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Spectra generated by LC-ESI-CID-MS/MS on the Bruker maXis HD system
Ion types:
283.3334
392.11041+
424.1469
488.31951+
559.35951+
609.20981+
637.20661+
786.48531+
851.29709+
886.54881+
1014.58931+
1111.64591+
1169.6728
1198.67311+
1255.69561+
1289.6423
1356.74211+
1433.6774
1472.76063+
1528.776312+
1631.7856
y4
y5
y6
y7
y8
y9
y10
y11
y12
b5 (++) + Hex
y10 (0)
b13++ + Hex
b4 (0) + Hex
y13
y3
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(910.9512), 50.6eV, 79.3min #16672
0.00
0.25
0.50
0.75
1.00
1.25
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO5736
Precursor ion mass 910.450195
Charge 2
Retention time 79.3
Hex on peptide 1
e-value 0.0005
Site allocated? N
Time point 20 hr
SCO number SCO4847
Precursor ion mass 1055.759155
Charge 3
Retention time 59.5
Hex on peptide 9
e-value 0.00083
Site allocated? N
313.15161+ 402.1992
1+
471.22161+
543.23821+
609.78342+
676.32371+
726.34191+
763.35721+
834.39371+
963.43551+ 1034.4670
1+
1070.46511+
1122.51091+
1218.55851+
1305.59131+
1376.62861+
1467.64461+ 1542.6593
1+
1629.6793
1706.77891+
y6
y8 y9y10
y11
y12
y13
y14
y15
y16
y17
b5
b6 (0)
[M+H - Hex(9)]+
y15 + Hex(2)
y14 + Hex(2)
b14 (++)
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(1055.7543), 58.5eV, 24.1min #4470
0.0
0.5
1.0
1.5
2.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 1148.484985
Charge 2
Retention time 25.1
Hex on peptide 4
e-value 0.0000041
Site allocated? N
323.0976
372.22901+
443.2669
530.29741+
586.2524
709.34542+
756.3151
788.37971+
824.8910
860.37911+
916.44321+
973.46211+
1044.49761+ 1131.5335
1+
1203.5814
1289.60821+
1401.6302 1501.63571648.7686
1809.8065
1972.8516
y4
y5
y6
y7
y8
y10
y11
y12
y13
y14
y9
y15
y16b17
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(1150.3926), 65.0eV, 25.1min #4707
0
1000
2000
3000
4000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 1229.501221
Charge 2
Retention time 24.8
Hex on peptide 5
e-value 0.0025
Site allocated? N
304.0325
372.22291+
416.1716
499.2139
530.29071+
568.2439
657.2792
732.3156
824.37322+
859.41421+
917.43571+
973.45531+
1044.48671+
1131.52051+
1202.56481+
1258.4999
1289.58751+
1322.5066
1417.64681+
1455.5655
1530.6548
1647.72491+
1688.7028 1752.68731971.8407
y4
y6
y8
y9
y10
y11
y12
y13
y14
y5
y7
y15
y16
b8
b16 (*++) + Hex(5)
[M+H - Hex(5)]+
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(1229.5012), 65.0eV, 24.8min #4637
0
1000
2000
3000
4000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
315.1211
372.22621+
410.16751+
443.26181+
499.21431+
530.29331+
586.24601+
659.33461+
709.3269
788.37781+
824.37401+
860.36471+
916.42751+
973.45421+
1044.48821+
1131.52511+
1202.5601
1289.59171+
1417.6366
1456.6162 1523.7359 1614.7197
1648.76641+
1809.7826
y4
y5
y6
y7
y8
y9
y10
y11
y12
y13
y14
y15
y16
b10 (*++) + Hex(7)
[M+H - Hex(6)]+
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(928.7089), 50.0eV, 24.1min #4477
0
2000
4000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 874.023254
Charge 3
Retention time 24.3
Hex on peptide 6
e-value 0.00025
Site allocated? N
372.22621+
410.16751+
443.26181+
530.29331+
586.24601+
659.33461+
709.3269
788.37781+
824.37401+
860.36471+
916.42751+
973.45421+
1044.48821+
1131.52511+
1202.5601
1289.59171+
1417.63661523.7359
1648.76641+
1809.7826
y4
y5
y6
y7
y8
y9
y10
y11
y12
y13
y14
y15
y16
b10*++ + Hex(7)
+MS2(928.7089), 50.0eV, 24.1min #4477
0
2000
4000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 928.040222
Charge 3
Retention time 24.1
Hex on peptide 7
e-value 0.012
Site allocated? N
372.22521+
443.26181+
530.29361+
604.25701+
659.33581+
788.37861+
824.37592+
860.37071+ 916.4354
1+
973.45641+
1044.49491+
1131.52551+
1202.56191+
1289.59401+
1417.65281+ 1648.7362
1+
y4
y5
y6
y7
y8
y9
y10
y11
y12
y13 + Hex(3)
y14 + Hex(3)
b7 (++) + Hex(8)
b1 + Hex(2)
b3 (*) + Hex(2)
y13
y14
y15
y16
b6
b5
b7
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(982.0595), 50.0eV, 23.8min #4403
0
2
4
6
8
