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SOUTHWEST LABORATORY OF OKLAHOMA, INC1700 W. Albany . Suite "C" . Broken Avow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. . REPORTS 323Sb570 DELAWARE AVE.BUFFALO, NY 14202 DATEi 08-22-90ATTN: PETER FAIRBANKS
LABORATORY BLANK
SAMPLE MATRIX i SOILSAMPLE IDs METHOD BLANK
DETECTIONCOMPOUND LIMIT (»Q/Ka)
TPH 10.0
TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE
> SAMPLE MATRIX I SOILSWLO # 3238.19/3238.20 (MS/MSD)PROJECT: DELAWARE SAND & GRAVELSAMPLE IDs UR-29 (MS/MSD)
SPIKE CONC. SAMPLE CONC. 1(•g/Kg) <«g/Kg)*
TPH 667 20
MSD CONC. MSD PERCENT(•g/Kg) RECOVERY
SAMPLE AMOUNTS 30SDILUTION FACTORS 1
AMOUNT FOUND(Md/Ka)
ND
RECOVERY DATA
MS CONC. HS PERCENT(*g/Kg)S RECOVERY
610 887.
RECOVERY PERCENTDIFFERENCE
TPH 59O 83V. 37.
DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS
0004 0
3B _.SOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lao Name: 314L-TULSA_______________ Contract: URS_______
t.gib Code: SWQK CaCT No.: UR5 9AS No.: _______ .§DB No.:
aoike - EPA Sample Ho.: UR-76_______ ; Leve !.:,<_! ow/incd) LQIO
COMPOUND
1 . 1-DicnloroetheneFricnloro^theneBenzeneToluene . ..Chlorobenzene
SPIKEADDED(ug/Kg)
59.559.559.559.559.5
SAMPLECONCENTRATION
( ug/Kg)
00000
MSCONCENTRATION
(ug/Kg)
52.448 . 334. 056.252 . 7 :
MS«//.
REC tt
83SI9194
. 89j
QCLIMITSREC.
59-17262-13766-1-3-259-ir°6O- t 33
COMPOUND
1 . l-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzen©
SPIKEADDED< ug/Kg)
59.559.559.559.559.5
MSDCONCENTRATION
(ug/Kg)
55. 749.355.757.755.0
MSDV/•
REC #
9483949792
V/•
.,RP& **__"7/_ *7»
-3— 7^-3
QC L3RPD
2224212121
HITS *REC . '
KTQ_ 1 7 - 1vj" 1 / *. »
62-137-16&-142!59-139!60-133!
;
F* Column to bm u ed to -^laa recovery and RPD values with an asterisk
* Values out»id« o-f QC limits
HFD: _2 out o-f _3. outside limitsSpit e Recoveryi _0. out o-f 10 outside limits
COMMENTSi —
lSr00043lFORM III VOA-2 " .1- - l'B7 R
101557
3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SWL-TUL5A_______' Contract; URS_______
Lab Code: SWOK Case -No.: URS SAS No. s m_____ SDB No.:
Matri;: Spike - EPA Sample No.: UR-36______'__ Level s (low/med) LOW
COMPOUND
Phenol2-Chloroohenol1 ,4-Dichlorobenrene ___N-NitrosQ-di— n-prop. ( 1 )1 . 2?4-Trichlorobenzene_4-Chloro-3-methy 1 phenolAcenaphthene4-NitroDhenol2 . 4-Dinitrotoluene ____Pen tac hi or o phenolPvrene
SPIKEADDED(ug/Kg)
1 59001590O794079407940 •15900794015900 .794O"159007940
SAMPLECONCENTRATION
(ug/Kg )
0Oo000 -0o000
MSCONCENTRATION
(ug/Kg)
969O10200521050306340131004910122006260158007010
MS/•
REC #
61646663SO8262777999S3
QCLIMITSREC .
26- 9025-10228 10441 12633 10726 10331-13711-11423- 3917-10935-142
COMPOUND
Phenol2-Chloroohenol1 „ 4-DichlorobenzeneN-Nitroso-di-n-prop". ( 1 )1 ,254-Trichlorobenzene_4-Ch 1 oro-3-me thy 1 pheno 1Acenaohthene4-NitroDhenol2-« 4-Din it ro toluenePefitachlorophenolPvrene
SPIKEADDED(ug/Kg)
159001590079407940 -7940159007940159007940
1 59007940
MSDCONCENTRATION
(ug/Kg)
102001140059005736'580O1270.05570116OO6190665O3340
MSD7.REC #
647274T1"*/ J^_
73SO70737342105
7.RPD *
-5— 12-11-1392
-1251
SI *-18
!DC LIMITS !RPD
35502733*L '
331950474736
REC . !s-— * s— ~ '26- 90!25-102!23 104!41 126!33 107!26 103!31-137!11-114!28- 89!17-109!35-142!
<1) N-Nitroso—di—n-propylamine
# Column to be used to -flag recovery and RPD values with an asterisk* Values outside of QC limits
RPD: _1_ out. o-f 11_ outside limitsSpike Recovery: 0 out of 22 outside Jimits
COMMENTS: UR-36 URSINSTrF SWL#3238.23. . ._
FORM III 3V-2 1/B7 Rev.
ARiOlSSS
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Names SWL-TULSA______________ Contract: UR§_______
Lab Code: 5MQK Case No.: URS SAS No.: ______ SDG No.
Matrix Spike - EPA Sample No.; * UR-36______ Level:(low/med) LOW
COMPOUND
gamma-BHC < Lindane ) ___HeotitchlarAldrinDieldrinEndrin4. 4 '-DOT
SPIKEADDED< ug/Kg )
oo • o63.363.3158158158
SAMPLECONCENTRATION
(ug/Kg)
000000
MSCONCENTRATION
< ug/Kg)
TT Ti-O • •-"
49.034.879.611667.2
MS7.
REC ft
37 *7755507343•
QC !LIMITS!REC. !
_______ i46-127!35-130!34-132!31-134!42-139!23-134!
ii
COMPOUND, EsssssBmscsssEsxssasa
gamma-BHC ( Lindan« ) ,Heptachlor ________
1 Aldrin
Endrin4,4* -DOT
SPIKEADDED{ug/Kg)sssacxsaea
63.363.363.3158158158
MSDCONCENTRATION
<ug/Kg)
l~>ae c;4.ta) • hJ
50.040.085.612379.2
MSD7.
RECS3K3K
40796354780
7.RPD ftESS-SEZK
-8-3-14-8-7-15
QC LIMITSRPD
503143384550
REC
46-12735-13034-1331-13442-13923-134
# Column to ba used to -flag recovery and RPD values with an asterisk
* Values outside o-f QC limits
RPD: _C| out o-f _& outside limitsSpike Recoveryi _2. out of 12 outside limits
COMMENTS:
FORM III PEST-2 — - -- Q/S7 Rt
5-00048
A R I D 1559"""
U.S. EPA - CLPERA SAMPLE NO,
6 " ________DUPLICATES
Lab Name: SOUTHWEST LAB OF OK Contract: 6S-D9-OOS9MU3823D
Lab Code: SWQK Case No.: 32381 SAS No.: SD(3 No.: MUT301
Matrix (water/sail): SOIL Level (low/med): LOW
7. Solids -for Sample: 45.1 "C Solids -for Duplicate: 35.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
J! Analyte1! Aluminum! Antimony! ArsenicI Barium '! Beryl lium! Cadmium! Calcium! ChromiumJCobalt1 Copper! I ronILead[Magnesium(Manganese! MercuryINickel! Potassium1 Seleniumi Silveri Sodium! Thai 1 ium! Vanadium! ZincI Cyanider
ControlLimit
88.7
_._
11.1
<•?
•?*? *?<£•&. •
11
Sample (S) C!I
29029.75301 !14. 0809 IB!2.6341 IB:94.09371 11.201418!1 . 3304 1 U I
502. 4249 IBS28.7104! 11 •— • • S5-_>S * c> i28.5291! J
26665. 498O! 120 . 6475 ! J983. 1386! Bt490 . 5392 I !
.1774IUI16.1720IBI
767.01141BJ1 .3304(Ui2.4168!&:
186. 6486! B!1. 33041 U!54.6419! !56.2147J !-i . 97-io i U i
i ii i
:Duplicate CD) C!
ii20961 -363OI !
1 1 . 5299 ! U 12-2173IU!9O.4920! I1 . 0426 1 B 11 . 4644 ! B !
522.9091 IB!24.40551 !1 T i A ; * R •i •-• • 1 O ._J i O i
28 . 4973 I i25277.86801 1
20.1986! !900,254718!515.7161! 1
. 1 7O6 i U !10. 9229! B!
540 . 0680 I B 11.3304 I U!1 • B6ji>-' t B i
162.74941U!1 , 3304 ! U !
48 . 7696 ! !64.4316! !3 . 8229 ! U !
i ii «
:y.RPD :
1
'— ' —--••-.•>
200 . 0 !200 . 0 .'
3.9114.2:
200 . o :4.0;16.2!5.11. 1 !
5.3:*•> ^ is.s:5.0:i38.7!34.7:
;
25.9:20 o . o :
;11 .4:13.6:
LI
*
rn;~
r
Pp
PPPPPPPPFPF'CVPPFPPpPPC
FORM VI - IN"V88
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY
' ab Names SOUTHWEST LAB OF OK Contract: 6S-D9-QOB9MU38
Lab Code: SWOK Case No.: "32381 SAS No.: SDE No.: MU3S01
Matrix: SOIL Level (low/med): LOW
/I Solids -for Sample: 45.1
Concentration Units (ug/L or mg/kg dry weight); MG/KG
i {Control1 ! LimitI Analyte ! 7.R
I Aluminum !J Antimony 175-1251 Arsenic I 75-125! Barium 175-125JB@ryllium!75-125! Cadmium 175-125! Calcium !! Chromium ! 75-125! Cobalt J 75-125! Copper ! 75-125ilron !(Lead 175-125agnesium!
.. langanese! 75-125I Mercury 175-125{Nickel 175-125! Potassium 11 Selenium 175-125! Silver 175-125(Sodium !i Thallium !75-125S Vanadium 175-125IZinc 175-125! Cyanide 175-125i i
Spiked SampleResult <SSR) C
!43.2981117.7206!969.9728!22.1600!30.8983!
!113.0438!223.9765 !143.3277!
!30 . 3947 !
ii690.9433!1.0440!
224.1379!t•
2 . 5366 !23.655O!
ri
21.7738!- 271.3027!
273.3179!41.8784!
i
SampleResult CSR) C
j14.0809IB2.6341 IB94.0937!1.2014JB1 .3304 I U
;28.7104!13. 8538 IB28.5291!
I20.6475!
!490 . 5392 !
-1774JU16.1720IB
j1.3304JU2.416810
;1.3304IU54.6419!56.2147!3 . 9736 ! U
!
_Spike
Added (SA)
219.5317.74878. 1421.9521.95
37.81219.53109.77
8.87'219.53
.92"? 1 O E?"T-Si 1 7 . -J.J-
4.4421.95
'22.17219.53219.5343.14
7.R
13.385 . 099.795.5140. S
96.095.7104.6
109.9
91.3113.594.7
57. 196.8
98. 298.798.997.1
Q!M
INftNIPIFIP!P
NIPINRIPIPIP!NRIFINRIPICVIPINR
NIFIPINRIFIPIP1CI
Comments
FORM V (Part 1) - IN
ARIOT56/
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 91&2S2-285B
CLIENT: URS CONSULTANTS, INC. REPORT: 323Sc570 DELAWARE AVE.BUFFALO, NY 14202 DATE: 08-22-90ATTNl PETER FAIRBANKS
LABORATORY BLANK
SAMPLE MATRIX* SOILSAMPLE ID i METHOD BLANK
DETECTIONCOMPOUND LIMIT (»q/Kg)
TPH 10.0
. TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE
* SAMPLE MATRIX I SOILSWLO # 3238.24/3238.23 (MS/MSD)PROJECT! DELAWARE SAND & GRAVELSAMPLE ID: UR-36 (MS/MSD)
SPIKE CONC. SAMPLE CONC. 1(•g/Kg) (wg/Kg)*
TPH 667 0
MSD CONC. MSD PERCENT(•g/Kg) RECOVERY
SAMPLE AMOUNTS . 30GDILUTION FACTOR: 1
AMOUNT FOUND(flip/Kg)
ND
RECOVERY DATA
IS CONC. MS PERCENT(•g/Kg)* RECOVERY
6OO 90%
RECOVERY PERCENTDIFFERENCE
TPH 600 907. 0%
DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS
A R I O I 5 6 2
3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lmb Name: SML-TULSA_______________ Contract: URS_______^ .
t Cedes Sl*JQ> Case No.: URS SAS No.: ______ SDG No.:
triv. inU a - EPA Sample No.: UR-44_______ Level : Clow/njed > LOW
COMPOUND
1 , l-l'ichloroethsn©^richloroethene
3 I '.'©no .......• \*~i i DroDenzene
SPIKEADDED(ug/Kg )
56.856. S« i. OwJO . O^A Q
56. 3
SAMPLECONCENTRATION
< ug/Kg';
00
' i.15C!
MSCONCENTRATION
(ug/Kg)
54 . 752". 3R4, O
63-3_._ .__ 6i.i
M5
REC #
9~6~921001O9103 .
" L'lCLI ni r=PEC .
59- I Z6J1-17766— I -^2c;o i "rs^JT L -• ~bU-I _-
COMPOUND
1 „ l-Dicnloro^theneTrichloroethgng&«n=en«TolueneCMcrobenzEin©
SPIKEADDED(ug/Kg)
56. S56.856.856. B56.8
MSDCONCENTRATION
< ug/Kg)
51.5-49.554.560 . 957.6
MSD
REC #
918796105101
RPD #
5, £447
iQC LIMITS !RPD ! REC. i
22 i 59— 1 72 !24 ! 62-137!21 166-1^2:~? i ; "=;ij_ i —c '.i. A 1 •— > J J. •—• t •
^ i ' fa ( ') —• i ~ ™ '; :
0 Column to bm used to -flag rgcov^ry and RPD values with an asterisk
* Values outmide o-f QC limits
o-f _ 5 outside limitsRecov^rvs _ Q_ o'u"t o-f 10 outside limits
COMMENTS:
6 000487FORM III VOA-2 — - 1/37 Re^
3DSOIL SEMIVQLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
_ab Names SWL-TULSA Contract: URS
_ab Code: SWQK Case No.: URS 3AS No.:""
latrix Spike - EPA Sample
COMPOUND
Phenol _2-Chloraphenol1 , 4-Dichlorobensene . .N-Nitraso— di-n-prap. ( 1 )1 ,2,.4-Trichlaraben2ene_4-Chl or o— 3— methyl phenolAcenaphthene4— Nitrophenol2 , 4-D in itro toluene ____PeritachlorophenolPvrene
SDG No. :
No.: UR-44 Level: ( low/med) 'LOW
SPIKEADDED( ug/Kg )
1 52001 5200"... 7580758075301520O7530152007530152007580
SAMPLECONCENTRATION
< ug/Kg >
00000 'o00 •
— - 000
.
MSCONCENTRATION
<ug/Kg )
37'2010000"5220434056201=06004540
"1 12005260115006400
MS
REC $
57666957747O6074697634
QCLIMITSREC.
26- vO25-10228 10441 12633 10726 1 0331-13711-11428- 3917-10935-142
>
COMPOUND
P hen a 12-Chlorophenol1 , 4-Dichlorobenzene ___N-Ni troso-di-n-prop . ( 1 )
4-Ch 1 oro-3-methy 1 pheno 1Acenaphthene4 -Nitro phenol2 «4-Din itro toluenePentachlorophenolPvrene
-
SPIKEADDED(ug/Kg)
1520015200758075307580
1 52007580152007580152007580
MSDCONCENTRATION
( ug/Kg )
1 020010200504044005630
1 1 i" 604970
1 25005720
1 22007030
MSD•/REC #
6757
58747366"8275SO93
• /
RPD *
-16
4
0-4-10-10— s-5-10
QC LRPD
T="
502733
1950474736
IMITSREC.
26- 90
2B 10441 12638 10726 10331-13711-11428- 3917-10935-142
(1) N-Nitroso-di-n-propylamine
# Column to be used to -flag recovery and RPD values with an asterisk* Values outside o-f QC limits
RPD: _0 out o-f 11 outside limitsSpike Recovery: _0 gut o-f 22 outside 1 imits
COMMENTS: UR-44 URSINST:F SWL#3238,09
FORM 111 SV-2 ^ . 1/87 ReveroobTso
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SHL-TULSA_______________ Contract: URS3_______
Lab Codes 5MQK Case No.: URS SAS No-s ______ SDG No.:
Matrix Spike - EPA Sample No • ; UR-44______ Level:(low/m@d) LOW
COMPOUND
gamma-BHC (Lindane) ___HeptachlorAldrinDieldrinEndrin4,4'-DDT
•
SPIKEADDED<ug/Kg>
60. 460.460.4151151151
SAMPLECONCENTRATION
(ug/Kg )
000000
MSCONCENTRATION
(ug/Kg )
46.368.245.0124137125
MSV.REC #
7711374829183
QCLIMITSREC.
46-12735-13(334-1323 1 - 1 3442-1392T--134
COMPOUND
aamrna-BHC (Lindane)HeotachlorAldrinDieldrinEndrin ~~~4,4'-DDT
SPIKEADDED< ug/Kg)
60.460.460.4151151151
MSDCONCENTRATION
< ug/Kg)
42.865.547.9129140137
MSD.//.REC #
7110879859391
•/.RPD #
85-7-4_jL.
-9
QC L]RPD
50314338
' 4550
ii[MI rs REC m
- — — -^46-12735-13074-13231-1 -.442-13923-134
# Column to be used to -flag rgcov^ry and RPD values with an asterisk
* Values outside o-f QC limits
RPD: _G! out 0<f _6. outmid© limitsSpike Recovery: _g. out o-f 12 outside limits
COMMENTS:
FORM III PEST-2 S/87
SRIOJ565* " •
U.S. EPA - CLPEPA SAMPLE NO.
6 ______DUPLICATES
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089MU3809D
Lab Code: SWOK Case No.: 32381 SAS No.: SDG No.: MU3801
Matrix (water/soil): SOIL Level <low/med): LOW
7. Solids -for Sample: 88.7 7. Solids -for Duplicate: 87.8
Concentration Units (ug/L or mg/kg dry weight): MG/KG
i1 Analyteir Aluminum! Antimony! Arsenic! Barium! Beryl lium! Cadmium! Calcium! Chromium! CobaltI CapperI IronI LeadI MagnesiumI ManganeseI Mercury1 Nickel1 Potassium1 SeleniumISilverI-Sodium! Thai liumI VanadiumIZincI Cyanidei•
ControlLimit
45.1
.7
.1
11.3
1.9-
iiSample (S) CI*•
7780.9541 I I5.8625IUI5.63701 UI58 . 8247 ! J
. 4359 I B I
. 67641 U!410.7929IBJ1 1 . 9042 1 14.2115IB!3.6077IU!
11807.4200! !74.01351 I320 . 3267 ! B 1199.6961! I
.42641 !5. 05281 B!
321.7134IBI.6764JUI. 6O84 ! B !
82.7508IU!. 6764 I U J
20.83011 !25.07291 11.S604IU!
i i
«iDuplicate CD) CIii
10990.8290! J5.7475IU!1.1053JU!
75.66171 I. 4886 ! B 1.6632IUI
321.4701 IB!13.5648! !4.1887:B!3.5369IU:
12364.98101 I71.7886! 1348.1100IB!195.8722! 1
.26491 I8.4617IBI
366.8301 !B!. 66- ji, i U i. 7053 ! B J
S1.12S3IUJ. 6632 I U !
21.9900! I30.62891 I2.os7s:u:
i ii i
.•/.RPD
34.2
25.011.4
24.413.0
.5
4.63.18.31.9
46.750.413.1
14.8
5.419.9
1
Q!Mi
*!PIPIFIPIPIPIPIP!PIPIP:FIPIP
* ICVIP;pIFIPIPIFIPIP1Ci
FORM VI - IN7/88
0-0004UO
flRI01566
u.5. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY
/ ' *b Name: SOUTHWEST LAB OF OK Contract: 6S-D9-0089MU3809S
Lab Code: SWOK Case No.: 32331 SAS No.: SDG No.: MU3801
Matrix: SOIL - - Level Clow/med): LOW
"/. Solids -for Sample: S3.7
Concentration Units (ug/L or mg/kg dry weight): MG/KG
I {Control! ! LimitI Analyte I */.R! !{Aluminum !{Antimony 175-125! Arsenic 175-125! Barium 175-1251 Bery 1 1 i urn I 75- 1 251 Cadmium I 75-125{Calcium I! Chromium ! 75-125! Cobalt .'75-125i Copper 175-125I Ironi Lead Iagnesium!
. Manganese ! 75-125! Mercury !75-i251 Nickel ! 75-125! Potassium!.' Se 1 en i urn 1 75- 1 25(Silver 175-125I Sodium I\ Thai lium 175-125! Vanadium 175-125I Zinc 175-1251 Cyanide ! 75- 125I !
Spiked SampleResult (SSR)
116.37022 . 0829
471.548910.S79214.2190
56 . 0626106.066553.0721
47.0158
313.0247.2523
110.5212
2.051611.1689
.6697127.6149126.439714.7471
C
B
U
SampleResult CSRJ C
ii5.S625JU5 . 6370 I U58.8247!
. 4359 ! B
.6764IUi
11.9042!4.2115JB.3.6077,'U
ii74.0135!
i199.6961 !
.4264!er r'le-'jp ' Q-J . V.J«£.O i O
»t.6764 I U. 6084 I B
».6764IU
20.3301 125.0729!1.8604JU
ii
SpikeAdded <SA)
111 .628.93
446.4911.1611.16
44.651 1 1 . 6255.81
4.46
1 1 1 . 62.54
1 1 1 . 62
2.23,11.16
11.16i 1 1 . 621 1 1 . 6218.18
"
•/.R
104.7TT -r*^w • -J>
92.493.6127.4
98.991.395.1
-605.3
101 .5-32.294.5
92 . 094.6
0 . 095.790.881.1
.
itQ!M
ii;NRIP
NIFIP!P
NIPINRIPIPIPINRIF!NRI F*
NICVIPINRIFIPINR
NIFIPIP:cj
Comments:
FORM V (Part 1) - IN
£-000491
A R J O I 5 6 7
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089
Lab Code: SWOK Case No.: 32381 SAS No.: SDG No.: MU3801
Solid LCS Source: EPA0287
Aqueous LCS Source: EPA-LV
i
I Analyteti! Aluminum! AntimonyI ArsenicI Barium! Beryl liumI Cadmium! Calcium! Chromium! Cobalt! Copper
-on. _ead! Magnesium1 ManganeseI Mercuryi NickelI Potassium1 SeleniumISilverI Sodium1 Thai lium1 VanadiumIZincI Cyanideit
Aqueous (ug/L>True Found
201O.O!1010.0!47.4!
1960. O!483.01.502 . 0 !
48700.0!510.01502.01515.0!2040 . 0 !4500.0!24600.0!504 . 0 !
i480 . 0 1
49OOO . 0 I52.6!500 . 0 !
49600 . 0 I97.01488.0!
31OO.OIitii
2039.997.44.
1969.479.506.
47777 .507.484.513.1944.4605.24119.
487.
490.47463 .
50.470.
49154.84.496.2880.
70!16!46!4O!52!55!OO!50!13!52130150!OO!31 !
i•44!00!06!8*-i i*L i
OO!75!69!30!
itti
•/.R
101.598.793.8100.599.3100.998.199.596.499.795.3102.398.096.7
102.296.995.294.299.187.4101.892.9
True
325.0!• 211.0!917.0!
4.8!19.4!45.41
196200.0!99.61
.144.O!6910.0122430.0!236.01
118100.0!208 . 0 !12.7!60.9!5O.O!TO *•* I•_>T • -t iO"» *"> i4U. . JL. t
50.0!39.0!65.8!187.0!5.6!
i
Solid (mg/kg)Found C
304.169.799.4.18.45.
220818.86.
l<j>*i> •7133.18995.227.
132763.214.14.52.69.08 .16.
r>Tr**_•_'-;. •
•1'C* .
59.167.5.
j 1••? i*? i6IB8!Bii4!•j' io *5 111t7 '/ 1718!1 !o;u8!6!7IB4!4!1 !9!!
