1 SPF-015 (Rev.C1)

MODIFICATION TRAVELERPrepared For the U.S. Department of Energy, Assistant Secretary for Environmental ManagementBy Washington River Protection Solutions, LLC., PO Box 850, Richland, WA 99352Contractor For U.S. Department of Energy, Office of River Protection, under Contract DE-AC27-08RV14800

TRADEMARK DISCLAIMER: Reference herein to any specific commercial product, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States government or any agency thereof or its contractors or subcontractors. Printed in the United States of America.

Release Stamp

1. MT No: MT-50398 Rev. 00

2. Title: 222-SL Modular Design Requirements

SECTION I REQUEST FOR MODIFICATION3. Requested Completion Date (Optional):

09/30/20204. CACN (optional): Clearance Review Restriction Type:

undefined 5. Project Number: ☐ N/A T1P116

6. Design Type:☐ I ☒ II ☐ III ☐ IV ☐ V ☐ VI

7. Project Type: 1

8. Workflow Approval Status:

9. Design Authority Designator: PRJ - 222-SL COLD LAB (T1P116)

10. Related Structures, Systems, and Componentsa. Related Building/Facilities ☐ N/A b. Related Systems ☒ N/A c. Related Equipment ID Nos. (EIN) ☒ N/A222-S222-SL

11. Problem DescriptionThe 222-SA Laboratory was constructed in the early 1980s, and was used to receive and store the chemicals used in performing the cold (i.e. nonradiological) analytical techniques within the 222-S Laboratory. Over the years, the roof of 222-SA had leaked several times, water damage had affected the flooring and sub-flooring such that sagging had occurred at several locations. The Heating, Ventilation, and Air Conditioning (HVAC) system was outdated and could not adequately handle the weather changes and electrically there were insufficient outlets for the work load. In 2015, 222-SA was demolished as part of the 222-S Lab Life Extension Plan.

12. JustificationTo support the 222-S Lab and WRPS Tank Farm Missions, a replacement facility needs to be built to handle the nonradiological analytical techniques. The proposed 222-SL Laboratory would meet this need. It would handl the reciept and storage of chemicals used in cold (nonradiological) analytical techniques, and it would provide more nonradiological laboratory space for theses processes, thus freeing up Radiological Space in 222-S Laboratory which is designed to support that work.

SECTION II REQUIRED FOR DESIGN TYPE 1 PROJECTS13. Project Design Review Required

(TFC-ENG-DESIGN-D-17.1)?14. Major Modification Evaluation Required

(Use 1189 Checklist)?15. Safety In Design Strategy Required?

☐ Yes ☒ No ☐ N/A ☐ Yes ☒ No ☐ N/A ☐ Yes ☐ No ☒ N/A

SECTION III PROPOSED SOLUTION16. Proposed SolutionThe new Cold Lab Facility will be located on the southeast corner of the 222-S site, designated as Building 222-SL. The overall building size is approximately 10,000 square feet, consisting of the following spaces:

Organic Analysis Room, Inorganic Analysis Room, Process Chemistry Room, Standards Room, Storage Room, Receiving Room, Janitors Closet, Men’s and Women’s Restrooms, Break/Conference Room, Mechanical / Electrical Equipment Room, and Gas Bottle Storage Area.

The building foundation will be constructed of cast-in-place reinforced concrete; the building will be modular construction. Heating, Ventilation, and Air-Conditioning for the 222-SA Cold Lab will consist of independent supply and exhaust systems. The outdoor-supply HVAC air systems will provide tempered air for heating and cooling and fresh air to meet ASHRAE requirements. A new electrical service and a new local, manual, fully addressable, low-energy fire alarm system will be installed for the 222-SL Cold Laboratory.

SECTION IV DESIGN INPUT RECORD

17. Design Inputs ☒ N/AType of Document Document Number Rev. Title

18. Other Design Input Requirements:See attached Design Requirements.

19. Other Design Input Considerations:

20. Preliminary Safety Classification:☐ SC ☐ SS ☒ GS ☐ N/A

21. Environmental Risk:(TFC-ENG-DESIGN-C-52 Att. D)☒ Yes ☐ No

22. Radiological Risk:(TFC-ENG-DESIGN-C-52 Att. D)☐ Yes ☒ No

23. Hazard Category<3 Radiological

24. Approval DesignatorsEDL-M, EDL-CS, R, S, F, EDL-E, E, EDL-V

SECTION V IMPACTS

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MODIFICATION TRAVELER MT No.: MT-50398 Rev. 00

2 SPF-015 (Rev.C1)

25. Impacted Documents ☐ N/AType of Document Document Number Rev. Title

26. Other Impacts

SECTION VI DESIGN OUTPUT RECORD

27. Design Outputs ☐ N/AType of Document Document Number Rev. Title 28. Work Package Numbers: ☐ N/A

29. Other Outputs

SECTION VII DESIGN INPUT AND CLOSURE APPROVALS

30. ApprovalsTitle Name Signature DateDesign Authority Design Input Approval Melvin, Max ADesign Authority Manager Lucas, DanDesign Engineering Green, Timothy MEngineering Discipline Lead-Civil/Structural Mackey, TomEngineering Discipline Lead-Electrical Rambo, Charles LEngineering Discipline Lead-Mechanical Goessmann, Glen EEngineering Discipline Lead-Ventilation Khabir, SharokFire Protection Keene, James ROriginator Melvin, Max ARadiological Control Marks, JeffIndustrial Safety Sullivan, Frank JSpecialty Approver Design Input Approval Smith, Brian L

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222-SL Modular Building Design Requirements

1.0 Architectural:1.1 Building size approximately 10000 SF, consisting of:

1.1.1 Process Chemistry Room1.1.2 Organic Analysis Room1.1.3 IH Analysis Room1.1.4 HPLC Lab1.1.5 Standards Lab1.1.6 Sample Receiving Room1.1.7 Chemical Storage Room1.1.8 Mechanical/Electrical Equipment Room1.1.9 Standards Lab Admin Room1.1.10 Break/Conference Room1.1.11 Janitor Room1.1.12 Storage Room1.1.13 Men’s and Women’s Restrooms1.1.14 Lab Coat Rooms (2)

1.2 Refrigerators, freezers, ovens, and other analytical equipment will be provided and installed by others, however, all need to be accounted for in the design of this modular space.

1.3 Due to the sensitive nature of several of the processes being performed and the instrumentation being used it is requested that the design reduce external vibrations where possible.