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 982.059509
Charge 3
Retention time 23.8
Hex on peptide 8
e-value 0.0018
Site allocated? N
372.22481+
443.26261+
530.29221+
586.25361+
659.33921+
709.33252+
788.37651+
824.37602+
859.41661+
916.43231+
973.45991+
1044.49671+
1075.5665
1131.52561+
1203.57471+
1258.51291+
1290.59731+
1418.64611+
1501.6421
1647.72991+
1810.8246 1971.8817
y4
y5
y6
y7
y8
y9
b2 (++) + Hex(3)
y11
y15 (++) + Hex(6)
b17
y14
y15 [M+H - Hex(9)]+
[M+H - Hex(7)]+
y16 (++)
y12
y10
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(1036.0814), 55.5eV, 23.6min #4343
0
2000
4000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4739
Precursor ion mass 1036.081421
Charge 3
Retention time 23.6
Hex on peptide 9
e-value 0.00034
Site allocated? N
385.17001+
442.19611+
499.2495
561.26831+
692.3021
743.33451+ 805.3970
1+
846.41172+
906.43641+
1005.5092
1102.55521+
1249.62421+
1306.64931+
1370.2138
1435.68771+
1507.7464
1560.7565
1593.76261+
1690.80421+
1762.83891+
1933.9386
b7 + Hex(3)
y5
y6
y7
y8
y9
y10
y11
y12
y13
y14
y15
y16
y17
b6
b2 (0) + Hex(3)
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(1210.5563), 65.0eV, 75.7min #15897
0.0
0.2
0.4
0.6
0.8
1.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO0996
Precursor ion mass 1210.556274
Charge 2
Retention time 75.7
Hex on peptide 3
e-value 0.00003
Site allocated? N
230.6622
297.1546
396.22251+
460.25111+
515.28931+
559.31311+
614.3270
663.37591+
760.43751+
846.45691+
903.48491+
982.52921+
1063.51021+
1095.61771+
1144.57371+
1176.58981+
1209.71121+
1289.67731+
1401.7106
1436.73941+
1537.80311+
1663.85471+ 1734.8871
1831.94801+
1943.3299
y4
y5
y9
y6
y10
y11
y12
y13
y15 y16
y17
y8
y7
y3
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(919.7880), 50.0eV, 121.6min #27117
0.0
0.2
0.4
0.6
0.8
1.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4905
Precursor ion mass 919.787964
Charge 3
Retention time 121.6
Hex on peptide 3
e-value 0.000000016
Site allocated? N
329.1503388.1883
1+463.2035
507.7532
604.29961+
664.30942+
703.36781+
760.7872
832.40161+
903.44331+
944.8965
1031.51251+
1102.51241+
1219.58651+
1262.5743
1314.5684
1381.6302
1502.5944 1570.7741
y5
y6y7
y8
y9
y10
y11 (0)
[M+H - Hex(3)]+
[M+H - Hex(2)]+b4
B933 Keenan 20 min_2-C,1_01_1395.d: +MS2(853.3777), 45.4eV, 27.9min #5366
0
1000
2000
3000
4000
5000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 20 hr
SCO number SCO4934
Precursor ion mass 853.377747
Charge 2
Retention time 27.9
Hex on peptide 3
e-value 0.023
Site allocated? N
317.1438
360.22211+
388.17971+
507.24572+
604.28901+
703.35651+
832.39751+
903.43791+
931.3474
1031.49361+
1118.52951+
1219.57011+
1382.6212
y4
y5
y6
y7
y8
y9
y10
y11
b8 (++) + Hex(2)
[M+H - Hex(2)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(772.3414), 41.7eV, 27.4min #5245
0.00
0.25
0.50
0.75
1.00
1.25
1.50
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO4934
Precursor ion mass 772.341431
Charge 2
Retention time 27.4
Hex on peptide 2
e-value 0.00019
Site allocated? N
360.22161+
507.24661+
557.26171+
604.29001+
664.3026
703.35551+
832.39981+
860.3577
903.43561+
1031.49781+
1118.52041+
1219.56991+
1345.60141+
1381.62311+
y4
y5
y6
y7
y9
y10
y11
y8
[M+H - Hex(2)]+
[M+H - Hex(3)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(853.3676), 47.7eV, 27.0min #5157
0.0
0.5
1.0
1.5
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO4934
Precursor ion mass 853.367615
Charge 2
Retention time 27
Hex on peptide 3
e-value 0.00024
Site allocated? N
313.15291+
384.1887
489.23301+
543.2381
609.78552+
676.32611+
763.35821+
834.39551+
963.44151+
1034.47871+
1121.50001+
1218.56051+
1305.59161+
1376.63061+
1467.64031+ 1542.6649 1706.7930
1+
y8
y9
y10
y11
y12
y13
y14
y15
y16
y17
b5 (0)b6
[M+H - Hex(9)]+y14 + Hex(2)
b14 (++)
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(1055.7600), 58.5eV, 23.3min #4220
0.0
0.5
1.0
1.5
2.0
2.5
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO4847
Precursor ion mass 1055.759155
Charge 3
Retention time 59.5
