REPORT OF ENVIRONMENTAL MONITORING · pressure, percent methane, percent Lower Explosive Limit (LEL), and depth to water in each of the gas probes and punch bar locations. Also documented

us EPA RECORDS CENTER REGION 5

478996

REPORT OF ENVIRONMENTAL

MONITORING

FOR THE: STICKNEY AVENUE AND TYLER STREET LANDFILLS

LOCATED IN LUCAS COUNTY, OHIO

PREPARED FOR: CITY OF TOLEDO

DIVISION OF SOLID WASTE 3962 HOFFMAN ROAD TOLEDO, OHIO 43611

PREPARED BY: HULL & ASSOCIATES, INC. 3401 GLENDALE AVENUE

SUITE 300 TOLEDO, OHIO 43614

MARCH 2008

& associates, inc. March 18, 2008

Mr. Michael A. GIfford U.S. EPA, Region 5 77 West Jackson Boulevard Chicago, liiinois 60604

RE: Report of Environmental Monitoring for the Stickney Avenue and Tyler Street Landfills; COT192.100.0009.DOC

Dear Mr. GIfford:

This report was developed by Hull & Associates, Inc. (Hull) on behalf of the City of Toledo (City) to document the findings of environmental performance monitoring activities for the Stickney Avenue and Tyler Street Landfills (facilities) in accordance with the Administrative Order on consent. Docket No. V-W-97-C-433. The attached data Is provided for the facilities as specified below.

SampUnd and Analysis HulLpersohnel iribhite of 31 rnethane gas probes and vents on July 26, 2007 and October 31, 2007 (third and fourth quarters of 2007). j

I

Leachate sampling activities vyere completed at the Tyler facility pn July 24, 2007 and the Stickriey facility on July 25, 2007. Ail samples were collected by represehtatives of Hull and analyzed by Beimohf .Labs. A total Of nme leachate monitoring points were sampled at the Tyler facility and eight monitoring points at the Stickney facility.

Data Presentation This package coritainS the following information:

1. Appendix A - Static water levels presented on Field Data Sheets (FDS) ,for ieachate monitoring wells from sampling dates July 24, 2007 (Tyler) and July 25, 2007 (Stickney). The record calibration forms are also included for each sampling event. '

2. Appendix B - Data summarized for leachate monitoring wells at each facility on Table 1 (Tyler) and-Tables 2 and 3 (Stickney) to document the results !of the sampling activities completed at the facilities on July 24, 2007 and July 25, 2007. Table 1 contains data from monitoring wells T-MW-19, T-MW-21, iT-MW-23, T-MW-25, T-MW-27, T-MW-29, T-MW-31, T-MW-33, and T-MW-35; Table 2 contains data from monitoring wells S-MW-21, S-MW-24, S-MW-27, S-MW-30, S^MW^33, and S-MW-35; and Table 3 contains data from monitoring wells S-MW-36 and S-MW-37, which are designated as sentinel wells. '

3. Appendix C - Laboratory analytical reports for the leachate sampling activities completed on July 24, 2007 (Tyler) and July 25, 2007 (Stickney). In addition

c./ ^

3401 Glendale Avenue, Suite 300, Toledo, Ohio 43614 ^ 419.385.2018 419.385.5487 fax www.hullinc.com

Mr. Michael A. Gifford COT192.100.0009.DOC March 18, 2008 Page 2

to the results for the leachate monitoring well samples, results are also presented for duplicate, matrix spike, and matrix spike duplicate samples as well as two field blanks and a trip blank analyzed for quality control/assurance purposes. Laboratory analytical reports for the additional sampling activities completed on November 6, 2007 (Stickney) from monitoring wells PX-58 and PX-59 as requested by EPA is also provided In Appendix C.

4. Appendix D - Methane Monitoring Field Data Sheets (MMFDS) for monitoring activities completed on July 26, 2007 for the Third Quarter monitoring event and October 31, 2007 for the Fourth Quarter event. Also included is the MMFD for the September 7, 2007 monitoring at the Tyler Avenue Landfill after repairs were conduced to the blower system. The MMFDS document the gas pressure, percent methane, percent Lower Explosive Limit (LEL), and depth to water in each of the gas probes and punch bar locations. Also documented on the MMFDS are the weather-related monitoring parameters including ambient barometric pressure, ambient air temperature, relative humidity, and observed weather conditions.

5. Appendix E - Inspection field forms for the Inspection activities completed for the leachate monitoring well system and landfill on July 24, 2007 and for the gas monitoring well system on July 26, 2007. As documented on the inspection forms, no action items were identified during the inspection.

Data Review Reviews of the leachate and explosive gas data provided for the Stickney Avenue and Tyler Street Landfills Indicate that this data is similar to data reported for the landfill facilities in the past. All data for the field and trip blanks were reported below the respective laboratory Practical Quantitation Limits (PQLs). Values footnoted with a J on the data summary tables represent estimated values that were detected between the Method Detection Limit (MDL) and the laboratory PQL.

The results of the gas probe sampling indicate that landfill gas was reported at two of the gas probe locations^ (TGP-02 and TGP-10S) at the Tyler facility during the quarterly events. Inspection of the gas blower system determined that the blower was not working properly. The blower was subsequently repaired and on September 7, 2007 the readings recorded in the vicinity of the blower system indicated that no gas was reported in the TGP-02 gas probe. In addition, as documented on the MMFDS, field personnel were unable to verify the location of all gas probes during the monitoring activities therefore, punch bar sampling was conducted along the entire perimeter of the landfill. No gas was reported at any punch bar locations during either of the quarterly sampling events.

Mr. Michael A. Gifford COT192.100.0009.DOC March 18, 2008 Page 3

Should you have any questions or comments regarding the environmental monitoring program at the facility, please contact me at your convenience.

Sincerely,

âre/""' ^ Senior Scientist

KWO/jab

Appendices

ct: Archie Lunsey, Ohio EPA-NWDO (w/Appendlces) Casey Stephens, City of Toledo-Division of Solid Waste (w/Appendlces) Ed Irelan, City of Toledo-Division of Solid Waste (w/Appendlces)

> •0 "O m z g X >

APPENDIX A

Field Data Sheets (FDS) and Record Calibration Forms for Sampling Events Completed on

July 24, 2007 (Tyler) and July 25, 2007 and November 6, 2007 (Stickney).

HULL & ASSOCIATES, INC. MARCH 2008 TOLEDO, OHIO COT192.100.0009.DOC

Hu & associates, inc. 9401 QIailOlli Avanul, Suitt 900 • ToMO, Ohio 49014

GROUNDWATER MONITORING WELL FIELD DATA SHEET

MONITORING POINT;

DETECTION:

ASSESSMENT:

FACILITY INFORMATION Tyler Street Landfill , NAME:

ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 CONTACT: David Laffler

PROJECT NUMBER: TELEPHONE:

COT192

(419) 936-2643

COORDINATES: MONITORING WELL DATA

.N CONDITION OF WELL:

GROUND SURFACE ELEVATON: TOTAL DEPTH (PROM QROUNO SURFACE): SCREENED INTERVAL (INCLUDINOSANOPACK): SCREENED FORMATION:

CASING MATERIAL/DIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (FROM TOP OP CASINQ): SCREENED DEPTH (SCREEN ONLY):

WEATHER: BAROMETRIC PRESSURE:

LjAr ,/fsri

PERSONNEL PRESENT: MEASURED TOTAL DEPTH (FROM roc): VOLUME OF STATIC WATER:

WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F):

FIELD MEASURED PARAMETERS

STATIC WATER LEVEL (FROM roc):

GROUNDWATER ELEVATION:

DATE OF PURGING: 7/Ly/up'). PURGING DATA

PURGING METHOD: II PURGING RATE: Icc J

TIME OF PURGING: VOLUME PURGED: /o

WELL VOLUMES PURGED inltiai 1 2 3 4 S 8/Finai

Time 07 M 070 p o7M crjivi 1

PH ,.irs <71 Tamp. /3-1- Ar >3-/ n,) Spec. Cond. Corr. Cond. 7X3J 7?yo ")W/J

Redox Pot. -n,^. -•zoir D.O. 0. u 5.0'^ p.

Turbidity hi/ /WUA }w<» /CMO

Water Levei* I3ST. n4x.

VOLUME TO PURGE CALCULATION TABLE Weli casing

DIamatar (in.)

Gallons Par Foot

of Daplh

Paat of Standing

Watar

swell

Volumes

Total volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

B 1.469 X X3

* measurement from top of casing

DATEn-IME OF SAMPLING: SAMPLING METHOD:

SAMPLING DATA SAMPLING RATE (IPUSINODBOICATEDPUMP): STATIC WATER LEVEL (AFTER SAMPUNO):

NOTES

BXPLOSIVe OAS RBADINQ PRIOR TO STATIC WATBR LEVEL TT

Hu & associates, inc. M01 QlandBli Avanua, Sulla 900 • Tolado, Ohio 49SI4


MONITORING POINT;^

DETECTION: _

ASSESSMENT:

>JJ

FACILITY INFORMATION NAME: Tyler Street Landfill ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 CONTACT: David Leffler


COT192 (419) 936-2643


_N CONDITION OF WELL: "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (PROM OROUND SURFACE): SCREENED INTERVAL (INCLUDING SAND PACK): SCREENED FORMATION:

CASING MATERIAL/DIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (FROM TOP OP CASING): SCREENED DEPTH (SCREEN ONLY):


/yAr A'1 7o oy


PERSONNEL PRESENT: MEASURED TOTAL DEPTH (FROM roc): VOLUME OF STATIC WATER:

FIELD MEASURED PARAMETERS C' l%a.



DATE OF PURGING: PURGING METHOD: I IM, PURGING RATE: A/

PURGING DATA

TIME OF PURGING: VOLUME PURGED: / o

1 WELL VOLUMES PURGED | Initial 1 2 3 4 5 e/Flnal

Time rrsUf oSf-'3 OjOb

PH tyy 6-vr t'/r Temp. W.4- /?-•» m Spec. Cond.

Corr. Cond.

Redox Pot '/ZT. ./«•/ • •/s'3 -/sV D.O. W.AX <t.7r o^t Turbidity 3V« w Water Level* /13r 03^ /J7''

VOLUME TO PURGE CALCULATION TABLE Wall casing

Olamstar (In.)

Gallons Par Foot

of Dapth

Peat of Standing

Water

swell

Volumes

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

6 1.469 X X3


DATE/TIME OF SAMPLING: SAMPLING METHOD:

SAMPLING DATA OSr< SAMPLING RATE (IF USING OSDICATHO PUMP):

STATIC WATER LEVEL (AFTER SAMPLING):

NOTES

EXPLOSIVE GAS READING PRIOR TO STATIC WATER LEVEL: «LBL ±2^

Hu & as ociates, inc.

U0^ Oiandile Avanut, Sulta 300 • Tolado, Ohio 43014


MONITORING POINT;

DETECTION:

ASSESSMENT:

FACILITY INFORMATION

NAME: Tyler Street Landfill

ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611

CONTACT: David Leffler

PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2643

COORDINATES:

MONITORING WELL DATA

_N CONDITION OF WELL:

"E GROUND SURFACE ELEVATON:

TOTAL DEPTH (PROM OROUND SURFACE):

SCREENED INTERVAL (INCLUDINQ SAND PACK):

SCREENED FORMATION:

CASING MATERIAL/DIAMETER:

TOP OF CASING ELEVATION:

TOTAL DEPTH (PROM TOP OP CASINO):

SCREENED DEPTH (SCREEN ONLY):

WEATHER:

BAROMETRIC PRESSURE:

PERSONNEL PRESENT:

Jc*. O la

WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE ('F):

C«.

ASL. FIELD MEASURED PARAMETERS

c MpERS

.1^'rc.Jnu )

MEASURED TOTAL DEPTH (PROM roe):

VOLUME OF STATIC WATER:

STATIC WATER LEVEL (PROM TOO): /Ifc, /


DATE OF PURGING:

PURGING DATA

PURGING METHOD: {jue.l\

PURGING RATE: */ar M/

TIME OF PURGING:

VOLUME PURGED: Jta—

WELL VOLUMES PURGED I

initial 1 2 3 4 5 le/Flnall

Time OW-V oSis- OffG; oy-r

pH 6->l Temp. p.y n.v Spec. Cond.

Corr. Cond. LI Ho Redox Pot. -ps* D.O. 3 w- fiJO L.ii. Di/o

Turtldlty o.ol d.o7 acfi ! OcPj

Water Level* /Ifc-c n.L.1. /Tel. fl-iZ.

VOLUME TO PURGE CALCUU^TION TABLE

Wsll casing

DIamstar (In.)

Qallons Par Pact

of Daptl^

Past of Standing

Water

3 Wall

Volumes

Total Volume to

Purge (Qal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

6 1.469 X X3

' measurement from top of easlns

DATE/TIME OF SAMPLING:

SAMPLING METHOD:

SAMPLING DATA

U<.Jt 6012.^/-/?

SAMPLING RATE (ip USINO DeoicATSD PUMP):

STATIC WATER LEVEL (AFTER SAMPUNO):

NOTES

EXPLOSIVE OAS REAOINO PRIOR TO STATIC WATER LEVEL HCH4I 4?" %LBL

Hu & a: 3401 Qlai

associates, inc. auitt 300 a ToMo, onio 43ei4


MONITORING POINT;

DETECTION:

ASSESSMENT:



COT192 (419) 936-2643


,N CONDITION OF WELL: "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (PROM OROUND SURPACB): SCREENED INTERVAL (INCLUDING SAND PACK): SCREENED FORMATION:

CASING MATERIAUDIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (PROM TOP OP CASINO): SCREENED DEPTH (SCREBN ONLY):

WEATHER: ftrtly BAROMETRIC PRESSURE:


PERSONNEL PRESENT: MEASURED TOTAL DEPTH (PROM roc): VOLUME OF STATIC WATER:


STATIC WATER LEVEL (PROM roc):

GROUNDWATER ELEVATION: J2J^

PURGING DATA

DATE OF PURGING: 'ifufLii PURGING METHOD:"Û PURGING RATE:

TIME OF PURGING: VOLUME PURGED: SsMa

WELL VOLUMES PURGED |

Initial 1 2 3 4 3 8/Flnal

Time OtJa

PH i..(W iS'n Temp. M-to Spec. Cond.

Corr. Cond. J(PWO \LSo

Redox Pol -m -I7<i W±1 D.O. 6.o9 6. or Turbidity 2. \ / 1 1

Water Level* p.<ii O-'JI

VOLUME TO PURGE CALCULATION TABLE

Wall casing

Dlamaler (In.)

Gallons Per Foot

of Depth

Feat of Standing

Water

swell

Volumes

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.663 X X3

6 1.469 X X3

* measurement from top of caslns


2^ SAMPLING DATA

SAMPLING RATE (ipUSING DBDICATBD PUMP): STATIC WATER LEVEL (APTBRSAMPUNG):

itaJliJei'

NOTES

BXPLOSiVB OAS RBADINQ PRIOR TO STATIC WATER LEVEL: %0H4; 5-5. HLSL /OO

Hu associates, inc. MSI aiindilt Avanut, Sulla 300 • Tolado, OOla 43614


MONITORING POINT:

DETECTION:

ASSESSMENT:

FACILITY INFORMATION NAME: ADDRESS: CONTACT:

Tyler Street Landfill City of Toledo DSW, 3962 Hoffman Rd, Toledo, OH 43611 David Leffler


COT192 (419) 936-2643


.N CONDITION OF WELL: "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (pROMaRouNDsuRPAca): SCREENED INTERVAL (iNCLuoiNa SAND PACK): SCREENED FORMATION:

CASING MATERIAUDIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (PROM TOP OP CASING): SCREENED DEPTH (SCRBBNONLY):


WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F): -I J-ai l\t



MiLg. C.Ucreii.j< STATIC WATER LEVEL (PROM roc):


"lIlM I PURGING DATA

DATE OF PURGING: PURGING METHOD: UhAll PURGING RATE: i

TIME OF PURGING: VOLUME PURGED:

WELL VOLUMES PURGED Initial 1 2 3 4 5 6/Flnai

Time <yii> (>732 PH <p.4<j Tamp. 13'3 /33 l30 /a> Spec. Cond. Corr. Cond. -Pifo -70 yo 7(.<g Redox Pot. -nt' ',74 D.O. O,ow OoL Turbidity 1 J 1 Water Level* /j.w /V13 |3^^3 /S-i)


Olamelsr (In.)

Qallons Par Foot

of Dapth

Faat of Standing

Watar

3 Wall

Volumaa

Total Voluma to

Purga (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

e 1.469 X X3

* meaBurennent from top of casing

DATETTIME OF SAMPLING: SAMPLING METHOD:

_2Mfl3L SAMPLING DATA

SAMPLING RATE (IP USING OBOICATED PUMP): STATIC WATER LEVEL (APTBR SAMPUNG):

NOTES

BXPL08IVB OAS RBADiNO PRIOR TO STATIC WAT8R LSVBL %CH4: ^LEL:

Hu. & associates, inc. 9401 OlMdaliAvinut, Bulla 300 • ToMe. OOio 43014


MONITORING POINT: Atuiyj

DETECTION:

ASSESSMENT:

FACILITY INFORMATION NAME: ADDRESS: CONTACT:

Tyler Street Landfill City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 David Leffler


COT192 (419) 936-2643


.N, CONDITION OF WELL: "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (KROM QROUND SURPACB): SCREENED INTERVAL (INCLUDINO SANO PACK):

SCREENED FORMATION:

CASING MATERIAUDIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (FROM TOP OP CASINO): SCREENED DEPTH (SCREEN ONLY):


Ovdrcc;j^ ±L

WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F): 7o

FIELD MEASURED PA PERSONNEL PRESENT: MEASURED TOTAL DEPTH (PROM roc): VOLUME OF STATIC WATER:

4pVMETERS

L STATIC WATER LEVEL (PROMTOC): GROUNDWATER ELEVATION: —

DATE OF PURGING: PURGING DATA

PURGING METHOD: > U» /O PURGING RATE: U<» j

TIME OF PURGING: VOLUME PURGED: Ml <;*>/! jtJL

WELL VOLUMES PURGED


Time C^'\ «'^SI O'iS't /oOO yoo*p

PH (,4n. Temp, /y.<r /v.o If'V /T? //? Spec. Cond.

Cerr. Cond. Ueoe //ax ///CO

Redox Pot. -/ur •Zc?

D.O. ojt'i ao7 Turbidity I2tp Izi /Zl

Water Level* tr.tH K./y )S.H


Well easing

Diameter (In.)

Gallons Par Foot

of Depth

Feet of Standing

Water

3 Well

Volumes

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

e 1.468 X X3

' measurement from top of casing

DATEiTIME OF SAMPLING: SAMPLING METHOD: U4«.n

SAMPLING DATA 'Ol&% A->QJ SAMPLING RATE (IPUSINODBOICATHDPUMP):

STATIC WATER LEVEL (AFTER SAMPUNO):

NOTES

SXP1.08IVE OAS RBADINQ PRIOR TO STATIC WATER LEVEL %CH4; %LfiL

u associates, inc. 3401 QKnOlIt Annul, Sum 300 • TolMO, Ohio 4U14


MONITORING POINT:

DETECTION:

ASSESSMENT:

FACILITY INFORMATION NAME; Tyler Street Landfill ' ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 CONTACT: David Leffler


COT192

(419) 936-2643


.N CONDITION OF WELL; "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (pROMaRouNDsuwAca): SCREENED INTERVAL (INCLUOINQ SAND PACK): SCREENED FORMATION:

CASING MATERIAL/DIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (PROM TOP OP CASINO): SCREENED DEPTH (SCREBN ONLY):

WEATHER: BAROMETRIC PRESSURE: Go. u

WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F): 2IL





DATE OF PURGING:, PURGING METHOD:^ PURGING RATE: ZtiUL-

7HH PURGING DATA

TIME OF PURGING: VOLUME PURGED: SiZ/i

WELL VOLUMES PURGED

initial 1 2 3 4 3 6/Flnai

Time /"ir 2^ 'oi&

PH HI I^Yl Temp. /3.3 /t-fc li-l-Spec. Cond.

Corr. Cond.

Redox Pot. -hi -/3> •13? -risr -)JS D.O. ^/y Oi-I i Turbidity fej 7.V Zi> Water Levei* iS'gO /r-vc //.y-

VOLUME TO PURGE CALCUUVTION TABLE

Wall casing

DIamatar (In.)

Gallons Par Foot

of Oapm

Faat of Standing

Watar

3vyaii

Volumas

Total Voluma to

Purga (Gal.)

1 0.041 X X3

2 0.183 X X3

4 0.853 X X3

6 1.489 X X3

' measurement from top of casing

DATEH-IME OF SAMPLING: SAMPLING METHOD:

SAMPLING DATA yozd SAMPLING RATE (ipUSING DEDICATHD PUMP):

STATIC WATER LEVEL (AFTER SAMPUNO): Q^y//n,'

NOTES

BXPLOSIVe OAS RBAOtNO PRIOR TO STATie WATER LEVEL S£. %LBL /OO

Hu & as odates, inc.

M01 9l«ndil> Avtnui. Sulta WO • Tolado, Ohio 43014


MONITORING POINT: AlUJi3?

DETECTION:

ASSESSMENT:


NAME: Tyler Street Landfill



PROJECT NUMBER:

TELEPHONE:

COT192 (419) 936-2643

COORDINATES:


,N CONDITION OF WELL:

"E GROUND SURFACE ELEVATON: TOTAL DEPTH (FROM OROUND SURFACB):

SCREENED INTERVAL (INCLUDINO SAND PACK):

SCREENED FORMATION:


TOP OF CASING ELEVATION: TOTAL DEPTH (FROM TOP OF CASINO): SCREENED DEPTH (SCREEN ONLY):

WEATHER:

BAROMETRIC PRESSURE: 7"^ In

WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE ("F): :zr.

PERSONNEL PRESENT:

MEASURED TOTAL DEPTH (FROM roe):


FIELD M URED PARAMETERS

i STATIC WATER LEVEL (FROMTOO):


/y-"/

DATE OF PURGING:_

PURGING METHOD:' . iSihy

ux,|| U0T-L/)/-Q

PURGING DATA

PURGING RATE: ::?4i»

TIME OF PURGING:

VOLUME PURGED: K

WELL VOLUMES PURGED


Time fa-ic, IC^X. /bttjr

PH b<H APSS- ft Temp. i-ii 211,

Spec. Cond.

Corr. Cond. Oio Redox Pot -'S3 - tuj- Vfc? 0.0. 0 3T- o7«» 0 zr? Turbidity 7 Z, 7, Water Level* l^.4»'-


Wall casing

DIamstsr (In.)

Gallons Per Foot

of Depth

Feel or Standing

Water

swell

Voluntas

Total Volume to

Purge (Gel.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

6 1.469 X X3



SAMPLING METHOD:

SAMPLING DATA

LA.&X\ U>"-4^/'0

SAMPLING RATE (IF USINO DEDICATED PUMP):

STATIC WATER LEVEL (AFTER SAMPUNQ): —

NOTES

EXPLOSIVE OAS RBADINO PRIOR TO STATIC WATER LEVEL *CH4; %LBU ypQ

Hu & as ociates, inc. M01 Qlmdila Avmut, Sulta >00 • Tolado, Ohio 40014


MONITORING POINT: /SuOr"

DETECTION:

ASSESSMENT:



COT192 (419) 936-2643


_N CONDITION OF WELL: CaO'J "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (FROMQROUNDSURPACB): SCREENED INTERVAL (INOLUDINO SAND PACK): SCREENED FORMATION:

CASING MATERIAL/DIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (PROM TOP OP CASINO): SCREENED DEPTH (SCREEN ONLY):

WEATHER: BAROMETRIC PRESSURE: , d .•>»

WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F): .ZH


FIELD MEASURED P 'ARAMETERS

STATIC WATER LEVEL (PROM roc): GROUNDWATER ELEVATION:

-yof tif

DATE OF PURGING: PURGING METHOD: PURGING RATE:

PURGING DATA


JJJO_

WELL VOLUMES PURGED Initial 1 2 3 4 3 8/Flnal

Time lll^ //3b //Go

PH

Temp. M /5-.> /r-rfl PSTt

Spec. Cond. Corr. Cond. 312" Redox Pot. •11^ --'.V'L -ecY, D.O. C.J'} O-Oi.

Turbidity •Z, -t 2. 1-

Water Level* Tqr

VOLUME TO PURGE CALCULATION TABLE Well casing

Diamalsr (In.)

Gallona Par Pool

of Depth

Feet of Standing

Water

swell

Vdlumea

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.683 X X3

8 1.468 X X3



/ oy SAMPLING DATA

SAMPLING RATE (ip USINO DEDICATED PUMP): STATIC WATER LEVEL (APTER SAMPUNO): ^

NOTES

EXPLOSIVE OAS READINO PRIOR TO STATIC WATER LEVEL %CH4: %LBL:

Calibration Record

ynlia pH:

instruments: ly\Zi- - KWM, /-f." (iKtHr 6i5 Q.»sc,^f<.

Dats:

Time:

pH 4:

pH 7:

pHIO:

pH Slope:

Cond.

Cond. Slope:

D.O.

CH4 2.5 %:

LEL 50%:

ylLH h J

/Z3'J

M.w?

— -7.'' 1

/O. 4^ /

— —

o>

— —

— .—•" -

so

S.U. Conductivity: umhcs/cm D.O. mg/L

u &d! : as ociates, inc. M01 Qltndalt Avtnua, Sulta 300 • Teitdo. Ohio 43014


MONITORING POINT: l

DETECTION:

ASSESSMENT:


NAME: Stiekney Avenue Landfill



PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2643

COORDINATES:



'E GROUND SURFACE ELEVATON:

TOTAL DEPTH (FROM OROUNB SURFACE):


SCREENED FORMATION:



TOTAL DEPTH (FROM TOP CF CASINO):


WEATHER:

BAROMETRIC PRESSURE: id.

WEATHER CONDITIONS

WIND DIRECTION:

TEMPERATURE ("F): JL2.

PERSONNEL PRESENT:

MEASURED TOTAL DEPTH (PRCMTCC):



STATIC WATER LEVEL (FROM TOC):

GROUNDWATER ELEVATION: —

DATE OF PURGING:

PURGING METHOD:

PURGING RATE:

PURGING DATA

cu;

j2Sut-

TIME OF PURGING:

VOLUME PURGED:

WELL VOLUMES PURGED Initial 1 2 3 4 S e/Flnal

Time ofcHS C>k5"<» OtnTd

PH 6.Cr| Li.t L- fc'i Tamp. /ay /J 7 rxi i3.? Spec. Cond. Corr. Cond. 7V^ 7?AP Redox Pot. -in D.O. ifi- &.// aiz. o,i& a to Turbidity |ZL>(P H LS-Water Lever h-5> 'in- l-n


•lamatar (In.)

Gallons Psr Foot

of Depth

Feet of Standing

Water

swell

Volumes

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.183 X X3

4 0.853 X X3

8 1.489 X X3


DATEH-IME OF SAMPLING:

SAMPLING METHOD:

SAMPLING DATA SAMPLING RATE (IF USINQ DBDICATED PUMP):

STATIC WATER LEVEL (AFTBR SAMPUNO) : —

NOTES

eXPUOSIVE OAS READING PRIOR TO STATIC WATER LEVEL »0H4; -iO- %L£U

Hu as ociates, inc. 3401 QIandilt Avenua, Suite 300 • Toledo, Ohio 43014


MONITORING POINT:

DETECTION:

ASSESSMENT:


NAME: Stickney Avenue Landfill


CONTACT; David Laffler

PROJECT NUMBER;

TELEPHONE:

COT192 (419) 936-2643

COORDINATES:




TOTAL DEPTH (FROM OROUND auRPAee):


SCREENED FORMATION;

CASING MATERIAUDIAMETER:


TOTAL DEPTH (FROM TOP OF CASINO):


WEATHER:

BAROMETRIC PRESSURE: 3c>.o"»

WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE (®F);

PERSONNEL PRESENT:

MEASURED TOTAL DEPTH (FROM roc);





ll2.sl^y PURGING DATA

DATE OF PURGING:

PURGING METHOD: Uyt-U

PURGING RATE:

TIME OF PURGING:

VOLUME PURGED: / «-» r

WELL VOLUMES PURGED

Initial 1 2 3 4 S 6/Flnal

Tlma CfK oirZi" PH U- VL Tamp. /u<r fur iUta Spac. Cond.

Corr. Cond. mo 31V Radox Pot -//u -;/> -liH' •llS D.O, a3, p-Xf Turtidlty ai«i Water Laval* l-L-X.


Wall easing

Olamster (In.)

Qallons Par Poet

of Oapth

Faat of Standing

Watar

3 Wall

Volumas

Total Voluma to

Purga (Gal.)

1 0.041 X X3

2 0,163 X X3

4 0.653 X X3

6 1.469 X X3

* measurament from top of casing

DATE/TIME OF SAMPLING: 1 lz( /ji

SAMPLING METHOD:

SAMPLING DATA SAMPLING RATE (IFUSINQ DEDICATBD PUMP):

STATIC WATER LEVEL (AFTBR SAMPUNO): —

NOTES

eXPLOSIVE OAS REAOINO PRIOR TO STATIC WATER LEVEL: *CH4:

Hu as ociates, inc. 9401 aiandili Annua. Sulla 300 • Tolada, Ohio 43014


MONITORING POINT: ^11^33.

DETECTION:

ASSESSMENT:



ADDRESS: City of Toledo DSW, 3962 Hoffman Rd, Toledo, OH 43611


PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2643

COORDINATES:




TOTAL DEPTH (FROMOROUNDSUHPAOB):


SCREENED FORMATION:





WEATHER:

BAROMETRIC PRESSURE: 30. I«

WEATHER CONDITIONS

WIND DIRECTION:

1^5 TEMPERATURE ("F):

PERSONNEL PRESENT:

MEASURED TOTAL DEPTH (FROM roc):



STATIC WATER LEVEL (FROM TOO):


DATE OF PURGING: 2h£Lu PURGING DATA

PURGING METHOD: U'tx/'O

PURGING RATE: ^

TIME OF PURGING:

VOLUME PURGED:

o-7n /c.

WELL VOLUMES PURGED

Initial 1 2 3 4 s 8/Flnal

Time Oliu 01^ ft cni^ cnw o-JlV PH t tv Tamp. n-f. Jll na Spec. Cond.

Corr. Cond. rsh Redox Pot. -/W w/r - //w -//u D.O. 76'7 0.0L ao\ C>pi Turbidity i / ; / Water Level' 72«5


Wall easing

Dlainatar(ln.)

Gallons Par Foot

at Daotri

Past of Standing

Watar

3 Wall

Volumas

Total Voluma to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.6S3 X X3

6 1.469 X X3



SAMPLING METHOD: ilvl

SAMPLING DATA SAMPLING RATE (IFU8INOOEDICATHOPUMP):

STATIC WATER LEVEL (APTER SAMPUNO): "

NOTES

EXPLOSIVE OAS READING PRIOR TO STATIC WATER LEVEL HLEL

Hg Sid! associates, inc.

U0^ QlsndalB AwnuB, SuttB 300 a TolBdg, Ohio 43614


MONITORING POINT;

DETECTION:

ASSESSMENT:


NAME: Stickney Avenue Landfill "



PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2643

COORDINATES:


,N CONDITION OF WELL: Ccxjt

E

GROUND SURFACE ELEVATON:

TOTAL DEPTH (PROM GROUND SURPACB):

SCREENED INTERVAL (INCLUDING SAND PACK):

SCREENED FORMATION:



TOTAL DEPTH (FROM TOP OP CASING):

SCREENED DEPTH (SCRBENONLY):

WEATHER:

BAROMETRIC PRESSURE: Lil

WEATHER CONDITIONS

WIND DIRECTION:

TEMPERATURE ("F):

PERSONNEL PRESENT:

MEASURED TOTAL DEPtH (PROM roc):


FIELD MEASURED P.

/U i ifcC

'ARAMETERS ('


GROUNDWATER ELEVATION: _2Uik.

DATE OF PURGING:

PURGING DATA

PURGING METHOD:

PURGING RATE:

TIME OF PURGING:

VOLUME PURGED:

oSfCr

WELL VOLUMES PURGED |


Time UV/ Cfld? 1X0

PH 'r^1 Uri if/ cn Temp, lit /3-«- nr /ly Spec. Cond. 1

Corr. Cond. Hn'\3 tfllf V/Tkp

Redox Pot, -A/3 7yr -/vy vyy D.O. ».*t« 0<1- O-O'L 6.C.2.

Turbidity

Water Level* luj


Well casing Gallons Per Foot Fast of Standing swell Total Volume to

Diameter (In.) of Depth Water Volumes Purge (Gal.)

r 0.041 X X3

2 0.163 X X3

4 0.653 X X3

e 1.466 X X3

• measurement from top of casing


SAMPLING METHOD:

SAMPLING DATA SAMPLING RATE (ipUSING DBDICATBDPUMP):

STATIC WATER LEVEL (AFTER SAMPUNG):

NOTES

SXPLOaiVB OAS RBAOINQ PRIOR TO STATIC WATER LEVEL io «LeL /ô

u I associates, inc. M01 Qlindala Avtnua, Sulta 100 a Tolado. Ohio 43014


MONITORING POINT:

DETECTION:

ASSESSMENT:


NAME: Stiekney Avenue Landfill



PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2643

COORDINATES:


, N CONDITION OF WELL: gooJi


TOTAL DEPTH (FROM OROUND SURFACE):


SCREENED FORMATION:





WEATHER:

BAROMETRIC PRESSURE: ,•?<?- O .A

WEATHER CONDITIONS

WIND DIRECTION:

TEMPERATURE ("F): ZLL

PERSONNEL PRESENT:




STATIC WATER LEVEL (FROMroe):

GROUNDWATER ELEVATION: |l-^>

DATE OF PURGING:

PURGING DATA

PURGING METHOD:

PURGING RATE:

TIME OF PURGING:

VOLUME PURGED:

WELL VOLUMES PURGED I Initial 1 2 3 4 5 8/Flnal

Time OitJ cro7 OfVv

PH dF'OU LLFI_ Temp. tl-L. /ZJ-Spec. Cond.

Corr. Cond.

Redox Pot. '/3<f -/y3 -/VS D.O. L.H( 0.6I £>C|

Turbidity ha •zj-Water Level* m /XtL, 11. IL

VOLUME TO PURGE CALCULATION TABLE Well caalng

Diameter (In.)

Qallons Per Foot

of Oeptri

Feet of Stsnillng

Water

3 Well

Volumea

Total Volume to

Purge (Gal.)

1" 0.041 X X3

2 0.183 X X3

4 0.853 X X3

e 1.489 X X3


DATE/riME OF SAMPLING:

SAMPLING METHOD: 2jm

SAMPLING DATA o'iyj SAMPLING RATE (IF USING OEDICATSO PUMP):

STATIC WATER LEVEL (AFTER SAMPLINQ): <^100 Mi J.

NOTES

BXPLOSIVe OAS RBAOINO PRIOR TO STATIC WATSR LBVSL: %CH4: O

Hu & as ociates, inc. 3401 Qiendilt Avanua, Suite 300 • Toledo, Ohio 43014


MONITORING POINT; /Uu>lr

DETECTION:

ASSESSMENT:

FACILITY INFORMATION NAME: Stickney Avenue Landfill ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 CONTACT; David Leffler


COT192 (419) 936-2643


_N CONDITION OF WELL: "E

GROUND SURFACE ELEVATON: TOTAL DEPTH (FROM OROUND SURFACE): SCREENED INTERVAL (INCLUDINO SAND PACK): SCREENED FORMATION:

CASING MATERIAL/DIAMETER: TOP OF CASING ELEVATION: TOTAL DEPTH (FROM TOP OF CASINO): SCREENED DEPTH (SCREEN ONLY):

WEATHER: BAROMETRIC PRESSURE: 3o. O'n

WEATHER CONDITIONS WIND DIRECTION: TEMPERATURE ("F): 21.

FIELD M PERSONNEL PRESENT: MEASURED TOTAL DEPTH (FROM roc): VOLUME OF STATIC WATER:

ME>ÛRED PARAMETERS Ayi iiLg.



DATE OF PURGING: PURGING METHOD: lAJ<e.}\ PURGING RATE:

PURGING DATA


WELL VOLUMES PURGED

initial 1 2 3 4 6 e/Finai

TIma /««v /•/o

PH JO Tamp. t'h"'

Spac. Cond.

Corr. Cond. 'JTS'-W •• Radox Pot. -iil -nv D.O. - -/ Turbidity -io ir 1L. •u. Zo Watar Laval* L».ir ir la|/-


Wall casing

Dlamatar (In.)

Gallons Par Foot

of Dapth

Fast of Standing

Watar

3 Wall

Volumaa

Total Voluma to

Purga(Gal.)

1 • 0.041 X X3

2 0.163 X X3

4 0.853 X X3

8 1.489 X X3

* measuramant frem top of casing


SAMPLING DATA /a /o SAMPLING RATE (IF USINO DEDICATBB PUMP):

STATIC WATER LEVEL (AFTBR SAMPUNO): Ocas

NOTES

EXPLOSIVE OAS READINO PRIOR TO STATIC WATER LEVEL: HLBL

yi &ass( : associates, inc.