1.4 HVAC system, Electrical System, Floor Plan, and Fire Protection shall be designed based on the analytical equipment required as documented as part of these requirements.

2.0 Civil:2.1 Sanitary Water

2.1.1 Sanitary (potable) water is supplied from a 6” SW-CI line west of the proposed footprint. Existing Sanitary water line pressure is 110 psi.

2.1.2 Restrooms and Break/Conference room need to support approximately 31 people working 5 days/wk, 10 hour days.

2.1.3 The restrooms and break/conference room will drain to the sanitary sewer system. 2.1.4 Underground service piping shall be designed, installed and tested in accordance with

NFPA 24, Standard for the Installations of Private Fire Service Mains and the Appurtenances.

2.1.5 Modular Design is required to design the restroom and break/conference room sanitary water needs based on the above information. 2.1.5.1 Sanitary Sewer lift station designed and installed by others.

2.2 Process Water2.2.1 Process water will route to 207-SL Basin via the existing 207-SL Lift Station located on

the west side of the footprint. 2.2.1.1 All process sinks shall drain to 207-SL Lift Station

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2.2.1.2 All safety showers and eyewash stations shall drain to the 207-SL Lift Station.

3.0 Structural:3.1 The 222-SL Laboratory is a general service cold (non-radiological) laboratory. The modular

structure shall be designed to the following as defined in TFC-ENG-STD-063.1.1 The Natural Phenomena Design Categories (NDC) for the 222-SL Laboratory shall be NDC

– 1.3.1.2 Section 3.4.2 for anchorage of equipment shall apply, ACI-318, Building Code

Requirements for Structural Concrete.3.1.3 Section 3.5 for Design Loads is applicable.

3.1.3.1 Section 3.5.3 Snow Loads, the Precipitation Design Category (PDC) shall be PDC-1.

3.1.3.2 Section 3.5.4 Wind Loads, the Wind Design Category (WDC) shall be WDC-1. 3.1.3.3 Section 3.5.5 Seismic Loads refers to DOE-STD-1020-2016 which provides

seismic design and evaluation criteria based on Seismic Design Category (SDC). The 222-SL Laboratory shall meet SDC-1 and have a Limit State A per Table 5 of TFC-ENG-STD-06. Sections 3.5.5.1 and 3.5.5.2 are applicable from TFC-ENG-STD-06.

3.1.3.4 Section 3.5.6 Ashfall loads, the Volcanic Design Category (VDC) shall be VDC-1.

3.1.4 Section 3.6, Design Acceptance Criteria, design shall meet or exceed IBC and ASCE7.3.1.4.1 Section 3.6.1 is applicable.3.1.4.2 Section 3.6.2 is applicable.3.1.4.3 Section 3.6.8 is applicable.3.1.4.4 Section 3.6.9 is applicable.3.1.4.5 Section 3.6.10 is applicable.3.1.4.6 Section 3.6.11 is applicable.3.1.4.7 Section 3.6.12 is applicable.3.1.4.8 Section 3.6.15 is applicable.3.1.4.9 Section 3.6.16 is applicable.3.1.4.10 Section 3.6.17 – Pressure Vessels is applicable.3.1.4.11 Section 3.6.20 is applicable – See HVAC Requirements.

3.1.5 Section 3.7 is applicable.3.2 The 222-SL shall be installed on Slab-on-grade. 3.3 Site Topographical Survey, performed on 6/9/16, is attached.3.4 Applicable Codes and Standards:

3.4.1 ACI 318 - Building Code Requirements for Structural Concrete and Commentary3.4.2 AISC 341 - Seismic Design Manual3.4.3 ANSI-ANS 2.263.4.4 ASCE 73.4.5 DOE O 252.1A, Technical Standards Program.3.4.6 DOE O 420.1C, Facility Safety.3.4.7 DOE-RL-92-36, Hanford Site Hoisting and Rigging Manual3.4.8 DOE-STD-1020-2016, Natural Phenomena Hazards Analysis and Design

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3.4.9 DOE STD-1189-2016, Integration of Safety into the Design Process.3.4.10 DOE-STD-1090-2011, Hoisting and Rigging.3.4.11 IBC - International Building Code3.4.12 NFPA 101 Life Safety Code3.4.13 TFC-ENG-STD-06, Design Loads for Tank Farm Facilities3.4.14 TFC-ESHQ-S-STD-28, Hoisting and Rigging 3.4.15 TFC-ENG-FACSUP-C-25, Hoisting and Rigging 3.4.16 WAC 296-150F, Factory-Built Housing and Commercial Structures.

4.0 Mechanical:4.1 Water Systems

4.1.1 Provide Sanitary (potable) cold and hot water to Men’s and Women’s restrooms, break room, and janitor’s closet.

4.1.2 Process water system will provide cold and hot water to lab sinks and lab related equipment.

4.1.3 Meeting held on June 20, 2016 at 12:00PM to determine the building classification with the Water Purveyor. An Air gap design associated with cross-connection control is not required as the new facility was not deemed a "Severe" categorization by the water purveyor. An additional backflow prevention device needs to be provided on domestic water supply.

4.1.4 The Organic Analysis Lab requires Liquid Nitrogen4.1.5 Conditioned water - Provide central reverse osmosis system.

4.1.5.1 RO Water is needed in the Standards Lab 4.1.5.2 RO Water to be provided at one sink in the Process Chemistry Lab. 4.1.5.3 Polished water is needed in the IH Analysis and Standards Lab. 4.1.5.4 These units can drain to the process sinks and out to the 207-SL Lift Station.

4.1.6 Safety Showers and Eyewash Stations are required4.1.6.1 Design for one safety shower/eyewash station to go off at a time, meaning

that when a safety shower/eyewash station is used only that unit goes off.4.1.6.2 ANSI/ISEA Z358.1 provides specific requirements for water supplied to

emergency fixtures.4.1.6.3 Floor drains shall be provided and shall drain the 207-SL Lift Station.

4.1.7 Applicable Codes and Standards:4.1.7.1 ASME B31.3 - Process Piping4.1.7.2 ASME B31.9 - Building Services Piping4.1.7.3 NFPA 24, Standard for the Installations of Private Fire Service Mains and the

Appurtenances4.1.7.4 TFC-ENG-STD-47, Piping Data Specification Standard.4.1.7.5 Uniform Plumbing Code

4.2 Gases 4.2.1 Vacuum, compressed air, Nitrogen, Oxygen, and Helium gases are required to service

the rooms. See Table 1 - Analytical Instrumentation and Equipment Schedule for list of gases required in each room.

