Radiation Safety Engineering, Inc. · Samples requiring preservation were verified prior to sample analysis. See attached report from subcontracted laboratory for QA/QC information

SDMS DOCID#1142196

Test America THE LEADER IN ENVIRONMENTAL TESTING

l

t ~EC Ge.omatrix Consulta~ts, Inc. - AZ - :Client Project ID: I 8777 E. Vra de Ventura, Smte 396 ~ ~cottsdale, AZ 85258 .-:Attention: Brian Mcnamara

l

14682.013. PGA-North Sampled: 06/24/10

TestAmeri~"f~'15&rclt/~Ws1~c. Issued: 07/191!0

J. I

J ;

LABORATORY NUMBER

PTF1468-01 PTF1468-02 PTF1468-03 PTF1468-04

~AMPLE RECEIPT: ) .

f.crOLDING TIMES:

PRESERVATION:

~)'1-VQC CRITERIA:

r

Report Number: PTF1468

CASE NARRATIVE

SAMPLE DESCRIPTION

SASFS-P SAS-B 1-12-06241 0 SASFS-PSAS-B2-12-062410 SASFS-PSAS-B3-12-06241 0 SASFS-PSAS-B4-12-06241 0

SAMPLE MATRIX

Soil Soil Soil Soil

ANALYSES

Cobalt 60 Gross Alpha

Cobalt 60 Gross Alpha

Samples were received intact, on ice, and with chain of custody documentation.

See attached report from subcontracted laboratory for holding time information.

Samples requiring preservation were verified prior to sample analysis.

See attached report from subcontracted laboratory for QA/QC information.

'

11 If

LABORATORY PERFORMIN~ ANALYSES ! )

Radiation Safety Engineering, IndJ Radiation Safety Engineering, Inc;J~ Radiation Safety Engineering, Inci.l ; Radiation Safety Engineering, Inq, j .

l I 11

LI. It ! 1 ; '! ! $ IL ; 'J . n

. ~ J. ;;t .H . ,.j if

II II i ;~ ~ti ~ . ~ ; ~

d) I.

\lil. I'.' ~i; ~,;. I i

.tr ,:! .

I

(')BSERVATIONS: See attached report from subcontracted laboratory for observations made regarding this work order. "" J

SUBCONTRACTED: One or more samples were subcontracted to Radiation Safety Engineering, Inc.- 3245 N. Washington St., Chandler, AZ (AZ0462) for the analyses listed above. Results are attached.

hi;STAMERICA- PHOENIX, AZ (AZ0728)

.~ .. J'\ ~ 1\ \A..- /0 a fL ''~T'CJ

Carlene McCutcheon

H1:oject Manager The results pertain only to the samples tested in the /aborat01y. This report shall not be reproduced, except in

fit!/, without wrillen permissionfi'0/11 TestAmerica, Inc.

. ' .i

. .. ; . ' I' ~: ~ .

PTF146~ : ,l.

Page 1 ~fi;l

4625 East Cotton Center Boulevard Suite 189 Phoenix, AZ 85040 tel602.437.3340 fax 602.454.9303 www.testamericainc.com i:..r:~

r: 1,.

I i

Radiation Safety Engineering, Inc. 3245 N. WASHINGTON ST. CHANDLER, ARIZONA 85225-1121 Website: www.radsafe.com

(480) 897-9459 FAX (480) 892-5446

Radiochemical Activity in Water (pCi/L)

Sample ID

PTF1468-0l

PTF1468-02

PTF1468-03

PTF1468-04

TestAmerica Analytical Testing Corporation 4645 E. Cotton Center Blvd

Building #3, Suite #189 Phoenix, AZ 85040

Samples Received: June 25, 2010

Analysis Completed: July 13, 2010

Gross Alpha Activity Gross Beta Activity Method 900.0 Method 900.0

(pCi/g) (pCi/g)

53.0 4.0 28.9 1.8

38.0 3.1 27.4 1.5

12.6 1.5 23.9 1.2

32.6 2.4 30.8 1.4

Robert L. Metzger, Ph.D,, C.H.P.

Sample ID

I PTF1468-01

Analysis Dates


I


TestAmerica Phoenix 4625 East Cotton Center Blvd., Suite 189

Phoenix, AZ 85040

Sampling Date: June 24, 2010 Analysis Completed: July 1, 2010

Cesium-134 Cesium-137 Activity Activity Method Method 901.1 901.1

(pCi/g) (pCi/g)

< 0.039 I

< 0.034

July 1, 2010 July 1, 2010 07:09 07:09

I

(480) 897-9459 FAX (480) 892-5446

Cobalt-60 Activity Method 901.1

(pCi/g)

< 0.034

July 1, 2010 07:09

I

I

Sample ID




Phoenix, AZ 85040



(pCi/g) (pCi/g)

PTF1468-02 I

< 0.038 I

< 0.036

Analysis July 1, 2010 July 1, 2010 Dates 07:11 07:11

I

(480) 897-9459 FAX (480) 892-5446


(pCi/g)

< 0.035

July 1, 2010 07:11

I

Sample ID

I PTF1468-03

Analysis Dates


I



Phoenix, AZ 85040



(pCi/g) (pCi/g)

< 0.037 I

< 0.032

July 1, 2010 July 1, 2010 07:15 07:15

I

(480) 897-9459 FAX (480) 892-5446


(pCi/g)

< 0.031

July 1, 2010 07:15

I

I

Sample ID




Phoenix, AZ 85040



(pCi/g) (pCi/g)

PTF1468-04 I

< 0.037 I

< 0.035

Analysis July 1, 2010 July 1, 2010 Dates 07:16 07:16

I

(480) 897-9459 FAX (480) 892-5446


(pCi/g)

< 0.035

July 1, 2010 07:16

Robert L. M ger, Ph.D., C.H.P.

I

SENDING LABORATORY:

SUBCONTRACT ORDER TestAmerica Phoenix

PTF1468

RECEIVING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040

Radiation Safety Engineering, Inc.

3245 N. Washington St. Chandler, AZ 85225-1121

Phone: (602) 437-3340 Phone :(480) 897-9459

Fax: (602)454-9303 Fax: 480-892-5446 Project Manager: Carlene McCutcheon Project Location: AZ -ARIZONA

Receipt Temperature: Ice: Y I N

Standard TAT is requested unless specific due date is requested. => Due Date: ___ _ Initials:

Analysis Units Expires

Sample ID: PTF1468-01 {SASFS-PSAS-81-12-062410 Soil) Sam led: 06124110 10:30 Cobalt 60 pCi/L 07/02/10 10:30

Gamma Spectrometry mg/1 07/08/10 1 0:30

Gross Alpha-0 pCi/L 07/08/10 1 0:30

Gross Beta-0 pCi/L 07/08/10 1 0:30

Containers Supplied:

1 Liter Poly (A) 1 Liter Poly (B)

Sample ID: PTF1468-02 {SASFS-PSAS-82-12-062410 Soil) Sam led: 06124110 10

:45

Cobalt 60 pCi/L 07/02/1 0 10:45


Gross Alpha-0 pCi/L 07/08/1 0 10:45

Gross Beta-0


1 Liter Poly (A)

pCi/L

1 Liter Poly (B)

07/08/1 0 10:45

Sample ID: PTF1468-03 {SASFS-PSAS-83-12-062410 Soil) Sam led: 06124110 11

:46

Cobalt 60 pCi!L 07/02/10 11 :46


Gross Alpha-0 pCi/L 07/08/10 11:46

Gross Beta-0 pCi/L 07/08/10 11:46


1 Liter Poly (A) 1 Liter Poly (B)

Cttl ~l::d)l;) {4J~:b I !J {_) !.(4~ _h-. Released By Date/Time Received By

Released By Date/Time Received By

Comments

3 ICOC - Radiation Safety

ICOC - Radiation Safety



ICOC- Radiation Safety





c~z~- ~ /l .. (~-c)

Date/Time

Date/Time Page 1 of2

Analysis Units

SUBCONTRACT ORDER TestAmerica Phoenix

PTF1468

Expires

Sample ID: PTF1468-04 (SASFS-PSAS-84-12-062410- Soil) Sam led: 0612411011

:55

Cobalt 60 pCi/L 07/02/1 0 11 :55

Gamma Spectrometry

Gross Alpha-0

Gross Beta-0


1 Liter Poly (A)

mg/1

pCi/L

pCi/L

1 Liter Poly (B)

07/08/10 11 :55

07/08/1 0 11 :55

07/08/10 11:55

Comments




Page 2 of2

CHAIN OF CUSTODY FORM Test America THE LEADER IN ENVIRONMENTAL TESTING

~~ c 4625 E. Cotton Center Blvd., Suite 189, Phoenix, AZ 85040 (602} 437-3340 FAX (602} 454-9303 [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 [ 1 Las Vegas - 2520 E. Sunset, Suite 3, Las Ve.gas, NV 89120 (702} 798-3620 FAX (702} 798-3621

TAL-0013-550 (12/08)

Client Name I Address: IY~eC- !;;rk;:./1(11~ t.;>< Project!PO Number: Analysis Required

er=n E. ~/111 fl:P YFflll~lt 1 "fl:;:.~tt6 ; 1-ffiJ'C z .. 0 ~~ ..t p~ft f\lQPSJt

..

th ~~ ~ " 7Co1ff {)ftt-~/ A""l: g~,_~g - 0 ~ k ~~

() ~ Sample Description Sample Container #of Sampling

Sampling Preservatives \) ~ ~ .\., Matrix Type Cont. Date Time "'

5~~ -P5P6 -BI- iJ- ""062:fto c ;; H .. 2.. 6-~~(-'i~ jP ~ "jO J/f} ~ -~ ~ ~ ?~FJ- P5M -- ez., iJ_ ..-o(iYft-~ 5 jl 2... 6 ~r:.~t~1() 1/o.''/J' fl/j'{l, ""' "' ""- ""' _g.,.._s-fs -f>yf.S- ~3 - 12. - ot..Z'/Io ..5 LL 2.. t~..z'/~/1; lf:v6 !1LJ- '- "'\.. '-- " :;,.~-!S.-/_j.q.s-t Y-1.2- ct.t1/) ..5 IL .J_ 6~Y..# Jf: s-S" nlf '- ""' '- '

Rei~~ Date/Time: Received By: Date/Time: Turnaround Time: b-.,$.!7-/tJ- /700 h same day Relinquished By: Date/Time:

7i:By: Date/Time: 24 hours

48 hours

Relinquished By: Date/Time: ( Rect:!t in Lab By: { :ar:_~ihe~) Sample Integrity: . ~.- r '+fY1 intact r

of I

Special Instructions

P'"""(l:::"\1-\L..~-o\ -02 ~o_j

~

(Check)

72 hours

5 days

normal f (Check) '

on ice V ).3oc_

Note: By relinquishing samples to TestAmerica, client agrees to pay for the services requested on this chain of custody form and any additional analyses performed on this project. Payment for services is due within 30 days from the date of invoice. Sample(s) will be disposed of after 30 days.

