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King Abdulaziz University
Faculty of Engineering, Rabigh
Dep. of Chemical & Mat. Engineering
Thermogravimetric Analyzer TGA 4000
TGA is a quantitative technique:
The weight of a sample is continuosly monitored while
exposed to a change of Temperature in a controlled
atmosphere. It is also possible to measure decrease or increase
of weight in isothermal mode or changing the atmosphere
around sample.
Auto Stepwise TGA can give very good separation for
overlapping decompositions.
Thermogram is showing Auto Stepwise applied.
TGA can quantitatively measure the solvent trapped inside
crystals.
Stepwise TGA: Analysis of Automotive Components
The sample list of the tare weights of crucibles :
Applications
Sample volatility
Moisture content
Oxidation StabilityDecomposition
TemperaturePerformance of Stabilizer
Ash Content
King Abdulaziz UniversityFaculty of Engineering, RabighDep. of Chemical & Mat. Engineering
Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
Inductively coupled plasma mass spectrometry (ICP-MS) is a type of mass spectrometry which is
capable of detecting metals and several non-metals at concentrations as low as one part in 1015 (part
per quadrillion, ppq) on non-interfered low-background isotopes. This is achieved by ionizing the
sample with inductively coupled plasma and then using a mass spectrometer to separate and quantify
those ions.
As (Arsen) Fe (Iron) Sr (Strontium)
Be (Breyllium) Li (Lithium) Ti (Titanium)
Ca (Calcium) Mg (Magnesium) Tl (Thallium)
Cd (Cadmium) Mn (Manganese) V (Vanadium)
Co (Cobalt) Mo (Molybdenum Zn (Zinc)
Cr (Chromium) Ni (Nickel) Sb (Antimony)
Cu (Copper) Pb (Lead) Se (Selenium)
Detection of the following elements:
King Abdulaziz University
Faculty of Engineering, Rabigh
Dep. of Chemical & Mat. Engineering
The 2400 Series II system is comprised of four major zones:
• Combustion Zone
• Gas Control Zone
• Separation Zone
• Detection Zone
CHNS/O Elemental Analyzer
The PerkinElmer® 2400 Series II CHNS/O Elemental Analyzer (2400 Series II) is a
proven instrument for the rapid determination of the Carbon, Hydrogen, Nitrogen, Sulfur or Oxygen
content in organic and other types of materials.
Applications
Polymers Chemicals Pharmaceutical Environmental
King Abdulaziz UniversityFaculty of Engineering, RabighDep. of Chemical & Mat. Engineering
World's Smallest Laboratory FT-IR Spectrometer
The new ALPHA is in a class of its own; with its small footprint, affordable price, exchangeable
sampling accessories and easy to-use software; the new ALPHA will find a place in every
laboratory.
The small footprint of the ALPHA makes it ideal for quality control. The ALPHA in
combination with Bruker Optics powerful OPUS/Mentor software and extensive infrared
libraries provide easy-to-use turn key solutions. Unknown substances are identified in seconds.
Sampling modules allow the analysis of almost any kind of sample (e.g. solids, liquids or gases).
Transmission, diffuse and external reflection and attenuated total reflection (ATR) FT-IR
sampling accessories are available with the Quick Snap™ interface.
Alpha FTIR Analyzer
Applications
Identification of compounds in chemistry Study impurities in semiconductors
King Abdulaziz University
Faculty of Engineering, Rabigh
Dep. of Chemical & Mat. Engineering
Gas Chromatography / Mass Spectrometry
(GC/MSD)
Gas chromatography–mass spectrometry (GC-MS) is an analytical method that
combines the features of gas-chromatography and mass spectrometry to identify
different substances within a test sample.
Plumbing diagram for the 7890B/5977A GC/MSD’s concurrent, mid-point backflush option.
Capillary Flow Technologies enhance performance, productivity, and reliabilityAdvantages include:• Improved retention time stability for heavy-matrix samples• More stable chromatographic baselines • Shorter analysis times• Less source cleaning • Longer column life
The heart of performance:The combination of the Extractor EI source, heated monolithic gold-plated quartz quadrupole, and Triple-Axis Detector delivers the most sensitive, reliable results.
Agilent’s Inert Flow Path Split/Splitless inlet option ensures the inertness of flow path surfaces, allowing analytes to safely pass from injector to detector
GC/MSD high-sensitivity analysis for the full range of
biofuel analytes. The system is easily set up for
simultaneous SIM/SCAN data acquisition to maximize
sensitivity and selectivity, while providing full spectra
for qualitative analysis.
Applications
Pharmaceuticalmetabolomics
Chemicals Food Environmental Forensic/toxicology
King Abdulaziz University
Faculty of Engineering, Rabigh
Dep. of Chemical & Mat. Engineering
High-Performance Liquid Chromatography (HPLC)
High-performance liquid chromatography (HPLC) is a technique in analytical chemistry
used to separate, identify, and quantify each component in a mixture. It relies on pumps to pass a
pressurized liquid solvent containing the sample mixture through a column filled with a solid adsorbent
material. Each component in the sample interacts slightly differently with the adsorbent material, causing
different flow rates for the different components and leading to the separation of the components as they
flow out the column.
Schematic representation of an HPLC unit.
Applications
PharmaceuticalAnalysis
separation of similar molecules
food industry for quality control
King Abdulaziz UniversityFaculty of Engineering, RabighDep. of Chemical & Mat. Engineering
Total Organic Carbon Analyzer (TOC)
Total Organic Carbon Analyzer (TOC Analyzers):A TOC measures the amount of total organic carbon present in a liquid or water
sample. TOC detection is important because of the effects that TOCs may have on
health, not to mention the environmental effects and implications for the
pharmaceutical manufacturing processes. a TOC analyzer always requires some
accounting for the inorganic carbon (IC) that is always present.
Non-Dispersive Infra-Red (NDIR) Detector Non-Dispersive Infra-Red (NDIR) TOC fusion
Schematic representation of an TOC
Applications
Environmental :
Ground Water
Surface Water
Waste Water:Contamination
Drinking Water
Quality
High Purity
WaterSea Water