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4.2.2 Provide filtration system for gases as per designs for 222-S Laboratory Room Upgrades, 4S, 1G-B, 4C and 4N. Mechanical Drawings for room 4N included for Design Input Consideration. H-2--836809 Sh. 1-7.

4.2.3 All Gas piping systems shall meet the Ultra High Purity cleanliness requirements of ASTM G93 Level C.

4.2.4 Provide centralized vacuum system in all lab rooms.4.2.5 Two hydrogen generators are required. Plan for 4 GC/MS units running on hydrogen.4.2.6 Applicable Codes and Standards

4.2.6.1 ASTM G93, 2011 - Standard Practice for Cleaning Methods and Cleanliness Levels for Material and Equipment Used in Oxygen-Enriched Environments

4.3 Heating, Ventilation, and Air Condition (HVAC)4.3.1 THE HVAC system shall be designed with the equipment list provided.4.3.2 222-SL is a classified as a general service and shall be designed to NDC-1 requirements

per TFC-ENG-STD-06 (see structural above). 222-SL is classified as an Industrial Occupancy as defined by NFPA 101 and as a F-1 Occupancy as defined by International Building Code.

4.3.3 Design, fabrication, construction, testing, and commissioning of the 222-SL facility shall comply with the applicable implementing codes and standards as specified in TFC-ENG-STD-07, Ventilation System Design Standard.4.3.3.1 Section 3.2.1 Safety Classification lists the 222-S Laboratory as a General

Service facility in accordance with HNF-12125, 222-S Laboratory Documented Safety Analysis.

4.3.3.2 Section 3.2.2 System Design Criteria, all new Tank Operations Contract (TOC) Facilities shall meet the DOE building energy codes program per the latest edition of ASHRAE 90.1, Energy Standard for Buildings, Except Low-Rise Residential Buildings, as practically as possible.

4.3.3.3 Section 3.2.2 for Non-Nuclear Facilities is applicable.4.3.3.4 Section 3.3 Codes and Standards - 222-SL, shall be designed per TFC-ENG-

STD-07, Attachment A, Table A-1 for Non-Nuclear facilities, e.g., ANSI/AHIH Z9.2, ANSI/AHIH 9.2, etc.

4.3.3.5 Section 3.5 is applicable4.3.3.6 Section 3.6 is applicable.4.3.3.7 Section 3.8 is applicable.4.3.3.8 Section 3.9 is applicable.4.3.3.9 Section 3.10 is applicable. Fire Protection

4.3.3.9.1 Laboratory ventilation systems shall be designed to ensure that fire hazards and risks are minimized.

4.3.3.10 Section 3.11 is applicable.4.3.3.11 Section 3.12 is applicable.4.3.3.12 Section 3.13 is applicable.4.3.3.13 Section 3.15 is applicable.4.3.3.14 Section 3.16 is applicable.4.3.3.15 Section 3.17 is applicable.

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4.3.3.16 Section 3.18 is applicable. The following criteria shall also be used for ductwork design.

4.3.3.16.1 Duct design and application criteria shall comply with the Industrial Ventilation Manual and industrial standards and consensus as identified in STD-07, Section 3.18.2, e.g., ACGIH, ASHRAE, ANSI/AIHA Z.9.5, Z 9.2 for exhaust systems.Laboratory exhaust system ductwork complies with the appropriate sections of current versions of the Sheet Metal and Air Conditioning Contractors’ National Association (SMACNA) standards.

4.3.3.16.2 Ductwork and piping slopes shall comply with TFC-ENG-STD-07 Section 3.18.3.

4.3.3.16.3 Exhaust ductwork is designed in accordance with the current versions of ANSI/AIHA® Z9.2, the ASHRAE Handbook –Fundamentals, and NFPA 45.

4.3.3.16.4 Static pressure losses shall be estimated throughout the duct system by using Chapter 9 of the ACGIH manual for design.

4.3.3.16.5 Duct materials shall be chosen to be compatible with air contaminants exhausted.

4.3.3.16.6 Duct velocities shall be per STD-07 and sufficient to prevent the settling of dry aerosols. Where mists, sticky particles, or condensing materials are carried in the duct, provision for duct cleaning shall be provided. Common practice is to design such duct work for a velocity of approximately 1200 to 3000 ft/min (6–10 m/s) where only gases or vapors or both are exhausted.

4.3.3.16.7 Exhaust ducts through fire walls, automatic dampers shall be provided in the exhaust duct in accordance with local and NFPA codes. Standard for Exhaust Systems for Air Conveying of Vapors, Gases, Mists and Noncombustible Particulates, ANSI/NFPA 45 and 91. TFC-ENG-STD-07, Ventilation System Design Standard, Section 3.19 is applicable.

4.3.3.16.8 Flexible vibration isolators on fan inlet ductwork shall be mounted on the outside of the exhaust ducts. TFC-ENG-STD-07, Ventilation System Design Standard, Section 3.24 is applicable.

4.3.3.16.9 The design and installation of ducts from chemical fume hoodsshall be in accordance with NFPA 91 except that specific requirements in NFPA 45 shall take precedence.

4.3.3.17 Section 3.24 is applicable. The following shall also be used for Fan design.4.3.3.17.1 Selection shall consider possible system effect losses.4.3.3.17.2 AMCA 410, Recommended Safety Practices for Users and

Installers of Industrial and Commercial Fans; AMCA 99, Standards Handbook; AMCA 803, Industrial Process Fans: Site

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Performance Test Standard; AMCA 200, Air Systems; AMCA 201, Fans and Systems; AMCA 202, Troubleshooting; AMCA 203, Field Performance Measurement of Fan Systems and ACGIH® Ventilation Manual in Appendix for more information.

4.3.3.17.3 Fan selection shall consider long-term air contaminant effects on the fan and fan wheel. Fans serving corrosive vapor LEV systems shall be located on the clean-air side of the air cleaning device.

4.3.3.17.4 Where flammable vapors, gases, or dusts are carried in the air stream, precautions shall be taken to protect against ignition in accordance with NFPA and local fire code requirements.

4.3.3.17.5 Where wire mesh screen is used on the fan discharge, the screen opening shall be no smaller than necessary to prevent entry of birds or rodents.

4.3.3.17.6 Materials of construction shall be compatible with the process and air contaminants to be exhausted.

4.3.3.17.7 System components shall be constructed to be airtight on the upstream side of the fan; system components shall be constructed to be airtight on the downstream side of the fan when such components are inside the building.

