

-0.127383-0.390628

-0.127383-0.195314

-0.127383-0.390628

-0.1273830.097657

-0.127383-0.585942

-0.1248430

-0.1248430.097657

-0.124843-0.390628

-0.124843-0.195314

-0.124843-0.292971

-0.124843-0.097657

-0.124843-0.6836

-0.1248430.195314

-0.1248430.097657

-0.122303-0.292971

-0.1223030.195314

-0.1223030.195314

-0.119763-0.6836

-0.1197630.292971

-0.1197630.097657

-0.119763-0.488285

-0.1172230

-0.117223-0.585942

-0.1172230.195314

-0.1172230

-0.117223-0.097657

-0.117223-0.292971

-0.1146830

-0.114683-0.488285

-0.114683-0.292971

-0.114683-0.097657

-0.114683-0.195314

-0.112143-0.292971

-0.112143-0.390628

-0.1121430

-0.112143-0.585942

-0.109603-0.390628

-0.109603-0.488285

-0.109603-0.097657

-0.109603-0.292971

-0.1070630

-0.107063-0.195314

-0.107063-0.097657

-0.107063-0.6836

-0.1070630

-0.107063-0.195314

-0.1070630.097657

-0.107063-0.488285

-0.1070630.195314

-0.1070630

-0.1045230.195314

-0.1045230

-0.104523-0.488285

-0.101983-0.097657

-0.101983-0.6836

-0.1019830

-0.099443-0.390628

-0.099443-0.390628

-0.0994430.195314

-0.099443-0.6836

-0.0994430.097657

-0.099443-0.585942

-0.096903-0.195314

-0.096903-0.292971

-0.096903-0.195314

-0.096903-0.585942

-0.094363-0.195314

-0.094363-0.195314

-0.0943630.097657

-0.094363-0.390628

-0.094363-0.488285

-0.091823-0.390628

-0.091823-0.488285

-0.089283-0.488285

-0.089283-0.195314

-0.089283-0.488285

-0.089283-0.488285

-0.089283-0.390628

-0.089283-0.781257

-0.089283-0.292971

-0.089283-0.292971

-0.089283-0.292971

-0.086743-0.390628

-0.086743-0.292971

-0.086743-0.390628

-0.086743-0.292971

-0.084203-0.195314

-0.084203-0.292971

-0.084203-0.488285

-0.0842030

-0.081663-0.195314

-0.0816630.097657

-0.0816630

-0.0816630

-0.081663-0.097657

-0.0816630.097657

-0.079123-0.488285

-0.079123-0.097657

-0.079123-0.195314

-0.0791230.292971

-0.0765830.195314

-0.0765830.195314

-0.076583-0.195314

-0.076583-0.585942

-0.076583-0.292971

-0.0740430.097657

-0.0740430.195314

-0.074043-0.390628

-0.074043-0.097657

-0.071503-0.292971

-0.071503-0.488285

-0.071503-0.292971

-0.0715030.097657

-0.071503-0.097657

-0.071503-0.390628

-0.0715030.097657

-0.0715030.097657

-0.071503-0.195314

-0.068963-0.488285

-0.068963-0.292971

-0.0689630.195314

-0.066423-0.585942

-0.0664230.097657

-0.066423-0.097657

-0.063883-0.488285

-0.0638830.097657

-0.063883-0.292971

-0.063883-0.390628

-0.063883-0.097657

-0.063883-0.585942

-0.061343-0.097657

-0.0613430.097657

-0.061343-0.292971

-0.058803-0.585942

-0.058803-0.195314

-0.0588030

-0.0588030

-0.058803-0.195314

-0.0562630.097657

-0.056263-0.390628

-0.056263-0.488285

-0.0562630.097657

-0.053723-0.195314

-0.0537230.097657

-0.053723-0.292971

-0.0537230.097657

-0.0537230.195314

-0.053723-0.781257

-0.053723-0.195314

-0.0537230.097657

-0.053723-0.195314

-0.051183-0.097657

-0.051183-0.292971

-0.051183-0.195314

-0.048643-0.390628

-0.0486430

-0.0486430.195314

-0.0461030.195314

-0.046103-0.292971

-0.046103-0.292971

-0.046103-0.390628

-0.046103-0.292971

-0.046103-0.390628

-0.043563-0.390628

-0.0435630.097657

-0.043563-0.097657

-0.0435630

-0.041023-0.585942

-0.041023-0.195314

-0.0410230.195314

-0.041023-0.292971

-0.038483-0.390628

-0.0384830.195314

-0.038483-0.585942

-0.038483-0.097657

-0.0359430.097657

-0.033403-0.390628

-0.0334030

-0.033403-0.390628

-0.0334030.097657

-0.033403-0.195314

-0.0334030

-0.033403-0.488285

-0.033403-0.292971

-0.033403-0.488285

-0.0308630

-0.0308630.097657

-0.0283230

-0.0283230

-0.028323-0.292971

-0.025783-0.585942

-0.025783-0.292971

-0.025783-0.390628

-0.025783-0.097657

-0.0257830.195314

-0.025783-0.390628

-0.023243-0.390628

-0.0232430

-0.0232430

-0.0232430

-0.020703-0.097657

-0.0207030.097657

-0.020703-0.097657

-0.020703-0.097657

-0.0181630.195314

-0.0181630.195314

-0.018163-0.390628

-0.0181630

-0.018163-0.195314

-0.0181630.195314

-0.018163-0.488285

-0.015623-0.097657

-0.015623-0.292971

-0.0156230.097657

-0.015623-0.292971

-0.015623-0.390628

-0.015623-0.292971

-0.0156230.292971

-0.015623-0.292971

-0.013083-0.195314

-0.013083-0.488285

-0.0130830.195314

-0.0105430

-0.010543-0.292971

-0.0105430

-0.010543-0.390628

-0.0105430.097657

-0.0080030.292971

-0.0080030.097657

-0.0080030

-0.0080030.488285

-0.0080030

-0.0080030.292971

-0.0054630.195314

-0.005463-0.195314

-0.0054630.390628

-0.0029230.390628

-0.0029230.488285

-0.0029230.488285

-0.0003830

-0.0003830.097657

-0.0003830.097657

-0.0003830.488285

-0.0003830.390628

-0.0003830.6836

-0.0003830.488285

0.0021570.585942

0.0021570.097657

0.0021570.195314

0.0021570

0.0021570.781257

0.0021570.390628

0.0021570.6836

0.0021570.488285

0.0046970.781257

0.0046970.585942

0.00469