12
ORIGINAL ARTICLE Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture Younes Bagheri Fauziah Ahmad Mohd Ashraf Mohamad Ismail Received: 1 November 2012 / Accepted: 7 March 2013 Ó RILEM 2013 Abstract This study presents results of geotechnical investigations on treated silty sand soil with cement, lime and rice husk ash (CLR) and cement-lime (CL) admixture. Consolidated undrained triaxial test and unconfined compressive test were performed to esti- mate the potential of CLR and CL. The study investigates the influence of the amount of CLR%, main effective stress and curing days on soil strength, deformation, post peak behavior and brittleness. The percentages of the additives of CLR and CL varied from 2.5 to 12.5 % by dry weight of the soil with dry densities of 14.5 kN/m 3 and the curing times of 3, 7, 28 and 60 days were examined. From the results, the stress–strain response is strongly influenced by the CLR contents and effective confining pressure. Strength and post peak strength of the CLR–soil are greatly improved by an increase in binder content. An increase of the effective cohesion c 0 (kPa) and effective friction U 0 (degree) is observed with increas- ing the CLR content, consistently. Brittle behavior observed at lower confining pressures and high CLR content. For both CLR and CL additives, linear trend was observed for variation of the q u (kPa) with respect to the additives percentages. RHA was also found to be effective in increasing the shear strength of CLR–soil mixture. Keywords Silty Sand soil Stabilization Rice husk ash Shear strength Abbreviations CLR Cement, lime and RHA content CL Cement and lime content UCS Unconfined compressive strength CU Consolidated undrained triaxial compression test PI Plasticity index and RHA Rice husk ash List of symbols D r Relative density G s Specific gravity G sCLR Specific gravity of CLR I B Brittleness index d 50 Main particle diameter q p Peak deviator stress q r Residual deviator stress q u Unconfined compressive strength R 2 Coefficient of determination c 0 Effective cohesion U 0 Friction angle r 0 Effective principal stress Y. Bagheri F. Ahmad (&) M. A. M. Ismail School of Civil Engineering, USM Engineering Campus, University Sains Malaysia (USM), 14300 Nibong Tebal, Penang, Malaysia e-mail: [email protected] Y. Bagheri e-mail: [email protected] M. A. M. Ismail e-mail: [email protected] Materials and Structures DOI 10.1617/s11527-013-0044-2

Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

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Page 1: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

ORIGINAL ARTICLE

Strength and mechanical behavior of soil–cement–lime–ricehusk ash (soil–CLR) mixture

Younes Bagheri • Fauziah Ahmad •

Mohd Ashraf Mohamad Ismail

Received: 1 November 2012 / Accepted: 7 March 2013

� RILEM 2013

Abstract This study presents results of geotechnical

investigations on treated silty sand soil with cement,

lime and rice husk ash (CLR) and cement-lime (CL)

admixture. Consolidated undrained triaxial test and

unconfined compressive test were performed to esti-

mate the potential of CLR and CL. The study

investigates the influence of the amount of CLR%,

main effective stress and curing days on soil strength,

deformation, post peak behavior and brittleness. The

percentages of the additives of CLR and CL varied

from 2.5 to 12.5 % by dry weight of the soil with dry

densities of 14.5 kN/m3 and the curing times of 3, 7,

28 and 60 days were examined. From the results, the

stress–strain response is strongly influenced by the

CLR contents and effective confining pressure.

Strength and post peak strength of the CLR–soil are

greatly improved by an increase in binder content. An

increase of the effective cohesion c0 (kPa) and

effective friction U0 (degree) is observed with increas-

ing the CLR content, consistently. Brittle behavior

observed at lower confining pressures and high CLR

content. For both CLR and CL additives, linear trend

was observed for variation of the qu (kPa) with respect

to the additives percentages. RHA was also found to be

effective in increasing the shear strength of CLR–soil

mixture.