Hex on peptide 9
e-value 0.0003
Site allocated? N
372.22651+
443.26291+
530.29601+
604.25731+
659.33771+
709.33182+
788.38191+
824.37832+
860.37441+
916.43541+
973.45911+
1044.49381+
1131.52621+
1202.56021+ 1289.5976
1+
1417.64321+
1501.62201+ 1613.6930
1648.74281+
1809.79621+
1971.8388
y4
y5
y6
y7
y8
y10
y11
y12
y15 (++) + Hex(3)
b1 + Hex(2) b7 (++) + Hex(8)
y14 y15
y16
b10
[M+H - Hex(6)]+
b6
y16 (++)
[M+2H - Hex(8)]+
b17
[M+H - Hex(8)]+
[M+H - Hex(7)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(982.0628), 50.0eV, 23.3min #4233
0.0
0.5
1.0
1.5
2.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO4739
Precursor ion mass 982.062866
Charge 3
Retention time 23.3
Hex on peptide 8
e-value 0.0045
Site allocated? N
252.0000
372.22651+
443.2631
489.2341
530.29271+
586.25001+
659.3384
709.84081+
789.38021+
824.87832+
917.44501+
973.45971+
1044.49581+
1131.53231+
1164.1415
1202.5603
1290.60491+
1353.03971444.6306 1508.0959
1648.71271+
1809.7969
1887.71661971.8515
y4
y5
y6
y7 y8
y9
y10
y11
y12
y13
y14b2 (++) + Hex(3)
b4 (++) + Hex(6)
y15
[M+H - Hex(7)]+
[M+H - Hex(9)]+
[M+H - Hex(8)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(1036.0841), 55.5eV, 23.1min #4168
0
1000
2000
3000
4000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO4739
Precursor ion mass 1036.084106
Charge 3
Retention time 23.1
Hex on peptide 9
e-value 0.0087
Site allocated? N
363.1710
413.2030
480.23772+
529.27151+
583.7273
658.3056
723.33101+
759.35891+
826.9081
858.4288
891.7084
959.47201+
1001.47831+
1121.53481+
1230.5978
1283.5715
y5
y6
y7
y8
b6 + Hex(3)
[M+H - Hex(2)]+ [M+H - Hex]+
[M+H - Hex(3)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(723.3178), 35.8eV, 25.9min #4871
0
2000
4000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO1714
Precursor ion mass 723.31781
Charge 2
Retention time 25.9
Hex on peptide 3
e-value 0.019
Site allocated? N
298.14261+
341.1888
411.22791+
480.24381+
524.2434
567.2783
595.31351+
662.82902+
715.3777770.3346
827.39551+
914.42651+
968.4027
1027.52431+
1156.55651+
1227.6006
1324.64891+
1440.6369
1496.73571+
1559.8387
1650.77621771.7698
1814.8776
y4
y5
y6y7
y8
y9
y10
y11
y3
b10 (++) + Hex(2)
y11 (++)
[M+H - Hex(2)]+
B933 Keenan 35 min_2-C,3_01_1399.d: +MS2(910.9274), 50.6eV, 53.2min #12149
0
1000
2000
3000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO3540
Precursor ion mass 910.927429
Charge 2
Retention time 53.2
Hex on peptide 2
e-value 0.000055
Site allocated? N
319.16471+
360.1515
432.24441+
545.3323
615.2711
716.32441+
797.89452+
847.92202+
878.49761+
935.5302
1051.5564
1197.61851+
1269.6129
1299.66951+
1370.70011+
1434.0393
1468.75721+
1532.76332+
1613.30342+
1694.81841+
1775.8717
1856.86862+
1887.9977
1922.9766
y3y4
y5
y6
y8
y9
y10
y11
y12
y13
y14
y16
y17
b8 b18 (++)
b5
[M+H - Hex(9)]2+
[M+H - Hex(8)]2+
b19 (++)
b19
y18
b9
B927 Glycosylated_2-F,7_01_1255.d: +MS2(1507.6690), 65.0eV, 127.6min #29509
0
500
1000
1500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 35 hr
SCO number SCO0472
Precursor ion mass 1507.67395
Charge 3
Retention time 136.5
Hex on peptide 9
e-value 0.00021
Site allocated? N
323.1737
375.2333
447.18301+
505.27561+
536.2393
575.31881+
656.2800
688.40091+
733.4189
778.34261+
863.0543
931.48431+
1041.5163
1072.50292+
1147.5581
1198.6198
1261.5880
1349.5095
1408.64871+
1537.7398
1623.75641+ 1753.8115
1851.9278 1962.8678
y6
y8
y10
y11
y12
y7
y13
y3
y5
y14
y15
B927 Glycosylated_2-F,7_01_1255.d: +MS2(1070.9986), 62.2eV, 73.2min #17115
0
200
400
600
800
1000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 43 hr
SCO number SCO5204
Precursor ion mass 1070.998535
Charge 2
Retention time 73.2
Hex on peptide 1
e-value 0.012
Site allocated? N
317.1453
360.2264
394.1074 454.2144
507.25051+
570.2479 631.2970
703.3619
789.2649
832.40491+
903.43751+
939.4608
1032.49871+
1092.9248
1167.1756
1219.57941+
1257.5384
1290.57651359.4159
1489.46011567.5967
1758.72181816.7298
y8
y10
y7
y5
y4
y9
[M+H - Hex(3)]+B927 Glycosylated_2-F,7_01_1255.d: +MS2(853.3734), 47.7eV, 30.1min #5885