" men co THE LEADER IN ENVIRONMENTAL TESTING

't".i\MEC Geomatrix Consultants, Inc. - AZ - :Client Pro' ect ID :i 8777 E. Via de Ventura, Suite 396 ~ 1' ',;'

,(Scottsdale, AZ 85258

146821030(SASFS-UP1) Sampled: 08/25/10

TestAmeri&r~b'15B:ralt&Fl~$!fuc.

~~~ttention: Brian Mcnamara Issued: 09/23/10 Report Number: PTH1415

CASE NARRATIVE ()n

LABORATORY SAMPLE SAMPLE

(::: NUMBER DESCRIPTION MATRIX

PTH1415-01 SASFS-RBS1-3-082510 Soil PTH1415-02 SASFS-RBS2-3-08251 0 Soil PTH1415-03 SASFS-RBS3-3-082510 Soil PTH1415-04 SASFS-RBS4-3-082510 Soil PTH1415-05 SASFS-RBS5-3-082510 Soil PTH1415-06 SASFS-RBS6-3-082510 Soil

SAMPLE RECEIPT: Samples were received intact, on ice, and with chain of custody documentation.

HOLDING TIMES: Holding Times were met.

PRESERVATION: Samples requiring preservation were verified prior to sample analysis.

(jJvQC CRITERIA: See attached report from subcontracted laboratory for QA/QC information.

t)BSERVATIONS: No significant observations were made.

SUBCONTRACTED: One or more samples were subcontracted to Radiation Safety Engineering, Inc.- 3245 N. Washington St., Chandler, AZ (AZ0462) for the requested analyses. Results are attached.

TEST AMERICA- PHOENIX, AZ 0

Prpject Manager The results pertain only to the samples tested in the laboratory. This report shall not be reproduced, except in

full, without written permission from TestAmerica, Inc.

PTH14~"

Page 1 of 1

4625 East Cotton Center Boulevard Suite 189 Phoenix, AZ 85040 tel 602.437.3340 fax 602.454.9303 www.testamericainc::.com

Sample ID

PTH1415-01

PTH1415-02

PTH1415-03

PTH1415-04

PTH1415-05

PTH1415-06


Radiochemical Activity in Soil (pCi/g)

TestAmerica Analytical Testing Corporation 4645 E. Cotton Center Blvd

Building #3, Suite #189 Phoenix, AZ 85040

Samples Received: August 26, 2010

Analysis Completed: September 15, 2010

Gross Alpha Uranium Adjusted Activity Activity Gross Method Method Alpha

600/00-02 00-07 (pCi/g) (pCi/g) (pCi/g)

9.4 2.8 1.9 0.3 7.5 2.8

13.3 2.8 2.1 0.4 11.2 2.8

15.5 2.7 1.7 0.3 13.8 2.7

19.9 2.9 2.4 0.8 17.53.0

16.2 2.3 1.8 0.3 14.4 2.3

13.1 2.1 1.8 0.3 11.3 2.1

(480) 897-9459 FAX (480) 892-5446

Gross Beta Activity Method

900.0 (pCi/g)

12.7 2.3

16.7 2.1

19.0 1.9

18.7 1.8

22.4 1.5

23.4 1.5

Robert L. Metzger, Ph.D., C.H.P.

Sample ID

I PTH1415-01

Analysis Dates


I



Phoenix, AZ 85040

Sampling Date: August 25, 2010 Analysis Completed: August 27,2010


(pCi/g) (pCi/g)

Sample No.

PTH1415-01


238u

0.9 0.2

2.6 0.6

Comments:

Isotopic U rani urn Analysis

TestAmerica 4625 E. Cotton Center Blvd., Suite #189

Phoenix, AZ 85040

Sampling Date: August 25, 2010

Sample Received: August 26, 2010

Uranium Analysis Date: August 31, 2010

23su 234u

0.040 0.001 1.00.2

0.019 0.001 0.00016 0.00003

Total

1.9 0.3

2.6 0.6

(480) 897-9459 FAX [480) 892-5446

Activity (pCi/g)

Content (ug/g)


Sample ID

I PTH1415-02

Analysis Dates


I



Phoenix, AZ 85040



(pCi/g) (pCi/g)

Sample No.

PTH1415-02


2Jsu

1.0 0.2

2.8 0.7

Comments:


TestAmerica 4625 E. Cotton Center Blvd., Suite # 189

Phoenix, AZ 85040




23su 234u

0.044 0.002 1.10.2

0.021 0.001 0.00018 0.00004

Total

2.1 0.3

2.9 0.7

(480) 897-9459 FAX (480) 892-5446

Activity (pCi/g)

Content (ug/g)


Sample ID

I PTH1415-03

Analysis Dates


I



Phoenix, AZ 85040

Sampling Date: August 25, 2010 Analysis Completed: August 27, 2010


(pCi/g) (pCi/g)

Sample No.

PTH1415-03


23su

0.9 0.2

2.7 0.6

Comments:



Phoenix, AZ 85040




23su 234u

0.042 0.001 0.7 0.2

0.020 0.001 0.00011 0.00003

Total

1.7 0.3

2.7 0.6

(480) 897-9459 FAX (480) 892-5446

Activity (pCi/g)

Content (ug/g)


Sample ID

I PTH1415-04

Analysis Dates


I



Phoenix, AZ 85040



(pCi/g) (pCi/g)

Sample No.

PTH1415-04


2Jsu

1.10.2

3.3 0.7

Comments:


TestAmerica 4625 E. Cotton Center Blvd., Suite #189

Phoenix, AZ 85040




23su 234u

0.051 0.002 1.2 0.2

0.024 0.001 0.00020 0.00004

Total

2.4 0.3

3.3 0.7

(480) 897-9459 FAX (480) 892-5446

Activity (pCi/g)

Content (ug/g)


Sample ID

I PTH1415-05

Analysis Dates


I



Phoenix, AZ 85040


Cesium-134 Cesium-137 Activity Activity Method Method 901.1 901,1

(pCi/g) (pCi/g)

Sample No.

PTH1415-05


23su

0.8 0.2

2.5 0.5

Comments:

Isotopic Uranium Analysis


Phoenix, AZ 85040




23su 234u

0.039 0.001 0.9 0.2

0.018 0.001 0.00015 0.00003

Total

1.80.2

2.5 0.5

(480) 897-9459 FAX (480) 892-5446

Activity (pCilg)

Content (ug/g)

Ad;( g.~_) Robert L. Metzger, Ph.D., C.H.P.

Sample ID

I PTH1415-06

Analysis Dates


I



Phoenix, AZ 85040



(pCi/g) (pCi/g)

0.028 0.008 I

< 0.024

August 27, 2010 August 27, 2010 14:59 14:59

I

(480) 897-9459 FAX (480) 892-5446


(pCi/g)

< 0.023

August 27, 2010 14:59

Robert L. Metzge, h.D., C.H.P.

I

Sample No.

PTH1415-06


23su

0.7 0.2

2.2 0.5

Comments:

Isotopic Uranium Analysis


Phoenix, AZ 85040




23su 234u

0.034 0.001 1.0 0.2

0.016 0.001 0.00017 0.00003

Total

1.8 0.3

2.2 0.5

(480) 897-9459 FAX (480) 892-5446

Activity (pCi/g)

Content (ug/g)


Aug. 26. 20HJ 11: 07M~ SUBCONTRACT ORDER

TestAmerica Phoenix

No. 3235 F'. 1

PTH1415 11e..v~~ SENDING LABORATORY:

TestAmerica Phoenix 4625 East Cotton Center Blvd. Ste 189 Phoenix, Al. 85040

RECEIVING LA BORA TQRY;

Radiation Safety E:ngineering, Inc. 3245 N. Wast1ington St Chandler, AZ 85225-1121

Phone: (602) 437-3340 Phone :(480) 897-9459 Fax: (602) 4549303 Fax: 480-892-5446 Project Manager: Carlene McCutcheon Project location: 1'\Z.- ARIZONA

Receipt Temperature: C Ice: Y I N

Standard TAT is reqvested unless specific du.e date is requested. => Due !)ate; ~--- Initials: -~-

Analysis Units

~pie ID: PTH141501 (SASFS-RB$1-3-082510 Soli) Sampled: 08125110 07;15 ~sium 137 pCi/L 08/25/11 07:15 -Rlnbalt 60 pCI/g 09/02f10 07:15 4!~amm$ Spectrometry pCi/g 09/08/10 07:15

Fd;ross Alpha-0 pCi/g 09/08/10 07:15

litross Beta"O pCi/g 09/08/10 07:15 Furan'1um 234,235,238 lsotopi pCi/L 08/25/11 07:15 Pr' Containers Supplied:

-t-uter Poly (A)

~9~*jum 137 pCi/L 08/25/11 07:35 Cobalt 60 pCi/g 09/0zho 07:35 ~~~ma Spectrometry pCi/g 09/08/10 07:35 Gross Alpha-0 pCi/g 09/08{10 07:35

S.toss Beta-0 pCi/g 09f08/1 0 07:35 ijfanium 234,235,238 lsotopi pCi/L 08/25/11 07:35

'VJontainers Supplied:

'iSUter Poly (A)

f?lii,mple lb: PTH1415-03 (SASFS-RB$3-3082510- Soil) S I d ~ am e:

l"qesiurn 137 pCi/L 08/25/11 07:50 ~~obalt 60 pCi/g 09/02/10 07:50

w'Pamma Spectrometry pCi/g

Gross Alpha-0 pCi/g

SGtoss Beta-0 pCI/g

S~;.anium 234,235,238 lsotopi pCi/L

CohbtJin~rs Supplied:

:~~~Liter Poly (A)

~Jeased By

~fi.''

Dateffime

Dateffime

09/08/10 07:50

09/08/10 07:50

09/08/10 07:50 08/25/1-1 07:50

Comments


!COG - Radiatiort Safety

!CDC-Radiation Safety

IGOC. R.adlation Safety

!COG- R.adia.tion Safety

lCOC


ICOC- Ra.diat!on Safety

ICOC-Radiation Safety



1COC



!COG-Radiation Safety


!CDC - Radiation Safety

ICOC

:' r.ug.26. 201(1 11:0/A.iVI {:

'c ->,

"

Units

SUBCONTRACT ORDeR TestAmerlca Phoenix

PTH1415

Expires

S~mple ID: PTH141504 (SASFS-RBS4308251 0 Soli) Sampled: QS/2511 Q Oa:04

B.esium 137 pCi/L 08/25/11 08:04

.!~obalt 60 pCi/g 09/02/10 08:04 amma Spectrometry pCi!g 09/08/10 08:04

:~,@ross Alpha-0 pCi/g 09/08/10 08:04

~ross BetaO pCifg 09/08/10 08:04

