PROGRAMME : M. TECH CHEMICAL ENGINEERING CURRICULUM · PROGRAMME : M. TECH CHEMICAL ENGINEERING CURRICULUM ... multicomponent absorption, ... Phillip C. Wankat ,

SATHYABAMA UNIVERSITY FACULTY OF BIO AND CHEMICAL ENGINEERING

PROGRAMME : M. TECHCHEMICAL ENGINEERING

CURRICULUMSEMESTER - 1

Sl. No. COURSE CODE COURSE TITLE L T P C PAGE No.

1. SMT5104 Advanced Mathematics 3 1 0 4 2

2. SCH5101 Advanced Reaction Engineering 3 1 0 4 45

3. SCH5102 Modern Separation Processes 3 1 0 4 46

4. SCH5103 Environment and Safety in Process Industries 3 1 0 4 47

5. SCH5104 Process and Product Development 3 1 0 4 48

6. SCH5105 Process Design Engineering 3 1 0 4 49

PRACTICAL

7. SCH6531 Chemical Engineering Laboratory 0 0 6 3 74

TOTAL CREDITS: 27

SEMESTER - 2


1. SCH5106 Advanced Transport Phenomena 3 1 0 4 50

2. SCH5107 Advanced Process Control 3 1 0 4 51

3. Elective I 3 1 0 4

4. Elective II 3 1 0 4

5. Elective III 3 1 0 4

PRACTICAL

6. SCH6532 Computational Laboratory 0 0 6 3 74

7. S60PT Professional Training 0 0 10 5

TOTAL CREDITS: 28

SEMESTER - 3


1. SCH5201 Process Modeling and Simulation 3 1 0 4 61

2. Elective IV 3 1 0 4

3. Elective V 3 1 0 4

4. Elective VI 3 1 0 4

L - LECTURE HOURS, T – TUTORIAL HOURS, P – PRACTICAL HOURS, C – CREDITS

M.E. / M.Tech REGULAR xxii REGULATIONS 2015

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PRACTICAL

5. SCH6535 Chemical Process Simulation Lab 0 0 6 3 75

6. Project Work – Phase I

TOTAL CREDITS: 19

SEMESTER- IV


1. S60PROJ Project Work – Phase I and II 0 0 40 20 135

TOTAL CREDITS: 20

TOTAL CREDITS FOR THE COURSE: 94

LIST OF ELECTIVES


GROUP-1

1. SCH5601 Advanced Thermodynamics 3 1 0 4 135

2. SCH5602 Energy Audit and Conservation In Process Industries 3 1 0 4 136

3. SCH5603 Advanced Petroleum Refining Processes 3 1 0 4 137

4. SCH5604 Chemical Process Economics & Management 3 1 0 4 138

5. SCH5605 Membrane Separation Technology 3 1 0 4 139

6. SCH5606 Corrosion in Industry & Its Control 3 1 0 4 140

7. SCH5607 Advanced Nanotechnology 3 1 0 4 141

8. SCH5608 Process Heat Transfer 3 1 0 4 142

GROUP-2

1. SCH5609 Advanced Biochemical Engineering 3 1 0 4 143

2. SCH5610 Advanced Process Optimization 3 1 0 4 144

3. SCH5611 Advanced Instrumental Methods of Analysis 3 1 0 4 145

4. SCH5612 Project Engineering of Process Plants 3 1 0 4 146

5. SCH5613 Advanced Fluid Dynamics 3 1 0 4 147

6. SCH5614 Advanced Process Integration 3 1 0 4 148

7. SCH5615 Fluidization Engineering 3 1 0 4 149

8. SCH5616 Computational Fluid Dynamics 3 1 0 4 150

9. SCH5617 Multiphase Flow 3 1 0 4 151

M.E. / M.Tech REGULAR xxiii REGULATIONS 2015

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M.E. / M.Tech REGULAR 2 REGULATIONS 2015

SMT5104 ADVANCED MATHEMATICS

(Common to all M.E Branches and M.Tech Bio-Medical,Chemical)

L T P Credits Total Marks

3 1 0 4 100

UNIT 1 MATRIX THEORY 11 Hrs. QR decomposition – Eigen values using shifted QR algorithm- Singular Value Decomposition - Pseudo inverse- Least square approximations

UNIT 2 CALCULUS OF VARIATIONS 13 Hrs. Concept of Functionals - Euler’s equation – functional dependent on first and higher order derivatives – Functionals on several dependent variables – Iso perimetric problems - Variational problems with moving boundaries

UNIT 3 TRANSFORM METHODS 12 Hrs. Laplace transform methods for one dimensional wave equation – Displacements in a string – Longitudinal vibration of a elastic bar – Fourier transform methods for one dimensional heat conduction problems in infinite and semi infinite rod. Laplace equation – Properties of harmonic functions – Fourier transform methods for laplace equations. Solution for Poisson equation by Fourier transforms method

UNIT 4 ELLIPTIC EQUATIONS 11 Hrs. Laplace equation – Properties of harmonic functions – Fourier transform methods for Laplace equations – Solution for Poisson equation by Fourier transforms method.

UNIT 5 LINEAR AND NON-LINEAR PROGRAMMING 13 Hrs. Simplex Algorithm - Two Phase and Big M techniques – Duality theory - Dual Simplex method. Non Linear Programming – Constrained extremal problems - Lagranges multiplier method - Kuhn - Tucker conditions and solutions.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Richard Bronson, Schaum’s Outlines of Theory and Problems of Matrix Operations, McGraw-Hill, 1988. 2. Venkataraman M K, Higher Engineering Mathematics, National Pub. Co, 1992. 3. Elsgolts, L., Differential Equations and Calculus of Variations. Mir, 1977. 4. Sneddon,I.N., Elements of Partial differential equations, Dover Publications, 2006. 5. Sankara Rao, K., Introduction to partial differential equations. Prentice – Hall of India, 1995 6. Taha H A, “Operations research - An introduction, McMilan Publishing co, 1982.

END SEMESTER EXAMINATION QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 Hrs. PART A : 6 Questions of 5 Marks each – No Choice 30 Marks PART B : 2 Questions from each unit of internal choice, carrying 10 Marks each 50 Marks

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SCH5101 ADVANCED REACTION ENGINEERING L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To study the kinetics of solid catalyzed reactions, different types of reactors and their model equations. The

student will be able to select and design the type of reactor for a particular application.

UNIT 1 RTD FOR CHEMICAL REACTORS & ANALYSIS OF NON‐IDEAL REACTORS 12 Hrs. General characteristics, Measurement of RTD characteristics, RTD in ideal Reactors, Zero Parameter Models, Segregation Model, one parameter Models, The tanks in series Model, The dispersion model, Two parameter model, Testing the model and determining its parameters, other models of the non ideal reactors using the CSTR’s and PFR’s using RTD

UNIT 2 NON-CATALYTIC REACTIONS 12 Hrs. External diffusion effects on the Heterogeneous Reactions , Binary diffusion, External resistance to Mass Transfer, The shrinking core model, Progressive conversion model, Diffusion through gas film and ash layer .chemical reaction as the controlling steps-Development of equations for rate controlling steps.

UNIT 3 KINETICS OF FLUID SOLID CATALYTIC REACTIONS 12 Hrs. Classification and preparation of catalyst, nature and mechanism of catalytic reactions, Hougen-Watson model, Rate of adsorption, desorption, surface reaction, synthesizing rate law, mechanism and rate limiting steps, kinetics of catalyst deactivation and regeneration.

UNIT 4 DIFFUSION AND REACTION IN POROUS CATALYSTS 12 Hrs. Diffusion and Reactions in spherical catalyst pellets, Internal effectiveness factor, Falsefied kinetics, Overall effectiveness factor, Estimation of diffusion and reaction limited regimes, mass transfer and reaction in packed bed, The determination of limiting situation from reaction data

UNIT 5 DESIGN OF HETEROGENEOUS CATALYTIC REACTORS 12 Hrs. Heterogeneous data analysis for the reactor designs, experimental methods for finding rates, Isothermal and adiabatic fixed bed reactors, slurry reactors, trickle bed reactors, fluidized bed reactors, moving bed reactors ,chemical vapor deposition reactors.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Scott Foggler .H,” Element of Chemical Reaction Engineering”, 2 nd Edition, Prentice Hall of India,2003 2. Levenspiel.O, “Chemical Reaction Engineering”, 3 rd Edition, John Wiley & Sons, 2004 3. Smith.J.M, “Chemical Engineering Kinetics”, 3 rd Edition, Mc Graw Hill Publications,2000 4. Cranberry.J, “Chemical and Catalytic Reaction Engineering”, 3 rd Edition ,Mc Graw Hill Publications,2001 5. Froment G.F.and Bischoff,R.G.,”Chemical Reactor Analysis and Design” ,3rd Edition,John Wiley & Sons ,1990.


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SCH5102 MODERN SEPARATION PROCESSES L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The students are familiarized with the concepts of advanced separation processes like Membrane separation

processes, diffusional separation process, multicomponent absorption, azeotropic and extractive distillation.

UNIT 1 INTRODUCTION TO SEPARATION PROCESSES 12 Hrs. Fundamentals of separation process - OBJECTIVE, review of conventional processes, separation by phase addition, barrier, solid agent, gradient, mechanism, selection of feasible separation process, solid-liquid separation technique- theory and equipment used in cross flow filtration, cross flow electrofiltration, dual functional filter, sirofloc filter, recent advances in separation techniques.

UNIT 2 MEMBRANE SEPARATIONS 12 Hrs. Membrane based separation process-Fundamentals, Types and choice of membrane, plate and frame, tubular, spiral wound and hollow fibre membrane reactors and their relative merits and laboratory membrane permeators involving dialysis, reverse osmosis, pervaporation, gas permeation, ultrafiltration, microfiltration and nanofiltration, economics of membrane operations, ceramic membranes, Introduction to liquid membrane technology and their recent advances

UNIT 3 SEPARATION BY ADSORPTION TECHNIQUES 12 Hrs. Adsorption based separation process-Mechanism, types and choice of adsorbents, normal adsorption techniques, affinity chromatography and immuno chromatography, types of equipment and commercial processes, recent advances and process economics.