0
500
1000
1500
2000
2500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 43 hr
SCO number SCO4934
Precursor ion mass 853.373413
Charge 2
Elution time 30.1
Hex on peptide 3
e-value 0.0036
Site allocated? N
Time point 43 hr
SCO number SCO3540
Precursor ion mass 910.920837
Charge 2
Retention time 56.4
Hex on peptide 2
e-value 0.019
Site allocated? T2
333.1770
369.1818
497.24561+
567.2772
615.2691
662.8178
769.3328
827.38751+
914.41631+
968.4682
998.53021+
1027.50681+
1056.4437
1091.5063
1135.4777
1169.0321
1227.5876
1256.56351+
1326.6320
1452.6885 1563.7326
1599.6004
1659.5572 1766.7997
1889.6656
y4
y6
y7
y8
y10
y11
b2 + Hex(2)
b8 + Hex(2)
y11 (++)
B927 Glycosylated_2-F,7_01_1255.d: +MS2(911.4224), 50.6eV, 56.4min #12778
200
400
600
800
1000
1200
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
325.11521+
356.70282+
386.24301+
468.2136
554.33211+
641.36271+
673.29681+
712.40241+
799.42891+
856.45391+
963.41821+
1002.47632+
1077.47221+
1165.02382+
1205.52431+
1245.55432+
1275.5507
1398.6995
1452.60951+ 1619.7042
1702.69371771.7776
1828.73591899.5620
1942.8656
y4
y5
y6
b5
b7
b9
b10
b11
b12
b13
b14
b8
y7
y8
y9
y10
b18 (++) + Hex(6)
B927 Glycosylated_2-F,7_01_1255.d: +MS2(992.7609), 50.0eV, 35.9min #7343
0
1000
2000
3000
4000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 43 hr
SCO number SCO3357
Precursor ion mass 992.760925
Charge 3
Retention time 35.9
Hex on peptide 6
e-value 0.013
Site allocated? N
299.1232
388.18401+
489.27051+
604.30041+
658.2689
703.36401+
796.3430
832.41011+
903.44331+
1031.50141+
1073.4802
1118.5515
1219.58401+
1345.6037 1446.7225
y3
y4
y5
y6
y7
[M+H - Hex(2)]+
y10
y11
y8
y9
B933 Keenan 60 min_2-C,5_01_1403.d: +MS2(772.3501), 41.7eV, 27.7min #5353
0
2000
4000
6000
8000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 60 hr
SCO number SCO4934
Precursor ion mass 772.350098
Charge 2
Retention time 27.7
Hex on peptide 2
e-value 0.00019
Site allocated? N
299.1344358.0911
388.1836463.2039
604.29421+
664.3110
703.36501+
748.7485
832.40261+
861.3697
903.44321+
1014.4729
1158.5652
1219.57451+
1363.5698 1544.6834
y4 y5
y6
y7
y8
y9
y10
[M+H - Hex(3)]+
[M+H - Hex]+
b4
B933 Keenan 60 min_2-C,5_01_1403.d: +MS2(853.3753), 47.7eV, 27.4min #5262
0
500
1000
1500
2000
2500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 60 hr
SCO number SCO4934
Precursor ion mass 853.375366
Charge 2
Retention time 27.4
Hex on peptide 3
e-value 0.024
Site allocated? N
293.6770
327.16721+
474.57903+
508.26193+
550.28102+
598.80811+
662.83682+
711.36512+ 761.8945
2+
826.44581+
937.43371+
y10++
y10
y12++
y13++
y5
y5++
b4 + Hex
y8 (0)
y11++
b3
b7
b8 b9
b11
[M+3H-Hex]3+
+MS2(562.2795), 25.5eV, 31.2min #6271
0.0
0.5
1.0
1.5
2.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 60 hr
SCO number SCO4141
Precursor ion mass 562.279541
Charge 3
Retention time 31.2
Hex on peptide 1
e-value 0.04
Site allocated? N
401.2023440.2613
531.26182+ 584.3136
747.38111+
792.7966
845.36491+
915.4312
961.53211+
1060.50971+
1159.58991+
1222.5618
1384.62451+
1460.70781+
1546.67231+
1623.76721+
1784.79821+
y3
y5
y6
y7
y8
y10
y11
y9
b4b5
b7 b9
[M+H]+ - Hex(3)
[M+H]+ + Hex
[M+H]+ + Hex(2)
y10 + Hex
y10 + Hex(2)
y10 + Hex(3)
+MS2(973.9353), 53.7eV, 46.8min #10446
0
2000
4000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 60 hr
SCO number SCO4905
Precursor ion mass 973.935303
Charge 2
Retention time 46.7
Hex on peptide 3
e-value 0.0091
Site allocated? N
372.22651+
443.26331+
530.29271+
568.2423
659.3360
709.3328
788.37711+
824.37902+
860.37531+
916.44031+
973.45711+
1044.50211+
1131.53421+
1202.56561+
1276.52691+
1417.64841486.7403 1570.1965
1648.73031+
1809.79851+
y4
y5
y6
y7
y8
y10
y11
y12
y13 + Hex(2)
b4 (++) + Hex(6)
b5
b6
b8
b10
b12
b14
y13
y14
[M+2H-Hex(8)]2+
b2 (++) + Hex(3)
+MS2(982.0630), 50.0eV, 23.8min #4356
0
1000
2000
3000
4000
5000
6000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
Time point 60 hr
SCO number SCO4739
Precursor ion mass 982.062988
Charge 3
Retention time 23.8