MOI Qlendait Avonue, Suits SOO • Toledo, Onio 43014


MONITORING POINT:

DETECTION:

ASSESSMENT:



ADDRESS: City of Toledo DSW, 3962 Hoffman Rd, Toledo, OH 43611


PROJECT NUMBER:

TELEPHONE:

COT192 (419) 936-2643

COORDINATES:


_ N CONDITION OF WELL:


TOTAL DEPTH (FROMOROUNDSURPACS):

SCREENED INTERVAL (INCLUOINQ SAND PACK):

SCREENED FORMATION:





WEATHER:

BAROMETRIC PRESSURE: / J M

WEATHER CONDITIONS

WIND DIRECTION:

TEMPERATURE ("F):

ii PERSONNEL PRESENT:

MEASURED TOTAL DEPTH (PROM roc):


FIELD MEASURED P.

M\^. C AMMETER

!I2± STATIC WATER LEVEL (PROM TOO): /S*/ '/i"

GROUNDWATER ELEVATION: —

DATE OF PURGING:

PURGING METH0D:A) /CV> y,

PURGING RATE:

PURGING DATA

TIME OF PURGING:

VOLUME PURGED:

1 WELL VOLUMES PURGED

initial 1 2 3 4 1 S 16/Final Time />*3f /w*. PH 6 tir Temp. '7d' n^r /3d-Spec. Cond.

Corr. Cond. i-2?-Redox Pot -Ijz rttr •V/7 '//> -Hi D.O. o»i2 cx/c 0./2. 0.(L

Turbidity ]rL n // 72- n n Water Level* nm


Well easing

Olamstar (In.)

Gallons Par Foot

of Depth

Feel of Standing

Watar

3 Wall

VoluiTias

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.6S3 X X3

6 1.469 X X3



SAMPLING METHOD:

SAMPLING DATA SAMPLING RATE (IP USINO DBDICATBD PUMP):

STATIC WATER LEVEL (AFTER SAMPUNO): —

NOTES

BXPLOaiVe OAS RBADINQ PRIOR TO STATIC WATER LEVEL jO

associates, inc. M01 Slandala Avanua, Sulfa 300 • Talada, Olflo 43014


MONITORING POINT:

DETECTION:

ASSESSMENT:

FACILITY INFORMATION StIckney Avenue Landfill NAME:

ADDRESS: City of Toledo DSW, 3962 Hoffman Rd. Toledo, OH 43611 CONTACT; David Leffler


COT192 (419) 936-2643

COORDINATES:


.N CONDITION OF WELL:


TOTAL DEPTH (FROM GROUND auRFAca):

SCREENED INTERVAL (INCLUDING SAND PACK):

SCREENED FORMATION:



TOTAL DEPTH (FROM TOP OF CASING):

SCREENED DEPTH (SCREEN ONLY);

WEATHER:

BAROMETRIC PRESSURE: II.-JA

WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE (»F):

PERSONNEL PRESENT:




STATIC WATER LEVEL (FROMTOC):


DATE OF PURGING: lUshX PURGING DATA

PURGING METHOD: PURGING RATE: M*'y

TIME OF PURGING: VOLUME PURGED: /. C.

WELL VOLUMES PURGED I

Initial 1 2 . 3 4 S 8/Flnal

Time /a/ //>- //•// PH WW Temp. ?-?• /tp-Z r/aa Spec. Cond.

Corr. Cond. Kir* Redox Pot b/W •irr -iTV D.O. b.Vi Turbidity /yr Water Level* /->7 uir}


Wall casing

DIametsr (In.)

Gallons Par Foot

of Dapth

Faat of Standing

Water

3 Wall

Voluntas

Total Volume to

Purge (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.663 X X3

e 1.469 X X3

• measumment from top of casing


SAMPLING METHOD:

SAMPLING DATA

f/^( SAMPLING RATE (IF USING DEDICATED PUMP):

STATIC WATER LEVEL (AFTER SAMPLING): —

NOTES

EXPLOSIVE OAS READING PRIOR TO STATIC WATER LEVEL: %LEL:

Calibration Record ST-'tK/iey LA^bfU\

Instruments; (A.-Z.-L

CZf C^scop*.

Date;

Time;

pH 4;

pH 7;

pH 10;

pH Slops;

Cond.

Cond. Slops;

D.O.

CH4 2.0 %;

LEL 50%:

Units pH; S.U.

6 -yUs-U:).

CSIo

^•0 1

•— l-'O i_

-— /o *30

—

—

— —

z.r —

^0

Conductivity: umhos/cm D.O. mg/L

Hu 1 associates, inc. M01 Slendale Avenua, Sulla 100 • Talaoa, Olilo 43014


MONITORING POINT;

DETECTION:

ASSESSMENT:

PX-58


NAME: StIckney Rd Landfill

ADDRESS: City of Toledo, DSW, 2411 Albion St. Toledo, OH 43606


PROJECT NUMBER:

TELEPHONE:

COT192

(419) 936-2510

COORDINATES:


_ N CONDITION OF WELL:

"E GROUND SURFACE ELEVATON: TOTAL DEPTH (PROM OROUNO SURPACB):

SCREENED INTERVAL (INCLUOINO SAND PACK):

SCREENED FORMATION:



TOTAL DEPTH (PROM TOP OF CASINO):


PVC/2"

WEATHER:


WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE ("F):

PERSONNEL PRESENT:




STATIC WATER LEVEL (PROM roe):

GROUNDWATER ELEVATION: JIUJL.

DATE OF PURGING:,

PURGING METHOD:^

PURGING RATE:

9//e./cri

PURGING DATA

TIME OF PURGING:

VOLUME PURGED:

/yyv y.Q

WELL VOLUMES PURGED


Time /yA /'vrr PH b U> Temp. //.§> n 7 n.-/ Spec. Cond.

CoiT. Cond. S-V5

Redox Pot. wV) */>/» •jiS D.O. lij Turbidity Joe /c> yes' ioC Water Level* n^y i/-v)


Well casing

DIamstar (In.)

Gallons Par Foot

of Dspth

Fast cf Standing

Watar

3 Wall

Volumas

Total Voluma to

Purga (Gal.)

1 0.041 X X3

2 0.163 X X3

4 0.653 X X3

6 1.469 X X3

* measurement from top of casino


SAMPLING METHOD:

SAMPLING DATA yyisT SAMPLING RATE (IP USINO DEDICATEB PUMP):

STATIC WATER LEVEL (AFTER SAMPLINO):

NOTES

i^// c.( <=>>/ O,/ i^j 77<.rA

BXPUOStVe GAS RBAOiNG PRIOR TO STATIC WAT8R LBVEL HLBl:

Hu & as ociates, inc. M01 aiondila Avtnua, Bulla 300 0 Toiada, OOlo 43614


MONITORING POINT;

DETECTION:

ASSESSMENT:

PX-59


NAME: Stickney Rd Landfill

ADDRESS: City of Toledo, DSW, 2411 Albion St. Toledo, OH 43606


PROJECT NUMBER:

TELEPHONE:

COT192 (419) 936-2510

COORDINATES:




TOTAL DEPTH (PROMOROUNDBURPACH):


SCREENED FORMATION:




SCREENED DEPTH (BCRBEN ONLY):

PVC/2"

WEATHER:


WEATHER CONDITIONS

WIND DIRECTION: TEMPERATURE (°F):

PERSONNEL PRESENT:






PURGING DATA

DATE OF PURGING:

PURGING METHOD:

PURGING RATE: ) J^

TIME OF PURGING:

VOLUME PURGED: ±tc£^

WELL VOLUMES PURGED

Initial 1 2 3 4 S 8/Flnal

Time N/r /VI)- /y2AP

PH t, CL<i C'/f^ Temp. 'L-» /hi /Ir i/r //.y Spec. Cond.

Corr. Cond. V5'*7i' ct/-

Redox Pot. /Vt iO L. -iLl D.O. IM- 1 J>'fr J. ̂ 7 ^.S3 Turbidity ZZJ

Water Level- Ziyi /VV? Yvi


Well easing

Diameter (In.)

Gallcna Per Foot

of Deptn

Feet of Standing

Water

3 Well

Volumes

Total Volume to

Purge (Gel.)

1 0.041 X X3

2 0.183 X X3

4 0.8S3 X X3

e 1.489 X X3

' measurement from top of easing


SAMPLING METHOD:

SAMPLING DATA /yZ-O SAMPLING RATE (IPUSINO DSOICATEO PUMP):

STATIC WATER LEVEL (APTBR SAMPUNO):

NOTES

BXPLOSIVe QAa READING PRIOR TO STATIC WATER LEVEL *CH4:

Calibration Record Cjf"A\J<-

Instruments:

Date:

Time:

pH4:

pH 7:

pH10:

pH Slope:

Cond. ^

Cond. Slope:

D.O.

CH4 2.5 %:

LEL 60%:

Unite pH: S.U.

/3S-^

•—

—

— —

— — <•— -

• -

Conductivity: umhos/cm D.O. mg/L

> •D TJ m z g X 00

APPENDIX B

Table 1 (Tyler) and Tables 2 and 3 (Stickney) Documenting the Results of the Sampling Activities Completed on July 24, 2007 and July 25, 2007

HULL & ASSOCIATES, INC. MARCH 2008 TOLEDO, OHIO COT192.100,0009.DOC

CITY OF TOLEDO TYLER STREET LANDFILL

TABLE 1

LABORATORY ANALYTICAL DATA REPORTED FOR THE JULY 24,2007 SAMPUNG EVENT

P^rarhetef Units T-MW-i9 07/24/07

T-MW-19 Du plicate vrmm

T-MW-21 07/24/07

T-MW-23 07/24m7

T-MW-29 07/24/07

T-«W-2T 07/24AI7

T-MW-29 07/24W7

T-MW-31 07/24A)7

T-MW-33 07124107

T-MW-35 07/24/07

Metals Mercury

PCBs AroclorlOie Aroclor1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Arodor 1254 Aroclor 1260

Pesticides 4.4-DDT Aldrin Heptachlor

PAH'S Acenaphthene Benz(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluorantliene Benzo(K)Fluoranthene Chrysene Dlbenz(A,H)/\nthracerre lndeno(1,2,3-Cd)pyrene Naphthalene Pyrene

Field Parameters Conductivity Dissolved Oxygen pH Redox Potential Temperature Turtxdity

mg/L

mg/L mg/L mg/L mg/L mg/L mg/L mg/L

mg/L mg/L mg/L

mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L

mg/L

mg/L

umhos/cm mg/L S.U. mv •C

mg/L

0.00032

<0.0005 <0.0005 <0.0005 <00005 <0.0005 <0.0005 <0.0005

<0.00005 <000005 <0.00005

<0.01 <0.00026 0.00068 0.00091 ooooo-* 0.00042^ 0.0021 0.003 0.017

0.00067

7410 0.09 6.79 -205 13.1 1000

0.0003

<0.0005 <0.0005 <00005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.00039^ <0.00026 0.00075 0001

0.00082 0.00048^ 0.003 0.003 0.015

0.00053

7410 0.09 6.79 -205 13.1 1000

<00002

<0.0005 <0.0005 <0.0005 <00005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.00046 <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 <0.00022 <0.01 <0.01

3310 0.39 6.45 -154 13 9 364

<0.0002

<0.0005 <00005 <00005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.0026^ <0.00026 <0.0002 <0.00017 <00017 <0.01

<0.0002 <0.00022 <0.01 <0.01

6170 0.1 6.7 -180 17.8 0.09

<0.0002

<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.0021 •• <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 <0.00022 <0.01

0.0003^

8650 0.06 6.59 -179 14.6 13.91

<0.0002

<0.0005 <0.0005 <0.0005 <0.0005 <00005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.0023^ <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 <0.00022

<0.01 0.00031

7620 0.02 6.69 -177 13.3

1

0.00016 •*

<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0 00005 <0.00005

0.00042^ <0.00026 <0.0002 <0.00017 <0.0017 <0.01 0.0012 0.0012 0.0078^ 0.00033^

11100 0.03 682 -208 14.7 121

0.00012-'

<0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

0.00042^ <0.00026 <0.0002 <0.00017 <0.0017

<0.01 00014 0.0011

0.00041 •' 0 00016 •*

4490 0.71 6.41 -138 12.7 25

<0.0002

<00005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

<0.01 <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 <0.00022 <0.01 <0.01

5780 0.29 6.55 -167 21.2 2

<0.0002

<0.0005 <0.0005 <0.0005 <0.0005 <0 0005 <0.0005 <0.0005

<0.00005 <0.00005 <0.00005

<0.01 <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 <0.00022 <0.01 <0.01

3330 0.04 6.56 -202 15.2 2

J-Estimated value detected tietween the MDL and the laboratory PQL

HULL & ASSOCIATES. INC. TOLEDO. OHIO

DECEMBER 2007 COT192 100 0003 XLS

CITY OF TOLEDO STICKNEY AVENUE LANDFILL

TABLE 2

LABORATORY ANALYTICAL DATA REPORTED FOR THE JULY 25. 2007 SAMPUNG EVENT

Parameter Unite 8-MW-21 07/25/07

S-MW-24 07/25/07

8-MW-27 07/25/07

S-MW.27 liiiîciate 07/25/07

S-MW-00 07/25/07

8-MW-33 07/25/07

$-MVt/-3S 07/25AI7

Metals Mercury

PCBs Aroclcr 1016 Arodor 1221 Aroclor1232 Arodor 1242 Arodor 1248 Arodor 1254 Arodor 1260

Pesticides 4.4 - DDT Aldrin Heptachlor

AH's Acenaphthene Benz(A)Anthracene Benzo(A)Pyrene Benzo(B)Fluoranthene Benzo(K)Fluoranthene Chrysene Diben2(A.H)Anthracene lndeno(1.2,3-Cd)pyrene

Pyrene

Field Parameters Conductivity Dissdved Oxygen PH Redox Potential Temperature Turtxdity

mg/L


mg/L mg/L mg/L

mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L

umhos/cm mg/L S.U. mv •0

mg/L

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0 0002 <0.0002

<0.0005 <0.00005 <0 00005

0.0002 •• <0.00026 <0.0002

0.00012-' <0.0017 <0.01

0.00084 •• 0.00099 •' 0.0082^

<0.01

7830 0.10 6.61 -128 13.3 65

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0 0002 <0.0002 <0.0002

<0.0005 <0.00005 <0.00005

<0.01 <0.00026 <0.0002 <0.00017 <0.0017 <0.01 <0.0002 <0.00022 <0.01 <0.01

3270 0.29 6.87 -118 16.6 145

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002

<0 00005 <0.00005 <0.00005

<0.01 <0.00026 <0.0002 <0.00017 <0.0017 <0.01 <0 0002 <0.00022 <0.01 <0.01

3430 0.01 628 -116 12.8 1

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002

<0 00005 <0.00005 <0.00005

<0.01 <0.00026 <0.0002 0.00014 <0.0017 <0.01

0.00091 0.0011 <0.01 <0.01

3430 0.01 6.28 -116 12.8 1

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0 0002 <0.0002

<0.00005 <0.00005 <0.00005

0.005^ <0.00026 <0.0002 <0.00017 <0.0017 <0.01

0.00084 0.00082 0.00045

<0.01

4130 0.01 6.51 -144 13.4 1000

<0.0002

<0.0002 <0.0002 <0.0002 <0.0002 <0 0002 <0.0002 <0.0002

<0.00005 <0.00005 <0.00005

0.0013^ <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 0.0005 0.0061 •' 0.00017 •'

6400 0.01 6.62 -145 13.2 29

<0.0002

<0.0002 <0.0002 <0 0002 <0.0002 <0.0002 <0.0002 <0.0002

<0.00005 <0.00005 <0 00005

0.0019^ <0.00026 <0.0002 <0.00017 <0.0017 <0.01

<0.0002 0.00078 0 00014^ 0.0003 •*

5900 0.01 6.57 -175 13.9 26

J-Estimated value detected between the MDL and the laboratory PQL.

HULL & ASSOCIATES, INC TOLEDO, OHIO

DECEMBER 2007 COT192 100 0003 XLS

CITY OF TOLEDO STICKNEY AVENUE LANDFILL

TABLES

LABORATORY ANALYTICAL DATA REPORTED FROM THE SENTINEL MONITORING WELLS FOR THE JULY 25, 2007 SAMPLING EVENT

Parameter

PCBs Aroclor 1016 Aroclor 1221 Aroclor 1232 Aroclor 1242 Aroclor 1248 Aroclor 1254 Aroclor 1260

SEMIVOLATILE ORGANICS DImethylaniline

VOLATILE ORGANIC COMPOUNDSs ^ 1,1-Dlchloroethane Acetone Benzene Chlorobenzene Chloroethane Ethylbenzene M,p-Xylene Methylene Chloride O-Xylene Toluene

Field Parameters Conductivity Dissolved Oxygen pH Redox Potential Temperature Turbidity

Mfi


mg/L

mg/L mg/L mg/L mg/L mg/L mg/L

mg/L mg/L mg/L

mg/L

umhos/cm mg/L S.U. mv •c

S.MW-36 07/25rt)7

S-MW-37 07/25/07

<0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 0.047 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 0.038

<0.01 <0.01

<0.005 0.13 0.058 <1 0.022 0.14 0.0082 <0.25 0.059 <0.25 <0.005 2.1 0.0043 •• 7.6 <0.005 0.1 <0.005 4.5 0.0013 •* 1.2

5220 16200 0.12 0.03 6.46 6.82 -118 -155 13.5 16.2 13 188

J-Estimated value detected between the MDL and the laboratory PQL 1 - Only volatile organics detected above the MDL or laboratory PQL are listed. The complete list of sampled organics can be found on the laboratory analytical report included in /Appendix C.

HULL & ASSOCIATES, INC. TOLEDO. OHIO

DECEMBER 2007 COT192.100.0003J(LS

,

APPENDIXC J, U •

• T3." m; . • z:

Laboratory Arialytical Reports for the Leachate Sampling Activities Completed on July a 24, 2007 (Tyler) and July 25, 2007 and November 6, 2007 (Stickney). g

HULL & ASSOCIATES, INC. MARCH 2006 ° TOLEDO, OHIO COT192.100.0009.DOC

Thuisday, August 02,2007

Belmont'Labs' Tine Environmental Service Company.

Karen Okonta Hull and Associates, Inc. 3401 Glendale Avenue Toledo, OH 43614

TEL: (800)241-7173 FAX (419)385-5487

RE: COT192

Dear Karen Okonta:

Order No.: 0707C29

Belmont Labs received 11 sample(s) on 7/25/2007 for the analyses presented in the following report.

Belmont Lahs attests that all analytical methods were performed using acceptable methods, and that the QA/QC pmcedures stipulated in these methods were followed: USÂ's RCRA Program regards a statement of quality assurance as a legal means of assuring that acceptable and uniform laboratory methods and QA/QC practices were followed by the laboratory.

If you have any questions regarding the test results, please feel fiee to call me at 937.832.8242.

Respectfully submitted.

A

Holly Green J

Project Manager

QC LEVEL; LEVEL E

CC: Copy of invoice with report.

25 Holiday Drive Englewood. Ohio 45322 1.937.832.8242 1.937-832-2868 Fai

Belmont Labs Date: 02-Aug-07

CUENT: Hull and Associates, Inc. Project: COT192 CASE NARRATIVE Lab Order: 0707C29

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C29-001B: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C29-001BMS: Surrogate recovery for DCB is low due to matrix interfererrce, but the recovery for TCMX is acceptable. Spike recovery for Aroclor 1260 is low due to matris interference.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C29-001BMSD: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable. Spike recovery for Aroclor 1260 is low due to matris interference.




Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C29-009B: Surrogates out due to matrix interference.


Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-001B: Surrogates out due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-001BMS: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-001BMSD: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-001BMSD: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable. Spike recoveries low due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-001BMS: Surrogate recovery

Page 1 of 2

CLIENT: Hull and Associates, Inc. Project: COT192 CASE NARRA'llVE Lab Order: 07D7C29

for DCB is low due to matrix interference, but the recovery for TCMX is acceptable. Spike recoveries low due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-002B: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-007B: Surrogate recovery for DCB is low due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C29-009B: Surrogates out due to matrix interference.

Page 2 of2

Belmont Labs Date: 02-Aug-O7

CLIENT: Project:

Hull and Associates, Inc. COT192

Lab Order: 0707C29

Lab ID: 0707C29-001

CUent Sample ID: COT192:MW19:G072407:509

CoUection Date: 7/24/2007 7:14:00 AM

Matrix: GROUNDWATER

Analyses Result PQL Qual Units DF Date Analyxed

PCBS IN WATER SWB082 Analyst DG Arodor1016 BDL 0.50 MQrt. 1 7/30/2007 3:16:00 PM

AfOdorl221 BDL 0.50 MB/L 1 7/30/2007 3:16:00 PM

Arodor1232 BDL 0.50 MBA 1 7/30«007 3:16:00 PM

Arodor 1242 BDL 0.50 MB4. 1 7/30/2007 3:16:00 PM

AroclGr124a BDL 0.50 POA 1 7/30a007 3:16:00 PM

Arodor1254 BDL 0.50 IJB/L 1 7/30/2007 3:16:00 PM

Arodor 1260 BDL 0.50 MOA. 1 7/30«007 3:16:00 PM

Sum Decachlorobiphenyl 0 35-143 S %REC 1 7/30/2007 3:16:00 PM

Sum TelradUoio-m-xytena 43.0 37-116 *REC 1 7/30/2007 3:16:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heptadilor BDL 0.050 MOA 1 7/30n007 3:16:00 PM

Aldrln BDL 0.050 MOA. 1 7/30«007 3:16:00 PM

4.4-ODT BDL 0.050 M9A. 1 7/30/2007 3:16:00 PM

Sum Decachlorobiphenyl 0 28-172 S %REC 1 7/3(V2007 3:18:00 PM

Sum leirachlonHn-xylene 43.0 45-129 S %REC 1 7/30«007 3:16:00 PM

MERCURY, TOTAL SW7470A Analyst RJE Mercury 0.00032 0.00020 mg/L 1 8/1/2007 8:26:00 AM

PAH BY EPA 8270C SW8270C Analyst DG Naphthalene 17 10 MOA. 1 7/31/2007 3:14:00 AM

BDL 10 MBA. 1 7/31/2007 3:14:00 AM

Pyrene 0.67 10 J MBA. 1 7/31/2007 3:14:00 AM

Benz(a)anthrac8ne BDL 0.26 MflA- 1 7/31/2007 3:14:00 AM

Chrysena 0.42 10 J MBA. 1 7/31/2007 3:14:00 AM

0.91 0.17 MBA. 1 7/31/2007 3:14:00 AM

Benz6(k)ftuoranthene 0.60 1.7 J MBA. 1 7/31/2007 3:14:00 AM

Benzo(a)pyreRe 0.68 0.20 MBA. 1 7/31/2007 3:14:00 AM

lndeno(U.3-cd)pyrene 3.0 0.22 MBA. 1 7/31/2007 3:14:00 AM

2.1 0.20 MBA. 1 7/31/2007 3:14:00 AM

33.6 2(W3 %REC 1 7/31/2007 3:14:00 AM

Sum 2-Ruorobiphenyl 36.6 19-58 %REC 1 7/31/^7 3:14:00 AM

Sum p-Terphenykl14 19.8 ia«2 %REC 1 7/31/2007 3:14:00 AM

Pagelofl2


Lab ID: 0707C29-002 CUent Sample ID: COT192:MW19:G072407A:509

CoUection Date: 7/24/2007 7:14:00 AM Matrix: GROUNDWATER


CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 Project: COT192 Project: COT192

Lab m: 0707C29-005 Client Sample ffi: COT192:MW21 :G072407:509

CoUectlon Date: 7/24/2007 8:09:00 AM Matrix: GROUNDWATER

Analyses Result PQL Qual UniU DF Date Analyzed Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER SW8082 Analyst DG PCBS IN WATER SWa082 Analyst DG Arodor 1016 BDL 0.50 MOA 1 7/30/2007 6K)1:00 PM Arodor 1016 BDL 0.50 P9^ 1 7/30/2007 9:52:00 PM

Arodor1221 BDL 0.50 MQA 1 7/30«007 6:01«lPM Arodor 1221 BDL 0.50 pgA 1 7/30«007 9:52:00 PM

Arodor 1232 BDL 0.50 MOA 1 7/30/2007 6:01:00 PM Arodor1232 BDL 0.50 Pflrt- 1 7/30/2007 9:52:00 PM

Arodor 1242 BDL 0.50 MOA 1 7/30/2007 6K)1:00PM Arodor 1242 BDL 0.50 peA. 1 7/30/2007 9:52:00 PM

Arodor 1248 BDL 0.50 MOA 1 7/30/2007 6:01:00 PM Arodor 1248 BDL 0.50 P9A 1 7/30/2007 9:52:00 PM

Arodor1254 BDL 0.50 MQA 1 7/30/2007 6:01:00 PM Arodor1254 BDL 0.50 P9A 1 7/30/2007 9:52:00 PM

Arodor 1260 BDL 0.50 MQA 1 7/3(V2007 6i)1:00 PM Arodor 1260 BDL 0.50 POA 1 7/30«007 9:52:00 PM

Surr OecadUorobiphenyt 0 35-143 s %REC 1 7/30/2007 6:01:00 PM Sum Decachloroblphenyl 39.0 35-143 %REC 1 7/30/2007 9:52:00 PM

SUIT Tetrachlonwri'xylene 59.0 37-118 %REC 1 7/30a007 6:01:00 PM Sum Tetrachtoro-m-xytene 59.0 37-116 %REC 1 7/30^007 9:52:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heptachlor BDL 0.050 MQA 1 7/30/2007 6:01:00 PM Heptachlor BDL 0.050 pg/L 1 7/30/2007 9:52:00 PM

Aldrin BDL 0.050 POA 1 7/3(V2007 6:01:00 PM Aldhn BDL 0.050 POA 1 7/30a007 9:52:00 PM

4.4'-D0T BDL 0.050 MOA 1 7/30/2007 6:01:00 PM 4.4-DDT BDL 0.050 pgA 1 7/30/2007 9:52:00 PM

Surr Oecadiloroblphenyl 0 28-172 s %REC 1 7/30/2007 6:01:00 PM Sum Decadilorobipherryl 39.0 28-172 %REC 1 7/30«007 9:52:00 PM

Surr Tetrachloro-m-xylene 59.0 45-129 %REC 1 7/30C007 6:01:00 PM Sum. Tetrachloro-m-xylena 59.0 45-129 %REC 1 7/30/2007 9:52:00 PM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY, TOTAL SW7470A Analyst: RJE Mercury 0.00030 0.00020 mgA. 1 6/1/2007 8:34:00 AM Mercury BDL 0.00020 mg/L 1 a/1/2007 8:36:00 AM

PAH BY EPA 8270C SW8270C Analyst DG PAH BY EPA 8270C SWB270C Analyst DG Naphthalene 15 10 MOA 1 7/31/2007 525:00 AM BDL 10 PflA 1 7/31/2007 6:08:00 AM

Acenaphthene 0J9 10 J MOA 1 7/31/2007 525:00 AM Acenaphtherte 0.46 10 J pgA 1 7/31/2007 6:08:00 AM

Pyrene 0.53 10 J MOA 1 7/31/2007 5:25:00 AM Pyrerte BDL 10 pgA 1 7/31/2007 6:06:00 AM

Benz(a)anthracene BDL 026 POA 1 7/31/2007 525:00 AM Benz(a)anthracene BDL 026 PflA 1 7/31/2007 6:06^)0 AM

Chrysene 0.48 10 J PQA 1 7/31/2007 525:00 AM Chrysene BDL 10 PflA 1 7/31/2007 6:06:00 AM

Benzo(b)fluoranthene 1.0 0.17 POA 1 7/31/2007 525:00 AM Benzo(b}ftuoranthene BDL 0.17 PflA 1 7/31/2007 6:08:00 AM

Benzo(k)ntioranlhene 0.82 1.7 J POA 1 7/31/2007 5:25:00 AM Benzo(k)fluoranthene BDL 1.7 MflA 1 7/31/2007 6:06:00 AM

Benzo(a)pyrene 0.75 020 POA 1 7/31/2007 525:00 AM Benzo(a)pyrBne BDL 0.20 pgA 1 7/31/2007 6:08:00 AM

lncleno(1,2.3-cd)pyrene 3.0 022 PQA 1 7/31/2007 525:00 AM lndeno(1.2.3-cd)pyrene BDL 022 PflA 1 7/31/2007 6:08:00 AM

Dlbenz(a.h)anthracane 3.0 020 P9A 1 7/31/2007 525:00 AM Dibenz(a,h)anthfacene BDL 020 pgA 1 7/31/2007 6:08:00 AM

Surr Nitrobenzene-dS 33.0 2003 %REC 1 7/31/2007 525:00 AM Sum Nitrobenzene-d5 33.6 2063 %REC 1 7/31/2007 6:08:00 AM

Surr 2-FIuorpblpheriyl 32.0 1008 %REC 1 7/31/2007 5:25:00 AM Sum 2-Fluoroblphenyl 33.7 19-58 %REC 1 7/31/2007 6:08:00 AM

Surr p>Terphenyl-d14 15.6 1002 %REC 1 7/31/2007 5:25:00 AM Sum p-Terpheny(-d14 24.9 1062 %REC 1 7/31/2007 6:06:00 AM

Page2ofl2 Page 3 of 12

Belmont Labs Date; 02-Aug-07

Lab ID: 0707C29-006

Client Sample ID: Com92:MW23:G072«7:509 CoUectianDate: 7/24^007 8:34;00 AM

Matrix: GROUNDWATER


CLIENT: Hull and Associates, Inc. Lab Order; 0707C29 CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 Project: COT192 Project: COT192

Lab ID: 0707C29-007

Client Sanqile ID: COT192;MW25;G072407;509 CoUecUon Date: 7/24/2007 9:00:00 AM

Matrix; GROUNDWATER

Analyses Result PQL Qual Units DF Date Analyzed Analyses Result PQL Qua] Units DF Date Analyzed

PCBS IN WATER SWB082 Analyst DG PCBS IN WATER SW8082 Analyst DG

Arodor1016 BDL 0.50 1 7/30/2007 7:07K)0PM Arodor1016 BDL 0.50 pgrt. 1 7/3Q0007 8:46:00 PM

Arador 1221 BDL 0.50 poA 1 7/30«007 7:07:00 PM Arodor 1221 BDL 0.50 pg/L 1 7/30/2007 8:46:00 PM

Arador 1232 BOL 0.50 port. 1 7/3Qf2007 7:07M PM Arodor 1232 BOL 0.50 pgrt- 7/3000Q7 8:46:00 PM

Arodor 1242 BDL 0.50 port. 1 7/30«007 7:07:00 PM Arodor 1242 BOL 0.50 pgrt. 1 7/30/2007 8:46:00 PM

Arodor124a BDL 0.50 pgrt- 1 700/2007 7:07:00 PM Arodor 1248 BDL 0.50 pgrt. 1 7/30/2007 8:46:00 PM

Afodor 1254 BDL 0.50 pgrt. 1 7/30/2007 7:07:00 PM Arodor 1254 BDL 0.50 pgrt. 7/30/2007 8:46:00 PM

Arodor 1260 BDL 0.50 port. 1 7/30«007 7:07:00 PM Arodor 1260 BDL 0.50 pgrt. 1 7/30/2007 6:46:00 PM

Sum Decachloroblphenyi 33.0 35-143 S %REC 1 7/3QQ007 7:07:00 PM Sum Decachlorablphenyt 22.0 35-143 s %REC 1 7/30/2007 8:46:00 PM

Sum Tetrachloro-m^xylene 74.0 37-116 %REC 1 7/300007 7:07:00 PiA Sum Tetrachloro-m-xylene 60.0 37-116 %REC 7/30/2007 8:46:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG ORGANOCHLORINE PESTICIDES SW8081A Analyst: DG

Heptachlor BDL 0.050 MDA 1 7/30/2007 7:07:00 PM Heptachky BDL. 0.0S0 port. 7/30/2007 8:46:00 PM

Atdrln BDL 0.050 PDA- 1 7/30/2007 7:07.-00 PM Aldfin BDL 0.050 pgrt. 1 7/30/2007 8:46:00 PM

4.4'-DDT BDL 0.050 pgA 1 7/300007 7:07:00 PU 4.4-DDT BDL 0.050 pgrt. 1 7/30/2007 8:46.-00 PM

Sum. Decachlorabiphenyl 33.0 26-172 %REC 1 7/300007 7:07:00 PM Sum Decachlorobiphenyl 22.0 28-172 S %REC 1 7/30/2007 8:46:00 PM

Sum Tetractibro-m-xylene 74.0 45-129 %REC 1 7/30^007 7:07:00 PM Sum TetTBchloro-m-xylena 60.0 45-129 %REC 1 7/30/2007 8:46:00 PM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY, TOTAL SW7470A Analyst RJE

Mercury BDL 0.00020 rnort. 1 6/1/2007 8:43:00 AM Mercury BDL 0.00020 mg/L 1 a/1/2007 8:45:00 AM

PAH BY EPA8270C SW8270C Analyst DG PAH BY EPA 8270C SW8270C Analyst DG

Naphthalene BOL 10 pgrt. 1 7/31/2007 6:51:00 AM Naphthalene BDL 10 pgrt. 1 7/31/2007 7:33:00 AM

2.6 10 J port. 1 7/31/2007 6:51:00 AM Acenaphthene 2.1 10 J pgrt. 1 7/31/2007 7:33:00 AM

Pyrene BDL 10 port. 1 7/31/2007 6:51:00 AM Pyrene 0.30 10 J pg/L 1 7/31/2007 7:33:00 AM

Benz(a)anthrac8ne BOL 0.26 port. 1 7/31/2007 6:51:00 AM Benz(a)anthracena BDL 0.26 pgrt. 1 7/31/2007 7:33:00 AM

Chrysene BDL 10 pgrt- 1 7/31/2007 6:51K)0 AM Chrysene BDL 10 pg/L 1 7/31/2007 7:33:00 AM

Benzo(b)fhJoranthert8 BDL 0.17 pgrt- 1 7/31/2007 6:51:00 AM Benzo(b)fUioranthene BDL 0.17 pgrt. 1 7/31/2007 7:33:00 AM

Benzo(k)fluofanthene BOL 1.7 pgrt. 1 7/31/2007 6:51:00 AM Benzo(li)fluoranlhene BDL 1.7 pgrt. 1 7/31/2007 7:33:00 AM

Benzo(a)pyrene BDL 0.20 port. 1 7/31/2007 6:51:00 AM BDL 0.20 pgrt. 7/31/2007 7:33:00 AM

lndeno(1,2,3-cd)pyrene BOL 0.22 pgrt. 1 7/31/2007 6:51:00 AM lndeno(1,2.3-al)pyreno BDL 0.22 pgrt. 1 7/31/2007 7:33:00 AM

Dibenz(a.h)anthracert8 BDL 0.20 pgrt. 1 7/31/2007 6:51:00 AM Dibenz(a.h)anthracene BDL 0.20 pg/L 1 7/31/2007 7:33:00 AM

Sum Nitrobenzene-d5 33.4 2063 %REC 1 7/31/2007 6:51:00 AM Sum Nilmbenzene-d5 34.4 2963 %REC 1 7/31/2007 7:33:00 AM

Sum 2-Buorobiphenyt 32.0 1968 %REC 1 7/31/2007 6:51:00 AM Sum. 2-Ruorobtphenyl 36.1 19-58 %REC 7/31/2007 7:33:00 AM

Sum p-Terphenyl-d14 20.0 1062 %REC 1 7/31/2007 6:51:00 AM Sum p-TerphenyPd14 24.4 ia«2 %R£C 7/31/2007 7:33:00 AM

Page 4 of 12 Pages of 12


Lab ro: 0707C29-008 CUent Sample ID: COT192:MW27:G072407:509

CoUecdon Date: 7/24/2007 9:32:00 AM Matrix: GROUNDWATER


CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 Project: COT192 Project: COT192

Lab ID: 0707C29-009 CUent Sample m: COTI92:MW29:G072407:S09

CoUeetion Date: 7/24/2007 10:00:00 AM Matrix: GROUNDWATER

Analyses Result PQL Qual Units DF Date Analyzed Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER SW80a2 Analyst DG PCBS IN WATER SW8082 Analyst DG Arodor 1016 BDL 0.50 Mrt- 1 7/30/2007 9:19:00 PM Arodor 1016 BDL 0.50 POA 1 7/3Q«}07 6:34:00 PM Afodor 1221 BOL 0.50 ygA 1 7/3(V2007 9:19:00 PM Arodor 1221 BDL 0.50 Pfl/L 1 7/30/2007 6:34:00 PM

Arodor 1232 BOL 0.50 port. 1 7/30a007 9:19:00 PM Arodor 1232 BDL 0.50 POA 1 7/30/2007 6:34:00 PM

Arodor 1242 BDL 0.50 POfl- 1 7/30C007 9:19:00 PM Arodor 1242 BDL 0.50 MOA 1 7/30/2007 6:34:00 PM

Arodor 1246 BDL 0.50 pofl- 1 7/30/2007 9:19:00 PM Arodor 1248 BDL 0.50 POA 1 7/30/2007 6:34:00 PM

Arodor 1254 BDL 0.50 port- 1 7/30/2007 9:19:00 PM Arodor 1254 BDL 0.50 POA 1 7/30/2007 6:34:00 PM