OT>cf
12763501635
16630079124600617770188
10O400177S
-4901915024511384
11
Limits 7.R I-ii
.0
.0
.0
.0
.5
.7
.0* ».0.0.0.0.0.0.5
*—>.0.1.5.0.6.7.0.3
424.0294 . 01199. 040 .0T*'"? T55.1
2256OO.O120.0162.07820.027080 . 0285.0
1 299OO . 0239 . 017.072.6
1000.059.429.0
1000.O53.579.9236,06.9
93.6!SO . 2 J37. 2!95. SI96.91
1 00 . 9 1112.5!86.6193.01103.2!84.7!96.3!112.41103 .2 !116.5!85.6!0 .0 I ••''99 . 0 !74. 3 IV465 . 4 (/85.6!90.3 !89.4!105.4!
ii
FORM VII - IN7/8B
£-000492
fl R I 0 1 5 6 8
r
U.S. ERA - CLP
7LABORATORY CONTROL SAMPLE
Lab Names SOUTHWEST LAB OF OK Contract: 6S-D9-0089
Lab Codes SWQK Case No.: 32381 SAS No.: " SDG No.: MU3801
Solid LCS Source: EPA02S7
Aqueous LCS Sources
*•i«! Analyte!! Aluminum! Antimony! Arsenic1 BariumI Beryllium1 Cadmium! Calciumt Chromium! Cobalt! Copper'on
.-•ad(MagnesiumI Manganese! MercurySNickelI PotassiumI SeleniumISilver) SodiumI Thai lium1 Vanadium!Zinc\ Cyanidei
AquecTrue
.
.
DUS <ug/LFound
- -
- .-
7.R__
SolidTrue Found C
f^^ l~\ ' "T/"iQ Q '-w .'j . yj i -_tijo . a >211 .01 163.1 I917.01 955.8!
4.8! 4. SIB19.4! 17.8!45.41 46.3!
196200. 01215861. 3!99.6! 83.7!144.0! 128.2!6910.0! 7481.2!22430.0! 18648.3!236.0! 229.2!
118100.0! 134970.3!208.0! 207.5112.7! 11.7!60.9! 51 .4150.0! 69.0IU39 . 2 I 37 . 4 I^*n "J 1 4 • •-* 1*i. - . 4. 1 i O . —— t
50.01 222.9 IB39.0! 42.6!65.8! 59.3!187.01 164.7!
5 A ' ^ c") *. O i *J . V it i
mg/kg )Limits
225.0! 424.0127.0! 294.0635.0!' 1199.00 . 0 I 40 . 0
1 1_ C" 1 T^ T*1 O . hJ t -i-J- . •-*
w*o . / i 3«J . X166800.01225600.0
79.2! 120.0124.0! 162.06006.0! 7820.017770.0! 27080.0188.0! 285.0
1OO400.0! 129900.0177.0! 239.0
8.5! 17.0::49.2! _ 72.6
0.0! 1000.019.11 59.4
:-15.5l 29.00.0! 1 000 . 024 . 6 ! 53 . 551.7! 79.9133.0! 236.0
4.3! 6.9ii
i
•/.R
95 . 077.3
104.2100.091.8102.011O.O84.089.0108.383. '97. |114. J|99.892.184.40.0
95.473.0
4-45.8109.290. 138. 189.3
FORM VII - IN7/88
0-OCU49
A R i O I 5 6 9
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. " REPORT: 3238a570 DELAWARE AVE.BUFFALO, NY 14202 DATEs 08-22-90,ATTN: PETER FAIRBANKS
LABORATORY BLANK
SAMPLE MATRIX* SOIL SAMPLE AMOUNT? 30GSAMPLE IDs METHOD BLANK DILUTION FACTORS 1
DETECTION AMOUNT FOUNDCOMPOUND_______________LIMIT (ma/Ka)____________
TPH 10.0 ND
TPH MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY__
SAMPLE MATRIXJ SOILSWLO # 3238-10/3238.12 (MS/MSD)PROJECT! DELAWARE SAND * GRAVELSAMPLE IDs UR-44 (MS/MSD)
SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT<»g/Kg) (mg/Kg» («g/Kg)« RECOVERY
TPH 667 22 S9O 857.
MSD CONC. MSD PERCENT RECOVERY PERCENT(ing/Kg) RECOVERY DIFFERENCE
TPH 610 98'/. -3V.
* ^ DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS
A R I O I 5 7 0
3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Name! SWL-TULSA_______________ Contract: URS_______
Lab Code: BVJQK Case No.: URS SAS No.: ______ „ SDG No.:
Matri,; Spike - EPA Sample No. : 'BC-6-1______ Level :< low/med) LOW
COMPOUND
1 » i-Dichlorogthgne ____
EenzsngToluene •_...Chlorabgnzfme
SPIKE !ADDED(ug/Kg) !
54.4 !54.4 !54.4 !54.4 !54.4 !
!
SAMPLECONCENTRATION
(ug/Kg )
O00O0
MSCONCENTRATION
(ug/Kg)
= 42.639-247.551.848.6
MS
REC
• 7B72879539
! CfC !SLIMITS!
# ! REC . !. ... ' .... _ 1 - *
159-172!162-137!!66-142!159-139!160-133!"i i
COMPOUND
1. l-Dichloraeth«n» ____Trichlora^theneBenc^n©Tolu«naChloro benzene
SPIKEADDED(ug/Kg)
54-454.454.454.454.4
MSDCONCENTRATION
<Lig/Kg>
46.239.648.752.148.3
MSDmi
REC *
asT-T
909689
~
•f/.RPD #
-9. -1
-1O
QC L:RPD
f *"/
74
21*. u.^1
:MITS REC.^
59-17262-13766-1^259-13960- 1 33
S Column to b^ used to -flag recovery and RPD values with an asterisk
* Values outside o-f QC limits
RPD: _0 out o-f _5. outside limits "3piK» Recov*rys _0 out of 10 outside limits
COMMENTSi SC-c-1 - URSINSTsI SWL#367S.30 5
FORM Til VOA-2 -- - 1/37 Re
6-000495
3DSOIL SEMTVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
» Lab Name: 5WL-TUL5A______________ Contract:
Lab Code: SMOK Case No.: URS SAS No.: ______ SDG No.:
Ma .;; Spike - EPA Sample No.: BC-6-1______ Level:(low/med> LOW
COMPOUND
Phenol - _2-Chlorophenol1 ,4-Dichlorobenzene ___N-Nitroso-di-n-prop. ( i )1 , 2,4-Trichlorabenzene_4-Ch loro-3-methyl phenolAcenaphthene4-NitroDhenol2, 4-Din itro toluene ____F'entachlorophenolPvrene
SPIKEADDED(ug/Kg)
1450O145007250725072501 45007250145007250145OO7250
SAMPLECONCENTRATION
(ug/Kg)
O00000000o0
MSCONCENTRATION
(ug/Kg)
543051502960244O 2850594O281053402890369O3030
MS
REC #
37364134 *39413937402542
QC !LIMITS!REC. !
26- 90!25-102!28 104!41 126!38 107!26 103!31-137!11-114!28- 89117-109!35-142!
It
COMPOUND
Phenol_______2-Chlorophenol.1,4-Dichloroben2@ne___N-Nitroso-di-n-prop.<1)1.2,,4-Trichlorobenzene_4--Ch loro-3-methyl phenolAcenaphthene____4-Nitrophenol________2,4-Dinitrotoluene____Pentachlorophenol_____Pvrene ___________....
SPIKEADDED< ug/Kg)
1450014500725072507250145007250145OO7250145007250
MSD ! MSDCONCENTRATION! 7.
< ug/Kg) ! REC
35
2Q *5* *#-
sMisa
RPD
6OS-252S.
8
10
QC LIMITSRPD
50273823331950474736
REC
26- 9025-10228 10441 12638 10726 10331-13711-11428- 8917-10935-142
tl> N-Nitroso-di-n-propylamine
# Column to be used to -flag recovery and RPD values with an asterisk# Values outside o-f QC limits
RPD: _ 0 out of 11 outside limits .Soike Recovery: «3. v out o-f 22 outside limits
COMMENTS: BC-6-1 ._ URSI NST : F SWL#3678 . 30
\\
FORM III SV-2 , 1/37 Rev.
0-00049C
A R I O I 5 7 2
3FSOIL PESTICIDE "MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Names SWL-TULS.fi______________ Contract: URS_____
Lab Code: SfrJQK Case No.: URS SAS No,: ______ SDG No.:
Matrix Spike - EPA Sample No.: BC-6-1_____ Level:(low/med> LQW__
COMPOUND
gamma-BHC ( Lindane ) ___HeotachlorAldrinDieldrinEndrin4,4'-DDT
SPIKEADDED(ug/Kg>
5.78s, "7Q
5.7814.514.514.5
SAMPLECONCENTRATION
(ug/Kg)
0O0Oo0
MSCONCENTRATION
< ug/Kg)
3.496OQ
4. • / wl
20.317.67.70
MS7.REC #
6O12148140 *121S3
DC !LIMITS!REC . I
46-127!35-130!34-132131-134!42-139!23-134!
!
COMPOUND
gamma-BHC (Lindane),Heptachlor________Aldrin___________Dieldrin__________Endrin____________4,4'-DDT__________
SPIKEADDED(ug/Kg)
IBIS se rn.sc am at
5.785.785.7814.514.514.5
MSDCONCENTRATION
(ug/Kg)
4.O48.124.469.3518.99.75
MSD7.REC #sar«aea>s
7014O *776413O67
7.RPD #33JB3ES3B
-15-15-46 *75 *-7
QC LIMITSRPD
503143384550
REC.
46-1235-13034-13231-13442-13923-134
ft Column to be used to -flag recovery and RPD values with an asterisk
* Values outside o-f QC limits
RPD: _i out of _6 outside limitsSpike Recovery: _2 out of 12 outside limits
COMMENTS:
FORM III PEST-2 B/87 Rev.
0-00049
ARIOI573
AffiRICA* ANALYTICAL t TECHKICAL SERVICESMtTRtt SPIKE EVALUATION FORK
UfiS
SAMPLE IB BC-6-1HS
H£T MT. 10.0
atount aiount itountno in spl. added detected I TARGET
added ppt ppt ppt recovery recovery lints2378 TCDF 2.5 0 250 298.5 119 60 - 140 IHPC8F 10 0 1000 1513.0 151t 60 - 140 X,
25 0 2500 3859.0 154* ' 60 - 140 I
2378 TCSa 2.5 0 250 424.6 170* 60 - 140 IPCBO 10 0 1000 1596.3 1601 60 - 140 Xmm 10 o 1000 1502.3 isot 60 - 140 z
DUPLICATE SAMPLE EVALUATION
SAWLE ID BC-i-lMS 8C-6-1HSD
»a JIT. to.o 10.0aiount amount RPDin spl. in spl.ppt ppt
2378 7CBF 298.5 313.8 5.0HPCDF 1513.0 1390.0 8.5OCDF 3B59.0 3732.0 3.3
2378 TCDD 424.6 385.7 9.6PCDD 1SH.3 1507.7 5.7HICDD 1502.3 1520.8 1.2
AHE8ICAH AWU.YTICAL i TECHNICAL SERVICES
HATfUX SPIKE EVALUATION FORH
URS
SAMPLE ID BC-6-1HSD
«£T HT. 10.0
aiout itount amountng in spl. iddefl detected Z TARGET
added ppt ppt ppt rttovtry recovery liiits2378 TCDF 2.5 0 250 313.8 126 60 - 140 IHPC0F 10 0 10W 1390.0 139 60 - 140 Z
25 0 2500 3732.0 149* 60 - 140 Z
2371 TCD0 2.5 0 250 385.7 1541 60 - 140 ZPCM 10 0 1000 1507.7 151* 60 - 140 ZHICD0 10 0 1000 1520.8 152* 60 - 140 Z
DUPLICATE SAMPLE EVALUATION
SAHPtE IS IC-6-1HS IC-6-1HSS
»T. 10.0 10.0
await tflIB spl. in spl.ppt ppt
237i TCDF 291.5 313.S 5.01513.0 1390.0 8.53859.0 3732.0 3.3
2371 TCDD 424.6 385.7 9.6PCDD 1596.3 1507.7 5.7HXCDD 1502.3 1520.fi 1.2
U.S. EFA ---CLPEPA SAMPLE NO.
6 _____ ___DUPLICATES
Lao Name: SOUTHWEST LAB OF OK Contract: 63-D9-OO39 ___________
l_ab Code: SWOK Case Mo.: 367S1 SAS No.: SDG No.: MU7B01
Matrix (water/soi1>: SOIL Level (low/med): LOto
y. Sclids tor Sample: 88.4 7. Solids -for Duplicate: 33.4
Concentration Units lug/L or mg/kg dry weight): MG/KG
i1 Anaiytei
; Al u/ni nunt1 Antimonyi Arseni c! Bar i um! Beryl I ium1 Cadmium; Calcium1 Chromium! Cobalt! Copper! IronJLead1 Magnesium! Manganesei Mercury-INicksl'! Potassi um! Sel'eni um! Si 1 veri Sodi umI Thai 1 ium! VanadiumIZinc! Cyanide!
ControlLimi't
2-i 2
5.6
.7
,
.
11.24.5
Sample CS> C
95 1O. 9846;1 1 . 4336 ! B1. 1200 I L1
24. 8567 IB. 5283 ! B. 6720 ! U
146. 6689 JB10.897912.8044IB3.5841IU
16912.3700!4.7489!
219. 6590! B82.3636!
t6. 2663 IB
173. 4436 IB. 4430 ! U1.0961 !3
112.352713. 6720 HJ
19.3959!10. 19O4!2. 1833JU
!
Duplicate CD) C
4450. 3073 I13.332OIB1. 1312JU9. 1307! 3. 333S ! B.67971U
91. 2007 IB8. 06 OS!1 . 3875 J B3.9051 i
13433.1690!- 2-36431106. 1221 IB21.7678!
15. 1405JB
i 23. 5063 i 32.2624!U. 9024 ! B
1 OO.3359 IB". 67S71U9. 2842 IB5.1448!1. 1312JU
1 • !
y.RPD/ jll . u'
1 -li * •'-*
92. 145. i
46.629. 967.6200.022. 967.069. 7116.4
1 9. 7~ r*i *•»
19.410.3
70.565. S
I
Q
*
#
'•*•**
*
*
M
PPFPPPPPPPc-
FF'PNRPp.FPP—PPC
FORM VI - IN7/88
U.S. EPA - CLP
5A EPA 3AMF,_SPIKE SAMPLE RECOVERY"" "
) 1 MU7830SLab Names SOUTHWEST LAB OF OK- Contract: 68-D9-5089 ! __Ji£r4:J______ !
Lmb Code: SWOK Cam© No.: 36781 SAS No.: " SDG Mo.: MU7801
Matrix: SOIL Level Clcw/med): UDW
% Solids -for Sample: 92.5
Concentration Units Cug/L or mg/kg dry weight): MG/KG
! ; Control1 ! Limitt Anmlyte ,' XRI :* Aluminum !I Antimony (75-125f Arsenic : 75-125i Bar ium ! 75-1 25JBeryllium!75-i25J Cadmium t 75-125i Calcium ;! Chromium 175-125! Cobalt ,'75-125
.! Copper 175-125). Iron !^ILead ! 75-125
1 Magnesium!! Manganese ! 75-125{Mercury ! 75-1 25! Nickel ! 75-1251 Potassium I(Selenium '75-125{Silver 175-125'Sodium !! Thai lium ! 75-125< Vanadium I 75-125IZinc J75-125ICyanid® 175-1251 !1 4
Spiked SampleRMuIt (SSR) C
ii39. 7263 J5^3571 1
507.0297112.223O!15.5794!
ii57.32971123. 3475 i69.65231
11O. 46191
it181.4773!
.094O1U126,3848!
i1 . 0425 1 BSATTT- I. O <«••_> . i
i1
1 1 . 6628 1133.5733!132.4586!19.7477!
!
SampieResult CSR) C
>9. 9595 IB1-2131 !B
27- 1645SB.4011 ;B. 6422 ! U
ii1 1 . 5487 !2.3619IB3.42521U
i•5.59171
ii55.5301 1. 1029 !U
5.67121Bii
- 4232 ] U1 . 3207 1 B
ii. 6422 ! U
IS. 5623!13.9876!1 . 8575 ! U
ii
SpikeAdded (SA)
. 103.113.56
432.431 0.3110.81
:; 43.24108. 1154.05
4.28
108. 1 11 . 00
108.11
2. 141O.E1
10.701 OQ . 1 1108. 1118.02
1 11 < <1 !r i <
7.R ! Q I M ,i I
J ! NR !27.5!N,'P :D4.~;N!F !1 1 1 . O ! ! P !109. 4 ; IP !144. i ;N;P ;
J 1 NR !105.9! JP !111.9! i g128. 9!N, •
! ihP113.3! IF
i INR116.5! IP
O.OINICV112. 1 : IP
i ; NR43. 7;NJFi?.6 -NIP
: ; NR109,01 IF106!. 4: IP1O9. 61 IP109. /a, 1C
i ii i t
Comments:
FORM V (Part 1)- - IN
fir-00050*R!0!577
U.S. EPA - CLPEPA SAMPLE NO,
6DUPLICATES 1
! MU7830DLab Name: SOUTHWEST LAB OF OK Contract: 63-D9-O089 i _JJC^-j_____
Lab Code: SWOK .Case No.: 367B1 SAS No.: SDB No.: MU7BO1
Matrix (water/soil): SOIL Level <iaw/med): LOW
% Solids for Sample: 92.5 X Solids for Duplicate: 92.5
Concentration Units (ug/L or mg/kg dry weight): MG/KG
i AnalyteiI Aluminum1 Ant i manyJ Arsenic! Bar i umi Beryl 1 i um1 Cadmium! Cal ciumJ Chrcjmium! Cobal t1 Copper! Iron!Lead; Magnesium! ManganeseS Mercury! Nickel: Potassium: Selenium! Si 1 ver! Sodium! Thai 1 iumJ Vanadiumi ZincI Cyanide
ControlLimit
5.4
1O.74.3
Sample (S) C
1O61 1.4480!9. 9595 IB1.2181IB
27. 1645 IB-4O11 IB' . 6422 I U
185.432OIB1 1 . 5487 !2.3619!B3.4252JU
15599. 1060!5.5917!
2S4.09O3JB55.53011. 1029IU5.67121B
245. 6526 IB. 4282 ! U
1 . 3207 ! B131. 0220 !B
. 6422 1 U18.5623!13.9876!1 . 8575 ! J
Duplicate <D) C
9397. 7990 !3.5511 IB1.3124 IB25. 8074 IB.363213. 6436 ! U
187. 3804 IB11.2833! •3. 0387 IB6.80661
15665.0010!6.6422!
333. 1207 IB60.3643!. 1029 JU
7. 3242 IB250. 5 1 79 IB
. 4324 ! U1. 1359 iB
112. 9765,! B. 6486 J U
16.6006!14.0658!1 . 3900 ! U
7.RPD
12. 115.27.55. 19.9
1.0''3 "
25.1200 . 0
.417.215.99. 2
25.42 . 0
15.014. S
11.2.6
i
irIP
IP
IFfPIPIPIPIPIP
*!PIPIFIPIP;CVIPIPt ;""
IP
IP
! PIP1C
FORM VI --IN7/83
6-00050A R 1 0 I 5 7 8
3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab N«m»: SWL-TULSA_______________ Contract: URS______: "
Lab Codg: SVJOK Case No.: URS SAS No.: ______ SDG No.:
Matrix Spike - EPA Sample No.: BC-6-~______ Leveli(low/med) MED
{COMPOUND
1 . 1-Dichloro^th^ne ____Trichloro^th^neBenzene'Tolusng
! CHlorobenzen^i _..=
SPIKEADDED< ug/Kg)
67906790679067906790
SAMPLECONCENTRATION
( ug/Kg )
000o0
MSCONCENTRATION
(ug/Rg)
3440556060 1 060505950
MS
REC #
51 *823999SB
QCLIMITSREC.
59-17262-13766-14259-1 7?6O-133
COMPOUND
1 , l-Dichloroeth©ng ____Trichloro^th^neBenzeneTolueneChlorobgnzene
SPIKEADDED(ug/Kg)
67906770679067906790
MSDCONCENTRATION
(ug/Kg >
36505300626066006820
MSDV.REC #
54 *859297100
•//.RPD #
-6-4
_C3
-13
QC LIRPD
•T"?
24212121
iiEMITS '
REC. t
59-1726^__ 4 T"^^1—— 1 _' /
66-14259-13960-133
t* Column to bm used to flag recovery and RPD values with an asterisk
* Value* outmide o-f QC limit*
P.PDi _ 0 out o-f _ 5 outside limits ; :Spike RacDvervs. _ 2. OLJt o-f 1O outside limits
COMMENTS i
FORM III VOA-2 1/S7 Res
503DO05-^
A R I O I 5 7 9
3BSOIL VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVER/
Lab Name: SWL-TULSA_______________ Contract: URS_______
Lab Code: SUiOK Case No.: URS 3AS No.: ___^_ SDG No.:
Matrix Spike - EPA Sample No.: .BC-7—2_______, Level :(Iqw/med > LOW
COMPOUND
1 . 1-Dichloroethene ____TrichloroetheneBenzeneTolueneChlorobensene
SPIKEADDED< ug/Kg)
oo • w63.5od . kj63. 568.5
SAMPLECONCENTRATION
(ug/Kg)
60011.0 -9.73
M9CONCENTRATION
(ug/Kg)
e;o -7J 7 . i
~ e; cr•-t , . J
60.862.1 .61 .5
MS.//f
REC *
877789-re;
76
DCLIMITSREC.
59-17262-13266-14259-1 _.960- 1 .. »i
COMPOUND
1 , 1-Dichlordethene .__.TrichloroetheneBenzeneToluene?Chlorc-benzene .
SPIKEADDED(ug/Kg)
68.56S.563.563.563.5
MSDCONCENTRATION
< ug/Kg)
er^ f, i%J/ . T
52.961. 160.759.2
MSDf,
REC S
85773973-~n-,/ -i
•/fm
RPD tt
»•>00o>1=]
DC L .RPD
*?*24^* 1*. 12121
iMITSREC.
5=9-1 "262-13766-14259-13?60-1 ."
# Column to. be used to -flag recovery and RPD values with an asterisk
* Vslues outside o-f QC 1 imits
RPD: _0 out of _5 outside 1imitsSpike Recovery: _0, out of 10 outside limits ;
COMMENTS: 3C-7-2-- - -^ URSINST:I 3
FORM IIT"VOA-2-. .. . .. 1/B7 =e
000304
01580
3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SWL-TUL5A______________ Contracts URS_______
Lab Codei SMOK Case No.: URS SAS No.: ______ SDG Nol:"\
Ma. *x Spike - EFA Sample No.: BC-6-4______ Levels<low/med) LOW
COMPOUND
Phenol2-Chlorophenol1 ,,4-Dichlarobenzene ___N-Nitroso-di-n-prop.~( 1 )1 j,254-Trichlarobenzene_4-Chloro-3-methy 1 phenolAcenaphthene4-NitroDhenol2?4-Dinitrotoluene^ ___PentachloroohenolPyrene _ _ __
SPIKEADDED(ug/Kg)
7240724036203.620362072403620724036207240-p. t ~\s\
SAMPLECONCENTRATION
(ug/Kg)
00000O0000
MSCONCENTRATION
< ug/Kg)
565052102360199O250057902460608027708220*?QOf"i
MS•/Sm
REC #
7872655569SO'688477114 *_ ,
DC !LIMITS!REC. !
26- 90!25-102!28 104!41 126!38 107!26 103!31-137!11-114!28- 89!17-109!_^ e , , ,
t*
1 COMPOUNDJ MC3atSKXSE»^£3ES
! Phenol___2-Chlorophenol________154-DichlQrobenzen©___N-Nitroso-di-n-prop.(1)1?254-Trichlorobenz»ne_4-Chloro-3-methylphenolAcenaphthene_________4-Nitrophenol______- _._2«4-DinitrotoluenePentachlorophenol_____Pyrene___. _____._ -
SPIKEADDED(ug/Kg)£»« 35s=za:
7240724036203620362072403620724036207240362O
MSD J MSDCONCENTRATION! %
(ug/Kg) J REC #
3o 5393
84
i U1
RPD #
1*4.13-6-
QC LIMITSRPD
50273823331950474736
REC.
26- 9025-10:2S 104!41 126!39 107!26 103131-137!11-114128- 89!17-109!35-142!