4.3.3.17.8 Ductwork shall be accessible for inspection and maintenance, and shall be protected against external damage.

4.3.3.17.9 Where failure of the exhaust equipment could result in airborne concentrations of contaminants at or above IDLH levels, the exhaust and supply air systems and the process machinery controls shall be interlocked so process machinery can operate only when the exhaust and supply systems are in operation.

4.3.3.17.10 Air supply and exhaust fans, motors, and components shall be inspected at least annually.

4.3.3.18 Section 3.25 is applicable. The following shall also be used for Fan design.4.3.3.18.1 Stacks shall be located and designed per STD-07 and such that

there is no re-entrainment of exhausted air and workers in the vicinity of the stack are not exposed to hazardous concentrations of exhausted contaminants.

4.3.3.18.2 Stack outlets shall be sufficiently above adjacent air intakes or roof lines if they are within re-entrainment distance. Stacks at least fifty feet from air intakes, if possible; ten feet above adjacent roof lines and/ or air intakes if within fifty feet, and to provide a stack exit velocity of at least 3,000 ft/min to avoid backdrafting. Dispersion modeling can be another useful tool when designing stacks. ASHRAE Fundamentals, for more definitive measures and design guidance.

4.3.3.19 Section 3.26 is applicable.

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4.3.3.20 Section 3.28 is applicable.4.3.3.21 There is no requirement for abatement controls on the vent system/stack.

The lab will have a "Toxics" permit. This permit requires the installation of a sample port in the exhaust system.

4.3.3.22 Section 3.32.4 is applicable4.3.3.23 Section 3.32.5 is applicable.4.3.3.24 Section 3.32.6 is applicable.4.3.3.25 Section 3.32.7 is applicable.4.3.3.26 Section 3.33 is applicable.

4.3.4 The air pressure in the laboratory work areas shall be negative with respect to corridors and non-laboratory areas of the laboratory unit. Pressure cascades may need to be established within the confinement, e.g., 0.05 in.wg. pressure differential between cascade stages is generally adequate.

4.3.5 Lab Layout and Construction4.3.5.1 Air Locks are not required. However, the use of vestibules should be

considered based on the energy efficiency and hazards involved with the facility.

4.3.5.2 Lab layout and construction shall be designed to assure optimum combination of employee protection, capital investment, and operating economy for all factors associated with the production or materials handling in the facility.

4.3.5.3 The required exit access doors of all laboratory work areas within Class A or Class B laboratory units shall swing in the direction of exit travel per the NFPA 45.

4.3.5.4 The required exit access doors of all laboratory work areas within Class C or Class D laboratory units shall be permitted to swing against the direction of exit travel per the NFPA 45 or shall be permitted to be a horizontal sliding door complying with NFPA 101.

4.3.5.5 Exhaust volume flowrates and equipment sizes shall be selected to dilute air contaminants to an acceptable concentration in the LEV system, e.g., below 25% of the LFL during normal operation or worst credible accident.

4.3.5.6 Flow rates, power consumption, filter efficiencies, costs and system performance are related to static pressure as prescribed in the ACGIHIndustrial Ventilation manual of Recommended Practice for Design, 29th Edition.

4.3.5.7 Segregation of hazardous and non-hazardous operations.4.3.5.8 Isolate hazardous operations from non-hazardous work, e.g., place them in

a separate areas or room.4.3.5.9 Air cleaning equipment design shall consider unobstructed access for

maintenance, e.g., filter or collection media removal, cleaning, and repair of air cleaning equipment.

4.3.5.10 Protect systems and associated piping from freezing.4.3.5.11 Fire curtains should be provided as required by codes of the National Fire

Protection Association and the local authority having jurisdiction.

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4.3.5.12 Processes and equipment generate fumes, or vapors that may intermix and could result in a health or explosion hazard, or destructive corrosion, such air contaminants shall be exhausted by separate exhaust ventilation systems. Materials shall be selected based on resistant to corrosion by the agents to be used.

4.3.5.13 For rooms served by VAV ventilation systems, the Chemical Emergency mode of operation maximizes the room ventilation (air change per hour) rate.

4.3.5.14 Door operation for egress shall be maintained when the supply system shuts down and the lab exhaust system operates, creating a pressure differential.

4.3.5.15 Handling and storage of chemicals shall be in accordance with NFPA 400.4.3.5.16 Maintain a minimum average inflow velocity of 0.5 m/sec (100 ft/min)

through the chemical cabinet work access opening4.3.5.17 The location of air supply diffusion devices shall be chosen so as to avoid air

currents that would adversely affect the performance of chemical fume hoods, exhaust systems, and fire detection or fire-extinguishing systems.

4.3.6 Exhaust Air and Laboratory Hoods shall be designed as follows:4.3.6.1 Laboratory units and laboratory hoods in which chemicals are present shall

be continuously ventilated under normal operating conditions.4.3.6.2 Exhaust hoods shall be selected, designed, constructed, operated, and

maintained to provide control of routine and anticipated chemical or particulate emissions.

4.3.6.3 The design and construction of laboratory chemical hoods conform to the applicable guidelines presented in the latest edition of ACGIH® Industrial Ventilation, A Manual of Recommended Practice, and the most current codes, guidelines and standards, NFPA 45 Section 7.8, and any other applicable regulations and recommendations.

4.3.6.4 Wake effects of air entering the hood and flowing past persons standing near the hood.

4.3.6.5 It is not anticipated that exhaust air from chemical fume hoods and general laboratory spaces will require filtration or scrubbing. However, the Lab will be using mainly caustic (NaOH) and acids (HNO3, HCI, H2PO4), and little or no organic solvents and no perchlorates. Hoods will require chemical resistance to specific acids or solvents.

4.3.6.5.1 Based on environmental permits, should Filtration be required, TFC-ENG-STD-07, Ventilation System Design Standard, Sections 3.22 and 3.23 are applicable.

4.3.6.6 Capture and control velocities; Air motion in the vicinity of the hood; Employee work practices; thermal behavior of air contaminants; and Toxicity and hazardous properties of air contaminants.

4.3.6.7 Hood velocities measured at the hood face of 125 fpm minimum and 175 maximum fpm to comply with the TFC-ENG-STD-07 Section 3.18.2 unless specified differently by the process conditions per ANSI/AHIH Z9.5 and Z 9.2.