Arodor 1260 BDL 0.50 POA 1 7/300007 9:19:00 PM Arodor 1260 BDL 0.50 POA 1 7/30^007 6:34:00 PM

Surr Decachloroblphenyi 44.0 35-143 %REC 1 7/300007 9:19:00 PM Sum Decachloroblphenyi 0 35-143 S %REC 1 7/30/20076:34:00 PM

Sum Tetrachloro-m-xylene 61.0 37-116 %REC 1 7/300007 9:19:00 PM Sum Tetrachloro-m-xylene 27.0 37-116 S *REC 1 7/30^007 6:34:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG ORGANOCHLORINE PESTICIDES SWB081A Analyst: DG Heptadilor BDL 0.050 POA 1 7/300007 9:19:00 PM Heptachlor BDL 0.050 POA 1 7/30/2007 6:34:00 PM

Aldrin BDL 0.050 pgA 1 7/30/2007 9:19:00 PM Aldrin BDL 0.050 POA 1 7/30«007 8:34:00 PM

4.4-ODT BDL 0.050 POA 1 7/3Q0007 9:19:00 PM 4.4-DDT BDL 0.050 POA 1 7/30/2007 6:34:00 PM

Sum Decadilorobiphenyl 44.0 28-172 %REC 1 7/300007 9:19:00 PM Sum Decachloroblphenyi 0 28-172 s *REC 1 7/30/2007 6:34:00 PM Sum Tetrachloro-m-xylene 61.0 45-120 %REC 1 7/30/2007 6:19:00 PM 27.0 45-129 s %REC 1 7/3a«007 6:34:00 PM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY. TOTAL SW7470A Analyst RJE Mercury BDL 0.00020 mg/L 1 6/1/2007 6:47:00 AM Mercury 0.00016 0.00020 J mg/L 1 8/1/2007 8:49:00 AM

PAH BY EPA8270C SW8270C Analyst DG PAH BY EPA 8270C SW8270C Analyst DG Naphthalene BDL 10 POA 1 7/31/2007 8:16:00 AM Naphthalene 7.8 10 J PflA 1 7/31/2007 8:58:00 AM Acenaphthene 2.3 10 J POA 1 7/31/2007 8:16:00 AM Acenaphthene 0.42 10 J POA 1 7/31/2007 8:58:00 AM Pyrene 0.31 10 J POA 1 7/31/2007 8:16:00 AM Pyrene 0.33 10 J POA 1 7/31/2007 8:58:00 AM Benz(a)anthracene BOL 0.26 POA 1 7/31/2007 8:16:00 AM Benz(a)anthracene BDL 0.26 POA 1 7/31/2007 6:58:00 AM Chrysene BDL 10 PQA 1 7/31/2007 8:16:00 AM Chrysene BDL 10 POA 1 7/31/2007 8:58:00 AM Benzo(b)fluaranthene BOL 0.17 POA 1 7/31/2007 8:18:00 AM BenzoO>)fluorantherta BDL 0.17 POA 1 7/3172007 8:58:00 AM Benzo(k)fluoranthene BDL 1.7 POA 1 7/31/2007 8:16^10 AM Ber\zo{k)fluoranthene BDL 1.7 POA 1 7/31/2007 8:58:00 AM Benzo(a)pyrene BDL 0.20 POA 1 7/31/2007 8:16^)0 AM Benzo(a)pyrene BDL 0.20 pgA 1 7/31/2007 8:58:00 AM lndeno(1,2.3-cd)pyrene BDL 0.22 POA 1 7/31/2007 8:16:00 AM lndeno(1,2,3-cd)pyTene 1.2 0.22 pgA 1 7/31/2007 8:58:00 AM Dlbenz(a,h)anthracene BDL 0.20 POA 1 7/31/2007 8:16.-00 AM Dlbenz(a.h)anthracene 1.2 0.20 POA 1 7/31/2007 8:58:00 AM

Sum NitrobenzenesIS 34.1 2883 %REC 1 7/31/2007 8:16:00 AM 37.4 2083 SREC 1 7/31/2007 8:58:00/Uri Sum 2-Ruorobipheny1 31.5 1086 %REC 1 7/31/2007 8:16:00 AM Sum 2-Ruoroblphenyl 37.2 1088 %REC 1 7/31/2007 8:58:00 AM Sum p-Terphenyl-d14 21.2 1082 %REC 1 7/31/200/8:16:00 AM Sum p-Terphenyl-d14 24.9 1082 %R£C 1 7/31/2007 8:58:00 AM

Page 6 of 12 Page7ofl2

Belmont Labs Date: 02'Aug-O7 Belmont Labs Date: 02-Aug-07

CLIENT: Hull and Associates, Inc. Lab Order: 0707C29 CLIENT: Hull and Associates, Inc. Lab Order: 0707C29

Project: COT192 Project: COT192

Lab ID: 0707C29-010 CoUectloQ Date: 7/24/2007 10:28:00 AM Lab ID: 0707C29-011 CoUection Date: 7/24/2007 10:55:00 AM

CUent Sample ED: COT192:MW31:G072407:509 Matrix: GROUNDWATER CUent Sample ID: COT192:MW33:G072407:509 Matrix: GROUNDWATER

Analyses Result FQL Qual Units DF Date Analyzed Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER SW8082 Analyst 06 PCBS IN WATER SW8082 Analyst DG Arodor 1016 BDL 0.50 P0A. 1 7/3tV2007 8:13:00 PM Arodor 1016 BDL 0.50 pgA 1 7/30/2007 7:40:00 PM Arodor1221 BDL 0.50 1 7/30/2007 6:13:00 PM /krodor 1221 BDL 0.50 pgA- 1 7/30/2007 7:40:00 PM

Arodor 1232 BDL 0.50 MQA. 1 7/3(W007 0:13:00 PM Arodor 1232 BDL 0.50 port. 1 7/30«007 7:40:00 PM

Arodor 1242 BDL 0.50 M9A 1 7/30/2007 8:13:00 PM Arodor 1242 BDL 0.50 pgA 1 7/30/2007 7:40:00 PM Arodor 1248 BDL 0.50 pgA 1 7/30/2007 8:13:00 PM Arodor 1248 BDL 0.50 pgA 1 7/3G«007 7:40:00 PM

Arodor 1254 BDL 0.50 M9A 1 7/30/2007 8:13:00 PM Arodor 1254 BDL 0.50 pgA 1 7/30/2007 7:40:00 PM

Arodor1260 BDL 0.50 P9A 1 7/30/2007 8:13:00 PM Arodor 1260 BDL 0.50 pgA 1 7/30/2007 7:40:00 PM

Surr Decachloroblphenyl 43.0 35-143 %R£C 1 7/30/2007 8:13:00 PM Sum Decachloroblphenyl 38.0 35-143 %REC 1 7/30/2007 7:40:00 PM Surr TetracMoro-m-xylene 58.0 37-118 %R£C 1 7/30/2007 8:13:00 PM Sum Tetradiloro-m-xylene 72.0 37-116 %REC 1 7/3Qa007 7:40:00 PM

ORGANOCHLORINE PESTICIOES SW8081A Analyst DG ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heplachlor BDL 0.050 IJflA 1 7/30«007 8;13«) PM Heptachlor BDL 0.050 PQA 1 7/30/2007 7:40:00 PM Aldrln BDL 0.050 M9A 1 7/30/2007 8:13:00 PM Aldrln BDL 0.050 PQA 1 7/30/2007 7:40:00 PM 4.4'-DDT BDL 0.050 M04. 1 7/30/2007 8:13:00 PM 4.4'.DDT BDL 0.050 pgA 1 7/30C007 7:40:00 PM

Surr Decachloroblphenyl 43.0 28-172 %REC 1 7/30C007 8:13:00 PM Sum Decachlorobiphenyi 39.0 28-172 %REC 1 7/30/2007 7:40:00 PM Surr Tetrachloro-tn-xylene 58.0 45-129 *REC 1 7/3O/2O07 6:13:00 PM Sum Tetrachloro-m-xylene 72.0 45-129 %REC 1 7/30/2007 7:40:00 PM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY, TOTAL SW7470A Analyst RJE Mercufy 0.00012 0.00020 J mgA 1 6/1/2007 8:51:00 AM Mercury BDL 0.00020 mg/L 1 6/1/2007 8:53:00 AM

PAH BY EPA8270C SW8270C Analyst DG PAH BY EPA B270C SW8270C Analyst: DG Naphthalene 0.41 10: J pg/L 1 7/31/2007 9:41:00 AM Naphthalena BDL 10 POA 1 7/30/2007 7:59:00 AM Acenaphthene 0.42 10 J VQfl 1 7/31/2^7 9:41:00 AM Acenaphthene BDL 10 pgA 1 7/30^007 7:59:00 AM Pyrene 0.16 10 J M8A. 1 7/31/2007 9:41:00 AM Pyrene BDL 10 pgA 1 7/30flQ07 7:59:00 AM Benz(a)anthfacena BDL 0.26 ; VQIL 1 7/31/2007 9:41:00 AM BDL 0.26 pgA 1 7/30«007 7:59:00 AM Chrysene BDL 10 M9fl. 1 7/31/2007 9:41:00 AM Chrysene BDL 10 pgA 1 7/30/2007 7:59:00 AM Benzo(b)fluoranthene BDL 0.17 pg/L 1 7/31/2007 9:41K)0 AM Benzo(b)nuoranthene BDL 0.17 pgA 1 7/30/2007 7:59:00 AM Benzo(k)fluoranthene BDL 1.7 pgA 1 7/31/2007 9:41:00 AM BDL 1.7 PSA 1 7/300007 7:59:00 AM

BDL 020 P0A 1 7/31/2007 9:41:00 AM Benzo(a)pyrene BDL 0.20 PSA 1 7/300007 7:59:00 AM lndeno(1.2,3-cd)pyrene 1.1 022 PQA 1 7/31/2007 9:41 i)0 AM lndeno(1,2,3<d)pyrBne BDL 0.22 PSA 1 7/300007 7:59:00 AM Dlbenz(a.h)anthrac8ne 1.4 020 pgn. 1 7/31/2007 9:41:00 AM Dibenz(a,h)anthracene BDL 0.20 PSA 1 7/300007 7:59:00 AM

Sum Nitrobenzene-dS 33.8 2003 %REC 1 7/31/2007 9:41:00 AM Sum Nitrobenzene-dS 36.7 2083 %REC 1 7/300007 7:59:00 AM Sum 2-Ruorobiphenyl 34.0 1O50 *REC 1 7/31/2007 9:41:00 AM Sum 2-PluorDblphenyl 39.0 19-58 %REC 1 7/300007 7:59:00 AM Sum p-TerphenyJ-d14 25.5 1062 %REC 1 7/31/2007 9:41^90 AM Sum p-Terphenyl-d14 27.4 1082 %REC 1 7/300007 7:59:00 AM

Page Sofia Page 9 of 12

;s.

Belmont Labs Date: 02-Au^7 Belmont Labs Date: Ol-Aug-O?

CLIENT: Project:


Lab Order: 0707C29 CLIENT: Project:


Lab Order: 0707C29

Lab ID: 0707C:294)12 Client Sample ID: COT192:MW35:G072407:509

CoDection Date: 7/24/2007 11:30:00 AM Matrix: GROUNDWATER

Analyses Result PQL Qual UniU DF Date Analyzed

PCBS IN WATER SW8082 Analyst DG Aroclor 1016 BDL 0.50 PO/L 1 7/3000071025:00 PM

Arodorl221 BDL 0.50 POA. 1 7/3Q0007 10:25:00 PM

Arodor 1232 BDL 0.50 PflA 1 7/300007 10:25:00 PM

Arodor 1242 BDL 0.50 POA. 1 7/300007 10:25:00 PM

Arodor 1248 BDL 0.50 pg/L 1 7/300007 10:25:00 PM

Arodor1254 BDL 0.50 PflA. 1 7/300007 10:25:00 PM

Arodor 1260 BDL 0.50 pgA 1 7/300007 10:25:00 PM

Surr Decachlorobiphenyl 29.0 3&-143 S %REC 1 7/300007 10:25:00 PM

Surr Tetrachloro-m-xylene 60.0 37-116 %REC 1 7/300007 10:25:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heptachlor BDL 0.050 pgA. 1 7/3Q0007 1025.-00 PM

Aldrin BDL 0.050 pgA 1 7/3Q00071025:XPM

4,4-ODT BDL 0.050 pgA 1 7/3QOX7 1025:00 PM

Surr Decachlorobiphenyl 20.0 28-172 %R£C 1 7/30OM71D25:MPM

Surr TetrachlorcHn-xylene 60.0 48-129 %REC 1 7/3QOX710:25:X PM

MERCURY, TOTAL SW7470A Analyst RJE Mercury BDL 0.00020 mgA 1 8/10X7 8:55:MAM

PAH BY EPA 82700 SW8270C Analyst DG Naphthalene BDL 10 pgA 1 7/300007 8:42:00 AM

Acenaphthene BDL 10 pgA 1 7/3QOX7 8:42:XAM

Pyrene BDL 10 PflA 1 7/30OM7 8:42:WAM

Benz(a)anthrac8ne BDL 028 POA 1 7/300X7 8:42:X AM

Chrysene BDL 10 pgA 1 7/30OX7 8:42.x AM

Benzo(b)fluoranthene BDL 0.17 POA. 1 7/3QOX7 8:42:XAM

Benzo(k)fluoranthene BDL 1.7 pgA. 1 7/300X7 8:42:X AM

Benzo(a)pyrene BDL 020 pg/L 1 7/30/2X7 8:42:X AM

lrideno(1.2,3-cd)pyrene BDL 022 POA. 1 7/30OX7e:42:XAM

Dibenz(a,h)anthracene BDL 020 pgA 1 7/30OX7a:42:XAM

Surr Nllrobenzene-d5 37.6 2003 %REC 1 7/300007B:42:XAM

Surr 2-nuorobipheny1 34.6 1058 %R£C 1 7/3QOX7a:42:XAM

Surr p-Terphenyl-d14 22.4 1002 %REC 1 7/300007a;42:XAM

Lab ID: 0707C29-013 CUeot Sample ID: COT192:FBl:W072407:S09

Analyses Result

CoUectlon Date: 7/24/2007 12:00:00 PM Matrix: GROUNDWATER

PQL Qual UniU DF Date Analyzed

PCBS IN WATER ArodorlOia ArDdor1221. Arodof 1232 Arodor1242 Arador124a Aroclor12S4 An>clor1260

Surr Decachlonblphenyt Surr TetracftlorD-m-xytene

ORGANOCHLORINE PESTICIDES Heptachkv Aldjtn 4.4-DDT

Surr Decachkvobiphenyl Sum Telrachtoro-m-xylene

MERCURY. TOTAL Mercury

PAH BY EPA B270C Naphthaiena Aceruphthena Pyrene Beru(a)anthrac8ne Chrysene Benzo(b)nuoraniherw Benzo(k)fiuoranlhene Benzo(a)pyrene lndeno{1,2,3-cd)pyrena Oibenz(a3t)anthrac8ne

Surr Nitrobenzene-dS Surr 2-Ruoroblphenyl Surr p-Terphar]y(-d14

SW8082 Analyst DG

BDL OX PflA. 1 7/30/2X7 10:X:X PM

BDL o.x PBA. 1 7/300X7 10:58:X PM

BDL 0.x pg/L 1 7/3QOX7 10:X:X PM

BDL 0.x P9A. 1 7/30/2X7 10:X:X PM

BDL 0.x pg/L 1 7/30OX7 10:X:X PM

BDL 0.x pgA. 1 7/30/2X7 10:X:X PM

BDL D.X POA- 1 7/30OX7 10:X:X PM

50.0 35-143 %REC 1 7/30OX7 10:M:X PM

82.0 37-116 %REC 1 7/300X7 10:X:X PM

SW8081A Analyst DG BDL 0.0X pgA. 1 7/30OX7 10:X:X PM

BDL 0.0X M9A 1 7/30OX7 10:X:X PM

BDL 0.0X pg/L 1 7/300007 10:M:X PM

M.O 28-172 %REC 1 7/30OX7 10:58:X PM

82.0 45-129 %REC 1 7/3QOX7 10;X:X PM

SW7470A Analyst RJE BDL 0.00020 mg/L 1 a/10X7 8:X:XAM

SW8270C Analyst: DG BDL 10 pg/L 1 7/30OX7 9-25:XAM

BDL 10 PflA. 1 7/3QOX7 925:X AM

BDL 10 PflA. 1 7/30OX7 9-25;XAM

BDL 026 PflA. 1 7/30OX7 9:25:XAM

BDL 10 PflA. 1 7/30OX7fl25:XAM

BDL 0.17 PflA. 1 7/300007 9:25:XAM

BDL 1.7 PflA. 1 7/30OX7 925:X AM

BDL 020 pgA. 1 7/3QOX7g25:XAM

BDL 022 PflA. 1 7/30OX7 925:XAM

BDL 020 pg/L 1 7/300X7 9:2S:X AM

38.8 20-63 %REC 1 7/3QOX7g25:XAM

38.7 19-X SREC 1 7/300007e:25:XAM 382 1002 %REC 1 7/3QOX7g:25:XAM

Page 10 of 12 Page 11 of 12


CLIENT: Hull and Associates, Inc. Work Order: 0707C29 Project: COT192

ANALYTICAL QC SUMMARY REPORT TestCodc: HG GW

Sample ID: MB-14744 SampType: MBLK TestCode: HG.GW Units: man. Prep Date: 7/31/2007 RunNo: 6029S

aiont ID: 77777 Batch ID: 14744 TestNo: SW7470A Analysis Data: 8/1/2007 SeqNo: 754991

Analyte Result PQL SPK value SPK RefVal %REC LowUmIt HlohUmIt RPD RefVal %RPD RPDUmIt Qua]

Mercury BDL 0.Q0020

Sample ID: LCS.14744 SampType: LCS TestCode: HG_GW Units: mfl/L Prep Date: 7/31/2007 RunNo: 60299

aient ID: ZZZZZ Batch ID; 14744 TestNo: SW7470A Analysis Date: 8/1/2007 SeqNo: 754992

Analyte Result PQL SPK value SPK RefVal %REC LowUmtt HghUmlt RPD RefVal %RPD RPDLImIt Qual

Mercury

Sample ID: LCaD>14744 SampType: LCSD TestCode: HG.GW Units: mo/L Prep Date; 7/31/2007 RunNo: 60299

Qlent ID: ZZZZZ Batch ID: 14744 TestNa SW7470A Analysts Date: 8/1/2007 SeqNo: 799007

Analyte Result PQL SPK value SPK RefVal %REC LowUmIt HighUmit RPD RefVal %RPD RPDUmIt Qual

Mercury 0.008180 0.00020 0.00829 0 98.9 80 120 0.00826 1.61 20

Sample ID: 0707C29-a01CMS SampType; MS TestCode: HG_OW Units: mg/L Prep Date: 7/31/2007 RunNo; 60299

aient ID: COT192:MW19:G07 Batch ID: 14744 TestNo: SW747DA Analysis Date; 8/1/2007 SeqNo: 754999

Analyte Result PQL SPK value SPK RefVal %REC LowUmIt HIghUmIt RPD RefVal %RPD RPDUmIt Qual

Mercury 0.005740 0.00020 0.00625 0.000317 86.8 70 130 0 0

Sample ID: Q707C29-001CM3D SampType: MSD TestCode: HG.GW Unite: man. Prep Date: 7/31/2007 RunNo: 60209

aiont ID: COT192:MW19;Q07 Batch ID: 14744 TestNo: SW747QA Analysis Date: 8/1/2007 SeqNo: 794996

Analyte Result POL SPK value SPK RefVal %REC LowUmIt HlghUmlt RPD RefVal %RPD RPDUmIt Qual

Mercury 0.005850 0.00020 0.00823 0.000317 88.5 70 130 0.00574 1.90 30

Page I of 8

1

£ A

a

i a X d £

ielmont Labs Date: 02-Aug-07

'LIENT: Hull and Associates, Inc. Vork Order: 0707C29 >roJeet: COT192

ANALYTICAL QC SUMMARY REPORT TestCode: PAH 8270 W

jample tO: LCSD-14727 SampType: LCSD TestCode: PAH_B270_W Unila: pgrt. Prep Date: 7/27/2007 RunNo; 60273

Client ID: ZZZ72 Batch ID: 14727 TestNo: SW827QC (SW351QC) Analysis Data: 7/30ra007 SoqNo; 754752

âtyte Raault PQL SPK value SPKRefVal %REC LowUmIt HIghUmtt RPDRefVal %RPO RPDUmlt Dual

Surr 2-Fluorobiphenyt 15.27 0 40 0 38.2 19 58 0 0 0 SufT p-Tefphenyl-d14 20.36 0 40 0 50.9 10 62 0 0 0

Sample ID: 0707C29-001AMS SampType: MS TestCode: PAH_a270_W Units: nQfl- Prep Date: 7/27/2007 RunNo: 60273

Client ID: COT192:MWie:Q07 Batch ID: 14727 TestNo: SWB270C (SW3510C) Analysis Date: 7/31/2007 SeqNo: 754787

Vnalyte Result PQL SPK value SPKRefVal %REC LowUmlt HIghUmIt RPDRefVal %RPO RPDUmlt Qua!

^cenaptithene 78.86 10 100 0 78.9 69 93 0 0 Pyrene 67.81 10 100 0.67 67.1 35 101 0 0

Surr Nitrobenzene-dS 14.97 0 40 0 37.4 20 58 0 0 Surr 2-FIuorDt)lpt)enyl 14.49 0 40 0 38.2 19 58 0 0 Surr p-Terphenyt-d14 10.30 0 40 0 25.8 10 62 0 0

Sample ID: 0707C2S4I01AMSD SampType: M3D TestCode: PAH_8270_W Units: pg/L Prep Data: 7/27/2007 RunNo: 60273

Client ID: COT192:MW19:607 Batch ID: 14727 TestNo: SWa270C (SW3910C) Analysis Data: 7/31/2007 SaqNo: 754758

Vnalyte Result PQL SPK value SPKRefVal %REC LowLlmIt HlghUmlt RPDRafVal %RPD RPDUmlt Qual

•\cenaphthena 77.08 10 100 0 77.1 69 93 78.66 2.31 10 =V«ne 62.77 10 100 0.87 62.1 35 101 67.81 7.72 32

Surr Nltrobenzsne-dS 14.59 0 40 0 38.5 20 56 0 0 0 Sum 2-Ruofoblph0ny1 14.56 0 40 0 36.4 19 58 0 0 0 Sum p-TerphenyW14 7.210 0 40 0 18 10 62 0 0 0

Page 3 of 8

lelmont Labs Date: 02'Aug-07

LIENT: Hull and Associates, Inc. ANALYTICAL OC SUMMARY REPORT 'orlt Order: 0707C29

'reject: COT192 TestCode: PAH_8270.W

ample ID: MB-14727 SampType: MBLK TestCode: PAH_e270_W Units: pgfl. Prep Date: 7/27/2007 RunNo: 60273

illant ID: 77777 Batch ID: 14727 TestNo: SWB270C (3W351QC) Analysis Date; 7/30^007 SeqNo: 754750

^nalyte Result PQL SPK value SPKRefVal %REC LowUmlt HlghUmlt RPDRefVal %RPD RPDUmlt Qual

laphthalene BDL 10

canaphthene BDL 10 yrene BDL 10

BDL 0.26

Chrysene BDL 10

BDL 0.17

enzo(k)fluoranthena BDL 1.7

anzo(a)pyrane BDL 0.20

ideno(1.2,3-cd)pyrene BDL 0.22

[}lt)enz(B.h)anthrBC8ne BDL 0.20

Sum Nltrot)enzen»^S 14.83 0 40 0 37.1 20 63 0 0 Surr 2-Ruoroblphenyl 13.38 0 40 0 33.5 19 58 0 0

' Sum p-TerphanyM14 ia73 0 40 0 41.8 10 82 0 0

Sample ID: LCS-14727 SampType: LOS TestCode: PAH_827a_W Units: pgA. Prep Date: 7/27/2007 RunNo: 60273

•aient ID: 77777 Batch ID: 14727 TestNo: SWa27QC (SW3510C) Analysis Date: 7/30/2007 SeqNo: 754751

natyta Result PQL SPK value SPKRefVal %REC LowUmlt HlghUmlt RPDRefVal %RPD RPDUmlt Qual

canaphthene 81.66 10 100 0 81.7 64 103 0 0

Vme 77.81 10 100 0 77.8 35 107 0 0 15.80 0 40 0 39.5 20 63 0 0

Sum 2-Ruoroblphenyl 14.66 0 40 0 36.6 19 58 0 0 Sum p-TarphenylHjl4 18.57 0 40 0 46.4 10 62 0 0

Sample ID: LCSO-14727 SampType: LCSD TestCode: PAH_8270_W Units: pg/L Prep Date: 7/27/2007 RunNo: 60273

:tlant ID; ZZZZZ Batch ID: 14727 TestNo: SW8270C (3W3510C) Analysis Date: 7/30/2007 SeqNo: 754752

nalyta Result PQL SPK value SPKRefVal %REC LowLlmIt HlghUmlt RPDRefVal %RPD RPDUmlt Qual

cenaphthene 81.31 10 100 0 81.3 64 103 81.68 0.454 14

Van# 84.33 10 100 0 84.3 35 107 77.61 8.30 13

Sum Nitrcbenzane-d5 18.36 0 40 0 40.9 20 63 0 0 0

Page 2 of 8


CLIENT: Work Order:

Hull and Associates, Inc. 0707C29

ANALYTICAL QC SUMMARY REPORT Project: COT 192 TestCode: PCB_8082_W

Sample ID: 0707C29401BMS SampType: MS TestCode: PCB_8a82_W Units: ps/L Prep Date: 7/30/2007 RunNo: B02B9

Client ID: COT192:MW10:G07 Batch ID: 14729 TestNo: SW8082 (SW3910C) Analysis Date: 7/30/2007 SeqNo: 754922

Analyte Result PQL SPK value SPK RefVal %REC LowUmit HlghUmit RPD RefVal %RPD RPDUmit Oual

Arodor 1016 9.940 0.50 10 0 99.4 70 130 0 0

Arodor12e0 6.310 0.50 10 0 63.1 70 130 0 0 M

Surr Decachloroblphenyt 0.09000 0 1 0 9 35 143 0 0 S

Surr Tetrachloro-nviylene 0.8200 0 1 0 62 37 118 0 0

Sample ID: 0707C20-001BMSD SampType: MSD TestCode: PCB_eOB2_W Units: pg/L Prep Date: 7/30a007 RunNo: 60289

Client ID: COT192:MW19:G07 Batch ID; 14729 TestNo: SWB083 (SW3910C) Analysis Date: 7/30/2007 SeqNo: 784923

Analyte Result PQL SPK value SPK RefVal %REC LowLimit HlghUmit RPD RefVal %RPD RPDUmit Qual

ArodorlOie 9.310 0.50 10 0 93.1 70 130 9.94 6.55 25

Arodor 1260 5.080 0.50 10 . 0 50.8 70 130 6.31 5.37 25 M Surr Decachloroblphenyl 0.09000 0 1 0 9 35 143 0 0 0 s

Surr Tetrachlcro^xylene 0.5700 0 1 0 57 37 116 0 0 0

Page 5 of 8


CLIENT: Hull and Associates, Inc. Work Order: 0707C29 Project: COT192

ANALYTICAL QC SUMMARY REPORT TestCode: PCS 8082 W

Sample ID: MB-14729 SampType: MBLX TestCode: PCB_8083^W Units; pgn. Prep Dale: 7/30n007 RunNo: 80269

Client ID: 77777, Batch ID; 14729 TestNo: 8W8082 (SW3S10C) Analysis Date: 7/31/2007 SeqNo: 754934

Analyte Result PQL SPK value SPK RefVal %REC LowUmIt HIghUmIt RPD RefVal %RPD RPDLImIt Qual

Arodor 1016 BDL 0.50


Arodor 1232 . BDL 0.50 Arodor1242 BDL 0.50 Arodor124a BDL 0.50

Arodor1254 BDL 0.50


Surr Decachloroblphenyl 0.9100 0 1 0 91 35 143 0 0 Surr Tetrachloro-rrvxylene 0.6800 0 1 0 68 37 118 0 0

Sample ID: LCa-14729 SampType: LC3 TestCode: PCB_8082_W Unite; pgA. Prep Date: 7/3(W007 RunNo: 60289

aient ID: 77777 Batch ID: 14729 TestNo: SW8082 (8W3910C) Analysis Date: 7/31/2007 SeqNo: 754935

Analyte Result PQL SPK value SPK RefVal %REC LowUmlt HlghUmit RPD RefVal %RPD RPDUmit Qual

Arodor 1016 9.680 0.50 10 0 96.8 72 119 0 0 Arodor 1260 7.760 0.50 10 0 77.6 64 132 0 0

Surr Decachloroblphenyl 0.8200 0 1 0 82 35 143 0 0 Surr Tetrachloro-rrv-xytene 0.7600 0 1 0 78 37 lie 0 0

Sample ID: LCSD-1472e SampType: LCSO TestCode: PCB_8082_W Units: pg/L Prep Date: 7/30n007 RunNo: 60288

Batch ID: 14729 TestNo: 8W8082 (SW3510C) Analysis Data: 7/31/2007 SeqNo: 754936

Analyte Result PQL SPK value SPKRafVal %REC LowUmlt HlghUmit RPD Ref Vol %RPD RPDUmit Qual

ArodorlOie 10.41 0.50 10 0 104 72 119 e.sa 7.27 20 Arodor 1260 6.250 0.50 10 0 82.5 64 132 7.76 6.12 19.

Surr Decachloroblphenyl 0.7000 0 1 0 70 35 143 0 0 0 Surr Tetrachloro-m-xylene 0.6300 0 1 0 83 37 116 0 0 0

Page 4 of S

jlmont Labs Dote: 02-Aug-07

LIENT: ôrk Order: roject:

Hull and Associates, Inc. 0707C29 COT192

ANALYTICAL QC SUMMARY REPORT TestCode: PEST 8081 W

iample 10: 0707C29-001BMS SampType: MS

:ilentlD: COT192:MW19;G07 Batch ID: 14729

Knalyto Result

TestCode: PEST.aoSi. Units: pgn.

TestNo: SWB081A (SW3510C)

PQL SPK value SPKRefVal

Prep Date: 7/30/2007

Analysis Date: 7/30/2007

%REC LowLlmlt HIghLlmIt RPDRefVal

RunNo: 80289

SeqNo: 754938

%RPD RPDUmIt Quel

leplachlor 0.5700 0.050 1 0 57 70 130 0 0 M

^drln 0.3900 0.050 1 0 39 70 130 0 0 M

i,4'-DDT 0.3600 0.050 1 0 38 70 130 0 0 M Surr Decachloroblphenyl BDL 0 1 0 0 26 172 0 0 S Sum Tetrachloro-m-xylene 0.6400 0 1 0 64 45 129 0 0

'ample 10: 0707C29-001BMSD SampType: MSO TestCode: PEST_8081_ . Units: MO/I- Prep Date: 7/3Q/2Q07 RunNo: 60289

;llent ID: Can92:MW19:G07 Batch ID: 14729 TestNo: SW8081A (SW3810C) Analysis Date: 7/30/2007 SeqNo: 754839

Mialyte Result PQL SPK value SPKRefVal %REC LowLlmlt HIghUmit RPDRefVal %RPD RPDUmIt Qual

leptachlor 0.4900 0.050 1 0 49 70 130 0.57 15.1 25 M Jddn 0.3400 0.050 1 0 34 70 130 0.39 13.7 25 M .4--ODT 0.3500 0.050 1 0 35 70 130 0.38 8.22 25 M Sum Decachiorobiphenyi BDL 0 1 0 0 26 172 0 0 0 s Sum Tetrachloro-m-xylene 0.5900 0 1 0 59 45 129 0 0 0

Page 7 of 8

lelmont Labs Date: 02-Aug-07

LIENT: ork Order:

roject:

Hull and Associates, Inc. 0707C29 COT192

ANALYTICAL QC SUMMARY REPORT TestCotle: PEST 8081 W

imple ID: MB-14729 SampType: MBLK TestCode: PEST_8Q8 1_ Units: pg/L Prep Date: 7/30/2007 RunNo: 602B9

llent ID: ZZZZZ Batch ID: 14729 TestNo: sweoaiA (SW3S10C} Analysis Date; 7/31/2007 SeqNo: 754950

jiatyte Result PQL SPK value SPK RafVal %REC LowUmIt HIghUmIt RPDRefVal *RPD RPDUmIt Qual

sptachlor BDL 0.050

drin BDL 0.050

4--ODT BDL 0.050 Sum Decachloroblphenyl 0.9100 0 1 0 01 28 172 0 0 Sum Tetrachloro-m-xylene 0.6800 0 1 0 68 45 129 0 0

ample ID: LCS-14729 SampType: LCS TestCode: PEST_8081_ Units: MQA. Prep Date: 7/30^007 RunNo: 60289

.tent ID: ZZZZZ Batch 10: 14729 TestNo: SW808i A (SW3S10C) Analysis Date: 7/31/2007 SeqNo; '754951

'jialyte Result PQL SPK value SPKRefVal %REC LowUmit HlghUmlt RPDRefVal %RPD RPDUmIt Qual

'eptachlor 0.7700 0.050 1 0 77 71 117 0 0

drin 0.6100 0.050 1 0 61 81 107 0 0 4*-0DT 0.8100 0.050 1 0 81 41 132 0 0 Sum Decachloroblphenyl 0.8300 0 1 0 83 28 172 0 0 Sum Tetrachloro-m-xylene 0.6700 0 1 0 67 45 129 0 0

imple ID: LCSO-14729 SampType; LCSD TestCode: PEST_808 1_ Units: pg/L Prep Date: 7/30/2007 Runfto: 60289

lent ID: ZZZZZ Batch ID: 14729 TestNo: SWB061A (SW3910C) Analysis Date: 7/31/2007 SeqNo; 754882

uiatyte Result PQL SPK value SPKRefVal %REC LowUmIt HlghUmlt RPDRefVal %RPD RPDUmIt Qual

leptachlor 0.7500 0.050 1 0 73 71 117 0.77 2.83 17 drin 0.6600 0.050 1 0 66 81 107 0.01 7.87 12

4-DDT 0.8600 0.050 1 0 86 41 132 0.81 5.99 19 Sum Decachloroblphenyl 0.8700 0 1 0 87 28 172 0 0 0 Sum Tetrachloro-m-xylene 0.7600 0 1 0 76 45 129 0 0 0

imple ID: 0707C29r001BMS SampType: MS TestCode: PEST_8081_ Units: pgA. Prep Date: 7/30^007 RunNo: 80289

lent ID: COT192:MW19:G07 Batch ID: 14729 TestNo: SW8081A (SW3510C) Analysis Date: 7/30/2007 SeqNo: 754938

uiaiyte Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmlt RPDRefVal %RPD RPDLImit Qual

Page 6 of 8

HyJJ CHAIN OF CUSTODY RECORD :lates, inc.

oforc PAGE J OF^

NO. 015772 • Dublin. OH OlndlaMaalla. IN nM—on. OH aaalnn. QH .lifTolada. QH

«3Sr EmmW Pvkwy UUE.7«hSL 4BOOPvkmyOr. 6161 Cochnn Road >3401 OtandaliAM. Sum 200 3uR«17e SUM 100 SuMO SultaSOO Dublin, OH 43010 IndJmpetla. IN 40280 Mam. OH 40040 Sokm. OH 44130 1bMo. OH 43014 Phm: (014) 7034777 Ptuoa: (317) KS04S50 Phona: (013) 400-0077 Ptm: (440)818-2800 Phona; (410)305-2010 FiK (014) 7034070 FaK (317) 5554053 "

REPQRTTO; fccFen

c (513)4054000 i: (440) 015-2000 FaK (410) 31

n)rn<nT/1 y y / ANALYSES

/A/A/n/ / / / / /

Client -if

SIIB: T-''"'

Pniiact#: , Phaea: OU, Tsr

- Lerc l-i,. t a-HCL^

PROJECT SAMPLE SAMPLE NO LOCATION TYPES ID

Naop CONT.

METALS COLLECTION / OATEmME / / X y^v/ / / / COMMENTS

r JT|P|-L. = Moo 1 °l 3 7-2P SI-)

1 1 t

COTI'^X. ' Ml-<|1 fwR 3 IJ 1 1 1

c<-r;qx ' OS 7 H 7. 1 I 1

•. fos J lO ?• 41 . / 1 1

Cc^nt-Hon •.•S'A 3 hJ / 1 1 C-^r / «i 1. = M-J1-3 6U-7ZVO-7 ! S'o") 3 H 1 t 1 CuT/'iT. •AAWI.S' '.SaT? 3 N

? jw-'n 1 1 (

=ALJ"t"5- 1 s-'i 3 1 1 1

C-r, IT. =/ULJi.=| CaTu-lol :SMS 3 N" >*.Y—> I 1 /

c-^nS-L = /'.oTiWo-T • C-<5 •>> H / 1 1

C-r|C|Y. : fi-oryt.-? ; r.-S 3 p / / OT r-T 3 t> ZT -7^ 1 1 /

REUNQUISHEDBV^

RELiNQUtSHSD BV)

TMB;

COOLER TEMPERATURE AS RECEIVED: 3 ((C

Kjti RECEIVEOan

GATE 7/, y/.