Keywords Silty � Sand soil � Stabilization � Rice

husk ash � Shear strength

Abbreviations

CLR Cement, lime and RHA content

CL Cement and lime content

UCS Unconfined compressive strength

CU Consolidated undrained triaxial compression

test

PI Plasticity index and

RHA Rice husk ash

List of symbols

Dr Relative density

Gs Specific gravity

GsCLR Specific gravity of CLR

IB Brittleness index

d50 Main particle diameter

qp Peak deviator stress

qr Residual deviator stress

qu Unconfined compressive strength

R2 Coefficient of determination

c0 Effective cohesion

U0 Friction angle

r0 Effective principal stress

Y. Bagheri � F. Ahmad (&) � M. A. M. Ismail

School of Civil Engineering, USM Engineering Campus,

University Sains Malaysia (USM), 14300 Nibong Tebal,

Penang, Malaysia

e-mail: [email protected]

Y. Bagheri

e-mail: [email protected]

M. A. M. Ismail

e-mail: [email protected]

Materials and Structures

DOI 10.1617/s11527-013-0044-2

Page 2: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

s Shear stress at failure and

cd Dry unit weight

1 Introduction

Soil has been used as a base material in various

engineering infrastructures such as retaining walls,

pavements, water ways, irrigation and drainage net-

works, protective barrier and embankments. Particular

attention has been turn to the mechanical and chemical

stabilization of soil [1–3] in order to increase the soil

strength (s). However, the economic aspects of soil

stabilization projects limit the application of mechan-

ical approach. Regarding to the chemical stabilization

viewpoint, several additives such as cement, lime,

polymers and fly ash have been utilized. Cement and

lime are the most common additives amongst the

mentioned materials that produce positive effect on

soil performance [1, 4–8]. Cement and lime signifi-

cantly decrease the swell potential, plasticity index

(PI), increase the modulus of elasticity (Es), durability

index (Id) and shear strength of soils (s) [5, 9]. In recent

years, many investigations have been conducted on the

solution of environmental and economic problems due

to chemical stabilizers applications. Using the waste

natural material is one of the most effective approaches

in soil improvement as a green method. Agricultural

activities provide various waste natural materials such

as bran and husk. Paddy farms are composited of

5–8 % of bran, 72 % of rice and 20–22 % of husk on an

average by weight, that cause to generate rice husk ash

(RHA) as an alternative additive to eliminate the

chemical additives problems [10–12]. RHA contains

high amount of silica (87–97 % of SiO2) and thus can

be used as a pozzolanic material in lime and cement

mixture. During last few decades, different investiga-

tions on RHA performance in soil stabilization have

shown that RHA can be considered as a pozzolan

promising material with cement or lime as it can

improve the soil engineering properties [12–16] and

also reduce cement and lime consumption in soil

stabilization and concrete technology as well [13, 17].

Using RHA as a supplementary cementitious material

leads to a reduction in greenhouse gases (carbon

dioxide) emissions fallowing by the cement and lime

production [18–20]. Besides, it is figured out that

carbon remained in the ash is trapped in the soil or

concrete and won’t be distributed in atmosphere which

is environmentally so momentous [18].

The different amount of chemical additives and

curing time are also significant variable parameters

which render different reactions for treated soils [21–23].

By consideration on past investigations, it was

found that no treated soil with the combination of

cement–lime and RHA (CLR) has been utilized yet.

The present experimental work investigates the defor-

mability properties and shear strength of soil–CLR. In

addition, the effect of RHA was investigated on soil

strength.

2 Experimental works

2.1 Combined mixture preparation

According to the Unified Soil Classification System

(USCS), the studied soil was classified as silty sand

(SM) [24] with specific gravity (Gs) of 2.55. The

investigated grain-size distribution is plotted in Fig. 1.

The soil sample has 11.9 % gravel (D [ 2 mm),

37.7 % medium sand (0.425 \ D \ 2 mm), 14 % fine

sand (0.075 \ D \ 0.0425 mm), 28.6 % silt (0.002 \D \ 0.075 mm), and 7.8 % clay (D \ 0.002 mm),

with the main particle diameter d50 of 0.42 mm. The

geotechnical properties of the studied soil are summa-

rized in Table 1. Furthermore, in Table 2 the miner-

alogical composition of soil is presented according to

the soil analysis methods [25]. This soil consists of

*88 % silica and sesquioxides of iron and aluminum.

Accordance to Table 2, this soil is classified as

lateritic, because, the red or reddish brown, weathered

soils contain of silica to sesquioxide ratios between

1.33 and 2.0 are classified as laterite or lateritic soils

and those with ratios more than 2.0 are named

nonlateritic. Moreover, this soil is acidic (pH \ 5)

based on the soil pH classification [26].