~ranium 234,235,238 lsotopl pCi/L 08/25!11 08:04 ''1,"''

:&;,ontainers Supplied:

Pi Liter Poly (A)

~mpte !D: PTH141505 (SASFSRBSS-3-08251 0- Soli) ' Sampled: 08125/10 08:24

($esium 137 pCi!L r-,: ..

]obalt 60 pCi/g ,,~~mma Spectrometry pCifg ~;pross AlphaO pCi/g

~@rq,ss Beta-0 pCl/g ]r~~ium 234,235,238 lsotopi pCi/L

:Jiontainers Suppfied:

~lli Liter Poly (A)

OB/25/11 08:24

09/02/10 08:24

09/08/10 08:24 09/08/10 08:24

09/08/10 08:24

09/09/10 08/25!11 08;24

. :~ .. ~ ~,Wple ID: PTii1415-06 (SASFS-RBS6-3-082510 Soli) Sampled: 08,25110 OB:40

.. Qesium 137 pCi/L 08/25/11 08:40

!i~pbalt 60 pCifg 09/02/10 08:40 ,:~amma Spectrometry pCi/g 09/08/10 08:40 f.~ross Alpha-0 pCi/g 09108/10 08:40 ~iltross Beta-0 pCi/g 09/08/1 0 08:40 ~i. ii;lranium 234,235,238 lsotopl pCifL 08/25/11 08:40

_.-:W,6ntainers Supplied:

~Liter Poly (A)

,. '

Nc. 3235 f'. 2

Comments

ICOC Radiation Safety

Jcoc- Ra.diation Safety

!COG-Radiation Safety

ICOC Radiation S:'lfety


ICOC




JCOC - Radiation Safety


10


!COC - Radiation Safety




!COC

,, ,.

Page 2 of 2


TAL-0013550 (12/08) r NomoI~""" cdv . t/A .c.c 6 ev . I --~q(p :z1,1 f;. jGxde ,

~LD-r~c{ GL le, A7 ...... Pr~ctManage}tt M

. . . (.__ 6.. i"Vltvtl'-t ' y' ,,

Saf1lpler: J (2. pj 0 ~fu{ S. tJohnp~_r"' " Sample Description Sample Container Matrix Type

514SF5 -'RBSi-6- fi/iJ_t;;uJ :5' />-L SA~'" I< o.8:J.. ... 1 ,.. os; zs 1 o g l-t-I ~J Asrs - Qp.,

4625 East Cotton Center Blvd. Ste 189 Phoenix, AZ 85040 * (602) 437-3340 * Fax (602) 454-9303

August 20, 2010

Client:

Attn:

Work Order:

Project Name:

Project Number:

Date Received:

PGAN - TO15

PGA North

PTH0994

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report were

performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless otherwise noted

in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This report shall not be

reproduced, except in full, without written permission from TestAmerica.

TestAmerica Laboratories, Inc., Phoenix Laboratory certifies that the analytical results contained herein apply only to the specific sample(s)

analyzed.

The Chain of Custody, 1 page, is included and is an integral part of this report. This entire report was reviewed and approved for release.

If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-(602)437-3340

08/17/10

Scottsdale, AZ 85258

AMEC Geomatrix Consultants, Inc. - AZ - PGAN

8777 E. Via de Ventura, Suite 396

Brian Mcnamara

LABORATORY REPORT

Final Report: 08/20/10 16:11

Analyses included in this report were performed by the laboratory shown at the top of this report unless otherwise indicated.

CASE NARRATIVE: SAMPLE RECEIPT: Samples were received intact, at 20C and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in

accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the

report.


QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data

qualifiers.

COMMENTS: No significant observations were made.

SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information

included in this report.

Approved By:

Project Manager

Carlene McCutcheon

Page 1 of 13


Scottsdale, AZ 85258 Project:

Work Order:

PGAN - TO15

Received:

Project Number: PGA North

08/17/10AMEC Geomatrix Consultants, Inc. - AZ - PGAN


Brian Mcnamara

Reported: 08/20/10 16:11

PTH0994

SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE CONTAINER TYPE

PTH0994-01SASFS-PD52-30-08172010 08/17/10 S/N 0271 1L Canister

PTH0994-02SASFS-PD52-60-08172010 08/17/10 S/N 1290 1L Canister

Page 2 of 13



Work Order:

PGAN - TO15

Received:




Brian Mcnamara

Reported: 08/20/10 16:11

PTH0994

ANALYTICAL REPORT

Data

QualifiersPQLResult MethodAnalyst

Date

AnalyzedResult PQL

ug/m3ppbv

Dilution

Volatile Organic Compounds by EPA TO-15

Sample ID: PTH0994-01 (SASFS-PD52-30-08172010) Sampled: 08/17/101,1,1-Trichloroethane 0.50



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Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH0994-01 (SASFS-PD52-30-08172010) - cont. Sampled: 08/17/10Freon 113 0.50



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Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH0994-02 (SASFS-PD52-60-08172010) Sampled: 08/17/101,1,1-Trichloroethane 0.50



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PTH0994

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH0994-02 (SASFS-PD52-60-08172010) - cont. Sampled: 08/17/10Hexachlorobutadiene 1.0



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PTH0994

PROJECT QUALITY CONTROL DATA

Blank

Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed DateRL


10H0718-BLK1ppbv 10H0718



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Blank - Cont.



10H0718-BLK1ppbv 10H0718



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LCS - Cont.

Analyte UnitsResult % Rec. BatchQ

Target

Range Analyzed DateRL


10H0718-BS170 - 130 10H07188.25 82% ppbv1,1-Dichloroethene 0.50 08-18-2010

70 - 130 10H07187.75 78% ppbv1,2,4-Trichlorobenzene 2.00 08-18-2010

70 - 130 10H07188.76 88% ppbv1,2,4-Trimethylbenzene 0.50 08-18-2010

70 - 130 10H07188.33 83% ppbv1,2-Dibromoethane (EDB) 0.50 08-18-2010

70 - 130 10H07187.54 75% ppbv1,2-Dichlorobenzene 0.50 08-18-2010

70 - 130 10H07188.21 82% ppbv1,2-Dichloroethane 0.50 08-18-2010

70 - 130 10H07187.84 78% ppbv1,2-Dichloropropane 0.50 08-18-2010


70 - 130 10H07188.02 80% ppbv1,3-Butadiene 0.50 08-18-2010



70 - 130 10H07189.16 92% ppbv2,2,4-Trimethylpentane 0.50 08-18-2010

70 - 130 10H07188.79 88% ppbv2-Butanone (MEK) 1.00 08-18-2010

70 - 130 10H07189.28 93% ppbv2-Hexanone 1.00 08-18-2010

70 - 130 10H07188.26 83% ppbv2-Propanol 2.00 08-18-2010

70 - 130 10H07189.11 91% ppbv4-Ethyltoluene 0.50 08-18-2010

70 - 130 10H07189.07 91% ppbv4-Methyl-2-pentanone (MIBK) 1.00 08-18-2010

70 - 130 10H07187.70 77% ppbvAcetone 5.00 08-18-2010

70 - 130 10H07189.49 95% ppbvAllyl Chloride 0.50 08-18-2010

70 - 130 10H07188.10 81% ppbvBenzene 0.50 08-18-2010

70 - 130 10H07188.14 81% ppbvBenzyl Chloride 2.00 08-18-2010

70 - 130 10H07188.78 88% ppbvBromodichloromethane 0.50 08-18-2010

70 - 130 10H07189.43 94% ppbvBromoethene(Vinyl Bromide) 0.50 08-18-2010

70 - 130 10H07189.07 91% ppbvBromoform 0.50 08-18-2010

70 - 130 10H07188.29 83% ppbvBromomethane 0.50 08-18-2010

70 - 130 10H07188.11 81% ppbvCarbon disulfide 0.50 08-18-2010

70 - 130 10H07188.55 86% ppbvCarbon tetrachloride 0.50 08-18-2010

70 - 130 10H07188.59 86% ppbvChlorobenzene 0.50 08-18-2010

70 - 130 10H07187.70 77% ppbvChloroethane 0.50 08-18-2010

70 - 130 10H07188.22 82% ppbvChloroform 0.50 08-18-2010

70 - 130 10H07188.02 80% ppbvChloromethane 0.50 08-18-2010

70 - 130 10H07188.28 83% ppbvcis-1,2-Dichloroethene 0.50 08-18-2010

70 - 130 10H07188.45 84% ppbvcis-1,3-Dichloropropene 0.50 08-18-2010

70 - 130 10H07188.40 84% ppbvCyclohexane 0.50 08-18-2010

70 - 130 10H07188.95 90% ppbvDibromochloromethane 0.50 08-18-2010

70 - 130 10H07188.65 86% ppbvDichlorodifluoromethane 0.50 08-18-2010

70 - 130 10H07187.99 80% ppbvDichlorotetrafluoroethane(F-114) 0.50 08-18-2010

70 - 130 10H07188.60 86% ppbvEthyl Acetate 0.50 08-18-2010

70 - 130 10H07189.05 90% ppbvEthylbenzene 0.50 08-18-2010

Page 9 of 13



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PTH0994