- 'W

D•^êrTo:

Method of DallvBfy:

Atrbill Numbw:

NOTES:

TURN AROUND TIME: sT S> DAYS

Data Quallflers (Flogs)

D Anaiyte detected in the auoeioted Method Blonk

DDL Below Detection limit

C Sample result conHmied by reanalysii

E Value above quantitation range

P Unable to obtain a reliable reiult due to matrix interference

H Aiulyaii completed outiide holding limea

J Anaiyte detected below quantitation limito, eatimated concentration fbr TICi

fC Reiult fhim method of itondard addltiona

L Laboratory control sample recovery ouUide acceptance IlmiU

M Matrix spike and/or matrix spike duplicate recovery outiide acceptance limtti

N Presumptive evidence of anaiyte present

P Sample preservation does not meet method requiremenia

R RPD outaide accepted recovery limits

S Surrogate recoveo' outaide acceptance limits V Calibration criteria exceeded, but acceptable by method

NO No growth

t See Case Narrative

Page 8 of 8

dlsSwdates. inc

Proiect/Faciiitv: Tvler Street Landfill Sample Date:

Address: Citv of Toledo. DSW. 3962 Hoffman RdToledo. OH. 43611

Contact David Leffler Teleohone: (419)936-2643 Reoort to: Karen Okonta

Billlna Address/PO ft

SamoioIvDe; GROUNDWATER [7| Grab 1 1 Composite

PARAMETERS TO ANALYZED

GENERAL AND INORGANICS: ADDmONAL:

0 PCBa • 0 PAIte • 0 haplactilor • 0 Bidrin • 0 DDT • 0 Mercury, total •

•

HELD MEASURED PARAMETEBS

b Samples to be Analyzed by Laboratory Turbidty pH Dissolved Oxygen Conductivity Temperature Radon Pounlial

Notes Monitoring WeT Sample ID * m^ S.U. mgA umhos/on deg-C mv

Notes

MW-19 / CoinAr. s /tio 0.0s 7V/0 /3.I -"ZuS" ( MW-21 'TJ 3W t-VS" rt. 3-1 3jj. /31 -/s-v V

MW-23 1" acfi 6.ô a /o 6/30 /?.? -lie MW-25 1 Ool. rfaso yW<« -ni MW-27 e-05 l" 1 ^ J 4, (.'I O-OV 7tlO -n-j MW-29 CJ.V51- ' ! ill 6.*X o.=3 Hl<*> /yy ~2c.g

MW-31 t Z5- tw/ 0.-9 ( '4^ MW-33 ^ -2. isr 0.2<7 S9»> 2 1.1. MW-3S -s ? fe.S(. O-o"^ /•s- >

r 0 ^

DuoGcate ^ lO" 6.7} £xo<; Ti/'^ /3' -T-A' ^ • MSA4S0 <

i i«.j I

7V»»7 T-IN' 'A*. -.V.f

Field Blank C-'iS I". fS/ >• -

• Ship UPS • COant Pick-up • Site DeOveiy/Plch-up 0 Our Sampling

Samola ContaJnafs Provided By: Belmont AnaMicaJ LAboralories

Submitted bv: Received bv:

iPLEna MC:509

-SSiSL ^35~D1

vy Q

0 •s. 1 o ct

t

3 I

'^1

I i

i I

I I

1 I 3 1 S I

Belmont ̂ Labs' The Environmental Service Company.

Tuesday, January 08,2008

Karen Okonta Hull and Associates, Inc. 3401 Glendale Avenue

Toledo, OH 43614

TEL; (800)241-7173 FAX (419)385-5487

RE: COT192 Stickiiey Avenue Landfill

Dear Karen Okonta:

Order No.: 0707C90


Belmont Labs attests that all analytical methods were performed using acceptable methods, and that the QA/QC procedures stipulated in these methods were followed. USEPA's RCRA Program regards a statement of quality assurance as a legal means of assuring that acceptable and uniform laboratory methods and QA/QC practices were followed by the laboratory.

If you have any questions regarding the test results, please feel free to call me at 937.832.8242.


Holly Oreen

Project Manager

QC LEVEL: LEVEL II

cc: Copy of invoice with report.

25 Hdidey Drive Englewood. Ohio 45322 1.937 632 6242 I .937-632-2866 Fax

Belmont Labs Date: OS-Jan-OS

CLIENT: Hull and Associates, Inc. Project: COT 192 Stickncy Avenue Landfill Lab Order: 0707C90

CASE NARRATIVE

Analytical Comments for METHOD VOC_8260_W, SAMPLE LCSD; RPD was high, but the spike recoveries were acceptable.

Analytical Comments for METHOD VOC_8260_W, SAMPLE 0707C90-011 A: Surrogate recovery was high, but the sampe is BDL.

/Vnalytical Comments for METHOD SVOC_8270_S, S/kMPLE LCSD-14780: RPD out but all recoveries are acceptable.

Analytical Comments for METHOD SVOC_8270_W, SAMPLE 0707C90-008C: Surrogate out due to matrix interference.

Analytical Comments for METHOD SVOC_8270_W, SAMPLE 0707C90-009C: Surrogates out due to matrix interference.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C90-001 A: Surrogate recovery for DCB is out due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C90-009A: Surrogate recovery for DCB is out due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0707C90-003/kMSD: Surrogate recovery for DCB is out due to matrix interference, but the recovery for TCMX is acceptable.



Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C90-001B: Sample diluted due to matrix. Surrogates out in lOx nm due to matrix interference. Surrogate recovery for DCB is out due to matrix interference, but the recovery for TCMX is acceptable.

Analytical Comments for METHOD PEST 8081_W, SAMPLE 0707C90-002B: Sample diluted due to matrix. Surrogates out in lOx nm due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0707C90-004B: Surrogate recovery for DCB is out due to matrix interference, but the recovery for TCMX is acceptable.

Page 1 of2

CLIENT: Hull and Associaies, Inc. Project: COT 192 Sticlciicy Avenue Landfill Lab Order: 0707C90

CASE NARRATIVE



Page 2 of 2

Belmont Labs Date: OS-Jaa-08

CLIENT: Project:

Hull and Associates, Inc. COT192 Stickney Avenue Landfill

Lab Order: 0707C90

Lab ID: 0707C90-001

Client Sample ID: COT192:MW21;G072507:509

CoUecdoo Date: 7/25/2007 6:50:00 AM

Matrix: GROUNDWATER

Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER SW8082 Analyst: DG Arodor1016 BDL 0.20 pan. 1 8/7/2007 9:15:00 AM

Arodorl221 BDL 0.20 pg/L 1 8/7/2007 9:15:00 AM

Arodor1232 BDL 0.20 PQA 1 8/7/2007 9:15:00 AM

Anxlor1242 BDL 0.20 PQA 1 8/7/2007 9:15:00 AM

Arodor1248 BDL 0.20 pan. 1 8/7/2007 9:15:00 AM

Arodor1254 BDL 0.20 pan. 1 8/7/2007 9:15:00 AM

Arodor1260 BDL 0.20 MOA 1 8/7/2007 9:15:00 AM

24.0 35-143 S %REC 1 8/7/2007 9:15:00 AM

Surr TetrachlorDHn-xylene 64.0 37-116 %REC 1 6/7/2007 9:15:00 AM

ORGANOCHLORINE PESTICIDES SWB081A Analyst DG Heptachlor BDL 0.050 pan. 1 6/7/2007 9:15:00 AM

Aldrin BDL 0.050 pan. 1 8/7/2007 9:15:00 AM

4.4-ODT BDL 0.50 PQA 10 8/8/2007 5:32:00 PM

Surr Decachlorobiphenyl 24.0 28-172 S %REC 1 6/7/2007 9:15:00 AM

Surr Decachlorobiphenyl 0 28-172 S %REC ID 8/8/2007 5:32:00 PM

Sum Tetrach(oro-m-xylene 64.0 45-129 %REC 1 8/7/2007 9:15:00 AM

Surr: Tetrachloro-m-xy(ene 0 45-129 S %REC 10 8/8/2007 5:32:00 PM

MERCURY, TOTAL SW7470A Analyst- RJE Mercury BDL 0.00020 mg/L 1 8/1/2007 7:53:00 AM

PAH BY EPA B270C SW8270C Analyst DG Naphthalene 8.2 10 J pan. 1 8/4/2007 8:19:00 AM

Acenaphlhene 0.20 10 J pan. 1 a/4«007 8:19:00 AM

Pyrene BDL 10 fO/L 1 8/4/2007 8:19:00 AM

Benz(a)anthracene BDL 0.26 pg/L 1 8/4/2007 8:19:00 AM

Chrysene BDL 10 pgA 1 8/4/2007 8:19:00 AM

Benzo(b)Ruoranlhen6 0.12 0.17 J pan. 1 8/4/2007 8:19:00 AM

BenzoOc)fluoranlhene BDL 1.7 pan. 1 8/4/2007 8:19:00 AM

Benzo(a)pyrene BDL 0.20 pan. 1 8/4«007 8:19:00 AM

Indenod .2.3-cd)pyrene 0.99 0.22 pg/L 1 8/4/2007 8:19:00 AM

Dibenz(a,h)anthracene 0.64 0.20 pan. 1 8/4r200/ 8:19:00 AM

Sum Nitrobenzene-dS 38.2 2(W3 %REC 1 8/4/2007 8:19:00 AM

Sum 2-Fluorobiphenyl 37.4 19-58 %REC 1 8/4/2007 8:19i)0AM

Sum p-Terphenyl-d14 27.t 10^ %R£C 1 8/4/2007 8:19:00 AM

Page 1 of 15

Belitont Labs Date: 08-Jan-08 Belmont Labs Date: 08-Jan-08

CLIENT: Project:

Hull and Associates, Inc. COT192 Stickncy Avenue LandfiU

Lab Order: 0707C90

Lab ID: 0707C90-002

Client Sample ID: COT192:MW24:G072507:509

Analyses Result

CoUection Date: 7/2S/2007 7:25:00 AM

Malrii: GROUNDWATER

PQL Qual Units DF Date Analyzed

RGBS IN WATER Afoclor 1016

AfOClor1221

Arodor 1232

Afodor 1242

Arodor 1248

Arodor 1254

Arodor 1260 Surr DecacMcrobiphenyl

Sum Tetrachioro^-xylene

ORGANOCHLORINE PESTICIDES Heptachlcr

Aldrin

4.4-DDT

Sum Decachlorobiphenyl


Sum Telrachloro-m-xyiene

Sum Tetrachioro-m-xyiene

MERCURY, TOTAL

BOL

BDL

BDL

BDL

BDL

BDL

BDL

54.0 89.0

BDL

BDL

BDL

54.0

0

89.0 0

SW8082 0.20

0.20

020

020

0.20

0.20

020 35-143 37-116

SW8081A 0.050

0.050

0.50

28-172

28-172

45-129

45-120

SW7470A

pgA

MSA MflA MO/L MBfl-

MO/L ygfl-

%REC

%REC

pgA.

pg/L

POO. %REC

%REC

%REC

%REC

Mercury BDL 0.00020 mg/L 1 a/1/2007 7:55:00 AM Mercury

RAH BY ERA 8270C SW8270C Analyst DG PAH BY EPAa270C Naphthalene BDL 10 P0A 1 8/3/2007 9:51:00 AM Naphthalene

Acenaphlhene BDL 10 MQA 1 8/3/2007 9:51:00 AM

Pyrene BDL 10 pgA 1 8/3/2007 9:51:00 AM Pyrene

Benz(a)anthr3cene BDL 02& MOA 1 8/3/2007 9:51.00 AM Benz(a)anthracene Chrysene BDL 10 PflA 1 8/3/2007 9:51:00 AM Chrysene

Berxzo(b}fiuoranthene BOL 0.17 pg/L 1 8/3/2007 9:51:00 AM Benzo(b)fluoranthene Benzo(k )fluoranthene BDL 1.7 P9A 1 8^2007 9:51:00 AM Benzo(a)pyrene BDL 0.20 MOA 1 80C007 9:51:00 AM Benzo(a)pyrene Indenoi 1.2.3-cd)pyrene BDL 0.22 pgA 1 8^/2007 9:51:00 AM Indenol 1.2.3-cd}pyrene Dibenz(a.h)anthracene BDL 0.20 pgA 1 8/3/2007 9:51:00 AM Dibenz(a,h)anlhracene

Sum Nitrobenzene-dS 38.4 2(«3 %REC 1 8/3/2007 9:51:00 AM Sum. Nltrobenzene-d5 Surr: 2-ftuorobiphenyl 37.4 19-58 %REC 1 8/3/2007 9:51:00 AM Sum 2-F1uoroblphenyl

Sum p-Tefphenyl-d14 36.0 1&B2 %REC 1 8/3/2007 9:51:00 AM Sum p-Terphenyl-dl4

Analyst: DG 8/7/2007 9:48:00 AM 8/7/2007 9:48:00 AM

8/7/2007 9:48:00 AM

8/7/2007 9:48:00 AM 8/7/2007 9:48:00 AM a/7/2007 9:48:00 AM

8/7/2007 9:48:00 AM

8/7/2007 9:48:00 AM 8/7/2007 9:48:00 AM

AnatysL- DG

8/7/2007 9:48:00 AM

8/7/2007 9:48:00 AM

8/8/2007 6:05:00 PM

8/7/2007 9:48:00 AM

8/8/2007 6:05:00 PM

8/7/2007 9:48:00 AM 8/8/2007 6:05:00 PM

Analyst: RJE

CLIENT: Project:

Hull and Associates, Inc. COT192 Stickncy Avenue LandfUl

Lab Order: 0707C90

Lab ID: 0707C90-003


Analyses Result



RGBS IN WATER /Uodor 1016

Arodor 1221

Arodor 1232

Arodor 1242

Arodor 1248

Arodor 1254

Arodor 1260

Sum Decachtorobiphenyl

Sum Tetrachloro-tn-xylene

ORGANOCHLORINE PESTICIDES Heptachior

AJdrin

4.4-ODT

Sum. Decachlorobiphenyl


Sum Tetrachloro-m-xytene

Sum Tetradikxo-m-xytene

MERCURY, TOTAL

SW8082 Analyst: DG BDL 0.20 POA 1 8/7/2007 4:25:00 PM BDL 0.20 MOA 1 B/7/2007 4:25:00 PM

BDL 0.20 pgA 1 8/7/2007 4:25:00 PM

BDL 0.20 pgA 1 znnodj 4:25:00 PM

BDL 0.20 PSA 1 8/7/2007 4:25:00 PM

BDL 0.20 PBA 1 8/7/2007 4:25:00 PM

BDL 0.20 PSA 1 8/7/2007 4:25:00 PM

45.0 35-143 %REC 1 an'/2007 4:25:00 PM

67.0 37-116 %REC 1 a/7/2007 4:25:00 PM

SW8081A Analyst DG BDL 0.050 PSA 1 a/7/2007 4J!5:00 PM

BDL 0.050 pgA 1 8/7/2007 4:25:00 PM

BDL 0.050 pgA 1 8/8/2007 9:20:00 PM

45.0 28-172 %REC 1 8/7/2007 4:25:00 PM

32.0 28-172 %REC 1 a/8«007 9:20:00 PM

67.0 45-129 %REC 1 8/7/2007 425:00 PM

69.0 45-129 %REC 1 8/8/2007 920:00 PM

SW7470A Analyst RJE BDL 0.00020 mg/L 1 8/1/2007 7:58:00 AM

SW8270C Analyst DG BDL 10 pgA 1 8/3/2007 10:35:00/Uiit

BDL 10 pgA 1 8/3^007 10:35:00 AM

BDL 10 P9A 1 8/3/2007 10:35:00 AM

BDL 0.26 pgA 1 8/3C007 10:35:00 AM

BDL 10 pgA 1 8/3/2007 10:35:00 AM

BDL 0.17 pgA 1 6/3/2007 10:35:00 AM

BDL 1.7 pgA 1 8/3/2007 10:35:00 AM

BDL 0.20 pgA 1 6/3«007 10:35:00 AM

BDL 0.22 pgA 1 8ra«007 10.35:00 AM

BDL 0.20 pgA 1 8/3/2007 10:35:00 AM 40.6 2&«3 %REC 1 8/3/2007 10:35:00 AM

37.7 1^ %REC 1 8/3/2007 10.35:00 AM

38.1 10^2 %REC 1 8/3/2007 10:35:00 AM

Page 2 of 15 Pagc3ofl5

Belmont Labs Date: 08-Jan-0a

CLIENT: Project:

Hull and Associates, Inc. COT192 Sdckncy Avenue Landfill

Lab Order: 0707C90

Lab ID: 0707C90-004

Client Sample ID: COT192;MW27:G072507A:509 CoUection Date: 7/25/2007 7:54:00 AM

Matrix: GROUNDWATER

Belmont Labs Date: 08-Jan-08

CLIENT: Project:

Hull and Associates, Inc. COT 192 Stickney Avenue Landfill

Lab Order: 0707C90

Lab ID: 0707C90-005 Client Sample ID: COT192:MW30:G072507:509


Analyses Result PQL Qual Units DF Date Analyzed Analyses Result PQL Qua! UniU DF Date Analyzed

PCBS IN WATER SW8082 Analyst: DG PCBS IN WATER SW8082 Analyst DG AfodorlOie BDL 020 1 B/7/2007 7:10:00 PM Arodor 1016 BDL 0.20 POrt- 1 8/7/2007 9:23:00 PM

Arodor1221 BDL 020 PO/L 1 8/7/2007 7:10.00 PM Arodor1221 BDL 0.20 P8/t 1 znnmi 9:23:00 PM

Arodor 1232 BDL 020 pgA. 1 8/7/2007 7:10:00 PM Arodor 1232 BDL 0.20 pgfl. 1 8/7/2007 9:23:00 PM

Arodor 1242 BDL 020 POA 1 8/7/2007 7:10:00 PM Arodor 1242 BDL 0.20 pg/L 1 8/7/2007 9:23:00 PM

Arodor 1243 BDL 020 pgA 1 8/7/2007 7:10:00 PM Arodor 1248 BDL 0.20 PO/L 1 8/7/2007 9:23:00 PM

Arodor 1254 BDL 020 pg/L 1 8/7/2007 7:10:00 PM Arodor 1254 BDL 0.20 pg/L 1 8/7/2007 9:23:00 PM

Arodor 1260 BDL 0.20 POA 1 8/7/2007 7:10:00 PM Arodor 1260 BDL 0.20 M98- 1 a/7/2007 9:23:00 PM

Surr Oecachlorobiphenyl 39.0 35-143 %REC 1 8/7/2007 7:10:00 PM Sum Decachloroblphenyl 55.0 35-143 %REC 1 a/7/2007 9:23:00 PM

Surr Tetrachloro-m-xylene 60.0 37-116 %REC 1 8/7/2007 7:10:00 PM Sum Tetrachloro-m-xyler)e 87.0 37-116 %REC 1 8/7/2007 9:23:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG ORGANOCHLORINE PESTICIDES SWS081A Analyst DG Heptadilor BDL 0.050 PBA. 1 a/7/2007 7:10:00 PM Heptachlor BDL 0.050 PBA 1 8/7/2007 9:23:00 PM Aldrin BDL 0.050 pg/L 1 a/7/2007 7:10:00 PM Aldrin BDL 0.050 P0A 1 8/7/2007 9:23:00 PM

4.4'-DDT BDL 0.050 MQA 1 a/aa007 10:57:00 PM 4.4-ODT BDL 0.050 pgA 1 8/8/2007 11:30:00 PM Sum Decachlorabiphenyl 39.0 28-172 %REC 1 8/7/2007 7:10:00 PM Sum. Decachloroblphenyl 55.0 28-172 %REC 1 8/7/2007 9:23:00 PM

Surr. Oecachlorobiphenyl 25.0 28-172 S %REC 1 8/8/2007 10:57:00 PM 40.0 28-172 *REC 1 a/a«007 11:30:00 PM Sum Tetrachloro-m-xylene 60.0 45-129 %REC 1 8/7/2007 7:10:00 PM Sum Tetrachloro-m-xylene 67.0 46-129 %REC 1 8/7/2007 9:23.00 PM

Surr: Tetrachloro-m-xylene 66.0 45-129 %REC 1 8/8/2007 10:57:00 PM Sum Tetrachloro-m-xylene 72.0 45-129 %REC 1 8/8«007 11:30:00 PM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY, TOTAL SW7470A Analyst: RJE Mercury BDL 0.UUU2U mg/L 1 a/1/2007 8:04:00 AM Mercury BDL 0.00020 mg/L 1 8/1/2007 6:06:00/kM

PAH BY EPA 827DC SW8270C Analyst: DG PAH BY EPA 8270C SWB270C Analyst: DG BDL 10 PBA 1 8/3/2007 12:46:00 PM Naphthalene 0.45 10 J P0A 1 6/3/20071:29:00 AM

Acenaphlhene BDL 10 P08. 1 8/3/2007 12:46:00 PM /Kcenaphthene 5.0 10 J P9A 1 8/3/2007 1:29:00 AM Pyrene BDL 10 pgA 1 8««00712:46:00 PM Pyrene BDL 10 pg/L 1 8/3/20071:29:00 AM Benz(a)anthracene BDL 0.26 MQA. 1 8/3/2007 12:46:00 PM BDL 0.26 POA 1 8/3/2007 1:29:00 AM Chrysene BDL 10 pgA 1 aW2007 12:46:00 PM Chrysene BDL 10 pgA 1 6/3/2007 1-.29:00 AM Benzo{b)fluoranthene 0.14 0.17 J POA 1 ara/2007 12:46:00 PM Benzo(b}fluoranthene BDL 0.17 pgA 1 8««007 1:29:00 AM BenzD{k)fluoranthene BDL 1.7 POA 1 ara«007 12:46:00 PM Benzo(k)iluoranthene BDL 1.7 pgA 1 8/3/2007 1:29:00 AM Benzo(a)pyrene BDL 0.20 pgA 1 8/3/2007 12:46:00 PM Ben20(a)pyrene BDL 0.20 POA 1 aW20071:29:00 AM lndeno(1,2.S-cd)pyrene 1.1 022 P98- 1 8/3/2007 12:46:00 PM Indenot 1.2.3-cd)pyrene 0.62 0.22 PflA 1 8/3/2007 1:29:00 AM Dibenz(a.h)anthracene 0.91 020 pg/L 1 8/3/2007 12:46:00 PM Dibenz(a.h)anlhracene 0.84 0.20 pgA 1 • a/3«007 1:29:00 AM

Sum Nitrabenzene-dS 34.3 2003 %REC 1 8/3/2007 12:46:00 PM Sum Nitrobenzene-d5 38.6 2063 %REC 1 8/3/2007 1:29:00 AM Sum. 2-Ruorobiphenyl 33.4 19-58 %REC 1 8f3«0a7 12:46:00 PM 38.0 1068 %REC 1 8«C007 1:29:00 AM Sum. p-Terphenyl-d14 30.3 1002 %REC 1 8/3/2007 12:46:00 PM Sum p-Terphenyl-d14 28.8 1062 %REC 1 8/3/2007 1:29:00 AM



Lab ID: 0707C90-006

Client Sample ID: COTI92:MW33:G072507:509

Collection Date: 7/25/2007 9:43:00 AM

Matrix: GROUNDWATER


CLIENT: Hull and Associates, Inc. Lab Order: 0707C90 CLIENT: Hull and Associates, Inc. Lab Order: 0707C90 Project; COT 192 Stickney Avenue Landfill Project: COT192 Stickney Avenue Landfill

Lab ID: 0707090-007

CUcnt Sample ID: COTI92:MW35:G072507:509

CoUectioD Date: 7/25/2007 10:10:00 AM

Matrix: GROUNDWATER

Analyses Result PQL Qual UniU DP Date Analyzed Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER SW80&2 Anatysl: DG PCBS IN WATER swa082 Analyst: DG Arodor 1016 BDL 0.20 POA 1 8/7/2007 8:50:00 PM Arodor 1016 BDL 0.20 Pflrt. 1 8/7/2007 9:56:00 PM

Atoclof 1221 BDL 0.20 POA 1 8/7/2007 8:50:00 PM Arodor 1221 BDL 0.20 P04. 1 8/7/2007 9:56:00 PM

Arodor 1232 BDL 0.20 POA 1 8/7/2007 8:50:00 PM /Vrodor1232 BDL 0.20 pgrt- 1 8/7/2007 9:56:00 PM

Arodor 1242 BDL 0.20 POA 1 8/7/2007 8:50:00 PM Arodor 1242 BDL 0.20 P0fl- 1 8/7/2007 9:56:00 PM

Arodor 1248 BDL 0.20 pgA 1 8/7/2007 8:50:00 PM Arodor 1248 BDL 0.20 POA. 1 8/7/2007 9:56:00 PM

Arodor 1254 BDL 0.20 POA 1 8/7/2007 8:50:00 PM Arodor 1254 BDL 0.20 PBA- 1 8/7/2007 9:56:00 PM

Arodor 1260 BDL 0.20 POA 1 8/7/2007 8:50:00 PM Arodor 1260 BDL 0.20 PO/L 1 8/7/2007 9:56:00 PM

SUIT Decachlorobiphenyl 36.0 36-143 %REC 1 8/7/2007 8:50:00 PM Sum Decadilorobiphenyj 27.0 35-143 S %REC 1 6/7/2007 9:56:00 PM

Sum Telradiloro-m-xylene 63.0 37-116 %REC 1 8/7/2007 8:50:00 PM Sum Tetrachloro-fn-xytene 64.0 37-116 %REC 1 8/7/2007 9:56:00 PM

ORGANOCHLORINE PESDCIDES SW8081A Analyst: DG ORGANOCHLORINE PESTICIDES SW8081A Analyst: DG Heptachlor BDL 0.050 pgA 1 8/7/2007 8:50:00 PM Hepiachlor BDL 0.050 PO'L 1 8/7/2007 9:56:00 PM

Aldrin BDL 0.050 POA 1 8/7/2007 8:50:00 PM Aldrin BDL 0.050 P9A- 1 8/7/2007 9:56:00 PM

4.4-DDT BDL 0.050 P9A 1 8/9/2007 12:02:00 AM 4.4'-ODT BDL 0.050 pg/L 1 8/9/2007 12:35:00 AM

36.0 26-172 %REC 1 8/7/2007 8:50:00 PM Sum Decachlorobiphenyl 27.0 28-172 S *REC 1 8/7/2007 9:56:00 PM

Sum Decachlorobiphenyl 24.0 28-172 S %REC 1 8/9/200712:02:00 AM Sum Decadiloroblphenyl 18.0 28-172 S %REC 1 8«/2007 12:35:00 AM

Sum Tetrachloro-m-xyiene 63.0 45-129 %REC 1 8/7/2007 8:50:00 PM Sum Tetrachiofo-m-xylene 64.0 45-129 *REC 1 8/7/2007 9:56:00 PM

49.0 45-129 %REC 1 8W2007 12:02:00 AM Sum Tetrachloro-m-xyiene 70.0 45-129 *REC 1 a«/2007 12:35:00 AM

MERCURY, TOTAL SW7470A Analyst RJE MERCURY, TOTAL SW7470A Analyst RJE Mercury BDL 0.00020 mg/L 1 8/1/2007 8:08:00 AM Mercury BDL 0.UUU2U mg/L 1 8/1/2007 8:10:00 AM

PAH BY EPA 8270C SW8270C Analyst DG PAH BY EPA 8270C SW6270C Analyst DG Naphthalene 6.1 10 J POA 1 8/3/2007 2:13:00 AM Naphthalene 0.14 10 J MQA- 1 8^2007 2:57:00 AM Acenaphthene 1.3 10 J POA 1 ara«007 2:13:00 AM Acenaphthene 1.9 10 J PQA. 1 8«C007 2:57:00 AM Pyrene 0.17 10 J POA 1 8/3/2007 2:13:00 AM Pyrene 0.30 10 J POA. 1 6/3/2007 2:57:00 AM

Benz(a)3nthracene BDL 0.26 P0A 1 8/3/2007 2:13:00 AM Benz(a)anthracene BDL 026 pgA. 1 8/3/2007 2:57:00 AM Chrysene BDL 10 POA 1 8/3/2007 2:13:00 AM Chrysene BDL 10 pgA. 1 8/3^007 2:57:00 AM Benzo(b)fluoranlhene BDL 0.17 POA 1 8^2007 2:13:00 AM Benzo(b)fluoranlhene BDL 0.17 pgA. 1 a««007 2:57:00 AM

BDL 1.7 PO/L 1 8/3/2007 2:13:00 AM BenzoOc |fluoranthene BDL 1.7 Pfl/L 1 8/3/2007 2:57:00 AM Benzo(a)pyrene BDL 0.20 MQA 1 8/3/2007 2:13:00 AM Benzo(a)pyrene BDL 0.20 POA. 1 6/3/2007 2:57:00 AM

lndeno{1,2.3-cd)pyrene 0.50 0.22 POA 1 8/3/2007 2:13:00 AM 0.78 0.22 PBA. 1 8/3/2007 2:57:00 AM Dibenz(a.h)anlhracene BDL 0.20 pg/L 1 8/3/2007 2:13:00 AM Oibenz(a,h)anlhracene BDL 0.20 P9A. 1 8/3^007 2:57:00 AM

Sum Nitrobenzene-dS 39.0 20-63 %REC 1 8/3/2007 2:13:00 AM Sum Nitrobenzene-dS 41.2 2(W3 %REC 1 aO/2007 2:57:00 AM Sum 2-F1uorobiphenyl 39.3 19-58 %REC 1 8W2007 2:13:00 AM Sum. 2-FUjorobipheny1 37.7 19-58 %REC 1 8/3/2007 2:57:00 AM Sum p-Terphenyt-d14 30.3 1062 %REC 1 8/3/2007 2:13:00 AM Sum. p-Terphenyl-d14 30.0 1082 %REC 1 8/3/2007 2:57:00 AM



CLIENT: Project:

Hull and Associates, Inc. COTI92 Stickney Avenue Landfill

Lab Order 0707C90

Lab ID: 0707C90-008


Analyses Result

CoUeetion Date: 7/2S/2007 10:48:00 AM Matrix: GROUNDWATER

PQL Qua] Units DF Date Analyzed

PCBS IN WATER SW8082 Arodor 1016 BOL 0.20 MO/L Arodor 1221 BDL 0.20 vt/l. Arodof 1232 SDL 0.20 (JQ/L

Arodor 1242 BDL 020 van. Arodor 1248 BDL 020 iign.

Arodor 1254 BDL 020 Iig/L

Arodor 1260 BDL 020 (lOfl-

Sum Decachlorobiphenyi 28.0 35-143 S %REC

Sum TetradUoro-m-xylene 65.0 37-116 *REC

SVOC TENTATIVELY IDENTIFIED COMPOUNDS Dimethylaniline BDL 10 IJflA

VOLATILE ORGANIC ANALYSIS SW8260B n-Hexane BDL 5.0 ligfl.

Oidiiorodinuoromethane BDL 5.0 Ijgn.

BDL 5.0 fB'L Vinyl chloride BDL 1.0 lign. Bromomethane BDL 5.0 (jgn.

Chloroelhane 59 50 lign. Acrolein BDL 20 kS"-Acetonibile BDL 40 MQ/L Trichlorofluoromethane BDL 5.0 iig/L

Acetone 58 20 linn. 1.1-Oichloroethene BDL 5.0 MBA. Acrylonilrile BDL 20 BBA-lodomethane BDL 10 pgA.

Methylene chloride BDL 5.0 MBA-BOL 20 MBA-

trans-1,2-Oichloroethene BOL 5.0 CflA-Methyl tert-butyl ether BDL 10 BB/L l.l-Dichloroe thane BDL 5.0 BBA. Vinyl acetate BDL 10 BBA-2-Butanone • BDL 20 MBA. ds-12-Dichlaroethene BDL 5.0 MBA. Bromochloromethane BDL 5.0 BBA-Chloroform BDL 5.0 BBA. 22'Oichloropropane BDL 5.0 MBA-1,2-Dichloroethane BOL 5.0 BBA. 1.1.1-Trichloroe thane BDL 5.0 BBA-1,1-Dichloropropene BDL 5.0 BBA-Carbon tetrachloride BOL 5.0 MBA-Benzerte 22 5.0 BBA. Dibromomelhane BDL 5.0 BBA.