UNIT 4 IONIC SEPARATIONS 12 Hrs. Controlling factors, Applications, Types of equipment and design considerations for electrophoresis, di-electrophoresis, Ion Exchange chromatography and electrodialysis, Commercial processes and applications.

UNIT 5 OTHER SEPARATION TECHNIQUES 12 Hrs. Separations involving lyophilisation, zone melting, adductive crystallization, other separation processes, supercritical fluid extraction– fundamentals, Important supercritical processes and their applications – Decaffination of coffee, Extraction of oil from seeds, Residuum oil supercritical extraction, oil spill management, industrial effluent treatment by modern techniques. Surfactant based separations and Biofiltration: Concept, modeling, design aspects and applications.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Seader, J.D., Separation process principles, 2 nd Edition, John Wiley & sons,2006. 2. King, C. J., Separation Processes, 3rd Edition,Tata McGraw Hill Co., Ltd., 1982. 3. Nakagawal, O. V., Membrane Science and Technology,2nd Edition, Marcel Dekker, 1992. 4. Rousseau, R. W., Handbook of Separation Process Technology, John Wiley,2009. 5. Humphrey, J and G. Keller, Separation Process Technology,3rd Edition, McGraw-Hill, 1997. 6. Phillip C. Wankat , Separation Process Engineering,2nd Edition,Printice Hall,2007


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SCH5103 ENVIRONMENT AND SAFETY IN PROCESS

INDUSTRIES L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE This course makes the students aware of various safety methods adopted in chemical industries. Also gives

introduction to hazard analysis.

UNIT 1 SAFETY MANAGEMENT 12 Hrs. Introduction to Resources Management, Clean Development Mechanism, Command and control and Market Based Initiatives for pollution control. Safety Review, Preconditions and preparations, analytical procedures, Integrated approaches for safety management, Case studies in process safety management

UNIT 2 POLLUTION ABATEMENT IN INDUSTRIES 12 Hrs. Pollution Abatement in Process Industries Types of pollution in process industries, Modes of Surveillance Evaluation and Techniques for abatement. Design for effluent treatment in specific process Industries such as, Fertilizer, Petroleum, Pulp and Paper,Dairy etc.

UNIT 3 ENVIRONMENTAL ISSUES 12 Hrs. Environmental Issues in Process Industries ,Identifying and evaluating the probable environmental consequences of a proposed development project, Methods for Environmental Impact Assessment, Risk Assessment of the project. Uses, advantages and limitations of various environmental management tools. Case studies of Life cycle Assessment, Environmental Audit, Energy Audit and Water Audit.

UNIT 4 ENVIRONMENTAL REGULATIONS FOR SAFETY 12 Hrs. Environmental Regulations: Indian & International -Regulations to encourage pollution prevention and cleaner production. International standards on various aspects of environmental management, Process Design Practices -Chemical Process Industry (CPI) Safety Codes. Control technology to reduce accidents in CPI.

UNIT 5 HAZARD EVALUATION AND ANALYSIS 12 Hrs. Process Hazard Evaluation - Hazard Evaluation techniques, Qualitative Risk Analysis (QRA) Techniques, Risk Assessment (RA) accident probability, Hazard Operability Studies (HAZOP) Hazard Analysis (HAZAN), Fault Tree Analysis (FTA) and Event Tree Analysis (ETA) analysis of safety related information and safety measures.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1 Janes K. Lein,Integrated Environmental Planning,2nd Edition , Blackwell Publishing,1990 2. Steinbach.J, Safety Assessment for Chemical Proces,3rd Edition,Willey – VCT,1994


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SCH5104 PROCESS AND PRODUCT DEVELOPMENT L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The students should acquire theoretical and practical understanding of what influences a product development

process

UNIT 1 INTRODUCTION 12 Hrs. Goal of industrial research and development, Production structure of Chemical Industry, Task of Process Development, Creative Thinking. Preliminary Database Creation, Preliminary Process Synthesis, Examples. Product Development: Development of chemical product on laboratory scale, quality improvement, reproducibility etc. Case studies of products developed.

UNIT 2 CHEMICAL PRODUCTION PLANT AND ITS COMPONENTS 12 Hrs. Details about Catalyst, Reactors, Product Processing, Pipelines Pumps and Compressors, Product supply and storage, Water Disposal, Measurement and Control Technology, Plant Safety, Material Selection. Process Data: Chemical Data, Mass Balance, Physio-chemical data sources and estimation, Patenting and licensing situations, development cost, location, market situation, plant capacity, raw materials, waste disposals.

UNIT 3 COURSE OF PROCESS DEVELOPMENT 12 Hrs. Process development as an iterative process, Drawing up of an initial version of the process, checking the individual steps, Micro Plant: Link between the laboratory and the pilot plant, Testing the entire process on small scale.

UNIT 4 SCALING UP PROCESS 12 Hrs. Scaling up of process from laboratory to pilot plant and to industrial scale. Process Evaluation: Batch Versus Continuous, Equilibrium Limitations, Process alternatives, Preparation of study report.

UNIT 5 FLOW SHEETING 12 Hrs. Flow sheeting –presentation and preparation. Development of block diagram ,process flow diagram(PFD),piping and instrumentation diagram(P&ID),Standard symbols and rules.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Vogel.G.H Process Development - From the Initial Ideal to the Chemical Production Plant, 2nd Edition,Wiley- VCH Verlag

GmbH, 2005. 2. J M Douglas.J.M,Conceptual Design of Chemical Process,3rd Edition Mc Graw Hill Book Company. 1998. 3. Jordan ,Chemical Process Development,2nd Edition, Mc-Graw Hill,1996 4. SeiderW.D, Seader J.D, and Lewin D.R, Product and Process Design Principles-Synthesis, Analysis and Evaluation, 2nd

Edition, John Wiley and Sons. 2004. 5. Turton. R , Bailie R.C, Whiting W. B, Shaeiwitz J.A, Analysis, Synthesi and Design of Chemical Processes,3rd

Edition,Prentice Hall, New Jursey. 1998.


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SCH5105 PROCESS DESIGN ENGINEERING L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To understand advances in the design of Chemical process equipment

UNIT 1 INTRODUCTION 12 Hrs. The Nature of chemical process design, The Hierarchy of Chemical process Design - Formulation of Design problem –Continuous, Batch Process, Approaches to CPD - Nature of CPD - The Design OBJECTIVE (The Need) - Setting the Design Basis - Generation of Possible Design Concepts, Fitness Testing, Economic Evaluation, Optimization, and Selection, Detailed Design and Equipment Selection, Procurement, Construction, and Operation, approaches to Design, Design Reports, Process flow sheet development.

UNIT 2 DESIGN OF REACTORS 12 Hrs. General procedure for reactor design, Ideal and Real reactors, Reaction path, Reactor performance - conditions, Choice of reaction conditions, Heating and cooling of reactor systems, Heat exchanger devices as reactors, multiphase reactors. Batch processes - process yield, clean process technology for chemical reactors - Safety consideration in reactor design.

UNIT 3 CHOICE OF SEPARATOR & SEPARATION SYSTEMS - 1 12 Hrs. Separations of Heterogeneous & homogeneous fluid mixtures – Adsorption, Adsorbent selection, Reversible and irreversible adsorption, Design of adsorber. Liquid - Liquid separation - design of Decanters, hydro cyclones, extractors. Separation of dissolved components – Equipment selection, Design of Evaporators, Crystallizers.

UNIT 4 CHOICE OF SEPARATOR & SEPARATION SYSTEMS - 2 12 Hrs. Basic principles of distillation column design - Plate hydraulic design, Design of packed columns, Choice of column, height determination by cornell’s method, Column Auxillaries, Distillation Sequencing - using simple column, columns with more than two products thermal coupling - clean process technology for process operations.

UNIT 5 HEAT EXCHANGER NETWORK & UTILITIES – ENERGY TARGETS 12 Hrs. Heat Transfer Coefficients and Pressure Drops for Shell-and-Tube Heat Exchangers, Temperature Differences in Shell-and-Tube Heat Exchangers, Allocation of Fluids in Shell-and-Tube Heat Exchangers, Condensers, Reboilers and Vaporizers, Other Types of Heat Exchange Equipment Heat recovery pinch, The Problem table Algorithm, Utilities Selection, Energy targets capital & total Cost targets -Number of Heat Exchanger Units, Area Targets, Number of Shells Targets, Capital Cost Targets, Total Cost Targets.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Douglas, J.M., Conceptual Design of Chemical Process,2nd Edition, McGraw Hill, 1988. 2. Sinnot. R.K., Chemical Process Design, 2nd Edition, Butterworth-Heinemann, 2012. 3. Smith, R., Chemical Process: Design & Integration,2nd Edition, John Wiley & sons Ltd., 2005 4. Uday V. Shenoy Heat Exchanger Network Synthesis: Process Optimization by Energy and Resource Analysis, 1 st Edition

Gulf Professional Publishing, 1995


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SCH6531 CHEMICAL ENGINEERING LABORATORY L T P C Total Marks 0 0 6 3 100

1. Determination of the number of theoretical plate’s equivalent to packed column height (HETP) using Fenske’s equation and McCabe – Thiele method for the Methanol-Water system.

2. Verification of the principle of immiscible liquid mixture and determination of the vaporization and thermal efficiencies of Aniline-Water system.

3. Determination of the principle involved in a packed bed absorption column and to absorb CO2 from CO2-Air mixture using NaOH solution.