LCS - Cont.


Target



10H0718-BS170 - 130 10H07188.01 80% ppbvFreon 113 0.50 08-18-2010

70 - 130 10H07188.13 81% ppbvHeptane 0.50 08-18-2010

70 - 130 10H07188.18 82% ppbvHexachlorobutadiene 1.00 08-18-2010

70 - 130 10H07188.22 82% ppbvHexane 0.50 08-18-2010

70 - 130 10H07188.46 85% ppbvIsopropylbenzene 0.50 08-18-2010

70 - 130 10H071818.2 91% ppbvm,p-Xylenes 1.00 08-18-2010

70 - 130 10H07187.90 79% ppbvMethylene Chloride 0.50 08-18-2010

70 - 130 10H07188.65 86% ppbvMethyl-tert-butyl Ether (MTBE) 1.00 08-18-2010

70 - 130 10H07188.51 85% ppbvNaphthalene 5.00 08-18-2010

70 - 130 10H07188.38 84% ppbvn-Butylbenzene 0.50 08-18-2010

70 - 130 10H07188.94 89% ppbvn-Nonane 0.50 08-18-2010

70 - 130 10H07189.75 98% ppbvn-Octane 0.50 08-18-2010

70 - 130 10H07187.79 78% ppbvn-Propylbenzene 0.50 08-18-2010

70 - 130 10H07188.73 87% ppbvo-Xylene 0.50 08-18-2010

70 - 130 10H07188.48 85% ppbvPropene 0.50 08-18-2010

70 - 130 10H07188.57 86% ppbvsec-Butylbenzene 0.50 08-18-2010

70 - 130 10H07189.30 93% ppbvStyrene 0.50 08-18-2010

70 - 130 10H07188.53 85% ppbvtert-Butylbenzene 0.50 08-18-2010

70 - 130 10H07188.56 86% ppbvTetrachloroethene 0.50 08-18-2010

70 - 130 10H07188.59 86% ppbvTetrahydrofuran 2.00 08-18-2010

70 - 130 10H07188.54 85% ppbvToluene 0.50 08-18-2010

70 - 130 10H07188.30 83% ppbvtrans-1,2-Dichloroethene 0.50 08-18-2010

70 - 130 10H07188.75 88% ppbvtrans-1,3-Dichloropropene 0.50 08-18-2010

70 - 130 10H07188.44 84% ppbvTrichloroethene 0.50 08-18-2010

70 - 130 10H07188.22 82% ppbvTrichlorofluoromethane 0.50 08-18-2010

70 - 130 10H07188.32 83% ppbvVinyl Acetate 0.50 08-18-2010

70 - 130 10H07188.26 83% ppbvVinyl chloride 0.50 08-18-2010

70 - 130 10H071810.1Surrogate: 4-Bromofluorobenzene 101% 0.50 08-18-2010

UnitsAnalyte

Sample

DuplicatedBatchRPDResult

LCS Dup

Q

Spike

Conc % Rec.

Target

Range Analyzed DateLimitRL


10H0718-BSD18.64 3 30 10H0718 10.0 86%ppbv 70 - 1301,1,1-Trichloroethane 0.50 08-18-2010

7.89 1 30 10H0718 10.0 79%ppbv 70 - 1301,1,2,2-Tetrachloroethane 0.50 08-18-2010

8.58 2 30 10H0718 10.0 86%ppbv 70 - 1301,1,2-Trichloroethane 0.50 08-18-2010

8.28 1 30 10H0718 10.0 83%ppbv 70 - 1301,1-Dichloroethane 0.50 08-18-2010

8.56 4 30 10H0718 10.0 86%ppbv 70 - 1301,1-Dichloroethene 0.50 08-18-2010

Page 10 of 13



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PTH0994

UnitsAnalyte

Sample


LCS Dup - Cont.

Q

Spike

Conc % Rec.

Target



10H0718-BSD17.82 0.9 30 10H0718 10.0 78%ppbv 70 - 1301,2,4-Trichlorobenzene 2.00 08-18-2010

8.78 0.2 30 10H0718 10.0 88%ppbv 70 - 1301,2,4-Trimethylbenzene 0.50 08-18-2010

8.48 2 30 10H0718 10.0 85%ppbv 70 - 1301,2-Dibromoethane (EDB) 0.50 08-18-2010

7.60 0.8 30 10H0718 10.0 76%ppbv 70 - 1301,2-Dichlorobenzene 0.50 08-18-2010


8.08 3 30 10H0718 10.0 81%ppbv 70 - 1301,2-Dichloropropane 0.50 08-18-2010

9.04 3 30 10H0718 10.0 90%ppbv 70 - 1301,3,5-Trimethylbenzene 0.50 08-18-2010

8.27 3 30 10H0718 10.0 83%ppbv 70 - 1301,3-Butadiene 0.50 08-18-2010

7.98 1 30 10H0718 10.0 80%ppbv 70 - 1301,3-Dichlorobenzene 0.50 08-18-2010

7.90 0.8 30 10H0718 10.0 79%ppbv 70 - 1301,4-Dichlorobenzene 0.50 08-18-2010

9.31 2 30 10H0718 10.0 93%ppbv 70 - 1302,2,4-Trimethylpentane 0.50 08-18-2010

9.21 5 30 10H0718 10.0 92%ppbv 70 - 1302-Butanone (MEK) 1.00 08-18-2010

9.54 3 30 10H0718 10.0 95%ppbv 70 - 1302-Hexanone 1.00 08-18-2010

8.45 2 30 10H0718 10.0 84%ppbv 70 - 1302-Propanol 2.00 08-18-2010

9.29 2 30 10H0718 10.0 93%ppbv 70 - 1304-Ethyltoluene 0.50 08-18-2010

9.33 3 30 10H0718 10.0 93%ppbv 70 - 1304-Methyl-2-pentanone (MIBK) 1.00 08-18-2010

7.95 3 30 10H0718 10.0 80%ppbv 70 - 130Acetone 5.00 08-18-2010

9.84 4 30 10H0718 10.0 98%ppbv 70 - 130Allyl Chloride 0.50 08-18-2010

8.24 2 30 10H0718 10.0 82%ppbv 70 - 130Benzene 0.50 08-18-2010

8.30 2 30 10H0718 10.0 83%ppbv 70 - 130Benzyl Chloride 2.00 08-18-2010

8.65 1 30 10H0718 10.0 86%ppbv 70 - 130Bromodichloromethane 0.50 08-18-2010

9.82 4 30 10H0718 10.0 98%ppbv 70 - 130Bromoethene(Vinyl Bromide) 0.50 08-18-2010

9.23 2 30 10H0718 10.0 92%ppbv 70 - 130Bromoform 0.50 08-18-2010

8.39 1 30 10H0718 10.0 84%ppbv 70 - 130Bromomethane 0.50 08-18-2010

8.26 2 30 10H0718 10.0 83%ppbv 70 - 130Carbon disulfide 0.50 08-18-2010

8.83 3 30 10H0718 10.0 88%ppbv 70 - 130Carbon tetrachloride 0.50 08-18-2010

8.59 0 30 10H0718 10.0 86%ppbv 70 - 130Chlorobenzene 0.50 08-18-2010

8.02 4 30 10H0718 10.0 80%ppbv 70 - 130Chloroethane 0.50 08-18-2010

8.40 2 30 10H0718 10.0 84%ppbv 70 - 130Chloroform 0.50 08-18-2010

8.23 3 30 10H0718 10.0 82%ppbv 70 - 130Chloromethane 0.50 08-18-2010

8.60 4 30 10H0718 10.0 86%ppbv 70 - 130cis-1,2-Dichloroethene 0.50 08-18-2010

8.67 3 30 10H0718 10.0 87%ppbv 70 - 130cis-1,3-Dichloropropene 0.50 08-18-2010

8.58 2 30 10H0718 10.0 86%ppbv 70 - 130Cyclohexane 0.50 08-18-2010

9.09 2 30 10H0718 10.0 91%ppbv 70 - 130Dibromochloromethane 0.50 08-18-2010

8.84 2 30 10H0718 10.0 88%ppbv 70 - 130Dichlorodifluoromethane 0.50 08-18-2010

8.21 3 30 10H0718 10.0 82%ppbv 70 - 130Dichlorotetrafluoroethane(F-114) 0.50 08-18-2010

8.70 1 30 10H0718 10.0 87%ppbv 70 - 130Ethyl Acetate 0.50 08-18-2010

9.28 3 30 10H0718 10.0 93%ppbv 70 - 130Ethylbenzene 0.50 08-18-2010

8.23 3 30 10H0718 10.0 82%ppbv 70 - 130Freon 113 0.50 08-18-2010

8.34 3 30 10H0718 10.0 83%ppbv 70 - 130Heptane 0.50 08-18-2010

8.01 2 30 10H0718 10.0 80%ppbv 70 - 130Hexachlorobutadiene 1.00 08-18-2010

8.52 4 30 10H0718 10.0 85%ppbv 70 - 130Hexane 0.50 08-18-2010

Page 11 of 13



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PTH0994

UnitsAnalyte

Sample


LCS Dup - Cont.

Q

Spike

Conc % Rec.

Target



10H0718-BSD18.54 0.9 30 10H0718 10.0 85%ppbv 70 - 130Isopropylbenzene 0.50 08-18-2010

18.0 1 30 10H0718 20.0 90%ppbv 70 - 130m,p-Xylenes 1.00 08-18-2010

8.15 3 30 10H0718 10.0 82%ppbv 70 - 130Methylene Chloride 0.50 08-18-2010

8.85 2 30 10H0718 10.0 88%ppbv 70 - 130Methyl-tert-butyl Ether (MTBE) 1.00 08-18-2010

8.60 1 30 10H0718 10.0 86%ppbv 70 - 130Naphthalene 5.00 08-18-2010

8.44 0.7 30 10H0718 10.0 84%ppbv 70 - 130n-Butylbenzene 0.50 08-18-2010

9.00 0.7 30 10H0718 10.0 90%ppbv 70 - 130n-Nonane 0.50 08-18-2010

9.86 1 30 10H0718 10.0 99%ppbv 70 - 130n-Octane 0.50 08-18-2010

7.93 2 30 10H0718 10.0 79%ppbv 70 - 130n-Propylbenzene 0.50 08-18-2010

8.91 2 30 10H0718 10.0 89%ppbv 70 - 130o-Xylene 0.50 08-18-2010

8.75 3 30 10H0718 10.0 88%ppbv 70 - 130Propene 0.50 08-18-2010

8.71 2 30 10H0718 10.0 87%ppbv 70 - 130sec-Butylbenzene 0.50 08-18-2010

9.59 3 30 10H0718 10.0 96%ppbv 70 - 130Styrene 0.50 08-18-2010

8.76 3 30 10H0718 10.0 88%ppbv 70 - 130tert-Butylbenzene 0.50 08-18-2010

8.71 2 30 10H0718 10.0 87%ppbv 70 - 130Tetrachloroethene 0.50 08-18-2010

8.92 4 30 10H0718 10.0 89%ppbv 70 - 130Tetrahydrofuran 2.00 08-18-2010

8.80 3 30 10H0718 10.0 88%ppbv 70 - 130Toluene 0.50 08-18-2010

8.59 3 30 10H0718 10.0 86%ppbv 70 - 130trans-1,2-Dichloroethene 0.50 08-18-2010

9.01 3 30 10H0718 10.0 90%ppbv 70 - 130trans-1,3-Dichloropropene 0.50 08-18-2010

8.62 2 30 10H0718 10.0 86%ppbv 70 - 130Trichloroethene 0.50 08-18-2010

8.44 3 30 10H0718 10.0 84%ppbv 70 - 130Trichlorofluoromethane 0.50 08-18-2010

8.52 2 30 10H0718 10.0 85%ppbv 70 - 130Vinyl Acetate 0.50 08-18-2010