Analyst DG 6^/2007 10:29:00 PM

8ff/2007 10:29:00 PM

8/7/2007 10:29:00 PM

a/7/2007 10:29:00 PM

8/7/2007 10:29:00 PM

8/7/2007 10:29:00 PM

8/7/2007 10:29:00 PM

8/7/2007 10:29:00 PM

8/7/2007 10:29:00 PM

Analyst DG

8/4/2007 9:03:00 AM

Analyst: HG 7/31/2007 5:44:00 PM 7/31/2007 5:44:00 PM 7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

8W2007 3:25:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM 7/31/2007 5:44:00 PM 7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM

7/31/2007 5:44:00 PM 7/31/2007 5:44.-00 PM

7/31/2007 5:44:00 PM

Page 8 of IS


CLIENT: Project:


Lab Order: 0707C90

I/OLATILE ORGANIC ANALYSIS SW8260B Analyst UG l.241ichlcnipnipane BDL 5.0 M9A 1 7/31/2007 5:44:00 PM

Trichloroethene BDL 5.0 MBA 1 7/31/2007 5:44:00 PM

Bromodichloromethane BDL 5.0 pflA 1 7/31/2007 5:44:00 PM

2-Chloroethyl vinyl ether BDL 10 M0A 1 7/31/2007 5:44:00 PM

ds-1.3-Dichloropropene BDL 5.0 pgA 1 7/31/2007 5:44:00 PM

4-Methyl-2-pentanone BDL 20 MQA 1 7/31/2007 5:44:00 PM

BDL 5.0 M9A 1 7/31/2007 5.44:00 PM

1.12-Trichioroethane BDL 5.0 MSA 1 7/31/2007 5:44:00 PM

Toluene 1.3 5.0 J MOA 1 7/31/2007 5:44:00 PM

1,3-DichIoropropane BOL 5.0 pgA 1 7/31/2007 5:44:00 PM

2-Hexanone BDL 20 pgA 1 7/31/2007 5:44:00 PM

Dibromochloromethane BDL 5.0 MOA 1 7/31/2007 5:44:00 PM

BDL 5.0 PflA 1 7/31/2007 5:44:00 PM

Tetrachloroethane BDL 5.0 MQA 1 7/31/2007 5:44:00 PM

1,1.12-Tetrachloroethane BDL 5.0 MBA 1 7/31/2007 5:44:00 PM

Chlorobenzene 82 5.0 pgA 1 7/31/2007 5:44:00 PM

BDL 5.0 PBA 1 7/31/2007 5:44:00 PM

m.p-Xylene 4.3 10 J PBA 1 7/31/2007 5:44:00 PM

Bromoform BOL 5.0 MBA 1 7/31/2007 5:44:00 PM Styrene BOL 5.0 MOA 1 7/31/2007 5:44:00 PM

1.1.2.2-Telrachloroelhane BDL 5.0 MBA 1 7/31/2007 5:44:00 PM

o-Xylene BOL 5.0 MBA 1 7/31/2007 5:44:00 PM

Bromobertzena BDL 5.0 MflA 1 7/31/2007 5:44:00 PM

2-Chlorototuene BDL 5.0 MOA 1 7/31/2007 5:44:00 PM

4-Chlorotduene BDL 5.0 pgA 1 7/31/2007 5:44:00 PM Sum Dibromofluoromethane 103 60-125 %REC 1 7/31/2007 5:44:00 PM

Sum Dibromofluoromethane 69.3 60-125 %REC 10 timoOl 3:25:00 PM

123 49-127 %REC 1 7/31/2007 5:44:00 PM

66.8 49-127 %REC 10 6/2/2007 3:25:00 PM

Sum. Totuene-d6 72.1 50-128 SREC 10 8««007 3:25:00 PM

Sum ToIuene-d8 104 50-128 %REC 1 7/31/20075:44:00 PM Sum. 4-BrDmoBuorobenzerte 77.2 48-110 %REC 10 8/2/2007 3:25:00 PM Sum 4-BromQfluorobenzene 106 48-110 %REC 1 7/31/2007 5:44:00 PM

Page 9 of 15


CLIENT: Project:

Hull and Associates, Inc. COT192 Stickncy Avenue Landfill

Lab Order: 0707C90

Lab ID: 0707C90-009


CoUection Date: 7/25/2007 11:41:00 AM

Matrii: GROUNDWATER

Analyses Result PQL Qua] Units DP Date Analyzed

RGBS IN WATER SWB082 Analyst: DG Arodof 1016 BOL 0.20 P08. 1 8/7/2007 10:55:00 AM

Arodof 1221 BDL 0.20 pgA 1 8/7/2007 10:55:00 AM

Arodof 1232 BOL 0.20 pgA. 1 a/7/2007 10:55:00 AM

Arodor 1242 47 0.20 Pfl/L 1 8/8/2007 1:14:00 AM

Arodor 1248 BDL 0.20 pgA 1 8/7/2007 10:55:00 AM

Arodof 1254 BDL 0.20 MOA 1 8/7/2007 10:55:00 AM

Arodor 1260 38 0.20 M9A 1 8/7/2007 10:55:00 AM

Surr OecachloFobiphenyl 18.0 35-143 S %REC 1 8/7/2007 10:55:00 AM

Surr Tetrachtoro-m-xylene 53.0 37-116 %REC 1 8/7/2007 10:55:00 AM

Surr: Telrachloro-m-xylene 0 37-118 S %REC 1 8/8/2007 1:14:00 AM

SVOC TENTATIVELY IDENTIFIED COMPOUNDS Analyst: DG Oimethytaniline BOL 10 PBA 1 8/3/2007 11:35:00 AM

VOLATILE ORGANIC ANALYSIS SWB260B Analyst MG n-Hexane BDL 250 liOA 50 8/1/2007 12:59:00 PM

BDL 250 POA 50 8/1/2007 12:59:00 PM

Chloromethar)e BDL 250 MOA 50 8/1/2007 12:59:00 PM

Vinyl diloride BOL 50 MOA 50 6/1/2007 12:59:00 PM

Bromomethane BDL 250 MBA 50 8/1/2007 12:59:00 PM

Chloroe thane BDL 250 POA 50 8/1/2007 12:59:00 PM

Acrolein BDL 1000 MQA 50 a/1/2007 12:59:00 PM

Acelonitrile BDL 2000 MQA 50 8/1/2007 12:59:00 PM

Trichiorofluoromethane BDL 250 POA 50 8/1/2007 12:59:00 PM

Acetone BDL 1000 P9A 50 8/1/2007 12:59:00 PM

1.1-Oichloroethene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Acrylonitrile BDL 1000 pgA 50 8/1/2007 12:59:00 PM

lodomethane BOL 500 pgA 50 8/1/2007 12:591)0 PM

Methylene chloride 100 250 J POA SO 8/1/2007 12:59:00 PM

Cartxm disulfide BDL 1000 pgA 50 8/1/2007 12:59:00 PM

lrans-1.2-Oichloroethene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Methyl tert-butyl ether BDL 500 pgA 50 8/1/2007 12:59:00 PM 1.1-Oichloroe thane 130 250 J pgA SO 8/1/2007 12:59:00 PM

Vinyl acetate BDL 500 pgA 50 8/1/2007 12:59:00 PM

2-Butanone BOL 1000 pgA 50 8/1/2007 12:59:00 PM

ds-1.2-Dichloroethene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Bromochloromethane BDL 250 pgA 50 8/1/2007 12:59:00 PM

Chloroform BDL 250 pgA 50 8/1/2007 12:59:00 PM

2,2-Oichloropropane BDL 250 pgA 50 8/1/2007 12:59:00 PM

1.2-0(chloroethane BDL 250 POA 50 8/1/2007 12:59:00 PM

1.1.1-Trichloroethane BDL 250 pgA 50 8/1/2007 12:59:00 PM

1.1 -Oichtoropropene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Carbon tetrachloride BDL 250 pgA 50 8/1/2007 12:59:00 PM

Benzene 140 250 J pg/L 50 8/1/2007 12:59:00 PM

Page 10 of IS

Belmont Labs Date: 08-Jan-0S

CUENT: Project:


Lab Order: 0707C90

VOLATILE ORGANIC ANALYSIS SWB260B Analyst MG Dibromomethane BDL 250 MOA 50 8/1/2007 12:59:00 PM

1,2-DichlorDpropana BDL 250 MOA 50 8/1/2007 12:59:00 PM

Trichloroethene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Bromodichlaromethane BDL 250 pgA 50 8/1/2007 12:59:00 PM

2-Chloroethyl vinyl ether BDL 500 pgA 50 8/1/2007 12:59:00 PM

ds-1,3-Dichioropropene BDL 250 pgA 50 8/1/2007 12:59:00 PM

4-Methyl-2-pentanone BDL 1000 pgA 50 8/1/2007 12:59:00 PM

lrans-1 .S-Oichloropropene BDL 250 pgA SO 8/1/2007 12:59:00 PM

1.1.2-Trichloroelhane BDL 250 pgA 50 8/1/2007 12:59:00 PM

Toluene 1200 250 pgA 50 6/1/2007 12:59:00 PM

1.3-OichloroprDpane BDL 250 pgA 50 8/1/2007 12:59:00 PM

2-Hexanone BDL 1000 MQA 50 8/1/2007 12:59:00 PM

Dibromochloromethane BOL 250 pgA 50 8/1/2007 12:59:00 PM

1.2-Oibromoethane BDL 250 M9A 50 8/1/2007 12:59:00 PM

Tetrachloroelhene BDL 250 pgA 50 8/1/2007 12:59:00 PM

BDL 250 pgA 50 8/1/2007 12:59:00 PM

Chlorobenzene BDL 250 ugA 50 8/1/2007 12:59:00 PM

Ethylbenzene 2100 250 MgA 50 8/1/2007 12:59:00 PM

m.p-Xylene 7600 500 pgA 50 8/1/2007 12:59:00 PM

Bromoform BDL 250 pgA 50 8/1/2007 12:59:00 PM Styrene BDL 250 pgA 50 8/1/2007 12:59:00 PM

1.1,2.2-Tetrachloroethane BDL 250 pgA 50 a/1/2007 12:59:00 PM o-Xytene 4500 250 pgA 50 8/1/2007 12:59:00 PM

Bromobenzerte BDL 250 pgA 50 8/1/2007 12:59:00 PM

2-Chlaratoluene BDL 250 pgA 50 8/1/2007 12:59:00 PM

4-Chlorotoluene BDL 250 pgA 50 8/1/2007 12:59:00 PM

Sum DlbromofluorDmethane 67.9 60-125 %REC 50 a/1/2007 12:59:00 PM

Surr 1.2-DichloFoethane-d4 69.4 49-127 %REC 50 8/1/2007 12:59:00 PM

Surr ToUiene-dS 70.5 50-128 *REC 50 8/1/2007 12:59:00 PM

Surr 4-BromofluorDbenzene 76.9 40-110 %RBC 50 8/1/2007 12:59:00 PM

Page 11 of IS

Belmont Labs Date: 08-Jan-0S

CLIENT: Project:

Hull and Associates, Inc. COT 192 Stickncy Avenue LandfiU

Lab Order: 0707C90

Lab ID: 0707C90-010 Client Sample ID: COT192:FB1;W072507;509

CoUection Date: 7/2S/2007 12:10:00 PM Matrix: GROUNDWATER

Analyses Result PQL Qual Units DF Date Analyzed

PCBS IN WATER swa082 Analyst DG AfOdor1016 BDL 020 UflA 1 877/2007 11:02:00 PM

Arodor 1221 BOL 020 MOfl- 1 B/7/20G711:02:00 PM

Arodor 1232 BDL 020 MOA 1 8/7/2007 11:02:00 PM

Arodor 1242 BDL 020 ugA 1 8/7/200711:02:00 PM

Arodor 1248 BDL 0.20 U9A 1 8/7/2007 11:02:00 PM

Arodor 1254 BDL 020 |J0A 1 8/7/2007 11:02:00 PM

Arodor 1260 BDL 0.20 pgA 1 8/7/200711:02:00 PM

Sum Oecadilorobiphenyl 61.0 35-143 %REC 1 a/7/2007 11:02:00 PM

Sum TetrachloroHn-xyleno 73.0 37-116 %REC 1 8/7/2007 11:02:00 PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heplachlor BDL 0.050 |iOA 1 8/7/2007 11:02:00 PM

Aldrin BDL 0.050 W»A 1 8/7/200711:02:00 PM

4.4'-DDT BDL 0.050 MOA 1 B/a/20071:07:00 AM

Sum Decachlorobiphenyl 61.0 28-172 %REC 1 8/7/200711:02:00 PM

Sum Decachlorobiphenyl 64.0 28-172 %REC 1 ara«007 1:07:00 AM

Sum Tetrachloro-m-xylene 73.0 45-129 %REC 1 B/7/200711:02:00 PM

Sum Tetrachloro-m-xylene 76.0 45-129 %REC 1 aW2007 1:07:00 AM

MERCURY. TOTAL SW7470A Analyst RJE Mercury BDL 0.00020 mg/L 1 8/1/2007 8:17:00 AM

PAH BY EPA 827DC SW8270C Analyst: DG Naphthalene BDL 10 MQA 1 8/3/2007 3:40:00 AM Acenaphthene BDL 10 POA 1 8««007 3:40:00 AM

Pyrene BDL 10 MOA 1 B/3/2007 3:40:00 AM

Benz(a)anlhracene BDL 0.26 MOA 1 8/3/2007 3:40:00 AM Chrysene BDL 10 MflA 1 8/3^007 3:40:00 AM

Benza(b)fluoranthene BDL 0.17 MQA 1 8/3/2007 3:40:00 AM

Benzo(k)nuoranthene BDL 1.7 MOA 1 8/3/2007 3:40:00 AM

Benzo(a)pyrene BDL 020 MBA 1 arara)07 3:40:00 AM Indenod .2,3-aJ)pyrene BDL 0.22 MOA 1 8/3/2007 3:40:00 AM

Diben2(a.h)anthracene BDL 020 pgA 1 a/3r20U/3:40.00 AM

Sum Nitrobenzene-dS 42.0 2063 %REC 1 arafi!007 3:40:00 AM

38.8 19-58 %REC 1 8/3/2007 3:40:00 AM

Sum p-Terphenyl-d14 40.6 1062 %REC 1 a/3/2007 3:40:00 AM

Page 12 of 15


CUENT: Project:

Hull and Associates, Inc. COT192 Stickncy Avenue Landfill

Lab Order: 0707C90

Lab ID: 0707C90-011 CUent Sample ID: COT192:TB1:W72507:509

Analyses Result

CoUection Date: Matrix: TRIP BLANK


n-Hexane BDL 5.0 MBA 1 7/31/2007 4:28:00 PM

BDL 5.0 P9A 1 7/31/2007 4:28:00 PM

Chlofomethane BDL 5.0 . M9A 1 7/31/2007 4:28:00 PM

Vinyl chloride BDL 1.0 MOA 1 7/31/2007 4:28:00 PM

Bromomethane BDL 5.0 PBA 1 7/31/2007 4:28:00 PM

Chloroethane BDL 5.0 pgA 1 7/31/2007 4:28:00 PM

Acrolein . BDL 20 PQA 1 7/31/2007 4-.28:00PM

Acetonitrile BDL 40 MO/t 1 7/31/2007 4:28:00 PM

BDL 5.0 M9A 1 7/31/2007 4:28:00 PM

Acetone BDL 20 MOA 1 7/31/2007 4:28:00 PM

1,1-Oichloroethene BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Acrylonitrile BDL 20 MOA 1 7/31/2007 4:28:00 PM

BDL 10 MOA 1 7/31/2007 4:28:00 PM

Methylene chloride BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Carbon disutfide BDL 20 MQA 1 7/31/2007 4:28:00 PM

trans-1,2-DichloroeUiene BDL 5.0 MQA 1 7/31/2007 4:28:00 PM

Methyl tert-butyl ether BDL 10 MOA 1 7/31/2007 4:28:00 PM

1.1-Oichloroethane BDL 5.0 MQ/L 1 7/31/2007 4:28:00 PM

Vinyl acetate BDL 10 MOA 1 7/31/2007 4:26:00 PM

2-Butanone BDL 20 MOA 1 7/31/2007 4:28:00 PM

ds-1,2-Dichloroethene BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Bromochloromethane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Chloroform BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

2.2-Oichloropropane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

1.2-Dichloroethane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM 1.1.1-Trichloroethane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

1.1-Dichloropropene BDL 5.0 MOA 1 7/31/2007 4:28:00 PM Carixxi tetrachloride BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Benzene BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

Dibromomethane BDL 5.0 MQA 1 7/31/2007 4:28:00 PM 1.2-Dichloropropane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Tridiloroethene BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

Bromodichloromethane BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

2-Chloroethyl vinyl ether BDL 10 MOA 1 7/31/2007 4:28:00 PM

ds-1.3-Dichloropropena BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

4-Methyl-2-pentanone BDL 20 MOA 1 7/31/2007 4:28:00 PM

trans-1,3-Oichlor(^)ropene BDL 5.0 MOA 1 7/31/2007 4:28:00 PM 1,1,2-TrichlorDethane BDL 5.0 MOA 1 7/31/2007 4:28:00 PM Toluene BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

BDL 5.0 MOA 1 7/31/2007 4:28:00 PM 2-Hexanon8 BDL 20 MOA 1 7/31/2007 4:28:00 PM Dtbromochloromelhane BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

BDL 5.0 MOA 1 7/31/2007 4:28:00 PM

Page 13ofl5

Belmont Labs Date: 08-Jan-OS Belmont Labs Date: 08-Jan-08

VOLATILf ORGANIC ANALYSIS SW8260B Analyst: MG Tetrachloroethene BDL 5.0 MO/L 1 7/31/2007 4:28:00 PM

1,1,1.2-Tetrachloroethane BDL 5.0 MOA 1 7/31/2007 4:26:00 PM

Chiorot)enzene BDL 5.0 pgA 1 7/31/2007 4:28:00 PM

BDL 5.0 pgA 1 7/31/2007 4:28:00 PM

m.p-Xytene BDL 10 UOA 1 7/31/2007 4:28:00 PM

Bromoform BDL 5.0 PflA 1 7/31/2007 428:00 PM

Styrene BDL 5.0 MOA 1 7/31/2007 4:28i)0PM

1.1.2.2-Tetrachloroethane BDL 5.0 POA 1 7/31/2007 428:00 PM

o-Xylene BDL 5.0 MQA 1 7/31/2007 4:28:00 PM

Bromobenzene BDL 5.0 MQA 1 7/31/2007 428:00 PM

2-Chlorotoluene BDL 5.0 MOA 1 7/31/2007 428:00 PM

4-ChIorotoluene BDL 5.0 pgA 1 7/31/2007 428:00 PM

Sum Dibromofluoromethane 129 60-125 S %REC 1 7/31/2007 428:00 PM

Sum 1,2-0ichloroethan»^ 123 49-127 %REC 1 7/31/2007 4:28:00 PM

Sum ToIuene-d8 102 50-126 %REC 1 7/31/2007 428K}0 PM

Sum 4-BrDmofluorobenzene 100 46-110 %REC 1 7/31/2007 428:00 PM

CLIENT: Hull and Associates, Inc. Lab Order: 0707C90 CUENT: Hull and Associates, Inc. Lab Order: 0707C90 Project: COTI92 Stickney Avenue Landfili Project: COT192 Stickney Avenue Landfill

Data Qualiflers (Flags)

! See Case Nanaiive * Value exceeds Maximum Contaminant Level A Silica gel analysis not perfonned the total oil and grease is less than detectable limits B Analyte detected in the associated Method Blank

BDL Below Detection limit C Sample result confirmed by reanalysis E Value above quantitation range F Unable to obtain a reliable result due to matrix interference H Analysis completed outside holding limes J Analyte detected below quantitation limits, estimated concentration for TICs K Result from method of standard additions N Presumptive evidence of analyte present

NG No growth P Sample preservation does not meet method requirements

PQL Practical Quantitation Limit or surrogate S Surrogate recovery outside acceptance limits V Calibration criteria exceeded, but acceptable by method

Page 14 ofl5 Page 15ofl5

Hul CHAIN OF CUSTODY RECORD iates, inc.

PAGE i- OF

NO. 015767 •Dubtln. QH

Dublin, OH 4301B

•Uu • Mb«Bn. QH 4BOO Pvkwiy Dr. Suiti 100

•, IN 402B0 Mbton. OH 40040

nSQion. OH ei91 CotfirwRMd SultaD Solon. OH 44130

Phono: (014) 703-1777 Phono: (SIT) SSfrOBOB Phono: (013) 4S0-M77 Phono: (440) 61B-256S Phono: (41B) 300-2018 Poc (014) 7B3-9070 POK (317) 000-0553 PoK (013)46B-0Be» Fox; (440) 019-2SSO Fox: (41«) 300-0407

RyOHTTO: ok.o^r/^

aient Ctf/ 7a./e-/» -Ps—

SKe; /Ivtrvt. / Oi-nf'lL. Proieetft-SiZm^

PR(DJECT SAMPLE SAMPLE NO. LOCATION TYPE & ID

NO. OP CONT.

METALB cooEcnoN / / DATEmME / / / / / / / COMMENTS

=-77?; = •L •J-

: :

=

4-

RBJNQUI8HED BY!

ReUNQUISHCD BYi

COOLER TEMPERATURE

•alhmrTo: 7?e/iW.>-cr

Mathod of Dalhmy: C-FV

Alrttll Numbar

itivn ' '-LAOUSB (MUSTBaNETUmDWTTHKpam) VBIOW -LMUSB

PNC -RBWNEDBVHULL TURN AROUND TIME: sr^ DAYS

OlCFf 0.(^0

HuJJ CHAIN OF CUSTODY RECORD PAGE . op

iates, inc. NO, 015770 •Dublin. QH

0397 EmonM Pirkwoy Sulto 200 Dublin. OH 43010

•todlinaBfiUUM 0330 B. 70th SL Sultb 170

IN 40200 Mbion, OH 40040

•MMon. OH 4900 Pirtniray Or.

• aolan. QH 0101 Cochiin Robd '

Solon, OH 44130

^1 QltndilbAv*. Suit* 300 TbMo. OH.43014

Phon«: (014) TOS-Orn Phorw: (317) 050-0000 Phon«: (B13)40»-M77 Phena: (440) 010-2050 Phona: (410) 300-2010 Fu: (014) rB»:«070 Fan: (317) 000-0003 Fax: (013)409-9009 Fax: (440)019-2500 Fax: (419)305-0407

FEPOPTTo-— y Client F?. / w> "TS/gc/e

Site: .4irf'/ii>C i/it

Project * CifTn^ Phaae:_<iiu.i:g^

PROJECT SAMPLE SAMPLE NO. LOCATION TYPE SID

NO. OP CONT.

METALS DATEmME // y V ^ >£/

/ / / / COMMENTS

CCSTt'^X. •• A-1UJ7. 1 : r,o7 2Sa7 tr-<7 V M 1 1 1 1

-H / / / y

iLar/tx. =6«'72St>"> Y / 1 ( (

>aiw-X> •C.o->XSli'7y1-. S-? Y 1 1 1 (

V I- 1 / y y

Y y y y y

c^riîx. Jbti—^ •) .'5i-5 w N y r ) / 33 •(».>7X£<.'7 '..-roFj w A/ 1 / 1 (

Ca»riSX. ^36" : &<oxr«7 :r-? •Y A' 1 / / / An.-j3(o 6-->xru5 s-'-i 7 1 1

c-rnx. ;r-5 V r y Z 1 <.arl^x. 1 «Y r^. } 1 1 \

REUNQUISHEOBV:

RELINQUISHED BY:

RELINQUISHED BY

OATe:'?/irJ ^'7 TIME:

COOLER TEMPERATURE

AS RECEIVED:

RECEIVED BY

DATE: Deliver To:

Method of Delivery;

AlrblH Number

NOTES:

DISTRIBUTION^ WHm 1 •LABuao(Miarn>wnjiwEDwrT>ii4EPORn VBXOW -LABUOB

DBVHua TURN AROUND TIME: DAYS

otasuufll

I oiw.

itEs.mc

PARAMETERS TO BE ANALYZED

GENERAL AND INORGANICS:

• • • • • B

RGBs

PAHs

hepiacNor

alditn

DDT

Mercury, total

MUMuates. inc fcaM.M300aTcM

Proiect/Fadlitv: Sticknev Avenue Landfill Sample Data: 1 Proiect/Fadlitv: Sticknev Avenue Landfill Sample Dale: 7 Ixsl' »

Address: Citv of Toledo. DSW. 3962 Hoffman Rd.Totedo. OH. 43611

Contact David Leffier Telephone: (419)936-2643 Report to: Karen Okonta CortacI: David Leffler Telephone: 1419)936-2643 Report to: Karen Okonta

BiilioQ Address/PO #: Billina AddnBs6=0 #:

SampieTvue: GROUNDWATER 0 Grab 1 1 Composite SampieTvue: LEACHATE 0 Grab 1 1 Composite

GENERAL AND INORGANICS:

1x1 VOCs |x] PCBs 0 DImaltiibniJina

• • • • • • •

FIELD UEJSURED PAHAMETCRS

r~l Ship UPS Q CIMIII Pick-up

Sampla Conlaineiii Pipvidpti Hv: BelmonI ftnalvlica] LAiiorali

Suhmilled tnc "Sn . Received

n Silo DclivciyPick-iip 0 Our Sampling

S^PLEflS. MC:S09

HELD MEASURED PARAMETERS

1 Samplas to ba Analyzed try Latxwaiory | Tuitiidity PH Dissolved Orygen Conductnrily Temperature Redok Paential Notes

Sample ID f mg/L S.U. mg/L umhos/cm deg.C mv Notes

MW-21 f-r.5* * Ai.. 2.1 .• *.• 1 II'AA ) » tvS" O-l- 7830 /2 7 -n9 MVir-24 ^#52. A/s- tvV? O-ll JM? -lift

MW-27 cmx. 1 fc.Tfi O.Of 'V3o n» ^l/L

MW-30 lav 6SI O"! 4/3J i-'i -iH

MW-33 SJ\ O-ol (ffHOO T3.i, MW-35 CvT^fc Avals' 0-0( n<} DuDlicate : 6''yZr»>'> A: SA 1 t 28 O- 1 IXf -i/i-

' ? A-C. —

•fijo JVJ. ,1-lf

Samples to be Analyzed tiy Laboratory Tuibidity pH Dissolved Oxygen ConducUvily Temperature Redox Potsntla) Notes

Mtfitoring WeU SamptolDt mgA S.U. mg/L umhos/cm deg. C mv Notes

MW-38 /3 i-v*- S22v >7-1- -MW-37r*^lf 1 Iff un cJ.ol lUT.

• Ship UPS • CHerd Pick-up •

Sampla Containers Provided By; Belmont Analytical' a>'»ratDri«s

Sulkiiilled by: .

Site DeUveiyyptck-up 0 Our Sampling

• T-aOrPl //:3Q

Belmont Labs

CLIENT: Hull and Associates. Inc. Work Order: 0707C90 Project: COT192 Stickney Avenue Landfill

Date: 08-Jan-08

ANALYTICAL QC SUMMARY REPORT TestCode: HG GW

Sample ID; MB-14743

Client ID; ZZZZZ

Anaiyte

SampType: MBLK

Batch ID: 14743

TestCode: HG.QW.

TestNo: SW7470A

Units: mg/L




%REC LowUmit HighLlmit RPDRefVal

RunNo: 60294

SeqNc: 754977

%RPD RPDLimlt Qual

Mercury BDL 0.00020

Sample ID: LC3-14743

Client ID: 77777

SampType: LCS

Batch ID: 14743

TestCode: HG_GW

TestNo: SW7470A

Units: mg/L Prep Date: 7/31/2007


RunNo: 60294

SeqNo: 754978

Anaiyte Result PQL SPK value SPKRefVal %REC LowLlmIt HighLlmit RPDRefVal %RPD RPDLimlt Qual

Mercury 0.006300 0.00020 .0.00625 0 101 80 120 0 0

Sample ID: LCSD-14743

Client ID: ZZZZZ

SampType: LCSD

Batch ID: 14743

TestCode: HG.GW

TestNo: SW7470A



RunNo: 80294

SeqNo: 754990

Anaiyte Result PQL SPK value SPK RefVal %REC LowLlmit HighUmIt RPDRefVal %RPD RPDLimlt Qual

Mercury 0.006120 0.00020 0.00625 0 97.9 SO 120 0.0063 2.90 20

Sample ID: 0707C90-003DMS

Client ID: COT192:MW27:a07

SampType: MS

Batch ID: 14743

TestCode; HG_GW

TestNo: SW7470A



RunNo; 60294

SeqNo: 754983

Anaiyte Result PQL SPK value SPK RefVal %REC LowUmit HighUmIt RPDRefVal %RPD RPDUmIt Qual

Mercury 0.006110 0.00020 0.00625 0 97.8 70 130 0 0

Sample ID: 0707C90^03DM3D

Client ID: COT192:MW27:Q07

SampType: MSG

Batch ID: 14743

TestCode: HG.GW

TestNo: SW7470A

Units:. mg/L Prep Date; 7/31/2007


RunNo: 80294

SeqNo: 754984

Anaiyte Result PQL SPK value SPK RefVal %REC LowLlmIt HighUmIt RPDRefVal %RPD RPDLimlt Qual

Mercury 0.000150 0.00020 0.00625 0 98.4 70 130 0.00611 0.653 30

Page I of IS

J3 s I

V CQ

O

r /O

r a

s I

§ i i

I g

•s s

S o o o o c c c 1115 fj 'J o o

> 3

I t I s "S 0) g. S £ S s s

i 3

•> s

S s f I

W V) (O

3elmont Labs Date: 08-J(m-08

XIENT; Hull and Associates, Inc. Work Order: 0707C90 "reject: COT192 Stickney Avenue Landfill


Sample 10; LCSD-14741 SampType; LCSD TestCode: PAH_027O_W Units: pgA- Prep Date: 7/31/2007 RunNo: 60329

Client ID: ZZZZZ Batch ID: 14741 TestNo: SW8270C (SW3S10C) Analysis Date: 8/1/2007 SeqNo: 755447

Analyte Result PQL SPK value SPKRefVal %REC LowUmIt HIghLlmIt RPDRefVal %RPD RPDUmIt Qual

Surr 2-Ruoroblphenyl 15.34 0 40 0 36.4 19 58 0 0 0 Surr p-TerphenyW14 21.46 0 40 0 53.6 10 62 0 0 0

Sample ID: 0707C90-003CM3 SampType: MS TestCode: PAH_8270_W Units; PB/L Prep Date: 7/31/2007 RunNo: 60482

Client ID: COT192:MW27:Q07 Batch ID: 14741 TestNo: SW8270C (SW3S1QC) Analysis Date: 8/3/2007 SeqNo: 757667

^nalyte Result PQL SPK value SPKRefVal %REC LowLimIt HIghUmit RPDRefVal %RPD RPDLImit Quel

Acanaphthene 69.27 10 100 0 69.3 69 93 0 0 Pyrene 56.96 10 100 0 57 35 101 0 0

Surr Nitrobenzene-dS 16.63 0 40 0 41.6 20 58 0 0 Surr 2-Fluoroblphenyt 15.11 0 40 0 37.8 19 58 0 0 Surr. p-Terphenyl-d14 10.86 0 40 0 27.2 10 62 0 0

Sample ID: 0707C90-003CMSD SampType: MSO TestCode: PAH.8270_W Units: pg/L Prep Date: 7/31/2007 RunNo: 60482

Client ID: COT192:MW27:G07 . Batch ID: 14741 TestNo: SW8270C (SW3910C) Analysis Date: 8/3/2007 SeqNo: 757668

Vnalyto Result PQL SPK value SPKRefVal %REC LowUmIt HIghLlmIt RPDRefVal %RPD RPDUmIt Qual

Acanaphthene 71.80 10 100 0 71.8 69 93 60.27 3.59 10 Pyrene 52.41 10 100 0 52.4 35 101 56.96 8.32 32

Surr NItrobenzene-dS 16.47 0 40 0 41.2 20 58 0 0 0 Sum 2-FtuorT)blpheny1 15.04 0 40 0 37.6 19 58 0 0 0 Sum p-Terphenyl-d14 12.31 0 40 0 30.8 10 62 0 0 0

Page 3 of IS

Belmont Labs

LIENT: Hull and Associates, Inc. 'ork Order; 0707C90

Project: COT192 Stickney Avenue Undfill

Date; 08-Jan-OS


ample ID: MB.14741 SampType: MBLK TestCode: PAH_8270_W Units: pgn. Prep Date: 7/31/2007 RunNo: 60329

yient ID: 77777 Batch ID: 14741 TestNo: SW8370C (SW3510C) Analysis Dab: 8/1/2007 SeqNo: 755448

/Vnaiyte Result PQL SPK value SPKRefVal %REC Lov/Llmlt HIghLlmIt RPDRefVal %RPD RPDUmIt Qual

laphthalene BDL 10 cenaphthene BDL 10

yrene BDL 10 .jenz{a)anthrBcene BDL 0.26 Chrysene BDL 10

Senzo(b)fluoranihene BDL 0.17

)enzo(k)fluor8nthene BDL 1.7

enzo(a)pyrene BDL 0.20

tdeno(1.2.3<d)pyrene BDL 0.22

Dlbenz(a,hlanthracene BDL 0.20

Sum Nltrobenzene-d5 15.39 0 40 0 38.5 20 63 0 0 Sum 2-Fluoroblpheny1 14.75 0 40 0 36.9 10 58 0 0 Sum p-Terphenyl-d14 18.67 0 40 0 46.7 10 62 0 0

sample ID: LCS-14741 SampType: LCS TestCode: PAH_8270_W Unib: pg/L Prep Dab: 7/31/2007 RunNo: 60320

rjtont in- 77777 Batch ID: 14741 TestNo: SW8270C (SW3510C) Analysis Date: 6/1/2007 SeqNo: 755446

Jiatyte Result PQL SPK value SPKRefVal %REC LowLlmlt HIghLlmIt RPDRefVal %RPD RPDLImit Qual

cenaphthene 79.26 10 100 0 79.3 64 103 0 0

Pyrene 85.08 10 100 0 85.1 35 107 0 0

Sum Nltrobenzene-d5 16.04 0 40 0 40.1 20 63 0 0 Sum 2-Ruoroblphenyl 14.92 0 40 0 37.3 19 58 0 0 Sum p-TerphenylHj14 20.43 0 40 0 51.1 10 62 0 0

..ample ID: LCSD-14741 SampType: LCSD TestCode: PAH_8270_W Unib: pg/L Prep Date: 7/31/2007 RunNo: 60329

:ilent ID: ZZZZZ Batch ID: 14741 TestNo: SW8270C (SW3510C} Analysis Date: 8/1/2007 SeqNo; 755447

nalyte Result PQL SPK value SPKRefVal %REC LowLlmlt HIghUmit RPDRefVal %RPD RPDLImit Qual

cenaphthene 81.59 10 100 0 81.6 64 103 79.26 2.90 14

Vsne 87.62 10 100 0 87.6 35 107 85.08 2.94 13

Sum Nltrobenzene>d5 16.72 0 40 0 41.8 20 63 0 0 0

Page 2 of IS

Belmont Labs

CLIENT: Hull and Associates, Inc. Work Order: 0707C90 Project: COT192 Stlckney Avenue Landfill

Date: OS-Jon-OS

ANALYTICAL QC SUMMARY REPORT

TestCode: PCB 8082 W

Sample ID; 07Q7C90-003AMS SampType; MS TestCode: PCB.8082_W Units; pg/L Prep Date: 7/31/2007 RunNo: 60518

Client ID: COT192:MW27:Q07 Batch ID: 14752 TestNo: SW80a2 (SW3910C) Analysis Date; 8/7/2007 SeqNo: 758251.

Analyte Result PQL SPK value SPK RefVal %REC LowLimit HighLlmlt RPD RefVal %RPD RPDUmIt Quel

AroclorlOie 10.67 0.20 10 0 107 70 130 0 0

Arodor 1260 8.010 0.20 10 0 80.1 70 130 0 0

SUIT: Decachiorebiphenyl 0.4200 0 1 0 42 35 143 0 0

Sum Tetrachloro-m-xylene 0.6300 0 1 0 63 37 110 0 0

Sample ID: 0707C90-003AMSD SampType: MSD TestCode: PC8.8082.W Units: pg/L Prop Date: 7/31/2007 RunNo; 60518

Client ID; COT192:MW27:G07 Batch ID: 14732 TestNo: 3WB0B2 (SW3510C) Analysis Date: 8/7/2007 SeqNo: 758252

Analyta Result PQL SPK value SPK RefVal %REC LowUmlt HighLlmlt RPD RefVal %RPD RPDUmIt Qual

Arodor1016 10.43 0.20 10 0 104 70 130 10.67 2.27 25 Arodor1260 7.220 . 0.20 10 0 72.2 70 130 8.01 10.4 25

Sum Decachiorebiphenyl 0.2600 0 1 0 26 35 143 0 0 0 S Sum TetrachlorO'm-xylene 0.6300 0 1 0 63 37 118 0 0 0

Page 5 of IS

Belmont Labs

CLIENT: Hull and Associates, Inc. Work Order: 0707C90 Project: COT192 Stlckney Avenue Landfill

Date: 08-Jan-08



Sample ID: MB-147S2 SampType: MBLK TestCode: PCB_8082_W Units: pg/L Prep Date: 7/31/2007 RunNo: 60518

Client ID: ZZZZZ Batch ID: 14752 TestNo: SW8082 (3W3910C) Analysis Date: B/7/2007 SeqNo: 758247

Analyta Result PQL SPK value SPK RefVal %REC LowUmlt HighLimit RPD RefVal %RPD RPDUmIt Qual

Aredor 1016 BDL 0.20 Aredor1221 BOL 0.20 Arodor 1232 BDL 0.20 Arodor1242 BDL 0.20 Arodor 1248 SDL 0.20

Arodor1254 BDL 0.20


Sum Decachiorebiphenyl 0.6300 0 1 0 03 35 143 0 0


Sample ID: LC3-14752 SampType: LCS TestCode: PCB_8082.W Units: pgA. Prep Date: 7/31/2007 RunNo: 60518

Client ID: ZZZZZ Batch ID: 14752 TestNo: 3Wa082 (3W3910C) Analysis Date: 8/7/2007 SeqNo: 758248

Analyte Result PQL SPK value SPK RefVal %REC LowLimit HighUmIt RPD RefVal *RPD RPDUmil Qual

Arodor 1016 10.51 0.20 10 0 105 72 119 0 0 Arodor 1260 8.960 0.20 10 0 89.6 64 132 0 0

Sum Decachiorebiphenyl 1.030 0 1 0 103 35 143 0 0 Sum Tetrachloro-m-xylene 0.8000 0" 1 0 80 37 116 0 0

Sample ID: LCSD-14752 SampType: LC3D TestCode: PCB.8082.W Units: pg/L Prep Date: 7/31/2007 RunNo: 80518

Client ID; ZZZZZ Batch 10: 14752 TestNo: SW8082 (SW3510C) Analysis Date: 8/7/2007 SeqNo; 758249

Analyte Result PQL SPK value SPK RefVal %REC LowLimit HIghUmIt RPD RefVal %RPD RPDUmIt Qual

Arodor 1016 11.23 0.20 10 0 112 72 119 10.51 6.62 20

Arodor 1260 9.360 0.20 10 0 93.6 64 132 6.96 4.37 19

Sum Decachlorobiphenyl 1.000 0 1 0 100 35 143 0 0 0

Sum Tetrachloro-m-xyiene 0.9100 0 1 0 61 37 116 0 0 0

Page 4 of 18

lelmont Labs Dote; 08-Jon-08

LIENT: Hull and Associates, Inc. Vork Order: 0707C90 »roject: COT192 Slickney Avenue Landfill


)ampla 10: LCS-14752 SampType: LCS TestCode: PEST_8081_ Units: nort- Prep Date: 7/31/2007 RunNo: 80583

Client 10: ZZZZZ Batch ID: 147S2 TestNo: SW8081A (SW3510C) Analysis Data: 8/8/2007 ' SeqNo: 759430

4nalyte Result PQL SPK value SPK RefVal %REC LowLlmlt HlghLlmlt RPDRefVal %RPD RPDUmIt Qual

.4--DDT 0.9S00 0.050 1 0 98 41 132 0 0

Sum Decachloroblphenyl 1.020 0 1 0 102 28 172 0 0

Sum Tetrachloro-m-xytene 0.8200 0 1 0 82 45 129 0 0

Sample ID: LCSO-14752 SampType: LCSD TestCode: PEST_8081_ Units: ]}glL Prep Date: 7/31/2007 RunNo: 60518

:ilent ID: ZZZZZ Batch ID: 14752 TestNo: SW8a81A (SW3910C) Analysis Date: 8/7/2007 SeqNo: 758271

inalyte Result PQL SPK value SPK RefVal %REC LowLlmlt HlghUmlt RPDRefVal %RPD RPDLImlt Qual

Heplachlor 0.8700 0.050 1 0 87 71 117 0.88 1.14 17

\ldrln 0.7900 0.050 1 0 79 61 107 0.81 2.50 12

Sum Decachloreblphenyl 1.020 0 1 0 102 28 172 0 0 0

Sum Tetrachloro-m-xyiene 0.8900 0 1 0 80 45 129 0 0 0

Sample ID: LCSD-14752 SampType: LCSD TestCode: PE3T_808 1_ Units: pg/L Prep Date: 7/31/2007 RunNo: 60583

miont ID: ZZZZZ Batch ID: 14792 TestNo: SW8081A (SW3510C) Analysis Date: 8W2007 SeqNo: 759431

inalyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghLlmlt RPDRefVal %RPD RPDUmlt Qual

laptachlor 0.8600 0.050 1 0 86 71 117 0.84 2.35 17

Mdrin 0.7800 0.050 1 0 78 61 107 0.75 3.92 12

•,4'.DDT 0.9500 O.OSO 1 0 95 41 132 0.98 3.11 19

Sum Decachioroblphenyl 1.030 0 1 0 103 28 172 0 0 0

Sum Tetrachlcro^-xylene 0.8500 0 1 0 85 45 129 0 0 0

Sample ID: 0707C90-003BM3 SampType: MS TestCode: PEST_8081_ Units: \tgn. Prep Date: 7/31/2007 RunNo: 60518

^4jent ID: COT192:MW27:G07 Batch ID: 14752 TestNo: SW6081A (SW35iaC) Analysis Data: 8/7/2007 SeqNo: 758273

nalyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghUmlt RPDRefVal %RPD RPDUmlt Qual

eptachlor 0.9300 0.050 1 0 93 70 130 0 0

Mdrin 0.7300 0.050 1 0 73 70 130 0 0 i4'.DDT 0.7300 0.050 1 0 73 70 130 0 0

Page 7 of 18

Jelmont Labs Date: 08-Jan-08

LIENT: Hull and Associates. Inc. ork Order: 0707C90

'roject: COTl 92 Slickney Avenue Landfill


ample ID: MB-14752 SampType: MBLK TestCode: PEST_8081_ Units: pg/L Prep Date: 7/31/2007 RunNo: 60918

ilent ID: ZZZZZ Batch ID: 14752 TestNo: SWBOaiA (SW3910C) Analysis Date: aff/2007 SeqNo: 758269

Mialyte Result PQL SPK value SPK Ref Val %REC LowUmIt HlghUmlt RPDRefVal %RPD RPDUmlt Qua]

eptachlor BDL 0.050 Idrin BDL 0.050 Sum Decachloroblphenyl 0.9300 0 1 0 03 28 172 0 0 Sum Tetrachloro-m-xylene 0.7400 0 1 0 74 45 129 0 0

Sample ID: MB-14752 SampType: MBLK TestCode: PEST_BQ81_ Units: pg/L Prep Date: 7/31/2007 RunNo: 60583

lllent ID: ZZZZZ Batch ID: 14792 TestNo: SW8081A (SW3510C) Analysis Date: 8/8/2007 SeqNo: 799429

nalyte Result PQL SPK value SPK Ref Val %REC LowUmIt HlghUmlt RPDRefVal %RPD RPDUmlt Qual

•ieptachlor BDL 0.050 'Jdrin BDL 0.050

,4"-DDT BDL 0.050 Sum Decachloroblphenyl 0.9200 0 1 0 92 28 172 Q 0 Sum Tetrachloro-m-xylene 0.8000 0 1 0 80 45 129 0 0

Sample ID: LCS-14792 SampType: LCS TestCode: PEST_8081_ Units: pg/L Prep Date: 7/31/2007 RunNo: 60518

4lent ID: 77777 Batch ID: 14752 TestNo: SWBOSIA (SW351QC) Analysis Date: 8/7/2007 SeqNo: 758270

nalyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghUmlt RPD Ref Val %RPD RPDUmlt Qual

ieptachlor 0.8800 0.050 1 0 88 71 117 0 0 tldrin 0.8100 0.050 1 0 81 61 107 0 0

Sum Decachloroblphenyl 1.080 0 1 0 106 28 172 0 0


iample ID: LCS-14782 SampType; LCS TestCode: PEST_8081_ Units: pgrt. Prep Date: 7/31/2007 RunNo: 60583

:ilont ID: 7Z77Z Batch ID: 14752 TestNo: SW8081A (SW3510C) Analysis Date: 8/8/2007 SeqNo: 759430

nalyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghLlmlt RPDRefVal %RPD RPDUmlt Qual

eptachlor 0.8400 0.050 1 0 84 71 117 0 0 4drin 0.7500 0.050 1 0 75 61 107 0 0

Page 6 of 13


CLIENT: Hull and Associates, Inc.