Hex on peptide 8
e-value 0.0041
Site allocated? N
Ion types:
Spectra generated using HCD and ETD fragmentation techniques on the Thermo Orbitrap Fusion Tribrid mass spectrometer
147.78260.14 318.17
387.191+
501.23
592.241+
706.313+
760.333+
863.34920.39
1000.40
1075.452+
1139.992+
1279.581+
1359.581417.64
1559.70 1618.72
1688.741+
1802.781+
c2 + Hex(3)
c5 + Hex(3)
c6 + Hex(3)
c8 + Hex(3)
c9 + Hex(3)
c10 + Hex(3)
c11 + Hex(3)c13 + Hex(3)
y1
y2y3
y5
y8
y11
z2
z5
z6
z7
z8
z9
z11
z13z14
z15
[M+3H]3+
[M+2H]2+
z16 (++) + Hex(3)
+MS, 22.9min #1
0.0
0.2
0.4
0.6
0.8
1.0
5x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO7218
Precursor m/z 759.9905
Charge 3
Retention time 22.9
Scan number 3332
Hex on peptide 3
e-value 0.00066
Site allocated? N
Method ETD_OT
407.221+
508.301+
662.401+
725.481+
863.301+ 949.58
1+
1000.311+
1087.271+
1450.581+
c2 + Hex(3)
c4 + Hex(3)
c5 + Hex(3)
z6c6 + Hex(3)
c9 + Hex(3)c11 + Hex(3)
c14 + Hex(3)y1 y2
y3
y6
z1 z2
z3 z4
z5
z14z16 (++)
z7 (+2)
z10 (+2)
z13 (+2)
[M+4H]4+
c18 (++) + Hex(3)
+MS2(725.48), 49.6min #1
0
1000
2000
3000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO7218
Precursor m/z 724.83
Charge 4
Retention time 49.6
Scan number 11845
Hex on peptide 3
e-value 0.0047
Site allocated? N
Method ETD_IT, ETD_OT
814.89
1177.83
1222.171+
c5 + Hex(6) c10 + Hex(6)c8 + Hex(6)
z12 (+2 ++) + Hex(3)
z9z6z5z4z3z2z1
[M+3H]3+
[M+2H]2+
z13 (++) + Hex(6)
+MS2(814.89), 17.0min #1
0
2
4
6
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3357
Precursor m/z 814.373
Charge 3
Retention time 17
Scan number 2155
Hex on peptide 6
e-value 0.029
Site allocated? N
Method ETD_IT
159.001+
476.291+
523.92
541.441+
812.561+
1025.611+
1083.451+
y1
y2 y3
y4
y6 + Hex
y8 + Hex
z1
z2z3 z8 + Hex
[M+2H]2+
[M+H]+
+MS2(541.44), 39.5min #1
0.0
0.2
0.4
0.6
0.8
4x10
Intens.
200 300 400 500 600 700 800 900 1000 m/z
SCO Number SCO2963
Precursor m/z 541.7381
Charge 2
Retention time 39.5
Scan number 8834
Hex on peptide 1
e-value 0.0065
Site allocated? N
Method ETD_IT
331.191+
514.481+ 585.33
1+
740.161+
871.531+ 947.51
1+
1018.591+
1110.241+
1201.651+
1271.721+
1347.691+
1480.651+
1888.891+
z4 (+2)
z6 z7
[M+3H]3+
[M+2H]2+
z10c8 + Hex
c9 + Hex
z13 (+2)
z14
c12 + Hex
c18 + Hex
c17 + Hex
c16 + Hex
c15 + Hex
+MS2(740.16), 71.6min #1
0.00
0.25
0.50
0.75
1.00
1.25
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4142
Precursor m/z 739.7253
Charge 3
Retention time 71.6
Scan number 32536
Hex on peptide 1
e-value 0.0019
Site allocated? N
Method ETD_IT
272.18 343.22
442.291+
499.31
662.38
694.683+
719.40
834.42
1042.022+
1248.61
1363.631420.65
1584.721640.74
1739.81 1810.84
c10 + Hex
c11 + Hex
c12 + Hex
c13 + Hex
c14 + Hex c15 + Hex
y5
z1
z2z3
z4z6 (+2)
z7
z8
z18 (++) + Hex
z16 (+2) + Hex
[M+3H]3+
[M+2H]2++MS, 46.3min #1
0.0
0.5
1.0
1.5
2.0
2.5
3.0
5x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3184
Precursor m/z 694.3423
Charge 3
Retention time 23.9
Scan number 46.3
Hex on peptide 1
e-value 0.000011
Site allocated? N
Method ETD_IT, ETD_OT
258.101+
346.231+
391.151+
433.231+
462.231+ 520.31
1+
577.411+
664.321+
735.411+
777.581+ 872.39
1+
915.192+
976.521+
1104.631+
1161.601+
1253.761397.69
b3
y1
y2
y3
y4
y5
b2 (0)
y7 y8
y10
y12
y11
y2 (*++)
y6
b5
y9
b4
+MS2(957.64), 17.4min #1
0
500
1000
1500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4142
Precursor m/z 956.9326
Charge 2
Retention time 17.4
Scan number 4208
Hex on peptide 1
e-value 0.048
Site allocated? N
Method HCD_IT
185.151+
245.101+
282.171+
316.211+
344.261+
396.261+
472.321+
498.18
547.311+
618.351+
668.391+
733.451+ 846.43
1+
895.191+
945.601+
1095.451+
1145.511+
1209.531+
1260.721+
1346.65 1416.811+
1518.801+
1558.651+
1735.161811.21
1934.87
b6 (++)
y6
y7
y8
y9 y11
y12
y14
y5
y15
+MS2(1345.98), 136.9min #1
0
100
200
300
400
500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4142
Precursor m/z 1345.3433
Charge 3
Retention time 136.9
Scan number 92043
Hex on peptide 1
Other variable mod Oxidation of M12
e-value 0.014
Site allocated? N