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4.3.6.8 Exhaust air flowrate selection shall be determined by capture, control, and containment requirements.

4.3.6.9 The air volume flowrate is a function of the capture or control velocity at the hood. This velocity is often the most critical parameter of the hood. It should always be based on emission control, system configuration, and containment performance requirements. Recommended air flowrates are found in the Industrial Ventilation Manual, appropriate ANSI, OSHA, and NIOSH standards, and in other publications.

4.3.6.10 Design sash position - Design sash opening and sash configuration (e.g. , for laboratory chemical hoods);

4.3.6.11 The maximum sash open area of the hood face that achieves the desired face velocity during any work inside the hood that produces airborne contaminants

4.3.6.12 Hoods and connecting equipment shall be designed and operated to avoid fires and explosions.

4.3.6.13 The hood shall be equipped with a mechanical sash stop when sash design opening area is less than the maximum sash opening area.

4.3.6.14 All hoods are equipped with a flow indicator, flow alarm, or face velocity alarm indicator to alert users to improper exhaust flow.

4.3.6.15 The flow-measuring device is capable of indicating that the air flow is in the desired range, and capable of indicating alarms when the flow is high or low by 20%.

4.3.6.16 Fire detection and alarm systems shall not be interlocked to automatically shut down chemical fume hood exhaust fans

4.3.6.17 Air exhausted from chemical fume hoods and other special local exhaust systems shall not be recirculated.

4.3.7 Makeup Air Systems4.3.7.1 Determine the appropriate static pressure relationship between the

exhausted space and adjacent spaces and provide makeup air volumes accordingly at nominal (+/-) 0.05 in W.C.

4.3.7.2 Optimize supply-to-exhaust- system airflow patterns in the space where hoods and snorkels are located in relationship to cross flows from doors and walking areas. Snorkels shall be capable of removing adequate cfm for meeting specific contaminants per the manufacturer recommendations. Snorkels shall be design to operate on demand and isolable when not in use.

4.3.7.3 The tempered supply air to the space should be located so clean is first passed over the workers and then to the contaminated area, where it will be removed by the exhaust system.

4.3.7.4 The ventilation system shall be designed based on the cascading flow from the clean areas to contaminated areas.

4.3.7.5 Avoid high velocities at worker locations to avoid vortices around a worker’s body which can create higher exposures.

4.3.7.6 Recirculated air (if designed) from a local exhaust ventilation system shall meet the requirements of ANSI/AIHA® Z9.7.

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4.3.7.7 Makeup air delivery shall not reduce the performance of the local exhaust ventilation system. The intake for the makeup air system shall be so located as to protect against the uptake of contaminants from exhaust systems, process vents, or other contaminant sources.

4.3.7.8 Makeup air (if designed) shall be filtered at the air intake to protect ventilation system equipment. Typical filters to protect fans and coils include ASHRAE 52.1 ratings of 30–90% and ASHRAE 52.2 MERV ratings of 4–10.

4.3.7.9 Makeup air units shall be designed and operated to supply appropriate air volume flowrates at all times. Makeup air shall be clean. When makeup air is used to provide thermal comfort for workers, the system shall be designed and operated in accordance with appropriate standards.

4.3.7.10 Abatement of heat generated by GC/MS instruments shall be considered.4.3.8 General Air Movement Requirements

4.3.8.1 Air movement in the Standard lab, process chemistry, organic analysis, and I.H. analysis, spaces shall consider workers activities and interactions with the contaminated air, e.g., direction, velocity, air temperature, mixing potential, supply, return flow conditions, direction, and air changes per hour.

4.3.8.2 Duct velocities of laboratory exhaust systems shall be high enough to minimize the deposition of liquids or condensable solids in the exhaust systems during normal operations in the chemical fume hood.

4.3.9 Supply Air Quality (SAQ) shall comply with ANSI/ASHRAE Standard 62.1.4.3.10 Testing, Balancing, and Operational Checks

4.3.10.1 Performance standards and operating criteria shall be established by the User for every component of an LEV system. Exhaust ventilation system including the hood or exhausted enclosure, the air cleaner, and the fan. Performance criteria usually includes such parameters as: hood static pressure, minimum air volume flowrate, average, minimum, and maximum hood face velocities, visual containment, measured containment performance factors, capture velocity, slot velocity, ASHRAE 110 ratings, SEMI F15 requirements for determining fugitive emissions by Using Tracer Gas, transport velocity, pressure drop across air cleaners, fan total pressure, motor amperage, and so forth, as appropriate.

4.3.10.2 A VAV hood is provided with an emergency switch that allows the hood exhaust volume to return to the maximum.

4.3.10.3 The User shall select test methods and test instruments appropriate to measure the established performance criteria. These may include some version of the ASHRAE 110 test method, containment tests using smoke or vapor, face and duct velocity measurement protocols, various ACGIH® Industrial Ventilation Manual testing procedures, and hood static pressure.

4.3.10.4 The hood shall capture, receive, or contain air contaminants at some specified performance criteria established by the owner, e.g., no visible emissions, estimate the ratio of the concentration of a contaminate in the

MT-50398 Rev.00 12/6/2018 - 9:33 AM 12 of 23

exhaust air vs. the concentration in the breathing zone of a person actually working in front of the hood Protection Factor PF = C exhaust air /C breathing zone.

4.3.11 Air Cleaning Equipment4.3.11.1 Air cleaning equipment including moisture separator, prefilter, HEPA filters

shall be built, operated, and/or modified after obtaining the appropriate emissions and/or air pollution permits required by local authorities.

4.3.11.2 Local exhaust ventilation air cleaning equipment including stack shall be located outdoor with no re-entrainment.

4.3.11.3 The design shall establish and operate testing and maintenance programs to assure reliable and consistent operation of the cleaning equipment.