Work Order: 0707C90 ANALYTICAL QC SUMMARY REPORT

Project: COT192 Stickney Avenue Landfill TestCode: VOC_8260_W

Sample ID: MBLK SampType: MBLK TeatCode: VOC_8260_W Units: pg/L Prep Date; RunNo: 60306

Client 10: 2Z72Z Batch ID; R60306 TestNo: SWa260a Analysia Date: 7/31/2007 SoqNo: 735288

Analyte Result PQL SPK value SPKRefVal %REC LowLlmIt HIghUmIt RPD Ref.Val %RPD RPDUmIt Qual

n-Hexane BDL 5.0 OichloredlRuoromethane BDL 5.0 Chloromethane BDL 5.0 Vinyl ctilorlde BDL 1.0

Bromomethane BDL 5.0 Chloroethane BDL 5.0 Acrolein BDL 20 Acetonltrlle BDL 40

Tfichiorofluoromethane BDL 5.0 Acetone BDL 20 1,1-Dlchloroetheno BDL 5.0 Acryionitriie BDL 20 iodomettiane BDL 10 Methylene chloride BDL 5.0 Carbon disulfide BDL 20 trans-1,2-Dlchloroethene BDL 5.0 Methyl tert-butyl ether BDL 10

1,1-Dichloroethane BDL 5.0 Vinyl acetate BDL 10

2-Butanone BDL 20

ds-i.2-DlchlorDethene BDL 5.0 Bromochloromethane BDL 5.0 Chloroform BDL 5.0 2,2-Dlchloropropane BDL 5.0 1,2-Olchtoroethane BDL 5.0 1.1.1-Trlchloroethane BDL 5.0 1,1>Dlchloropropene BDL 5.0

Carbon tetrachloride BDL 3.0 Benzene BDL 5.0 DIbromomethane BDL 5.0 1,2-Olchloropropane BDL 5.0

Page 9 of IS

Belmont Labs

CLIENT: Hull and Aasocmtes, Inc. Work Order: 0707C90

Project: COT192 Stickney Avenue Landfill

Date: OS-Jan-03

ANALYTICAL QC SUMMARY REPORT TejtCode: PEST 8081 W

Sample ID: 0707C90-Q03BMS SampType; MS TestCode: PEST_BQ81_ Units: pg/L Prop Date: 7/31/2007 RunNo: 60518

Client ID: COT192:MW27:G07 Batch ID: 14752 TestNo; SW8081A (SW3510C} Analysis Date: 6/7/2007 SeqNo: 758273

Analyte Result PQL SPK value SPKRefVal %REC LowLlmIt HlghUmit RPD Ref Val %RPD RPDUmIt Qual

Sum Decachloroblphenyl 0.4100 0 1 0 41 26 172 0 0 Sum Tetrachloro-m-xylene 0.6800 0 1 0 68 45 129 0 0

Sample ID: Q707C90-003BMS SampType: MS TestCode: PEST_8081^ Units: pg/L Prep Date: 7/31/2007 RunNo: 60583

Client ID: COT192:MW27:Q07 Batch ID: 14752 TestNo: SW8061A ISW3510C) Analysis Date: 8/8/2007 SeqNo: 759435

Analyte Result PQL SPK value SPK Ref Val %REC LowLlmIt HIghUmIt RPD Ref Val %RPD RPDLImit Qual

4.4--DDT 0.6300 0.050 1 0 63 70 130 0 0 Sum Decachloroblphenyl 0.3000 0 1 0 30 28 172 0 0 Sum Tetrachloro-m-xylene 0.7200 0 1 . 0 72 45 129 0 0

Sample ID: 0707C90-003BMSD SampType: MSD TeatCode: PEST_B081_ Units: MO/L Prep Date: 7/31/2007 RunNo: 60516

Client ID: COT192:MW27:G07 Batch ID: 14752 TostNo: SW8081A (SW3510C) Analysis Date: 8/7/2007 SoqNo: 758274

Analyte Result PQL SPK value SPKRefVal %REC LowUmIt HIghUmIt RPD Ref Val %RPD RPDLImit Qual

Hoptachlor 0.9200 0.050 1 0 92 70 130 0 0 25 Aldrin 0.7800 0.050 1 0 78 70 130 0 0 25 4.4--DDT 0.7800 0.050 1 0 78 70 130 0 0 25

Sum Decachloroblphenyl 0.4200 0 1 0 42 26 172 0 0 0 Sum Tetrachloro-m-xylene 0.7100 0 1 0 71 45 129 0 0 0

Sample ID; 0707C90-003BMSD SampType: MSD TeatCode: PEST_8081_ Units: pg/L Prop Date: 7/31/2007 RunNo: 60583

Client ID; COT192:MW27:G07 Batch ID: 14752 TestNo: SW8081A (SW3510C) Analysis Date: 8/8/2007 SeqNo: 759436

Analyte Result PQL SPK value SPKRefVal %REC LowUmIt HIghUmIt RPD Ref Val %RPD RPDUmIt Qual

4.4--DDT 0.6200 0.050 1 0 82 70 130 0.63 1.21 25 Sum Decachloroblphenyl 0.3000 0 1 0 30 26 172 0 0 0 Sum Totrachloro-m-xylene 0.7300 0 1 0 73 45 129 0 0 0

Page S of IS

3elmont Labs

:LIENT; Work Order:

®roject;

Hull and Associates. Inc. 0707C90 COT192 Stickncy Avenue Landfill

Date: 08-J(w-08


TestCode: VOC 8260 W

Sample ID: MBLK

Client ID: 77777

Analyte

SampType: MBLK

Batch ID; R60M6

TestCode: VOC_826Q_W Units: HQA.

TestNo: SW8260B


Prep Date:


%REC LowLimIt HighLlmlt RPDRefVal

RunNo: 60348

SeqNo: 735706

%RPD RPDLimIt Qual

n-Hexane Olchlorodlflucromethane Chloromethane Vinyl chloride Bromomethane Chloroe thane Vcrelein Acetonltrlle Trichlorofluorcmethane Acetone l.l-Dlchloroothene \crylonltrile odomethane Methylene chloride Carbon disulfide /ans-1.2-0[chlon3ethene Methyl tert-butyl ether 1.1-Dichlofoethane Vinyl acetate 2-Butanone :l8-l.2-Dichloroethene 3romochloromethane chloroform 2.2-OIchloropropane 1.2-Dlchloroethane 1,1,1-Trichloroethane 1,1-Olchloropropene Carbon tetrachloride Benzene DIbromomethane \2-Dlchloropropana

BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL

BDL

BDL

BDL BDL BDL BDL BDL BDL BDL BDL BDL

5.0 3.0 5.0 1.0 5.0 5.0 20 40

5.0 20

5.0 20 10 5.0 20 5.0 10 5.0 10 20

3.0

5.0 3.0 5.0

3.0

5.0 5.0 5.0

5.0

5.0

5.0

Pflge ! I of 18

Belmont Labs Date: 08-J<tn'08

LIENT: Hull and Associates, Inc. 'ork Order: 0707C90

Project: COT192 Stickncy Avenue Landfill



ample ID: MBLK SampType: MBLK TestCode: VOC.8280.W Units: pG

illent ID: ZZZZZ Batch ID: Re0306 TestNo: SW8260B

Analyte Result PQL SPK value SPKRefVal

richloroethene BDL 5.0

remodlchloromethane BDL 5.0

•Chloroethyl vinyl other BDL 10

Js-1,3-Olchloropropene BDL 5.0 4êthyl-2-pentanone BDL 20

Tans-I >0)chloropropene BDL 5.0 ,1.2<Trichloroe thane BDL 5.0

'oluene BDL 5.0 ,3-Dlchloropropane BDL 5.0

BDL 20

Dlbromochloromethane BDL 5.0

,2>Dlbromoe thane BDL 5.0 etrachloroethene BDL 5.0

,1,1,2'Tetrachloroethane BDL 5.0

^hiorobenzene BDL 5.0

ithylbenzene BDL 5.0

n,p-Xytene BDL 10

Iromoform BDL 5.0

tyrene BDL 5.0

1.1,2,2-Tetrachloroethane BDL 5.0

)-Xyl6ne BDL 5.0

romobenzene BDL 5.0

•Chlcrotoluene BDL 5.0

•Chlorotoluene BDL 5.0

Surr Dibromofluoromethane 56.94 0 50 0

Sum 1,2-Dlchlcroethane-d4 52.91 0 50 0

Sum Toluene-d8 52.55 0 50 0 Sun: 4*Bromofluorobenzene 50.40 0 50 0

Prep Date:


%REC LowUmIt HlghLlmit RPDRefVal

RunNo; i

SeqNo: 755288

%RPD RPDLImIt Qua!

114 60 125 0 0 106 49 127 0 0 105 50 128 0 0 101 48 110 0 0

Page 10 of 18



Work Order: 0707C90 ANALYTICAL QC SUMMARY REPORT

Project: COT192 Stickncy Avenue Landfill TestCode: VOC_8260_W

Sample ID; MBLK SampTypei MBLK TestCode: VOC_e26e _W Units; pg/L Prep Date: RunNo: 60382

Client ID: ZZZZZ Batch ID: R60382 TestNo; SWB260B Analysis Oata: 8ffl2007 SsqNo: 766100

Analyte Result PQL SPK value SPK RefVal %REC LowLlmlt HIghUmIt RPDRsfVal KRPO RPOUmIt Qual

n*Hexane BDL 5.0 Olchlorodlfluoromethane BDL 5.0

Chloromethane BDL 5.0

Vinyl chloride BDL 1.0

Bromcmethane BDL 5.0 Chioroe thane BDL 5.0

Acrolein BDL 20

Acetonltrlle BDL 40

Trichlorofluoromethane BDL 5.0

Acetone BDL 20 1.1-Olchloroethene BDL 5.0

Acrylonltrile BDL 20

BDL 10

Methylene chloride BDL 5.0 Carbon disulfide BDL 20

tran8-1.2-0lchloroethene BDL 5.0 Methyl tert-butyl ether BDL 10 1,1-Dlchloroa thane BDL 5.0 Vinyl acetate BDL 10

2-Butanone BDL 20

cis-1.2-Dlchloroethene BDL 5.0 Bromochloromethane BDL 5.0

Chloroform BDL 5.0 2,2-Dlchloropropane BDL 5.0

1,2-DichtorDethane BOL . 5.0 1,1.1-Trichloroethane BDL 5.0 l.l-Dlchloropropene BDL 5.0

Carbon tetrachloride BDL 5.0 Benzene BDL 5.0 Oibromomethane BDL S.O 1,2-Olchloropropane BDL 5.0

Page 13 of IS

Belmont Labs Dale; 08-Jaii-08

CLIENT: Hull and Associates, Inc. ANALYTICAL QC SUMMARY REPORT Work Order: 0707C90


Project: COT192 Stickney Avenue Landfill TestCode: VOC_8260_W

Sample ID: MBLK SampType: MBLK TestCode: VOC_B260_W Units: pg/L Prep Data: RunNo: 60346

Client ID; ZZZZZ Batch ID: R60346 TestNo: SW8260B Analysis Date: 8/1/2007 SeqNo: 755706

Analyte Result PQL SPK value SPK RefVal %REC LowLlmll HlghUmlt RPD RefVal %RPD RPDUmlt Qua!

Trichloroethene Bromodichlorofnethantt 2-Chtoroethyl vinyl ether de-1,3-D)chloropropene 4-M8thyl-2<pentanone trane-l ,3-D!chlofQprop8ne 1.1,2-Trtchloroethane Toluene 1,3>0lchlcropropane 2-Hexanon8 Dlbromochloromethane 1.2-Oibromoe thane Tetrachloroethene 1,1,1.2-Tetr8ch!croethane Chlorobenzene Ethytbenzene m.p-Xylene Bromcfonn Styrene 1.1.2,2-Tetrachloroethane o-Xylene Bromcbenzene 2-Chtorotoluene 4^hiorotoluene

BDL

BOL

BDL

BOL

BOL BOL

BOL

BDL

BDL

BDL BDL BDL

BDL

BDL BDL BDL

BOL

BDL

BDL BDL BDL

BDL

BDL BDL

5.0 5.0 10

5.0 20 5.0 5.0 5.0 5.0 20 5.0 5.0 5.0 5.0 5.0 5.0 10

5.0

5.0

5.0

5.0

5.0

5.0

5.0 Sum Dibromofluoromethane 33.66 0 50 0 67.7 60 125 0 0 Sum 1.2-DlchlorDethane-d4 31.14 0 50 0 62.3 49 127 0 0 Surr: Toluene-d8 35.51 0 50 0 71 50 128 0 0 Surr: 4-Bromofluorobenz8ne 38.80 0 50 0 77.6 48 110 0 0

Page 12 of 18

Belmont Labs

:LIENT; Hull and Associates, Inc. Work Order: 0707C90 **roject: COT 192 Stickney Avenue Landfill

Date: i)8-J(m-08

ANALYTICAL QC SUMMARY REPORT TestCode: VOC 8260 W

Sample ID: LOS SampType: LC3 TestCode: VOC_8260_W Units; M0/L Prep Date: RunNo: 60306

Client ID- 77777 Batch ID: Re0306 TestNo: 3W8260B Analysis Date: 7/31/2007 SeqNo: 755286

Analyte Result PQL SPK value SPK Ref Val %REC LowLlmIt HighUmIt RPORefVal %RPD RPDUmIt Qual

>Hexane 22.52 5.0 21.9 0 103 15 161 0 0 1,1-DlchtorDethene 21.30 5.0 20 0 106 49 158 0 0 Benzene 20.78 5.0 20 0 104 61 141 0 0 Trlchloroethene 20.71 5.0 20 0 104 53 140 . 0 0

Toluene 20.65 5.0 20 0 103 62 140 0 0 Chlorobenzene 21.81 5.0 20 0 109 66 135 0 0

Sum Dlbromoflucrcmethane 53.87 0 SO 0 108 60 125 0 0

Sum 1.2-Dlchloroethane-d4 54.42 0 50 0 109 49 127 0 0 Sum Toluone-dB 54.10 0 50 0 108 50 128 0 0 Sum 4-Bromofluorobenzene 53.46 0 50 0 107 48 110 0 0

Sample ID: LOS SampType: LCS TestCode: VOC_8260,W Units: pg/L Prep Date: RunNo; 80348

:ilent ID; ZZ7ZZ Batch ID: R80346 TestNo: 9W8280B Analysis Date: 8/1/2007 SeqNo: 755704

Analyte Result PQL SPK value SPK Ref Val %REC LowLlmll HighUmIt RPD Ref Val %RPD RPDUmIt Qua)

vHexane 18.12 5.0 21.9 0 73.6 15 161 0 0 1,1-Dlchloroethene 16.81 5.0 20 0 84 49 158 0 0 Jenzene 15.21 5.0 20 0 76 61 141 0 0

Trlchloroethene 16.36 5.0 20 0 81.8 53 140 0 0 Toluene 18.04 5.0 20 0 90.2 62 140 0 0 Chlorobenzene 18.11 5.0 20 0 90.6 66 135 0 0

Sum Dlbromofluoromethane 33.11 0 50 0 66.2 60 125 0 0 Sum 1.2-Dlchloroethane^4 35.37 0 50 0 70.7 49 127 0 0 Sum Toluene-dS 35.76 0 50 0 71.5 50 128 0 0 Sum 4-Bromo5uorobenzene 39.59 0 50 0 79.2 48 110 0 0

iampte ID: LC3 SampType: LCS TestCode: VOC,8280,W Unite: po/L Prep Date: RunNo: 60382

:ilentlD; 77777 Batch ID; R60362 TestNo: 3W8280B Analysis Date: 6/2/2007 SeqNo: 786098

Analyte Result PQL SPK value SPK Ref Val %REC LowUmlt HighUmIt RPD Ref Val %RPO RPOLImtt Qual

-Mexane 17.10 5.0 21.9 0 78.1 15 161 0 0

Page 15 of IS

Belmont Labs

LIENT; Hull and Associates, Inc. 'ork Order: 0707C90

Project: COT192 Stickney Avenue Landfill

Date: 08-Jan-08


ample (D: MBLK

lllentID: ZZZZZ

Analyte

SampType: MBLK

Batch ID: R60382

Result

TestCode: VOC_028O_W Units: UQIL

TestNo: SWe2eOB

PQL SPK value SPK Ref Val

Prep Date:


%REC LowUmIt HighUmIt RPORefVal

RunNo: 60382

SeqNo: 756100

%RPD RPDLImIt Qual

richloroethene romodlchloromethane -Chtoroethyl vinyJ ether

js-1.3-Olchloreprt)pene i-Methyl-2-pentanone >rans-1,3>Dlchloropropene

,1,2-Trlchloroethane 'oluene .3-Olchtoropropane

2>HexaRone Dlbromochloromethane ,2-Dlbromoe thane etrachloroethene ,1.1.2-Tetrachloroothano

l^hiorobenzene Ethylbenzene i,p-Xylene iromoform tyrene

1.1,2,2>Tetrachloroethane >Xylene romobenzsne -Chlorotoluene •Chlorotoluene

BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL

S.O 5.0 10 5.0 20 5.0 5.0 5.0 5.0 20

5.0

5.0

5.0

5.0

5.0

5.0 10

5.0

5.0

5.0

5.0

5.0

5.0

5.0 Sum Dlbromofluoromethane 33.73 0 SO 0 67.5 60 125 0 0

Sum 1.2-Dlchloroethane-d4 33.17 0 50 0 66.3 49 127 0 0 Sum. Toluene-d8 36.08 0 50 0 72.2 50 128 0 0

Sum 4-Bromof1uorobenzene 37.85 0 SO 0 75.7 48 110 0 0

Page 14 of 18


CLIENT: Hull and Associates. Inc. Work Order: 0707C90 Project: COT192 Stickney Avenue Landfill


Sample ID: LC3D SampType: LCSD TestCode: VOC_8260_W Units: \igfL Prep Date: RunNo: 60346

Client 10: ZZZZZ Batch ID: R60346 TestNo: SW8260B Analysis Date: 8/1/2007 SeqNo; 799705

Analyte Result PQL SPK value SPK RefVal %REC LowUmlt HlghLlmlt RPD RefVal %RPD RPDLImIt Quel

Benzene 16.43 5.0 20 6 82.2 61 141 15.21 7.71 8.6 Trlchloroethone 17.70 5.0 20 0 88.5 53 140 16.36 7.87 11 Toluene 18.55 5.0 20 0 92.8 62 140 18.04 2.79 9.6 Chlorobenzene 19.66 5.0 20 0 98.3 66 135 18.11 8.21 7.6 R

Surr: Olbremofluoromethane 34.73 0 50 0 69.5 60 125 0 0 0 Sum 1.2-Dlchloroethane-d4 31.91 0 50 0 83.8 49 127 0 0 0

Sum Toluene-d6 35.75 0 50 0 71.5 50 128 0 0 0 Sum 4-0romofiuoroben2ene 41.11 0 50 0 82.2 48 110 0 0 0

Sample tO: LCSD SampType: LCSD TestCode: VOC_a260 i_W Units: MB/k Prep Date: RunNo: 60382

Client ID: ZZZZZ Batch ID: R60382 TestNo: SW8260B Analysis Date: 8/2/2007 SeqNo: 796099

Analyte Result PQL SPK value SPK RefVal %REC LowUmlt HlghLlmlt RPD RefVal %RPO RPDUmlt Qual

n-Hexane 15.29 5.0 21.9 0 69.8 15 161 17.1 11.2 22 1.1-Dlchloroetheno 17.94 5.0 20 0 89.7 49 158 19.4 7.82 12

Benzene 16.36 5.0 20 0 81.8 61 141 17.78 8.32 8.6 Trichloroethene 17.32 5.0 20 0 86.8 53 140 18.19 4.90 11 Toluene 17.47 5.0 20 0 87.4 62 140 16.86 7.65 9.6 Chlorabenzene 18.88 S.O 20 0 94.4 66 135 20.01 5.81 7.6

Sum. Dibromofluoromethane 35.03 0 50 0 70.1 60 125 0 0 0 Sum 1.2-Dlchloroethane-d4 38.30 0 50 0 72.8 49 127 0 0 0 Sum Toluene^S 35.91 0 50 0 71.8 50 128 0 0 0

Sum 4-Bromofluorabenzene 40.09 0 SO 0 80.2 48 110 0 0 0

Paget 7 of 18

Belmont Labs

CLIENT: Hull and Associates, Inc. Work Order: 0707C90 Project: COT192 Stickney Avenue Landfill

Date: 08-Jan-08


Sample ID: LCS SampType: LCS TestCode: VOC_8260_W Units; pg/L Prep Date: RunNo: 60382

Client ID: ZZZZZ Batch 10: R6Q382 TestNo: SW8260B Analysis Date: 8/2/2007 SeqNo: 756098

Analyte Result PQL SPK value SPK RefVal %REC LowLlmIt HlghLlmlt RPD RefVal %RPD RPDLImIt Qual

l.l-Dlchloreathene 19.40 5.0 20 0 97 49 158 0 0 Benzene 17.78 9.0 20 0 88.9 61 141 0 0 Trichloroethene 16.19 5.0 20 0 91 53 140 0 0 Toluene 18.86 5.0 20 0 94.3 82 140 0 0 Chlorobenzene 20.01 5.0 20 0 100 66 135 0 0

Sum. Dibromofluoromethane 35.32 0 50 0 70.6 60 125 0 0 Sum 1,2-Dlchloroothano-d4 37.16 0 50 0 74.3 49 127 0 0 Sum Toluene-d8 35.45 0 50 0 70.9 50 128 0 0 Sum 4-Bromonuorobenzene 37.93 0 50 0 75.9 46 110 0 0

Sample ID: LCSD SampType: LCSD TestCode: VOC.8260_W Units: pg/L Prep Date: RunNo: 60306

Client ID: ZZZZZ Batch ID: R60306 TestNo: 3W8260B Analysis Date: 7/31/2007 SeqNo: 755287

Analyte Result PQL SPK value SPK RefVal %REC LowUmlt HighUmIt RPD RefVal %RPD RPDUmlt Qual

n-He*ane 22.98 5.0 21.9 0 105 15 181 22.52 2.02 22 1,1-Dlchloroethene 21.86 5.0 20 0 109 49 158 21.3 2.59 12 Benzene 20.94 5.0 20 0 105 61 141 20.78 0.787 8.6 Trichloroethene 20.87 5.0 20 0 104 53 140 20.71 0.770 11 Toluene 20.86 5.0 20 0 104 62 140 20.65 1.01 9.6 Chlorobenzene 21.76 5.0 20 0 109 66 135 21.81 0.230 7.8

Sum Dibromofluoromethane 57.00 0 50 0 114 60 125 0 0 0

Sum. 1,2-Dlchloroethan»K]4 56.31 0 50 0 113 49 127 0 0 0 Sum Toluene-d8 53.78 • 0 50 0 108 50 128 0 0 0

Sum 4-Bromofluorobenzene 54.86 0 50 0 110 48 110 0 0 0

Sample ID: LCSD SampType: LCSD TestCode: VOC_8260_W Units: pg/L Prep Date: RunNo: 60346

Client ID: 77777 Batch ID: R60346 TestNo: SW8260B Analysis Date: a/1/2007 SeqNo: 755703

Analyte Result PQL SPK value SPK RefVal %REC LowLimlt HIghUmit RPD RefVal %RPD RPDUmlt Qual

n-Hexane 21.44 5.0 21.9 0 97.9 15 161 16.12 28.3 22 R 1.1-Dlchloroethene 18.61 5.0 20 0 93 49 158 16.81 10.2 12

Page 16 of IS

Data Qualiners (Flags)

I) Anoiyic dviccicd in (he associaiud Method Qlonk BDL Below Detection limit

C Sample result conllrmed by reanoiysis E Value above quantitation range F Unable to obtain a reliable result due to matrix interference H Analysis completed outside holding times J Analyte detected below quantitation limits, estimated concentration for TlCs K Result IVom method of standord additions L Laboratory control sample recovery outside acceptance limits M Matrix spike and/or matrix spike duplicate recovery outside acceptance limits N Presumptive evidence of analyte present P Stntple preservation does not meet method requirements R RPD outside accepted recovery limits S Surrogate recovery ouUide acceptance limits V Calibration criteria exceeded, but acceptable by method

NG No growth I See Cose Narrative

A Silica gel analysis not perfornvd because the total oil and grease is less than detectable limits

Page 18 of 18

Wednesday, November 21,2007

Belmont "Labs' The Environmental Service Company.

Karen Okonta Hull and Associates, Inc. 3401 Glendale Avenue Toledo, OH 43614

TEL: (800)241-7173 FAX (419)385-5487

RE: COT192

Dear Karen Okonta:

Order No.: 0711329


Belmont Labs attests that all analytical methods were performed using acceptable methods, and that the QA/QC procedures stipulated in these metho<^ were followed. USÂ's RCRA Program regards a statement of quality assurance as a legal means of assuring that acceptable and uniform laboratory methods and QA/QC practices were followed by the laboratory.

If you have any questions regarding the test results, please feel free to call me at 937.832.8242.


Holly Grdy Project Manager

QC LEVEL: LEVEL H

CC: Copy of irrvolce with report.

25 HoUflUy Drive Englewood. Ohio 45322 1.937.832.8242 t.937-832-2868 Fax

Belmont Labs Date: lI-Nov-07

CLIENT: Hull and Associates, Inc. Project: COT 192 CASE NARRATIVE Lab Order: 0711329

Analytical Comments for METHOD PAH_8270_W, SAMPLE 0711329-002C: Surrogate out due to matrix interference.

Analytical Comments for METHOD VOC_8260_W, SAMPLE LCSD: n-Hexane was high, but was not detected in the samples.

Analytical Comments for METHOD VOC_8260_W, SAMPLE LCSD: n-Hexane was high, but was not detected in the samples.

Analytical Comments for METHOD VOC_8260_W, SAMPLE LCSD: 1,1-Dichloroethene was low in the LCSD, but accetpable in the MS, MSD.

Analytical Comments for METHOD VOC_8260_W, SAMPLE SAMPLEMS: Toluene and Chlorobenzene were low in the MS,MSD, but acceptable in the LCSJLCSD.

Analytical Conunents for METHOD VOC_8260_W, SAMPLE 0711329-002A: Sample had to be diluted due to matrix inteferences.

Analytical Comments for METHOD PCB_8082_W, SAMPLE 0711329-002D: Siurogate recovery out due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0711329-002D: Surrogate recovery.out due to matrix interference.

Analytical Comments for METHOD PEST_8081_W, SAMPLE 0711329-002D: Sample diluted due to matrix. Surrogates diluted out of lOOOx ruiL

Page 1 of 1

Belmont Labs Date: 29-Nov-07 Belmont Labs Date: 29-Nov-07

CUENT: Hull and Associates. Inc. Lab Order: 0711329 CLIENT: Hull and Associates, Inc. Lab Order: 0711329 Project: COT 192 Project: con 92

UbID: 0711329^01 Collection Date: 11/6/2007 2:20:00 PM

Client Sample ID: C0TI92:PX59:G110607:509 Matrix: GROUNDWATER

Analyses Result PQL Qual Units OF Date Analyzed

PCBS IN WATER SW8082 Analyst DG Arodor1016 BDL 0.20 van. 1 11/V2007 8:14:00 PM Anxla-1221 BDL 0.20 van. 1 u/aaoar 8:14I»PM Arodor1232 BDL 0.20 van. 1 11W2007 8:14:00 PM Arocior1242 BDL 020 van. 1 11/0/2007 8:14A) PM

Anxlor1248 BDL 020 van. 1 11/^2007 8:141X) PM ArocJ0f1254 BDL 020 van. 1 11/00007 8:14:00 PM ArDdor1260 BDL pyn van. 1 Uianooj 8:14:00 PM

Surr DecKhlGratMphenyt 52.0 35-143 %REC 1 11/B0007 8:14«)PM Surr TetracMomm-xytene 67.0 37-116 %REC 1 11/S/2007 8:14A}PM

ORGANOCHLORIHE PESTICIDES SWB081A Analyst DG Heptachlor BDL 0.050 van. 1 11/0«I07 8:14:00 PM Aklrii BDL 0.050 van. 1 11/0/2007 8:14:00 PM 4.4'-DDT BDL 0.050 van. 1 11/0/2007 8:14i)0PM

Surr DecachlordHphenyl 52.0 28-172 *REC 1 11/00007 6M4:00 PM Surr Tetrachloro-m-xytene 67.0 45-129 %REC 1 11/00007 8:14:00 PM

MERCURY, TOTAL SW7470A Analyst RJE Mercury 0.00013 aooo20 J mgA 1 1101/200710:52:00 AM

PAH BY EPA 8270C SW8270C Analyst DG Naphtha^ 2.7 10 J van. 1 11«2Q07 7:16A) PM

BDL 10 van. 1 11/tt2007 7:18:00 PM Pyrene BDL 10 van. 1 11/00007 7:18«»PM Benz(a)anthracene BDL 026 van. 1 11A0007 7:16:00 PM Chrysene BDL 10 van. 1 11/00007 7:18:00 PM Benzo(b)fluoraiithene BDL 0.17 van. 1 11/00007 7:18:00 PM Benzo(k)fluoranthene BDL 1.7 van. 1 11/B0007 7:18i»PM Benzo(a}pyrene BDL 020 van. 1 11/00007 7:18^)0 PM lnderw<l,2.8<d)pyrene BDL 022 van. 1 11/^2007 7:16i)0PM Da>enz(^}anthracene BDL 020 van. 1 11/00007 7:18d)0PM

Surr NitrabenzeneKl5 43.0 2B«3 %REC 1 11/00007 7:18:00 PM Surr 2-FluGrabiphenyl 35.6 10-56 %REC 1 11/00007 7:18:00 PM

Surr. p-TerphenyM14 33.5 10^ %REC 1 11/00007 7:18:00 PM

SVOC TEMTATIVELY IDENTIFIED COMPOUNDS Analyst DG Oimethylaniline BDL 10 J 1 11/90007 7:18:00 PM

VOLATILE ORGANIC ANALYSIS SW8260B Analyst HG rvHexane BDL 5.0 van. 1 11/150007 7:51:00AM DicMorQdiftucvQniettiane BDL 5.0 van. 1 11/150007 7:S1d)0 AM Chkranethane BDL 5.0 van. 1 11/150007 7:51ffll AM Vinyl cidGrida BDL 1.0 van. 1 11/1S2007 7:511K}AM Bromomethane BDL 5.0 van. 1 11/150007 7:511)0 AM Chkrathffie 1.3 5.0 J van. 1 11/150007 7:51D0 AM

VOLATILE ORGANIC ANALYSIS SW8260B Analyst MG Acrolein BDL 20 von. 1 11/15^007 7:51«0 AM Acetonitrfle BDL 40 van. 1 11/1S/2OO77:51D0AM Trtddorofluoromelhane BDL 5.0 van. 1 11/15/20077:51D0AM Acetm 25 20 van. 1 11/15/2007 7:51D0 AM l.l-DicMoroethene BDL 5.0 van. 1 11/15/2007 7:51D0 AM Aoylonarile BDL 20 van. 1 11/1S/2007 7:51D0AM kxkvnethane BDL 10 van. 1 11/15^007 7:S1D0 AM Methylene ctiknde BDL 5.0 van. 1 11/15a0077:51ll0AM

BDL 20 van. 1 11/1S/20O77:51£OAM irans-l 2-DicMorDethene BDL 5.0 van. 1 11/1S/20077:51D0AM

7.6 10 J van. 1 11/1S/20077:5in0AM BDL 5.0 van. 1 11/15/2007 7:51 DO AM

Wiyl acetate BDL 10 van. 1 11/15C0077:51D0AM 2-BulanQne BDL 20 van. 1 11/1SS0077:S1D0AM d»-12-DlcMoroethene BDL 5.0 van. 1 11/15«)07 7:51.-00AM BnxracNaramethara BDL 5.0 van. 1 11/15/20077:5100AM

Chtaratom BDL 5.0 van. 1 11/1S/20077:51D0AM 2.2-Oictitaraprapane BDL 5.0 van. 1 11/1S/20O77:S1:00AM 12-Didiioroelhane BDL S.O P8A 1 11/1S/20077:51130AM 1.1.1-Trichloroethane BDL 5.0 van. 1 11/150007 7:51 DO AM 1,1-OichtarQprapene BDL 5.0 van. 1 11/150007 7:51 DO AM Cartion tetrachtaride BDL 5.0 van. 1 11/150007 7:5100 AM Benzene 38 5.0 van. 1 11/1500077:5100 AM Dibromceiiethane BDL 5.0 van. 1 11/1S00077:5100AM 12-0idilorc|)ropane BDL 5.0 van. 1 11/1S00077:5100AM TrUilaroetlwne BDL 5.0 van. 1 11/1500077:5100 AM

BDL 5.0 van. 1 11/1500077:5100 AM 2-Chkrathyldnyl ether BDL 10 van. 1 11/1500077:5100 AM cis-1>Dichlaropfopene BDL 5.0 van. 1 11/15O0077:51:00AM 4-Methy4-2-penianone BDL 20 van. 1 11/1500077:5100 AM

BDL 5.0 van. 1 11/1S00077:S100AM 1.12-TrichtarDethane BDL 5.0 van. 1 11/150007 7:5100 AM Tohnne 3.2 5.0 J van. 1 11/150007 7:5100 AM 1,3Dicirioraprapane BDL 5.0 van. 1 11/150007 7:5100 AM 2-He«anore BDL 20 van. 1 11/150007 7:5100 AM

BDL 5.0 van. 1 11/150007 7:5100 AM 12-OB)romoethane BDL 5.0 van. 1 11/150007 7:5100 AM Tetrxhloraetheiv BDL 5.0 van. 1 11/1500077;5100AM

BDL 5.0 van. 1 11/1500077:5100 AM BDL 5.0 van. 1 11/150007 7:5100 AM

Ethytoaene 20 5.0 J van. 1 11/150007 7:5100 AM nvp-Xylene 2.7 10 J van. 1 11/150007 7.5100 AM Brcmofonn BDL 5.0 van. 1 11/150007 7:5100 AM Styrene BDL 5.0 van. 1 11/15/20077:5100AM