4. Calculation of the Drying time for removing moisture content from Ragi using Rotary dryer. 5. Residence Time Distribution of Mixed Flow Reactor 6. Combined Reactors (MFR followed by PFR) 7. Combined Reactors (PFR followed by MFR) 8.Adiabatic Reactor 9.Packed bed Catalytic Reactor

SCH6532 COMPUTATIONAL LABORATORY L T P C Total Marks 0 0 6 3 100

1. Solving Chemical Engineering Problems by using MATLAB and SPREAD SHEET

SCH6533 ENVIRONMENTAL ENGINEERING LABORATORY – I

L T P C Total Marks 0 0 6 3 100

1. Measurement of pH and Conductivity 2. Measurement of Total Dissolved salts 3. Estimation of Alkalinity 4. Estimation of Hardness by EDTA method 5. Estimation of Residual Chlorine. 6. Estimation of Optimum Coagulant Dose by Jar Test 7. Estimation of Ammonia Nitrogen 8. Estimation of Sulphate 9. Estimation of Chlorides 10. Estimation of D.O. by Wrinkler's methods 11. Estimation of Suspended, Settleable, Volatile and fixed solids. 12. BOD test for water and waste water. 13. COD test for water and waste water. 14. Determination of Turbidity by using Nephelometer. 15. Sampling and analysis of air pollutants ambient and stacks (SPM, RPM, SO2, NOX and CO). 16. Physiochemical analysis of solid wastes.

SCH6534 REMOTE SENSING AND GIS LABORATORY L T P C Total Marks 0 0 6 3 100

1. Creation of coverage and adding features by digitization 2. Editing map elements, cleaning, building and transportation 3. Attribute data entry and manipulation 4. Data analysis, overlay, buffer and map conversion 5. Grid analysis 6. AML Programming using basic commands 7. Introduction to Arc GIS modules 8. Case studies.

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SCH5106 ADVANCED TRANSPORT PHENOMENA L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The objective of this course is for the student to gain an enhanced understanding of transport phenomena

andsolve problems involving transports of momentum, energy and mass in chemical systems using a unified approach.

UNIT 1 INTERPHASE TRANSPORT IN ISOTHERMAL SYSTEMS 12 Hrs. Definition of Friction Factors, Friction Factors for Flow in Tubes, Pressure Drop Required for a Given Flow, Flow Rate for a Given Pressure Drop, Friction Factors for Flow around Spheres Determination of the Diameter of a Falling Sphere, Friction Factors for Packed Columns.

UNIT 2 MACROSCOPIC BALANCES FOR ISOTHERMAL FLOW SYSTEMS AND POLYMERIC LIQUIDS 12 Hrs. The Macroscopic Mass Balance , The Macroscopic Momentum Balance , The Macroscopic Mechanical Energy Balance , Estimation of the Viscous Loss , Power Requirement for Pipeline Flow , Use of the Macroscopic Balances for Steady-State, Pressure Rise and Friction Loss in a Sudden Enlargement , Isothermal Flow of a Liquid through an Orifice. Examples of the Behavior of Polymeric Liquids, Rheometry and Material Functions,Non-Newtonian Viscosity and the Generalized Newtonian Models ,Laminar Flow of an compressible Power-Law Fluid in a Circular Tube , Flow of a Power-Law Fluid in a Narrow Slit , Tangential Annular Flow of a Power- Law Fluid , Elasticity and the Linear Viscoelastic Models, Molecular Theories for Polymeric Liquids.

UNIT 3 INTERPHASE TRANSPORT IN NONISOTHERMAL SYSTEMS 12 Hrs. Definitions of Heat Transfer Coefficients, Calculation of Heat Transfer Coefficients from Experimental Data , Analytical Calculations of Heat Transfer Coefficients for Forced Convection through Tubes and Slits , Heat Transfer Coefficients for Forced Convection in Tubes , Design of a Tubular Heater , Heat Transfer Coefficients for Forced Convection around Submerged Objects , Heat Transfer Coefficients for Forced Convection through Packed Beds , Heat Transfer Coefficients for Free and Mixed Convection, Heat Loss by Free Convection from a Horizontal Pipe , Heat Transfer Coefficients for Condensation of Pure Vapors on Solid Surfaces.

UNIT 4 MACROSCOPIC BALANCES FOR NONISOTHERMAL SYSTEMS 12 Hrs. The Macroscopic Energy Balance, The Macroscopic Mechanical Energy Balance, Use of the Macroscopic Balances to Solve Steady-State Problems with Flat Velocity Profiles, The Cooling of an Ideal Gas , Mixing of Two Ideal Gas Streams, Parallel- or Counter-Flow Heat Exchangers, Flow of Compressible Fluids through Head Meters.

UNIT 5 INTERPHASE TRANSPORT IN NONISOTHERMAL MIXTURES 12 Hrs. Definition of Transfer Coefficients in One Phase, Analytical Expressions for Mass Transfer Coefficients, Correlation of Binary Transfer Coefficients in One Phase, Evaporation from a Freely Falling Drop, Mass Transfer in Creeping Flow through Packed Beds, Mass Transfer to Drops and Bubbles, Definition of Transfer Coefficients in Two Phases, Determination of the Controlling Resistance, Estimation of the Interfacial Area in a Packed Column, Estimation of Volumetric Mass Transfer Coefficients.

Max. 60 Hours TEXT / REFERENCE BOOKS 1. Bird R.B., Stewart, W. E. and Lightfoot, E. N., Transport Phenomena, 2nd Edition,John Wiley and Sons, 2007. 2. Welty, J.R., Wicks, C. E. and Wilson, R. E., Fundamentals of Momentum, Heat Mass Transfer, 5th Edition , John Wiley and

Sons, 2010. 3. Brodkey, R. S. and Hershey, H. C., Transport Phenomena – A Unified Approach,3rd Edition Brodkey Publishing, 2004 4. John C. Slattery, Advanced Transport Phenomena, 2nd Edition ,Cambridge University Press,1999.


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SCH5107 ADVANCED PROCESS CONTROL L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To familiarize the students with various advanced theories in process control, different types of controllers and

control strategies in real time systems and z transforms for digital signal processing.

UNIT 1 ADVANCED CONTROL STRATEGIES 12 Hrs. Cascade control, Feed forward control, Ratio control , Selective and Split-Range control, Dead time compensator – the Smith predictor, Override Control, Adaptive and Inferential Control System

UNIT 2 INTERNAL MODEL CONTROL 12 Hrs. Introduction to Model-Based Control. Practical Open-Loop Controller Design. Generalization of the Open-Loop Control Design Procedure. Model Uncertainty and Disturbances. Development of the IMC Structure. IMC Background. The IMC Structure. The IMC Design Procedure. Effect of Model Uncertainty and Disturbances.

UNIT 3 MULTIVARIABLE PROCESSES 12 Hrs. Control loop interaction - General Pairing Problem, Relative Gain Array (RGA), Properties, Application and Sensitivity of RGA. Multivariable control – Zeros and Performance Limitations, Directional Sensitivity and Operability, Decoupling

UNIT 4 SAMPLING AND THE Z-TRANSFORMS 12 Hrs. Sampling Continuous Signals. The Impulse Sampler,The Reconstruction of Continuous Signals , Types of Hold-Elements and Their Characteristics,Converting Continuous to Discrete-Time Systems. The z-Transform and Its Properties, The z-Transform of Some Basic Functions,The Inversion of z-Transforms,The Relationship Between Laplace and z-Transforms.

UNIT 5 SAMPLED-DATA SYSTEMS 12 Hrs. The Pulse Transfer Function of a Continuous Dynamic System,The Transfer Function of Discrete-Time Dynamic Systems, The Equivalence Relationship between Continuous and Discrete Time Dynamic Systems,Conditions for Stability of Sampled-Data Systems,The Effect of Sampling on the Closed-Loop Response of Sampled-Data Systems,The Design of Sampled-Data

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Bequette, B. Wayne. Process Control: Modeling, Design, and Simulation,7th Edition, Prentice Hall PTR, 2003. 2. George Stephanopoulos, Chemical Process Control, 2nd Edition, Prentice Hall of India Pvt. Ltd., 1990 3. William L.Luyben, Process Modeling, Simulation and Control For Chemical Engineers, 2nd Edition, McGraw Hill International

Editions,1990. 4. Thomas E. Marlin, Process Control: Designing Processes and Control Systems for Dynamic Performance, 2nd Edition,

McGraw Hill,2000


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SCH6531 CHEMICAL ENGINEERING LABORATORY L T P C Total Marks 0 0 6 3 100

1. Determination of the number of theoretical plate’s equivalent to packed column height (HETP) using Fenske’s equation and McCabe – Thiele method for the Methanol-Water system.

2. Verification of the principle of immiscible liquid mixture and determination of the vaporization and thermal efficiencies of Aniline-Water system.

3. Determination of the principle involved in a packed bed absorption column and to absorb CO2 from CO2-Air mixture using NaOH solution.

4. Calculation of the Drying time for removing moisture content from Ragi using Rotary dryer. 5. Residence Time Distribution of Mixed Flow Reactor 6. Combined Reactors (MFR followed by PFR) 7. Combined Reactors (PFR followed by MFR) 8.Adiabatic Reactor 9.Packed bed Catalytic Reactor

SCH6532 COMPUTATIONAL LABORATORY L T P C Total Marks 0 0 6 3 100

1. Solving Chemical Engineering Problems by using MATLAB and SPREAD SHEET

SCH6533 ENVIRONMENTAL ENGINEERING LABORATORY – I


1. Measurement of pH and Conductivity 2. Measurement of Total Dissolved salts 3. Estimation of Alkalinity 4. Estimation of Hardness by EDTA method 5. Estimation of Residual Chlorine. 6. Estimation of Optimum Coagulant Dose by Jar Test 7. Estimation of Ammonia Nitrogen 8. Estimation of Sulphate 9. Estimation of Chlorides 10. Estimation of D.O. by Wrinkler's methods 11. Estimation of Suspended, Settleable, Volatile and fixed solids. 12. BOD test for water and waste water. 13. COD test for water and waste water. 14. Determination of Turbidity by using Nephelometer. 15. Sampling and analysis of air pollutants ambient and stacks (SPM, RPM, SO2, NOX and CO). 16. Physiochemical analysis of solid wastes.