The ordinary Portland cement that was used has a

specific gravity (Gs) of 3.05. Hydrated high calcium

lime [Ca(OH)2] was used with a Gs of 2.14. Lime and

cement materials were passed through sieve No. 40

before usage.

Rice husk was burned in the gas furnace to produce

ash (RHA) at 500 �C for a period of 120 min with high

pozzolanicity, maximum fineness and silica quantity

(&90 %) [12, 27]. The specific gravity of RHA is

1.42. To measure pozzolanic activity of RHA the

Materials and Structures

Page 3: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

strength activity index method was utilized, according

to ASTM C 311-11a [28]. This index is determined by

comparing the compressive strengths of cement mor-

tars with 15 % pozzolan and without it. According to

the standard, the pozzolanic activity index of the

sample which contains pozzolan should be more than

75 % after 28 days of curing. In this research, the

pozzolanic activity index of RHA after 7 and 28 days

of curing was estimated 79 and 88 % respectively.

In this work, the behavior of a combined additive of

cement, lime and RHA materials known as CLR were

investigated. To quantify the behavior of soil–CLR

mixture, the factors of deformability, soil strength

parameters (U0 and c0) and brittleness index (IB) were

investigated.

To find the best mixture of cement, lime and RHA in

combination with soil, unconfined compression strength

test (UCS) was employed for different percentage of the

studied mixtures. Tests were conducted on similar

conditions which is cd = 17 kN/m3, CLR by 10 %

weight and 28 days curing time. The mixtures with

higher values of cement show a considerable value of

qu (kPa) but resulted in negative economical and

environmental issues (Table 1). Therefore, the com-

bination of 25 % cement, 50 % lime and 25 % RHA as

the best mixture was selected for this investigation

(Table 1). The properties of the studied soil–CLR

combination are summarized in Table 1.

2.2 Experimental design

Consolidated undrained (CU) triaxial tests and UCS

were carried out to evaluate the mechanical behavior

Fig. 1 Grain size distribution for the studied soil

Table 1 Summary of the properties of the investigated soil, additives and mixture

Soil properties Quantity Additives properties Quantity/

qualitative factor

Mixture percentage;

CLR (A/B/C)aqu

(kPa)

Specific gravity 2.55 Specific gravity 2.17 (15/50/35) 673

Sand (%) 51.70 Cement (% by weight) 25 (25/50/25) 1014

Silt (%) 28.60 Lime (% by weight) 50 (35/50/15) 1582

Clay (%) 7.80 RHA (% by weight) 25 (25/40/35) 1005

USCS classification SM Fineness passing 45 lm (%) 76 (35/40/25) 1649

pH 12.43 (35/30/35) 1898

Liquid limit (%) 48.05 Color Gray (15/60/25) 457

Plastic limit (%) 31.50 (25/60/15) 828

PI (%) 16.53

Optimum moisture (%) 16.30

Maximum dry density (kN/m3) 17.52

Minimum dry density (kN/m3) 10.34

a The signs of A, B and C show the percentage of the cement, lime and RHA, respectively

Table 2 Chemical and mineralogical of the soil

Properties Value

Silica (SiO2) 57.1 (%)

Alumina (Al2O3) 21.6 (%)

Iron oxide (Fe2O3) 9.70 (%)

Potash (K2O) 0.13 (%)

Magnesia (MgO) 0.16 (%)

Calcium oxide (CaO) 0.12 (%)

Silica: sesquioxide ratio 1.82

pH 4.76

Materials and Structures

Page 4: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

of CLR–soil and CL–soil. The performance of the

additives percentage, main effective stress and curing

days on soil strength, deformation, post peak behavior

and brittleness were investigated. The experimental

test program is summarized in Table 3.

2.3 CU triaxial test

The specimens were prepared by mixing oven-dry soil

and optimum water content of 16.3 %, with 2.5, 5, 7.5,

10 and 12.5 % of CLR thoroughly until a uniform color

was observed. The diameter and height of the samples

prepared for the triaxial test were 70 and 140 mm

respectively. Each sample was immediately com-

pacted (based on standard method [29]) after mixing

in three layers of 47 mm thickness in a rigid cylindrical

mold to the dry density of 14.5 kN/m3 (i.e., a relative

density of Dr = 70 %). The mixing and compaction

were completed within an hour to avoid large amount

of water losses. After compaction, the specimens were

kept in the mold for about 12 h. Finally, the specimens

were then removed from the mold and immediately

wrapped in rubber membrane and cured in a covered

container with a wet sponge in humid room at 26 �C

� 2 �C to avoid significant changes in moisture

content until testing at 3, 7, 28 and 60 days. The

sample was weighted prior to the test in order to

control the moisture of the sample. It was found that

the moisture lost is\1 % compared with the reading

recorded during preparation day. The similar samples

prepared for this investigation were kept in the same

condition (moisture content, density and curing time)

to minimized effects on the test results.