(1) N-Nitroso-di-n-propylamine
# Column to be u*»d to -flag recovery and RPD valuem with an asterisk* Value* outside o-f QC limits -
: QHs out o-f 11 outside limitsSpike Recovery: \ S* out o-f 22 outside limits
COMMENTS : BC-6-4 URSINSTsF SWL83678.33
FORM III SV-2 - 1/87 Re
flR-l-ai58
3DSOIL SEHIVQLATILE MATRIX SPlKE/MAfRIX SPIKE DUPLICATE RECOVERY
Lab Name: SWL-TULSA______________ Contract: URS_______
Lab Code: SWOK Case No.: URS SAS No.: ______ SDB No.:
Ma. ,x Spike - EPA Sample No.: BC-7-2______ Level:<low/med) LOW
COMPOUND
Phenol2-Chloroohenol1 ,4-DichIorobenzeneN-Nitroso-di-n-prop. ( 1 )1 ,2,4-Trichlorobenzene_4-Ch 1 oro-3— me thy 1 pheno 1Acenaohthene4-Nitroohenol2. 4-Din itro toluenePentachlorcohenolPvrene
SPIKEADDED(ug/Kg)
912091204560456045609120456091 2O456091204560
SAMPLECONCENTRATION
(ug/Kg)
880000000
. 0000
MS ! MSCONCENTRATION! 7.
(ug/Kg) ! REC *
IfTo-ros* me*Tl3o 7SG£ ! 5 34-UH&3TO6 !C»tW"3*40«4£ W-953if3o3-&aO. H5&A
*)H*lo TS kO ! ZS4."31 GO -TO 1-6 s Sa.es.^ fD~l 1 flJ l l Ifcfi V 7?^ — itU
Sio " jj o rw 7t
QC !LIMITS!REC. !
26- 90!25-102!28 104!41 126!38 107!26 103!31-137!11-114!28- 89!17-109!35-142!
COMPOUND
Phenol2-Chlorophenol1 ,4-DichlorabenzerieN-Nitroso-di-n-prop. ( 1 )1 ,2,4-Trichloroben2ene_4-Ch loro-3-methyl phenolAcenaphthene4-Nitrophenol2 ? 4-Din itro toluene ____PentachloroDhenolPyrene
SPIKEADDED(ug/Kg )
18300 "18300914091409140183009140183009140183009140
MSDCONCENTRATION
(ug/Kg)
117001020060705240588O111005890111006 ISO130006720
MSD !X ! 7.REC #! RPD $
59 Pfe-fe> -*56 !3 4S*66 ! 3 MS.57 IMS* *64 !lUS561 J^I-SS *•64 !M*3i *61 ffl«t 34-68 ! )4 S*-71 !3S«S-*74 ! 1 -4.
ii
DC L]RPD
3550273823
195O474736
[MITSREC,
26- 9025-10228 10441 12638 10726 10331-13711-11428- 8917-10935-142
(1) N-Nitroso-di-n-propylamine
# Column to be used to -flag recovery and RPD values with an asterisk* Values outside of QC limits
RpD: Q "S out of 11 outside limit'sSpike Recovery: o » out of 22 outside limits
COMMENTS: BC-7-2 URSINST:F SWL83678.25
J/ .1
FORM III SV-2 1/87 Rev.
0000506
flRIOl582
3FSOIL PESTICIDE' MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Names SWL-TULSA______________ Contract: URS______
Lab Code: SUJQK Case No.: URS SAS No.: ______ SDG No.:
Matrix Spike - EPA Sample No.: BC-6-4_____ Level i (low/med) LOW
COMPOUND
aamma-BHC (Lindane)HeotachlorAldrin
' DieldrinEndrin _ _4. A * — nnT~T * T MM 1
SPIKEADDED(ug/Kg)
5.785.785.78
14.514.514. =;.Jk T • J "
SAMPLECONCENTRATION
(ug/Kg)
00OO0-u
MSCONCENTRATION
(ug/Kg)
6.4610.81.823.794.747.50
MS ! QC !7. [LIMITS!
REC #! REC. IrSSSSSX J 3KM353 ———— j
112 J46-127!187 *! 35-1 30!31 *!34-132!26 *!31-134!33 * 142-139!&*^ t TT i T A iU*. i 2si 1 -?4 i
1 11 1
{:{ COMPOUND
g »mma-BHC ( Lindane ) ___HeptachlorAldrin
t DieldrinI Endrini 4,4'-DDTii
SPIKEADDED(ug/Kg)
SEKS3»atat3KK
5.785.785.7814.514.514.5
MSDCONCENTRATION
(ug/Kg)SBXEa^SCKESKaraB
7.6810.11.715.544.756.8O
MSD'/.
REC *s»ssa
133 *175 *30 #3833 *47
'/.RPD #
azaaeixats
-1773
-38010
•
QC L]RPD
503143384550
iEMITS {
REC. '».*» A46-12.135-13034-13231-13442-13923-134
# Column to be used to flag recovery and RPD values with an asterisk
* Values outgide of QC limits
RPD: _0 out of _^ outside limitsSpike Recovery: _B out of _12. outside limits
COMMENTS:
FORM III PEST-2 :- 3/87 Rev
£00050
fl-R-1'01583 -
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Names SWL-TULSA______________ Contract: URS _____
Lab Code: 3WQK Case No.: URS SAS No.: ______ SDG No.:
Matrix Spike - EPA Sample No.: BC-7-2_____ Level:<low/med) LOW
COMPOUND
aamma-BHC (Lindane)HeDtachlorAldrinDieldrinEndrin4.4'-DDT
-
SPIKEADDED(ug/Kg)
7.197.197. 1918.018.018.0
SAMPLECONCENTRATION
(ug/Kg)
O00O00
MSCONCENTRATION
(ug/Kg)
9.074.69A- m J-±
7.439.4213 . 4
MS7.REC #
1266531 *4152
. 74
QCLIMITSREC.
46-12735-13034-13231-13442-13923-134
~
COMPOUND
qamma-BHC ( Lindane )HeptachlorAldrinDieldrinEndrin4.4' -DOT
SPIKEADDED(ug/Kg )
7.197.197. 1918 1018.018. 0
MSDCONCENTRATION
(ug/Kg )
2.066.954 . 3713.916.620 . 7
MSD
REC 3
29 *97617792115
XRPD #
125 *-4O *-65 *-61 *-56 *-43
QC LRPD
503143384550
EMITSREC.
46-12735-13034-13231-13442-13923-134
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: _5 out of _6 outside limitsSpike Recovery: _2 out of 12 outside limits
COMMENTS;
FORM III PEST-2 B/87 Rev.
0TQ0050S
IS AMERICAN AKALYTICAl fc TECHNICAL SERVICES
MAIRII SPIKE EVALUATION FORK
URS
S&HPLE ID BC-6-4HS
K£T HT. 10.0
atotmt «ount Mountng in spi. idderf detected Z TARGET
added ppt ppt ppt recovery recovery liiits2371 TCDF 2.5 0 250 285.3 114 iO - 140 IHPCDF 10 0 1000 t4ii.fr 144$ 40 - 140 1OCBF 25 0 2500 34B9.0 1481 40 - 140 I
2378 TCDD 2.5 0 250 379.9 1321 40 • 140 IPCDD 10 0 1000 1334.4 133 40 - 140 1HXCDS 10 0 1000 1424.5 142* 40 - 140 I
DUPLICATE SAMPLE EVALUATION
SAMPLE ID BC-4-4HS BC-4-4HSD
KT «T. 10.0 10.0
atount iiount RPDin spl. in spl.ppfc ppt
2378 TCDF 285.3 313.4 9.5HPCDF 1441.0 1099.0 28.3OCDF 3489.0 3415.0 2.0
2378 TCDD 379.9 287.7 27.4PCDD 1334.4 1144.0 13.5HICDQ 1424.5 1493.7 17.3
\ tl u I
ISO AMERICAN AHAUTIML 4 TECHNICAL SERVICESHATRU SPIKE EVALUATION FORM
URS
5AHPLE ID BC-4-4HSD
«ET *T. ' 10.0
iiount aiount uountnq in spl. added detected Z TfiRSET
added ppt ppt ppt recovery recovery 1nits237B TCDF :.5 0 250 313.4 125 60 - 140 XHPCDF 10 0 1000 1099.0 110 60 - 140 I(OF 25 0 2500 3415.0 1451 40 - 140 I
2378 TCDD 2.5 0 - 250 287.7 115 40 • 140 ZPCDD 10 0 1000 1144.0 117 40 - 140 ZH2CDD 10 0 1000 • 1493.7 i49t 40 - 140 Z
DUPLICATE SAHPLE EVALUATION
SAHPLE ID BC-4-4HS BC-4-4HSD
MET »T. 10.0 10.0
itount iiount RPDin spl. in spl.ppt ppt
2378 TCDF 285.3 313.4 9.5HPCDF 1441.0 1099.0 28.3QCDF 3489.0 3415.0 2.0
2373 TCDD 379.9 287.7 27.4PCDD 1334.4 1144.0 13.5HKCDD 1424.5. 1493.7 17.3
flR 101 5.8.6
MS AMERICAN ANALYTICAL I TECHNICAL SERVICES
HATJtII SPIKE EVALUATION FORK
URS
SAKPLE ID BC-7-2«S
MET XT. 10.0
KT. 10.0 10.0
iiount iicunt Mountn§ in spl. added detected Z TARGET
iddtd ppt ppt ppt recovery recovery liiits2371 TCDF 2.5 0 250 233.4 113 40 - 140 ZHPCDF 10 0 1000 1115.0 112 40 - 140 ZOCDF 25 0 2500 3129.0 125 40 • 140 Z
2378 TCDO 2.5 0 250 343.3 137 40 - 140 ZPCDD 10 0 1000 1155.8 114 40 - 140 ZHXCDQ ID 0 1000 1485.4 149t 40 - 140 Z
DUPLICATE SAHPLE EVALUATION
SAKPIE ID BC-7-2K3 BC-7-2RSB
atount uount RPDin spl. in spl.ppt ppt
2373 TCDF 283.4 312 9.5HPCDF 1115.0 1125.0 .9OC3F 3129.0 370B.O ' 14.9
2379 TCDD 343.3 341.3 5.1PCD0 1155.B 1190.8 3.0HXCDD 1495.4 1852.4 9.4
00031 iAR.LOLI.587
-SB .AMERICAN ANALYTICAL 4 TECHNICAL SERVICES
HATRIX SPIKE EVALUATION FORM
URS
SAHPLE ID BC-7-2HSD
WET NT. 10.0
iiount atount atountng in spl. idded detected Z TARGET
idfled ppt ppt ppt recovery recovery Huts2378 TCDF 2,5 0 250 312 125 40 - 140 ZHPCDF 10 0 1000 1125.0 • U3 40 - 140 ZOCDF 25 0 2500 3708.0 1481 40 - 140 Z
2378 TCDO 2.5 0 250 341.3 145t 40 - 140 ZPCDD !0 fr 1000 1190,8 119 40 - 140 ZHXCDO 10 0 1000 1852.4 ISSt 40 - 140 Z
DUPLICATE SAMPLE EVALUATION
SAHPLE ID 8C-7-2HS BC-7-2HSD
NET NT. 10.0 10.0
iiount atount RPIin spl. in spi.ppt ppt
2378 TCDF 283.4 312 9.5HPCDF 1U5.0 1125.0 .9QCDF 3129.0 3708.0 14.9
2378 TCDD 343.3 341.3 5.1PCDD 1155.8 1190.8 3.0H1CDO 1485.4 1852.4 9.4
U.S. EPA - CLPEPA SAMPLE
6 ::DUPLICATES
MU7S32DLab Name: SOUTHWEST LAB OF OK Contract: 68-D9-O039 _fiL'-il-l___.
Lab Code: 3WQK Case No.: 36761 SAS No.: 5DS No.: MU7801
Matrix (water/soil): SOIL Level (low/med): LOW
*/. Solids far Sample: 92.1 % Solids for Duplicate: 92.1
Concentration Units (ug/L or mg/kg dry weight): MG/KG
i) Analyte
! Aluminum! Antimony! Arseni c} BariumJ B©ryl 1 i umt Cadmium1 Calcium1 ChromiumJ CobaltI Copper! Iron! Lead! MagnesiumEMangangss! MercurySNickel; PotassiumJ Selenium! Si 1 v©ri SodiumI Thallium! VanadiumIZinc[Cyanideti
ControlLimit
2.2
•
1'O.S4.3
-
Sample (S) C!
4646. 4307! ,5.5901 !U!l . 2234 ! B !16.7191 IB!.4229JB!. 645O ! U !
156.3603IB!/ • 0000 * i3.5501 IB;3.4401 !U!
13728.9170! f3.6469! !
135- 9334! 91177.9587! !
. 1150JU!4. 3087! Bi
217.9754JB!. 430O ! U 1.9391 !B!
137.0512JB!. 6450 ! U I
12. 4945 J !10.1195! i1 .98S61U!
iDuplicate <D> C!
4363.8708! !12.8291 IB!1.6178JB!14.9548JB!. 4689 { B !.6515IU!
109.4148!B!13.6247! !5.7253IB!4.9418JB!
18229.4650! i4. 2150 f I
1 19. 8473! B!243.76O5J !
. 1085 !U!5. 1274 !B!
165.7213IBJ. 4799 ! B J
1.2397IB!94. 3032! B!.6515!U!
14.9479: !12.6690! !1 . 7289 ! U !
6.3200 . 027.811.11O.3
T^ T
53.446.9
200. 028.214.512.6-"^1.2
i. 427. 2
200. 027. 637.0
17.922.4
•
1
0!«!PI o( ~
!F!PIP!P!P j
*!P i!P;p
*!P!FiP
*!P!CV;P;P1 i ~!PIPIFfPIP:c
FORM VI - IN7/SS
.,,,,,_ 8-00051nR i u i 088
U.
5A EFASPIKE SAMPLE RECOVERY
! MU73Lab Nams: SOUTHWEST LAB OF OK' Contract: 68-D9-0089 \ fiC-W-
Lab Code: SWOK Case No.: 367S1 SAS No.: SDG No.: r-;U73<.-l
Matrix-: SOIL " .. ^ "~ _ Level flow/med > : ":_3W
% Solids tor Samolez" 91.5
Concentration Units (ug/L or mg/kg dry weight): MS/KC3
! Analyte
! Al umi HLim1 Antimony; Arsenic: Ban U.T;-: Beryl 1 ium! Cadmium; Cal ci um! Chromi um! Cobalti Capper< Iron.' Lsad! Magnesium! Manganese' Msrcurv! Nickeli Potassiumi Seleniumi Si 1 ver: SodiumI Thai 1 1 um: Vanadi umi 2 i n c •! Cyani ciei
ControlLimit7.R
75-12575-125~7ef— 1 •"!"=;/ j i -—•-./75-12575-125
75-12575-12575-125
75-125
75-12575-125
75-12375-125".
75-12575-12575-12575-125
So iked SampleResult CSSR)
79.33316. 9727
497.715812.O99015.8869
55.2387127. 110665.7576
Q T' TTt?
579.8893. 084O
123.7382
1 . 25258.9202
1 1 . 9257128.6896126.319320.8341
C
U
~~
Samp 1 eResult (SR) C
;12. 4853 IB1 . 3727 ! B
23. 4055 iB.3941 IE. 6557 i U
•6.6758!6. 9369 IB3.4973JU
!o * - 1 Q V *
t487.5951 i
. 0993 \ U4. 7480 IB__.... ._. i.4372 ! U
1. 1603 IB— - . ,
. 6557 I U11. 1026!9.6251 I2.0239IU
I
Spike :Added <SA) !
1 i109., 298.74
437., it10.9310. 93
• 43.72109 ,,2954.64
4 37
109. 291 , OO
1 09 „ 29
2. 191 0 ., 93
1 0 „ 93109- 291 09 „ 2921,. 60
1 1 •
:'.R • Q : M :
I INR!5 i . 6 . N ! P :s4. : :M;F j-.03.5; ,P ;;07. 1 . IP I145. 4:N!P !
. ; NR :111.2! IP !i i 0 . o : IP !120. 7 ' .: P !
. I NR !i 1J-. 3 IF !
. I NR !>O. *5 I IP I0. 'JiNlCV!
Iv8. "' IP !INR!
57. C NIF J71 .». M:P ;
. I NR I1 'I 9 . 1 - : F . !I 07. ,T. !P iJLV6.3 P i56.'.;; :c Ii• i
Ji• '
Lommenrs:
FORM V (Part 1) - IN
0-00051.1ARi01590
U.S. EPA - CLPEPA SAMPLE N
6 ____ „__* DUPLICATES
MU7S33DLab Name: SOUTHWEST LAB OF OK Contract: 68-D9-OO89 _C£i&T.iL___.
Lab Code: 5WOK Case No.: 36781 SAS No.: " SDG No.: MU78O1
Matrix (water/soil): SOIL Level (low/med): LOW
7. Solids -for Sample: 91.5 */. Solids for Duplica-e: 91.5
Concentration Units Cug/L or mg/kg dry weight): MG/KBiI Analytei*i Aluminum[Antimony1 ArsenicI Barium! Beryl 1 ium! CadmiumI Calcium! ChromiumI CobaltI Capper! IronILead1 MagnesiumI ManganeseI t^ercuryINickelI Potaseiumf Sal gniumI Si 1 ver! SodiumJ Thall ium! VanadiumIZincI Cyanidei
ControlLimit
2. 2
.7
•
10.94.4
11Sample (S) CI
!4346.6061! !
12. 4853! E!1 . 3727 I B !
23. 4055 JB!.3941 IB!. 6557 ! U i
100. 0753 IB!6. 6758 J I6. 9369! B!3. 4973! U!
14542.368O! !3.2109! I
187.9976iBI437.59511 !
. O993 I U I4-748OJB;
267. 3667 IB I. 4372 ! U !
1. 1603! B I94.2277EB!
. 6557 I U I11. 1026! I9.6251! !T> «*\*?T1Q Ml1-i. Vjiwv » U »
i it i
ii
Duplicate "£D> C!i
3745.9021 : !12.49321BIl.O9~29!U!
21. 8287 IB!. 3987 ! B I. 6557 I U I
99.3719IB!7.1878! 16.O304IB!3.7858IBI
13133.4110! I2.7060! !
179.5024IBI419. 15561 i
. O993 I U !3.3285131
248. 3855 IB!. 43721 U I
1. 1126 IB!8O.2186IU!
. 6557 I U I10. 30051 E I9.1568! I2.0543IU!
< t
XRPD
14. S. 1
20O.O7,01.2
_. 77.414.0200.010.217. 14.615. 1~r,~\ "35.27.5
4 r>2OO . 0
7.55.0
I Ii r
QittiiIPIP!FIPIP-IPIPIPIPIPIPIFIPIPicv!P!P.IFIPIPIF!PIP1Cii
FORM VI - IN7/88
U.S. "EPA - CLP
5A EPA SAMSPIKE SAMPLE RECOVERY
- . --- --- - - I - MU7S25SLab Name: SOUTHWEST LAB OF OK Contract: 63-D9-0089 I
Lab Code: SWOK Case No.: 36781 SAS No.: SDG NO.: MU7801
Matrix: SOIL - .. Level (lcw/msd> : LOW
'•i Sol ids -for Sampl e: 75.6 :
Concentration Units tug/L cr mg/kg dry weight): MG/KS
111t
! Anal yteiii Al uminumI Anti manyI Arsenici Bari urn! Beryl 1 ium! Cadmium! Cal ci um! Chromi um
kl Cobaltml Copper\\ Irony I Lead! Magnesium1 ManganeseI MercuryINickel; Potassium\ SeleniumI Silver! Sodi um! Thai lium! Vanadium; ZYhcI Cyani de• _
ControlLimity.R _
75-12575-12575-12575-12575-125
75-12575-12575-125
75-125
75-12575-12575-125
75-12575-125
75-12575-12575-12575-125
3pi ked SampleResult <SSR>
43.81347.9601
646.335615.161013. 1264
76.37.21151.82248 1 . 6300
18.9193
485. 1221. 1017
168.9687
.523911.2276
14.3852184.719O165. 596626.3896
C
U
U
Samp 1 eResult (SR) C
i•16.O99B!i . 322S ! U87.4473;
,9122 IB. 7937 i U
i19.4224!S . 6730 ! B7.4502!
ii15.50261
t315. 1506;
. 1150IU20.07161
i.5291 iU
i . 5722 ; Bi
. 7937 I U37.5476; _O1™^ TT^T * I^ *i. . •_'•_' •_> i i2. 3963 I U
i
So i keAdded <SA)
130. 9710.48
tJ-£C- . OC5
13. 10i T ^ t~\i •-» . - V
52.39130.9765.43
5.24•130.97
1.00130.97
2.6213. 10
13. 10130.97130.9725. 15
7.R
:? 1 •"?7 is . 0
1 06 . 7108.8138. 4
1 08 . 7109.3113.4
65.2
129.30 . 0
113.7
0 . 073, 7
. 109. G112.4109.41 04 . 9
I1
Q!MiiINR
N ! Pr- cr; PI P
NIPINRIPI F'IPINR
NIF!NR
NIFNICV;pINR
NIFN I P
; NR; p
IPp
f c ;1 . .
Commentsj
FORM V (Fart 1 ? -^ IN
ARID,592
U.S. EPA - CLPEPA SAMPLE N
6, DUPLICATES !
i MU7E25DLab Names SOUTHWEST LAB OF OK Contract: 68-D9-OOS9 I 6t->2,
Lab Code: 3WOK Came No.: 36781 SAS No.: SDG Nc.: MU7SO1
Matrix (water/soil): SOIL Level Clow/med): LOW
7. Solids -for Samole: 75.6 7. Solids for Duplicate: 75.6
Concentration Units £ug/L or mg/kg dry weight): MG/KG
J
! ! Control! Analyte ! Limiti *i i1 Aluminum I; Antimony I 15.9I Arsenic i(Barium ! 52.9I Beryl lium! 1.31 Cadmium !I Calcium II Chromium J.'Cobalt ! 13.2! Copper I 6.6ilron I! Lead I! Magnesium!I Manganese I.Mercury :INickel I 10.6; Potassium II Sel en ium :! Si 1 ver'.Sodium iI Thai lium !! Vanadium 1 13.2JZinc ! 5.3! Cyan id© !' I< *
Sampl© (S) C
25121.3620!16.0998!1 . 3228 ! U87.4473!
-9122SB. 7937 ! U
400. 4679 !B19.4224!8. 6730 IB7.4502!
20344. 1900!15.5026!
671. 7352 IB315. 1506!
. 1150IU20.0716!468. 6218 IB
.5291 IU1 . 5722 ! B
227. 1672 IB. 7937 I U
37.5476!22.3331J2. 3963 I U
i
Duplicate (D> C
31856.3160!18.5799!2.36771997.2592!1 . 3274 I1.2191IB
463. 1079 !B26.3699!13.4489!10.6197!
31775.5910:14.8545!
317. 4666 IB451.673S!
. 1017IU3G.2025!515.0419IE
.5291 IU2.4201 IB
157.7153IB. 7937 ! U
56.6599!31.6140!2. 5052 I U
ir
•/.RPD
23.614.3
20O. 010.637. 1200.014.530.343.235. 143.94. 319.635. <b12.240 . 39.4
42.536. 1
40. 634.4
1 11
QIMi
*!P;PIFIFIPIP!P
*!PIPIP
*!PIFIP
# ! PICVf P! P'IF!PIPiF
*!P*!P1C(
FORM VI - IN7/as
0-000517A R I OT5W ~ ~ ~"
U.S. EPA - CLPEPA SAMPLE NO.
6 _______DUPLICATES ! " ~!
! MU7326D ;Lab Name: SOUTHWEST LAB OF OK . Contract: 63-D9-0089 ! .JL -Jtl____:
i_ab Code: SWOK Case No.: 36761 SAS No.: 5-DG No.: MU7S01
Matrix- (water/soi 1 ; : SOIL Level (low/med) : LOW
'/ Solids -for Sample: 79.B 7. Solids tor Duplicate: 79.6
Concentration Units (ug/L cr mg/kg dry weight): MG/KG
11
! Analyte
: Al umi numi Antimony! ArsenicI BariumI Beryl 1 ium! Cadmiumi CalciumI Chromiumi CobaltI CopperI IronI LeadI Magnesi um! ManganeseI MercuryI Nickel! PotassiumI SeleniumI Si 1 veri Sod i umI Th a i 1 i um! Vanadium! Zinc! Cyan! deii
ControlLi mi t
14". 9
49.6
6.2
"
9.9
12.45.0
Sample <S) C
20O1 9 . 240O !' 22. 3234 i
1 . 2407 ! U78.8315:. 7320 ! B. 7444 ! U
382. 1595!B25.9492!9.0070137.8232!
26644.6380!12.0O44!
953. 01 00 IB228.56521
. 10891019.9041 I
523.3804! B4.9629IU2.055913
166.7619IB.7444 I U
35.3649!24.4604!2.4O06IU
>
Duplicate (D) C
: 23014- 5900!20. 9739!2.4417!B66.3145!
. 9493 I B
. 7444 I U415. 2675 IB21.8126!12. 1154 IB7.79O3!
30717.7240!13.0946!
798. 4257 IB400.960O!
. 0963 I U14.0933!
569. 4953 !B. 4963 ! U
2.30OOIB152.6615SB
. 7444 ! U33.7432!26. 1872!2. 1606 iU
!
