Quy Dinh Trinh Bay BCTT, DACN Va LVTN

I H P TP. HCM

KHOA C

NH

LU T NGHI P

A.

1.

2.

3. Nhi m v

4. L i c

5. Nh a ng d n ho c th c hi

6. M c l c: ch i m c l c c p 2

7. Danh m c b ng bi u

8. Danh m

9. vi t t t (n hi u t vi t t t)

10. u (n u)

11. T t

t ng n g thuy t khoa h c,

c

12. u hay Th c nghi m

t d ng c , thi t b u s d u.

C c th c nghi m c ti n

t trong

13. K t qu n

i v i t ng ph n th c nghi m ng v i ph i t

qu c, p , n t qu c t th c nghi m.

14. K t lu n

ng n g n nh ng k t lu n c t k t qu ,

.

15. Ki n ngh

Ki n ngh nh n u ti p theo t k t qu c a

16. u tham kh o

Ch bao g n, s d c p t s d ng

trong lu .

17. Ph l c (n

T ng ph l c minh ch t qu c t

n c c, k t qu chi ti k t qu

n ph m, nh t ng n g n v nh nh lu t s d ng

trong . Ph l a

B.

1. n

C ch ph n n i dung c s d ng ki u ch

ch 13.

nh c ch c th u ch

vi i, t ng ki u ch c, c

ch .

c

th ng.

Canh l : l i 3cm, l ph i 2cm.

trang: trang m c 3

10 theo dng ch ph n n i dung t m c 11

17 theo dng s ph n ph l c

s p x p theo tr t t c a ph n n i dung, size 12, font Times New Roman.

2.

c b u b u trang (n t trang

t bu c ph i qua trang mi).

t in hoa (Arial) c 16 m, canh gi a.

u m c c a lu n theo s

s m c 1, ti u m c 2 trong mc 1).

y v

T i m u m c ph u m

nh d ng c a nh c, ti u m i gi ng

3. u

c th hi n b ng ph n m

c s d Word.

h v ng bi t ngay trong ph c p t ng

h p s xu t hi n c ho c b ng bi t hi n m t kho ng

tr ng l c b ng qua trang k ti o

kho ng tr ng.

a b ng n m a

b th t trong lu a b ng

ch vi

b ng ng v i c ch

a b ng i vi t ng n g i d

hi hi c n c p t

n ph b n.

N u b ng s u

tham kh m u tham kho)

B ng c g t trang. N u chi n,

n ph i ghi

l ng ph i ghi l t.

u ngang l

N u ngang kh gi u

b n ch

ph c th hi ch s

th sao chp l i

c p t i b ng bi u ho i dung

lu t bu c ph i vi th t c n ph i vi

4.

th ng nh t m nh

d , c s d i s d ng

n m t. c b t bu c ph i s d ng ph n

m m Chemoffice. Ph c ph i s d ng ch

ho c ph n m

, s trong ngoc

chung v i nhau

N i u m i l u xu t hi u,

. N u s u s d ng trong lu

hi u lu n A, b c c lu

5.

T t c ng bi n, g li c s d ng

t nh ng ngu n g c xu t x c

trong m u tham kho

th hi n m c tham kho t

hi th t c u tham kh o. S th t

theo s r p t i l n.

u tham kho c a nh ng ki n th bi n, m i

u bi t, nh ng n ph n tham

kh n.

6.

6.1.

, T , t b n, m xu t b n, s trang s trang,

.

:

[1]. , ,

xu t b i h p H , 15 24, 2009.

6.2.

, T , s cu n (n t b n,

m xu t b n, s trang s

:

[1]. ,

, t b i h

H 24, 2009.

6.3. y u h i ngh

, t y u h i ngh , cu n s , trang s

- trang s .

:

[1]. G. Pevere et al, The International Journal of Infrared

Design, 33, 56-99, 1979.

6.4. Trang web

, Internet: http://www.(url) p nh t.

:

[2]. Anne Marie Helmenstine, Internet:

http://chemistry.about.com/cs/growingcrystals/a/aa012604.htm, 16/10/2011.
http://www.(url)/http://chemistry.about.com/cs/growingcrystals/a/aa012604.htm

6.5.

, , cu n s , s trang s trang,

d :

[3]. B.Bart , Globe and Mail, 2(3), 1 4, 32002

6.6. Lu t nghi p

, b ng c .

:

[4]. Bi 2 b c i thi n ho

Lu t nghi p, i h c Khoa h c t n T H

Minh, 2010.