SCH6534 REMOTE SENSING AND GIS LABORATORY L T P C Total Marks 0 0 6 3 100

1. Creation of coverage and adding features by digitization 2. Editing map elements, cleaning, building and transportation 3. Attribute data entry and manipulation 4. Data analysis, overlay, buffer and map conversion 5. Grid analysis 6. AML Programming using basic commands 7. Introduction to Arc GIS modules 8. Case studies.

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SCH5201 PROCESS MODELING AND SIMULATION L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To impart to the student knowledge on modeling and simulation, classification of mathematical models, steady

and unsteady state lumped and distributed systems and other modeling approaches

UNIT 1 INTRODUCTION 12 Hrs. Introduction to modeling and simulation, classification of mathematical models, application of mathematical model, the role of models in process system engineering, model characteristics, a systematic approach in model building, conservation equations and auxiliary relations.

UNIT 2 STEADY STATE LUMPED SYSTEMS 12 Hrs. Degree of freedom analysis, single and network of process units, systems yielding linear and non-linear algebraic equations, flow sheeting – sequential modular and equation oriented approach, tearing, partitioning and precedence ordering, solution of linear and non-linear algebraic equations.

UNIT 3 UNSTEADY STATE LUMPED SYSTEMS 12 Hrs. Analysis of liquid level tank, gravity flow tank, jacketed stirred tank heater, reactors, flash and distillation column, solution of ODE initial value problems, matrix differential equations, simulation of closed loop systems.

UNIT 4 STEADY STATE DISTRIBUTED SYSTEM 12 Hrs. Introduction to steady state distributed system. Analysis of compressible flow, heat exchanger, packed columns, plug flow reactor, solution of ODE boundary value problems.

UNIT 5 UNSTEADY STATE DISTRIBUTED SYSTEM 12 Hrs. Analysis laminar flow in pipe, sedimentation, boundary layer flow, heat exchanger, heat transfer in packed bed, diffusion, packed bed adsorption, plug flow reactor, hierarchy in model development, classification and solution of partial differential equations - Empirical modeling, parameter estimation, population balance and stochastic modeling.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Ramirez, W., Computational Methods in Process Simulation, 2 nd Edition.,Butterworths, 2000. 2. Luyben, W.L., Process Modelling Simulation and Control,5th Edition, McGraw-Hill Book Co., 1973. 3. Felder, R. M. and Rousseau, R. W., Elementary Principles of Chemical Processes, 3rd Edition,John Wiley, 2000. 4. Franks, R. G. E., Mathematical Modelling in Chemical Engineering, John Wiley, 1967. 5. Balu. K,Padmanabhan. K, Modeling and Analysis of Chemical Engineering Processes, 1st Edition, I. K. International Pvt

Ltd,2007


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SCH6535 CHEMICAL PROCESS SIMULATION LABORATORY


1. Introduction to software (flow sheeting) 2. Simulation of flash drum 3. Simulation of distillation columns 4. Simulation of absorption columns 5. Simulation of Reactors 6. Simulation of Heat Exchangers. 7. Simulation of Pumps and Compressors 8. Simulation of Mixers 9. Simulation of Evaporators 10. simulation of Ethylene Glycol from Ethylene oxide

SCH6536 ENVIRONMENTAL ENGINEERING LABORATORY – II


1. Microbial analysis of soil & water i) Media preparation. ii) Sterilization. iii) Culturing techniques and growth curve determination. iv) Enumeration of total heterophobic microbial population in soil and water. v) Determination of coli forms in water by MPN

2. Determination of toxic pollutants in effluents. i) Determination of phenol. ii) Determination of heavy metals.

3. Determination of soil N, P, K analysis.

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SCH5601 ADVANCED THERMODYNAMICS L T P Credits Total Marks 3 1 0 4 100

COURSE OBJECTIVE This subject implies in-depth knowledge and advanced concepts of Thermodynamics for multicomponent systems

routinely used in the industrial calculations and comparisons.

UNIT 1 BASIC CONCEPTS 12 Hrs. Energy and first Law; Reversibility and second Law; Review of Basic Postulates, equilibrium criteria, Legendre Transformation and Maxwell’s relations

UNIT 2 STABILITY AND PHASE TRANSITION 12 Hrs. Stability of thermodynamic systems, first order phase transitions and critical phenomenon, phase rule, single component phase diagrams, thermodynamic properties from volumetric and thermal data

UNIT 3 MULTICOMPONENT MIXTURES 12 Hrs. Partial molar properties, fugacities in gas and liquid mixtures, activity coefficients, Ideal and Non-ideal solutions, Gibbs-Duhem equation, Wilson, NRTL, and UNIQUAC equations, UNIFAC method.

UNIT 4 PHASE EQUILIBRIUM 12 Hrs. VLE - Equations of state, corresponding states, Henry’s Law, lattice theory, criticality, high pressure VLE. Other phase equilibriums- SLE/LLE/VLLE.

UNIT 5 CHEMICAL EQUILIBRIUM 12 Hrs. Homogeneous gas and liquid phase reactions, heterogeneous reactions – phase and chemical equilibrium. Tutorials for application of principles.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Rao.Y.V.C., Chemical Engineering Thermodynamics,4th Edition, University Press,2005 2. Tester. J. W. and M. Modell, Thermodynamics and Its Applications, 3rd Edition. Prentice Hall,1997. 3. Prausnitz, J.M., Lichtenthaler R.M. and Azevedo, E.G., Molecular thermodynamics of fluid-phase Equilibria, 3rd Edition,

Prentice Hall Inc., 1999


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SCH5602 ENERGY AUDIT AND CONSERVATION IN

PROCESS INDUSTRIES L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The subject addresses use of methods in industrial process energy usage, energy audit and regulations that

contribute to sustainable development.

NIT 1 SAFETY MANAGEMENT 12 Hrs. Introduction to Resources Management, Clean Development Mechanism, Command and control and Market Based Initiatives for pollution control. Safety Review, Preconditions and preparations, analytical procedures, Integrated approaches for safety management, Case studies in process safety management

UNIT 2 POLLUTION ABATEMENT IN INDUSTRIES 12 Hrs. Pollution Abatement in Process Industries Types of pollution in process industries, Modes of Surveillance Evaluation and Techniques for abatement. Design for effluent treatment in specific process Industries such as, Fertilizer, Petroleum, Pulp and Paper,Dairy etc.

UNIT 3 ENVIRONMENTAL ISSUES 12 Hrs. Environmental Issues in Process Industries ,Identifying and evaluating the probable environmental consequences of a proposed development project, Methods for Environmental Impact Assessment, Risk Assessment of the project. Uses, advantages and limitations of various environmental management tools. Case studies of Life cycle Assessment, Environmental Audit, Energy Audit and Water Audit.

UNIT 4 ENVIRONMENTAL REGULATIONS FOR SAFETY 12 Hrs. Environmental Regulations: Indian & International -Regulations to encourage pollution prevention and cleaner production. International standards on various aspects of environmental management, Process Design Practices -Chemical Process Industry (CPI) Safety Codes. Control technology to reduce accidents in CPI.

UNIT 5 HAZARD EVALUATION AND ANALYSIS 12 Hrs. Process Hazard Evaluation - Hazard Evaluation techniques, Qualitative Risk Analysis (QRA) Techniques, Risk Assessment (RA) accident probability, Hazard Operability Studies (HAZOP) Hazard Analysis (HAZAN), Fault Tree Analysis (FTA) and Event Tree Analysis (ETA) analysis of safety related information and safety measures.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Janes K. Lein,Integrated Environmental Planning, 2nd Edition , Blackwell Publishing,1990 2. Steinbach.J, Safety Assessment for Chemical Proces,,3rd Edition,Willey – VCT,1994


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SCH5603 ADVANCED PETROLEUM REFINING PROCESSES

L T P Credits Total Marks 3 1 0 4 100

COURSE OBJECTIVE To understand the advanced petroleum processing and advanced concepts of refining operations to derive the

targeted derivatives and specific finished products.

UNIT 1 CRACKING 12 Hrs. Thermal Cracking Introduction, Thermal Cracking, Visbreaking, Coking, Delayed Coking, Fluid Coking and Flexicoking Catalytic Cracking Introduction, Fixed Bed Processes, Moving Bed processes, Fluid Bed processes, Reaction chemistry of FCC, Mechanism and Kinetics, Process Variables: Feedstock Quality, Feedstock Preheating, Feedstock Pressure, Feedstock Conversion, Reactor Temperature, Recycle Rate, Space Velocity, Catalyst Activity, Catalyst Oil Ratio, Regenerator Temperature, Regenerator Air Rate. Catalysts for Cracking

UNIT 2 HYDROTREATING 12 Hrs. Introduction, Hydrodesulfurization: Process configuration, Reaction chemistry and Kinetics, Downflow Fixed Bed Reactor, Upflow expanded Bed Reactor, Demetallization Reactor (Guard Bed Reactor), Catalysts. Distillate Hydrosulfurization, Residuum Hydrodesulfurization, Ultra low sulfur Diesel.