•/.RPD13.9a. 4
200 . o.17.225.8
83• •— '17.329.4. 4
14.28.717.754.846.234. 23 . 3
11.2a. (39. 16. 3
r
!Q
!i!!!i!I!iiiiii
!*!!1iiiir
it
i!I
M
PPFPPPPPPpPFPPCVPPFPF'crPPr*
FORM VI - IN7/88
£-000513
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: SOUTHWEST LAB OF OK Contract: 68-09-0089
Lab Coae: SWOK Case No.: 367E1 5AS Ho.: = DG Mo
Soli a LCS Source: EPAO237
Aqueous uCS Source:
1
Anai viz©
AluminumAnri.TionvArmsnicBariumBervi liumCadmium
1 Calcium•J Chromi um^/CobaltJCoopsrI Iron!Le*dJ MagnesiumJ Manganesei MercurvlNick»l! PotassiumI SeleniumS SilverI Sod iumI Thai 1 iumI Vanadiumi ZincI Cyanidei
Aqueous (ug/L)True Found "CR
t.
!
~
Solid (mg/kg >True Found C Limits */.R
325.0! 270.3!211.0! 207.7!917.0! 659.2!
4R * ^i "? f R. O ' *J. •— • I O
19.4! 19.2! .45.4! 48.2!
196200.01 197950.0!99.6! 103. 1!144.0! 137.3!6910.0! 7138. O!22430.01 19675.5!
236. Oi 240.7!118100.0! 12241O.O!
208.0! 211.7!12.71 12.5!60.9! 50. B!50. 0! 69.0 JUTO *? ' - T7 jL t•_> v . *i. i •_• / . C i
22.2! 20. 6 i50.0; ' 73. 4! U39.0! 29.6!65.8! 64.7!
187. 0! 151.0!5.61 5.71
i •
225 . 0127.0635 . 00. 0
16.535.7
166800.079.2
124.06OO6. 017770.0
188. 01.0O4OO . 0
177.03.5
49.20. 019. 115.50 . 0
24.651.7
1 33 . 04.3
424. ! : 83.2r94.v! 93.41199.0. 71.940. O: i 10.422.71 99.053. 1 ; 106.2
22560O.O! 100.9120.01 IQT^
16- v: 7aro. v ic H27030.-.'! So2S5.O: 102.0
1Z9900. :•: 103.639. :-: 101.5:7. :-; 93.472. h. F53.4
' ''.'OO. '"' ' 0* C59.*. '"5.9Z9.OI ?2.8
iooo. . . o.o-* 'j- . -re- a_l^._.- / _J • 7
"o. 9 ; 98. 3Zo. .•: SO. 7o . ° : 1 0 1 . S
FORM VII - IN 7/es
flRIO!595
U.S. EPA .- CLP
7LABORATORY CONTROL SAMPLE
Lab Name: SOUTHWEST LAB OF OK Contract: S8-D9-OOS9
Lab Code: 5WOK .___. Case No.: 367S1 3AS No.: SDG No.: MU7301
Solid LCS Source: EPA02S7
Aqueous LCS Source:
1
i AnalytetJ Aluminum! AntimonvI Arseni c! Bari umI Beryl 1 ium! Cadmium! Calcium
V ChromiumJ Cobalt
! Copper! IronI Lead! MagnesiumI Manganese! Mercury! NickelI Potassium! Seleni um! Si 1 ver! Sodium! Thai! ium! Vanadi umiZincICyani dei
Aqueous Cug/L)True Found XR
'
Solid (mg/kg)True Found C Limits 7.R
5.6 5.9
:
4.3 =>.9 105.4
FORM VII - IN7/BS
#0005 0
t nP. ID1594>
SOUTHWEST LABORATORY OF OKLAHOMA, INC.7700 W. Albanv . Suitf "C" . Broken Arrow. Oklahoma 74012 . 918-251-2858 . FAX: 918-251-2599
ANALYTICAL REPORT
URS CONSULTANTS, INC. REPORT: 3678-1570 Delaware AvenueBuffalo, New York 14202
REPORT DATE: 10/05/90
SAMPLE NO.: 3678.01 - 3678.39DATE RECEIVED: 09/08/90
fl&ZQC
DESCRIPTION PARAMETER RESULTS
MATRIX SPIKE BC-7-2 ' TOTAL SULFIDE ' 44% RECOVERYMATRIX SPIKE BC-6-4 TOTAL SULFIDE 43% RECOVERSMATRIX SPIKE BC-6-1 TOTAL SULFIDE 64% RECOVERY
DUPLICATE BC-6-4 TOTAL SULFIDE 5.2% RPDDUPLICATE BC-6-4 TOTAL SULFIDE 31% RPDDUPLICATE BC-6-1 TOTAL SULFIDE 9.6% RPD
A R I O I 5 9 7 frT)C052i
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700W.Albanv . Suite "C" . Broken Arrow, Oklahoma 74012 , 918-251-2858 , FAX: 918-251-2599
ANALXT1CAL..PEPQET
"RS CONSULTANTS, INC." REPORT; .3677-1570 Delaware AvenueBuffalo, New York 14202
REPORT DATE: 10/02/90
SAMPLE NO.: 3677.01-- 3677.04DATE RECEIVED: 09/08/90
QA/QC
OKCRIEXIQH PARAMETER RESULTS
TCLP BLANK 09/13/90 ARSENIC -:0.05 mg/LTCLP BLANK 09/13/90 BARIUM <0 .02 mg/LTCLP BLANK 09/13/90 CADMIUM <0.005 mg/LTCLP BLANK 09/13/90 CHROMIUM <0 . 005 mg/LTCLP BLANK 09/13/90 ' LEAD <0.05 mg/LTCLF BLANK 09/13/90 MERCURY <0.0002 mg/LTCLP BLANK 09/13/90 SILVER <0.01 mg/LTCLP BLANK 09/13/90- SELENIUM : <0-05 mg/L .
BLANK SPIKE - 09/16/90 MERCURY _ . 106% RECOVERY
MATRIX SPIKE DC-1 REACTIVE SULFIDE 117% RECOVERYMATRIX SPIKE DC-1 REACTIVE CYANIDE 0% RECOVERY
0-DC05f l R i n i 5 9 8
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. REPORT: 3677*570 DELAWARE AVENUEBUFFALO, NY 14202 DATE: 10-02-90ATTNs PETER FAIRBANKS
SAMPLE MATRIX! E.P. TOX EXTRACTION FLUIDSWLQ * E.P. TOX METHOD BLANKDATE EXTRACTEDJ 09-12-90DATE ANALYZED! 09-16-90METHOD REFERENCES SWB46-8150, EPA METHODOLOGYSAMPLE IDs E.P. TQX BLANK
RESULTS REPORTED IN mg/1 OR Parts Per Million
E.P. TOX DET.HERBICIDES___________LIMIT___________RESULTS
2,4-D 1.0 ND2,4,5-TP (SILVEX) 0.1 . ND
QA/QC SURROGATE RECOVERY
2,4,5-T 741/.
ND « NOT DETECTED ABOVE QUANTITATION LIMITJ » ESTIMATED VALUEl CONCENTRATION BELOW LIMIT OF QUANTITATIQNB m ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE* - SURROGATE RECOVERY OUTSIDE OF QC LIMITS
A R I O I 5 9 9 0-00052J
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. " REPORT s 3677b570 DELAWARE AVENUEBUFFALO, NY 14202 DATE: 10-02-90ATTN: PETER FAIRBANKS
SAMPLE MATRIX: WATER .SWLO * METHOD BLANKDATE EXTRACTED: 09-12-90DATE ANALYZED: 09-16-90METHOD REFERENCE: SW846-8150, EPA METHODOLOGYSAMPLE ID: METHOD BLANK
RESULTS REPORTED IN mg/1 OR Parts Per Million
E.P. TOX DET.HERBICIDES___________LIMIT _________RESULTS
294-D 1.0 ND2,4,5-TP (SILVEX) 0.1 ND
QA/QC SURROGATE RECOVERY
2,4,5-T 797.
ND « NOT DETECTED ABOVE DUANTITATION LIMITJ = ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATIONB « ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE* = SURROGATE RECOVERY OUTSIDE OF QC LIMITS
f l R I O l S O O#000521
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. REPORT: 3677c
DATE: 10-03-90
SAMPLE MATRIX: SOIL, E-P. TOX EXTRACTIONSWLO # 3677.02/3677.03 (MS/MSD)DATE EXTRACTED! 09-12-90DATE ANALYZEDs 09-16-90PROJECT: DELAWARE SAND & SRAVELSAMPLE IDi DC-1 (MS/MSD)
HERBICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS
MSSPIKE ADDED AMT. FOUND AMT. FOUND PERCENT
(ug/1) SMP. (ug/1) MS (ug/1) RECOVERY
2,4-D 97 0 68 70'/.2,4,5-TP (SILVEX) 25 0 20 SI'/.
MSDAMT. FOUND PERCENT RECOVERY PERCENTMSD (ug/1 ) RECOVERY DIFFERENCE
2, 4-D 6B.5 71% 0.6%2,4.,5-TP (SILVEX) 17.8 71"/. 12. 5"/.
AR I 01601 #'000520
SOUTHWEST LABORATORY OF OKLAHOMA, INC1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. REPORT: 3677d570 DELAWARE AVENUEBUFFALO, NY 14202 DATE: 10-03-90ATTN: PETER FAIRBANKS
SAMPLE MATRIXs E.P. TOX EXTRACTION FLUIDSWLO # E.P. TQX BLANKDATE EXTRACTED? 09-12-90DATE ANALYZED : 09-17-90PROJECT: DELAWARE SAND & GRAVELMETHOD REFERENCES SW846-8080., EPA METHODOLOGYSAMPLE ID: E.P. TOX BLANK
RESULTS REPORTED IN mg/L OR Parts Per Million (PPM)
PESTICIDES/PCB'S DETECTION LIMIT ; RESULTS
GAMMA-BHC 0.040 NDHEPTACHLOR 0.0008 NDENDRIN 0.002 NDHEPTACHLOR EPOXIDE 0.0008 NDTECH CHLORDANE ' O.OO3 NDMETHOXYCHLOR 1.0 NDTOXAPHENE 0.050 ND
QA/QC SURROGATE RECOVERIES
DIBUTYLCHLORENDATE ( 24-154) 857.
ND « NOT DETECTED ABOVE QUANTITATION LIMITJ « ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATIONB « ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE* « SURROGATE RECOVERY OUTSIDE OF QC LIMITS
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. ' REPORT: 3677©570 DELAWARE AVENUEBUFFALO, NY 14202 DATE: 10-03-90ATTN: PETER FAIRBANKS
SAMPLE MATRIX: WATERSWLO # METHOD BLANKDATE EXTRACTED: 09-12-90DATE ANALYZED J 09-17-90PROJECT: DELAWARE SAND «t GRAVELMETHOD REFERENCES SW846-8080, EPA METHODOLOGYSAMPLE ID: METHOD BLANK
RESULTS REPORTED IN mg/L OR Parts P«r Million (PPM)
PESTICIDES/PCB'S DETECTION LIMIT RESULTS
GAMMA-BHC 0.040 NDHEPTACHLOR 0.0008 NDENDRIN 0.002 NDHEPTACHLOR EPOXIDE 0.0008 NDTECH CHLORDANE 0.003 NDMETHOXYCHLOR 1.0 NDTOXAPHENE 0.050 ND
QA/QC SURROGATE RECOVERIES
DIBUTYLCHLORENDATE (24-154) 66'/.
ND - NOT DETECTED ABOVE QUANTITATION LIMITJ - ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATIONB - ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE* - SURROGATE RECOVERY OUTSIDE OF QC LIMITS
ARIUTBUT #"000527
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. REPORT: 3677f570 DELAWARE AVENUEBUFFALO, NY 14202 DATE: 10-03-90ATTN: PETER FAIRBANKS
SAMPLE MATRIX: SOIL, E.P. TOX EXTRACTIONSWLO # 3677.02/3677.03 (MS/MSD)DATE EXTRACTED: 09-08-90DATE ANALYZED: 09-17-90PROJECT: DELAWARE SAND & GRAVELSAMPLE IDs DC-1 (MS/MSD)
PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULTS
MSSPIKE ADDED AMT. FOUND (SAMPLE) AMT. FOUND (MS) PERCENT(ug/L) (ug/L) (ug/L) RECOVERY
GAMMA-BHC 1.00 0 0.60 607.HEPTACHLOR i. 00 0 0.66 667.ALDRIN 1.00 0 0.66 66'/.DIELDRIN 2.50 0 1,47 597.ENDRIN 2.50 0 1.70 717.4,4'-DDT 2.50 0 1.69 687.
MSD RELATIVEAMT. FOUND (MSD) PERCENT PERCENT
(ug/L) RECOVERY DIFFERENCE
GAMMA-BHC . 63 637. 4«97.HEPTACHLOR .72 727. 8.7%ALDRIN .70 707. 5,97.DIELDRIN 1.56 627. 5,97.ENDRIN 1.83 737. 2,87.4,4'-DOT 1.88 757. 10.67.
f l R I O I G O U . . /H>005:
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. , REPORT: 3676c570 DELAWARE AVENUE .BUFFALO, NEW YORK 14202 DATES 09-19-90ATTNi PETER FAIRBANKS
SAMPLE MATRIX: WATERStfLO * METHOD BLANKDATE ANALYZED i 09-12-90METHOD REFERENCES SW846-S240, EPA METHODOLOGYSAMPLE ID: METHOD BLANK
RESULTS REPORTED IN ug/L OR Parti P«r Billion (PPB)
TOLP DET.VOLATILEi LIMIT RESULTS
BENZENE 5 NDCARBON TETRA CHLORIDE 5 NDCHLOROBEMZENE 5 NDCHLOROFORM 5 ND1,2-DICHLOROETHANE 5 ND:fl-DICHLOROETHESE 5 NDTETRACHLOROETHENE 5 KIDTRICHLOROETHENE 5 NDVINYL CHLORIDE 10 NDhETHYL ETHYL KETONE 10 ND
OA/QC SURROGATE RECOVERIES
TOLUENE-d9(S8-110) 965: BROMOFLUOROBENZENE(86-115) 98« l,2-DICHLOROETHANE-d4(76-H4) 94*
NOT DETECTED ABOVE QUANTITATION LIMITESTIMATED VALUEl CONCENTRATION BELOW LIMIT OF QUANTITATIONANALYTE DETECTED IN BLANK AS WELL AS SAMPLESURROGATE RECOVERY OUTSIDE OF QC LIMITS
A R I O I 6 0 5
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Saute "C" . Broken Arrow, Oklahoma 74012 . 918-251-2&58
.***
CLIENTS URS CONSULTANTS, INC. . REPORTi 3676d570 DELAWARE AVENUEBUFFALO, NEW YORK 14202 DATEs 09-19-90ATTNi PETER FAIRBANKS
SAMPLE MATRIX s WATERSWLO » METHOD BLANKDATE EXTRACTED* 09-11-90DATE ANALYZED I 09-18-90SAMPLE IDs METHOD BLANK
DET. METHODPARAMETER ______________ LIMIT UMIT _____ RESULTS REFERENCE
TCLP SEHI-VOLATILES
0-CRESOL . 10 ug/L ND SW 8270M-CRESOL 10 ug/L ND SW 8270P-CRESOL 10 ug/L ND SW 8270TOTAL CRESOL'S** 10 ug/L ND SW 82701,4-DICHLORQBENZENE 10 ug/L ND SW 82702,4-DINITROTOLUENE 10 ug/L ND 8W 8270HEXACHLOROBENZENE 10 ug/L ND 8W 8270NITROBENZENE 10 ug/L ND SW 8270PENTACHLQROPHENOL 10 ug/L ND SW 82702,4,5-TRICHLOROPHENQL 10 ug/L ND " SW 827<>2,4,6-TRICHLORPHENOL 10 ug/L ND SW 8270HEXACHLOROBUTADIENE 10 ug/L ND SW 8270HEXACHLORDETHANE 10 ug/L ND SW 8270PYRIDINE 10 ug/L ND SW 8270
OA/QC SURROGATE RECOVERIES
NITROBEMZENE-d5(33-114) 48* 2-FLUQROBIPHENYL(43-116) 54* TERPHENYL-d:i4 (33-141) 58'PHENOL-d5 (10-94) 36fc 2-FLUOROPHENOL (21-100) 42« 2,4, 6-TRIBR(3MQPHENOL< 10-123) 52'
D = SURROGATES DILUTED OUT** = COMBINATIONS OF 0, M, AND P CRESOLSND = NOT DETECTED ABOVE QUANTITATIQN LIMITJ » ESTIMATED VALUEi CONCENTRATION BELOW LIMIT OF QUANTITATIONB s ANAtYTE DETECTED IN BLANK AS WELL AS SAMPLE« - SURROGATE RECOVERY OUTSIDE OF QC LIMITSSW = EPA METHODOLOGY HKSW846% THIRD EDITION
A R i O ! 6 0 6
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS, INC. REPORT: 3676b570 DELAWARE AVENUEBUFFALO, NEW YORK 14202 DATE: 09-19-90ATTNi PETER FAIRBANKS
SAMPLE MATRIX: WATERSWLO # METHOD BLANKDATE EXTRACTED: 09-11-90DATE ANALYZED s 09-13-90METHOD REFERENCES SW846-80BO. EPA METHDDOL08YSAMPLE IDi METHOD BLANK
RESULTS REPORTED IN ug/L OR Part* P.r Billion (PPB)
PESTICIDES/PCB'S DETECTION LIMIT RESULTS
BAMMA-BHC 0.04O NI?HEPTACHLOR 0.OOOS NDENDRIN 0.001 NDHEPTACHLOR EPOXIDE O.OOOS NDTECH CHLORDANE 0.003 NDMETHOXYCHLOR . 1.0 NDTOXAPHENE O.050 ND
QA/QC SURROGATE RECOVERIES
DIBUTYLCHLORENDATE < 24-154) 79'/.
I * SURROGATE NOT QUANTITATIBLE DUE TO MATRIX INTERFERENCEND » NOT DETECTED ABOVE QUANTITATION LIMITJ - ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATIONB - ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE* » SURROGATE RECOVERY OUTSIDE OF QC LIMITS
#00053
M/0/607
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W, Albany . Suite "C" . Broken Arrow, Oklahoma 74012 . 918-251-2858
CLIENT: URS CONSULTANTS. INC. REPORT: 3676*570 DELAWARE AVENUEBUFFALO, NEW YORK 14202 DATE: 09-19-90ATTNi PETER FAIRBANKS
SAMPLE MATRIX: WATERSWLO # METHOD BLANKDATE EXTRACTED: 09-11-9ODATE ANALYZED: 09-13-90METHOD REFERENCE: SWB46-S150, EPA METHODOLOGYSAMPLE ID: METHOD BLANK
RESULTS REPORTED IN mg/L OR Parts Per Million
TCLP DET.HERBICIDES____________LIMIT____________RESULTS
2,4-D 1.0 ND2f4,5-TP (SILVEX) 0.1 ND
QA/QC SURROGATE RECOVERY
2,4,5-T 697.
ND - NOT DETECTED ABOVE QUANTITATION LIMITJ » ESTIMATED VALUE: CONCENTRATION BELOW LIMIT OF QUANTITATIONB = ANALYTE DETECTED IN BLANK AS WELL AS SAMPLE» = SURROSATE RECOVERY OUTSIDE OF QC LIMITSI = NOT QUANTITATIVE DUE TO MATRIX INTERFERENCE
6-000332
f l R I O I 6 0 8
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany . Suite "C . Broken Arrow, Oklahoma 74012 . 918-251-2858
ANALYTICAL REPORT
URS CONSULTANTS, INC. REPORT: 3S7S-1570 Delaware Avenu©Buffalo, New York 14202
REPORT DATE: 09/18/90
SWLQ IDENTIFICATION
SAMPLE NO.: 3676.01DATE RECEIVED: 09/08/90
QA/QC
DESCRIPTION PARAMETER RESULTS
METHOD BLANK 09/13/90 " ARSENIC <0.0"5 mg/LMETHOD BLANK O9/19/90 BARIUM <0.02 mg/LMETHOD BLANK 09/19/90 CADMIUM <0.005 mg/LMETHOD BLANK 09/19/90 CHROMIUM <O.OOS mg/LMETHOD BLANK 09/19/9O LEAD <O.05 mg/LMETHOD BLANK 09/19/90 MERCURY <0.0002 mg/LMETHOD BLANK 09/19/90 SELENIUM <0.05 mg/LMETHOD BLANK 09/19/90 SILVER <0.01 mg/L
#1)00333
A R I O J 6 0 9
SOIL VOLATILE LABORATORYCONTROL SPIKE RECOVERY
In*. ID:
client Code: _JLLE=L__ Episode #:Matrix Spikc-LCS No.: J?2dl li___. Level (low/med):
COMPOUND
1,1-DichloroetheneTrichlorocthcncBenzeneTolueneChlorobenzene
SPIKEADDED(ug/Kg)
H?
V
•
//
MSCONCENTRATION
(«g/Kg)
'M«51«5D5B61
MS%
REC*3fe
{02t 001(30IOA
QCLIMITSREC.
59-17262-13766-14259-13960-133
#CoIumn to be used to flag recovery and RPD values with an asterisk
•Values outside of QC limits
Spike Recovery! 0 mit of 6_____outside limits
Comments:
A R I O I 6 I O 0nj0053'i
SOIL VOLATILE LABORATORYCONTROL SPIKE RECOVERY
lost. ID:
Tah Matnf ___________ Ol r rinA* Fpiwlr *•
Matrix Spike- LCS No.:_2Illii£L!____ Lcrel Oow/meeD:
COMPOUND
1 , 1-DichlorocthcneTrichloroetheneBenzeneTolueneChlorobenzene
SPIKEADDED(ug/Kg)
W
i,
r
//
MSCONCENTRATION
(ug/Kg)
4fciw<5DLta
£ b
MS%
REC*
3k3$loow(00
QCLIMITSREC.
59-17262-13766-14259-13960-133
#Column to be used to flag recovery and RPD values with an asterisk
•Values outside of QC limits
Spike Recovery:____ out of _2______outside limits
Comments:
f l R I O I G
SOIL VOLATILE LABORATORYCONTROL SPIKE RECOVERY
last, ID:-
/ i C ^ . c? TztteLab Name:_________________ m^r rviH ( A. rv > Ffrfgnrfg »• JJ •=» / —
f"— / w c c : - -Spike-rrs M<V- - ~ " — Level Oow/mccD:
COMPOUND
IJ-DichloroctfacncTrichloroetheneBenzeneTolueneChlorobcnzene
SPIKEADDED(ug/Kg)
^ f^—.
\V
MSCONCENTRATION
(us/Kg)
A3-//*<?w5H-
MS%
REC#
l<5^^c<:\%'S}OS
QCUMTTSREC
59-17262-13766-14259-13960-133
#Column to be used to flag recovery and RPD values with an asterisk
•Values outside of QC limits
Spike Recovery:____ out of >___outside limits
Comments:
$-000530AR1Q1G12._______
50IL VOLATILE riATRIx -=pn -E/nATRI X SPIKE DUPLICATE RECOVERY
l_aD Name: SUJL - TULSA ____________ Contract: URS ____ '
Coae: SldQK Case No.: URS 3 AS No.: ______ . SDG No.:
Matrix Spike - .EPA Sample No.: TBC-i _______ Level : < low/med ) MED
COMPOUND '
1 . 1-DichloroetheneTrichloroetheneBgnreneTolueneChlorooenrene
—
l- -SPIKEADDED(ug/Kg)
79107910791079107910 .
SAMPLECONCENTRATION
(ug/Kg)
000
SI 60706
MSCONCENTRATION
(ug/Kg )—- ———— g! —— — »S — S = — —
41706930741030600saoo
MS : QC! LIMITS
REC #i REC.
62 ! 59- 172S3 162-13:794 ; 66-142234 *!D9-139102 160-133
ii
COMPOUND
1 , 1-Dichloroethene ____TrichloroetheneBenzeneTolueneChlorodenzene
SPIKEADDED(ug/Kg )
791079 1O791079107910
MSDCONCENTRATION
(ug/Kg)
5250699O766O304009020
MSD'/.
REC #
66S39728 1 *105
i"/. !