In order to evaluate the soil stress–strain and strength

behavior, a series of CU triaxial tests with pore-pressure

measurement were carried out according to the standard

[30] on untreated and treated soil specimens with

various percentages of CLR content. Before starting the

test, freshly de-aired water is drawn into the triaxial cell

and the tests were fully controlled by data acquisi-

tion. During the saturation process, the samples were

fully saturated by applying a cell pressure and a back

water pressure to achieve a B value of at least 0.95. The

complete saturation process for each sample requires

about 2–3 days. Then, the samples were consoli-

dated under a specific isotropic confining pressure.

The consolidation stage is completed when the excess

pore-water pressure had dissipated completely and the

water volume changes remain constant. Finally, when

consolidation condition is achieved, the specimen was

loaded vertically in strain controlled condition with a

low axial strain rate of 0.02 mm/min under the confining

pressure of 50, 100 and 250 kPa. Shearing is complete

when the axial strain reached 25 % or the deviator stress

reached a constant value. In this investigation, the area

corrections and membrane adopt the suggestions pro-

posed by La Rochelle et al. [31].

2.4 Unconfined compression test

First, dried soil was passed through the sieve # 6. The

largest soil particle diameter must be smaller than 1/6

mold diameter [32]. Test specimens were obtained by

mixing oven-dry soil and the determined quantities of

CLR as long as the mixture acquired a uniform color

and consistency. The amount of additives for each

Table 3 Experimental

program summaryVariable Consolidated undrained

triaxial test

Unconfined

compression test

Initial mean effective stress 50, 100, 250 kPa 0 kPa

CLR content (%) 2.5, 5, 7.5, 10, 12.5 5, 7.5, 10, 12.5

Curing time with CLR (days) 3, 7, 28, 60 7, 28, 60

CL content (%) 10, 12.5 5, 7.5, 10, 12.5

Curing time with CL (days) 3, 7, 28 7, 28, 60

Degree of saturation (%) – [95

Rate of strain (mm/min) 0.02 1

Soil type SM SM

Relative density (%) 70 70

Water content (%) 16.3 16.3

Standard method ASTM D4767 ASTM D2166

Materials and Structures

Page 5: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

specimen was determined based on the weight of dry

soil. The tests were carried out on soils treated with 5,

7.5, 10 and 12.5 % of CLR by weight. Each specimen

used for the determination of UCS was compacted in 3

layers with 25 mm thickness in a rigid cylindrical mold

to a target dry density (14.5 kN/m3) with optimum

water content of the untreated soil (16.3 %). The height

and diameter of the samples prepared for the UCS test

were 76 and 38 mm respectively. After completion of

the compaction, specimens were immediately cured in

a covered container with a wet sponge in humid room at

26 �C � 2 �C to prevent significant changes in mois-

ture content until testing at 7, 28 and 60 days.

Unconfined compression test was performed on

treated SM samples with CLR to evaluate the influ-

ences on CLR content and curing time on the strength

of each specimen. The compressive strength test was

carried out using an automatic loading machine with

axial loading speed at a rate of 1 mm/min and

maximum capacity of 10 kN. During UCS tests,

failure compressive load and deviator stress were

recorded. For each case, three specimens were tested

and each sample with the same condition should not be

different from the mean strength by more than 10 %

[33].

The same analogy with soil–CLR preparation was

used for preparing the soil–cement and lime mixture

(soil–CL) samples to investigate the RHA effect on

soil properties.

3 Observations and discussions

3.1 CU triaxial compression test

The variation of deviator stress–strain and pore-water

pressure with respect to axial strain for both untreated

(CLR = 0 %) and treated specimens with 10 % CLR

after 28 days curing is plotted in Fig. 2. The data are

derived from CU triaxial compression test.