8.42 2 30 10H0718 10.0 84%ppbv 70 - 130Vinyl chloride 0.50 08-18-2010

10.0 10H0718 10.0 100%Surrogate: 4-Bromofluorobenzene ppbv 70 - 130 0.50 08-18-2010

Page 12 of 13



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PTH0994

CERTIFICATION SUMMARY

Analyses included in this report were performed by TestAmerica Phoenix, 4625 E. Cotton Center Boulevard, Building 3, Suite 189,

Phoenix, AZ 85040.

TestAmerica Phoenix (Lab ID 154268) is accredited by the American Industrial Hygiene Association (AIHA) in the industrial hygiene

program for the analytical techniques noted on the scope of accreditation for the following methods: NIOSH 0500, NIOSH 0600,

NIOSH 1003, NIOSH 1005, NIOSH 1007, NIOSH 1010, NIOSH 1015, NIOSH 1022, NIOSH 1300, NIOSH 1400, NIOSH 1401,


NIOSH 1606, NIOSH 1609, NIOSH 1610, NIOSH 1611, NIOSH, 1613, NIOSH 1615, NIOSH 2000, NIOSH 2016, NIOSH 2532,


NIOSH 7300, NIOSH 7303, NIOSH 7600, NIOSH 7903, NIOSH 9100, NIOSH 9102, EPA IP-6A, EPA IP-6C, OSHA PV2120, OSHA

7, OSHA 42, OSHA 47, OSHA 48, OSHA 64, OSHA 69, OSHA 111, OSHA ID-140, OSHA ID-121, OSHA ID-125G, OSHA IS-215,

OSHA 1001, OSHA 1002, OSHA 1003, OSHA 1004, OSHA 1005 and OSHA Chemical and Sampling Information for Silane. Volatile

organic compounds on 3M Organic Vapor Monitors, Assay Technology Passive Monitors and SKC Passive Monitors. Formaldehyde and

other aldehydes and ketones on Assay Technology Passive Monitor. Aldehydes and ketones by EPA TO-11A.

The TestAmerica Phoenix is also licensed through the State of Arizona (AZ0728) for EPA method TO-15.

TestAmerica Phoenix also holds NELAC accreditation through the State of Oregon (AZ100001) for the analytical techniques noted

on the scope of accreditation and the State of New York (11898) for NIOSH 6009.

Samples were analyzed using methods outlined in references such as:

-OSHA - Occupational Safety and Health Administration, U. S. Department of Labor, OSHA Analytical Methods Manual.

-NIOSH - National Institute for Occupational Safety and Health, U. S. Department of Health and Human Services, NIOSH Manual of

Analytical Methods, Fourth Edition, 1994, and Updates. NIOSH Method 7300 analyses are performed using a modified digestion

procedure to eliminate the use of perchloric acid.

-EPA - U. S. Environmental Protection Agency, Compendium of Methods for the Determination of Toxic Organic Compounds in

Ambient Air, Second Edition, 1999.

-EPA - U. S. Environmental Protection Agency, Analytical Methods, Emission Measurement Center (EMC).

Analytical Comments:

Unless otherwise noted, all method blanks and laboratory control spikes met method and/or laboratory quality control objectives for

the analyses included in this report.

Unless otherwise noted, sample results have been corrected for method blank values.

For information concerning certifications of this facility or another TestAmerica facility, please visit our website at

www.TestAmericaInc.com

Page 13 of 13


Client Contact Information

Canister Samples Chain of Custody Record

TestAmerica Laboratories, Inc. assumes no liability with respect to the collection and shipment of these samples.

2008, TestAmerica Laboratories, Inc. All rights reserved. TestAnierica & Design1"' are trademarks ofTeslAmerica Laboratories, Inc.

Project Manager::R ,.,-". t:i-VI f\1\L_~f(_

TestAmerica Phoenix 4645 E. Cotton Center Blvd; Bldg 3, Ste 189 Phoenix, AZ 85040

Phone 602.437.3340 Fax 602.454.9303

I Page _l_ of _( COCs Company: -1\-M 6-C Goe-6 ~~\ .K ... "" 3'1~- (.)..'('-{ Samples Collected By: s .. Wti!A nb Address: ~~11 r; VI o.de V~&. 3'1 ~mail: I"" City/State/Zip ht:i)'i-K.c;lJ..e. _1.}7_ c c

0 0 Phone: I Site Contact: li) ti ti I "' "' FAX: LAB Contact: Q) .. .. Ill .. ..

Project Name: \"~A ~ ra

~ ~ Analysis Turnaround Time (!) 'C

c c Site: MTS Standard (Specify) a Q) .E .E >< .2:- .2:-PO# o t t1 lo-~;;( il7 1\-S r-D) Rush (Specify) ~ !. ;:; a ;:; "' "' 5 "' c. Q) ~ c. .. .. -.r "' ~ ~ Ill "' :i "' U> .... ra U> .... "' );;, (!) "' !:!:. (.) 0 "' I0~3CJ io :Jilf 0.~~~6.0 (};).'7/ IX l ~ 12 ~ ~ ~11\SrS- tDS.2""G:>O -D~\101DIO ftb 1 ftc .~Jiri;.J H=~ ifo...> 0.4, @.o t;;J..00 ~

-Ol -()Z. I

::>"' 0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

I 0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

0.4, 1.0, 6.0

Special lnstructions/QC Requirements & Comments: c

Samples Shipped by: Datemme: Samples Received by: ./~

2oCj~ Samples Relinquished by: Datemme: / Received by: A I .... /J/1 -~~~,~- Datemmg//7- }0 ICr.>cf& l Rec~ )

l

Lab Use Only Shipper Name: Opened by: Condition: TAL-0042 (02/08)


August 24, 2010

Client:

Attn:

Work Order:

Project Name:

Project Number:

Date Received:

PGAN - TO15

0146821030(SASFS)

PTH1161

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report were

performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless otherwise noted

in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This report shall not be

reproduced, except in full, without written permission from TestAmerica.

TestAmerica Laboratories, Inc., Phoenix Laboratory certifies that the analytical results contained herein apply only to the specific sample(s)

analyzed.

The Chain of Custody, 1 page, is included and is an integral part of this report. This entire report was reviewed and approved for release.

If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-(602)437-3340

08/19/10




Brian Mcnamara

LABORATORY REPORT

Final Report: 08/24/10 16:19

Analyses included in this report were performed by the laboratory shown at the top of this report unless otherwise indicated.

CASE NARRATIVE: SAMPLE RECEIPT: Samples were received intact, at 20C and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in

accordance with the TestAmerica Sample Acceptance Policy unless otherwise noted in the

report.


QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data

qualifiers.


SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information

included in this report.

Approved By:

Project Manager

Carlene McCutcheon

Page 1 of 17



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Brian Mcnamara

Reported: 08/24/10 16:19

PTH1161

SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE CONTAINER TYPE

PTH1161-01SASFS-PDS1-30-08192010 08/19/10 S/N 1334 1L Canister

PTH1161-02SASFS-PDS1-30-08192010Dup 08/19/10 S/N 0237 1L Canister

PTH1161-03SASFS-PDS1-60-08192010 08/19/10 S/N 0616 1L Canister

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PTH1161

ANALYTICAL REPORT

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-01 (SASFS-PDS1-30-08192010) Sampled: 08/19/10 08:311,1,1-Trichloroethane 0.50



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Reported: 08/24/10 16:19

PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-01 (SASFS-PDS1-30-08192010) - cont. Sampled: 08/19/10 08:31Hexachlorobutadiene 1.0



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Received:




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Reported: 08/24/10 16:19

PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-01RE1 (SASFS-PDS1-30-08192010) Sampled: 08/19/10 08:312-Butanone (MEK) 5.025 8/24/2010 bb EPA TO1574 14.7 5.0

Acetone 2576 8/24/2010 bb EPA TO15180 59.4 5.0

Surrogate: 4-Bromofluorobenzene Limit 70-13095 %