RPD #!SSSSESX J :
-6 !o :-3 :i :
—3 !1
QC LIMITSRPD ! REC A
_«.__ —— rrrew t -™— »™ —— - H
22 159-17224 ;62-13721 i 66-14221 =59-13921 160-133
;
Column to be used to tlag r^cov^ry and RPD values with an asterisk
Values outside o-f QC limits
out of _ 5. outside 1 imitsSpike R^coveryi _ ^. out o-f 10 outside limits
COMMENTS: TBC-1 ' URSINST : C „ 4B/ 1 OML/50UL
FORM III VOA-2 1/S7 Rev
^000537
=iD name: .5WL-r:JL5A
ac Ciae: swQfeSftr i/ase No.s
; COMPOUND_ . . . .. 1 , i-Dicr-loroetnene _.'- Tr-icr.rc-roethene; Benzene- " ~~-"rToluene : " -
\ ChiorQ&enzene'
; COMPOUND
1 - i , l-Dicriioraetnene_ ___S Trichloroetnene: Ben 2 en e: Toluene: Chlorocenzene"
\ SPIKE
; <ug/Ka }• —— _ —i •?!=;•>,-.i / J •-".-: 530; -7530! -753O V:1 7*3c-
! SPIKE; ADDED! j; ug/Kg ;
! 7530
I 7530; 7530! 7530. .;
; slftMP LEi CCNCE?-n*RATION
. ™ — . - ....._
- ;! ;'v62osr
"i -' i3±i"t>Wi ""'"~" " " 3i 3S : ,-.';i '.> "
; CONCENTRATION: ( ug/Kg /
i 5.7203220
: 21100: 605000
"4OO1
! CC^iC
,;
j _ ;_I ~''?2
i ri
! MSDi .•'.! REC
; 76! 1 091 65; -soI 1S1i
rISENTRATTCr:ua/Ka ;
7290
2 1 4OOi . oSo.-
# i RPD ff
i ' 24 *; _7
* ; 6- * 1 __~Vj;-'j *
•?• !. *.'
,
' PI 3 ' '.:'_*i \ Llr:;T3"^
; '"•' / . D T — 1 _;; i t*i "• -, ~' — ; ~"~
: 69. '66- 14"'• - - - » » . =•» _ •< — -— .i . . Mi- -* > w;1?"" i. ._. Tr A r* -«"!t so-i". - - • -
i ii iQC i-lhXTS
! *PD ! REC. '
! 22 159-172!; 24 "62-137': ^1 ?66-l42;
>-. * - =• « _ -, ^ •— . •_A *J T — i ._ T •
21 ' 6C1-- .3;;
3 Column tio De used to -flag recovery and PPD /alues with ^n asterisk
« values outside o-f QC limits
5 outside . iSoike Recbvej : '_5 out o-f 10 outside limits
ICMMENTS: "TC-1 URSINST:C,4S/10ML/5UL F
FORM IlI"VQA-2 ~ - ' 1/S7 e>
A R I O I 6 I U
SOIL 5EMI VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECCvER f
NAm*i SUJL - TyLSA ____________ Contract: URS _______
Code: SldQK Case No,.: URS2 3AS No. i _____ SDG No.:
- EPA Sample No.: TBC-1 _______ Level :< low/med ) i-QUJ
COMPOUND
Phenol _.. ._ _Z-Chloroongnol1 , 4-Dichlorob^nzgn^N-Nitroso-di-n-prop. ( 1 )1,2, 4-TrichloroDens@ng_•i-Chloro-3— methyl phanolAcsnaohth^ng4-NitroDhgnoi2.4-Dinitrotolu^n^P*nt£iChloroDhenoiPvr«n»
'SPIKE •ADDED(ug/Kg )
1690016900S430843084 30
1 69008430169008430169008430
SAMPLECONCENTRATION
< ug/Kg )
2980000O0-000
. 00
MSCONCENTRATION
(ug'/Kg )
1080014800683049706030_9330632062004760
1 32005180
MS JC•; .LIMITS;
REC *; EC.
46 26- *?038 '5-10231 23 1 :-459 ,41 12671 7-3 10756 ; Z6 103— tr "**_!• ""7. j . . i _ /
." 11-114^6 ' -V3- 39-3 I--K.^Jl 73-142 "
; '
.
COMPOUND
Phenol2-ChlaroDh©nol1 ,4-Dichlorobsnzen*N-Nitroso-di-n-prop. < 1 )1 ,2.4-Trichlorobenzene4-Ch loro-3-methyl phenolAcgn^pnthen©4-NitroDhenolC, 4-Din itro toluenePen t AC n 1 orooheno 1Pyren©
SPIKE 1 MSDADDED ! CONCENTRATION< ug/Kg) ! (ug/Kg)
16900 ! 923016900 i 139008430 ! 63603430 ! 43308430 J 565016900 I 943O3430 J 6030169OO ! 122008430 ! 4380169OO ! 127008430 ! 5020
i
MSDy.
REC S
378275s-"?U-i6756-? t/ .£.7*7
527560
7.RPD #
/-j*-j— »/s
1 3—04
-64 *74T*
:QC LIMITSRPD fiEC.
75 16- ^50 '25-10-27 23 10473 41 11623 .73 10777 : 26 1071^ 71-17750 11-11447 IS- -8947 17- 10°76 35 - 1 4^j
'
\ 1 )• N-Nitromo-di-n—
4 Column to be us»d to -flag recovery and RPD values with an»" VA!U*S outside o-f DC limits
out o-f 1 1 outside limitsP»cov«ry: _ 0 out o-f 22 outside limits
COMMENTS : TBC- 1 URSINSTsF SWL#5037.01
FORM III SV-2 - 1/B" R-
ft-000539
3DSOIL SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SWL - TULSA_____;_______ Contract:
Lab Code: SWOtC?' Case No7: .URS SAS No.: ______ SDQ No.:
Matrix Spike - EPA Sample No.: TTC-1_____• Level:<low/med> MED
COMPOUND
Phenol2-Chlorophenol1 .4-DichlorobBnzch»N-Nitroso-di— n-prbp. < 1 )
4-^Nitrophenol2,4-Dinitrotoluene ____Pen tac h 1 orooheno 1Pvrene
SPIKEADDED< ug/Kg)
4820OO48200024100024100024100082000
48200024100048200O241000
SAMPLECONCENTRATION
< ug/Kg)
403OO000o w
• = o ,o0
3080
MSCONCENTRATION
(ug/Kg)
289OOO22700013100O12BOOO140000
_„ 253000.~ 148000 f-
29200O13600051SOOO3140O
MS
REC #
524754s'Z
535261615610333 *
QCLIMITS!REC. ;
26- 90!25-102!29 104!41 126!33 107!26 103!31-137!11-114!29- 39 t17-109!35-142!
i
itiCOMPOUND - - !
ssassssssaeaesssssaisssaaEaKssassa {Phenol !2-Chloroohenol !1 54-Dichlorob*n2»n» ___ !N-Nitroso-di-n-prop. ( i ) i1 .2,4~Trichlarob»nz»n«_i4-Chloro-3-m«thylph«nol !Acenaohthen* - 14-NitroDhenol i2.4-Dinitrotolu«n» ____ !Pentachloroohenol ' •Pvrene !
•
SPIKEADDED< ug/Kg)
3sa:*»3sss5s
4820004S20OO2410002410OO2410004820002410004820002410OO482000241000
MSDCONCENTRATION
< ug/Kg)==ssss:acesae33asaB
24600018900010400O1070001160002390OO132OOO90SOO13200047000082400
MSD%REC #S=KSVS3
4339434448SO5519359833 *
RPD #
1919231919410105 *2100
QC LIMITSRPD
33SO2738
195047476
REC.
26- 9O!25-102!28 104!41 126138 107!26 103!T * _ i -r 1 >*>i — lo/ i11-1.14!28- 89!17-109!35-142!
(1) N-Nitro»dTdi-n-propylamin«
# Column to bit used to -flag recovery and RPD values with an asterisk* Values outside of QC limits
RPD: _i_ out o-f 11 outside limitsSpike Recovery: _£ out of 22 outside limits
COMMENTS: TIC-1 URS 1G SOILS ,
FORM III SV-2 1/87 Rev,
1 0 1 6 1 6
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: SML-TULSA______________ Contract: URS_______
Lab Code: 3VJQK Case No.: URS2 SAS No.: ______ SDG No.:
Matrix Spike - EPA Sample Nc.: TBC-1______ Level:(low/med) LOW
COMPOUND
gamma-BHC < Lindane ) ___HeotachlorAldrinDieldrinEndrin _ _ _ _ _4.4' -DDT
SPIKEADDED< ug/Kg)
67.467.467.4163168169
SAMPLECONCENTRATION
(ug/Kg)
00O000
MSCONCENTRATION
(ug/Kg)
59.30
53.1237206131
.
MSV.
REC ft
390 *79141 *123103
QCLIMITSREC.
46-12735-13034-13231-13442-13923-134
~"
COMPOUND
gamma-BHC ( Lindane ) ___HeotachlorAldrinDieldrinEnarin4.4' -DDT
SPIKEADDED< ug/Kg)
67.467.467.4169169163
MSDCONCENTRATION
< ug/Kg )
47.9043.2161160193
MSD
REC #
710 *649695115
/•RPD #
0213326-6
QC LJRPD
503143394550
tMRE^j
46-12735-13034-13231-134
." r23-134
# Column to be used to flag recovery and RPD value* with an asterisk
* Values outside of QC limits
RPD: _ 2 out of _ & outside limitsSpike Recovery: _ out of 12 outside limits
COMMENTS:
FORM III PEST-2 — 8/87 F
6-000541
A R I O I 6 1 7 - - . — — -
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE IMPLICATE RECOVERY
Lab Name: SHfr-TULSA____________ Contract: UHS_____
Lab Code; SWLQ Case No.; opg SAS No.; _____ SDG No.;
Matrix Spike,- EPA Sample No.: TTC-1______ Level: (low/med) M££~
COMPOUND
gamma-BHC (Lindane) ___Heptaehlor .,... ,AldrinBiftldrinEndrin • . .._ -4.4--DDT
SPIKEADDED(ug/Kg)
241024102410602060206020
SAMPLECONCENTRATION
(ug/Kg)
0000
5810
MSCONCENTRATION
(ug/Kg)
208021102110559063006940
MS%REC
86888893
' 95115
! QC! LIMITS
*! REC..— i ___.—«,_146-12'!35-13(134-13^! 31-13<I42-13S123-13*i
COMPODND
gamma- BHC (Lindane ) ___fiftDtachlorAldrinDieldrinEndrin4. 4 '-DDT
SPIKEADDED(ug/Kg)
241024102410602060206020
MSDCONCENTRATION
(ug/Kg)
365016903440774086507540
MSD%REC *
152 *70143 *129134125
%RPD #
-55 *23-48 *-32-34— A
QC LIMITSRPD ! REC.
50 ! 46- 12731 135-13C43 134-13238 131-13*45 142-13$50 123-13*i
t* Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: _2. out of 6 outside limitsSpike Recovery: _2. out of 12 outside limits
COMMENTS:
FORM III PEST-2 8/87 Rev.
6 00054
01618
ItS SOUTHWEST LABORATORY OF QKLAHOM
MATRIX SPIKE EVALUATION FQRH
URS
SASPLE ID T8C-1HS
. NET MT. 10,0
iiount itount iiountno in sol. added detected Z TARSET
added ppt ppt ppt recovery recovery huts2378 TCDF 2.5 'o 250 299.5 120 60 - 140 ZHPCDF 10 • 0 1000 900.0 90 60 - 140 ZQCDF 25 0 , 2500 2863.0 115 60 - ;40 X
2378 TCDS 2.5 0 250 219.4 98 60 - 140 IPCDD 10 0 1000 1109.4 Hi 60 - 140 IH)(CDD 10 0 1000 368.9 37 60 - 140 I
DUPLICATE SAHPLE EVALUATION
SAHPLE ID TBC-IHS TBC-1HSD
MET »T. 10.0 10.0
uouftt aaount RPGin sol. in spl.ppt pot
2378 TCDF 299.5 293.5 2.0HPCDF 900.0 748.0 18.4OCDF 2863,0 2950.0 3.0
2378 TCDD 219.4 195.1 11,7PCDD 1109.4 954.1 15.1HICDD 868.9 865.8 . .4
I O I 6 I 9
1SD SOUTHKEST LABORATORY OF 3KLAHDRA
HATRIX SPIKE EVALUATION FORA
SAMPLE ID TBC-1HSD
MET NT. 10.0
aiount aiotint uountno in sol. added detected Z TARSET
added ppt ppt pot recovery recovery lmt?237S TCDF 2.5 0 250 293.5 117 60 - 140 ZKPCDF 10 0 1000 748.0 75 60 - 140 ZEOF 25 0 2500 2950.0 118 60 - 140 Z
2378 TCDD 2.5 0 250 * 195.1 78 60-1402PCDD 10 0 1000 954.1 95 60 - 140 ZHXCDB 10 0 1000 865.8 87 60 - 140 X
DUPLICATE SAHPLE EVALUATION
SA«PIE ID TBC-1HS TBC-1HSD
KET HT. 10,0 10.0
uount atount RPDin sol. in spl.SDt ppt
2371 TCDF 299.5 293.5 2.0HPCDF 900.0 743.0 18.4QCDF 2863.0 2950.0 3,0
2371 TCDD 219.4 195.1 11.7PCDD 1109'.4 954.1 15.1HICDD 868.9 365.8 .4
f l R I O I 6 2 0
"ftTRH SPIKE EVALJATION ?•£*
SAHPLE !3 r"-l*S
S£T ST.*
IQad sec
2"S "DF 2.5H&CDF 10DCDF 25-.--Q *«*r_ - s. . ; 0 . wJt- , .-v
:C3D ID-XC3B :)
SAMPLE ID
KET «7. '
•;7Tq Trnciij.' C . w-yr
HPCDFI-C3F
"fa rrrvn.» j g ; wuvirnri• tf>'W
HXCD0
aaount:a sol.crt5U^
v -.A
TTC-1HS
10.0
aiountin sol.cot
''SI 'A3i.it220.02937.0
it! iiwi .0
1074.5352.4
:C.O
diOUHt alCURt
533EC :etecteg '; , "ARSETDot sot .rscoverv rscoverv :is;:=2^0 231.: - 112 aO - MO Iim -320.0 ' 32 iO - 140 I2500 2997.0 119 aO - MO Z
250 - MJ.i *i 60 - 140 Z1 00 1074,5 ^ -107 60 - !40 X
.. :000 5:2.4 85 oO - i40 I
DUPLICATE SAMPLE EVALUATION
TTC-iHSD
10. C
aiount RPDin sol.;ot291.3 3.6903. 0 9.63233.0 8.1
207.4 31.11077.3 .3725.2 16.0
flRIO!62l «2r 000545
TRH SPIKE SVAUJATIW «3RK
x!
2"8 TC3FMPCDFJC3F
::?s -CUD5C9D"tCDD
SAMPLE ID
HET Iff.
2378 "CD?H^CDF-
&h /a ! wrfU
"33HSCDD
-r.
taount"0 ;T SDI.
,GGec :ct" e, 0«4kl kC
10 S25 •)
2.5 v:o o:» :
TTC-1MS
10.0
tflountin sol.OBt2S1.I820.0C07 A
151.61074.5852.4
4 V r v
i.icunt ssoun:idaifl :§t§ctsa A *^R8£Toat art 'icoverv "sccvtrv ;?;:i250 :?.:.'• 117 B0 - 140 S:ooo • ==> .c *?o "• BO -T40 :sroo :; s.o :30 so - ;40 "250 . 207. 33 sO - 1*0 ".ICOO 1C77.8 108 iO - ;iO Z)300 -5.: -3 iO--S40S;
DUPLICATE SAtfLS EVALUATIDN
TTMHSD:o.o
aacunt RPDin ssl.sot291.3 3.i303.0 5.63233.0 9.1
207.4 3M1077.8 ,372s. 2 lfe.0
6T000546SR10J622
U.S. EPA - CLP
5A , EPA SAMPLE NO.SPIKE SAMPLE RECOVERY _____________
Lab Name: SOUTHWEST LAB OF OK" Contract: 63-09-0089MDTBCI:
•_aD Code: SWOK Case No.: 50371 SAS No.: SDG No.: MDTBCI
Matrix: SOIL - _ ...Level ( low/med >': LOW
% Solids for~"Samp"le: SO.4
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analvte
AluminumAn timonyArsenicBarium3ervl liumCadmiumCalciumChromiumCobaltCoooerI ranLeadMagnesiumManganeseMercuryNickel'PotassiumSeleniumSilverSodium "Thai 1 iumVanadiumZinc 'Cyanide
ControlLimit7.R
75-12575-12575-125"7= — 1 /~>c:/ —j i *.»j75-125
75-12575-12575-125
75-125
75-125-7C1 __ •( O="/ U~liU~7 — i '?'=;/ *J 1 .i-wJ
75-12575-125
-75-12575-12575-12575-125
Spiked SampleResult (3SR)
10.43163.2773
577.783514.511612.4942
34 . 4445143.013579 . 6400
12.5112
579.1353.5258
152.4353
1 .951513.6120
14.9552169.3467161.057321.3735
C
B
SampleResult (SR)
•.!'' • / •.!• 1 •->
* -2.010977.47331 .1617.4975
27.33658.6703
1 4 . 4230
7.9739
338.9954.lies
13.7647
.4975
.7463
.497537.665829.24222.3919
C
UsBU
B
U
Uuu
u
SpikeAdded < 3A >
124.339.95
497.5112.4412.44
49.75124.3362.19
4.98
" 124.38.57
124.33
2.4912.44
12.44124.33124.32T-t T~?.-i. . •«• /
1 1i 1i 1
:.R :.Q ; M< ii *! INR
3.4INIP33.01 NIF100. a! !P107.31 IPiOO.4! IP
; INR113.8; JPlos.o: IP104.9! iP
I INR91 .1 ; :F
! INR152.9!N!P9 .2! ICV
111.51 IP: !NR
9.4! IF109.41 IP
; INR120.2; IF106.3: IP106.UI IP95.61 1C
Comments:
FORM V (Part 1) - IN
01623 6-OOOQ47
U.S. EPA - CLP
SB EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY __________
MDTBCIALab Name: SOUTHWEST LAB OF 0(C Contract: 6S-D9-0089
Lab Code: SWOK Came No.: 50371 SAS No.: SDG No.: MDTBCI
Matrix: SOIL Level (low/med): LOW
Concentration Units: uq/L
ittiS Analyt©i•1 Aluminum! Antimonv! ArsanicI BariumI B»rvl liumJ Cadmium.CalciumI ChromiumI CobaltI CopperI IronIL@ad\ Magnesium! ManganeseI MercurvI Nickel'! PotassiumI SeleniumISilvgr! SodiumI Thai lium! VanadiumI Zinc 'I Cyanide1
ControlLimit;<R
Spiked SampleResult <SSR)
991.97
~~
4636.58
"
CSample
Result CSR)'
15.00
1 kjo- i • 76
C
u
SpikeAdded (3A)
1 20 . 0---
.3100.0
_
••'.R
326.6
99. 1
~"
ii
Q!Mii,'NRIP:NRINRINRINR!NR!NR:Mmiiw:NR:NR;pINRINRINRfNRINRINRINRINRINRINR
_! __
Comments:
FORM V (Part 2) - IN
#-000545
U.S. EPA - CLPEPA SAMPLE NO,
6 . . ___________._DUPLICATES ! . .
i MDTBC1Di_ab. Names SOUTHWEST LAB OF OK Contract: 63-D9-0039 ! ___________
Lab Code: SWOK Case No.: 50371 SAS No.: SDG No.: MDTBCI
Matrix (water/soil): SOIL .. Level (low/med): LOW
!•: Solids -for'"Samples " SO.4 . % Solids for Duplicate: ~?7.3
Concentration Units (ug/L or mg/kg dry weight): MG/KG
11
i Analyte
: Aluminum! AntimonyArsen ic
i Barium! Beryl II um"! Cadmiumi Calcium! Chromium{Cobalt1 Copper1 I ran! Lead; Magnesium1 ManganeseI Mercurv ~; Nickel; PotassiumI SeleniumI Silver; Sad ium1 Thai 1 ium' Vanadiumi Zinc .": Cvanide „•i
ControlLimit
.- 49. S
-
6.2
1 0 . 0
-
12.45.0
_
_Sample (S) C
22303 . 3330 !3 . 73 1 3 ! U2.Q10.9.J.B
77 , 4733 I .1 * 1&17 1 B.4975IU
739 . 4037 ! B27.3365!8. 6703 I B14.42301
26597.318017.97391
952. 1577 IB333. 9954 J
.U85IU13.76471
303. 5476 IB.4975IU.7463 I U
600. 0479 IB. 4975 I U
37 .6653 I" Q •"!> /I *"? *"? '
... 2.._3919.UJii
Duplicate (D)
13903.3100o . / •_;• j. 31.2514
..61 .6182. 9704.4975
569.435326.31503 . 370713. 6934
19337.43207 . 0522
923.3140391 .3016
.lias10.4364
651.2190.4975.7463
519.6455.4975
30.772024 . 4657
•-i -r Q O T.._.. - * '-•.«•*•'
C
u8
BUB
B
B
U
BUUBU
u
;y.RPD !
46 . 4 {I
46.6 i'"*•'•> Q (jl-ji. m O 1
17.9!I
32.415.61•-' . sJ 1
cr ^ ii_J > - i31-. 4 IL /% '
. •"? =; i« . vJ 1
,711
27 .5 !20.91
I! .
14.41t
20 . 1 1" J. / . ci i
|
I
Q
*
*
M
PPFPPPPPPPPFPPCVP 'PFpPFPPC
FORM VI - IN7/83
flR!Oi625 6-000543
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
AD Name: SDUTHW£ST LAB OF OK Contract: 6S-D9-O039
ab Code: SWQK Case No.: 50371 SAS No.: SDG No.: MDTBCI
olid LCS Source: EPA0287
us LCS Source: EPA-LV
ii! Anftlvt*iI riiuminum; Antimonv{ Arm^nir; BariumIServlliumi CadmiumI Calcium! ChromiumICobalt{Cooper1 Iran!L«aI Magnemium! Manaanesel rcurvJfJickBii PotaamiumJ Seleniumi SilverI SodiumJ Thai lium ;I Vanadiumi ZincJ CvanidB)i i
i AquecTrue
>
r
"L.
i
!
Dus Cug/LFound
=
---- —
-
)KR True
325 . 0211.0917.04.8
. 19.445.4
196200.099.6
144.06910.022430 . 0236 . 0
113100.0208 . 0
12.760 „ 950 . 039.222 . 250 . 039.065.31S7._05.6
SalicFound
234.2161.5706 . 43. 6
21.943.5
179570.3112.6155.16381.3
13661 .7217.7
1 1 1 730 . 0T"»O OjL.ji.V . O
12.369. 167.524,823.377.545.063.3
190.45.3
JC
B
B
B
\ mg/kg)J. Limits
225.0! 424.0: 127.0! "94.0635 . 0 I 1 1 99 . 00 . 0 i 40 . 0
14, <=: » o*? Tl a . o i — i • o— —35.71 55.1166800.01225600.0
79.21 120.0124.01 162.06006 . 0 I 7320 . 017770.0! 27080.0
138.01 235.01 00400 . 0 I 1 29900 . 0
: 177.0! 239.03er i i ~* A. wJ 1 J. / . '.J
: 49.2; 72.60 .01 1 000 . O
19.1! 59.4.15.51 29.00 . 0 I 1 000 ; 0
r-i /\ f i c"~ cr^l^.Oi i '_•»•_!
51.71 79.9133.0! 236.0
4.3! 6.9ii
•/.R
37.76.77.i75.'
112.'95. <91 :Aiov99T33.:92.:94. c
no.;96.'
113..135.'63. "
107.-155.-115.-104.*101 .£1 03 . <:
FORM VII - IN7/SS
1RIOJ626
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ___
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089MDTTC1S
Lab Code: SWOK Case No.: 50131 SAS No.: SDG No.: MDTTC1
Matrix: SOIL Level (low/med): LOW
% Solids for Sample: 71.6
Concentration Units (ug/L or mg/kg dry weight): MG/KG
! i Control! ! Limit! Analyte ! %Ri i1 __..._LJ. ,-IIL-T —— --.--- ——— 1 __________________
! Aluminum [{Antimony ! 75-125! Arsenic [75-125! Barium 175-125JBeryllium} 75-125! Cadmium ! 75-125! Calcium !! Chromium ! 75-125! Cobalt 175-1251 Copper . !klron • ,'jLead [75-125! Magnesium !! Manganese!! Mercury ! 75-125! Nickel !{Potassium!! Selenium 175-125[Silver ! 75-125! Sodium I! Thallium 175-125i Vanadium 175-125{Zinc 175-125! Cyanide ! 75-125i i• >
Spiked SampleResult (SSR) C
|12.83911B5.7765!
708.4941!16.9762!-17.1288!
!108.8243!171.6450!116.5039!i325.3140!
]1042.4277!
1.0265!425.5360!i
1.6844J14.7436!i16.4302!205.4687!343.4626!24.0788!t... — - i _
SampleResult (SR) C
i4.1899IU2.8827!