4.3.11.4 Airflow through the fair cleaning equipment, e.g., filter housing, is shut down during filter change-out.

4.3.12 Applicable Codes and Standards:4.3.12.1 10 CFR 851, Worker Safety and Health Program.4.3.12.2 American Industrial Hygiene Association (ANSI/AIHA) Z9.2, Local exhaust

Ventilation Systems.4.3.12.3 American Industrial Hygiene Association (ANSI/AIHA) Z9.5, Laboratory

Ventilation.4.3.12.4 ANSI/ASHRAE Standard 52.14.3.12.5 ANSI/ASHRAE Standard 62.14.3.12.6 ASHRAE 90.1, Energy Standards for Buildings4.3.12.7 DOE O 252.1A, Technical Standards Program.4.3.12.8 DOE O 420.1C, Facility Safety. 4.3.12.9 DOE-STD-1066 4.3.12.10 DOE STD 1189 Integration of Safety into the Design Process.4.3.12.11 DOE STD 3009, DOE Standard Preparation Guide for U.S Department of

Energy Nonreactor Facility Documented Safety Analyses.4.3.12.12 HNF-12125, “222-S Laboratory Documented Safety Analysis.4.3.12.13 International Building Code (IBC)4.3.12.14 International Mechanical Code (IMC)4.3.12.15 International Plumbing Code (IPC)4.3.12.16 MGT-ENG-IP-05, R3, ORP Fire Protection Program.4.3.12.17 NFPA 45, Fire Protection for Laboratories Using Chemicals4.3.12.18 NFPA 90A, Installation of HVAC Equipment4.3.12.19 NFPA 90B, Standard for the Installation of Warm Air Heating and Air

Conditioning Systems4.3.12.20 NFPA Standard 91, Standard for Ventilation Systems for Air Conveying of

Vapors, Gases, Mists, and Noncombustible Particulate Solids4.3.12.21 NFPA 1014.3.12.22 TFC ENG STD 01, Human Factors In Design.4.3.12.23 TFC ENG STD 02, Environmental/Seasonal Requirements for TOC Systems,

Structures, and Components. 4.3.12.24 TFC-ENG-STD-06, Design Loads for Tank Farm Facilities

MT-50398 Rev.00 12/6/2018 - 9:33 AM 13 of 23

4.3.12.25 TFC-ENG-STD-07, Ventilation System Design Standard4.3.12.26 Washington Administrative Codes (WAC).

4.3.12.26.1 Chapter 173 401.4.3.12.26.2 Chapter 51 50, “State Building Code adoption and amendment

of the 2012 edition of the International Building Code.”4.3.12.26.3 Chapter 51 52, “State Building Code adoption and amendment

of the 2012 edition of the International Mechanical Code.”4.3.12.26.4 Chapter 51 56, “State Building Code adoption and amendment

of the 2012 edition of the Uniform Plumbing Code.”4.3.12.26.5 Chapter 246 247, “Radiation Protection – Air Emission.”

5.0 Fire Protection5.1 A new fire protection system shall be designed and installed in the new Cold Laboratory.

The fire sprinkler system shall be an automatic sprinkler system and shall be hydraulically calculated, designed, installed, tested, and seismically restrained in accordance with NFPA13, Standards for Installation of Sprinkler Systems.

5.2 A new addressable, low-energy fire alarm system shall be installed in the Cold Laboratory Building.

5.3 The new fire alarm system shall be designed, installed, and tested in accordance with NFPA 72, National Fire Alarm Code. Alarm and trouble signals will be sent to the Hanford Fire Department (HFD) via a narrow head radio transceiver integrated into the building fire alarm control panel.

5.4 Duct smoke detectors will be provided in the air handling unit discharge ductwork that will shut down the unit and activate the fire alarm system upon detection of smoke in the airstream.

5.5 Building HVAC supply systems shall comply with National Fire Prevention Association (NFPA) 69, “Standard on Explosion Prevention Systems;” Standard 90A, “Installation of Air Conditioning and Ventilation Systems;” NFPA 90B, “Standard for the Installation of Warm Air Heating and Air Conditioning Systems,” and NFPA Standard 91, “Standard for Ventilation Systems for Air Conveying of Vapors, Gases, Mists, and Noncombustible Particulate Solids.”

5.6 Applicable Codes and Standards:5.6.1 DOE-STD-1066, Fire Protection.5.6.2 HNF-12125, Rev. 09, 222-S Laboratory Documented Safety Analysis5.6.3 HNF-36147, Rev. 4, DOE Fire Protection Handbook, Hanford Chapter5.6.4 HNF-SD-CP-FHA-003, Rev. 3, 222-S Laboratory Fire Hazards Analysis5.6.5 MGT-ENG-IP-05, R3, ORP Fire Protection Program.5.6.6 NFPA 13: Standard for the Installation of Sprinkler Systems 5.6.7 NFPA 24, Standard for the Installations of Private Fire Service Mains and the

Appurtenances5.6.8 NFPA 45, Fire Protection for Laboratories Using Chemicals5.6.9 NFPA 72: National Fire Alarm and Signaling Code5.6.10 NFPA 90A, Installation of HVAC Equipment5.6.11 NFPA 90B, Standard for the Installation of Warm Air Heating and Air Conditioning

Systems

MT-50398 Rev.00 12/6/2018 - 9:33 AM 14 of 23

5.6.12 NFPA Standard 91, Standard for Ventilation Systems for Air Conveying of Vapors, Gases, Mists, and Noncombustible Particulate Solids

5.6.13 TFC-ENG-STD-07, Ventilation System Design Standard5.6.14 TFC ESHQ FP STD 02, Fire Protection Design Criteria.5.6.15 TFC ESHQ FP STD 06, Fire Hazard Analysis and Fire Protection Assessment Requirements.

6.0 Electrical:6.1 Electrical installation shall be in accordance with the National Electrical Code 2017 edition,

NFPA 70. 6.2 Design facility to accommodate analytical equipment required for 222-SL.6.3 General lighting, provide dimmable LED luminaires. Illuminate lab rooms to 50 foot-candles

average, with maximum to minimum intensity variation of no more than 10 to 1 ratio. 6.4 Automatic lighting dimming with occupancy sensor controls is not required.6.5 Safety Shower Requirements

6.5.1 Provide dedicated lights above each safety shower location.6.5.2 Safety Showers must annunciate and light up to inform others of an emergency.

6.6 Provide emergency lighting with battery backup inverters and emergency egress lighting using NFPA 101 as guidance.

6.7 Receptacles and communication circuits shall be run in pole/channel raceway. Top channel: general service power; middle channel: conditioned power; bottom channel: communication circuits.

6.8 Provide one-way public address system in all occupied rooms. 6.9 Provide HLAN telephones distributed through all normally occupied rooms. 6.10 Provide HLAN and SLAN computer Ethernet wiring distributed throughout 222-SL.6.11 Provide one 20kVA double-conversion conditioned power UPS with output distribution

panel.6.12 Lightning Protection Considerations: DOE-STD-1020, Natural Phenomena Hazards Analysis

and Design NFPA 780, Installation of Lightning Protection Systems - Annex L, Lightning Risk Assessment are to be used for guidance for lightning protection.