UNIT 3 HYDROCRACKING 12 Hrs. Introduction, Processes and Process Design: Reaction chemistry and Kinetics, CANMET, Gulf HDS, H-G Hydrocracking, H-Oil. IFP Hydrocracking, Isocracking, LC fining, MAK, HDC, Microcat RC, Mild Hydrocracking, MRH, RCD, Unibon (BOC), Residfining, Residue Hydroconversion, Unicrackking, Veba, Combi-Cracking

UNIT 4 PRODUCT IMPROVEMENT 12 Hrs. Desulfurization and Heteroatom Removal: Hydrotrating, Hydrogen Sulfide Removal Reforming: Thermal Reforming, Catalytic reforming, Dehydrogenation, Catalysts, Reformulated Gasoline and other oxygenates like MTBE and others.Isomerization, Alkylation and Polymerization Process Types, Chemistry, Commercial Processes, Catalysts

UNIT 5 HYDROGEN PRODUCTION AND FUELCELLS, 12 Hrs. Introduction, Feedstocks, Process Chemistry, Commercial Processes: Heavy Residue Gasification and Combined Cycle Power Generation, Hybrid Gasification Process, Hydrocarbon Gasification, Hypro Process, Shell Gasification (Partial Oxidation) Process, Steam Methane Reforming, Steam Naphtha Reforming, Synthesis Gas Generation, Texaco Gasification (Partial Oxidation) Process. Catalysts, Hydrogen Purification and Fuelcells.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Rao .B.K.B,Modern Petroleum Refining Processes,4th Edition, Oxford & IBH Publishing Pvt. Ltd 2006 2. Nelson.W.L, Petroleum Refinery Engineering,3rd Edition, McGraw-Hill International,2005 3. Sarkar.G.N, Advanced Petroleum Refining,4th Edition, Khanna Publishers,2004 4. Ram Prasad, Petroleum Refining Technology, 4th Edition Khanna Publishers,2003


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SCH5604 CHEMICAL PROCESS ECONOMICS &

MANAGEMENT L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To implement with a great deal of scientific-technical knowledge that is integrated with knowledge

of economics, management in project preparation, and execution.

UNIT 1 INTRODUCTION 12 Hrs. General reMarks on process plant design. Project-small size plants, medium size plants and large scale plants. Demands on project engineers, Overview of activities-project planning and project execution

UNIT 2 PROJECT PLANNING 12 Hrs. Product development, Plant type: Location kind of premises. Capacity availability lifespan, Degree of automation, Legal requirements, Costs, Investment, Operating costs. Inquiry/ Invitation to tender, Project controlling, Plant manufacturer: Risk analysis, Basic engineering, Process development, Balancing, Basic and process flow diagram, Materials concept, Main apparatus, Layout, Quotation, Quotation price, Contract negotiations

UNIT 3 CONTRACT 12 Hrs. Order basis, Regulations, Labour employment, Subcontractors, Project documentation, Technical part, Contractor’s scope of supply and services, Employer’s scope of supply and services, Commercial part: Deadlines penalties, Warranties penalties, Defects acceptance, Prices terms of payment bonds, Alterations claims, Terminations/suspension, Insurance, Secrecy, Severability clause, Coming into effect, Signature policy

UNIT 4 PROJECT MANAGEMENT 12 Hrs. Project Planning and Scheduling, Schematic Representation of Project Management, Pitfalls in Project Planning, Milestones and Milestone Planning, Work Breakdown Structure (WBS), Gantt Chart, Hierarchical Plan, Project Network, Activity Floats, Programme Evaluation & Review Technique (PERT), Critical Path, Project Control, Decision Making, Project Reporting, Project Meetings, Project Failure and Success. How Public Investment in Projects is initiated in India? Steering Committee, Tender Committee, Joint Venture Organizations, Main Contributing Factors For Successful Projects, Management of Projects, Project Management Consultants (PMCs). Orientation, Indian Individuality, Organization Management Functions, Project Management Team, Desirable Characteristics, Competencies of Project Manager, Duties of A Project Manager, Project Team, Problem Areas of Concern.

UNIT 5 PROJECT EXECUTION 12 Hrs. Project organization: Project structures, Systematic, Project manual, Correspondence system, Revision service, Cost monitoring, Time scheduling/monitoring of dates, Computers in plant manufacturing. Approval planning, Component procurement, Piping and instrumentation diagrams, Electrical, Measurement and Control engineering, Layout and building design, Layout design, Building design, Piping planning, Documentation, Erection, Commissioning

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Frank Peter Helmus,Process Plant Design – Project Management from Inquiry to Acceptance,3rd Edition Wiley-VCH Verlag

GmbH & Co., 2008 2. Sivasubramanian.v, Process Economics And Industrial Management,1st Edition, galgotia publication,2002.


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SCH 5605 MEMBRANE SEPARATION TECHNOLOGY L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To gather collective information and principles of membrane types and modules, selectivity and advanced

membrane separation processes in large scale applications.

UNIT 1 INTRODUCTION 12 Hrs. Historical Development of Membranes, Types of Membranes – Processes, Membrane Transport Theory - Solution diffusion Model, Pore flow Model, Boundary Layer Film Model, Determination of the Peclet number, Concentration Polarization in Liquid and Gas Separation Processes.

UNIT 2 MEMBRANES AND MEMBRANE MODULES 12 Hrs. Isotropic Membranes – Isotropic Micro Porous and Isotropic Non Porous membranes, Anisotropic Membranes, Metal Membranes, Ceramic Membranes, Zeolite membranes, Liquid Membranes, Hollow Fiber Membranes - Membrane Modules- Plate and frame modules, Tubular modules, Spiral wound modules, Hollow fibre modules, selection.

UNIT 3 MEMBRANE PROCESSES – 1 12 Hrs. Reverse Osmosis - Cellulosic Membranes, Noncellulosic Polymer Membranes, Interfacial Composite Membranes, Other Membrane Materials, Microfiltration and Ultrafiltration - Principle, Membranes and Materials, Membrane Selectivity, Modules, Concentration Polarization, Membrane Fouling and Cleaning - System Design.

UNIT 4 MEMBRANE PROCESSES – 2 12 Hrs. Pervaporation, Dialysis, Electrodialysis - Principle, Theory, Membrane Materials and Structure, Process Design, Chemistry of Ion Exchange Membranes, Homogeneous membranes, Heterogeneous membranes, Transport in Electrodialysis Membranes – Concentration polarization and limiting current density, current efficiency and Power consumption, System design and Applications.

UNIT 5 APPLICATIONS OF MEMBRANE TECHNOLOGY 12 Hrs. Medical applications - Hemodialysis, Blood Oxygenators, Controlled Drug Delivery, Biodegradable systems, Osmotic systems. Applications of Membrane Reactor, Ion-conducting Membrane Reactors, Membrane Contactors and Membrane Distillation, Diffusion Dialysis and Piezodialysis.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Richard W. Baker, Membrane Technology and Applications, 3rd Edition John Wiley & Sons, , 2012. 2. Seader, Ernest, Roper, Separation Process Principles, 4th Edition,John Wiley & Sons, 2010. 3. Kaushik Nath, Membrane Separation Process,4th Edition, PHI, 2008. 4. Mulder. M, Basic principles of membrane Technology, 2nd Edition, Kulwer Academic Publishers 1996. 5. Scott & Hughes, Industrial Membrane Separation Technology, 3rd Edition Blackie Academic & Professional, 1996.


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SCH5606 CORROSION IN INDUSTRY & ITS CONTROL L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To develop fundamental knowledge in the theory of corrosion of materials in industry and to study the control

measures of corrosion in different contexts.

UNIT 1 BASIC ASPECTS 12 Hrs. Introduction, classification, economics, emf series, Galvanic series. Corrosion theories: derivation of potential – current relationships of activation controlled and diffusion controlled corrosion processes. Potential – pH diagrams Fe-H2O system, application and limitations. Passivation-definition, anodic passivation theory of Passivation.

UNIT 2 FORMS OF CORROSION 12 Hrs. Definition, factors and control methods of various forms of corrosion: uniform, galvanic, pitting, inter granular, crevice, dezincification, stress corrosion, corrosion fatigue, hydrogenembrittlement.

UNIT 3 TMOSPHERIC CORROSION AND PROTECTIVE COATINGS 12 Hrs. Atmospheric corrosion – classification, factors influencing atmospheric corrosion, temporary corrosion preventive methods; organic coating – surface preparation, natural, synthetic resin, paint formulation and applications. Paint testing and evaluation.

UNIT 4 IMMERSION CORROSION AND ELECTROCHEMICAL PROTECTION 12 Hrs. Corrosion in immersed condition: effect of dissolve gases, salts, pH, temperature and flow rates of corrosion; marine corrosion. Underground corrosion – corrosion process in the soil, factors influencing soil corrosion, Biological corrosion definition, mechanism of biological corrosion control of bio corrosion. Electrochemical methods of protection theory of cathodicprotection, design of cathodicprotection, sacrificial anodes, impressed current anodes, anodic protection. Corrosion inhibitors for acidic, neutral and alkaline media, cooling water system - boiler water system. Corrosion resistant alloys.

UNIT 5 CORROSION MONITORING 12 Hrs. Modeling corrosion processes. Accelerated chemical tests for studying different forms ofcorrosion.Electrochemical methods of corrosion rate measurements by Gravimetric, Tafelpolarization, linear polarization, cyclic polarization, impedence spectroscopy, harmonics and NDT techniques- ultrasonics, radiography eddy current.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Banerjee S.N An Introduction to Corrosion Science and Corrosion Inhibition, 2nd Edition,Oxonian Press P.Ltd., 1985. 2. Zaki Ahmad, Principles of Corrosion Engineering & Corrosion Control,3rd Edition, ButterworthHeinemann, 2006. 3. Fontana M.G, Corrosion Engineering, 4th Edition,Tata McGraw Hill, 2005. 4. Shrier L.L, Corrosion, Vol. I & II, Butterworth Heinemann, 1994. 5. Uhlig H.H and Revie R.W, Corrosion and Corrosion Control, 3rd Edition, A Wiley – Inter Science Publication John Wiley &

Sons,1985.


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SCH5607 ADVANCED NANOTECHNOLOGY L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE This course covers the entire spectrum of nano materials ranging from overview, synthesis, properties, and

characterization to fabrication and its recent developments.

UNIT 1 INTRODUCTION 12 Hrs. Nanoscale Science and Technology- Implications for Physics, Chemistry, Biology and Engineering-Classifications of nano structured materials- nano particles quantum dots, nanowires-ultra-thin films-multilayered materials. Length Scales involved and effect on properties: Mechanical, Electronic, Optical, Magnetic and Thermal properties.