227.5388!1.2288IB1.7559!i60.3654!14.7497!365.8036!i141.1011Ji745.8838,'
.2095}2124.6472Ji
.5587JU
.838QIUi
.5587JU51.7159!151.4737J2.63521Ui---—..——..- ———— _ i —
iSpike
Added (SA) !i- —— „ _,,riL.,— ti139. 66 i.11.17!558.66,'13.97!13.97!
!55.87!139.66!69.83!i139.66!i139.66!
.70!139.66!i
2.79!13.97!i13.97!139.66!139.66!26.15!. i
-._.. ... • .. i • - — .——— 1
t 1t 11 1
%R 1 Q JMi r——— _ — _. i _ i —! !NR
9.2!N!P25.9INJF8.6 . 1 ! |P112.7! IP110.0! jP
! INR86.7! |P
112.3J |P-357.0J |P
I INR131.9!N|P
1 INR212.3! IP116.7! {CV
-1216.6! IP! INR
60. 4! N|F105.5} IP! ;NR117.6! IF110.1! |P137.5INIP92.11 |Ct i_ _. i _ i - —
Comments:
FORM V (Part 1) - IN
A R I O I 6 2 7
U.S. EPA - CLP
EPA SAMPLE NO.
Lab Name: SOUTHW2ST LAB OF OK Contract: 68-D9-0089MDTTC1A
Lab Code: SWOK Case No.: 50131 SAS No.: SDG No.: MDTTC1
Matrix: SOIL Level (low/med): LOW
Concentration Units: ug/L1111! Analyte
! Aluminum! Antimonyi Arsenic1 Barium{BerylliumI Cadmium! Calciumj Chromium! Cobalt1 CopperIronjLeadI Magnesium! Manganese' Mercury! Nickel{Potassium{Selenium{Silver! Sodium! Thallium! Vanadium{ZincI Cyanide
ControlLimitXR
______ ___
Spiked SampleResult (SSR)
1069.36
1439.72
1577.04.--•- . ___ ———— ———— 1_;_L_——— • ——————
C
—
SampleResult (SR)
15.00
505.14
542.28
C
U
SpikeAdded (SA)
120.0 '
'
1000.0
"
1100.0
XB
891.1
93.5
1
94.1
i ii ti iQ!M !
1 l
INR!IP 1INR!INR!INR!INR!INR!INR!|NR!1 W Jl;Ht p ^w
INR!INR!!NR!INR!INR!INR!INR!INR!INR!INR!jP !1 I! !
Comments:
FORM V (Part 2) - IN
f l R i O I 6 2 8
U.S. EPA - CLPEPA SAMPLE NO
6 __________DUPLICATES
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089MDTTC1D
Lab Code: 3WOK Case No.: 50131 SAS No.: SDG No.: MDTTC1
Matrix (water/soil): SOIL Level (low/med): LOW
% Solids for Sample: 71.6 % Solids for Duplicate: 71.6
Concentration Units (ug/L or mg/kg dry weight): MG/KG11! Analyteii Aluminum{ Antimony[Arsenic! Barium{Beryllium\ CadmiumI Calcium} Chromium! Cobalt; Copper| Ironi LeadI Magn.es ium! Manganese! Mercury! Nickel! Potassium! Selenium| Silver! Sodium[Thallium; Vanadium|Zinc} Cyanide(
ControlLimit
2.855.91.41.4
1396.6
14.0
.1
.
14.0
~-Sample (S) C
21129.3282!4.1899JU2.8827}
227.538811.2288IB1.7559!
1958.2286!B0.3654!14.7497!365.8036!
38626.6257!141.1011!801.1008IB745.8838{
.2095!2124.6472!425.6128JB
.5587{U
.8380JU611.8179JB
.5587|U51.7159!151.4737!
2..6352JUi- — - - — t ___
Duplicate (D) C
26439.0299!4.1899IU2.8827!
137.7546!1.7028!2.0792!
426.5426JB40.9722!14,7700!70.8662!
46676.2151!100.5415!888.6482IB784.3788!
.4260,'367.2465!508.9126IB
.558710
.8380|U1095.2859JB
.5587IU65.0117!148.4193!2.6057!Ui>
i%RPD 1i
22.3! i0.0!49.2!32.3!16.9!
128.5138.31
.1!135.1!
18.9!33.6!10.4!5.0}68.1!141.0!17.8! it\56.6! t22.812.0! iiti
i
QIMi
*|PIPIF
*|PIP!P*;p*{PIP
*|PIP
*|PIPIP
*|CV*!PIPIFIP.1 Pi ±IFIPIP1C1i
FORM VI - IN7/88
&-QC0553A R I O I 6 2 9
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089
Lab Code: SWOK Case No.: 50131 SAS No.: SDG No.: MDTTC1
Solid LCS Source: EPA0287
Aqueous LCS Source: EPA-LV
111I! Analyteii — -•-! AluminumI Antimonyj ArsenicI Barium{Beryllium! Cadmium{Calcium' ChromiumCobalt{ Copper1 Iron,' Lead{Magnesium! Manganese! Mercury! Nickel; Potassium! Selenium{Silver! SodiumI Thai lium{ Vanadium{Zinc! Cyanidei•
AquecTrue
.... ........ ._ . .....
3US ( Ug/LFound
- ——— ... ————— ——-•_..!_-
)
XBSolid (
True Found C
325.0! 284. 2\211.0! 161.5!917.0! 706.4!4.8! 3.6IB
19.4! 21.9!45,4! 43.5!
196200.01179570.3!99.6! 112.6!144.0{ 155.1!
6910.01 6881.3!22430.0! 18661.7,'236.0! 214.2!
118100.0ll29159.il208.0) 229.8!12.7! 12.3!60.9J 69.1!50.0! 67. SIB39.2! 24.8!22.2! 23.8!50.0J 77.5JB39.0! 45.0!65.8! 68.8!187.0! 190.4!5.6! 5.9!i i—————— . i — - ———— i _
mg/kg)Limits %R
225.0! 424.0! 87.4127.0,' 294.0! 76.5635.0; 1199.0! 77.00.0! 40.0! 75.0
16.5! 22.31112.9.35. 7{ 55.11 95.8
166800.0[225600.0! 91.5;79.2) 120.0!113. |124.01 162. 01107. 06006.0! 7820.0! 99.5117770. 0! 27080.0! 83.2!188.0! 285.0! 90.8!
100400 . 0 J 129900 . 0 ! 109 . 4 J177.0! 239.0I110.5!
8.5J 17.0! 96.9!49.2! 72.61113.50.0! 1000.0[135.0
19.1! 59.4! 63.3.15.5! 29.01107.2!0.0! 1000.0!155.0!24.6! 53.5J115.4!51.71 79.91104.6!138.0! 236.01101.8!4.3! 6.9J105.4J
i i t_______ i ——————— i ———— i
FORM VII - IN7/88
flR!OI630 6-000554
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-0089
Lab Code: SWOK Case No.: 50131 SAS No.: SDG No.: MDTTC1
Solid LCS Source: EPA0287
Aqueous LCS Source: EPA-LV ._..__..
1I1t! Analyte
{ Aluminum{ Antimony! Arsenic! Barium! Beryl lium! Cadmium[ Calcium< Chromium| Cobaltt Copper! Iron[Lead{Magnesium[Manganese[ Mercury{NickelJ Potassium! Selenium[SilverJ Sodium[Thallium{ Vanadium[Zinc{ Cyanide
Aqueous ( ug/L )True Found XR
Solid (mg/kg). True Found C Limits XR
12.7 14.2
"
8.5 17.0
1
111.8
FORM VII - IN7/88
flRI0163
U.S. EPA - CLP
LABORATORY CONTROL SAMPLE ; ..
Lab Name: SOUTHWEST LAB OF OK Contract: 68-D9-OOB9
Lab f>.'fr: ^HHf Case No.: 5014.1 SAS No.: . ?DG No. : MBR114
Solid LCS Source: EPAQ2S7 :
LCS Source: EPA-LV
1111
I AluminumI An Lxmonv! Arsenic! Barium! P r* r v 1 1 1 1 "n
! r^ 3 c > um
! C^b-- 1 t! CODDPr! Iron! Lead1 Mnpn^'sium! flHnn-^nea^r-I Mercurv•Hi cl- *»1! Potassium! SeleniumI Sll vpr! Sod i u m! Th^ 1 1 iumj Van^d a umI ZincM%«md«
£nueou5 (ug/L )T""?1 Found ";R
"
.._
— -_.
. __.
-
Sal id ''mciYkg )True Found C - Limits %P>
325 . 0211.0917.04.3
.19.445.4
196200.099.6
1 44 . 06910.022430.0236.0
1 13100.0208 . 012.760 . 950 . 039.222.250 . 039 . 065.8187.05.6
234.2161 .5706.43.6
21 .943.5
179570.3112.6155.1
6881 .318661 .7217.7
1 1 1 780 . 0229.8
1 *? T.!.*.••_'
69.167.524.823.877.545 . 066.3
1 O . 45.8
rs
B
B
225 . 0127.0635.0
'!> . 016.5
• 35.7166SOO.O
• 79.21 24 . 06006.017770.0188.0
1O0400 .O1 77 . 08.549.20 . 019. 115-50 - 024.65.1 .7138.0
: : 4.3
424.0294 . 01199. 040 . 022.355. 1
225600 . 0120.0,162.0
782O . 027080 . 0235 . 0
129900 . 0239.017.072.6
1 000 . 05.9.429.0
1 000 . 053.579.9236 . 06."
87.'76.77. t75. (112. r95. E91 .:
10 199S3.:92.:94.*
1 1.0 . f96. c113.'135.63.107.155.'115.1 04 . .1 0 1 . £•103.*
FORM VII - IN7/88
flfi(OI632
SOUTHWEST LABORATORY OF OKLAHOMA, INC.1700 W. Albany • Suite "C" • Broken Arrow, Oklahoma 74012 • 918-251-2858 • FAX: 918-251-2599
./JR r_..-:3" J CATjT" . _ _. ..._.__. __ . _ ._. .. REPORT: ?0 L 4 67.70 DEi_ AWARE ...AVENUE I •"BUFFALO. NEW YORK 14202. ' . ... " _" . =/:;-_: " "'DATE: "" 07-1..1-91AfrN: PETER FAIRBANKS
9AMPLE MATRIX: SOILSWLO t 50.14.02 . •••PROJECTS 35214; DELAWARE SAND & GRAVELCLIENT ID: TBR-1 (24') (MS/MSD*
TPH MATRIX SPIKE/MATRIX SPIKEJDUPLIGATE RECOVERY DATfl
SPIKE CONC. SAMPLE CONC. MS CONC. MS PERCENT(mg/kg) (mg/kg)* (mg/kg)* RECOVERY
657 16 610 8 "'1
MSD CONC. MSD PERCENT RECOVERY PERCENT(mg/kg)* RECOVERY DIFFERENCE
~H 616 907. -17.
* = DILUTION FACTOR NOT APPLIED TO THESE CONCENTRATIONS
A R J O I 6 3 3
WATER VOLATILE LABORATORYCONTROL SPIKE RECOVERY
Inst. ID:
Lab Name: fti""' " UiPfMTrf/ffMm\«nt Code: (A- £-- Episode #: $ '*? 5 *
Matrix Spikc-LCS No.: ff / -
COMPOUND
1 , l-DichlorocthcncTrichiorocthcneBenzeneTuolcneChlorobcnzcne
SPIKEADDED(ug/1)
5 O~ri//V
MSCONCENTRATION
Cug/0
<-f>^M>^^^
MS%
REC#
q^qsqA9A^
QCLIMITSREC.
61-14571-12076-12776-12575-130
# Column to be used to flag recovery and RPD values with an asterisk
•Values outside of QC limits
Spike Recovery: f~**\____out of ^ S___outside limits
Comments:
U.S.. EPft -- CLP
r*& EPA BAHPi.t. MO-SF'I KG SAMPLE RECOVERY
i JlfttVfft^Sl.ab Mama: snUTHWE&'I LAS UP-' OK * Contracts 6BHD9-OO09 !„„„„„„._.._
Lab Docior &WOK U<*s>e? Ho.. ;;- 437 &JL SAB No. s SDG No. s HR!:-TKv:
MA Kr i x s WATER Lcsvel. (lowXfn-a-d > s LOW
''•» Sol Lei is "ror Sample:: O.O
c^n fcra t\3 un Units C'-tg/L or mg/kg dry weight) r LiCi/'L.
1
1
An a 3 y te»
AluminumAn •{• imonyi^rseiii c:BariumBe?ryl liumC&dmiumO*il ci i.tfl'iChr ttmiuriiCobaltHopperPi ronLoadl1&gne«F.j urnriang«Ane&9Mercury'NickelPol-ass ium<^r-"i i»r» i umSx 1 v&-rSodiumThai 1 i urnV*n«id:i.UT(!£ :t j*i t.Oy&jiicie.... ...... ...._. „,.-.. _..
I Control iLimi 1 ! Spited Sampler"i'R { ©"sul 'I*. C EiGi*? i
75-175 i " 5789, 122675-125 I 152.404775—1*25 ! 75- 525O.•'"S""!! ! K3&6 1> VJVxM"? "i -- 1 S? * ' 49 S"L "i775-125 ..I 65^2a?S
:75-125 J 7!39.87"5l7S-125 ! 572*869475-125 J 256.1931
I 2537 65. 560075-125 i SA.7500
iI 9154-3419
,/ ..1 •* i, X™ s.' i i»C3*TW\.'
"/?- j 2'5 ! 8 J.8 . 5306ii
75-125 ! .10.. 43.5O7 A- 125 ! 55.04O1
;
75-125 ! 48.3OOO7S-J.25 ! 491.0294;' is ~- i :•? 5 ; 323 .. 34 4 175-125 ! 146. 81 55-«.--..,_„..„.„._ ' __ __. _ ._.,_..„ _ , _ ,„. ..
c:
B
..
SampleResult CSJ-O" C.
•1707. 4604 J30.0000JU^O»t:125O-t
93V.. 879 ;1 "-\ 1 T:i ' TW
4. 3 1 3.0 !»J
B9.Bio:M'8S.1 - 7B4S !17.742VJB
279022.3100!53.2000!
!9366. 1973 ;
,4OOO!U33 O- 6917.: J
I1 « 429EnO * B
*1 X IOj*''i '. —— _ — .._ t_
1O*0000|U2.0OOOIU
333,9921 !16.7000JU
t...., .„ —....-— .._*_.-*.,*,...-.„-.-..- * ....
r i
Spike ! [A eld rod i S A i l ";R ;Q
J:OOC-..OO[ f.u4.:l ;NMO « 00 ; -~0 , l:t J N4O,00! J 11 -li!
^oOo .. 0 .3 ; y... :;•> ;">0 ., 00 ! ^7«O :
; ;• Oo,.0o; 10O-G j••OO.. 00 I r»'H-0 !50 ..00! -;ili.4!
1OOO .. 00 ! •-i'.'C.o ."'•' ;20.00J 167.3 IN
i >300.00; -42.4!
1..00! 84.0!SOO-OO ! V7. 6 !
; i.l.O ,. OH.) J 91 .. 'J. ;e.O,30; 84 -2 !
i i
50 H 00 ! v6.6 <riOO,,OO ; S' .X!;5OO „ 0^ ! 9 ,'>.*? ;10O..OO-; :f'4<:..BiH
1 1 <... . ....™-.. ._». ._....— .™ 1 — .— — — — ™ ' ~
1.
-.-.,. *r 1O i
1
r :p :P'.' »p iHft ;P :*'' !< ' it:- i> tJIT '
NR !P ;
cv;p :NR ;F 1P !NR :t:' ;P !K !."• '
i.___ !
FORM V <PA:-t 1) - -IW
A R 1 0 1 6 3
u .. s - fc:i -A - CLI"'
sf EPA SANPLfc' rKJPOST DIGEST SPIKE SAMPLE RECOVERY "
L*b Maine s SOUTHWEST L( B OF OK , Con*.r*ft.s 6R -09-0039 I ..,.____ _
I <*b Code: :5WPK UAK» No.;: S^M SA'J Mo. a ' BOG HO-S WRWi Ri'
Mwvtr i x i WATER ! ,c*vel (luw/rnrwci ; u uQto
Con cc-nt ration Uni Ira* ucj/L
I Control! ; Lind t; wi'iuilxte J 5sR< i*...,,«,». „. •-* . ' __ „_ __.--....»-__
1 Aluminum !; Antimony ;! Ar^eri^ c Ii £i,\rium I: jtorylJ ium I, i^ j is l--Mt.ini LUlui r» . *i • (t win it I* it U rt 1 t
! Chromium .*! Cobalt I"opper ;T IT*!**? *< J, J (7* 1 i
! L©AOI MAgn&snuin!illAnqamece*I Mercury •1 hid ckfe*! ;! Pataa.g.ium!!St»l*nium iI Bi Ivoi- 1I cj .J 'i 2 «U U (L U i< i )
, Thc.iJ.1 i um {! VAn^diutn ;1 7.1 nc II Cyanide. i• .
ISpiked SAmplf*- ; S Ann pieR«-BU 1 1 ( SSR 5 C: ; i ie*"u 1 i C SR )
.-•-i— u vH — i-irt . «.i«~-«_.» ,« ' ...«...<-». - - .—— ,«— .
13801*. 00 ; '"' ; """"' " 47077 50J5O.oo ;u; '.rto.oo
1 11 Ii i1 11 1t 1f 11 1l r,' ',1 11 .1 «> 11 i1 1i rf 1I 11 tr 11 11 rI t1f1 1t f( 1
1 1« 1! 1
I1 I1 tI 1t 11 11 11 11 11
1f1 Sprite
C i Haded ifSAjii
„ .. L „ . _„ „..„ . . isf™.™. „„ , _ „.
1 ' 9400 „ 5u; i 2-0-0• ;
;>•iii•iir
i'
14
rti
l
t1 \lt
1t;!t1
1 1 t1I I! C
-. 1-' I (4 \ M; r
«. ™. .. _>.- -«« ™ i „, ' „__.9c>.7'| IF'o „ o ; ; p
; ;NP: : NR; INR1 ' Mf-1i rir*i t t r"11 4 f*H l
: : NR: ;NP. ; Nr|: IMf-1; ! NP:; INK:. ; NR; i NR• : NR; ; NR; ; Mr--
— ; INR1 ' Wf-'1 1 ~1 *
! 1 NR•: INR! I NR; : NR' 1
(Pvtrt 2} - IN
A R I O I 6 3 6
EPA SAflP'LE NO,
'i .ICATFB """ """ •"•"••""" ™
Lab Names SOUTHWEST LAB OF OK Contracts 6.S-D9-OOB9 „...„...„__.„.
L*n Codes SWOK " Case No-s 4&7t*l . iSAS N-j. . s , SDG Hi-.,,.: HRS
Matrix <«rf twr/soi 1) s WriTER " "Level < low/med 1 c I. > JUt
"•; Sol set** •for' 'SAinples" O*O r» ?JoIid«» for 3>upl i Crvl'e:; O
Con can t r & t i an Un i is*, c y.g .••' L o r rnq / l<g d r v ue i g h t )i:; t .JO ' L.
1
Aluminum ;Antimony !Aris-fcTj.i. c iBarium IBer v.ll ium [Cadmium fCa 1 c i u in ,Chromium ICobal t ICopper IT ran ' " 'Lead 1Htfonesium \
Mercury !Nickel Ir-'atciss ium i$«£ Ionium !feilver ;Sodium !Thai l_i urn IUanadiiifli I7inc !CyoTKi-de? i-.... ........ ..— ,™~- .. _ -. :
Control•Limit
—
1O,620O.O
SOOO.O
t-0 . 0
3OOOTO
3000 , O
1O.O5000-0
„ —... — ., — . — . —.— .
i! Sample
! 47O7; 30
. 30: 939' 1I *
1 4! 20193! WV1; fciv-! 17I :WOi;:2! 33< i i *-• 't jr ,L j. x_ .L *-i
it; 330; 49c-41 •«r -*.T "i 3! 135*471 'i r-1 .L *.-r ••••», .v.I 3331 i i4r •'• *t3i
i(S) ' C:
i-4AO4! !.OOOOIU!,&£50! !-(3796; ;.:s:i 3S!n;«31 !.0 1 & !-ISiO; ;.0103! I.78 i:i| ;„ 74 W ! H |. 3100J I,2000; 1(U' 0 ' '
" 1 7 3 ;' '-4000IUJ.6912! IB P^TijJO ! &«29so; B;. 40i!s l :.c-o^oi ;. ooooiu :,oooo;ui*9tt2i * ;.7000 ', U !__ _ -= _ ^__. .1 ___ i
Duplicate
4 '364.30 *29.938.
1 -4 -
19736.88.;JQ -11,
274C21..48..
11O93-922 J ,
H
328-?iO7 f^ «
1.'! '"•''
13400.10..*'; •
34 .U16.
_ — „_.„.. ««..._....
31' l'i!OOOO ! UIS 50!1153!3124 IB7491 IB2 530!5SAA !49 &i !S7:l6 IB12OO;•?$tOv !S' AO '5830 I4OOO ! U4?79I6753 IOuOO ! iJ5840 I2 WO !oooo : uOOOO ! U3194 17000 I U
r_......-*_. t ....
' • ; !i . 1
1 1 I
! J .. 11. 1 1:': ; : p
; 5-31 ; ;Fi t f i i 1 1i .. i : •: ; Pi Q '3 " ' ' C-i 7 « , i i | r
! .<•; « r> [ t , P; .U4; ! IF! ;.:..:.s; : IP"; 4'L.%;> ; ; ;ri 1 ., H ! . i i'1'
& - "^ ' ' ' FI *l - i. I ! ', f'1'
! ! I CV• , , j .,-v
1 « . . ' ; i l 1
, .<L .. .J. , ) ( r
! 200.01 ! IF1 .:>.. ••;; ; :Pi -I I i ' ' ILi, ! « • . . , i Ii i i i:.~i ! i i 'i ' > ' ( . . •i i , i r, ..) K O i i i r*
i • • ' r1 1 1 ' *-•i 1 1 •! ,„. ,_._=;„...-, • i „ ' ——
-IN
bflR!OI637
L'.S.. EPA - CLP
7LABORATORY CONTROL «
L.«-*ta Names ^OUTHWEST LrtF* OF OK f;ar» I r«»rt s *8 »»9;-C/O8y
L«tb COCI»K SUJDK CA*e Ho,:: 4H751 OrV'i Nows ' SDG Ho
:;o1-irt I.H? Source;* ^
Aqueous. LCS Sources &.PA-LV
I Aq u ff ou » { ug / L > } Bo lid ( rrtcj / ky )! True ' Found W' ! f' ue Found C _ .--Limits
201O.O;An td rnony j l o to . O I 1033 . W \ 1O2- 3Ar^enl r : 47.4; 'J4-1?! 9o-^Barium ! 196O-6J 1929-121 98.4H&ry t 1 A..UH : 483. O ! 4Ft6 - .ii ; 1 00 - 8CAcJmium I Mfi.O; 403.65"; 9O.4{Calcium :4870O.O;4SG4R 59; 10O-SChromium I 310.01 526. 8?! 103. S
t I UO2-0; 4B».53 I ..7!' I 51S.OJ 504.24! 97.9
I X ran j £040 . O ! 1896 „ -Vt J 93 - C97-5! 99.O3; 3O1.6
^ -oOO » O I 2AOO3 . 33 ! 1O5 - 7W4 . o : 3O1 .951 99. 6
48O- 0 ! MO. 47 ! 104.. 5
: Se:i w ium ; TO. & ;• si.90: 99„ *JSJIvor ; 5OG-0! 486.931 97.4;Godium ;47600,0 JR0291.00 1101 * 4
I 97,O! 94.201 97.1
310O.O!
flRIOI638
VI L - TM7/se
ENVIRONMENTAL HEALTH RESEARCH AND TESTING, INC.RESULT SHEET
WSTOMER NAME:
SAMPLE SOURCE:
SAMPLE TYPE:
DATE RECEIVED:
ANALYST:
SAMPLEEHRT NO.
313323135331374
3133531335313353134131356
K13561356o135631377313773137731377
,313803138031338313383135931359
313473134731368313683138931389
113656134431386
NO.
URS CONSULTANTS
Delaware Sand & Grave)
Quality Control
01-29-91
M. Copper & P. Ward
CUSTOMER NO.