Figure 2a, c indicates that the deviator stress–strain

and pore-water pressure behaviors for untreated spec-

imens echo the ductile material acting manner. Both

deviator stress (kPa) and pore-water pressure (kPa)

Fig. 2 The variation of

pairs [deviator stress (kPa)-

strain (%)] and [pore–water

pressure (kPa)-strain (%)]

a Soil deviator stress (kPa)–

strain (%) with 0 % CLR,

b soil deviator stress (kPa)–

strain (%) with 10 % CLR

after 28 days curing, c soil

pore–water pressure (kPa)–

strain (%) with 0 % CLR,

d soil pore–water pressure

(kPa)–strain (%) with 10 %

CLR after 28 days

Materials and Structures

Page 6: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

significantly increased at failure by addition of CLR

and curing time. The improvement in shear strength for

CLR addition is due to the development of more

cementation in the stabilized matrix. Furthermore, the

increase of ductility for treated specimens will results

in confining pressure redundancy since denser speci-

mens will emerge due to high confining pressure.

Higher brittle response of the specimens were observed

at lower confining pressure whereas deviator stress was

significantly reduced after peaking deviator stress as

shown in Fig. 2b. Although post peak strength is

reduced, nevertheless, this factor is always being found

more than untreated specimens.

Figure 3 shows the variation of pairs stress–strain

and pore-water pressure-strain for different CLR con-

tents (%) at a constant confining pressure (= 100 kPa)

after 28 days curing.

The similar tendencies have been observed for

other confining pressures (= 50 and 250 kPa) but is not

shown for the sake of conciseness. These results

provide evidence for soil strength enhancement and

pore-water pressure growth due to strong cementation

effects caused by the increment of CLR content. It is

observed that the increment of pore water pressure

(kPa) is related to the development of linkage amongst

the particles created by CLR. The observed trend

includes two different behaviors of rapidly increasing

and gradually decreasing followed by leveling off at

constant values. The maximum value of pore-water

pressure (kPa) depends on the amount of confining

pressure. The maximum values of pore-water pressure

(kPa) for 10 % CLR contents were found to be

approximately two times more than the untreated

specimens. Table 4 presents the deviator stress values

at failure level for CLR stabilized specimens after 3, 7,

28 and 60 days curing. The considerable effect of

different confining pressure on deviator stress can also

be seen in Table 4.

The deviator stresses at failure increases as the CLR

and curing days, from 3 to 28 days increase. For

60 days curing, a distinct increase in the deviator stress

for 10 % CLR content was observed. However, the

decrement of deviator stress when CLR content varied

from 10 to 12.5 % for 60 days curing is discernable.

This attributes to the pH of CLR–soil mixture. The

highest chemical activation of lime with soil has a

value of pH = 12.3–12.4 [34], because silica has high

level of solubility in the mixture. Figure 4 illustrates

the variation of pH with respect to CLR content in

different days of curing where the proper value of pH

can be observed for value of CLR = 10 %.

Figure 5a, b presents the Mohr–Coulomb failure

criterion (Mohr envelope) for the studied combined

soil–CLRs at 28 days curing and different curing time.

The effective angle of internal friction U0 (degree) and

effective cohesion c0 (kPa) from CU triaxial tests were

estimated by drawing the Mohr–Coulomb failure

envelopes tangentially to the Mohr circles at different

confining pressures.

It can be concluded that, the effective cohesion c0

(kPa) increases as the CLR content increases (Fig. 6a).

However, the trends for different curing days were

similar but in different growth rates. For curing days of

7 and 28, the data levels to a constant value of effective

cohesion about 100 kPa. It can be seen that, the

observed increasing behavior of cohesion against CLR

is a result of bonding improvement amongst the

mixture particles.

Figure 6b shows the variation of friction angle U0

(degree) with respect to CLR content. For curing time

Fig. 3 The variation of

pairs [deviator stress(kPa)–

strain(%)] and [pore–water

pressure(kPa)–strain(%)] in

the triaxial CU test under

100 kPa confining stress on

untreated and treated

Materials and Structures

Page 7: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

of 28 days, a relatively rapid increase was observed in

the variation of friction angle for 0 \ CLR \ 10 and

then stabilized at around 34� (Fig. 6b). For curing of 3

and 7 days with values of CLR \ 10, the variation of

Friction angle is independent from CLR variation

(Fig. 6b). A distinctive increase in friction angle can

be found for CLR [ 10 %. This behavior can be

attributed to the pH effect.