UNIT 2 SYNTHESIS AND FABRICATION OF NANOMATERIALS 12 Hrs. Bottom-up (building from molecular level) and top-down (breakdown of microcrystalline materials) approaches. Preparation of nano scale metal oxides, metals, Carbon nanotube(CNT), functionalized nano porous adsorbents, nano composite- Chemical vapour deposition (CVD), Sol gel, Sonochemical, Microwave, Solvothermal, Plasma, Pulsed laser abalation, Magnetron sputtering, Electrospinning.

UNIT 3 CHARACTERISATION OF NANOMATERIALS 12 Hrs. Instrumentation for Nanoscale Characterization- Scanning electron microscope (SEM), Transmission electron microscope (TEM), X-RAY DIFFRACTION (XRD), Fourier transform infra –red (FTIR), Atomic force microscopy (AFM), Scanning probe microscopy (SPM),Scanning tunneling microscopy (STM) for characterization of properties .Limits of each technique.

UNIT 4 NANO-BIOTECHNOLOGY 12 Hrs. Biologically-Inspired Nanotechnology- Basic biological concepts and principles that may lead to the development of technologies for nanoengineering systems. molecular nanoscale engineered devices, nanoscale biotechnologies, nano products-BIO CHIPS, BIOMACROMOLECULES –DRUG DELIVERY SYSTEMS, BIOLOGICAL MEMBRANES etc.

UNIT 5 ENVIRONMENTAL APPLICATIONS 12 Hrs. Applications in Micro and Nano technology including, Micro fluidics, Micro Electron Mechanical Systems (MEMS), Nanoelectromechanical systems (NEMS), Gas sensors, and Lab on chip (LOC), catalytic and photocatalyic applications, Nano materials for ground water remediation, adsorbents, membrane processing applications.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Wilson.M, Smith K.K.G, Simmons.M and Raguse B; Nanotechnology,3rd Edition, Chapman & Hall,1998 2. Glen E Fryxell and Guozhong Cao,Environmental applications of nanomaterials-Synthesis, Sorbents and Sensors,3rd

Edition, worldscibooks,2001 3. Mark Wisener, Jeo Yues Bolteru, Environmental nanotechnology,5th Edition,McGraw Hill,2007 4 RaoC.N.R, Mulller, Cheetham A.K, The Chemistry of Nanomaterials, Sysnthesis, Properties and applications,5th Edition,

WILEY-VCH Verlag GmbH & Co,2004


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SCH5608 PROCESS HEAT TRANSFER L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE This aim of the course is to introduce the phenomena of heat transfer and to provide useful information on the

performance and design of particular processes.

UNIT 1 INTRODUCTION AND IMPORTANCE OF HEAT TRANSFER 12 Hrs. Introduction and importance of the subject, Relevance of subject in industrial environment, Techniques of heat transfer, Heat transfer under Steady and Un-steady state conduction. One dimensional and two dimensional concept, Dissipation of energy in industry, Concept of flow patterns and its uses in industry, Analogy between momentum and heat transfer. Colburn and Reynolds analogy, Application of analogy equations in free and forced convection.

UNIT 2 HEAT TRANSFER APPLICATIONS TO FLUID MECHANICS 12 Hrs. Comparative study of Newtonian and non‐Newtonian fluid in context with heat transfer, Newtonian and non‐Newtonian heat transfer in circular tube, coils and other configuration, Non‐Newtonian heat transfer in PFR, CSTR, Concept of vibrating / oscillating heat transfer. Concept of multi phase flow, Concept of flow patterns and gas hold up in multi‐phase flow, Spouted bed heat transfer, Concept of semi-fluidization and its industrial use Design of fluidized bed boiler and other related equipments.

UNIT 3 HEAT EXCHANGER DESIGN AND APPLICATIONS 12 Hrs. Design concept of heat exchanger, Concept of LMTD method and its merits & demerits, Use of LMTD technique in designing heat exchangers, Range and Approach, Use of Correction factor Charts in multi-pass heat exchangers, Recuperators and regenerators, Condensers types Shell type, Direct contact type, finned type , plate and parallel etc.

UNIT 4 COMPARITIVE STUDIES ON HEAT EXCHANGER 12 Hrs. Purpose of introducing NTU techniques, NTU approach in Parallel and Counter-flow heat exchanger, its merits & demerits over LMTD method, Comparative design of double pipe heat exchanger, shell & tube heat exchanger, Single and Multi-Pass heat exchangers, Plate type, re-boilers, oscillating heat exchanger. Heat recovery pinch.

UNIT 5 HEAT TRANSFER APPLICATIONS IN REACTION KINETICS 12 Hrs. Mechanisms of heat transfer in packed bed reactor, fluidized bed reactor and moving bed reactor, heat transfer in dilute phase transport, application of basic heat transfer equation in design. Use of heat transfer in furnaces, pipe still, thermo siphoning and other chemical industries.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Knudson D.G. and Katz D.L., Fluid dynamics & heat transfer, 2nd Edition,Mc Graw Hill,1958 2. Hewitt G F, Shires G L, Bott T R, Process heat transfer, 4th Edition, CRC process,1994 3. Harison & Davidson, Fluidization engineering, 2nd Edition, Mc Graw Hill,1968


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SCH5609 ADVANCED BIOCHEMICAL ENGINEERING L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The aim of the course is to study the advanced concepts regarding the system behavior and apply principles of

biochemical engineering to the design, development, and analysis of processes that use biocatalysts.

UNIT 1 BATCH AND CONTINUOUS CULTURES 12 Hrs. Batch and Continuous Cultures,Growth Rate: The Kinetics of Cell Growth,Measurement of Cell Growth,Effects of Environment on Cell Growth,Temperature,pH,Oxygen, Oxygen Uptake Rate (OUR), Medium requirements for fermentation processes- Carbon, nitrogen, minerals, vitamins and other complex nutrients; Medium formulation for optimal growth and product formation- examples of simple and complex media; Design of commercial media for industrial fermentations, medium optimization methods

UNIT 2 MICROBIAL GROWTH 12 Hrs. Microbial Growth, Phases of cell growth in batch cultures, Microbial Growth Kinetics, The Stoichiometry of Microbial Reactions,Medium Formulation and Yield Factors,Material Balance of Cell Growth,Degree of Reduction, Fed Batch Culture,Fed-Batch Model Formulation, Comparison Between Fed-Batch and Continuous Bioreactors, Advantages of Fed-Batch System, Application of Fed-Batch System

UNIT 3 MIXING AND MASS TRANSFER 12 Hrs. Mixing and Mass Transfer, Macro-mixing, Micro-mixing, Methods for Characterising Mixing, Oxygen Transfer,Gas-Liquid Mass Transfer,Oxygen Transfer Rate,Oxygen Consumption in Cell Growth, Factors Affecting Cellular Oxygen Demand, Measurement of kla in Continuous-Stirred-Tank Bioreactor and Airlift Bioreactor,Continuous-Stirred-Tank Bioreactor,Airlift Bioreactor, Liquid Mixing,Types of Mixing and Stirrers Types of Flows in Agitated Tanks,The Mechanism of Mixing Power Requirement for Mixing ,Un-gased Newtonian Fluids, Un-gased non-Newtonian Fluids, Gased Fluids

UNIT 4 BIOCHEMICAL KINETICS 12 Hrs. Kinetics of Substrate Utilisation, Product Formation and Biomass Production in Cell Cultures, The kinetics of substrate consumption in cellular growth and enzyme-catalysed reaction and their relationship with bioreactor modelling,Unstructured Batch Growth Models,Structured Kinetic Models,Compartmental models,Metabolic models,Product Formation Kinetics, Unstructured model ,structured product formation,kinetic modelling, Microbial and enzyme kinetic models and their applications in bioreactor design, Sterilisation,Introduction , Applications ,Heat Sterilisation

UNIT 5 BIOREACTOR DESIGN 12 Hrs. Bioreactor Design,Downstream Processing in Biochemical Engineering, Introduction to downstream processing, Cell disruption methods for intracellular products, removal of insolubles, biomass separation techniques; flocculation and sedimentation, centrifugation and filtration methods, Solid-Liquid Separation, Filtration/Ultrafiltration, Centrifugation, Liquid-liquid Extraction, Cell Rupture/Disruption,Product Recovery,Purification, Solvent recovery, Drying, Crystallisation.

Max. 60 Hours TEXT / REFERENCE BOOKS 1 Pauline Doran, Bioprocess engineering principles, 1st Edition, Academic Press, 1995. 2. Arthur T. Johnson, Biological Process Engineering: An Analogical Approach to Fluid Flow, Heat Transfer, and Mass Transfer 3. Applied to Biological Systems,2nd Edition John Wiley and Sons, 1998. 4. Michael Shuler and FikretKargi, Bioprocess Engineering: Basic Concepts, 2nd Edition, Prentice Hall, 2002. 5. Bailey.J.Fand , Ollis.D.F, Biochemical Engineering Fundamentals, 2nd Edition, Mc-Graw Hill, Inc., 1986. 6. Stanbury P.E., Whitaker A., Hall S.J, Principles of Fermentation Technology, 2nd Edition, Pergamon Press, 1995. 7. Harvey W. Blanch, Douglas S. Clark, Biochemical Engineering, 2nd Edition, Marcel Dekker, Inc, 1997.


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SCH5610 ADVANCED PROCESS OPTIMIZATION L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To get a broad picture of the various applications of optimization methods used in Chemical Engineering used in

industries for design and production of products, both economically and efficiently.

UNIT 1 INTRODUCTION TO OPTIMIZTION 12 Hrs. Basic concept of optimization, formulation of optimization problems: Classification of optimization problems – single variable problems, multivariable problems with constraints, unconstrained one-dimensional search; analytical methods, numerical methods, scanning and bracketing techniques, region elimination methods.