AS-BK1AS-BK8AS-BK15
AS-BK2AS-BK2AS-BK2AS-BK4AS-BK9AS-BK9AS-BK9AS-BK9AS-BK16AS-BK16AS-BK16AS-BK16
AS-BK17AS-BK17AS-BK3AS-BK3AS-BK10AS-BK10
AS-BK6AS-BK6AS-BK13AS-BK13AS-BK20AS-BK20
AS-BK12AS-BK5AS-BK19
(Blank)(Spike)(Spike)
(Blank)(Blank)(Blank)(Blank)(Spike)(Spike)(Spike)(Spike)(Spike)(Spike)(Spike)(Spike)
(Blank)(Blank)(Spike)(Spike)(Spike)(Spike)
(Blank)(Blank)(Spike)(Spike)(Spike)(Spike)
(Blank)(Spike)(Spike)
(Prolect #35214)
PROJECT NO.: 12583
DATE ANALYZED:
LAB NOTEBOOK NO.:
ANALYSIS &METHOD
NIOSH Method 10031,2-DteWoroethane1 ,2-Dlchloroethane1 ,2-Dlchioroethane
NIOSH Method 1501Benzene
Ethyi benzeneTotal XyieneTolueneBenzene
Ethyi benzeneTotal XyieneTolueneBenzene
Ethyi benzeneTotal XyteneToluene
NtOSH Method 1300Methyl Ethyi Ketone
Methyl Isobutyi KetoneMethyl Ethyl Ketone
Methyl Isobutyt KetoneMethyl Ethyl Ketone
Methyl Isobutyl Ketone
NIOSH Method 5020Bis(2-Ethyl Hexyi)Phthalate
Di-N-Butyl PhthalateBls(2-Ethyi Hexyl)Phtnalate
DI-N-Butyf PhthafateBls(2-Ethyf Hexyl)Phthalate
Di-N-Butyi Phthalate
NIOSH Method 5503PCSPCBPCB
01-31/02-07-91
160. Pg.' 50
RESULTS(ug/FBter)
• '
< 2090.1% Spike Recovery91% Spike Recovery
< 15< 15< 22< 15
88% Spike Recovery88.1% Spike Recovery82.1% Spike Recovery90.3% Spike Recovery85.8% Spike Recovery84,3% Spike Recovery81 .6% Spike Recovery92.6% Spike Recovery
< 15< 15
93.9% Spike Recovery108.51% Spike Recovery91.77% Spike Recovery101.17% Spike Recovery
<20< 20
104.9% Spike Recovery98.8% Spike Recovery93.2% Spike Recovery93.2% Spike Recovery
<0.0596.9% Spike Recovery105.1% Spike Recovery
Ol639 J-0005GJ
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY .________
1 tI AS-BK7S I
Lab Name; ENVIR._HEALTH_RESEARCH_TE Contract: .URS_____ I___________I
Lab Code: WS8__ Case No.: 35214 SAS No. s 12583. SDG No.:
Matrix (soil/water): WATER Level (low/nmd):
Concentration Unit* (ug/L or mg/kg dry weight): US/L_
I i i1 1 Control 11 i Limit i1 Analyte 1 XR 11 1 1(Aluminum I i(Antimony 1 I1 Arsenic 175-125 J1 Barium 1 iIBerylliuml I1 Cadmium 175-125 1ICalcium 1 i1 Chromium 175-125 1i Cobalt 1 i1 Copper __ 1 75-125 J _1 Iron i 1ILead 175-125 1IMaanesiuml I1 Manganese t I1 Mercury i I1 Nickel 175-125 11 Pot ass ium 1 11 Selenium 175-125 1I Silver 1 11 Sodium 1 i1 Thai lium 1 i(Vanadium I 1IZinc 175-125 1(Cyanide 1 11 Tin 1 •
11
Spiked Sample 1Result (5SR) CI
11 11 1
332.0000 t 1i 11 1
920.7000 I I1 1
____ 924. 1888 J 1955.1000 1 1
_____ 1166. 0000 J I1 I
940.7000 1 11 1f 1i t
909.6800 1 tt 1
831.6080 1 11 11 1f il l
923.9000 1 I1 1
965.00 1 i
I 1 11 i
Sample 1 Spike 1Result <SR) ClAdded (SA) 1 *R
i iI 11 1
10- 1450IUI1 1i 1
1.8320IUII 1
____ 37. 6000I J_6.8300IUI
____ 98. 90001 J.1 1
16.0000IUI1 1t 11 1
12.0000IUI1 1
22.0270IUI1 I1 11 1f 1
22.7000I i1 1
20.0 IU 1
11
1800.01 83.211
1888.01 92.11
__ 1888. 0 1 __ 86. 61
__ 1888.8I_186.71
10dC.CH 94.1i11
1000.01 91.01
1000.0! 83.21111
__ 1888.81 __ 90.11
1000.0 I 97.0
I It I1 1
01 Ml1 tJNRIJNR!
IP 1.INRI~INR1
IP 1INRIJPJ
INRIJPJJNRIIP 1JNRIJNRiJNRI"iP 1INRIIP 1INRI
JNRI
"INRI.IP iJNRI
1 1
Comments:
FORH V (PflRT 1) - IN
A R I O I 6 l * 0
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ___________
I II ASBK21S i
Lab Names ENVIR._HEALTH_RESEARCH_TE Contract: URS_____ I___________I
Lab Code: W88__ Case No. : 35214 SAS No. : 12583. SDG No.: 000000
Matrix (soil/water): WATER Level (low/med): ___
Concentration Units (ug/L or mg/kg dry weight): US/L_
1 1 1! 1 Control!i 1 Limit 1I Analyte i %R 1i I I(Aluminum 1 t1 Antimony 1 11 Arsenic I75-1£5 1(Barium I 11 Bervl i ium 1 1(Cadmium 175-125 11 Calcium 1 i1 Chromium J 75-125 J .1 Cobalt 1 l"(Copper 175-125 11 Iron 1 1i Lead ____ 1 75-125 J .IMaanesiuml t1 Manganese) 11 Mercury 1 1i Nickel __ 1 75-125 J.(Potassium! 1ISeleniumJ 75-125 J.1 Silver 1 1(Sodium 1 11 Thai lium t i(Vanadium 1 1I Zinc 175-125 1(Cyanide 1 I| Tin 1 |
11
Spiked Sample 1Result (SSR) CI
1t 11 1
804.6000 1 11 11 1
943.9000 1 11 1
____ 962.4000J 1986.2000 t 11149.0800 i 1
1 1975.4000 1 t
1 t1 11 1
____ 937.9000 1 11 I
____ 831.2888JJ1 11 11 1t 1
971.5088 1 11 I
858.70 | |
1 11
Sample 1 Spike 1Result <SR) CI Added (SA)
11 11 1
10. 1458IUI1 11 1
1.8320IUI1 1
____ 37. 6000I J_6.8300IUI98.98801 1
1 i____ 16.0080IUL
1 11 1t 1
____ 12.0000IU1_1 1
22.8270IUI1 1t 11 11 i
22.7000I 11 1
20.0 |U |
___1000. 0
1008.8
__ 1808.8
1800.0
___ 1000.0
__ 1888. 0
__ 1000.0
1 1 i1 1 11 t 1
*R IQI MlI 1 t1 INRI1 INRI
88.51 IP ii INRI1 INRI
94.4IJP 11 INRI
__ 92. 51 JPJ1 INRI
105.01 IP 11 INRI
__ 97. 51 JPJINRIINRIINRI
93.8 IP iINRI
__ 83.1 JPJINRIINRIINRiINRI
1888.81 94.9 IP 11 INRI
1000.0 | 86.0 | | i
Comments:
FORM V (PART 1) - IN 7/87f t R ! O I 6 l * l £-00056;;
3FSOiL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: Environmental Health Research & Testing, Inc.
Customer Name: URS CONSULTANTS
Project No.: 12728_______ Method No.: EPA 8080
Customer Sample No.: TC8-1/1200/45_____ EHRTNo.: 32205
COMPOUNDgamma-BHC (Lindane)HeptachkxAJdrinDieldrinEndrin4,4'-DDT
SPIKE ADDED(uo/ko)505050505050
SAMPLE CONC.(UQ/kfl)000000
MS CONC.(ua/ka)56.5563.3463.5459.1659.6459.82
MS%REC*111.6126.8127.09118.56119.29120.6
QC LIMITSREC.46-12735-13034-13231-13442-13923-134
COMPOUNDQtmma-BHC (Undine)HftptachtorAldrinDMdnnEndrin4,4'-DDT
SPIKE ADDED(ua/ka)505050505050
MSD CONC.(ua/ka)51.1758.8958.4953.4454.0155.04
MSD%REC*101.3116.8116.9107.09108
110.97
%RPD*9.997.288.2810.29.918.32
QCURPD503143384550
MITSREC.46-12735-13034-13231-13442-13923-134
# Column io be used to flag recovery and RPD values with an asterick
* Values outside of QC limits
RPD: _____Q_____ out of 6 outside limitsSpike Recovery:_____0____ out of 12 outside limits
COMMENTS: ...-:
3FSOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: Environmental Health Research & Testing, Inc.
Customer Name: URS CONSULTANTS ___
Project No.: 12728________ Method No.: EPA 8080
Customer Sample No.: TBC-1/1800/45_____ EHRTNo.: 32211
COMPOUNDqamma-BHC (Lindane)HeptachlorAldrinDieldrinEndrin4,4'-DDT
SPIKE ADDED(ug/kg)505050505050
SAMPLE CONC.(ua/ka)000000
MS CONC.(ua/ka)52.9364.1362.1755.5456.7959.15
MS%REC*105.76128.28124.34111.3113.58119.25
QC LIMITSREC.46-12735-13034-13231-13442-13923-134
COMPOUNDaamma-BHC (Lindane)HeptachlorAldrinDieldrinEndrin4,4'-DDT
SPIKE ADDED(ua/ka)505050505050
MSD CONC.(ua/ka)48.0157,1455.0348.5949.7354.38
MSD%REC*91.97114.39110.0797.3799.46109.63
%RPD*9.7511.512.213.313.38.4
QCURPD503143384550
MITSREC.46-12735-13034-13231-13442-13923-134
# Column to be used to flag recovery and RPD values with an asterick
* Values outside of QC limits
RPD: _____0____fc out of 6 outside limitsSpike Recovery: 0____m out of 12 outside limits
COMMENTS:
p , A-00056YPage 1 <V
A R I O I 6 I 4 3
-U.S. EPA - CLP
5B EPA SAMPLE NC .POST DIGEST SPIKE SAMPLE RECOVERY .———————————__
Lab Name: ENVIR. HEALTH RESEARCH TF. Contract: ras______ I___BC215
Lab Code: uaa Case No.: 3-740 SAS No.: 12728 SDG No.: QQOOOO
Matrix (soil/water): SOIL Level (low/med): ___
Concentration Units: ug/L
1 I I| | Control Ij j Limit I Spiked Sample1 Analyte | %R ] Result (SSR)! 1 i1 Aluminum 1 1] Antimony 1 1I Arsenic | 1 49.301 Barium j 11 Beryllium I 11 Cadmium I fI Calcium j |I Chromium 1 !I Cobalt 1 iI Copper i 1i Iron ] I1 Lead 1 |1 Magnesium! 11 Manganese! [1 Mercury I II Nickel I 1j Potassium! j(Selenium 1 j(Silver | 1j Sodium I i1 Thallium i 11 Vanadium I IIZinc 1 11 Cyanide | j1 1 1
CSample
Result (SR)
6.90
CSpike
Added (SA)
500.0
%R
84 _ a
...
..
Q
[
M
Comments :(AS) DILUTION VALUE; SAMPT.F HTTTTTFT^ 1:10 THEN SPTVFTI —— TOTAL HETAT.S ANALYSTS
32203
^ 6-OC05GSFORM \ 0 I 6**l 7/87
U.S. EPA - CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,—————_______
1 TBC230Lab Name: ENVIR, HEALTH RESEARCH TF Contract: ITRS_____ I____
Lab Code: us a Case No.: 3-740 • SAS No.: 12728 SDG No.: 000000
Matrix (soil/water)r SOIL Level (low/raed): _____
Concentration Units: ug/L
11i1 Analytei} Aluminum| Antimony1 Arsenic1 Barium(Beryllium1 Cadmium1 CalciumI Chromium1 Cobalt1 CopperI IronI Lead1 MagnesiumI Manganese1 Mercury1 NickelI Potassium| Selenium1 SilverI SodiumI Thai lium1 VanadiumIZinc1 Cyanide1
Control :Limit%R
.
Spiked SampleResult (SSR)
50.10
CSample
Result (SR)
8.6
CSpike
Added (SA)
50.0
%R
83.0
i
Q
111
M |1i11111ij11111i11I111I!11'
Comments:(AS) DILUTION VALUE: SAMPLE DILUTED 1:10 THEN SPIKED. TOTAL METALS ANALYSIS.
TBOI/12QQ/30__32204 ________________
0-000560FORM V pA- 01 61*5 7/S
-U.S. EPA - CLP
5B EPA SAMPLE NO.jrwoi u.i.V9£**3 x &r«Lric* 0/uifj t* *\**ww » A^^V* . • — - — — —— ™ — _ ——
I TBC245Lab Name: ENVIR. HEALTH RFSFARCH TF Contract: TJRS 1
Lab Code: Case No.: ;
Matrix (soil/water) : SOIL
J-74Q SAS No.:12728 SDG No. : 000000
Level (low/med) :
Concentration Units: ug/L
1 1 !j 1 Control i| | Limit | Spiked Sample| Analyte 1 %R 1 Result (SSR) Ct I 11 Aluminum 1 11 Antimony I !I Arsenic ! i 50.401 Barium ! i1 Beryllium! !} cadmium 1 I1 Calcium | 11 Chromium ! 11 Cobalt I I(Copper I 1llron i tI Lead I 1j Magnesium! 1(Manganese! I1 Mercury 1 1! Nickel [ |I Potassium! * 1I Selenium I 1(Silver j 1( Sodium 1 j(Thallium 1 I(Vanadium 1 1IZinc 1 11 Cyanide 1 11 i 1
—
—
SampleResult (SR)
2.20
C
u"
"«
~
-
SpikeAdded (SA)
50.0
%K
101
i11
Q! MIi
.1iiitiitiiiiiii!i11
1i11
Comments :(AS) DILUTION VALUE: SAMPLE DILUTED 1:10 THEN SPIKED. TOTAL METALS ANALYSIS.
TRr i n ?nn/Aswns
6-0005YOFORM V 7/87
.U.S. EPA - CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,————————__
I TBC515Lab Names ENVIR. HEALTH RESEARCH TF Contract: URS_____ I_____Lab Code: yaa Case No.: 3-740 SAS No.: 12728 SOG No,: OOQOOQ
Matrix (soil/water) : SOIL Level (low/med) : ___
Concentration Units: ug/L
1111 Analytei(Aluminum| Antimony1 Arsenicj BariumJBerylirum1 Cadmium| Calcium1 Chromium1 Cobalt1 Copper(Iron!Le*d{Magnesium1 Manganesei MercuryI Nickel1 Potassium( SeleniumI Silverj Sodium(Thallium(vanadiumIZinc1 CyanideI
ControlLimit%R
Spiked SampleResult (SSR)
5(5.30
c
m
SampleResult (SR)
2.9
CSpike
Added (SA)
SfKO
iii
%R IQi11
Q^.a 1I1I11!1i1!i 'I!1i11Ii1
._!i
M
Comments:(AS) DILUTION VALUE: "SAMPLE DILUTEE 1-20 THEM SPTEFTi.——TOTAL MFTAT.q ANATY<!Tq
32206
fr-00 (J5 7 iFORM V (PART 2 7/87
ARI016U7
,U.S. EPA - CLP
SB EPA SAMPLE NO.
1 TBC530 !Lab Name: EKVIR. HEALTH RESEARCH TT? Contract: TTRS 1 l
Lab Code: y Case No.:
Matrix (soil/water) : §gx^
5-740 SAS No. :12728 SDG No. : 000000
Level (low/med) :
Concentration Units: ug/L
1 1 i| | Control 1| | Limit | Spiked Sample| Analyte | %R | Result (SSR) C1 1 i1 Aluminum f i1 Antimony I I1 Arsenic 1 1 51.70j Barium 1 11 Beryllium 1 11 Cadmium [ II Calcium i I(Chromium I !1 Cobalt 1 I1 Copper | Illron 1 1I Lead I 11 Magnesium] 1(Manganese! i1 Mercury 1 • 11 Nickel I ij Potassium! I1 Selenium 1 I(Silver ! I1 Sodium 1 I(Thallium 1 Ij Vanadium ! !(Zinc | I( Cyanide 1 11 t 1
—
-
SampleResult (SR)
6.9
C
*
-
—
"
"
—
\Spike
Added (SA)
so.o
%R
89.6
Q
~
-
-
1I1
M i
t|111'it\\11|IiiiililIliii
Comments :fAS> DILUTION VALUE;. SAMPLE DILUTED 1:10 THEK SPIKED. TOTAL METALS. ANALYSTS ——
T-ar i /i srtn/^n32207
0-000572FORM V (PART 2) fl R | Q j 6 1*8
. U.S. EPA - CLP
5B ' EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,———————______
I TBC545Lab Name: EXVIR. HEALTH RESEARCH TF. contract: URS_____ 1_____
Lab Code: uaa Case No.: 3-740 SAS No.: 12728 SDG No.: QOQQQO
Matrix (soil/water) : SOIL Level (low/med) : _____
Concentration Units: ug/L
i111 Analyte1| Aluminumj Antimonyt Arsenic1 Barium(Beryllium1 Cadmium| Calcium1 ChromiumI Cobalt1 Copper1 IronILead(Magnesium{ ManganeseI Mercury(Nickelj Potassium! Selenium(SilverI Sodium[Thallium(VanadiumIZinc( Cyanide1
1ControlLimit*R
.'Spiked SampleResult (SSR)
48.00
.
cSanpl*
Result (SR)
4.90
1_.c
SpikeAdded (SA)
sn n
%R
a*, 7
.
Q
„
M
Comments :/^ nTTTTTTAM VAT.TTFt ——— QAMPT_g HTT TTTPH 1.10 THFM gPTVFD ——— TOTAT, MFTAT S flNflT
TBC-1/15QO/45•322DT
000573FORKV (PART 2) - A R I 0 i 6 U 9
- CLP :
5B EPA SfiMPLE NC.POST DIGEST SPIKE SflMPLE RECOVERY ____
I TBC31'N*m«: £N\;lR._HEflLTH_RESEflRCHjTE Contract: URS_____ i ._-... _
Lab Cxie: iJSe__ JC*w No.: 3-748 SnS No.: 1£7£8_ SDG. No. : -3000130
fla'Sri- iBc:I.**are»-! : SGIL_ Level (loW
Concentration Units: ug/L ug/L
i : i i i i; 1 Control! i 1 I
i Limit t Spiked Sample E Sample 1 Spike 1lfln*lyte I *R i Result (SSR) CI Result CSR) Clftdded <SA) It i l 1 1 1IRluwimiia i f I 1 I I 1Iflntuoony I I f 1 I I 1iflrsenic i 1 47. £13 1 1 £.£& IUI 50.911 Barium I I I I i t 1iBerylliural I 1 ! I I 1ICadroium 1 1 i 1 I I iICalciurn 1 1 1 i _ i I 11 Chromium I I I I 1 i 1ICobalt I I 1 1 I I iICoDoer 1 1 I I I I 11 Iron 1 1 I I I f 1ILead I I I I I I 1IMaonesium! 1 I I I I 1IM-naaneiel ! I I I I 1i Mercury I I t f I t 1INicksl 1 i I I I I I1 Pot ass i urn 1 1 i 1 11 1
i Selenium ! ! 1 i I I I1 Silver 1 I ' l l I I 11 S o d i u m I 1 I I I I IIThalliura I I I I I I I1 Vanadium 1 ! 11 1 1 1iZinc 1 1 I I . I I 11 Cyanide 1 1 I I I I 1i 1 1 I I f 1 1
1 1 i1 1 , !1 I 1
%R IQI Ml1 ! 11 I N R I1 i NR 1
94. H| IF 11 J N R I1 INR!! INRI1 I N R l1 INRI1 INRI1 I N R I1 INRI1 I N R I1 INR!i I NRI1 INR!1 I N R Ii INRI1 I N R I! INRI
1 I N R I1 INRI
1 INRI1 I N R II 1 1i 1 1
Comment s:<flS> DILUTIQN_VflLUEs_Sft«PLE DILUTED_1: i0_THEN_SPIKEDTBC-l/1800/15
TOTflL METflLS ftNflLYSIS
FORM V CPflRT £) - IN 7/87
ARIOI65[£OG0574
- U.S. EPA - CLP
SB EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY .——————————__
~ +. TBC830Lab Name: ENVIR. HEALTH RKSFA'srH TE Contract: TRR_____ i______
Lab Code: waft Case No.: 3-740 SAS No.: 12728 SDG No.: 000000
Matrix (soil/water): grm Level (low/med): ___
Concentration Units: ug/L
i ^ 11 " 1i1 Analyte1| Aluminum| Antimony1 Arsenic1 Barium(Beryllium1 Cadmiumj Calciumj Chromium1 Cobalt1 Copper1 IronILe.d1 Magnesium| Manganese1 Mercury1 Nickel1 Potassium| Selenium[Silver1 Sodium1 Thai liumj VanadiumIZinc1 Cyanidet
ControlLimit%R
•
Spiked SampleResult (SSR)
51.10
9.60
19.2 .
-J
C
i -•*"»: --, . - • .33?«Us.
SampleResult (SR)
a in
9.60
2.14 -
~3*w=i
C
B
«.
'•-'Spike
Added (SA)
50.0
?n.n
20.0
'
%R
fiS.60
104.5
96.0
Q M
i
Comments:m*m- .l HV4- -l.i-.LJ ,1 1-1 - _i tJ i «i. -..i-t |f||-i||r ............... ... - —————— •
T-RC } 1
322101800/3Q —————— - ———————————————————————————————————————— • ——————
6-000575FORM V (PART : fiR j 0 | 65 I 7/8?
U.S. EPA - CLP
5fl EPA SAMPLE NO..SPIKE SAMPLE RECOVERY
Lab NAM«I ENVIR. HEALTH RESEARCH IE C
_ab Code: U88 __ Caie No.: 3-740
Matrix (soil/water): SOIL_
Concentration Units (ug/L or
I I I t1 IControll 11 1 Limit I Spiked Sample i! Analyte 1 *R t Result (SSR) CI Ril i t 1( Aluminum 1 1 1 1 '(Antimony I I 1 11 Arsenic 175-125 1 39.9612 I 1! Bar ium 175-125 1 87.3327 1 1IBervlliutwl l 1 1 ....1 Cadmium 175-125 ! 45,8390 1 1(Calcium 1 1 I Ii Chromium 175-125 I 44.3938 I 11 Cobalt 1 1 I I1 Copper I I I Illron 1 1 . 1 1(Lead 175-125 1 49.2726 1 1IMaanssiuml 1 1 1IManqanese! t I 11 Mercury 175-125 1 1.2233 I 1(Nickel 1 . i 1 1(Potassium! 1 1 11 Selenium t 1 I I1 Silver (75-1S5 1 43.5596 1 1i Sodium 1 1 I I[Thallium 1 1 I I
i : i1 TSC845S i
ontract: URS I 1
SAS No. : 12728_ SDG No. : 000000
Level (low/med): ___
mg/kg dry weight): MG/KG
i 1 1 i !1 • 1 i l l
Sample 1 Spike 1 I I I>sult (SR) C [Added (SO) I %R IQI Ml
1 i i l lI I I I INRII I 1 1 I NRI
0.5432IBI 48.5! 81.31 IF 134.64601 1 43.51 108.61 IP I
1 1 1 1 I NRI0.4850IUI 48.51 94.51 IP t
I I 1 1 INRI3.88941 1 48.51 83.51 IP 1
I I i I I N RfI I 1 1 INRII I 1 i INRI
0.52381 1 48.51 100.51 IF 1( I 1 I INRII I I 1 (NR1
0.0244IUI 1.21 100.81 ICVI1 1 1 1 I NRII t 1 ! INR!I I i ( 1 ) i INRI
0.4850IU1 48. 5 1 89. SI IP !I I f I I NRI( I I I I N R
(Vanadium I I I I I t I I INRIIZinc 1 1 1 1(Cyanide 1 1 1 I1 1 1 I I
I I I I I N RI t I I I N RI I I i I
Comments:TBC-1/ 1803/453E211TOTAL METALS ANALYSIS
1. Sample was spiked, digested and analyzed. 5 times to determine aSpike Recovery because of the matrix problem the spikes were not reproducible:(1) W\ (2) 50% (3) 68% (M 61% (5) 61%
FORM V (PART 1) - TW _ 7/87
A R I D
U.S. EPfi - CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ___ ______
1 TBC845Lab va e: ENVIR. _HEfiLTH_RESEflRCH_TE Contract: URS_____ I________
Lad C:.Je: U68__ Case No.: 3-743 3AS No.: l£7£fl_ SDG No.: 000000
Matrix s-:: I/water* s SOIL Level (leu
Concentration Units: ug/L ug/L
i l l . ! t ii _ iControll 1 i ^ 11 1 Limit 1 Spiked Sample 1 Sample I Spike 11 A*alytr~ 1 " ?-R 1 Result TSSR) CI Result <SR) C Ifldded tSfl) 1] ^ ../ - r r —*t;"!". "^ " ""' •" -* -*-r- -•—'-{ ----- -**>*. _»«,•=-..=£ .,.- . * • -,i {-_-Iftluminum ! ! "' ' •" - ~~t--| —— -- -,---—— j { j(Antimony 1 ' 1 I f I I 11 Arsenic ! . _ . 1 I I I I 1
1 B a r i u m I I 1 ! 1 1 1IBervlliuml 1 I I I f 1(Cadmium 1 1 t 1 I I I[Calcium I 1 I f " " f 1 1
l Chromium ( I I I I t 1f Cobalt I I I I ( 1 (ICoDoer I I 1 1 ! I 11 Iron 1 1 I t I I 1ILead I I 1 1 ( t 1IMaanesiuml 1 1 1 I I !