The brittleness index IB is defined as the following

equation [35]:

IB ¼qp � qr

qp

ð1Þ

where, qp, and qr are the peak deviator stress and

residual deviator stress, respectively. The variation of

IB with respect to confining pressures for the studied

CLR (%) and curing times is shown in Fig. 7. The

variation of IB are similar for curing times of 3 and

7 days, whereas larger values were observed for 28

and 60 curing days (Fig. 7c, d). This increment is

significant in the lower studied percentages of CLR

(2.5 and 5 %) (Fig. 7c).

The ductility or rigidity of the specimens can be

assessed by brittleness index. If the IB of specimen is

close to zero this means that the specimen indicates a

ductile behavior. The ultimate post peak strength in all

tests varies within a narrow range from 140 to 210 kPa

compared to the peak strength (gray line, Fig. 3a) and

thus the brittleness increases as a function of peak

strength. As a conclusion, the increase of brittleness

does not have an effect on the total strength and

functionality of the treated soil.

To evaluate the performance of RHA on soil

strength, the variation of pairs (stress–strain) and (poreTa

ble

4D

evia

tor

stre

ssat

fail

ure

lev

el

Mix

ture

Cu

rin

gp

erio

d(d

ays)

3d

ays

curi

ng

7d

ays

curi

ng

28

day

scu

rin

g6

0d

ays

curi

ng

r 3=

50

(kP

a)

r 3=

10

0

(kP

a)

r 3=

25

0

(kP

a)

r 3=

50

(kP

a)

r3

=1

00

(kP

a)

r3

=2

50

(kP

a)

r3

=5

0

(kP

a)

r 3=

10

0

(kP

a)

r 3=

25

0

(kP

a)

r 3=

50

(kP

a)

r3

=1

00

(kP

a)

r3

=2

50

(kP

a)

So

il–

2.5

%C

LR

95

.81

39

.02

81

.71

11

.51

56

.83

06

.11

37

.11

99

.73

85

.5–

––

So

il–

5%

CL

R1

21

.31

63

.42

96

.81

59

.92

08

.53

56

.82

32

.63

12

.14

59

.7–

––

So

il–

7.5

%C

LR

17

8.6

24

0.4

35

1.1

26

1.0

32

0.9

46

5.4

37

1.4

46

9.2

59

5.2

––

So

il–

10

%C

LR

23

6.2

33

4.4

46

7.0

34

0.5

42

6.5

55

8.1

43

6.2

56

0.9

72

7.5

49

9.5

62

4.8

77

7.9

So

il–

12

.5%

CL

R2

42

.93

51

.24

96

.53

61

.44

66

.56

01

.34

25

.95

34

.97

21

.54

79

.25

91

.47

41

.6Fig. 4 The variation of the pH with respect to CLR content in

different days curing

Materials and Structures

Page 8: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

Fig. 5 Variation of the shear strength s (kPa) with respect to the r0 (kPa), a for all the studied combined soil–CLR samples at 28 days

curing, b in different curing days at CLR = 10 %

Fig. 6 Variation of soil

strength parameters with

respect to the CLR

percentage content in

different curing times, 3, 7

and 28 days, a effective

cohesion c0 (kPa),

b effective friction U0

(degree)

Fig. 7 Variation of the

brittleness index (IB) for

treated soils with respect to

the CLRs contents at

different confining pressures

and curing times, a 3 curing

days, b 7 curing days, c 28

curing days, d 60 curing

days

Materials and Structures

Page 9: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

water pressure–strain) for CLR and CL treated spec-

imens in 50 kPA confining pressure, after 28 days

curing, are plotted in Fig. 8. It can be stated that, the

deviator stress values at failure and maximum pore

water pressure are higher when CLR is used with the

combination of cement and lime.

The soil strength parameters for soil–CLR and soil–

CL treated are presented in Table 5. The results

demonstrate that the effective friction angle changes

from 25.85� to 30.66� for soil–CL and 26.75–34.22�for soil–CLR (depending on the additives percentage

and curing time). The effective cohesion rising rate of

soil–CLR treated is higher than the CL-treated soil.