Method HCD_IT
243.161+
311.261+
401.231+
427.261+
468.251+
513.291+ 581.39
1+
640.291+
710.281+
765.481+ 857.54
1+908.80
2+
977.491+
1020.30
1084.402+
1191.731+
1248.681+
1335.87
1446.741+
1547.881+
1600.721676.83
1+
1723.72 1783.83
b3
b4
b5
b6
b13 + Hex
b14 + Hex
b15 + Hex
b7 (*) + Hex
b8 (0) + Hex
b10 (0) + Hex
b12 (++) + Hexy1
y2
y3
y4
y5
y6
y7 y8
y9 y13
y14
y22 (*++) + Hex
b11 + Hex
b26 (++) + Hex
+MS2(1084.40), 92.0min #1
0
200
400
600
800
1000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4142
Precursor m/z 1083.8683
Charge 3
Retention time 92
Scan number 58627
Hex on peptide 1
e-value 0.000036
Site allocated? N
Method HCD_IT
185.071+
248.221+
288.141+
328.221+
441.221+
499.241+
556.361+
603.32
669.301+
722.151+
801.471+
854.591+ 944.83
1+
1029.581+
1100.671+
1151.93 1277.39
1321.781+
1388.791+
1506.821+
1578.901+
1690.99
b2
b3b7
b9 (*) + Hex
b20 (++) + Hex
b22 (* ++) + Hex
y2y3
y4
y5
y7
y10
y13
y14
y15
y16
y9
+MS2(1388.79), 136.0min #1
0
200
400
600
800
1000
1200
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4142
Precursor m/z 1388.3427
Charge 3
Retention time 136
Scan number 91188
Hex on peptide 1
e-value 0.00078
Site allocated? N
Method HCD_IT
175.011+
213.121+ 294.25
1+
399.261+
472.371+ 530.36
1+ 564.391+
614.551+
670.451+
701.072+
733.541+
775.391+
830.401+
876.491+
937.521+
995.281+
1073.421+
1184.53 1303.551+
b2 (0) b8 + Hex
y1y3
y4
y5
y6
y7
y8
y9
y11
b1y8 (++)
+MS2(733.54), 48.7min #1
0
1000
2000
3000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO2156
Precursor m/z 733.3296
Charge 3
Retention time 48.7
Scan number 25242
Hex on peptide 1
e-value 0.0015
Site allocated? N
Method HCD_IT
157.091+
185.081+
272.171+
298.161+ 398.13
1+
469.081+
510.90
567.411+
678.331+703.43
1+
766.171+
818.441+
895.601+
949.401+
974.531+
1024.561+
1064.442+
1121.611+
1193.43
1268.781+
1353.621+
1449.681+
b2
b3
b7 + Hex
b4 (0++) + Hex
b10 (++) + Hex
b11 (*++) + Hex
y1y2
y3y4 y5
y6y7
y8
y9y10
y11
y12
y19 (++)
y20 (++) + Hex
+MS2(895.60), 109.8min #1
0
1000
2000
3000
4000
5000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO5646
Precursor m/z 894.7915
Charge 3
Retention time 109.8
Scan number 72287
Hex on peptide 1
e-value 0.0059
Site allocated? N
Method HCD_IT
169.081+
226.191+
298.131+
385.241+
463.391+
513.261+
613.531+
640.03
692.291+
753.541+
805.491+
832.541+
906.391+
934.14
1032.70
1102.53
1145.591+
1249.66
1443.801+
1506.67 1580.94
y4
y6
y7
y8
y9
y10
y11
y5
y12
y13y14
b9
b3 (0)
+MS2(753.54), 76.4min #1
0
500
1000
1500
2000
2500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO0996
Precursor m/z 753.3517
Charge 3
Retention time 76.4
Scan number 46383
Hex on peptide 2
e-value 0.00082
Site allocated? N
Method HCD_IT
155.021+
185.101+
256.171+
385.211+
442.111+
577.301+
660.441+
692.311+
743.221+
805.371+
847.012+
882.351+
906.451+
957.491+
1103.551+
1250.711+
1307.601+
1437.751+
1506.691+
y1y4
y5
y6
y7
y8
y10
y12
y13
+MS2(1211.06), 74.7min #1
0
500
1000
1500
2000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO0996
Precursor m/z 1210.5497
Charge 2
Retention time 74.7
Scan number 45042
Hex on peptide 3
e-value 0.021
Site allocated? N
Method HCD_IT
175.131+
242.091+
288.141+
372.291+
431.271+
532.471+
583.401+
638.441+
683.351+
709.681+
760.101+
824.671+
874.161+
924.702+
960.211+
1024.322+
1119.59
1189.661+
1300.581+
y1
y2y3 y5
y7
b1
b2
b9 + Hex
b5 (*) + Hex
b3
y18
[M+2H - Hex]2+
y10 (++)
y12 (++)
y14 (++)
y15 (++)
y16 (++)
y17 (++)
y18 (++) + Hex
y19 (++) + Hex
+MS2(737.44), 35.6min #1
0.0
0.2
0.4
0.6
0.8
1.0
4x10
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3184
Precursor m/z 737.0407
Charge 3
Retention time 35.6
Scan number 16323
Hex on peptide 1
e-value 0.0014
Site allocated? N
Method HCD_IT
129.091+
175.081+
217.051+
262.221+
288.091+
344.23
474.352+
524.991+
577.351+
674.441+
783.171+
826.521+
890.421+
998.531+
1047.541+
1144.531+
1231.721+
1331.67 1416.521488.58 1585.47
b11 + Hex
y5
y6
y8
y9
y10
y11y3 (0)
b2
b3
+MS2(890.42), 54.1min #1
0
200
400
600
800
1000
Intens.
