SSFL ANALYTICAL CHEMISTRY€¦ · SSFL ANALYTICAL CHEMISTRY Rockwell International, Rocketdyne Div. (818) 586-5827 D/392 SS21 TO: Rocketdyne Environmental Protection Requester: Bonnie

SSFL ANALYTICAL CHEMISTRYRockwell International , Rocketdyne Div .

(818) 586-5827 D/392 SS2 1

TO : Rocketdyne Environmental Protection

Requester : Bonnie Burns

Dept/Group : 543-000 MAIL: JA16 PHONE: 392-5325

Log Number

9208044 7

REPORT DATE : 09/10/92

SAMPLE INFORMATION

Sample Descrption : Soil, West of Concrete Pit, Sodium Disposal Facility

Requested Analysis : Metals and pH

Sampler : B. Burns Sampler ID#: 92-886-75A Sampled : 08/21/92 @ 6 :35 :00

ANALYTE RESULT UNITS MDL METHOD/SOURCE

Antimony ND mg/kg 3.2 6010/SW 846

Arsenic ND mg/kg 5.3 60101SW 846

Barium 97 mg/kg 0 .2 6010/SW 846

Beryllium ND mg/kg 0.03 6010/SW 846

Cadmium 1 .5 mg/kg 0 -4 6010/SW 846

Cadmium , WET Extract 0.040 mg /L 0.04 6010/SW 846

Chromium 18 mg /kg 0.7 6010/SW 846

Cobalt 9.9 mg/kg 0.7 6010/SW 846

Copper 14 mg/kg 0.6 6010/SW 846

Lead 4 .9 mg/kg 4 .2 6010/SW 846

Mercury 0 .79 mg/kg 0.02 7471/SW 846

Mercury, WET Extract ND mg/L 0.002 7470/SW 846

Molybdenum ND mg/kg 0 .8 6010/SW 846

Nickel 13 mg/kg 1 .5 6010/SW 846

pH 7.4 pH units 0 .01 9045/SW 846

Selenium ND mg/kg 7.5 6010/SW 846

Silver ND mg/kg 0 .7 6010/SW 846

Thallium ND mg/kg 4 .0 6010/SW 846

Vanadium 38 mg /kg 0 .8 6010/SW 846

Vanadium , WET Extract 1.4 mg/L 0.08 6010/SW 846

WET Extraction 09/01 /92 DNA DNA Title 22

Zinc 48 mg/kg 0.2 6010/SW 846

------------------------------------- -------------------- -------- ------ -------------------------

SPECIFICATION : Title 22

SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances , Sec. 66699

COMMENTS : Revised report to contain STLC data .

APPROVED : SIGNED :

Rocketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistr y

iI I I I uBNA00380578

HDMSe00436611

SSFL ANALYTICAL CHEMISTRYRockwell International , Rocketdyne Div.

(818) 586-5827 D/392 5521

TO: Rocket dyne Environmental ProtectionRequester : Bonnie Burns

Dept/ Group : 543-000 MAIL : JA16 PHONE: 392-5325

SAMPLE INFORMATION =

Sample Descrption : Bin 15063 , Sodium Disposal FacilityRequested Analysis : Metals and pH

Lag Number

92080373

REPORT DATE : 09/10/9 2

Sampler : B. Burns Sampler ID#: 92-886-65B Sampled: 08 / 18/92 @ 6:45 :00

ANALYTE RESULT UNITS MDL METHOD /SOURCE


Arsenic ND mg/kg 5 .3 6010/SW 846Barium 110 mg /kg 0 .2 6010/SW 846

Barium, WET Extract 4.3 mg /L 0.02 6010/SW 846

Beryllium ND mg/kg 0 .03 6010/SW 846

Cadmium 1 .6 mg/kg 0.4 6010/SW 846

Cadmium , WET Extract ND mg /L 0.04 6010/SW 846

Chromium 24 mg/kg 0.7 6010/SW 846

Cobalt 10 mg/kg 0.7 6010/SW 846

Copper 17 mg/kg 0.6 6010/SW 846

Lead ND mg/kg 4.2 6010/SW 846

Mercury 19 mg/kg 0.02 7471/SW 846

Mercury, WET Extract 0.0029 mg/L 0 .002 7470/SW 846

Molybdenum NO mg/kg 0 .8 6010/SW 846

Nickel 16 mg /kg 1 .5 6010/SW 846

pH 8.7 pH units DNA 9045/SW 846


Silver ND mg /kg 0 .7 6010/SW 846

Thallium NO mg /kg 4 .0 6010/SW 846

Vanadium 42 mg/kg 0 .8 6010/SW 846



Zinc 81 mg/kg 0 .2 6010/SW 84 6

------------------------------------- -------------------- -------- ------ -------------------------