UNIT 2 MULTIVARIABLE OPTIMIZATION 12 Hrs. Analytical methods: classification, stationary points, direct substitution, constrained variation, penalty function, Kuhn-Tucker theorem, quadratic programming (GP), Geometric programming, Numerical methods: general principles, convergent check, direct search, pattern search, acceleration in direct search, gradient methods, the complete method of box office.

UNIT 3 NONLINEAR PROGRMING (NLP) 12 Hrs. Constrained nonlinear programming (NLP) – Methods for multivariable constrained problems: Quadratic programming generalized reduced gradient methods, successive linear and successive quadratic programming, and integer & mixed integer programming.

UNIT 4 NON-TRADITIONAL OPTIMIZATION TECHNIQUES 12 Hrs. Statistical optimization techniques- Introduction, concepts, models and applications, Genetic Algorithm (GA), fitness function, GA operators, simulated annealing, Ant colony optimization, TABU search multi-OBJECTIVE optimization, artificial neural network and Fuzzy logic.

UNIT 5 APPLICATIONS OF OPTIMIZATION IN CHEMICAL ENGINEERING 12 Hrs. Optimization of staged and discrete processes, optimization of liquid-liquid extraction process, economic operation of fixed bed filter, flow sheet optimization, information flow in the design process, process simulators and optimization codes.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Edger T. F., Himmelblau D. M and Lasdon L. S., Optimization of Chemical Processes, 2nd Edition, McGraw- Hill, 2001. 2. Seider W. D., Seader J. D. and Lewin D. R., Product and Process Design Principles- Synthesis, Analysis, and Evaluation, 2nd

Edition, John Wiley and sons inc., 2008. 3. Singuresu S. Rao, Engineering Optimization- Theory and practice,3rd Edition, New Age International Publishers,1998 4. Gordon S. G. Beveridge and Robert S Schecter, Optimization Theory & Practice, 2nd Edition, McGraw- Hill, 1996


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SCH5611 ADVANCED INSTRUMENTAL METHODS OF

ANALYSIS L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To emphasize the principles of Instrumentation followed by the various instrumental techniques from molecular

levels used in the analytical methods for various industrial samples and products.

UNIT 1 INTRODUCTION TO INSTRUMENTAL ANALYSIS 12 Hrs. Classification of Analytical Methods – Classical and Instrumental Methods - Selection of an analytical method – Calibration of Instruments – Precision and Accuracy - Selectivity – Sensitivity – Detection Limit – Errors in measurement – Systematic Errors and Non systematic errors - Signals and Noise – Techniques involved in Noise Reduction.

UNIT 2 MOLECULAR SPECTROSCOPY 12 Hrs. Electromagnetic Radiation and its properties – Electromagnetic Spectrum – Louis De broglie Theory - Absorbance and Transmittance – Beer Lambert’s Law – Its Limitations – Theory behind Ultra Violet / Visible and Infra Red Spectroscopy - Instrumentation involved in UV/VIS and IR spectroscopy – Single beam and double beam spectrophotometers - Applications in Industry and R&D - Nuclear Magnetic Resonance Spectroscopy (NMR) – Basics and Principle Involved, Instrumentation and applications.

UNIT 3 ADVANCED SPECTROSCOPIC TECHNIQUES 12 Hrs. Principle, Instrumentation and applications of Atomic Absorption Spectroscopy (AAS) – Interferences in AAS – Pressure Broadening – Doppler Broadening – Zeeman Effect – Principle, Instrumentation and applications of Atomic Emission Spectroscopy (AES), SEM, TEM, AFM, XRD, particle analyzer Mass Spectroscopy - Theory, Types and Applications.

UNIT 4 ELECTROANALYTICAL TECHNIQUES 12 Hrs. Fundamentals of Electro Chemistry – Faradays Laws of electrolysis – Strong and weak electrolytes – Specific and equivalent conductance – Its Experimental determination - Ph – Conductance – Potentiometry – Cyclic Voltammetry – Coulometry – Theory behind Electrochemical Impedence Spectroscopy (EIS) and its applications – Polarography.

UNIT 5 CHROMATOGRAPHIC SEPARATION TECHNIQUES 12 Hrs. Fundamentals of Chromatography – Types of Chromatography – Working principle, Instrumentation and applications of Chromatographic techniques – Paper chromatography - Column Chromatography - Gas Chromatography – High Performance Liquid Chromatography – Ion Exchange Chromatography – Thin Layer Chromatography – Supercritical Fluid Chromatography – Affinity Chromatography – Gel Permeation Chromatograpy .

Max. 60 Hours TEXT / REFERENCE BOOKS 1. Willard, Merritt, Dean, Settle, Instrumental Methods of analysis, 7th Edition, Wadsworth , 1988. 2. Skoog , West, Holler, Analytical Chemistry, 7th Edition, HARCOURT ASIA PTE LTD, 2001. 3. Peter T. Kissinger, William R. Heineman , Laboratory Techniques in Electroanalytical Chemistry, 2nd Edition, CRC Press,

1996. 4. William Kemp, Organic Spectroscopy,3rd Edition, Palgrave Publishers, 2011. 5. Colin N. Banwell , Elaine M. Mccash , Fundamentals of Molecular Spectroscopy,4th Edn, Mc-Graw Hill Higher Education,

1994.


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SCH5612 PROJECT ENGINEERING OF PROCESS

PLANTS L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE The aim of the course is to study the basics of planning, selection, procurement of equipments, and the process

safety measures get involved in execution of the projects.

UNIT 1 INTRODUCTION 12 Hrs. Project definition, Scope of Project Engineering, Role of Project Engineer, Project Profile and standards, Feedback information (MIS), Evaluation and Modification, Selection, Criteria.

UNIT 2 PROJECT PLANNING 12 Hrs. Planning the process, Strategic and Managerial Planning, Organizing the process planning, cost and costing, Cost Control systems, Economic Balancing, Network Planning, Methods (PERT/CPM), Engineering Flow Diagrams, Cost requirements, Analysis and Estimation of Process Feasibilities (Technical/Economical) Analysis, Cost– Benefit Ratio Analysis, Project Budgeting, Capital Requirements, capital Market, Cash Flow Analysis, Break even strategies.

UNIT 3 PROJECT ENGINEERING 12 Hrs. Plant Engineering Management, OBJECTIVE, Programme, Control, Plant Location and Site Selection, Layout diagrams, Selection and procurement of equipment and machineries, Installation, Recommission, Commissioning and performance appraisal, Strategies choice and Influence, Product planning and development, Provision and maintenance of service facilities.

UNIT 4 ROCESS SAFETY 12 Hrs. Process safety, Materials safety and Handling regulations, Safety in equipment and machinery operations, Design considerations of safety organization and control, Pollution, Pollution control and Abatement, Industrial Safety Standard Analysis.

UNIT 5 REGULATIONS 12 Hrs. Government regulations on procurement of raw materials and its allocation. Export –Import regulations, Pricing policy, Industrial licensing procedure, Excise and other commercial taxes, Policies on depreciation and corporate tax, Labour laws, Social welfare legal measurements, Factory act, Regulations of Pollution Control Board.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Cheremisinoff, N. P., Practical Guide to Industrial Safety: Methods for Process Safety Professionals, 2nd Edition ,CRC Press,

2001 2. Couper, J. R., Process Engineering Economics, 3rd Edition,CRC Press, 2003. 3. Perry, J. H. Chemical Engineer’s Hand Book, 8th Edition, McGraw Hill,2007. 4. Peters, M. S., Timmerhaus, C. D. and West, R. E., Plant Design and Economics for Chemical Engineers, 5th Edition, McGraw

Hill, 2003. 5. Silla, H., Chemical Process Engineering: Design and Economics,3rd Edition, CRC Press, 2003. 6. Watermeyer, P., Handbook for Process Plant Project Engineers,4th Edition ,John Wiley and Sons, 2002.

ND SEMESTER EXAMINATION QUESTION PAPER PATTERN Max. Marks : 80 Exam Duration : 3 Hrs. PART A : 6 Questions of 5 Marks each – No Choice 30 Marks PART B : 2 Questions from each unit of internal choice, carrying 10 Marks each 50 Marks

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SCH 5613 ADVANCED FLUID DYNAMICS L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE Review and understand the continuity, momentum and energy equations and to develop problem solving skills in

areas of fluids-related engineering.

UNIT 1 INTRODUCTION 12 Hrs. Equation of continuity, equation of motion, Navier Stokes equation, Euler equation, Bernoulli equation, Momentum boundary layer theory (Laminar boundary theory & turbulent boundary layer theory), dimensionless number and its significance.

UNIT 2 NON‐NEWTONIAN FLUIDS 12 Hrs. Classification of fluid behavior, Laminar flow (Fluid with a yield stress)‐ Laminar flow in cylindrical tubes, Laminar flow between parallel plates, Laminar flow in annuli(Newtonian fluids Bingham Plastic Fluids), Laminar flow(fluids without a yield stress), Power law fluids, Compressible fluids : ‐ Flow through variable area‐conduits, Flow of gas through a nozzle or orifice (isothermal flow, non isothermal flow).

UNIT 3 AGITATION AND MIXING 12 Hrs. Agitation of Liquids, Mixing mechanisms (Laminar mixing, Turbulent mixing), Circulation, Velocities in stirred tanks, Flow patterns in stirred tanks, Power consumptions in stirred vessels, Mixing Equipments (Impellers. Propellers Turbines, Extruders, Baffles).

UNIT 4 FLOW OF MULTIPHASE MIXTURES 12 Hrs. Two phase gas vapor liquid flow, horizontal and vertical flows of gas ‐ liquids, gas – solid mixtures, slip and hold up effects, phase separation and settling behavior ,pressure, momentum and energy relations, practical methods for evaluating pressure drop.