6.13 Calculations and design shall be performed and provided to Washington River Protection Solutions for the main transformer.

6.14 13.8kV power is available at site.6.15 Install main 480V, three-phase distribution board served by main transformer (as

determined above) via underground conduit and cables to main 480V breaker disconnect. This distribution board is located in a dedicated, secure electrical room (not shared with mechanical or process equipment).

6.16 Provide three-phase 208/120V electrical distribution panels as required to supply variable refrigerant fans, process specific and general receptacle loads throughout 222-SL facility.

6.17 Provide 480/277V, 3-phase power to general HVAC loads (supply fans, heaters, vacuum pumps, heat pumps, energy recovery pump) and lift station sump pump loads.

6.18 Applicable Codes and Standards6.18.1 TFC-ENG-STD-14 Set point Standard6.18.2 TFC-ENG-STD-15, Standard for Raceway Systems and Flexible Cords and Cables6.18.3 TFC-ENG-STD-31, Electrical Distribution Studies6.18.4 TFC-ENG-STD-41, Electrical Installation

MT-50398 Rev.00 12/6/2018 - 9:33 AM 15 of 23

7.0 Hoisting and Rigging7.1 Hoisting and Rigging requirements shall meet the following codes, standards, and

procedures.7.1.1 DOE-RL-92-36, Hanford Site Hoisting and Rigging Manual7.1.2 TFC-ESHQ-S-STD-28, Hoisting and Rigging 7.1.3 TFC-ENG-FACSUP-C-25, Hoisting and Rigging

8.0 General Requirements:8.1 Equipment Identification numbers shall be per ATS-310, Section 11.18 and TFC-ENG-

FACSUP-C-23, Equipment Identification and Data Management.8.2 The Cold Laboratory shall be designed for Ordinary Hazard Group 2 hazard classification.8.3 The modular facility must meet the Washington State Gold Seal standards. 8.4 The modular facility shall be designed and fabricated in conformance with the best industry

practices using new and first quality materials and shall meet Chapter 296-150F WAC and the latest requirements of the Washington State Energy Code.

8.5 The modular facility shall include, as applicable, the principles of HPSB, High Performance and Sustainable Buildings.

8.6 Reference, TFC-PLN-112, Graded Approach to Quality.

MT-50398 Rev.00 12/6/2018 - 9:33 AM 16 of 23

The

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naly

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pag

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stru

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MT-

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17 o

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Tab

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pag

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stru

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MT-

5039

8 R

ev.0

012

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018

- 9:3

3 AM

18 o

f 23

Tab

le 1

. A

naly

tical

Nee

ds (7

pag

es)

222-

SL In

stru

men

tatio

n an

d E

quip

men

t

Typ

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Size

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Snor

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ter w

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tatio

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Non

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Ana

lysi

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MT-

5039

8 R

ev.0

012

/6/2

018

- 9:3

3 AM

19 o

f 23

Tab

le 1

. A

naly

tical

Nee

ds (7

pag

es)

222-

SL In

stru

men

tatio

n an

d E

quip

men

t

Typ

eG

ases

Nee

ded

Size

Ven

tilat

ion

222-

SL

Loc

atio

nC

urre

nt

Loc

atio

n

HLA

N c

ompu

ter w

orks

tatio

nN

one

3' x

5'

Non

eO

rgan

ic

Ana

lysi

s4-

TUV

HLA

N c

ompu

ter w

orks

tatio

nN

one

3' x

5'

Non

eO

rgan

ic

Ana

lysi

s4-

S

HLA

N c

ompu

ter w

orks

tatio

nN

one

3' x

5'

Non

eO

rgan

ic

Ana

lysi

sN

ew/B

acku

p

HLA

N c

ompu

terw

orks

tatio

nN

one

3' x

5'

Non

eO

rgan

ic

Ana

lysi

sN

ew/B

acku

p

HLA

N c

ompu

ter w

orks

tatio

nN

one

3' x

5'

Non

eO

rgan

ic

Ana

lysi

sN

ew/B

acku

p

Mill

i-Q W

ater

Sys

tem

Non

e2'

x 2

'N

one

Org

anic

A

naly

sis

New

Ref

riger

ator

Non

e3'

x 3

' N

one

Org

anic

A

naly

sis

New

Ref

riger

ator

Non

e3'

x 3

' N

one

Org

anic

A

naly

sis

New

Ref

riger

ator

Non

e3'

x 3

' N

one

Org

anic

A

naly

sis

New

Free

zer

Non

e3'

x 3

' N

one

Org

anic

A

naly

sis

New

Free

zer

Non

e3'

x 3

' N

one

Org

anic

A

naly

sis

New

Hyd

roge

n G

ener

ator

Non

e2'

x 2

'N

one

Org

anic

A

naly

sis

New

Hyd

roge

n G

ener

ator

Non

e2'

x 2

'N

one

Org

anic

A

naly

sis

New

4-cy

linde

r gas

bot

tle ra

cks

Non

e2'

x 5

'N

one

Org

anic

A

naly

sis

New

Bal

ance

on

tabl

e -n

eed

at le

ast 1

"4

plac

e" in

the

lab

Non

e2'

x 2

'Sn

orke

lO

rgan

ic

Ana

lysi

sN

ew/U

sed

14 S

umm

a St

orag

e C

ages

Non

e2'

x 6

' (x1

4)N

one

Org

anic

A

naly

sis

Var

ious

Hea

d Sp

ace

Ass

embl

y A

rea

Non

e3'

x 5

'N

one

Org

anic

A

naly

sis

B1-

G

MT-

5039

8 R

ev.0

012

/6/2

018

- 9:3

3 AM

20 o

f 23

Tab

le 1

. A

naly

tical

Nee

ds (7

pag

es)

222-

SL In

stru

men

tatio

n an

d E

quip

men

t

Typ

eG

ases

Nee

ded

Size

Ven

tilat

ion

222-

SL

Loc

atio

nC

urre

nt

Loc

atio

n

Elec

troch

emis

try--

4' x

3' w

ork

stat

ion

plus

6' F

ume

Hoo

dPr

oces

s C

hem

istry

4-P

Solu

bilit

y Te

stin

g--

2.5'

x 1

0'N

one

Proc

ess

Che

mis

try4-

P

Opt

ical

Mic

rosc

ope

--2.