SPECIFICATION: Title 22

SPECIAL NOTES: Inorganic Persistent and Bioaccumulative Toxic Substances , Sec . 66699

COMMENTS : Revised report to contain STLC data.

APPROVED : K~ UL Sl`GPED :Rocketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistry

I I I IIBNA00380579

HDMSe00436612

SSFL ANALYTICAL CHEMISTRYRockwell International , Rocketdyne Div .

(818) 586-5827 D1392 SS2 1



Dept/ Group : 543-000 MAIL: JA26 PHONE: 392-5325

Log Number92080368

REPORT DATE : 09/10/9 2

SAMPLE INFORMATION

Sample Descrption : Bin 15018 , Sodium Disposal Facility -


Sampler : B. Burns Sampler ID# : 92-886-66B Sampled : 08/18 /92 @ 6 :15 :00



Arsenic ND mg/kg 5 .3 6010/SW 846

Barium 110 mg/kg 0 .2 6010/SW 846

Barium, WET Extract 4.9 mg/L 0.02 6010/SW 846


Cadmium 1 .4 mg/kg 0 .4 6010/SW 846

Cadmium, WET Extract ND mg/L 0 . 04 6010/SW 846

Chromium 26 mg/kg 0 . 7 6010/SW 846

Cobalt 9 .9 mg/kg 0.7 6010/SW 846

Copper 16 mg/kg 0 .6 6010/SW 84 6

Lead ND mg/kg 4 .2 6010/SW 84 6

Mercury 13 mg/kg 0 .02 7471/SW 846

Mercury, WET Extract 0.0029 mg/L 0.002 7470/SW 846


Nickel 15 mg/kg 1 .5 6010/SW 846

pH 8 .6 pH units DNA 9045/SW 846

Selenium ND mg/k9 7.5 6010/SW 846

Silver ND mg/kg 0 . 7 6010/SW 846

Thallium ND mg/kg 4 . 0 6010/SW 846

Vanadium 41 mg/kg 0 .8 6010/SW 84 6

Vanadium , WET Extract 0 .45 mg/L 0 .08 6010/SW 84 6

WET Extraction 09/01/92 DNA DNA Title 2 2

Zinc 92 mg/kg 0.2 6010/SW 846

------------------------------------- -------------------- -------- ------ ------ -- -----------------


SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances , Sec . 66699


APPROVED :- SIGNED :

Rocketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistry

I I I I I I I

BNA00380580HDMSe00436613

SSFL ANALYTICAL CHEMISTR YRockwell International , Rocketdyne Div .

(818) 586-5827 D/392 5S2 1



Dept/Group : 543-000 MAIL : JA16 PHONE : .392-5325 REPORT DATE: 09/10/92

• SAMPLE INFORMATION

Sample Descrption : Bin 15082 , Sodium Disposal Facility


Sampler : B . Burns Sampler IDS: 92-886-68B ampled : 08/18/92 @ 5 :30 :00


-------------------- ------------------------ -

Antimony ND mg/ kg 3 .2 6010/SW 846

Arsenic ND mg/kg 5.3 6010/SW 846

Barium 100 mg/kg 0.2 6010/SW 84 6

Barium, WET Extract 4 .5 mg/L 0.02 6010/SW 84 6


Cadmium 1 .4 mg/kg 0 .4 6010/SW 846

Cadmium, WET Extract NO mg/L 0 .04 6010/SW 846


Cobalt 9.3 mg/kg 0.7 6010/SW 846

Copper 15 mg/kg 0.6 6010/SW 846


Mercury 13 mg/kg 0 .02 7471/SW 84 6

Mercury, WET Extract ND mg/L 0 .002 7470/SW 846


Nickel 14 mg/kg 1 .5 6010/SW 846



Silver ND mg/kg 0.7 6010/SW 846

ThaIIiun ND mg/kg 4.0 6010/SW 846

Vanadiun 37 mg/kg 0 .8 6010/SW 846

Vanadium, WET Extract 0 .44 mg/L 0 .08 6010/SW 846

WET Extraction 09101/92 DNA DNA Title 2 2

Zinc 94 mg/kg 0 .2 6010/SW 846

------------------------------------- -------------------- ------- ------ -------------------------


SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances , Sec . 6669 9

COMMENTS : Revised to contain STLC data .

APPROVED :

Rocketdyne SSFL Analytical ChemistrySIGNED :

Log Number

92080363

Rocketdyne SSFL Analytical Chemistry

I i I IIBNA00380581

HDMSe00436614

SSFL ANALYTICAL CHEMISTRYRockwell International, Rocketdyne Div .(818) 586-5827 D/392 SS21

TO : Rocketdyne Environmental ProtectionRequester: Bonnie Burns

Dept/Group : 543-000 MAIL : JA 1 6 PHONE: 392-5325

Log Number

92080358


SAMPLE INFORMATION

Sample Descrption: Bin

Requested Analysis : Met

Sampler : B . Burns

15041, Sodium Dispos

als and pH

Sampler ID# :

al Facility

92-886-72B Sampled : 08/18/92 @ 4 :55 :00

ANALYTE RESULT UNITS MDL METHOD/SOURC E



Barium 120 mg/kg 0 .2 6010/SW 846

Barium, WET Extract 4 .3 mg/L 0 .02 6010/SW 846


Cadmium 1 .4 mg/kg 0 .4 6010/SW 846

Cadmium, WET Extract ND mg/L 0 .04 6010/SW 846

Ch romi un 24 mg/kg 0.7 6010/SW 846

Cobalt 10 mg/kg 0.7 6010/SW 846

Copper 16 mg/kg 0.6 6010/SW 84 6

Lead ND mg/kg 4.2 6010/SW 84 6

Mercury 12 mg/kg 0.02 7471/SW 846

Mercury, WET Extract 0 .0044 mg/L 0.002 7470/SW 84 6

Molybdenum ND mg/kg 0.8 6010/SW 846

Nickel 15 mg/kg 1 .5 6010/SW 846




Thallium ND mg/kg 4.0 6010/SW 84 6

Vanadium 40 mg/kg 0.8 6010/SW 84 6

Vanadium, WET Extract 0 .45 mg/L 0.08 6010/SW 84 6


Zinc 88 mg/kg 0.2 6010/SW 846

------------------------------------- -------------------- -------- ------ -------------------------




APPROVED : G ~ .


SI N D:


I I I I I IBNA00380582

HDMSe00436615

SSFL ANALYTICAL CHEMISTR YRockwell International , Rocketdyne Div.

( 818) 586-5827 D/392 SS2 1

TO: Rocketdyne Environmental Protection


Dept/Group : 543-000 MAIL : JA16 PHONE : 392-5325

Log Number

92080353


SAMPLE INFORMATION

Sample Descrption : Bin 15065 , Sodium Disposal Facility _Requested Analysis : Metals and pHSampler: B . Burns Sampler IDI: 92-886-67B Sampled : 08/18/ 92 @ 7 :35 :00

ANALYTE RESULT UNITS MDL METHOD /SOURCE

Antimony ND mg /kg 3.2 6010/SW 846

Arsenic ND mg/kg 5.3 6010/SW 846

Barium 130 mg/kg 0.2 6010/SW 846

Barium , WET Extract 4.3 mg/L 0.02 6010/SW 846


Cadmium 1.3 mg/kg 0.4 6010/SW 846



Cobalt 11 mg/kg 0.7 6010/SW 846

Copper 19 mg/kg 0 .6 6010/SW 846


Mercury 10 mg/kg 0.02 7471/SW 846


Molybdenum ND mg /kg 0 .3 6010/SW 846

Nickel 18 mg/kg 1.5 6010/SW 846



Silver ND mg/kg 0 .7 6010/SW 846

Thallium ND mg/kg 4 .0 6010/SW 846


Vanadium , WET Extract 0.36 mg /L 0.08 6010/SW 846

WET Extraction 09/01/92 DNA DNA Title 22

Zinc 70 mg/kg 0.2 6010/SW 846


SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances , Sec. 66699


APPROVED : GNSIGNED : CRocketdyne SSFL Analytical Chemistry Rccketdyne SSFL Analytical Chemistry

iI I I IBNA00380583

HDMSe00436616

SSFL ANALYTICAL CHEMISTR YRockwell International , Rocketdyne Div .( 818) 586-5827 D/392 SS2 1