BDL 5.0 van. 1 11/1S00077:5100AM o-Xylene 1.7 5.0 J van. 1 11/1500077:5100AM

BDL 5.0 van. 1 11/1500077:5100AM 2-ChtGrololuene BDL 5.0 van. 1 11/150007 7:5100 AM

Page I of 12 Page 2 of 12

Belmont Labs Date: 29-Nay-07 Belmont Labs Date: 29-Nov-07

VOLATILE ORGANIC ANALYSIS SW8260B 4-Chlaralohjene BDL 5.0 MOA

99.4 32-127 %REC 81.B 32-122 %REC

Surr Totueno^lB 63.7 46-130 %REC 73.3 36-116 %REC

Analyst UG 11/150007 7:511)0 AM 11/150007 7:51DO AM 11/150007 7:51D0 AM 11/1^2007 7:51DO AM 11M50007 7:51D0 AM

CLIENT: Hull and Associates, Inc. Lab Order: 0711329 CUENT: Hull and Associates, Inc. Lab Order: 0711329 Project: COT192 Project: COT192

)ID: 0711329-002

Client Sample ID; COT192:PX58:G 110607:509

Collection Date: 11/6/2007 2:55:00 PM

Matrix: GROUNDWATER

Analyses Result PQL Qiial UniU DF Date Analyzed

PCBS IN WATER SWB0S2 Analyst D6 Arodar1016 BOL 0.20 POA 1 11/20Q007 3:07DO PM An>dor1221 BDL OJO pg/L 1 11/20*2007 3:071)0 PM An)eiQfl232 BDL 0.20 pgA 1 11/20a007 3:07DO PM Aradar1242 BOL 0.20 P0A 1 11/20a007 3:07UO PM Anidor1246 BDL 0.20 MSA 1 11/2CV2007 3:07D0 PM Arodar1254 BDL 0.20 WA 1 11/20«007 3D7flO PM AFodor1260 BDL 0.20 MQA 1 11/20*2007 3D7.-00PM

StfT OecadXarabiphenyl 51.0 35-143 %REC 1 11/20/2007 3:07.00 PM Swr TetrachtanHn-xylene 2.00 37-116 S %REC 1 11/2QS007 3;0700PM

ORGANOCHLORINE PESTICIDES SW&0B1A Analyst: DG Heptacbtar BDL 0.050 MBA 1 11/20C007 3 07.00 PM AUrin BDL 0.050 MBA 1 11/2QS007 3:0700 PM 4.4'-DDT BDL SO MBA 1000 11/100007 6:3200 AM

0 26-172 S %REC 1000 11/100007 6:3200 AM Siar DecacMgobiphenyl 51.0 28-172 %REC 1 11/2QQ007 3:0700 PM

0 45-129 S %REC 1000 11/10«)07 6:3200 AM Surr TetracMinHn-xytene 2.00 45-129 S %REC 1 11/20a007 3:0700 PM

UERCURY, TOTAL SW7470A Analyst: RJE Mereuy 0.00015 0.00020 J mg/L 1 11/21/2007 10:54:00 AM

PAH BY EPA 8270C SW8270C Analyst: OG Naphthalene 96 10 MBA 1 11/9/2007 9:49:00 AM Acenaphthene 17 10 PBA 1 11/9«I07 9:49:00 AM Pyrene 11 10 pgA 1 11/9/2007 9:49:00 AM Benz(a)anlhracene 4.3 0.26 MBA 1 11/9/2007 9:49:00 AM Chrysene 4.2 10 J MBA 1 11/90007 9:49:00 AM Benzo(b)fluoranlhene 42 0.17 pgA 1 11/90007 9:49:00 AM Benzo<k)fluannthene 3.4 1.7 MBA 1 11/90007 9:49:00 AM

1.4 0.20 MBA 1 11/90007 9:49:00 AM lndeno(U.3KxJ)pyrene 1.2 0.22 MBA 1 11/90007 9:49:00 AM DaKnz<a,h)anthrac«ie BDL OJO MBA 1 11/90007 9:49:00 AM

Siar Nitrobenzen&OS 2.92 2063 s %REC 1 11/90007 9:49:00 AM Surr 2-Fluorabq)heny1 20.4 19-56 %REC 1 11/90007 9:49:00 AM StfT p-Terphenyt-d14 11.9 1(L62 %REC 1 11/90007 6:49:00 AM

SVOC TENTATIVELY IDENTIFIED COMPOUNDS Analyst: DG BDL 10 J MBA 1 11/90007 9;46:XAM

VOLATILE ORGANIC ANALYSIS SW82G0B Analyst: UG rvHeiane BDL 50 MBA 10 11/1K007 e:46H0AM Dichtanxfifluaramethane BDL 50 MBA 10 11/1»2007 6:46D0AM

BDL SO MflA 10 11/190007 e:46D0AM VnylcHorida BDL 10 PflA 10 11/190007 8:461)0 AM

Page3ofl2 Page 4 of 12

Belmont Labs Date: 29-Nav-07


Project: COT192 Lab Order: 0711329

VOLATILE ORGANIC ANALYSIS SW82G0B Analyst HG BOL SO POA 10 lina/2007 8:46110 AM

Ctilcroethane BDl. SO 10 11/10/2007 S:46D0 AM

Acrolein BDL 200 VgIL 10 11/19Q007 8:46DOAM

Acetonttrile BDL 400 M9A 10 11/100007 8:46D0 AM BDL SO UOA 10 11/1»20078:46DOAM

Acetone BDL 200 POA 10 11/100007 8:46H0 AM

1.1-DicHaroelhene BOL 50 VIA. 10 11A0O007B:46D0AM

Acrylanitrile BDL 200 vA 10 11/100007 8:461K) AM

lodcniethane BDL 100 vA 10 11/100007 8:46110 AM

Methylene chlonde BDL SO vA 10 11/100007 8:46110 AM

Cartxn disulfide BOL 200 vA 10 11/100007 8:461)0 AM

trans-1i-Dichloroethene BDL 50 vA 10 11/1000078:461)0 AM

BDL too P9A 10 11/100007 8.46D0 AM

LI-DKhtoroethane BDL SO vA 10 11/100007 B:46D0 AM

Vinyl acetate BDL 100 vA 10 11/100007 8:46D0 AM

2-Bia9iane BDL 200 vA 10 11/100007 8:46D0 AM

BDL SO vA 10 11/100007 8:461)0 AM

Bromochlcromelhane BDL SO vA 10 11/100007 8:46D0AM

Chloroform BDL SO P9A 10 11/100007 8:46D0 AM

2L2-Dichloropropane BOL SO vA 10 11/100007 8:46D0AM

1.2-DicHoroethane BDL SO vA 10 11/100007 8:46D0 AM

1.1,1-Trichloroethane BDL so vA 10 11/100007 8:46110 AM

1.1-OichlflrQprcperte BDL 50 vA 10 11/100007 8:461)0 AM

Cartnn tetrachloride BDL SO pgA. 10 11/100007 8:461)0 AM

Benzene 82 SO vA 10 11/100007 8:46D0AM

Dtbramomethana BDL SO vA 10 11/100007 a:461X) AM

1,2-Oichion:ipropane BDL SO vA 10 • 11/100007 6:46D0AM

TricWoroethene BOL 50 vA 10 11/100007 8:46D0AM

BOL SO vA 10 11/100007 B:46D0AM

2-ChloroetlTylUnyi ether BDL 100 vA 10 11/100007 8:46D0 AM

BOL SO vA 10 11/100007 8:46:00 AM

4-Meth)4-2-perUanone BDL 200 vA 10 11/100007 B:46D0AM

BOL SO vA 10 11/100007 6:46D0 AM

1.1,2-Trlchloroethane BDL SO vA 10 11/100007 8.461X) AM

Tduene 76 so vA 10 11/100007 8:461)0 AM

1.3^3ichloropropane BOL so vA 10 11/100007 8:46D0 AM

2-Hexanone BDL 200 vA 10 11/1tf2007 8:46D0AM

BDL SO vA 10 11/160007 8:46110 AM

BOL SO vA 10 11/100007 8:461)0 AM

Tetrachloroethene BDL so vA 10 11/100007 8:46D0 AM

1.l.1,2-TetrachloroethJ» BDL 50 vA 10 11/100007 8:46D0 AM

BDL SO vA 10 11/100007 8:46D0 AM

Elhylbenzffie 530 50 i>A 10 11/100007 8:46D0 AM

m.p-Xylene 1500 100 vA 10 11/10O0076:46D0AM

Bromoform BDL SO vA 10 11/100007 8:46D0 AM

Styrene BOL SO vA 10 11/100007 8:461)0 AM 1.1.2,2-Tetrachloroeth^ BDL 50 vA 10 11/100007 8:46D0 AM

o-Xylene 250 50 vA 10 11/100007 8:46D0AM

Page 5 of 12

Belmont Labs Date: 29-Nov-07

CLIENT: Hull and Associates, Inc. Lab Order: 0711329 Project: con 92

VOLATlLf ORGANIC ANALYSIS

2-Chlarataluene 4-Chlarotaluene

Surr OaranaA Surr U-Did*rathane-d4 Sivr Tobena^lS Surr 4-BranxAjuiJtMnzene

SW8260B Analyst UG BDL 50 vA 10 11/100007 8:46110 AM

BDL 50 vA 10 11/100007 8:46D0AM

BDL 50 vA 10 11/100007 8:46D0 AM

63.8 32-127 %REC 10 11/100007 6:461)0 AM

84.3 32-122 *REC 10 11/100007 6:46D0 AM

86.8 46-130 %REC 10 11/100007 6:46110 AM

66.0 36-116 %REC 10 11/100007 8:46D0AM

Page6ofl2

Belmont Labs Ditc: 29-Nov^7 Belmont Labs Date: 29-Nov-07

CLIENT: Hull and Associates, Inc. Lab Order: 0711329 CLIENT: Hull and Associates, Inc. Ub Order: 0711329 Project: COT192 Project: COT 192

UbID: 0711329-003

Client Sample ID: COT192:FBI :W110607:509 CoUection Date: 11/6/2007 1:10:00 PM

Matrix: GROUNDWATER

Analyses Result PQL Qiul Units DF Date Analyzed

RGBS IN WATER SW8082 Analyst DG Arodor1016 BDL 0.20 UOA- 1 11/9/2007 6:47:00 PM Arod0r1221 BDL 0.20 pgA 1 11/00007 a:47:XPM Arodcr 1232 BDL OiO van. 1 11/B0007 6:47:XPM Arodor1242 BDL 0.20 van. 1 11fflQ007a:47XPM ArDdor124a BDL 0.20 van. 1 11/»20078:47A)PM ArDdor1254 BDL 0.20 van. 1 11/00007 8:47«)PM Arodar1260 BDL 0.20 van. 1 11A/20078:47tt)PM

Surr Decachlorobiphenyl 67.0 35-143 *REC 1 11/00007 8:47XPM Sum Tetrachloro-m-xylene 63.0 37-116 %REC 1 11/00007 8:47A)PM

ORGANOCHLORINE PESTICIDES SW8081A Analyst DG Heptachlor BDL 0.050 van. 1 11A0007 8:47:mPM AUiin BDL 0.D50 van. 1 11/90007 6:47XPM 4.4--DDT BDL 0.050 van. 1 11/»2007 6:47:XPM

Sum Decachlorobiphanyt 67.0 26-172 %REC 1 11A0007 6:47XPM Sum. Tetrachtoro-m-xytene 63.0 45-129 %REC 1 11/900078:47XPM

MERCURY. TOTAL SW7470A Analyst RJE Mercury BDL 0.00020 mort. 1 1101/200710:Se:XAM

PAH BY EPA8270C SW8270C Analyst: DG Naphthalene 0.14 10 J part. 1 11/00007 6:340) PM Acenaphthene BDL 10 pgfl. 1 1100007 6:34:XPM Pyrene BDL 10 van. 1 11/90007 6:34.iDPM Benzta)anthrac8ne BDL 0.26 van. 1 11/90007 6;34XPM Chrysene BDL 10 van. 1 11/00007 6:34XPM Benzo(b)flucranthene BDL 0.17 van. 1 11/00007 6:34fl)PM Beftta(k)Buoranltier>e BDL 1.7 van. 1 11/B0007B;34XPM Benzo(e)pyrene BDL 0.20 van. 1 11/90007 6;34XPM

BDL 0.22 van. 1 11/00007 6:34XPM Dibenz(a.h)anthracene BDL 0.20 van. 1 11/00007 6:34:MPM

Sum NltrobenzeneOS 45.0 2fr«3 *REC 1 11/B00076:34:XPM Sum 2-RuarDblpteiy1 41.6 19-56 %REC 1 11^2007 6:34iX)PM Siar p-Terphenyf-d14 46.5 10B2 %REC 1 11/^2007 6:34D0PM

SVOC TENTATIVELY IDENDHED COMPOUNDS Analyst DG Oimethyfanaine BDL 10 J pafl- 1 11/W2007 6:34.x PM

VOLATILE ORGANIC ANALYSIS SW8260B Analyst MG rt-Hexane BDL 5.0 pgA 1 11/1S0007 700:00 AM Didilorodifluoromethane BDL 5.0 van. 1 11/1M007 700XAM Chloromelhane BDL 5.0 van. 1 11/1&2007 700XAM Vnyl chloride BDL 1.0 van. 1 11/1S0007700DOAM Bromomethane BDL 5.0 van. 1 11/150007 7001)0 AM Chloroethane • BDL 5.0 van. 1 11/1^2007 70000 AM

VOLATILE ORGANIC ANALYSIS Acrolein

TrictilGrQBuaramethane

l.l-Ochlaroethene Aoykntrile tadometfiane Methylene cHorUe Cwlxn dsutfide trans-U-Dlchtooelteie

Methyl totbutyl ether

1.1-t WiylB 2-ButanQne

ds-U-Dichloroethene

BromoctilorQmethane Chtorafonn

2^-DkMorflf)rapane

12-0idiloroethane

I.LI-TrkMoroethane l.l-OicMoroprofiew CartMnletracMoride

Dteomantethane 1.2-Oichiaraprapane Trichkrattow BromodicHoramethm 2-Chiaroethyl unyt ether d»-1.M3ichlarDpraper« 44tethyt-2-pentanone trans-1.3-Didiloropropene I.U-Trichloroelhm Toluene 1.3-Oictdaroprapane

2-HexBrm

DaranochloramethBne

t^-Uiranoethane

SW8260B Analyst HG BDL 20 van. 1 11/1S«XI7 7:20DOAM

BDL 40 van. 1 1in5Q007 7i0D0AM BDL 5.0 van. 1 11/1Sa0O7 7:20.D0AM BDL 20 van. 1 11/15^007 720D0 AM

BDL 5.0 van. 1 11/15/2007 7:20D0 AM BDL 20 van. 1 11/150007 7:20.D0 AM

BDL 10 van. 1 11/150007 700.110 AM

BDL 5.0 van. 1 11/150007 70ODO AM

BDL 20 van. 1 11/150007 70O.1M) AM

BDL 5.0 van. 1 11/150007 7001)0 AM

BDL 10 van. 1 11/150007 70ODO AM

BDL 5.0 van. 1 11/150007 70ODO AM BDL 10 van. 1 11/150007 7:2OD0 AM BDL 20 van. 1 11/150007 7:2DD0 AM

BDL 5.0 van. 1 11/150007 70ODO AM

BDL 5.0 van. 1 11/150007 70ODO AM

BDL 5.0 van. 1 11/150007 7:20DO AM

BDL 5.0 van. 1 11/150OO770OHOAM BDL 5.0 van. 1 11/150007 700.00 AM

BDL 5.0 van. 1 11/150007 70ODO AM BDL 5.0 van 1 11/150007 7001)0 AM

BDL 5.0 van 1 11/150007 70ODO AM

BDL 5.0 van 1 11/150007 70ODO AM BDL 5.0 van 1 11/150007 7:20D0 AM BDL 5.0 van 1 11/150007 70ODO AM

BDL 5.0 van 1 11/150OO770O:OOAM

BDL 5.0 van 1 11/150007 7:2OD0 AM BDL 10 van 1 11/150007 70ODOAM

BDL 5.0 van 1 11/150OO770ODOAM BDL 20 van 1 11/150007 7-0ODO AM BDL 5.0 van 1 11/150007 7-0ODO AM BDL 5.0 van 1 11/150007 700:00 AM 2.2 5.0 J PBA 1 11/150007 700110 AM

BDL 5.0 van 1 11/150007 70ODO AM BDL 20 van 1 11/150007 700:00 AM BDL 5.0 van 1 11/1S0OO770ODOAM BDL 5.0 van 1 11/150007 70ODO AM BDL 5.0 van 1 11/150007 70ODO AM BDL 5.0 van 1 11/150007 70ODO AM

BDL 5.0 van 1 11/150007 700110 AM BDL 5.0 van 1 11/150007 700110 AM

2.0 10 J pgA. 1 11/150007 70ODO AM BDL 5.0 van 1 11/150007 70000 AM

BDL 5.0 van 1 11/150007 700.00 AM

BDL 5.0 van 1 11/150007 70000 AM 1.2 5.0 J pgA 1 11/150007 7:2000 AM

BDL 5.0 van 1 11/150007 70000 AM BDL 5.0 van 1 11/150007 700.00 AM

Page 7 of 12 Page8ofl2


VOUTILE ORGANIC ANALYSIS SW8260B 4-ChlarDtQiuene BOL 5.0 M9rt-

Surr Dbromonuaromethare 67.5 32-127 %REC Surr 12-Dichloroelh»fr<M 79.4 32-122 %REC Surr TduenfrOS 63.4 46-130 %REC

69.9 36-116 %REC

Analyst HG 11/15«)07 720.1X)AM 11/150007 7i0i)0 AM 11/150007 720:00 AM 11/150007 720i)0 AM 11/150007 720:00 AM

CLIENT: Hull and Associaies, Inc. Lab Order: 0711329 CUENT: Hull and Associates, Inc. Lab Order: 0711329 Project: COT 192 Project: COT 192

Lab ID: 0711329-004 Client Sample ID: C0TI92:TB1:WI 10607:509

Collection Date:

Matrii: TRIP BLANK

Analyses Result PQL Qual Units DF Date Analyied

VOLATILE ORGANIC ANALYSIS SVV8260B Analyst UG n-Hexana BOL 5.0 TOfl- 1 11/15/2007 6:46:00 AM

BOL 5.0 P9rt- 1 11/150007 6:4800 AM CMoramethane BOL 5.0 WA 1 11/150007 6:4600 AM Vinyl cNoride BOL 1.0 fOA 1 11/150007 6:4800 AM Bronnnettune BOL 5.0 U9A 1 11/150007 6:4600 AM Chloraethane BOL 5.0 WA 1 11/1500076:4800AM Aadein BOL 20 P9A 1 11/150007 6:4600 AM Acetonitrfle BOL 40 MA 1 11/1500076:4800AM

BOL 5.0 M9A 1 11/1S00076;46.00AM Acetone BOL 20 pgA 1 11/1500076:46.00AM 1,1-DkMoraethena BOL 5.0 MA 1 11/1S00076:4800AM Acrylantrfle BOL 20 WA 1 11/1500076:4600AM lodameihane BOL 10 WA 1 11/150007 6:4600 AM Methylene crdoride BOL 5.0 UQA 1 11/1500076:4800AM Oban disiSftle BOL 20 iigA 1 11/1S00076:4600AM

BOL 5.0 MA 1 11/150007 6:4800 AM Methyl tan-butyl ether BOL 10 WA 1 11/1500076:4600AM 1.1-OkMoroethane BOL 5.0 MA 1 11/150007 6:4800 AM Vinyl acetate BOL 10 MOA 1 11/1500076:48.00AM 2-Butanane BOL 20 irgA 1 11/150007 6:46.00 AM ds-12-Dkhloroethene BOL 5.0 MA 1 11/150007 6:4600 AM

BOL 5.0 MA 1 . 11/1500076:4600AM Chtaroform BOL 5.0 U9A 1 11/150007 6:4600 AM

BOL 5.0 P9A 1 11/1500076:4800AM BOL 5.0 MA 1 11/1S00076:4600AM

1.1.1-Trlctrianiethm BOL 5.0 M9A 1 11/15/2007 6:4600 AM BOL 5.0 MA 1 11/150007 6:4600 AM

Cartxn tetrachloride BOL 5.0 POA 1 11/1SO0D76;46O0AM Benzene BOL 5.0 P0A 1 11/1500078:4600AM

BOL 5.0 MOA 1 11/1S00076:46.00AM BOL 5.0 MOA 1 11/150007 6:4600 AM

Trichioroethene BOL 5.0 M0A 1 11/15O0076:4flO0AM Bnmodichloraniethartt BOL 5.0 MOA 1 11/150007 6:46.00 AM 2-Chlaroelhyl vinyl ette BOL 10 POA 1 11/1S00076:4600AM

BOL 5.0 pflA 1 11/150007 6:46.00 AM 44wlethyt^2-pentanane BOL 20 POA 1 11/150007 6:46-00 AM

BOL 5.0 POA 1 11/150007 6:4600 AM 1.12-Tricrtorodhane BOL 5.0 POA 1 11/1500078:46.00AM ToAiene BOL 5.0 poA 1 11/150007 6:4600 AM 1.3-Dk:hlarapnv>aw BOL 5.0 poA 1 11/1500076:48:00 AM 2-Hexanane BOL 20 POA 1 11/150007 6:4600 AM Dtttfonnchianxnethane BDL 50 POA 1 11/1500076;4600AM 12^ftwitocthane BOL 5.0 P9A 1 11/150007 6:4600 AM

Pagc9ofJ2 Page 10 of 12


VOLATILE ORGANIC ANALYSIS S W8260B Analyst MG TetracNoroethene BDL 5.0 POA 1 11/1Sa0076:48:00AM 1.1.1,2-TetrBchloroelhane BDL 5.0 WA 1 1in5aoa76:46:OOAM Chkaobenzene BDL 5.0 P9A 1 11/15«I076:48D0AM Ethylbenzene BDL 5.0 WA 1 11/1»0a7e:4SA)AM m.p>Xylene BDL 10 pgA 1 11rt5O0076:4ei)0AM Brcmolonn BDL 5.0 WA 1 11/15^1076:48:00 AM Styrene BDL 5.0 MOA 1 11/1»0076:46DOAM 1.1,2,2-Tetractiknethane BDL 5.0 POA 1 11/15/2007 6:48:00 AM o-Xytew BDL 5.0 POA 1 11/15B0076:48«)AM Bromcbenzene BDL 5.0 POA 1 11/150007 6:48:00 AM 2-Chlcratduene BDL 5.0 P9A 1 1VI 500076:48:00 AM 4-Chlarotcluene BDL 5.0 PftfL 1 11/15O0076:48:00AH

S3.4 32-127 %REC 1 11/1»0076:48XK>AM Surr U-DichlcroetharwKM 76.5 32-122 %REC 1 11/15O0076:48a0AM SumTduenfrdS 79.1 46-130 %REC 1 11/1SO0076:48D0AM Surr 4-Bromofluorobenzen8 662 36-116 %REC 1 11/1500076:48:00 AM

CLIENT: Hull and Associates, Inc. Lab Ordcn 0711329 CUENT: Hull and Associates, Inc. Lab Order: 0711329

Project: COT192 Project; COT 192

Data Qiialifien (Flags)

! See Case Namiive * VoliK exceeds Maximum Contaminant Level A Silica gel analysis not perfonned hrcniisr the total oil and grease is less than detectable limits B AnaJyie delected in the Bssodaied Method Blank

BDL Below Detection limit C Sample result confuined reanalysis E Value above quanihatioiran^ F Unable to obtain a reliable result due to matrix interference H Analysis completed outside holding times J AnaJyie detected below quantitation limits, estimated cotKcnlraiian for TlCs K Result from method of standard additians N Presumptive evidence of analyte present

NG No growth P Sample preservation does not meet method requiremenu

PQL Practical Quantitation Limit or sunogale S Surrogate recovery outside acceptance limits V Calibration oiteria exceeded, but acceptable by method

Pagell ofl2 Page 12 of 12

Belmont Labs Date: 2I-Nov-07

CLIENT: Hull and Associates, Inc. Work Order: 0711329 Project: COT 192


Sample ID: MB-15846 SampType: MBLK TestCode: PAH_8270_W Units: poA Prep Date: 11/8/2007 RunNo: 64244

Client ID: 77777 Batch ID: 13B47 TostNo: SW8270C (SW3510C) Analysis Date: 11/9/2007 SeqNo: 820166

Analyta Result PQL SPK value SPKRefVal %REC LowUmll HighUmIt RPDRefVal %RPD RPDUmIt Qua)

Naphthalene SDL 10

Acenaphthene BDL 10 Pyrene BOL 10

Banz(a)anthrac8ne BDL 0.26 Chryaene BDL 10

Benzo(b)fluoranth6ne BDL 0.17

BDL 1.7

Benzo(a}pyrene BDL 0.20

Indeno(1.2.3-cd)pyron0 BOL 0.22

0Ibenz(a,h)anthrac8na BDL 0.20 Surr Nltrobenzene^S 23.42 0 40 0 56.6 20 63 0 0

Surr 2-FIuoroblphenyt 17.48 0 40 0 43.6 19 58 0 0 Surr p-Terphenyl-d14 20.33 0 40 0 50.6 10 62 0 0

Sample ID: LCS-15848 SampType: LC3 TestCode: PAH_8270,W Units: MBA Prep Date; ii/anoo7 RunNo: 64244

Client ID: ZZZZZ Batch ID: 19847 TestNo: SW8270C (SW3910C) Analysis Dale: 11/9/2007 SeqNo: 820167

Analyta Result PQL SPK value SPKRefVal %REC Lov^mlt HlghUmit RPDRefVal %RPO RPDUmll Qual

Acanaphthana 80.75 10 100 0 60.6 64 103 0 0

Pyrene 103.2 10 100 0 103 35 107 0 0 E

Surr Nllrobanzana-dS 19.35 0 40 0 48.4 20 63 0 0 Surr 2-Ruorot)lphanyl 21.18 0 40 0 53 19 58 0 0

Sum p-Tarphanyl-dU 23.63 0 40 0 59.1 10 62 0 0

Sample ID: LCSD-1SB46 SampType: LCSD TestCode: PAH_a270_W Units: pgn. Prep Date: 11/8/2007 RunNo: 64244

Batch ID: 15847 TestNo: SW8270C (SW3910C) Analysis Date: 11/9/2007 SeqNo: 820160

Analyta Result POL SPK value SPKRefVal %REC LowUmIt HIghUmIt RPDRefVal %RPD RPDUmIt Qual

Acenaphthene 84.12 10 100 0 64.1 64 103 80.75 4.09 14

Pyrene 92.42 10 100 0 92.4 35 107 103.2 11.1 13

22.66 0 40 0 56.6 20 63 0 0 0

Page 2 of 13

Belmont Labs Date: 2l-Nov'07

CLIENT: Work Order:

Hull and Associates, Inc. 0711329


Project: COT192 TestCode: HG_GW

Sample ID: MB-15971

Client ID: 72ZZZ

SampType: MBLK

Batch ID: 19971

TestCode: HO.GW

TestNo: SW7470A



RunNo; 64615

SeqNo: 825669

Analyta Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmit RPDRefVal %RPD RPDUmIt Qual

Mercury BDL 0.00020

Sample ID: LCS-15g71

aient ID: ZZZZZ

SampType: LOS

Batch ID: 19971

TestCode: HQ_GW

TestNo: SW7470A

Units: mgA Prep Dole: 11/21/2007

Analysis Data; 11/21/2007

RunNo: 64615

SeqNo: 829666

Anelyte Result PQL SPK value SPK RefVai %REC LowUmIt HighUmIt RPDRefVal %RPD RPDUmIt Quel

Mercury 0.006010 0.00020 0.00625 0 96.2 80 120 0 0

Sample ID: LCSD-15971

Qlent ID: ZZZZZ

SampType: LCSD

Batch ID: 19971

TestCode: HG.GW

TestNo: SW7470A

Units: mgA Prep Date: 11/21/2007


RunNo: 64619

SeqNo: 825672

Analyta Result PQL SPK value SPK RefVal %REC LowUmit HlghUmit RPDRefVal %RPD RPDUmIt Qual

Mercury 0.005670 0.00020 0.00625 0 90.7 80 120 0.00601 5.82 20

Sample ID: Q71132B-003B MS

Client 10; COT192:FB1:W1106

SampType: MS

Batch ID: 15971

TestCode: HG.GW

TestNo: SW7470A



RunNo; 64619

SeqNo: 829870

Anelyte Result PQL SPK value SPK RefVal *REC LowUmIt HIghUmIt RPDRefVal %RPD RPDUmll Qua!

Mercury 0.005950 0.00020 0.00625 0 95.2 70 130 0 0

Sample ID: G711329-003B MSD

Client ID: COT102:FB1:W110e

SampType: MSD

Batch ID: 15971

TestCode: HG.GW

TestNo: SW7470A

Units: mgn. Prep Date: 11/21/2007

Analysis Data; 11/21/2007

RunNo: 64619

SeqNo: 829671

Anelyte Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmit RPDRefVal %RPD RPDUmIt Qual

Mercury 0.006040 0.00020 0.00625 0 06.6 70 130 0.00595 1.50 30

Page J of 13

ielmont Labs Date: 2I-Noy-07

•LIENT: Vork Order: roject:

Hull and Asaoctates, Inc. 0711329 COT192



Sample ID: MB-1584a SampType: MBLK TestCode: PCB_8Q82_W Units: pgA Prep Date: 11/8/2G07 RunNo: 64239

:ilent ID: 77777 Batch ID: 19848 TestNo; SWaoaZ (SW351QC) Analysis Date: 11/B/2007 SeqNo: 820081

^nalyte Result PQL SPK value SPK Ref Val %REC LowUmll HighUmIt RPDRefVal %RPD RPDUmlt Quel

\rodor1016 BDL 0.20 ^rodor1221 BDL 0.20 \rodor 1232 BDL 0.20 ^rodor1242 BDL 0.20 \rodor1248 BDL 0.20

^rodor1254 BDL 0.20 ^n)dor1260 BDL 0.20

Sum Decachlorot)lphenyf 0.9000 0 1 0 00 35 143 0 0 Sum Tetrachlcro-m-xylene 0.8900 0 1 0 65 37 118 0 0

Sample ID: LCS-19B48 SampType: LC3 TestCode: PCB_80B2_W Units; port. Prep Date: 11/8/2007 RunNo: 64239

laienl ID: 77777 Batch ID: 19848 TestNo: SWa082 (SW3910C) Analysis Date: 11/9/2007 SeqNo: 820082

^natyte Result PQL SPK value SPK Ref Val %REC LowUmlt hUghUmit RPDRefVal %RPD RPDUmlt Qual

Xredor 1016 10.14 0.20 10 0 101 72 lie 0 0 Vfodor 1260 7.990 0.20 10 0 70.9 64 132 0 0

0.9700 0 1 0 97 35 143 0 0 Sum Tetrachloro-m-Kylene 0.8800 0 1 0 88 37 116 0 0

Sample ID: LC3D-1S84a SampType; LC3D TestCode: PCB_8082_W Units: poA Prep Date: 11/8/2007 RunNo: 64239

:ilent ID: ZZZZZ Batch ID: 15840 TestNo: SW8062 (3W3910C) Analysis Date: 11/9/2007 SeqNo: 820083

knatyte Result PQL SPK value SPK Ref Val %REC LowUmlt HlghUmlt RPDRefVal %RPO RPDUmlt Qual

krociorlOIS 11.13 0.20 10 0 111 72 119 10.14 9.31 20 Uodor1260 6.180 0.20 10 0 81.8 84 132 7.99 2.35 19

Sum Decachloroblphenyl 0.6600 0 1 0 66 35 143 0 0 0 Sum TetrachlorcHn-xylene 0.8500 0 1 0 65 37 116 0 0 0

Page 4 of 13

)elmont Labs

LIENT: Hull and Associates, Inc. i'ork Order: 0711329 roject: COT192

Date: 2i-Nov-07


TestCode: PAH 8270 W

lample ID: LCSD<1S046

;ilentlD: ZZZZZ

Uialyta

SampType: LC30

Batch ID: 1SB47

TestCode: PAH^82rO_W Units: poA

TeatNo: SW6270C {SW3510C)

PQL SPK value SPK Ref Val



%REC l.awUmlt HlghUmlt RPDRefVal

RunNo: 64244

SeqNo: 820189

%RPD RPDUmlt Qua!

Surr 2-Ruoroblphenyl

Sum p-Terphenyt-d14 19.93

19.89

40

40

19 10

58

62

Page 3 of 13

Belmont Labs Date: 2l-Nov-07

CLIENT: Work Order: Project:

Huil and Associates, Inc. 0711329 COT192


Sample ID; M8LK SampType: MBLK TestCode: VOC_8260_W Units: MB^. Prep Date: RunNo: 64499

aient ID; 77777 Batch ID; R64499 TestNo: SW8260B Analysis Date: 11/15/2007 SeqNo: 824091

Analyte Result PQL SPK value SPKRefVal %REC LowLlmit HIghUmit RPDRelVal %RPD RPDLImit Qual

n-Hexane BOL 5.0

Diehlorodlfluoromathane BDL 5.0 Chloromethane BDL 5.0

Vinyl chloride BDL 1.0 Bromomethane BDL 5.0

Chlofoe thane BDL 5.0 Acrolein BDL 20

Acetonllrlle BDL 40 Trichlorofluoromethane BDL 5.0

Acetone BDL 20 1.1-Dlchloroethene BDL 5.0

Aoylonitrile BDL 20

lodomelhane BDL 10

Methylene chloride BDL 5.0

Caiton disulfide BDL 20

BDL 5.0

Methyl lert-butyl ether BDL 10

1.1-Olchloroethane BDL 5.0 Vinyl acetate BDL 10 2-Butanone BDL 20 d8-1,2-Dlchloroethene BDL 5.0

Bromochloromethane BDL 5.0 Chloroform BDL 5.0

2,2-Olchloropropane BDL 5.0

1,2-Dichtoroe thane BDL 5.0 1.1.1-TrichlorDe thane BOL 5.0 1,1-Dlchloropropene BDL 5.0 Caiton tetrachloride BDL 5.0 Benzene BDL 5.0

BDL 5.0 1.2-Olchloropropane BDL 5.0

Page 6 of 13


CLIENT: Hull and Associates, Inc. Work Order: 0711329 Projeet: COT192


Sample ID: MB-1984a SampType: MBLK TestCode: PE3T_8081_ Units: pg/L Prep Date: 11/8^007 RunNo: 64239

Client ID: 77777 Batch ID: 19848 TestNo: 3WB0aiA (SW3910C) Analysis Date: 11/9^007 SeqNo: 820076

Analyta Result PQL SPK value SPKRefVal %REC LowLImIt HIghUmit RPD Ref Val %RPD RPOUmit Qual

Heptachlor BDL 0.050

Aldrin BDL 0.050 4.4--ODT BDL 0.050

Surr Decachloroblphenyl 0.9000 0 1 0 90 28 172 0 0 Sum Tetrachlcro-nvxylene 0.8500 0 1 0 85 45 129 0 0

Sample ID: LCS-19848 SampType: LC3 TestCode: PE3T_ea81_ Units: MO'I- Prep Date: 11/8a007 RunNo: 64239

Client ID: 77777 Batch ID: 19848 TestNo: 3W8081A (SW3910C) Analysis Date: 11/9/2007 SeqNo: 820077

Analyte Result PQL SPK value SPKRefVal %REC LowLImIt HIghUmit RPD Ref Val %RPD RPDUmIt Qual

Heptachlor 0.9100 0.050 1 0 91 71 117 0 0

Aldrin 0.8100 0.050 1 0 81 81 107 0 0

4.4'-DDr 0.8100 0.050 1 0 81 41 132 0 0 Surr Decachlorobiphenyl 0.9600 0 1 0 98 28 172 0 0 Surr Tetrachloro-m<xylene 0.8400 0 1 0 84 45 129 0 0

Sample ID: LCSD-19848 SampType: LCSD TestCode: PE3T_B081_ Units: \ialL Prep Date: 11/8nOD7 RunNo: 64239

Client ID: 77Z3Z Batch ID: 19848 TestNo: SWB081A (SW3910C) Analysis Date: 11/9/2007 SeqNo: 820078

Analyte Result PQL SPK value SPKRefVal %REC LowUmlt HIghUmit RPD Ref Val %RPD RPDLImit Qual

Heptachlor 0.9400 0.050 1 0 94 71 117 0.91 3.24 17

Aldrin 0.8400 0.050 1 0 84 61 107 0.81 3.64 12

4,4--DDT 0.8800 0.050 1 0 86 41 132 0.81 5.99 19

Surr Decachlorotilphenyl 0.9700 0 1 0 97 28 172 0 0 0

Surr Tetrachloro-m-xylene 0.8300 0 1 0 83 45 129 0 0 0

Page 5 of 13

elmont Labs Date: 2l-Nov-07

LIENT: Hull and Associates, Inc. ork Order: 0711329 •oject: COT192

ANALYTICAL QC SUMMARY REPORT TcstCode: VOC 8260 W

ample 10: MBLK

lleni ID:

nalyta

SampType: MBLK

Batch ID: R64S41

TestCode: VOC_B260.W Units: pgR.