7.

7.1. n t t nghi p: B .

7.2. c t y tr nh, b c

8.

p 02 cu ng

d n, h , l c c

v c giao. Nh ng h p t i quy t

b tr v .

C.

I H P TP. HCM

KHOA C

U V PH N

NG D NG

Gi ng d n: Th.S TR N TH LAN ANH

c hi B

MSSV: 08257751

L p: CDHC10

2008-2011

Tp. H t

i

I H P TP.HCM

C

C I CH T NAM

c l p T do - H

H n Thanh Tun

MSSV: 08265301

L p: CDHC10

H

n t t nghi p:

Nhi m v c n:

1.

2.

3.

n:

n:

H ng d n:

Ch nhi m b

Tp. H

ng d n

ii

L I C

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TP. H

H

ii

NH NG D N

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Ph

c th c hi n: ................................................................................................

N i dung th c hi n: ............................................................................................

............................................................................................

T ng h p k t qu : ...............................................................................................

m b ng s : .................................... m b ng ch : .......................................

Tp. H ..... .....

ng d n

iii

NH N BI N

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Ph

c th c hi n: ........................................................................................

N i dung th c hi n: ...................................................................................

...................................................................................

T ng h p k t qu : ......................................................................................

m b ng s : ............................... m b ng ch : ....................................

Tp. H ..... ..... 10

ph n bi n

iv

M C L C

NG QUAN V PH N ................................. 1

n ............................................................................... 2

c v n c a ph n .......................................... 4

a ph n u ... Error! Bookmark

not defined.

n xu t Ethylbenzene .......................... Error! Bookmark not defined.

n .......................... Error! Bookmark not defined.

............. Error! Bookmark not defined.

i theo c u t o c n ng ........ Error! Bookmark not

defined.

........................................... Error! Bookmark not defined.

p ch ....... Error! Bookmark not defined.

1.6.2. D n xu t halogen ................................................ Error! Bookmark not defined .

1.6.3. Ancol, ete, este, oxit olefin ................................. Error! Bookmark not defined.

p ch t mu i b c 4 c a amin ..................... Error! Bookmark not defined.

............................... Error! Bookmark not defined.

............................. Error! Bookmark not defined.

1.7.1. Axit phi proton ................................................... Error! Bookmark not defined.

1.7.2. Axit proton .......................................................... Error! Bookmark not defined.

...................................................... Error! Bookmark not defined.

ng c a m t s ph n d ng ...... Error! Bookmark not

defined.

ph n .......................................... Error! Bookmark not defined.

th ...................................... Err or! Bookmark not defined.

th n t SE2 ................................... Error! Bookmark not defined.

g c ng olefin nhi cao .......... Error! Bookmark not

defined.

ph n ng ph ........................................... Error! Bookmark not defined.

v

1.10.1. Phn i ti p .............................. Error! Bookmark not defined.

1.10.2. Phn ng nh ........................................... Error! Bookmark not defined.

1.10.3. Phn .................. Error! Bookmark not defined.

1.10.4. Phn ............................. Error! Bookmark not defined.

u t .... Error! Bookmark not defined.

............................................ Error! Bookmark not defined.

1.11.2. N t tham gia phn ng ............... Error! Bookmark not defined.

1.11.3. Nhi ............................................................ Error! Bookmark not defined.

t .............................................................. Error! Bookmark not defined.

1.11.5. S khu y tr n .................................................... Error! Bookmark not defined.

1.12. M t s ....................................... Error! Bookmark not defined.

C- C- Error! Bookmark

not defined.

O- O- ... Error! Bookmark not defined.

S- T ng h p mercaptan t Error!

Bookmark not defined.

1.12.4. N- T ng h p metylamin t metanol Error! Book mark not defined.

1.13. Gi i thi u v -naphtyl metyl ete) ......... Error! Bookmark not defined.

c v nerolin............................................. Error! Bookmark not defined.

t v c ................ Error! Bookmark not defined.

u ch ...................................... Error! Bookmark not defined.

C NGHI M..................................... Error! Bookmark not defined.

2.1. M u .......................... Error! Bookmark not defined.

2.2. t b ............................ Error! Bookmark not defined.

2.3. Th c nghi u ch nerolin t ........ Error! Bookmark not

defined.

....................................... Error! Bookmark not defined.