Page 5 of 17



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Reported: 08/24/10 16:19

PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-02 (SASFS-PDS1-30-08192010Dup) Sampled: 08/19/10 08:371,1,1-Trichloroethane 0.50



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Received:




Brian Mcnamara

Reported: 08/24/10 16:19

PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-02 (SASFS-PDS1-30-08192010Dup) - cont. Sampled: 08/19/10 08:37m,p-Xylenes 1.0



Work Order:

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PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-02RE1 (SASFS-PDS1-30-08192010Dup) Sampled: 08/19/10 08:372-Butanone (MEK) 5.044 8/24/2010 bb EPA TO15130 14.7 5.0

Acetone 25110 8/24/2010 bb EPA TO15260 59.4 5.0

Propene 2.528 8/24/2010 bb EPA TO1548 4.30 5.0

Surrogate: 4-Bromofluorobenzene Limit 70-13094 %

Page 8 of 17



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PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-03 (SASFS-PDS1-60-08192010) Sampled: 08/19/10 10:071,1,1-Trichloroethane 0.50



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PTH1161

Data


Date

AnalyzedResult PQL

ug/m3ppbv

Dilution


Sample ID: PTH1161-03 (SASFS-PDS1-60-08192010) - cont. Sampled: 08/19/10 10:07Hexachlorobutadiene 1.0



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PTH1161

PROJECT QUALITY CONTROL DATA

Blank



10H0869-BLK1ppbv 10H0869



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PTH1161

Blank - Cont.



10H0869-BLK1ppbv 10H0869



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PTH1161

LCS - Cont.


Target



10H0869-BS170 - 130 10H08699.38 94% ppbv1,1-Dichloroethene 0.50 08-23-2010

70 - 130 10H08697.90 79% ppbv1,2,4-Trichlorobenzene 2.00 08-23-2010


70 - 130 10H086910.5 105% ppbv1,2-Dibromoethane (EDB) 0.50 08-23-2010


70 - 130 10H086911.2 112% ppbv1,2-Dichloroethane 0.50 08-23-2010

70 - 130 10H086910.7 107% ppbv1,2-Dichloropropane 0.50 08-23-2010


70 - 130 10H086910.3 103% ppbv1,3-Butadiene 0.50 08-23-2010



70 - 130 10H086910.4 104% ppbv2,2,4-Trimethylpentane 0.50 08-23-2010

70 - 130 10H086911.4 114% ppbv2-Butanone (MEK) 1.00 08-23-2010

70 - 130 10H086912.1 121% ppbv2-Hexanone 1.00 08-23-2010

70 - 130 10H086911.5 115% ppbv2-Propanol 2.00 08-23-2010

70 - 130 10H08699.94 99% ppbv4-Ethyltoluene 0.50 08-23-2010

70 - 130 10H086911.8 118% ppbv4-Methyl-2-pentanone (MIBK) 1.00 08-23-2010

70 - 130 10H086910.9 109% ppbvAcetone 5.00 08-23-2010

70 - 130 10H086912.1 121% ppbvAllyl Chloride 0.50 08-23-2010

70 - 130 10H086911.7 117% ppbvBenzene 0.50 08-23-2010

70 - 130 10H08699.46 95% ppbvBenzyl Chloride 2.00 08-23-2010

70 - 130 10H08699.30 93% ppbvBromodichloromethane 0.50 08-23-2010

70 - 130 10H086911.9 119% ppbvBromoethene(Vinyl Bromide) 0.50 08-23-2010

70 - 130 10H086911.1 111% ppbvBromoform 0.50 08-23-2010

70 - 130 10H086910.1 101% ppbvBromomethane 0.50 08-23-2010

70 - 130 10H08699.76 98% ppbvCarbon disulfide 0.50 08-23-2010

70 - 130 10H08699.39 94% ppbvCarbon tetrachloride 0.50 08-23-2010

70 - 130 10H086910.9 109% ppbvChlorobenzene 0.50 08-23-2010

70 - 130 10H086910.2 102% ppbvChloroethane 0.50 08-23-2010

70 - 130 10H08699.52 95% ppbvChloroform 0.50 08-23-2010

70 - 130 10H086911.0 110% ppbvChloromethane 0.50 08-23-2010

70 - 130 10H08699.64 96% ppbvcis-1,2-Dichloroethene 0.50 08-23-2010

70 - 130 10H086911.2 112% ppbvcis-1,3-Dichloropropene 0.50 08-23-2010

70 - 130 10H086910.7 107% ppbvCyclohexane 0.50 08-23-2010

70 - 130 10H086910.8 108% ppbvDibromochloromethane 0.50 08-23-2010

70 - 130 10H086910.2 102% ppbvDichlorodifluoromethane 0.50 08-23-2010

70 - 130 10H08699.49 95% ppbvDichlorotetrafluoroethane(F-114) 0.50 08-23-2010

70 - 130 10H086911.3 113% ppbvEthyl Acetate 0.50 08-23-2010

70 - 130 10H086910.3 103% ppbvEthylbenzene 0.50 08-23-2010

Page 13 of 17



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Reported: 08/24/10 16:19

PTH1161

LCS - Cont.


Target



10H0869-BS170 - 130 10H08698.94 89% ppbvFreon 113 0.50 08-23-2010

70 - 130 10H08698.69 87% ppbvHeptane 0.50 08-23-2010

70 - 130 10H08699.10 91% ppbvHexachlorobutadiene 1.00 08-23-2010

70 - 130 10H086910.4 104% ppbvHexane 0.50 08-23-2010

70 - 130 10H08698.94 89% ppbvIsopropylbenzene 0.50 08-23-2010

70 - 130 10H086919.4 97% ppbvm,p-Xylenes 1.00 08-23-2010

70 - 130 10H08699.43 94% ppbvMethylene Chloride 0.50 08-23-2010

70 - 130 10H086910.5 105% ppbvMethyl-tert-butyl Ether (MTBE) 1.00 08-23-2010

70 - 130 10H08698.41 84% ppbvNaphthalene 5.00 08-23-2010

70 - 130 10H086910.2 102% ppbvn-Butylbenzene 0.50 08-23-2010

70 - 130 10H086911.2 112% ppbvn-Nonane 0.50 08-23-2010

70 - 130 10H086911.0 110% ppbvn-Octane 0.50 08-23-2010

70 - 130 10H08698.00 80% ppbvn-Propylbenzene 0.50 08-23-2010

70 - 130 10H08699.50 95% ppbvo-Xylene 0.50 08-23-2010

70 - 130 10H086911.0 110% ppbvPropene 0.50 08-23-2010

70 - 130 10H086910.2 102% ppbvsec-Butylbenzene 0.50 08-23-2010

70 - 130 10H086910.5 105% ppbvStyrene 0.50 08-23-2010

70 - 130 10H086910.1 101% ppbvtert-Butylbenzene 0.50 08-23-2010

70 - 130 10H08698.41 84% ppbvTetrachloroethene 0.50 08-23-2010

70 - 130 10H086911.8 118% ppbvTetrahydrofuran 2.00 08-23-2010

70 - 130 10H086911.7 117% ppbvToluene 0.50 08-23-2010

70 - 130 10H08699.25 92% ppbvtrans-1,2-Dichloroethene 0.50 08-23-2010

70 - 130 10H086912.1 121% ppbvtrans-1,3-Dichloropropene 0.50 08-23-2010

70 - 130 10H08698.19 82% ppbvTrichloroethene 0.50 08-23-2010

70 - 130 10H08699.18 92% ppbvTrichlorofluoromethane 0.50 08-23-2010

70 - 130 10H086911.2 112% ppbvVinyl Acetate 0.50 08-23-2010

70 - 130 10H086910.8 108% ppbvVinyl chloride 0.50 08-23-2010

70 - 130 10H08699.32Surrogate: 4-Bromofluorobenzene 93% 0.50 08-23-2010

UnitsAnalyte

Sample


LCS Dup

Q

Spike

Conc % Rec.

Target



10H0869-BSD18.76 7 30 10H0869 10.0 88%ppbv 70 - 1301,1,1-Trichloroethane 0.50 08-23-2010

8.62 4 30 10H0869 10.0 86%ppbv 70 - 1301,1,2,2-Tetrachloroethane 0.50 08-23-2010

8.97 16 30 10H0869 10.0 90%ppbv 70 - 1301,1,2-Trichloroethane 0.50 08-23-2010


9.06 3 30 10H0869 10.0 91%ppbv 70 - 1301,1-Dichloroethene 0.50 08-23-2010

Page 14 of 17



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Received:




Brian Mcnamara

Reported: 08/24/10 16:19

PTH1161

UnitsAnalyte

Sample


LCS Dup - Cont.

Q

Spike

Conc % Rec.

Target



10H0869-BSD18.22 4 30 10H0869 10.0 82%ppbv 70 - 1301,2,4-Trichlorobenzene 2.00 08-23-2010


8.98 15 30 10H0869 10.0 90%ppbv 70 - 1301,2-Dibromoethane (EDB) 0.50 08-23-2010



8.94 18 30 10H0869 10.0 89%ppbv 70 - 1301,2-Dichloropropane 0.50 08-23-2010


9.43 9 30 10H0869 10.0 94%ppbv 70 - 1301,3-Butadiene 0.50 08-23-2010



10.1 3 30 10H0869 10.0 101%ppbv 70 - 1302,2,4-Trimethylpentane 0.50 08-23-2010

10.1 12 30 10H0869 10.0 101%ppbv 70 - 1302-Butanone (MEK) 1.00 08-23-2010

11.2 8 30 10H0869 10.0 112%ppbv 70 - 1302-Hexanone 1.00 08-23-2010

9.61 18 30 10H0869 10.0 96%ppbv 70 - 1302-Propanol 2.00 08-23-2010

10.3 3 30 10H0869 10.0 103%ppbv 70 - 1304-Ethyltoluene 0.50 08-23-2010

10.8 9 30 10H0869 10.0 108%ppbv 70 - 1304-Methyl-2-pentanone (MIBK) 1.00 08-23-2010

8.88 20 30 10H0869 10.0 89%ppbv 70 - 130Acetone 5.00 08-23-2010

11.4 6 30 10H0869 10.0 114%ppbv 70 - 130Allyl Chloride 0.50 08-23-2010