Dept/Group : 543-000 MAIL : JA16 PHONE : 392-5325

Log Number

9208034 4


Sample Descrption : Bin 15067 ,

uested AnalRe sis : Metals and

SAMPLE INFORMATION

Sodium Disposal Facility

Hq y

Sampler : B . Burns

p

Sampler ID#: 92-886-73B Sampled : 08/17 /92 @ 9 :35 :00

ANALYTE RESULT UNITS MDL METHOD /SOURC E

Antimony 5 .5 mg /kg 3 .2 6010/SW 846


Barium 120 mg/kg 0.2 6010/SW 846

Barium, WET Extract 5 .0 mg/L 0.02 6010/SW 846


Cadmium 1 .3 mg/kg 0.4 6010/SW 846

Cadmium, WET Extract ND mg/L 0.04 6010/SW 846

Chromium 24 mg/kg 0 .7 6010/SW 84 6

Cobalt 10 mg/kg 0 .7 6010/SW 84 6

Copper 17 mg/kg 0 . 6 6010/SW 846

Lead ND mg /kg 4 .2 6010/SW 846

Mercury 5 .1 mg/kg 0.02 7471/SW 846

Mercury, WET Extract 0 .0033 mg/L 0.002 7470/SW 846


Nickel 17 mg/kg 1 .5 6010/SW 846


Selenium ND mg /kg 7.5 6010/SW 84 6

Silver ND mg/kg 0.7 6010/SW 84 6

Thallium ND mg/kg 4.0 6010/SW 846



WET Extraction 09/01/92 DMA DNA Title 22

Zinc 65 mg /kg 0.2 6010/SW 84 6

------------------------------------- --------------------




APPROVED : SIGNED :

Rocketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistry

I I I I I I I

BNA00380584HDMSe00436617

SSFL ANALYTICAL CHEMISTRYRockwell International , Rocketdyne Div.(818) 586-5827 D/392 SS21

TO: Rocketdyne Environmental Protection

Requester: Bonnie Burns

Dept/Group : 543-000 MAIL : TA16 PHONE: 392-5325

Log Number

92080339


SAMPLE INFORMATION



Sampler : B. Burns Sampler ID#: 92-886 -71B Sampled : 08/17 /92 @ 10 :13 :0 0


Antimony ND mg /kg 3.2 6010/SW 846

Arsenic ND mg /kg 5.3 6010/SW 846

Barium 110 mg/kg 0 .2 6010/SW 846

Barium, WET Extract 4 .9 mg /L 0 .02 6010/SW 846


Cadmiun 1 .4 mg/kg 0 .4 6010/SW 846

Cadmiun, WET Extract ND mg/L 0 .04 6010/SW 846

Chromiun 26 mg/kg 0.7 6010/SW 846

Cobalt 10 mg /kg 0.7 6010/SW 846

Copper 18 mg/kg 0.6 6010/SW 846

Lead ND mg /kg 4 .2 6010/SW 846

Mercury 15 mg/kg 0 .02 7471/SW 846


Molybdenum ND mg /kg 0 .8 6010/SW 846

Nickel 17 mg/kg 1 .5 6010/SW 846

pH 8.6 pH units DNA 9045/SW 84 6

Selenium ND mg/kg 7 . 5 6010/SW 84 6

Silver ND mg /kg 0.7 6010/SW 846

ThaLlium ND mg/kg 4.0 6010/SW 846


Vanadium, WET Extract 0 .44 mg / L 0 .08 6010/SW 846


Zinc 73 mg/kg 0 .2 6010/SW 84 6


SPECIAL NOTES : Inorganic Persistent and Bioaccumulative Toxic Substances, Sec . 66699


APPROVED :

Ro ketdyne SSFL Analytical Chemistry Rocketdyne SSFL Analytical Chemistry

I

U O (l r._-~

i II f IBNA00380585

HDMSe00436618

SSFL ANALYTICAL CHEMISTRYRockwell International, Rocketdyne Div .