200 400 600 800 1000 1200 1400 1600 m/z
SCO Number SCO4013
Precursor m/z 890.4368
Charge 2
Retention time 54.1
Scan number 29320
Hex on peptide 1
e-value 0.023
Site allocated? N
Method HCD_IT
175.021+
227.121+
302.131+
331.171+
373.131+
402.141+
488.351+
529.321+
623.301+
724.01
786.192+
899.621+
935.491+
996.581+
1083.501+
1199.601+
1270.651+
1342.92
1417.681+
1473.571+
1570.881+
1699.77
1796.911+
y1
y3
y5
y7
y8
y9
y10
y11
y13
y14
y15
y16
b3
b4
y14 (++)+MS2(1179.90), 109.3min #1
0
200
400
600
800
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4885
Precursor m/z 1180.5522
Charge 2
Retention time 109.3
Scan number 71923
Hex on peptide 1
e-value 0.00000081
Site allocated? N
Method HCD_IT
175.091+ 244.13
1+
276.151+
355.191+
429.191+
461.331+
526.361+
589.331+
688.411+
723.671+
801.451+
857.331+
900.581+
957.551+
995.691+
1035.481+
1070.561+
1170.491+
1286.781+
1428.571+
1641.861+
b3
b5
y9
y1
y2 y4
y5
y6 y7
y8
y10 y12 y13
+MS2(995.69), 98.4min #1
0
500
1000
1500
2000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3044
Precursor m/z 995.119
Charge 3
Retention time 98.4
Scan number 63503
Hex on peptide 3
e-value 0.000032
Site allocated? N
Method HCD_IT
200.061+
244.121+
354.191+
412.181+
454.311+
483.301+
527.261+
555.361+
625.371+
668.461+
726.411+
769.591+ 840.51
1+
872.611+
941.581+
1012.591+
1083.671+
1112.571+
1212.651+
1254.50
1313.771+
1441.631+
1529.43
1584.83
b3
y2 y4
y5
y6
y7 y8
y9
y10
y11
y12
y13
y14
+MS2(954.66), 57.4min #1
0
500
1000
1500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3540
Precursor m/z 954.489
Charge 2
Retention time 57.4
Scan number 31744
Hex on peptide 2
e-value 0.0002
Site allocated? N
Method HCD_IT
143.091+
200.091+
244.131+
302.121+
327.211+
355.021+
454.281+
483.311+
555.441+
598.49669.26
1+
712.821+
769.261+ 840.57
1+
888.511+
941.631+
1013.591+
1084.701+
1121.481175.77
1213.751+
1314.791+
1372.49
1441.911+
1560.82 1646.78 1747.54 1866.01
y2y4
y5
y6
y7 y8
y9y10
y11
y12
y13y14
b3
+MS2(1036.36), 50.7min #1
0
100
200
300
400
500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3540
Precursor m/z 1035.5149
Charge 2
Retention time 50.7
Scan number 26747
Hex on peptide 3
e-value 0.000022
Site allocated? N
Method HCD_IT
141.131+
169.081+
226.111+
275.131+
298.161+
386.171+
411.251+
498.371+
567.341+
640.301+
663.091+
730.451+
758.431+
783.921+
827.391+
911.531+
990.83
1027.531+
1156.491+
1227.551+
1265.571+
1325.661+
1371.77
1497.741+y2
y3
y4
y5
y6
y7
y8
y9
y10
y11
+MS2(911.53), 46.3min #1
0
250
500
750
1000
1250
1500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3540
Precursor m/z 910.9199
Charge 2
Retention time 46.3
Scan number 23511
Hex on peptide 2
e-value 0.00039
Site allocated? N
Method HCD_IT
169.131+
197.111+
244.25
301.181+
341.091+
416.241+443.23
2+ 499.291+ 534.88
1+588.34
1+
659.481+
689.351+
758.401+788.42
1+
885.451+
984.471+ 1055.53
1+
1086.461+
1120.812+
1185.501+ 1256.62
1+
1355.681+
y2 y3y4
b5y7
y8
y9
y10b1
b2
b4
b7b8
b9
b10
b11 b12
b13
+MS2(909.73), 51.0min #1
0
2000
4000
6000
8000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO2096
Precursor m/z 909.4205
Charge 3
Retention time 51
Scan number 26945
Hex on peptide 3
e-value 0.0059
Site allocated? N
Method HCD_IT
159.05204.15
288.06357.10
414.291+
460.25504.231+ 555.33
1+
644.361+
715.361+
758.601+
814.391+
843.431+
887.241+
947.70
1027.34
1067.571+
1138.751+
1225.68
1334.621440.78
1561.80
y2y5
y7
y8
y9
y11
y12
y13
y14
y15
b5b3
+MS2(1027.34), 32.4min #1
0
200
400
600
800