10.6 10 30 10H0869 10.0 106%ppbv 70 - 130Benzene 0.50 08-23-2010

9.40 0.6 30 10H0869 10.0 94%ppbv 70 - 130Benzyl Chloride 2.00 08-23-2010

9.02 3 30 10H0869 10.0 90%ppbv 70 - 130Bromodichloromethane 0.50 08-23-2010

10.6 11 30 10H0869 10.0 106%ppbv 70 - 130Bromoethene(Vinyl Bromide) 0.50 08-23-2010

10.1 9 30 10H0869 10.0 101%ppbv 70 - 130Bromoform 0.50 08-23-2010

8.91 12 30 10H0869 10.0 89%ppbv 70 - 130Bromomethane 0.50 08-23-2010

9.05 8 30 10H0869 10.0 90%ppbv 70 - 130Carbon disulfide 0.50 08-23-2010

8.75 7 30 10H0869 10.0 88%ppbv 70 - 130Carbon tetrachloride 0.50 08-23-2010

9.65 12 30 10H0869 10.0 96%ppbv 70 - 130Chlorobenzene 0.50 08-23-2010

8.96 13 30 10H0869 10.0 90%ppbv 70 - 130Chloroethane 0.50 08-23-2010

8.93 6 30 10H0869 10.0 89%ppbv 70 - 130Chloroform 0.50 08-23-2010

9.39 16 30 10H0869 10.0 94%ppbv 70 - 130Chloromethane 0.50 08-23-2010

8.98 7 30 10H0869 10.0 90%ppbv 70 - 130cis-1,2-Dichloroethene 0.50 08-23-2010

10.1 11 30 10H0869 10.0 101%ppbv 70 - 130cis-1,3-Dichloropropene 0.50 08-23-2010

9.99 7 30 10H0869 10.0 100%ppbv 70 - 130Cyclohexane 0.50 08-23-2010

10.1 7 30 10H0869 10.0 101%ppbv 70 - 130Dibromochloromethane 0.50 08-23-2010

9.09 11 30 10H0869 10.0 91%ppbv 70 - 130Dichlorodifluoromethane 0.50 08-23-2010

8.58 10 30 10H0869 10.0 86%ppbv 70 - 130Dichlorotetrafluoroethane(F-114) 0.50 08-23-2010

10.2 11 30 10H0869 10.0 102%ppbv 70 - 130Ethyl Acetate 0.50 08-23-2010

10.3 0.2 30 10H0869 10.0 103%ppbv 70 - 130Ethylbenzene 0.50 08-23-2010

8.52 5 30 10H0869 10.0 85%ppbv 70 - 130Freon 113 0.50 08-23-2010

8.35 4 30 10H0869 10.0 84%ppbv 70 - 130Heptane 0.50 08-23-2010

9.40 3 30 10H0869 10.0 94%ppbv 70 - 130Hexachlorobutadiene 1.00 08-23-2010

9.74 7 30 10H0869 10.0 97%ppbv 70 - 130Hexane 0.50 08-23-2010

Page 15 of 17



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Brian Mcnamara

Reported: 08/24/10 16:19

PTH1161

UnitsAnalyte

Sample


LCS Dup - Cont.

Q

Spike

Conc % Rec.

Target



10H0869-BSD19.09 2 30 10H0869 10.0 91%ppbv 70 - 130Isopropylbenzene 0.50 08-23-2010

20.8 7 30 10H0869 20.0 104%ppbv 70 - 130m,p-Xylenes 1.00 08-23-2010

8.93 5 30 10H0869 10.0 89%ppbv 70 - 130Methylene Chloride 0.50 08-23-2010

9.76 8 30 10H0869 10.0 98%ppbv 70 - 130Methyl-tert-butyl Ether (MTBE) 1.00 08-23-2010

8.73 4 30 10H0869 10.0 87%ppbv 70 - 130Naphthalene 5.00 08-23-2010

10.8 5 30 10H0869 10.0 108%ppbv 70 - 130n-Butylbenzene 0.50 08-23-2010

10.6 5 30 10H0869 10.0 106%ppbv 70 - 130n-Nonane 0.50 08-23-2010

10.7 3 30 10H0869 10.0 107%ppbv 70 - 130n-Octane 0.50 08-23-2010

8.23 3 30 10H0869 10.0 82%ppbv 70 - 130n-Propylbenzene 0.50 08-23-2010

9.90 4 30 10H0869 10.0 99%ppbv 70 - 130o-Xylene 0.50 08-23-2010

9.94 10 30 10H0869 10.0 99%ppbv 70 - 130Propene 0.50 08-23-2010

10.5 3 30 10H0869 10.0 105%ppbv 70 - 130sec-Butylbenzene 0.50 08-23-2010

10.8 3 30 10H0869 10.0 108%ppbv 70 - 130Styrene 0.50 08-23-2010

10.4 3 30 10H0869 10.0 104%ppbv 70 - 130tert-Butylbenzene 0.50 08-23-2010

8.29 1 30 10H0869 10.0 83%ppbv 70 - 130Tetrachloroethene 0.50 08-23-2010

10.6 11 30 10H0869 10.0 106%ppbv 70 - 130Tetrahydrofuran 2.00 08-23-2010

9.42 21 30 10H0869 10.0 94%ppbv 70 - 130Toluene 0.50 08-23-2010

8.95 3 30 10H0869 10.0 90%ppbv 70 - 130trans-1,2-Dichloroethene 0.50 08-23-2010

9.94 20 30 10H0869 10.0 99%ppbv 70 - 130trans-1,3-Dichloropropene 0.50 08-23-2010

8.07 1 30 10H0869 10.0 81%ppbv 70 - 130Trichloroethene 0.50 08-23-2010

8.57 7 30 10H0869 10.0 86%ppbv 70 - 130Trichlorofluoromethane 0.50 08-23-2010

10.2 10 30 10H0869 10.0 102%ppbv 70 - 130Vinyl Acetate 0.50 08-23-2010

9.37 15 30 10H0869 10.0 94%ppbv 70 - 130Vinyl chloride 0.50 08-23-2010

10.1 10H0869 10.0 101%Surrogate: 4-Bromofluorobenzene ppbv 70 - 130 0.50 08-23-2010

Page 16 of 17



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Brian Mcnamara

Reported: 08/24/10 16:19

PTH1161

CERTIFICATION SUMMARY

Analyses included in this report were performed by TestAmerica Phoenix, 4625 E. Cotton Center Boulevard, Building 3, Suite 189,

Phoenix, AZ 85040.

TestAmerica Phoenix (Lab ID 154268) is accredited by the American Industrial Hygiene Association (AIHA) in the industrial hygiene

program for the analytical techniques noted on the scope of accreditation for the following methods: NIOSH 0500, NIOSH 0600,



NIOSH 1606, NIOSH 1609, NIOSH 1610, NIOSH 1611, NIOSH, 1613, NIOSH 1615, NIOSH 2000, NIOSH 2016, NIOSH 2532,


NIOSH 7300, NIOSH 7303, NIOSH 7600, NIOSH 7903, NIOSH 9100, NIOSH 9102, EPA IP-6A, EPA IP-6C, OSHA PV2120, OSHA

7, OSHA 42, OSHA 47, OSHA 48, OSHA 64, OSHA 69, OSHA 111, OSHA ID-140, OSHA ID-121, OSHA ID-125G, OSHA IS-215,

OSHA 1001, OSHA 1002, OSHA 1003, OSHA 1004, OSHA 1005 and OSHA Chemical and Sampling Information for Silane. Volatile

organic compounds on 3M Organic Vapor Monitors, Assay Technology Passive Monitors and SKC Passive Monitors. Formaldehyde and

other aldehydes and ketones on Assay Technology Passive Monitor. Aldehydes and ketones by EPA TO-11A.

The TestAmerica Phoenix is also licensed through the State of Arizona (AZ0728) for EPA method TO-15.

TestAmerica Phoenix also holds NELAC accreditation through the State of Oregon (AZ100001) for the analytical techniques noted

on the scope of accreditation and the State of New York (11898) for NIOSH 6009.

Samples were analyzed using methods outlined in references such as:

-OSHA - Occupational Safety and Health Administration, U. S. Department of Labor, OSHA Analytical Methods Manual.

-NIOSH - National Institute for Occupational Safety and Health, U. S. Department of Health and Human Services, NIOSH Manual of

Analytical Methods, Fourth Edition, 1994, and Updates. NIOSH Method 7300 analyses are performed using a modified digestion

procedure to eliminate the use of perchloric acid.

-EPA - U. S. Environmental Protection Agency, Compendium of Methods for the Determination of Toxic Organic Compounds in

Ambient Air, Second Edition, 1999.

-EPA - U. S. Environmental Protection Agency, Analytical Methods, Emission Measurement Center (EMC).

Analytical Comments:

Unless otherwise noted, all method blanks and laboratory control spikes met method and/or laboratory quality control objectives for

the analyses included in this report.

Unless otherwise noted, sample results have been corrected for method blank values.

For information concerning certifications of this facility or another TestAmerica facility, please visit our website at

www.TestAmericaInc.com

Page 17 of 17

Test America CHAIN. OF CUSTODY FORM [ 1 Phoenix- 4625 E Cotton Center Blvd Suite 189 Phoenix AZ 85040 (602) 437-3340 FAX (602) 454 9303 ., , ' -

THE LEADER IN ENVIRONMENTAL TESTING [ 1 Tucson -1870 W. Prince Road, Suite 59, Tucson, AZ 85705 (520) 807-3801 FAX (520) 807-3803 \ TAL-0013-550 (12/08) [ 1 Las Vegas - 2520 E. Sunset, Suite 3, L!:!S Vegas, NV 89120 (702) 798-3620 FAX (702) 798-3621 Page I of l"' ~/Add'""' . Project/ P.O Numher: . An.alysis Hequired 11ft 6MX . . _ . -. . 6 ll..f 0 fA lp ?iJ

f) '1 'l 5 ~ \] ~ cu3e V ~-t-'~'fl,l.ru. ) S k 1 '1G: [Strs0 J Sc.om tied~ fr?.~ G ~t Manage~N 'Phone Number: ~ 4 V\ t~xA lf81J -3 4.

4625 East Cotton Center Blvd. Ste 189, Phoenix, AZ 85040 (602) 437-3340 Fax:(602)

454-9303

LABORATORY REPORT