5' x

4'

Non

ePr

oces

s C

hem

istry

4-P

Pola

rized

Lig

ht M

icro

scop

e--

2.5'

x 5

'N

one

Proc

ess

Che

mis

try4-

P

Bal

ance

in H

ood

Non

eN

/A6'

Fum

e H

ood

Proc

ess

Che

mis

try4-

P

Bal

ance

on

Tabl

eN

one

2' x

2'

Non

ePr

oces

s C

hem

istry

4-P

Bal

ance

on

Tabl

eN

one

2' x

2'

Non

ePr

oces

s C

hem

istry

4-P

Sim

ulan

t Pre

para

tion

and

Test

ing

--2.

5' x

10'

6' F

ume

Hoo

dPr

oces

s C

hem

istry

4-P

Met

hod

Dev

elop

men

t Wor

ksta

tion

Non

e2.

5' x

10'

Non

ePr

oces

s C

hem

istry

4-P

HLA

N c

ompu

ter w

orks

tatio

nN

one

3' x

5'

Non

ePr

oces

s C

hem

istry

4P

Che

mic

al S

tora

ge C

abin

ets

Non

e2'

x 3

've

nted

Proc

ess

Che

mis

tryFu

ture

XR

F--

5' x

6'

Non

ePr

oces

s C

hem

istry

Futu

re

SEM

--4'

x 8

'N

one

Proc

ess

Che

mis

tryFu

ture

XR

D--

18' x

11'

Non

ePr

oces

s C

hem

istry

Futu

re

Che

mic

al P

repa

ratio

n an

d Te

stin

g--

2.5'

x 1

0'4'

Fum

e H

ood

and

snor

kel

Proc

ess

Che

mis

tryFu

ture

Mill

i-Q W

ater

Sys

tem

Non

e2'

x 2

'N

one

Proc

ess

Che

mis

tryN

ew

Ben

ch S

pace

Non

e2.

5' x

50'

Non

eSt

anda

rds

Lab

4-D

MT-

5039

8 R

ev.0

012

/6/2

018

- 9:3

3 AM

21 o

f 23

Tab

le 1

. A

naly

tical

Nee

ds (7

pag

es)

222-

SL In

stru

men

tatio

n an

d E

quip

men

t

Typ

eG

ases

Nee

ded

Size

Ven

tilat

ion

222-

SL

Loc

atio

nC

urre

nt

Loc

atio

n

Ther

mo

Ove

nN

one

2' x

2'

Non

eSt

anda

rds

Lab

4-D

Ultr

ason

ic B

ath

Non

e2'

x 3

'N

one

Stan

dard

s La

b4-

D

Den

sito

met

er--

2' x

2'

Non

eSt

anda

rds

Lab

4-D

Bal

ance

on

tabl

e -n

eed

at le

ast 1

"4

plac

e" in

the

lab

Non

e2'

x 2

'N

one

Stan

dard

s La

bN

ew

Bal

ance

on

tabl

eN

one

2' x

2'

none

Stan

dard

s La

bN

ew

Ref

riger

ator

Non

e3'

x 3

' N

one

Stan

dard

s La

bN

ew

Ref

riger

ator

Non

e3'

x 3

' N

one

Stan

dard

s La

bN

ew

Free

zer

Non

e3'

x 3

' N

one

Stan

dard

s La

bN

ew

Free

zer

Non

e3'

x 3

' N

one

Stan

dard

s La

bN

ew

Stan

dard

s Pre

para

tion

--B

ench

Spa

ce6'

Fum

e H

ood

Stan

dard

s La

bN

ew

Equi

pmen

t Cle

anin

g--

N/A

4' F

ume

Hoo

dSt

anda

rds

Lab

New

Sam

ple

Rec

eipt

Ben

chN

one

2.5'

x 1

0'N

one

Sam

ple

Rec

eivi

ngN

ew

Fum

e H

ood

--N

/A4'

Fum

e H

ood

Sam

ple

Rec

eivi

ngN

ew

Ref

riger

ator

s (3)

Non

e3'

x 3

'N

one

Sam

ple

Rec

eivi

ngN

ew

Free

zers

(2)

Non

e3'

x 3

'N

one

Sam

ple

Rec

eivi

ngN

ew

Che

mic

al S

tora

ge C

abin

ets (

5)N

one

2' x

3'

Non

eC

hem

ical

St

orag

eN

ew

Fum

e H

ood

--N

/A4'

Fum

e H

ood

Che

mic

al

Stor

age

New

MT-

5039

8 R

ev.0

012

/6/2

018

- 9:3

3 AM

22 o

f 23

Tab

le 1

. A

naly

tical

Nee

ds (7

pag

es)

222-

SL In

stru

men

tatio

n an

d E

quip

men

t

Typ

eG

ases

Nee

ded

Size

Ven

tilat

ion

222-

SL

Loc

atio

nC

urre

nt

Loc

atio

n

Ref

riger

ator

Non

e3'

x 3

'N

one

Che

mic

al

Stor

age

New

He:

Ultr

a-hi

gh p

urity

hel

ium

Liqu

id N

2: L

iqui

d ni

troge

n (c

ryog

enic

coo

ling)

N2:

Nitr

ogen

H2:

Hyd

roge

n, ty

pica

lly fr

om H

2 ge

nera

tors

O2:

Oxy

gen

CLD

= C

hem

ilum

insc

ent D

etec

tor

CV

AA

S=

Col

d V

apor

Ato

mic

Abs

orpt

ion

Spec

trom

eter

GC

= G

as C

hrom

atog

raph

yH

LAN

= H

anfo

rd L

ocal

Are

a N

etw

ork

HPL

C=

Hig

h-pe

rfor

man

ce L

iqui

d C

hrom

atog

raph

yIC

= Io

n C

hrom

atog

raph

yIH

= In

dust

rial H

ygie

neLC

/MS

= Li

quid

Chr

omat

ogra

phy

/ Mas

s Spe

ctro

scop

yM

SD=

Mas

s Sel

ectiv

e D

etec

tor

SEM

= Sc

anni

ng E

lect

ron

Mic

rosc

opy

SVO

A=

Sem

iVol

atile

Org

anic

Ana

lysi

sTD

U=

Ther

mal

Des

orpt

ion

Uni

tTO

F=

Tim

e of

Flig

htV

OA

= V

olat

ile O

rgan

ic A

naly

sis

XR

D=

X-r

ay D

iffra

ctio

nX

RF

= X

-ray

Flu

ores

cenc

e

MT-

5039

8 R

ev.0

012

/6/2

018

- 9:3

3 AM

23 o

f 23