1 Manganese i 1 I I f 1 11 Mercury I I I I I t !INickel I I 1 1 I I 1IPotassiuml 1 i 1 I t !! Selenium 1 1 £0.70 f 1 £.14 lUt £0.®ll Silver I 1 ( i I I 1
i Sod ium i 1 1 I 11 I(Thallium i 1 t 1 I f 1
1 Vanadium I I I I f 1 ' 1iZinc I I t 1 1 1 1(Cyanide 1 1 1 i I I t
i 1 :' 1 ! i
1 !%R IQI I"U
I I 11 INR!1 I N R i1 I N R I
1 I N R It INR!1 [NRI1 INRI1 INRII IMP'
t INPit INRIi I N R I1 I NRI
1 I N R I1 I NRt1 INRI1 I N R l
103.51 IP i1 INPI1 INR!1 I N R i
1 I N R i! I N R It 1 . i
Comments:TBC-i/1300/4532211TOTAL METftLS ANALYSIS
FORM V (PART £)
B R I O I 6 5 3
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY _^___ ___
I TBC845SLsb Mam*: ENVIR._HEALTH_RESEARCH-TE Contract: URS_____ i________
C:-dts U88__ Came No. : 3-740 SAS No. : 1£728_ SDG No. : 000000
Matrix is:.-. 1'water i : WATER Level (low/med) : __^
Concentration" Units (ug/L or mg/kg dry weight): US/L_
I 1 1 i 1 1...I 1 Control I i 1 L1 1 Limit i Spiked Sample t Sample t Spike 1lAnalyte 1 *R 1 Result (SSR) CI Result (SR) CtAdded (SA) tI t ! 1 I I
*R
(Aluminum 1 1 I I - I I 1(Antimony 1 I •1 Arsenic *175-125 1i Bar ium (75-125 11 Beryllium! 1ICadauum 175-125 11 Calcium 1 11 Chromium 175-125 I1 Cobalt 1 IICoDoer I (I Iron I !ILead 175-125 IIMaanesiuml tIManaanesel !t Mercury 175-125 11 Nickel 1 1I Potassium! !1 Selenium »l 75-125 (1 Silver (75-125 Ii Sod i ura l 1! Thai Hum 1 1(Vanadium 1 11 Zinc 1 I1 Cyanide 1 1
1 168.3000 i 1805.9000 1 t
. . i t497,5000 1 1
1 1463.8000 1 i
f i.i tl i
508.5000 i 11 t
1 14.6800 1 !
I 11 t
17.2000 1 1485.9000 1 t
1 I1 1
i t1 11 1
1 I£5.30001 1
310.00001 11 t
5.00001U!1 1
6.5000fUi1 1t 11 1
11.6000IUI1 11 1
0. 10001 Ul1 t1 1
2. 1420IU15.0000(UI
1 1f 11 11 11 1
1.50.01
500. 0 11
500. 0 11
500. 0 i1t1
500. 0 11
i5.01
11
20.01500.01
i1t11
36.099.2
99.5
92.8
101.7
93.6
86.097.2
i
1
11 1 1 1 1 I I t
NRII INRIIJFJ1 JPJI JNRII JPJI JNRl1 JPJI JNRIi I N R I
INRIIPJI N R I
I JNRIIJCVI[JNRII JNRI
i "IF ii JPJI J.NRII JNRII JNRII JNRII JNRI1 I i
Comments:TBC-1/1800/4532211_____~TCLP METALS ANALYSIS
FORM V (PART 1) - IN 7/87
(3-000573
- U.S. EPA - CLP
SB EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY .———————.————
Lab Name: ENVTK. HFAT.TW pygpAoru TF Contract: URS______ I TTC215
Lab Code: W88 Case No.: 3-740 SAS No.: 12728 SDG No.: QQQQQQ
Matrix (soil/water) : SOIL Level (low/med): _____
1 - -11 " "1I Analyte11 Aluminumj Antimony1 Arsenic1 BariumI Beryllium1 Cadmiumj Calciumj Chromium1 Cobalt1 Copper.llronILeadt Magnesium1 Manganese! Mercury1 Nickelf Potassium| SeleniumI SilverI Sodium| Thalliumj VanadiumI ZincI Cyanidei
k-ControlLimit%R
Spiked SampleResult (SSR)
52.70
34.20
_17,40
~
c
—— --.___,-„._
~" SampleResult (SR)
4.0
12.5
9 1 L
CSpike
Added (SA)
so.o
20.0
20.0
%R
25.4
108.5
87.0
Q
W
i
M
Comments:
URS# TTC-1/1 200/1 S
SAMPT.B nTLlTTED 1 - i n THEN SPTITim ———————
FHRT# 3?194
FORMV A R 1 0 I 6 S- i5 7/87ft-00057'
U.S. EPA - CLP
SB EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY __._
\ TTC215 ILab Namt: ENVIR.J€flLTH_RESEftRCH_TE Contract: URS_____ I___________I
Lab Code: W88__ Casm No.: 3-740 SflS No.: 127£8_ SDG_No. : 0001300
Matrix dci1/water)E WATER Level (low/med): ___
Concentration Units: ug/L ug/L
i t t 11 1 Control! 11 I Limit 1 Spiked Sample 11 Analyte t *R 1 Recult (SSR) Ci) t I 1I Aluminum I I I I1 Antimony I 1 1 11 Arsenic 1 1 48. 40 1 11 Barium I t I f1 Beryllium! t I 11 Cadmium I f 1 1(Calcium l i I f1 Chromium I t 1 11 Cobalt 1 i 1 1ICopoer I I 1 !1 Iron 1 i I IILtad I t I IiMannesiuml I t 11 Manganese! 1 t 11 Mercury ! 1 f t(Nickel t 1 I IIPotasiiuml t 11 Selenium 1 I l*r. !•% 1 1ISilver 1 II S o d i u m 1 1 i l
1 t 1 1 11 1 i l l
Sample 1 Spike 1 1 1 1Result (SR) Clfldded (SA) I %R IQI Ml
1 1 I I II I 1 1 INRI1 1 i i INRI
£.£0 iUl 50.01 36. SI IF 11 1 t ! INR!i 1 t 1 INRI
1 ! 1 i INRIt i 1 1 INR!I I I i INRI1 1 1 1 INRII I i i iNRI1 ! 1 1 INRI! 1 t 1 INRII t t 1 INRI
I 1 1 ^1: I f • INP.1 1 ! 1 iNRI1 i i 1 INRI
:' ••+ IUi £0.01 S&.5! IF I. 1 1 ! INRI
I 1 ! ; INR.
hall i u m 1 ( I I I IVanadium 1 1 1 I | 1 IN R iin-- i . - - i 1 i INRIICya- •» t 1 I ' 1 I I ?
Comments:TTC-i/l£00/15
TCLP fr -.^ flNfiL
FORM V (PART £) - TN 7/87
A R I D 1656 0-000500
5B EPA SAMPLiE3QST DISE5T SPIKE SAMPLE RECOVERY
__ " £PS No.: l£?28_ SDG No.:
_ -..-•-..- Level (low/med) :
C or cent rat i on Lr. 115: u g .' L ug / L
: ! i ; 1 1'• ! Control ! I i . 1
i 1 Limit 1 SpiUed Sample 1 Sample 1 Spi^e !'Qr-.slyte- i %R i Result (SSR) CI Result (SR) CIAdded (Sfi) 1
• i ' I 1 1 1Iftlaminum 1 i i 1 i 1 f
l Antimony i 1 1 ! I I i1 Arsenic i 1 49.50 1 i £.20 IU! 50.0!
1 B a r i u m I I 1 - 1 1 1 1IBe^vlliuml 1 1 i I I 1! Cadmium 1 1 1 1 t 1 11 Calcium 1 1 I I - I I t
1 Chromium 1 1 I I I I 1ICoQalt I I I I . 1 1 t
1 Copper I I t 1 I I 1llron t i 1 1 I I fILead 1 1 I I I I 1IMannesiuml S I t 1 1 1IMarqanesel 1 I I I I 1I Mercury t I I t I I IINickel 1 I 1 1 1 1 11 Potassium! t I I I I i
1 Selenium I t I t I I 1ISilver t M 1 1 1 i 1 .
l Sodium I I I I 1 i I1 Thai lium 1 1 I t I I i
1 Vanadium I t 1 1 I I 1IZinc 1 1 I t I I 1
i !i ! li 1 1
*R IQl Mli i E"INRI
I INRi99.01 IF 1
I INRI1 INR!1 INRI
____ ! JNRIi "INR'I1 INRI1 INR!1 INRI
1 INRI1 INRI
i I N R I1 I N R I
i I NRI1 INRI
1 I N R i1 INRII INRI1 i N R I1 INRI1 INRI
1 Cyanide I 1 I I I I t 1 1 1! I I I 1 1 f f i l l
Comment s 3(AS) DILUTION VALUE :_D I LUTED Is 10 THE_SPIKED.TTC-1/1200/30_____________________________32195_______TOTAL .METALS_ANALYSIS.
FORM V (PART £) - IN 7/87.
A R I O I 6 5 7 fe'°C05Si
JJ.S. EPA - CLP
SB EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,—————————____
Lab Name: ENVIR. HEALTH RESEARCH TE Contract: ims_____ 1 TTC245
Lab Code: uaa Case No.: 3-740 SAS.No.: 12728 SDG No,: QOQOOO
Matrix (soil/water): SOIL Level (low/med):
Concentration Units: ug/L
1 i 1j j Control 1| j Limit I Spiked Sample| Analyte | %R 1 Result (SSE)1 ! I1 Aluminum I Ii Antimony i 11 Arsenic 1 I ^ 7ni Barium 1 i1 Beryllium! 11 Cadmium 1 jI Calcium I 11 Chromium 1 !1 Cobalt i 11 CctePer 1 1llron I I1 Lead I 1I Magnesium 1 1(Manganese! iI Mercury i • 1(Nickel I 11 Potassium I Ij Selenium 1 1tsilver 1 1j Sodium 1 1(Thallium 1 11 Vanadium t 1IZinc i 11 cyanide i 11 ! I
CSample
Result (SR)
6.2
CSpike
Added (SA)
50.0
*R
.
95.0
Q
i!1
M li1iii[
i1I1I1iii111i!111!
Comments:(AS) DILUTION VALUE: SAMPLE DILUTED 1:10 THEN SPIKED. TOTAL MP,T*T-fi AWAT.YSTS
"""TTC-I/ 1200/4532196 ___________________________
FORM V (PART 2)-lflR|0|658
*U,S. EPA - CLP
5B EPA .SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,_———————————
Lab Name: ENVIR. HEALTH RESEARCH TR Contract: jmo_____ j FTC515
Lab Code: was Case No,: 3-740 SAS No.: 12728 SDG No.: OQQQOO
Matrix (soil/water) : SOTT. Level (low/med) : ___
Concentration Units: ug/L
11i1 Analyte1| Aluminum| Antimony1 Arsenic1 Bariumj Beryllium1 Cadmiumj Calcium| Chromium1 Cobalt1 CcpperllronI Lead1 Magnesium(ManganeseI MercuryI Nickel(Potassium1 Seleniumt Silver1 Sodiumj Thai liumI Vanadium"IZinc1 Cyanide1
ControlLimit*R
...
Spiked SampleResult (SSR)
53.70
CSample
Result (SR)
2.7
CSpike
Added (SA)
50.0
%R
102.0
.
Q
,
M
Comments:
rrr-i /T-.AQ/I32197
L5 —— . ———————————————————————————————————————————————————
FORM V (PART 2 A R i 0 I 6 5 9 7/8?
*U.S. EPA - CLP
SB EPA SAMPLE NO.
I TTC530Lab Name: ESVIR, HEALTH RESEARCH TE Contract: URS 1.
Lab Code: y^8 Case No.:
Matrix (soil/water) : SOIL
3-740 SAS No. :12728 SDG No. : 000000
Level (low/med) :
Concentration Units: ug/L
1 1 11 j Control i1 j Limit j Spiked Sample| Analyte [ %R 1 Result (SSR)1 t 1(Aluminum 1 i(Antimony I i1 Arsenic 1 i svon1 Barium [ 1I Beryllium! II Cadmium j |I Calcium j j1 Chromium ! !1 Cobalt 1 (1 Copper I |llron I 1! Lead ( ij Magnesium! j1 Manganese 1 )(Mercury 1 1(Nickel I (1 Potassium] * i(Selenium 1 1ISilver I !1 Sodium ! I(Thallium 1 i(Vanadium 1 iI Zinc I (1 Cyanide I I1 1 I
Comments :fAS> DTLUTTON 'V&T.TTF? gAMPT.f *nTf ; yf _L —————————————————————————————— _..
C
~
—
—
_
_
SampleResult (SR)
5.0
C
*~
~
•CT-, 1:10 THEN SPIKED.
SpikeAdded (SA)
50.0
%R
97.8
Q
"
1
1M |
11i
THTAT METALS ANALYSTS
TTC-1/1500/3032198
&OOQ584FORM V (PART 2) - I«A R I 0 I 6 6 0 7/87
U. 5. EPS .- CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ___________
i TTC545Lab Name: ENVIR* _HEftLTH_RE5E3RCH_7E Contract": URS_____ ! ________
Cods: wS3__ Case No. : 2-7- 3 SfiS No. : 127£8_ SDG No. :
'-i-^ = : i '; •<*. airs:'; :-.uCI-_ . " " :/. "".._" .Level (low/med):
C:<r,ceritration Units: ug/L ug/L
1 1 1 1 I II (Control ! t • f i! i Limit 1 Spiked Sample t Sample 1 Spike 1lAnaiyts ! %R \ Result CSSR) CI Result CSR) ClAdded (SA) I
1 ' ! 1 ! 1 1: Aluminum i f i - 1 I I Iiflyitimoriv 1 i ' I I 1 1 ii flr-sentc I i 51.30 1 1 2.20 tUi 50.131
1 Barium I t 1 i t 1 1IBervlliuwl i I I i t i
i Cadmium 1 1 1 1 1 1 1! Calcium i t I t I I 1(Chromium ( 1 I I I I 1i Cobalt I I ' I I I i 1ICoooer I . I I I I t Iilron I I I I I I 1(Lead 1 1 I I I I !IMaanesiumi I t 1 t i 1'Manpanesel 1 I I I I ti Mercury 1 1 1 1 1 1 tINickel 1 1 I I 1 1 !! P o t a s s ium! ! 1 1 I f t(Selenium i t I I ' 1 1 ti Silver 1 1 I I t i 1
1 Sodium 1 i I I 1 , 1 1i Thai lium I t t 1 f ! 1
1 Vanadium I f I t 1 i t(Zinc I I t 1 I f 1IC/anide I I 1 1 I I i
1 i i1 ! '\ { \
%R IQI Mi1 ! 11 INR;t iNR!
103.6! IF f1 I N R Ii I N R II INRIi INRI1 INRI1 INR!
1 I N R I1 I N R It INRI! INRI
i INRI1 INRI
i I N R Ii INRI
1 INRI1 INRI
1 I N R I1 I N R I1 INRIE INRI
i 1 11 ( 1 E l i t 1 1 1 1
Comments:(flS) DILUTIDN_VfiLUE:_SAMPLEjnLUTED 1:10_THEN_SPIKED.TTC-1/1500/45_________________________________32199 ___ _________TOTAL METALS ANALYSIS
FORM V (PORT £) - IN 7/87
A R I O I 6 6 1
.U.S. EPA - CLP
5B . EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ..——————______
Lab Name: EXVIR. HEALTH RESEARCH TE Contract: I-RS_____ |_TTC815
Lab Code: ua a Case No.: 3-740 SAS No.: 12728 SDG No.: OQQQQQ
Matrix (soil/water): SOTL Level (low/med): _____
Concentration Units: ug/L
I I I1 i Control ]I j Limit I Spiked Sample| Analyte 1 %R | Result (SSR)1 1 11 Aluminum 1 |1 Antimony 1 iI Arsenic I | 53.4t Barium I iI Beryllium I 1j Cadmium j II Calcium j f1 Chromium I i! Cobalt i |I Copper I |1 Iron I [ILe*d | I1 Magnesium! |1 Manganese] |1 Mercury I 1i Nickel i 1I Potassium! 1I Selenium | 1ISilver i Ij Sodium 1 ![Thallium 1 |I Vanadium j 1(Zinc I i(Cyanide I |.1 1 I
CSample
Result (SR)
7.1
. .
CSpike
Added (SA)
50.0
11i*R 1Q
i1I
92.6 IiI1111i!11111ii1!1i111
I
M |1
!1IAJt
1
Comments:(AS) DILUTION VALUE: SAMPLE DILUTED 1:10 THEN SPIKED. TOTAL METALS ANALYSIS.
TTC-J/180Q/1532200 ____________________
6-OOOSSi,FORM V (PART 2 A R [ Q I 6 6 2
' U.S, EPA - CLP
5B EPA SAMPLE NO.POST DIGEST SPIKE SAMPLE RECOVERY ,-—————.———————
TTC630Lab Name: ENVIR...HEALTH RESEARCH TF Contract: URQ_____ i,______
Lab Code: _jas Case No.: 3-740 SAS No.: 12728 SDG No.: 000.000.
Matrix (soil/water): SOIL - -- - Level (low/med): _____
Concentration Units: ug/L
Ii!i Analyte1| Aluminum| Antimony1 ArsenicI Barium(Beryllium1 Cadmium1 Calcium1 ChromiumI Cobalti CcpperilronILeadj Magnesium| Manganese1 Mercuryi Nickelj Potassium| SeleniumISilverj Sodium[Thalliumj VanadiumIZinc1 Cyanide1
ControlLimit%R
Spiked SampleResult (SSR)
b4.50
,
CSample
Result (SR)
iQ.n
CSpike
Added (SA)
50.0
1 11 !1 1
%R IQi M1 I1 11 1
85.8 I 11 !! 1i 11 1! i1 1i 11 11 11 !
. i ii ! '! !1 !1 1 '1 1 :i i1 11 11 11 11 ._ I
Comments:
TT01/ 1800/10 ———————————————32201
s O 005 3. VFORMV (PART 2) AR 101663 ""* '
, U.S. EPA - CLP
SB ' EPA SAMPLE KC.
~ _ ! TTC845ALab Name: ESVIR. HEALTH RESEARCH TF Contract: URS 1
Lab Code: ysf. Case No.: 3-740 SAS No.: 12728 SDG No.: 000000
Matrix (soil/water) : SOIL Level (low/med) :
Concentration Units: ug/L
t 1 1j | Control.!| | Limit 1 Spiked Sample| Analyte I %R 1 Result (SSR)1 ! 11 Aluminum 1 i1 Antimony 1 11 Arsenic 1 | 67.?n1 Barium 1 I1 Beryllium I 11 Cadmium { 1I Calcium j \I Chromium i 11 Cobalt I I1 Copper I II Iron I I]Le*d j i 45.9i Magnesium! j(Manganese! I1 Mercury I . |I Nickel [ I! Potassium! j(Selenium I 1 19.40ISilver i |1 Sodium | 1! Thallium I I1 Vanadium j I(Zinc i 1I Cyanide 1 1I 1 i
C
*••
SampleResult (SR) C
23.4
24.fi
2.14
-
~
—
-
-
SpikeAdded (SA)
50.0
20.0
20,0
%R
8 8. .6
106.5
97.0
1 1! 1I |
Ql M I1!
.1 11
.111 |1 J1jii11 I! 1! !1 11 1
.1J! !
1i 11 Lt I1 1
t
Comments :(AS.) DILUTED VALUE: SAMPLE DILUTES 1:4 THEN' SPIKES-' THTAT METALS AMLIS1S. —————(PB) DILUTED VALUE; SAMPLE DILUTED. I;4Q THEN SPIKEP- ————————— —
URS* rrc-1/1800/45 EHRTff 32202
•0^00583FORM V (PART 2) -Afl 101664 7'''s '
U.S. EPA - CLP
5B EPA SAMPLE NO.
~ *. *. ! TTC845Lab Name: EXVIR. HEALTH RESEARCH TE Contract: URS 1 iLab Code: waa
Matrix (soil/water)
Case No.: 3-740 SAS No.:
: SOIL
12728 SDG No. : OOOODO
Level (low/med) :
Concentration Units: ug/L
11iI Analyte1(Aluminum| Antimony1 Arsenic| Barium| Beryl liumI CadmiumI Calcium1 Chromium! CobaltI Cc/pperI Iron(Lead| Magnesium1 Manganese! MercuryI Nickel| Potassiumj Seleniumj Silver1 Sodium(Thallium(vanadium1 Zinc( cyanide1
ControlLimit%R
Spiked SampleResult (SSR) C
66,30
SampleResult (SR)
21.7
C
"
"
-
SpikeAdded (SA)
50.0
*R
89.2
Q M
1!111
Comments :(AS) DILUTION VALUE: SAMPLE DILUTED 1:4 THEN SPIKED. TOTAT. MFTAT c ANALYSTS.
XTC-l/IROn/AS32202 B - • -
FORM V (PART 2) T ft R ] Q | fi 6 S /&?
U.3. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY ___ .
I TTC845SLib N«MII EN'vIR. J-iEALTHJ-JESEARCHJFE Contract: URS_____ I_________
Lub Cede i MSB__ .___.. Case No. : 3-740 SAS No.: 1£728_ SDG No.:
Matrix ;i.:il/&*aterj t WATER Level (low/med):
Concentration Units (ug/L or rng/kg dry weight): U6/L_
I l l 1 1 11 1 Control 1 _ L 1 . . 1 .1 t Limit l Spiked Sample 1 Sample 1 Spike 1lAnalytg 1 *R 1 Result (SSR) CI Result <SR) ClAdded (SA) 1I I I 1 I fI Aluminum 1 !1 Antimony I 11 Arsenic * 175-125 11 Barium 175-125 1IBervlliuml 11 Cadmium 175-125 1iCalcium i 11 Chromium 175-125 1ICobalt I 11 Cooper 1 11 Iron I lILead 175-125 1IMaanesiuml 1
1 Manganese! Ii Mercury 175-125 1INickel i 1(Potassium) 1J Sel em um*I 75-125 1i Silver 175-125 11 Sod i um t 11 Thai Hum l I1 Vanadium 1 IIZinc 1 11 Cyanide t I1 I I
1 11 1
43.4000 1 1617.3000 t 1
1 1439.3000 1 1
1 1 •455.0000 1 1
' 1 11 11 I
502.4000 1 11 I
1 14.9100 1 1
1 i1 1
17.0000 1 1449.8000 1 1
1 11 I
1 11 1
I 11 1
1 11 1
4. 60001 Bl123.2000IBI
1 15. 00001 Ul
1 16. 50001 Ul
1 t1 11 1
13.00001 11 11 1
0. 10001UI1 i1 1
2. 1420IUI5. 00001111
1 11 11 11 11 11 I
11
50.01500. 0 1
1500.01
1500. 0 1
I11
500. 0 11
15.01
11
20.01500.01
1111
11
*R
87.93.
97.
91.
97.
98.
85.90.
1 1 11 1 i1 1 I101 Ml
1 1 E1 INRI1 INRI
61 IF 181 IP f
t I N RI91 IP 1
t INRI01 IP 1
i INRI1 INRI1 INRI
91 IP 1f INRI
1 I N RI2! ICV!
1 I N R I1 INRI
01 IF 101 IP 1
1 INRI1 INRI1 INRI1 iNRI
f INRI1 1 I
Comments:TTC-1/1800/4532E02TCLP METALS ANALYSIS
^
FORM V (PART 1) - IN 7/87
flRJO!666 A,
STAGE 1
ONSITE IAB SCREENING ANDONSITE LAB COMPATIBILITY
TESTING RESULTS
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