UNIT 5 MOTION IN THE FLUIDIZED BED 12 Hrs. Fluidization, behavior of the fluidized bed, minimum fluidization velocity, different types of fluidization, particulate fluidization, bubbling fluidization, semi fluidization, mixing and segregation in fluidized bed, application of fluidization.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Knudsen & Katz, Fluid Dynamics and Heat Transfer,2un Edition, McGraw Hill Book Co.,1974. 2. McCabe, Warren L., Smith, Julian C. and Harriot, P., Unit Operations of Chemical Engineering, 7th Edition McGraw Hill, 2005 3. Gupta, Santosh K., Momentum Transfer Operations,3rd Edition, Tata McGraw Hill, 1984. 4. Nevers Noel De., Fluid Mechanics for Chemical Engineering, 2nd Edition, McGraw Hill Inc., 1991. 5. Backhurst J.R., Harker J.H., Coulson J.F., Richardson J.M., ChemicalEngineering, Volume 1, 6th Edition ,Butterworth

Heinemann, 1999


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SCH5614 ADVANCED PROCESS INTEGRATION L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To acquire a deep and systematic conceptual understanding of the principles of process design and integration in

relation to the petroleum, gas and chemicals sectors of the process industries

UNIT 1 INTRODUCTION 12 Hrs. Introduction to Process Integration. Importance of Process Integration and applications in Chemical Industries. Overview of Process Integration.

UNIT 2 HEAT EXCHANGER NETWORKING 12 Hrs. Hot Composite Curve, Cold Composite Curve, Problem Table Algorithm, Grand Composite Curve, Area Targeting by Uniform Bath formula and Unit Targeting by Eulers’ formula, Heuristics for Pinch Design, Maximum Energy Recovery Design, Evolution of Network.

UNIT 3 REACTOR INTEGRATION 12 Hrs. Choice of Idealized reactor model and reactor performance. Reactor configurations: Temperature Control, Gas-Liquid and Liquid Liquid Reactors, Choice of Reactors. Heat Integration characteristics of reactors, Appropriate placements of reactors. Use of GCC for Heat Integration of reactors.

UNIT 4 DISTILLATION INTEGRATION 12 Hrs. Distillation sequencing, Heat Integration characteristics of Distillation column, appropriate placement of distillation column, various configurations for heat integration of distillation column.

UNIT 5 MASS EXCHANGER NETWORK SYNTHESIS 12 Hrs. Mass Exchanger Network, Minimum Mass Separating Agents (MSA), Mass exchange networks for minimum external MSA. Minimum Number of Mass Exchangers.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Robin Smith, Chemical Process Design and Integration, 3rd Edition,John Wiley and Sons,2005. 2. Warren D. Seider, J. D. Seader and Daniel R. Lewin, Product & Process Design Principles, Wiley Publication, 2004. 3. Shenoy U.V., Heat Exchanger Network Synthesis, 2nd Edition,Gulf Publication,2001


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SCH5615 FLUIDIZATION ENGINEERING L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To make the student aware of fundamentals of fluidization and understand the design aspects of fluidized bed

systems

UNIT 1 INTRODUCTION 12 Hrs. Introduction to gas-liquid fluidization, Significance and Characteristic of fluidized bed, The Fluidized state, Nature of hydrodynamic suspension, particle forces, species of Fluidization, Regimization of the fluidized state, operating models for fluidization systems, Applications of fluidization systems.

UNIT 2 HYDRODYNAMICS OF FLUIDIZATION SYSTEMS 12 Hrs. General bed behaviour, pressure drop, Flow regimes, Incipient Fluidization, Pressure fluctuations, Phase Holdups, Measurements Techniques, Empirical Correlations for Solids holdup, liquid holdup and gas holdup. Flow models – generalized wake model, structural wake model and other importantmodels

UNIT 3 SOLIDS MIXING AND SEGREGATION 12 Hrs. Flow regimes, Bubbling and Slugging, Fixed bed and Fluidized bed, Phase juxtapositions operation shifts, Reversal points, Degree of segregation, Mixing Segregation equilibrium, and Generalised fluidization of poly disperse systems, liquid phase mixing and gas phase mixing.

UNIT 4 HEAT AND MASS TRANSFER IN FLUIDIZATION SYSTEMS 12 Hrs. Mass transfer – Gas Liquid mass transfer, Liquid Solid mass transfer and wall to bed mass transfer, Heat transfer – column wall – to – bed heat transfer, Immersed vertical cylinder to bed heat transfer, Immersed horizontal cylinder to bed heat transfer.

UNIT 5 MISCELLANEOUS SYSTEMS 12 Hrs. Conical Fluidized bed, Moving bed, Slurry bubble columns, Turbulent bed contactor,Two phase and Three phase inverse fluidized bed, Draft tube systems, Semifluidized bed systems, Annular systems, Typical applications, Geldart’s classification for power assessment, Powder characterization and modeling by bed collapsing

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Fan, L. S., Gas- liquid Solid Fluidization Engineering, 2nd Edition,Butterworths, 1989, 2. Kwauk, M., Fluidization - Idealized and Bubbleless, with applications, 3rd Edition,SciencePress, 1992. 3 Kunii, D. and Levenspiel, O., Fluidization Engineering, 2ndEdition,Butterworth Heinemann, London, 1991.


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SCH 5616 COMPUTATIONAL FLUID DYNAMICS L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE To give the students a critical attitude and need of the limitations in advanced simulation programs and to select

suitable models and performing advanced simulations with best practice guidelines.

UNIT 1 CONSERVATION LAWS 12 Hrs. Introduction: Transport equations, Governing equations of fluid flow and heat transfer –mass conservation, momentum and energy equation, differential and integral forms, conservation and non-conservation form, Analytical and numerical solution of transport equations

UNIT 2 TURBULENCE 12 Hrs. Characteristics of turbulent flows, Time averaged Navier Stokes equations, Turbulence models – one and two equation, Reynolds stress, LES and DNS, Analogical behavior of momentum, mass and energy transport; Partial differential equations: types, boundary conditions;

UNIT 3 FINITE VOLUME METHOD 12 Hrs. Diffusion problems – explicit and implicit time integration; Convection-diffusion problems – properties of discretisation schemes, central, upwind, hybrid, QUICK schemes; Solution of discredited equations. Finite difference, finite element and finite volume schemes: Grid generation and discretization; accuracy, consistency, stability and convergence; explicit and implicit formulation;

UNIT 4 FLOW FIELD COMPUTATION 12 Hrs. Pressure velocity coupling, staggered grid, and SIMPLE algorithm, PISO algorithm for steady and unsteady flows, solution of Navier Stokes equation with various approach of simulation, staggered grid and collocated grid solution, Solution of Convective diffusion equation

UNIT 5 GRID GENERATION 12 Hrs. Physical aspects, simple and multiple connected regions, grid generation by PDE solution, grid generation by algebraic mapping. Solution of chemical engineering problems ; Introduction to multiphase and turbulence modeling.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Anderson, J. D., Computational Fluid Dynamics: The Basics with Applications,2nd Edition, McGraw-Hill, 1995. 2. Fletcher, C. A. J., Computational Techniques for Fluid Dynamics, 2nd Edition, Springer Verlag, 1997. 3. Versteeg, H.K. and Malalasekera, W., An Introduction to Computational Fluid Dynamics: The Finite Volume Method,, 3rd

Edition,Pearson Education Ltd., 2007.


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SCH5617 MULTIPHASE FLOW L T P Credits Total Marks

3 1 0 4 100

COURSE OBJECTIVE This subject gives the underlying concepts of multiphase flows and different approaches to model such flows

under different conditions in process industries with multiphase contactors.

UNIT 1 CHARACTERISTICS OF MULTIPHASE FLOWS 12 Hrs. Significance of multiphase flows, classification of particle shapes, shape factors, shape regimes of fluid particles, important non-dimensional numbers, parameters of characterization, calculation and measurement of particle size, size distributions and moments, size distribution models.

UNIT 2 PARTICLE FLUID INTERACTION 12 Hrs. Equation of motion for a single particle, calculation of drag, motion of a particle in twodimensions, effects of unsteady and non-uniform flow fields, effects of acceleration,effects of coupling; Interaction between particles – mechanisms of interaction,interparticle forces, hard sphere model, soft sphere model, discrete element modeling, semi-empirical methods, kinetic theory, force chains.

UNIT 3 MODELLING OF MULTIPHASE FLOWS 12 Hrs. Flow patterns - identification and classification - flow pattern maps and transition -momentum and energy balance - homogeneous and separated flow models - correlations for use with homogeneous and separated flow models - void fraction and slip ratio correlations - influence of pressure gradient - empirical treatment of two phase flow - drift flux model - correlations for bubble, slug and annular flows

UNIT 4 CONSERVATION EQUATIONS 12 Hrs. Averaging procedures - time, volume, and ensemble averaging, quasi-one-dimensionalflow, two-fluid volume-averaged equations of motion, turbulence and two-way coupling. Single particle equation, Continuity equation, Translational Equation, Angular momentum equation, Energy equation.

UNIT 5 MULTIPHASE SYSTEMS 12 Hrs. Flow regime and hydrodynamic characteristics of packed bed, fluidized bed, pneumaticconveying, bubble column, trickle beds; Conventional and novel measurement techniques for multiphase systems including CARPT, Laser Doppler anemometry,Particle Image Velocimetry.

Max. 60 Hours

TEXT / REFERENCE BOOKS 1. Clift, R., Weber, M.E. and Grace, J.R., Bubbles, Drops, and Particles, 2nd Edition, Academic Press, 1978. 2. Crowe, C. T., Sommerfeld, M. and Tsuji, Y., Multiphase Flows with Droplets and Particles,3rd Edition, CRC Press, 1998 3. Fan, L. S. and Zhu, C., Principles of Gas-solid Flows,2nd Edition, Cambridge University Press, 1998 4. Govier, G. W. and Aziz. K., The Flow of Complex Mixture in Pipes,,2nd Edition, Van Nostrand Reinhold,1972. 5. Kleinstreuer, C., Two-phase Flow: Theory and Applications,4th Edition, Taylor & Francis, 2003 6. Rhodes, M., Introduction to Particle Technology,2nd Edition,John Wiley & Sons, 1998.


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