TestNo: SW8260B


Prep Date:


HREC LowLlmIt HlghUmll RPORefVal

RunNo; 64941

SeqNo: 824776

%RPO RPDUmit Qual

•Hexane

Ichlorodlfluofomethane

hloromethane

inyl chloride

romo

crolein

cetonitrlle

ichlcroflucromethane

cetone

1-Dlchloroethene

crylonitrlie

domethane

ethylene chloride

artMvi disulfide

ins-1.2-DIchloroelhen8

ethyl tert-butyl ether

1<DlchIoroethane nyl acetate

Butarwne

»'1.2-Dlchloroethene

omochlorDmethana

iloroform

2-DlchlorQpropane

2-Dlchk)roethane

1.1-Trichloroelhane

1-Dlchloropropene

irt)on tetrachloride

inzene

bromomethane

2-Olchloropropane

BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL

9.0

5.0

5.0

1.0

9.0

5.0 20 40

5.0

20

5.0

20

10

5.0

20

5.0

10

5.0

10.

20 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 3.0 5.0 5.0

Pages of 13

elmont Labs

LIENT: ork Order: •oject:

Hull and Associates. Inc. 0711329 COT192

Dale: 2l-NoV'07


ample ID: MBLK

llent ID;

lalyte

SampType: MBLK

Batch ID: R64499

TestCode: VOC.82eO_W Units: pg/L

TestNo: SWa26aB

PQL SPK value SPKRafVal

Prep Date:

Analysis Date; 11/19^007

%REC LowLimlt HIghUmit RPORefVal

RunNo: 84499

SeqNo: 824091

%RPD RPDUmit Qual

iehloroethene

omodlchloromethane

Chloroethyl vlrryl ether

»-1.3-Olchloropropene

Melhyl-2-pantanone ins-1 .a-Dlchlorepropene

1,2-Trtchlaroethane

3lusne

3-OichlofoprQpane

Hexanone

ibromochloromethane

2-Olbromoe thane

strachloroelhene 1,1.2-Tetrachloroethane

Dlorobenzene

hylbennne

.p-Xylene

omoform

yrene 1.2.2-Telrachtaroethane

Xylene

omobenzene

Chiorotoluene

Chlorotoluene

BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL

S.O 5.0 10

5.0 20 9.0 9.0 5.0 5.0 20 5.0 5.0 S.O 5.0 5.0 5.0 10

5.0 9.0 5.0 5.0 5.0 5.0 5.0

Surr DIbromofluoromethane 43.46 0 50 0 86.9 32 127 0 0 Surr 1.2-Dlchloroethane-d4 40.07 0 50 0 80.1 32 122 . 0 0

Sum Toluene-d8 42.10 0 50 0 84.2 48 130 0 0 Sum 4-Bromofluorobenzene 35.27 0 50 0 70.5 36 116 0 0

Page 7 of 13


CLIENT: Hull and Associates, Inc. Work Order: 0711329 Project: COT192



Sample ID: LCS SampType: LCS TestCode: VOC.8260.W Units: pg/L Prep Date: RunNo: 844B9

Client ID: 77777 Batch ID: R64499 TestNo: SW8260B Analysis Date: 11/150007 SeqNo: 824089

Anaiyte Result PQL SPK value SPK RefVal %REC LowUmIt HfghUmit RPD RefVal %RPD RPOUmIt Oual

n-Hexane 19.03 5.0 20 0 98.2 28 146 0 0

1.1-Olchioroethene 16.21 5.0 20 0 81 01 142 0 0 Benzene 18.32 5.0 20 0 91.6 65 132 0 0 Trtchloroethene 23.32 5.0 20 0 117 66 145 0 0 Toluene 19.06 5.0 20 0 95.3 73 127 0 0 Chiorobenzene 19.35 5.0 20 0 98.8 60 123 0 0

SUIT Dlbromofluoromethane 42.82 0 50 0 85.6 32 127 0 0 Surr 1,2-0lchloroethan«14 40.08 0 50 0 80.2 32 122 0 0 Surr Toluene-d8 42.08 0 50 0 84.2 48 130 0 0 Sum 4-Bromofluorobenzene 30.78 0 50 0 73.0 36 116 0 0

Sample ID: LCS SampType: LCS TestCode: VOC.8260_W Units: ngfL Prep Date: RunNo: 64541

Client ID: ZZZZZ Batch ID: R64541 TestNo: SW8260B Analysis Date: 11/19/2007 SeqNo: 824770

Anatyte Result PQL SPK value SPK RefVal %REC LowLImIt HighLimit RPD RefVal %RPD RPDUmil Qual

n-Hexane 14.85 5.0 20 0 74.2 17 123 0 0 1.1-Olchloroetheno 10.23 5.0 20 0 81.2 49 144 0 0 Benzene 14.94 5.0 20 0 74.7 56 120 0 0 Trtchloroethene 15.70 S.O 20 . 0 78.8 56 135 0 0 Toluene 15.35 5.0 20 0 76.8 64 116 0 0 Chiorobenzene 15.07 5.0 20 0 75.4 64 131 0 0

Sum Dlbromofluoromethane 43.38 0 50 0 80.8 32 127 0 0 Sum 1,2-0lchloroethan»14 47.59 0 50 0 95.2 32 122 0 0 Sum TotuenenlS 41.30 0 50 0 82.6 48 130 0 0 Sum 4-6romofluorobenzene 40.98 0 50 0 82 36 116 0 0

Sample ID: LCSO SampType: LCSO TestCode: VOC.8260_W Units: pg/L Prep Date: RunNo: 64499

Client ID: ZZZZZ Batch ID: RB4499 TeatNo: SWB260B Analysis'Data; 11/150007 SeqNo: 824090

Anaiyte Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmlt RPD RefVal %RPD RPDUmIt Qual

n-Hexane 39.39 5.0 20 0 197 28 146 19.03 67.0 10 L

Page 10 of 13


CLIENT; Hull and Associates, Inc. Work Order: 0711329 Project: COT192



Sample ID: MBLK SampType: MBLK TestCode: VOC_8260_W Units: pg/L Prep Data: RunNo: 64541

Batch ID: RB4541 TestNo: SWBZeOB Analysis Date: 11/190007 SeqNo: 824778

Anaiyte Result PQL SPK value SPK RefVal HREC LowUmIt HlghUmlt RPD RefVal %RPD RPDUmIt Qual

Trtchloroethono BromodicMoromethana 2-Chloroethyl vinyl ether de-l .S-DIchioropropena 4-Methyl-2'pentanone trans-1,3-Oichloropropene 1.1.2-Tr1chloroeihane Toluene 1,3-OichiorDpropane 2-Hexanona Dlbromochloromethane 1.2-Dlbromoe thane Tetrachlofoelhene 1,1,1,2-Telrachloroelhane Chiorobenzene Ethylbenzene m,p>Xy1ene Bremoform Styrene 1.1.2.2-Tetrachloroethane o-Xylono Bromobenzene 2-Chlorotoluene 4<)hlorDtoluene

BOL BDL BOL BDL BOL BOL BOL BDL BDL BDL BOL BDL BDL BDL BDL BDL BDL BDL BDL

BDL

BDL BDL

BDL

BDL

5.0

5.0 10

5.0 20 S.Q 5.0

5.0 5.0 20

5.0

5.0

5.0

5.0 5.0

5.0 10 5.0 5.0 5.0 5.0 5.0 5.0 5.0

Sum Dlbromofluoromethane 44.96 0 50 0 89.9 32 127 0 0

Sum 1.2-Dlchloroethane-d4 45.59 0 50 0 91.2 32 122 0 0

Sum Toluene-da 43.57 0 50 0 87.1 48 130 0 0 Sum 4-Bfomonuorobenzene 44.03 0 50 0 68.1 36 116 0 0

Page 9 of n

Belmont Labs Dote: 2l'Nov-07

XIENT: Hull and Associales, Inc. ôrk Order: 0711329 rojecl: COT192

ANALYTICAL QC SUMMARY REPORT TestCodc: VOC 8260 W

^mple ID; SAMPLEMS SampType: MS TeslCode: VOC_8260_W Unite: MOfl- Prep Date: RunNo; 64499

:ilant ID: ZZZZZ " Batch ID: R64499 TeslNo: SWB260B Analysis Date: 11/19/2007 SeqNo: 824114

^natyte Result PQL SPK value SPK RefVal %REC LowLimlt HIghUmft RPORefVal %RPD RPOUmIt Qual

ienzene 16.08 5.0 20 0 80.4 71 125 0 0

rrichioroethene 18.77 5.0 20 0 93.8 67 137 0 0

roluene 18.57 5.0 20 2.09 72.4 75 118 0 0 M tfhiorobenzena 15.78 5.0 20 0 78.9 87 106 0 0 M

Surr Dlbromofluoromethane 40.97 0 50 0 81.9 32 127 0 0

SUIT 1.2-Dlchloroethane-d4 38.78 0 50 0 77.8 32 122 0 0 SUIT Toiuene-dB 40.10 . 0 50 0 80.2 48 130 0 0

34.37 0 SO 0 68.7 36 118 0 0

iample ID: SAMPLEMSD SampType: MSD TestCode: VOC_B2BO_W Units: HQ/L Prep Date: RunNo: 64499

Batch ID: R64499 TestNc: SW8260B Analysis Date; 11/19n007 SeqNo: 624115

Vnalyta Result PQL SPK value SPKRofVal *REC LowUmIt HghUmlt RPDRefVal %RPD RPDUmIt Qual

tâxane lfl.47 5.0 20 0 92.4 70 130 18.31 0.870 25

l,1-Dlch1oroethane 14.60 5.0 20 0 73 65 135 14.3 2.08 11

lenzene 16.30 9.0 20 0 81.5 71 125 18.08 1.36 10

filctiloroethene 18.10 5.0 20 0 90.5 67 137 18.77 3.63 10

'oluene 18.17 9.0 20 2.09 70.4 75 118 18.57 2.44 10 M ^loiDbenzana 15.39 9.0 20 0 77 87 106 15.78 2.50 10 M

42.08 0 90 0 84.1 32 127 0 0 0 Surr 1.2-Dichioroelhan»^4 39.48 0 50 0 79 32 122 0 0 0 Sum Tduena-dB 40.n 0 50 0 81.5 48 130 0 0 0 Sum 4-Bromofluoreban2Bne 35.38 0 90 0 70.8 38 116 0 0 0

Page 12 of 13

lelmont Labs Date: 2I-Nov-07

LIENT: Hull and Aasocintea, Inc. r-ork Order: 0711329 roject: COT192

ANALYTICAL QC SUMMARY REPORT TeslCode: VOC 8260 W

iample ID; LCSD SampType: LCSD TestCode: VOC_B260_W Units: pg/L Prep Date: RunNo: 64499

atent ID: 77777 Batch ID: R64490 TestNo: SWB260B Analysis Date: 11/15«007 SeqNo: 824090

âlyte Result PQL SPK value SPK RefVal *REC LowUmIt HlghUmlt RPDRefVal KRPD RPDLImtt Qual

i.1-0lchloroethene 11.60 9.0 20 0 58 61 142 18J21 33.2 14 L

enzene 17.85 5.0 20 0 89.2 65 132 18.32 2.60 10

/tchloroethsne 23.12 9.0 20 0 118 66 145 23.32 0.861 14

oluene 18.48 9.0 20 0 92.4 73 127 19.06 3.09 12

^lorebenzene 19.20 5.0 20 0 96 60 123 10.35 0.778 10

Sum Dltmmofluofomethane 40.57 0 50 0 81.1 32 127 0 0 0 Sum 1,2-Dlchloroethane-d4 38.62 0 SO 0 77.2 32 122 0 0 0

Sum Toluene-d8 39.64 0 50 0 79.3 48 130 0 0 0

Sum 4^romofluorebenzene 34.72 0 50 0 69.4 36 116 0 0 0

Iample (D: LCSD SampType: LCSD TestCode: VOC.8260_W Units: mlL Prep Date: RunNo: 64541

'Jlent ID: Z22ZZ Batch ID: R64541 TestNo: 8Wa260B Analysis Date: 11/19/2007 SeqNo: 824771

nalyte Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmlt RPDRefVal %RPD RPDUmll Qual

Kîexane 14.11 5.0 20 0 70.9 17 123 14.65 5.11 18

.1-DlchlorDethono 18.36 9.0 20 0 81.8 49 144 16.23 0.796 14

enzene 14.96 5.0 20 0 74.8 56 120 14.94 0.134 10

15.03 5.0 20 0 75.2 56 135 15.76 4.74 14

oluene 19.59 5.0 20 0 77.8 64 116 15.35 1.29 12

.hlorottenzene 15.36 9.0 20 0 76.8 64 131 15.07 1.91 10

42.93 0 50 0 65.9 32 127 0 0 0

Sum 1,2-Olchloroethane-d4 44.52 0 SO 0 89 32 122 0 0 0

Sum Toluene-d8 42.42 0 so 0 84.8 48 130 0 0 0

Sum 4^rofno8uorobenzBne 41.01 0 50 0 62 36 116 0 0 0

ample ID: SAMPLEMS SampType: MS TestCode; VOC_8260_W Units: pgA. Prep Date: RunNo: 64499

-llent ID: 77777 Batch ID: R64499 TestNo: SWB260B Analysis Date: 11/15/2007 SeqNo: 824114

nalyte Result PQL SPK value SPK RefVal %REC LowUmIt HlghUmlt RPDRefVal %RPD RPOUmIt Qual

•Herane 18.31 5.0 20 0 91.6 70 130 0 0

,1-Dlchloroethene 14.30 5.0 20 0 71.5 69 135 0 0

Page 11 of 13

HUM Crtl

iates, inc.

nOubltn. QH nindtonapQ»B. IN HMaaan. OH 6397EnwraMPvtway e330E.759iSL 4900PadmayDr. 6161 CoeftrwiRoad *' 3401 GlandataAm Sulla 200 SuSaira SuilalOO SdtaD SidlaSOO OuMft. OH 43016 IndlanapeCa. (N 46380 Maaen, OH 46040 Solan, OH 44139 Italado. OH 43814 Phona: (814) 7SM777 Phena: (317) 656-0686 Ptana: (513)4S9'0677 Pitona: (440)019-2699 Phona; (419)369-2010 Fac (614) 7934070 Fax: (317) 6564993 ' FOE (613)46M888 Fax:(440)619-2960 Fax:(419)309-9487

CHAIN OF CUSTODV RECORD

âtado. OH

PAGE _Z_ 'OFJ-

NO. 015 too

REPORT TO- Ajartz-i

z PRESERVATIVES

Client nf T" !f ^ site; jr^ Aye.. ! Project ft Phase: oC. iy

it^llLC dUrreL../

/L / ANALYSES ~7

/W/p./A.M/ / ./ / ./ ./I7

PROJECT SAMPLE SAMPLE NO. LOCATUM TYPE A ID

NO, Of

CONT. METALS

COltECnON / / DATE/nHE / / 7vv//// / / COMMENTS

cvnsi. • /'ys--; =c//oi:vo-^ H - , 1 1 1 >

c.'T')9L. • PieiTti !C;i "LoJ-. f.-<7 •j' N liu-y) - 1. I 1 1

'' Pi%l • 1 f-S <r z. 1 / t

'• TPl u ") : ia 7 z. H z. 1 1 1

: : ^ ' ( ; .

J / \

• ;• : ; • •

REUNQUtSHB) BVl ^ OATB: /Z/z/e/i RECEIVEOBV: ' DATt J//U^ J / REUNQUtSHB) BVl ^

TIME:

RECEIVEOBV: '

TtME: •

•\v'ao^ DATE:

TIME:

RECE1VEDBY1 ...A .

r,jjR,T REUNQUtSHEDBYl ISATE: RECEIVED FOR LAB BV: DATE: REUNQUtSHEDBYl

TIME:

RECEIVED FOR LAB BV:

TIME:

ASRECEnrED: ^

DiaTRiatmoN: MMHt -uauutMuUBiwniWMDwminiPORr) VILIOW -LMUM

Deliver To: _ZLlZx - »• J '

Method of Delivery: U Pj

Airbill Number

TURN AROUND TIME: _ST^

Data QuaUflen (Flags)

B Analyte delected in the aasocioied Method Blank BDL Below Detection limit

C Sample result confirmed by rean&iyBis E Value obove quintitntion range F Unable to obtain a reliable result due to matrix interference H Analysis completed ouuide holding times J Analyte detected below quantitation limits, estimated concentration Ibr TlCs IC Result from method of standard additions L Uboretory control umple recovery ouuide acceptance limits

Metrix spike end/or matrix spike duplicate recovery outside acceptance limits Presumptive evidence of analyte present Sample i tion does not meet r RPD outside accepted recovery limits Surrogate recovery outiide acceptance Hmiu Calibration criteria exceeded, but acceptable by method

NQ No growth I Sea Cose Narrative

A Silica gel analysii not performed bccauoe the toul oil and g e is leu than detectable limits

Page 13 of 13

Proiect/Facilttv: Sticknev Avenue Landfill Sample Date: l/luf* I Address: City of Toledo. DSW, 3962 Hoffman Rd,Toledo. OH. 43611 Contact David Leffler Telephone: (419)936-2643 Report to: Karen Okonta Billing Addressff'O #:

Sample Type: LEACHATE Q Grab I I Composte

PARAMETERS TO BE ANALYZED

GENERAL AND INORGANICS;

VOCt (for trip blank only)

RGBs

Dimethylaniline

PAHa

haptachlor

atdrin

DDT

Mercury, total .


Samples to be Analyzed by Laboratory Turbidity pH Dissolved Oxygen Ccnductlvily Temperature Rfldox Potential Notas

Monitoring Well Sample ID « mgP. S.U. mg/L umhosfom deg.C mv Notas

PX-58 -c-rm /"S in 4 V/ nv -i-ia PX-89 tii-bo?:,vi T.1-3 i- fcl 3. <•& tCe/O

Field Blank (NOVOCilC-»*''<t f-'') - - - - - - -Trip Blank (VOC» ONLY)'^ iiokoj.r-'l "

• r~i swpups • CUent Pick-up • SIIB Mlwiyff'ick-up H Our Sampling

Sample Conlalnar^ Pmvldad By Belmont Analiplcel Labomtoriei

Submitted by: Received tnr

SAMPLERS: MC:509

X

APPENDIX D

Methane Monitoring Field Data Sheets Containing Gas Probe and Punch Bar Readings Obtained on July 26, 2007, October 31, 2007, and September 7, 2007

> TJ TJ m z g X o

HULL & ASSOCIATES, INC. MARCH 2008 TOLEDO, OHIO COT192.100.0009.DOC

STICKNEY/TYLER LANDFILLS TOLEDO, OHIO

METHANE MONITORING FIELD DATA SHEET

TESTING COMPLETED BY: Mike Charcoal CO2/O2 INSTRUMENT TYPE: GEM - Model No. 500 CALIBRATION GAS: 15%CH^ / 15%C0^

DATE: 07/26/07 DATE LAST CALIBRATED: 07/26/07 SAMPLING METHOD: Air pump

PRESSURE INSTRUMENT TYPE: Maanahelic Gaoe - Model No. 2005

WATER LEVEL INSTRUMENT TYPE: Solinst-Model No. 101

Probe Designation Time of

Sampling Pressure^

Percent Combustible

Gas' %LEL'

Percent Gas'

Punch Bar Results' Time of

Sampling Initial Sus

tained 0, COa Percent Gas'

Percent LEL'

S-GP-1S 11:40 0 0 0 0 3.7 14.2 0 0

S-GP-1D 11:40 0 0 0 0 19.6 0.6 0 0

S-GP-1A 11:50 0 0 0 0 15.0 8.5 0 0

S-GP-2S 14:00 0 0 0 0 18.4 0.2 0 0

S-GP-2D 14:00 0 0 0 0 9.8 0.1 0 0

S-GP-2A 14:07 0 0 0 0 20.5 0.3 0 0

S-GP-10S 13:50 0 0 0 0 21.0 0 0 0

S-GP-10D 13:50 0 0 0 0 17.3 3.8 0 0

S-GP-11S NA NA NA NA NA NA NA 0 0

S-GP-11D NA NA NA NA NA NA NA 0 0

S-GP-12 NA NA NA NA NA NA NA 0 0



BE-BP-01 NA NA NA NA NA NA NA 0 0

BE-BP-02 NA NA NA NA NA NA NA 0 0

T-GP-01S 15:33 0 0 0 0 19.7 1.3 0 0

T-GP-01D 15:33 0 0 0 0 19.8 1.2 0 0

T-GP-02S 15:15 0 8 8 100 14.2 0.5 0 0

T-GP-02D 15:15 0 0 0 0 20.3 0.4 0 0

T-GP-03S 15:00 0 0 0 0 17.3 3.8 0 0

T-GP-03D 15:00 0 0 0 0 20.3 0.3 0 0

T-GP-07S NA NA NA NA NA NA NA 0 0

T-GP-07D NA NA NA NA NA NA NA 0 0

T-GP-07A 11:00 0 0 0 0 1.0 7.2 0 0

T-GP-10S 16:00 0 55 55 100 1.6 30.0 0 0

T-GP-10D 16:00 0 0 0 0 12.3 9.7 0 0





T-GP-15 NA NA NA NA NA NA NA 0 0 Horizontal

Well NA NA NA NA NA NA NA NA NA

Pre-System NA NA NA NA NA NA N A NA NA

Btwn GACs NA NA NA NA NA NA N A NA NA Post-

System NA NA NA NA NA NA NA NA NA

HULL & ASSOCIATES, INC. TOLEDO, OHIO

DECEMBER 2007 COT192.100.0010.DOC

NOTES: 1. All pressure readings are expressed as Inches of H2O 2. All readings are 0-100% gas by volume by air 3. (LEL) Lovwer Explosive Limit 4. All depth measurements are expressed in feet

NA - Not available (Not located) (-) - Not measured

CLIMATOLOGICAL CONDITIONS Ambient Barometric Pressure: 30.01 ( i) Observed Weather Conditions: Cloudv Wind Direction and Soeed: SSW 10-15 moh Relative Humldltv: 64 % Ambient Temperature ( Ft 76 COMMENTS: Punch bar samollna was performed around the oerimeter of the landfill

HULL S ASSOCIATES, INC, DECEMBER 2007 TOLEDO, OHIO COT192.100.0010.DOC



TESTING COMPLETED BY: Rvan Murohv CO2/O2 INSTRUMENT TYPE: GEM - Model No. 500 CALIBRATION GAS: 15%CH^ / IsyoCO^

DATE: 09/07/07 DATE LAST CALIBRATED: 09/07/07 SAMPLING METHOD: Air pump

PRESSURE INSTRUMENT TYPE: Maanahelic Gaae - Model No. 2005


Probe Designation Time of

Sampling Pressure*

Percent Combustible

Gas' %LEL'

Percent Gas'

Punch Bar Results' Time of

Sampling Initial Sus-

talned 0, COi Percent Gas'

Percent LEL'

S-GP-1S ~ - ~ ~ - - - -- -

S-GP-1D - - - ~ - - - - -

S-GP-1A - - - - - - - - -

S-GP-2S ~ - - - - ~ ~ - -

S-GP-2D - ~ - - - - - - -

S-GP-2A - - - - - - - - -

S-GP-10S - - ~ - - - - - -

S-GP-10D ~ - - - ~ - - - -

S-GP-11S - - - - ~ ~ - ~ -

S-GP-11D - - - - - - ~ - -

S-GP-12 - - - - - - - ~ -

S-GP-14 - - - - - - ~ - -

S-GP-15 - ~ ~ - - - - ~ -

BE-BP-01 - ~ - ~ - - - ~ ~

BE-BP-02 - - ~ - - - - - -

T-GP-01S - - - - - - ~ - -

T-GP-01D _ _ — — _ — — — —

T-GP-02S 07:30 ~ 0.2 0.2 0 14.6 0.1 — —

T-GP-02D 07:30 - 0 0 0 19.9 1.0 ~ -

T-GP-03S • - - - ~ ~ ~ - ~ -

T-GP-03D - - - - - - - - -

T-GP-07S ~ - - - - - - - -

T-GP-07D - ~ - - - ~ - - ~

T-GP-07A - - - - - - - - -

T-GP-10S 09:00 - 61.9 61.9 100 0.2 28.8 - -

T-GP-10D 09:00 - 0 0 0 14.9 6.5 - -

T-GP-11S - - - - - - - - -

T-GP-11D - ~ - - - - - - -

T-GP-12S - - - - - - - - ~

T-GP-12D - - ~ - - - - - -

T-GP-15 - - ~ ~ - - - ~ -

Horizontal Well ~

— — — — — —

Pre-System ~ - - ~ ~ ~ - - -

Btwn GAGs - - - ~ - - - - ~

Post-System - — — — — " — ~

HULL a ASSOCIATES, INC. TOLEDO, OHIO

DECEMBER 2007 COT192.100.0012.DOC

NOTES: 1. All pressure readings are expressed as inches of H2O 2. All readings are 0-100% gas by volume by air 3. (LEL) Lower Explosive Limit 4. All depth measurements are expressed In feet

NA - Not available (Not located) (-) - Not measured

CLIMATOLOGICAL CONDITIONS Ambient Barometric Pressure: 30.01 (i) Observed Weather Conditions: Clear Sunnv Wind Direction and Speed: 1-5 moh Relative Humidity:. Ambient Temperature f"F1 70 COMMENTS:

HULL S ASSOCIATES, INC, DECEMBER 2007 TOLEDO, OHIO COT192.10G.0012.DOC



TESTING COMPLETED BY: Mike Charcoal CO2/O2 INSTRUMENT TYPE: GEM - Model No. 500 CALIBRATION GAS: 15%CH^ / 15%C0y

10/31/07 DATE: DATE LAST CALIBRATED: SAMPLING METHOD: Air pump

10/31/07

PRESSURE INSTRUMENT TYPE: Maonahelic Gaoe - Model No. 2005


1 Probe Designation Time of

Sampling Pressure^

Percent Combustible

Gas' %LEL' Percent

Gas' Depth to Punch Bar Results' Time of Sampling

Initial Sustained 0, COj

Vvcikvl Percent

Gas' Percent

LEL'

S-GP-1S 7:35 0 0 0 0 16.9 3.1 DRY - -

S-GP-1D 7:40 0 0 0 0 16.7 0.7 7.88 0 0

S-GP-1A 7:55 0 0 0 0 16.9 9.0 8.73 0 0

S-GP-2S 8:20 0 0 0 0 9.7 4.7 DRY - ~

S-GP-2D 8:26 1.2 0 0 0 12.6 1.4 3.80 0 0

S-GP-2A 8:35 0 0 0 0 14.9 1.0 DRY - ~

S-GP-10S 8:55 0 0 0 0 14.7 7.6 DRY - -

S-GP-10D 9:02 0 0 0 0 8.7 8.4 DRY - -

S-GP-11S 9:12 0 0 0 0 12.9 6.8 5.18 0 0

S-GP-11D 9:18 0 0 0 0 19.4 0.6 12.81 0 0

S-GP-12 NA NA NA NA NA NA NA NA 0 0



BE-BP-01 NA NA NA NA NA NA NA NA 0 0

BE-BP-02 NA NA NA NA NA NA NA NA 0 0

T-GP-01S 12:15 0 0.5 0 0 20.3 0 5.16 0 0

T-GP-01D 12:11 0 0 0 0 20.3 0 6.39 0 0

T-GP-02S 12:22 0 0 0 0 0.5 17.3 10.39 0 0

T-GP-02D 12:27 0 0 0 0 19.5 0.1 DRY - ~

T-GP-03S 12:45 0 0 0 0 9.4 4.5 DRY - -

T-GP-03D 12:50 0 0 0 0 1.9 7.0 DRY - -

T-GP-07S NA NA NA NA NA NA NA NA 0 0

T-GP-07D NA NA NA NA NA NA NA NA 0 0

T-GP-07A 9:51 0 12.9 12.9 100 1.0 9.1 6.22 0 0

T-GP-10S 10:03 0 62.7 62.7 100 1.5 27.1 DRY - -

T-GP-10D 10:08 0 0 0 0 16.2 6.50 8.48 0 0

T-GP-11S NA NA NA NA NA NA NA NA 0 0


"r-GP-12S NA NA NA NA NA NA NA NA 0 0


T-GP-15 NA NA NA NA NA NA NA NA 0 0 Horizontal

Well 1300 NA 35.0 3.5 100 0.6 14.5 NA NA NA

Pre-System 1305 NA 8.5 8.5 100 9.4 7.6 NA NA NA

Btwn GACs 1310 NA 8.4 8.4 100 9.7 7.7 NA NA NA Post-

System 1315 NA 8.6 8.6 100 10.1 7,7 NA NA NA

HULLS ASSOCIATES, INC. TCLEDC, CHIC

DECEMBER 2007 CCT192.100,0011.DCC

NOTES: 1. All pressure readings are expressed as Inches of H2O 2. All readings are 0-100% gas by volume by air 3. (LEL) Lower Explosive Limit 4. All depth measurements are expressed in feet

NA - Not available (Not Located) (-) - Not measured

CLIMATOLOGICAL CONDITIONS Ambient Barometric Pressure: 30.01 (i ) Observed Weather Conditions: Sunnv Wind Direction and Speed: SSW 20 - 25 moh Relative Humiditv: 44 % Ambient Temperature f" F1 62 COMMENTS: Punch bar samolino was performed around the perimeter of the landfill

HULL & ASSOCIATES, INC. DECEMBER 2007 TOLEDO, OHIO COT192.100.0011.DOC

APPENDIX E

Field Forms for Facility Inspections Completed on July 24 and 26, 2007

>; ?!• m g -X m

HULL & ASSOCIATES, INC. MARCH 2008 tOLEDO.OHIO COT192.100.0009.DOC

MONITORING WILL INSPECTION FORM STICKNEY/TSfLER LANDFILLS

Name: Mike. Qjyxu<.Uo)

Date: U >

Affiliation: l4ull J-/d.cx «.c.«rej

Time:

Location/Identification S!iriace_Seal External Caaina Intemal CasinB 1. Is the well accessible:

2. Is surface seal 'damaged?

3, Is casing in good condition?

11. Is the intemal casing at least 1 foot above around?

2, Is the well protected from traffic?

6. Is the seal secure against the casing and sround?

9, Is casing locked? 12, Is intemal riser within 2 inches of too cao?

3, Is the well in low spot or standing water?

'

10. Is lock in good condition?

13, Is casing free of debris, kinks, bends?

4. Is the well labeled inside and out?

7, Is the seal sloped away from the wellhead?

14, Is cap in good condition?

WellLD. Inspected Requires Action

Items/Froblems Requiring Actipn (list number from above)

SMW-21 LP • SMW-24LP 5? • SMW-27LP • SMW-30LP • SMW-33LP • SMW-33LP sc • SMW-36LP •B • '""" SMW-37LP • TMW*.19LP Di • TMW-21LP • TMW-23LP • TMW-25LP isr • 4

TMW-27LP ET • . TMW-29LP la' • TMW-31LP • • TMW-33LP • TMW-35LP BT •

• •

Attach a detailed description of recommended actions at specific locations:

LAXDFILL INSPECnON FORM STICKNIY/TYLER LANDFILLS

TOLEDO, OHIO

Today's Date: T/ZV /O ?

Your name: MIKL CIOCZ-CTIO /

Are you completing this form for: • Sdckney Avenue Landfill X Tyler Street Landfill

(Please use a separate form for each landfill)

Item Yes or No

SECURITY

1. Is perimeter fencing Intact:

2, Are posted signs present and in good condition;

3, Were gates locked and locks intact;

4. Are gates and locks easy to open?

ACCESS ROAD

5, Does access road have rock surface layer? (List any areas requiring placement of additional rock.)

6. Is access road and adjacent tivf firee of ruts? (List any areas requiring repair with rock or top-soil)

yes

es

Recommended Corrective Action And

Schedule for Completion

LANDFILL INSPECTION FORM SUCKNEY/TYUCR LANDFILLS

TOLEDO, OHIO

Item Yes or No Recommended Corrective Action And


7, Are grused areas adjacent to access road free of ruts? (List any areas requiring grading, topsoil or seeding) /ej

VEGETATION

8, Is this vegetation on the top and side slopes free from bare spots and of sufficient density to protect cover system?

9, Is the pavement on the parking surface in good repair? ^

10, Are the perimeter trees free from observable stress and fallen limbs? \Jej

11,. Is the surfrice free of any evidence of rodents or burro^ng animals?

12. Is the surface free of woody vegetation other than perimeter trees? ^6^

LANDFILL INSPECTION FORM STICKNEY/TYLER LANDFILLS

TOLEDO, OmO

Item

13, Are the slopes or perimeter features free of any evidence of gas migrôn (stressed vegetation)?

Yes or No Recommended Corrective Action And


14. Are the slopes or perimeter features free of any evidence of leachate migration (excessive riprap staining or surface water discoloration)? Vgy

DRAINAGE AND EROSION CONTROL

12. Are drainage ways free from obstruction? ye. t

16. Are erosion control materials intact?

17. Are all surfaces free of erosion rills?

SETTLEMENT CONTROL

18. Are surface slopes uniform without local depressions or ponded areas? 4^

Item

LANDFILL INSPECTION FORM STICKNEY/TYLER LANDFILLS

TOLEDO, OHIO

Yea or No Recommended Conective Action And


RTVERBANX STABIUrY

19, Doea slope area appear to be stable and d'ee of localized settlement or

, slumps?

20. Is berm in place at top of slope and free of erosion or washouts?

21. Are underdrain outlet pipes (500-foot inter-vils) intact and drain freely?

22. Are underdrain outlet Pipe markers present?

23. Are slope monitoring points intact and appear to be in normal alignment?

24. Are letdown channels intact and free of erosion, dainage or debris?

25. Is riprap intact and free of localized depressions or voids in riprap slope cover?

Jej.

4^

LANDFILL INSPECTION FOBM SnCKNEY/TYLER LANDFILLS

TOLEDO, OHIO

Yes or No Recommended Corrective Action And


26, Is riprap berm at bottom of riprap slope intact and fiira of erosion or undercutting?

27. Is riprap surface free of debris and excessive woody vegetation? Vc/

Description of recommended action; (attach addition^ pages as required)

Item Number Description

HGURE 3-3 GAS MONITORING WELL INSPECTION FORM

STICKNEY/TYLER LANDFILLS

Name: Mgcc cWyTC.!^''!

Date: if ZC,lo'7

Affiliation: ^L^{\ ^ >^cfoc^(c>g/

Time: —

Location/Identification Vents Probes 1. Is the probe/vent accessible?

5. Is the vent damaged and need repair?

7. Are the probes and/or casings damaged and need repair?

2. Is the probe in low spot or standing water?

6. Are the vent sampling ports damaged and need repair?

8. Are probe casings visible?

3. Is probeArent free of obstruction?

9. Is probe casing subject to beins submerged?

4. Is the probe/vent labeled inside and out?

Well ProbeArent LD.

Inspecte d

Requires Action

Items/Problems Requiring Action (liat number from above)

S-GP-IS K • S-GP-ID • S-GP-IA • S-GP-2S S • S-GP-2D & • S-GP-2A 30^ •

, S-GP-IOS • S-GP-IOD • S-GP-llS • • /jof

S-GP-llD • • CJ*A<^ /W-S-GP-12 • • CoulcX /ur S-GP-14 • • S-GP-15 • BE-BP-01 • • C£xj\«J /vA /9c<Ae. BE-BP-02 • • T-GP-OIS • T-GP-OID • T.GP-02S • T-GP-02D r • T-GP-03S ffl- • T-GP-03D r •

T-GP-07S • • T-GP-07D • • T-GP-07A K • T-GP-IOS •

T-GP-IOD • T-GP-llS • . • ClcX>lcA rtiiV- lae-<> f-f-

T-GP-llD • • T-GP-12S • • CjiOiA /Iff )a<Leyl-e^

T-GP-12D • • >ipe#kfe_

T-GP-15 • • • Horizontal Well • Pre-System • Btwn GACs • Post - Sys •

• • • •

Attach a detailed description of recommended actions at specific locations below:

Hull LETTER OF TRANSMITTAL

& associates, inc. 3401 Glendale Avenue, Suite 300 • Toledo, Ohio 43614 • (419) 385-2018

TO; Mr. Michael A. Gifford

DATE: March 18, 2008 HA! Job No: COT192

SUBJECT: Environmental Monitoring

U.S. EPA Region 5

77 West Jackson Boulevard

Chicago, Illinois 60604

We are sending you 13 Reports •Prints

•Work Order •Change Order

•Specifications •Copies

•invoice •Plans

Item Date Copies Description ||

1 March 2008 1 Report of Environmental Monitoring for the Stickney Avenue and Tyler Street Landfills ||

1 These are transmitted as checked below:

•For signature •For review and comment

REMARKS:

•For approval •As requested SForyour use

COPY TO: W/ENCLOSURE oefAr Archie Lunsey, Ohio EPA - NWDO X

Casey Stephens, City of Toledo -Division of Solid Waste

X

Ed Irelan, City of Toledo - Division of Solid Waste

X

SIGNED:

if enclosures are not as noted, kindly notify Hull & Associates, Inc. at once.

Documents

REPORT OF ENVIRONMENTAL MONITORING · pressure, percent methane, percent Lower Explosive Limit (LEL), and depth to water in each of the gas probes and punch bar locations. Also documented