The effective cohesion of specimens treated with

12.5 % CLR and cured for 7 days were estimated at

102 kPa was compared with the specimens treated

with CL at the same condition and it was found that,

the effective cohesion improved *30 % (Table 5).

Thus, it is clearly observed the more efficiency of CLR

on soil treatment compared to soil treated by CL.

3.2 UCS

Figure 9a, b present the effect of the studied additives

(CLR and CL) on UCS (kPa) factor. Results of the

UCS tests show noticeable achievement of higher qu

(kPa) by adding RHA to the samples. For both CLR

and CL, a linear trend was observed for variation of qu

with respect to percentages of the investigated addi-

tives. Overall, a higher growth rates can be found for

linear trends as the curing time increases in both CLR

and CL. However, for CLR the qu increases more

rapidly compared to CL samples with respect to the

percentage of additives.

Strength of the treated soil increased due to the

adding of CLR as presented in Fig. 9. In order to explain

the prescribed response of treated soil using CLR, high

amount of silica in RHA (90 %) was considered.

Addition of RHA to lime–soil blended with water

increases the pozzolanic reaction due to the reaction

between Ca(OH)2 and SiO2 [9, 36]. This eventually

leads to the formation of cementations bonds through

the production of cement material including calcium-

silicate-hydrates. Subsequently, cement helps to com-

pound the finer particles together to form larger

aggregates in CLR–SM blends [3, 16]. Besides, as

shown in Fig. 9 and comparing the results of CLR and

CL in different curing times on soil strength (qu),

another important point is distinguished which is

utilizing RHA to reduce cement and lime consumption.

For instance, average strength of 60 days cured samples

with 12.5 % CL is approximately equal with those with

7.5 % CLR and 60 days curing (qu = 516 kPa)

(Fig. 9). It means by adding RHA, which is a waste

material and a cause of environmental pollution, there

has been a 60 % reduction in cement and lime

consumption and it is both environmentally and

economically important and reasonable.

4 Conclusions

This research highlights the responses of soil stabi-

lized by a new combined additive (CLR) in terms

strength behavior, deformability, post peak and brit-

tleness. Based on the results, the following remarks

can be concluded:

• The untreated soil presents a ductile behavior. The

peak strength increases by the addition of CLR

content. The post peak strength of treated speci-

mens was found to be more than the untreated

specimens.

Fig. 8 Comparison results

of triaxial CU test under

50 kPa confining stress on

both treated samples of CLR

and CL: a deviator stress,

b change in pore-water

pressure

Materials and Structures

Page 10: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

Ta

ble

5T

he

soil

stre

ng

thp

aram

eter

sfo

rso

il–

CL

Ran

dso

il–

CL

trea

ted

fro

mth

etr

iax

ial

CU

test

Tes

t

iden

tifi

cati

on

s

(CL

R-A

/B/C

)

Dev

iato

rst

ress

atfa

ilu

re

(kN

/m2)

Eff

ecti

ve

Fri

ctio

nan

gle

(deg

rees

)

Eff

ecti

ve

coh

esio

n

(kN

/m2)

Ult

imat

e

dev

iato

r

stre

ss(k

N/m

2)

Tes

t

iden

tifi

cati

on

s

(CL

-A/B

/C)

Dev

iato

rst

ress

atfa

ilu

re

(kN

/m2)

Eff

ecti

ve

fric

tio

n

ang

le(d

egre

es)

Eff

ecti

ve

coh

esio

n

(kN

/m2)

Ult

imat

e

dev

iato

r

stre

ss(k

N/m

2)

(CL

R-1

0/5

0/3

)2

36

.22

6.7

56

5.4

89

0.0

6(C

L-1

0/5

0/3

)2

10

.52

7.1

44

8.3

77

1.4

2

(CL

R-1

0/1

00

/3)

33

4.4

26

.75

65

.48

11

4.8

3(C

L-1

0/1

00

/3)

30

8.3

27

.14

48

.37

11

1.5

7

(CL

R-1

0/2

50

/3)

46

7.0

26

.75

65

.48

23

3.3

9(C

L-1

0/2

50

/3)

46

5.5

27

.14

48

.37

28

5.7

1

(CL

R-1

0/5

0/7

)3

40

.52

7.3

89

8.0

11

33

.18

(CL

-10

/50

/7)

31

5.2

25

.64

92

.68

22

7.7

2

(CL

R-1

0/1

00

/7)