2.3.2. Kh ng c a t l mol ...................... Error! Bookmark not defined.

2.3.3. Kh ng c a nhi ph n ng ....... Error! Bookmark not defined.

2.3.4. Kh ng c a th i gian ph n ng ...... Error! Bookmark not defined.

a nerolin sn ph m .. Error! Bookmark not

defined.

vi

T QU N.................... Error! Bookmark not defined.

3.1. K t qu kh u t n hi u su t t o nerolin.................. Error!


3.1.1. K t qu kh ng c a t l mol metanol:naphthol . Error! Bookmark

not defined.

3.1.2. K t qu kh ng c a nhi ........... Error! Bookmark not defined.

3.1.3. K t qu kh ng c a th i gian ......... Error! Bookmark not defined.

3.2. Kh n nerolin b ............... Error!


u x tia X (XRD) ................... Error! Bookmark not defined.

h ng ngo i (IR) ..................... Error! Bookmark not defined.

n t ........... Error! Bookmark not defined.

T LU N NGH ................ Error! Bookmark not defined.

t qu c......................................... Error! Bookmark not defined.

u ch nerolin t -naphthol ........................... Error! Bookmark not defined.

n nerolin qua thc nghi m ... Error! Bookmark not defined.

4.2. Nh ng n c hi c ................... Error! Bookmark not def ined.

4.3. Ki n ngh ............................................................... Error! Bookmark not defined.

U THAM KH O .............................................. Error! Bookmark not defined.

PH L C ........................................................................ Error! Bookmark not defined.

vii

DANH M C B NG BI U

B ng 1. 1. S gi ......... Error!


B ng 1. 2. ng th khi ch n axit ..................... Error! Bookmark not defined.

B ng 1. 3. Nh ng thu n l d 2SO4Error! Bookmark

not defined.

B ng 1. 4. Hi u ng nhi t c a m t s ph n ng alky ng ........................... 1

B ng 3. 1. ng c a t l n hi u su tError! Bookmark

not defined.

B ng 3. 2. ng c a nhi n hi u su t ........................................................... 4

B ng 3. 3. ng c a th n hi u su t ....... Error! Bookmark not defined.

viii

DANH M NH

. bi u di n m ng c Error! Bookmark

not defined.

. Bi th gi Error! Bookmark not

defined.

. 2SO4 .............................................. Error! Bookmark not defined.

. Bi c s d ng 2 lo i axit t n nay

....................................................................................... Error! Bookmark not defined.

. i thi t b ph n ng s d i

3 .................................................................. Error! Bookmark not defined.

. s n xu t etyl- ...................................... 2

. s n xu t ter-butylmetylete Error! Bookmark not defined.

. s n xu t metylamin ........... Error! Bookmark not defined.

. C u t o c a nerolin ....................................... Error! Bookmark not defined.

. n u ch nerolin ...... Error! Bookmark not defined.

. u ch nerolin .................................. Error! Boo kmark not defined.

. Hi u su t nerolin theo nhi ph n ng ....................................................... 4

. Hi u su t c a nerolin theo thi gian ............. Error! Bookmark not defined.

. Ph XRD c a nerolin ...................................................................................... 8

. Ph IR c a nerolin ........................................ Error! Bookmark not defined.

. ........................................................................................... 9

ix

L U

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1

NG QUAN V PH N

1.1.

B ng 1. 1. Hi u ng nhi t c a m t s ph n ng

t b - kJ/mol

RCH=CH2

Calph H

Car H

O H

84 100

96 104

50 63

RCl

Car H

O H

N H

34 42

0 25

2

Benzen

AlCl3

1

2

3

7

8

912 15

1617

18

14136

4

5

10

11

Polyalkylbenzen

Olefin

HCl

Polyalkylbenzen

NaOH

H2O

1. s n xu t etyl-

3

2: U

2. 1.

2. 2.

2. 3.

4

3: K T QU N

3. 1.

B ng 3. 1. ng c a nhi n hi u su t

% TB

1 75

2.9385 46.44 47.31

2 3.0481 48.17

3 80

4.6351 73.25 71.29

4 4.3865 69.32

5 85

4.9810 78.72 77.39

6 4.8124 76.05

7 90

4.9912 78.88 79.05

8 5.0129 79.22

1 ng c a nhi ph n n hi u su t nerolin

20

40

60

80

100

70 75 80 85 90 95 100

0C)

5

K T LU N

6

KI N NGH

7

U THAM KH O

8

PH L C

Ph l c 3. 2. Nhi u x XRD c a nerolin

9

Ph l c 3. 3 a nerolin

Documents

Quy Dinh Trinh Bay BCTT, DACN Va LVTN