(818) 586-5827 D/392 SS2 1


Requester : Bonnie Burn s

Dept/Group: 543-000 MAIL : JA16 PHONE: 392-5325

Log Number

92080334


SAMPLE INFORMATION

Sample Descrption : Bin 15030 , Sodium Disposal FacilityRequested Analysis : Metals and pHSampler : B. Burns Sampler ID#: 92-886-70B Sampled: 08/17/92 @ 8 :50 :00

ANALYTE RESULT UNITS MDL METHOD/SOURC E

Antimony 4.3 mg/kg 3.2 6010/SW 846


Barium 97 mg/kg 0.2 6010/SW 846

BeryLLium ND mg/kg 0.03 6010/SW 846

Cadmium 1 .5 mg/kg 0.4 6010/SW 846


Chromium 26 mg/kg 0 .7 6010/SW 846

Cobalt 8 .5 mg/kg 0 .7 6010/SW 846

Copper 19 mg/kg 0 .6 6010/SW 846

Lead ND mg/kg 4 .2 6010/SW 846

Mercury 1 .7 mg/kg 0.02 7471/SW 846



Nickel 21 mg/kg 1 .5 6010/SW 846

Nickel, WET Extract 0.35 mg/L 0 .15 6010/SW 846

pH 8 .3 pH units DNA 9045/SW 846




Vanadium 34 mg/kg 0.8 6010/SW 846

Vanadium, WET Extract 0.33 mg/L 0.8 6010/SW 846

WET Extraction 09/01/92 DNA DNA Title 22

Zinc 72 mg/kg 0 .2 6010/SW 846




APPROVED : ----Rocketdyne SSFL Analytical Chemistry

4~ c . . ,SIGNED :


I I I I I I LII I

BNA00380586HDMSe00436619

SSFL ANALYTICAL CHEMISTRYRockwell International, Rocketdyne Div .(818) 586-5827 D/392 SS21



Dept/Group : 543-000 MAIL: JA16 PHONE: 392-5325

Log Number

92080329


SAMPLE INFORMATION



Sampler : B. Burns Sampler ID# : 92-886-69B Sampled: 08/17 /92 @ 7 :45 :00

ANALNTE RESULT UNITS MDL METHOD/ SOURCE

Antimony ND mg/kg 3.2 6010/SW 84 6

Arsenic ND mg/kg 5.3 60101SW 846

Barium 180 mg/kg 0 .2 6010/SW 846

Barium, WET Extract 4.5 mg/L 0 .02 6010/SW 846

Beryllium ND mg /kg 0 .03 6010/SW 846

Cadmiun 1 .2 mg /kg 0 .4 6010/SW 846


Chromium 21 mg /kg 0.7 6010;SW 846

Cobalt 9 . 7 mg/kg 0 . 7 6010/SW 846

Copper 16 mg /kg 0.6 6010/SW 846

Lead ND mg/kg 4 .2 6010/SW 846

Mercury 0 .67 mg/kg 0 .02 7471/SW 846



Nickel 13 mg/kg 1 .5 6010/SW 846

pH 9.1 pH Units DNA 9045/SW 846


Silver ND mg /kg 0 .7 6010/SW 846


Vanadium 31 mg/kg 0.8 6010/SW 846

Vanadium, WET Extract 0.22 mg/L 0 .08 6010/SW 846


Zinc 61 mg/kg 0 .2 6010/SW 846

------------------------------------- -------------------- -------- ------ -------------------------




APPROVED : 4 LL-Rocket'yne SSFL Analytical Chemistry

0-SIGNED :


II I I I I i IBNA00380587

HDMSe00436620

Documents

SSFL ANALYTICAL CHEMISTRY€¦ · SSFL ANALYTICAL CHEMISTRY Rockwell International, Rocketdyne Div. (818) 586-5827 D/392 SS21 TO: Rocketdyne Environmental Protection Requester: Bonnie