Prepared For: AMEC Geomatrix Consultants, Inc. - AZ - PGAN



Attention: Brian Mcnamara 03/04/09

03/04/09

08/03/09 13:37

The results listed within this Laboratory Report pertain only to the samples tested in the laboratory. The analyses contained in this report

were performed in accordance with the applicable certifications as noted. All soil samples are reported on a wet weight basis unless

otherwise noted in the report. This Laboratory Report is confidential and is intended for the sole use of TestAmerica and its client. This

report shall not be reproduced, except in full, without written permission from TestAmerica. The Chain(s) of Custody, 2 pages, are

included and are an integral part of this report.

This entire report was reviewed and approved for release.

Sampled:

Received:

Revised:

Project: 14682.013.0

NELAP #01109CA Arizona DHS#AZ0728

CASE NARRATIVE

MATRIXCLIENT IDLABORATORY ID

PSC0231-01 SASFS-B103-0.5-03042009 Soil

PSC0231-02 SASFS-BJ14-0.5-03042009 Soil

PSC0231-03 SASFS-BJ14-0.5-03042009FD Soil

PSC0231-04 SASFS-BK03-0.5-03042009 Soil

PSC0231-05 SASFS-BC06-0.5-03042009 Soil

PSC0231-06 SASFS-BG08-0.5-03042009 Soil

PSC0231-07 SASFS-B014-0.5-03042009 Soil

PSC0231-08 SASFS-B014-0.5-03042009FD Soil

PSC0231-09 SASFS-BE04-0.5-03042009 Soil

PSC0231-10 SASFS-B905-0.5-03042009 Soil

PSC0231-11 SASFS-B703-1.5-03042009 Soil

PSC0231-12 SASFS-B1104-0.5-03042009 Soil

PSC0231-13 SASFS-BH04-0.5-03042009 Soil

PSC0231-14 SASFS-EB1-03042009 Water

Project Manager

TestAmerica Phoenix

PSC0231

Tina Paulauskas


454-9303




Attention: Brian Mcnamara

Sampled:

Received:

03/04/09

03/04/09Report Number:

Project ID:

PSC0231

14682.013.0

SAMPLE RECEIPT: Samples were received intact, at 2C, on ice and with chain of custody documentation.

HOLDING TIMES: All samples were analyzed within prescribed holding times and/or in accordance with the TestAmerica

Sample Acceptance Policy unless otherwise noted in the report.


QA/QC CRITERIA: All analyses met method criteria, except as noted in the report with data qualifiers.

N1-The RPD exceeded the acceptance limit due to sample matrix effects.

R1-The RPD exceeded the acceptance limit.


SUBCONTRACTED: Refer to the last page for specific subcontract laboratory information included in this report.

Chain-of-Custody requests Percent Moisture and Percent Solids on samples -01 through -05. Per client

request, Percent Moisture and Percent Solids have been analyzed on every soil sample.

Original report was issued on 03/23/09. Due to a laboratory error, the Cyanide results were miscalculated

and reported incorrectly. This revised report includes the corrected Cyanide results.

ADDITIONAL

INFORMATION:

Reviewed By:

Project Manager

TestAmerica Phoenix

PSC0231

Tina Paulauskas

The results pertain only to the samples tested in the laboratory. This report shall not be reproduced,

except in full, without written permission from TestAmerica.


454-9303





Sampled:

Received:

03/04/09


Project ID:

PSC0231

14682.013.0

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

POLYCHLORINATED BIPHENYLS (EPA 3550/8082)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSC0231-12 (SASFS-B1104-0.5-03042009 - Soil) Sampled: 03/04/09

Reporting Units: mg/kg dry

3/6/20093/4/2009SW8082Aroclor 1016 0.058P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1221 0.058P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1232 0.058P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1242 0.12P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1248 0.058P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1254 0.058P9C0407 1ND

3/6/20093/4/2009SW8082Aroclor 1260 0.058P9C0407 1ND

69 %Surrogate: Decachlorobiphenyl (11-131%)

53 %Surrogate: Tetrachloro-m-xylene (29-147%)

Project Manager

TestAmerica Phoenix

PSC0231

Tina Paulauskas




454-9303





Sampled:

Received:

03/04/09


Project ID:

PSC0231

14682.013.0

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

POLYCHLORINATED BIPHENYLS BY GC (EPA 3510/8082)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSC0231-14 (SASFS-EB1-03042009 - Water) Sampled: 03/04/09

Reporting Units: ug/l

3/14/20093/11/2009SW8082Aroclor 1016 1.0P9C1203 V11ND

3/14/20093/11/2009SW8082Aroclor 1221 1.0P9C1203 1ND

3/14/20093/11/2009SW8082Aroclor 1232 1.0P9C1203 1ND

3/14/20093/11/2009SW8082Aroclor 1242 1.0P9C1203 1ND

3/14/20093/11/2009SW8082Aroclor 1248 1.0P9C1203 1ND

3/14/20093/11/2009SW8082Aroclor 1254 1.0P9C1203 1ND

3/14/20093/11/2009SW8082Aroclor 1260 1.0P9C1203 1ND

90 %Surrogate: Tetrachloro-m-xylene (10-140%)

98 %Surrogate: Decachlorobiphenyl (10-133%)

Project Manager

TestAmerica Phoenix

PSC0231

Tina Paulauskas




454-9303





Sampled:

Received:

03/04/09


Project ID:

PSC0231

14682.013.0

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOPHOSPHORUS PESTICIDES (EPA 8141A)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSC0231-01 (SASFS-B103-0.5-03042009 - Soil) Sampled: 03/04/09


3/14/20093/9/2009SW8141AChlorpyrifos 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141ADemeton, Total 0.52P9C0921 0.998ND

3/14/20093/9/2009SW8141ADiazinon 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141ADisulfoton 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141AEthion 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141AFenthion 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141AMalathion 0.26P9C0921 V10.998ND

3/14/20093/9/2009SW8141AMethyl parathion 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141AParathion 0.26P9C0921 0.998ND

3/14/20093/9/2009SW8141APhosmet NAP9C0921 0.998ND

10 % S6Surrogate: TPP (18-140%)

37 %Surrogate: Tributylphosphate (28-135%)

Sample ID: PSC0231-02 (SASFS-BJ14-0.5-03042009 - Soil) Sampled: 03/04/09






3/14/20093/9/2009SW8141AEthion 0.26P9C0921 0.996ND




3/14/20093/9/2009SW8141AParathion 0.26P9C0921 0.996ND

3/14/20093/9/2009SW8141APhosmet NAP9C0921 0.996ND

9 % S6Surrogate: TPP (18-140%)


Project Manager

TestAmerica Phoenix

PSC0231

Tina Paulauskas




454-9303





Sampled:

Received:

03/04/09


Project ID:

PSC0231

14682.013.0

Analyte Method

Date

Extracted

Date

Analyzed

Dilution

Factor

ORGANOPHOSPHORUS PESTICIDES (EPA 8141A)

Data

QualifiersBatch

Reporting

Limit

Sample

Result

Sample ID: PSC0231-03 (SASFS-BJ14-0.5-03042009FD - Soil) Sampled: 03/04/09


3/14/20093/9/2009SW8141AChlorpyrifos 0.26P9C0921 1ND

3/14/20093/9/2009SW8141ADemeton, Total 0.52P9C0921 1ND

3/14/20093/9/2009SW8141ADiazinon 0.26P9C0921 1ND

3/14/20093/9/2009SW8141ADisulfoton 0.26P9C0921 1ND

3/14/20093/9/2009SW8141AEthion 0.26P9C0921 1ND

3/14/20093/9/2009SW8141AFenthion 0.26P9C0921 1ND

3/14/20093/9/2009SW8141AMalathion 0.26P9C0921 V11ND

3/14/20093/9/2009SW8141AMethyl parathion 0.26P9C0921 1ND

3/14/20093/9/2009SW8141AParathion 0.26P9C0921 1ND

3/14/20093/9/2009SW8141APhosmet NAP9C0921 1ND

21 %Surrogate: TPP (18-140%)


Sample ID: PSC0231-04 (SASFS-BK03-0.5-03042009 - Soil) Sampled: 03/04/09






3/13/20093/9/2009SW8141AEthion 0.26P9C0921 0.998ND




3/13/20093/9

Documents

Radiation Safety Engineering, Inc. · Samples requiring preservation were verified prior to sample analysis. See attached report from subcontracted laboratory for QA/QC information