42

6.5

27

.38

98

.01

16

9.1

6(C

L-1

0/1

00

/7)

40

2.6

25

.64

92

.68

23

8.4

1

(CL

R-1

0/2

50

/7)

55

8.1

27

.38

98

.01

28

4.9

9(C

L-1

0/2

50

/7)

51

0.9

25

.64

92

.68

35

2.6

0

(CL

R-1

0/5

0/2

8)

43

6.2

34

.22

10

8.8

01

01

.60

(CL

-10

/50

/28

)4

07

.13

0.6

69

9.7

01

49

.57

(CL

R-1

0/1

00

/28

)5

60

.93

4.2

21

08

.80

18

5.1

1(C

L-1

0/1

00

/28

)4

69

.63

0.6

69

9.7

02

77

.07

(CL

R-1

0/2

50

/28

)7

27

.53

4.2

21

08

.80

29

5.6

2(C

L-1

0/2

50

/28

)6

93

.33

0.6

69

9.7

04

34

.61

(CL

R-1

2.5

/50

/3)

24

2.9

27

.43

78

.02

96

.55

(CL

-12

.5/5

0/3

)2

28

.22

6.4

06

6.6

81

66

.44

(CL

R-1

2.5

/10

0/3

)3

51

.22

7.4

37

8.0

21

49

.93

(CL

-12

.5/1

00

/3)

29

4.8

26

.40

66

.68

20

2.7

8

(CL

R-1

2.5

/25

0/3

)4

96

.52

7.4

37

8.0

22

68

.90

(CL

-12

.5/2

50

/3)

41

8.5

26

.40

66

.68

30

0.2

3

(CL

R-1

2.5

/50

/7)

36

1.4

29

.68

10

2.0

01

50

.83

(CL

-12

.5/5

0/7

)3

20

.92

5.8

57

8.2

51

88

.61

(CL

R-1

2.5

/10

0/7

)4

66

.52

9.6

81

02

.00

16

2.8

9(C

L-1

2.5

/10

0/7

)4

05

.12

5.8

57

8.2

52

38

.64

(CL

R-1

2.5

/25

0/7

)6

01

.32

9.6

81

02

.00

26

3.1

4(C

L-1

2.5

/25

0/7

)4

96

.22

5.8

57

8.2

53

49

.25

(CL

R-1

2.5

/50

/28

)4

25

.93

4.0

29

7.8

31

67

.35

(CL

-12

.5/5

0/2

8)

37

3.2

28

.52

89

.60

16

7.2

1

(CL

R-(

12

.5/1

00

/28

)5

34

.93

4.0

29

7.8

31

96

.73

(CL

-12

.5/1

00

/28

)4

08

.62

8.5

28

9.6

02

63

.14

(CL

R-1

2.5

/25

0/2

8)

72

1.5

34

.02

97

.83

33

1.2

4(C

L-1

2.5

/25

0/2

8)

55

1.8

28

.52

89

.60

29

3.7

3

CL

Ro

rC

L-A

/B/C

:A

per

cen

to

fad

dit

ives

(CL

Ro

rC

L),

Bco

nfi

nin

gp

ress

ure

ink

N/m

2,

Cd

ays

of

curi

ng

Materials and Structures

Page 11: Strength and mechanical behavior of soil–cement–lime–rice husk ash (soil–CLR) mixture

• The increase of CLR additive percentage and

curing time substantially increases the deviator

stress peak of the soil up to 10 % of the CLR

content. The deviator stress when CLR content

changes from 10 to 12.5 % for 60 days curing is

discernable. This attributes to the pH of the soil–

CLR mixture.

• The effective cohesion c0 (kPa) and effective

friction angle U0 (degree) increase when the CLR

content (%) increases.

• Brittle behavior is observed at a lower confining

pressures and higher CLR content (%).

• A linear trend is observed for the variation of both

CLR and CL additives percentages with respect to

qu (kPa).

• Results show that the RHA significantly increases

the shear strength of soil–CLR mixture and

reduces the cost and environmental impact of

cement and lime additives.

Acknowledgments The authors are grateful to Universiti Sains

Malaysia (USM) for their financial support and geotechnical

laboratory technicians for their assistance. The authors are also

grateful to the anonymous reviewers of the paper for their valuable

comments that improve the original manuscript.

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