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO2035
Precursor m/z 1026.959
Charge 2
Retention time 32.4
Scan number 14239
Hex on peptide 2
e-value 0.0066
Site allocated? N
Method HCD_IT
175.101+
244.221+
315.141+
372.321+
473.371+
560.441+
659.351+
769.741+
871.381+
935.591+ 985.64
1+
1044.521+
1098.59 1258.711+
y2
y4y5
y6
y7
y8
y9
y10
b1
+MS2(769.74), 53.3min #1
0
1000
2000
3000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3848
Precursor m/z 769.7249
Charge 3
Retention time 53.3
Scan number 28662
Hex on peptide 1
e-value 0.00047
Site allocated? N
Method HCD_IT
155.141+
200.131+
244.181+
270.151+
327.211+
385.241+
437.361+ 473.26
1+
560.421+
659.401+
702.031+ 758.42
1+
823.531+
856.301+ 985.61
1+
1064.661+
1125.47 1187.731+ 1272.73 1401.74
1+
y2
y5
y6
y7
y8
y10
y9
y13 y14
b1
+MS2(823.53), 52.2min #1
0
1000
2000
3000
4000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3848
Precursor m/z 823.7414
Charge 3
Retention time 52.2
Scan number 27876
Hex on peptide 2
e-value 0.00053
Site allocated? N
Method HCD_IT
136.081+
189.011+
242.121+
343.201+
409.241+
519.251+
597.311+
655.521+
799.361+
856.371+
913.851+
969.401+
1040.451+
1110.35
1139.591+
1210.561+
1277.36
1370.911+
1487.851+
1572.23
y3y5
y6
y7
y8
y9
y10
y11
y14b5
y12
[M+3H - Hex2]3+
b3 (0)
+MS2(1105.79), 91.9min #1
0
500
1000
1500
2000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4130
Precursor m/z 1109.5142
Charge 4
Retention time 91.9
Scan number 58511
Hex on peptide 2
e-value 0.00036
Site allocated? N
Method HCD_IT
173.121+
268.161+
297.161+
327.161+
372.191+
396.221+
460.281+
499.241+
559.281+
600.172+
663.401+
708.531+
754.521+
810.451+
857.741+
903.451+
949.331+
1063.461+
1144.761+
1176.581+
1208.92 1289.781+
1437.671+
1536.632+
1646.78 1834.061+
y1
y3
y4
y5
y6
y9
y10
y11
y12y13
+MS2(920.52), 132.6min #1
0
500
1000
1500
2000
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO4905
Precursor m/z 919.7954
Charge 3
Retention time 132.6
Scan number 4335
Hex on peptide 3
e-value 0.024
Site allocated? N
Method HCD_IT
129.191+
175.12
226.29272.15 359.06
1+
527.281+
582.521+
607.26
631.631+
652.81
754.691+
782.461+
813.541+
835.72
877.251+
922.07
954.601+
1041.47
1089.15 1141.701+
1215.62
1302.60
1350.54
1445.89 1504.43 1607.04
y2
y5
y8
y10
y11
y13
y14
y15
y9 (0)
+MS2(877.25), 20.4min #1
0
100
200
300
400
Intens.
200 400 600 800 1000 1200 1400 1600 m/z
SCO Number SCO4548
Precursor m/z 877.4079
Charge 2
Retention time 20.4
Scan number 6204
Hex on peptide 3
e-value 0.00042
Site allocated? N
Method HCD_IT
200.261+
228.161+
301.071+
371.161+
439.251+
479.041+
568.892+
612.191+
676.361+
789.371+
894.501+
933.611+
985.541+
1038.481+
1135.581+
1223.671+
1309.531+
1505.761+
y1
y2
y3
y4
y5
y6
y7
y8y9
y10
y11
y12
y14
b1
b2b5
b7
b8
b9
y10 (++)
+MS2(933.61), 50.1min #1
0
500
1000
1500
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3357
Precursor m/z 933.099
Charge 3
Retention time 50.1
Scan number 26320
Hex on peptide 3
e-value 0.0023
Site allocated? N
Method HCD_IT
129.13
175.021+
240.181+
368.192+
425.301+
451.111+
496.401+
522.281+
600.071+
631.22
696.341+
747.332+
811.401+
882.351+
939.561+
995.501+
1066.531+
1115.36
1167.531+
1215.29
1259.631+
1295.651+
1331.69
1382.63 1519.73
y1 y2
y5
y6
y7
y8
y9
y10
y11
y12
b2 (0)
b3 (0)
+MS2(939.56), 45.6min #1
0
200
400
600
Intens.
200 400 600 800 1000 1200 1400 1600 1800 m/z
SCO Number SCO3891
Precursor m/z 938.9214
Charge 2
Retention time 45.6
Scan number 22941
Hex on peptide 2
e-value 0.00091
Site allocated? N
Method HCD_IT