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Analytical Chemistry: Volume 81, Issue 22 (ACS Publications)

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Table of Contents

Larger Cover

November 15, 2009

Volume 81, Issue 22

Pages 9203-9530

In this issue:

● Articles

● Technical Notes

About the Cover:

The cover shows a differential interference contrast (DIC) image of a cell with multiple layers of peptide-functionalized gold

nanospheres inside. At the bottom is a side view of the cell. The article is by Wei Sun, Gufeng Wang, Ning Fang, and Edward S.

Yeung of Iowa State University and Ames Laboratory, U.S. Department of Energy. View the article.

indicates the article is freely available through sponsorship by the author or related funding agency. More about this program.

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Wavelength-Dependent Differential Interference Contrast Microscopy: Selectively Imaging

Nanoparticle Probes in Live Cells

Wei Sun, Gufeng Wang, Ning Fang and Edward S. Yeung

pp 9203–9208

Publication Date (Web): September 29, 2009 (Article)

DOI: 10.1021/ac901623b

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Figure 1 of 6

Inverse-Fluorescence Correlation Spectroscopy

Stefan Wennmalm, Per Thyberg, Lei Xu and Jerker Widengren

pp 9209–9215

Publication Date (Web): October 27, 2009 (Article)

DOI: 10.1021/ac9010205

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Figure 1 of 7

Multistep Approach for the Structural Identification of Biotransformation Products of

Iodinated X-ray Contrast Media by Liquid Chromatography/Hybrid Triple Quadrupole Linear

Ion Trap Mass Spectrometry and 1H and 13C Nuclear Magnetic Resonance

Jennifer Lynne Kormos, Manoj Schulz, Manfred Wagner and Thomas A. Ternes

pp 9216–9224


DOI: 10.1021/ac9011717


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Figure 1 of 4

Strategy of Accelerated Method Development for High-Throughput Bioanalytical Assays

Using Ultra High-Performance Liquid Chromatography Coupled with Mass Spectrometry

Guowen Liu, Heidi M. Snapp, Qin C. Ji and Mark E. Arnold

pp 9225–9232


DOI: 10.1021/ac901316w


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Figure 1 of 7

Recyclable Molecular Trapping and SERS Detection in Silver-Loaded Agarose Gels with

Dynamic Hot Spots

Paula Aldeanueva-Potel, Erwan Faoucher, Ram n A. Alvarez-Puebla, Luis M. Liz-Marz n and Mathias Brust

pp 9233–9238


DOI: 10.1021/ac901333p

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Figure 1 of 6

A Noninvasive Thin Film Sensor for Monitoring Oxygen Tension during in Vitro Cell Culture

Peter C. Thomas, Michael Halter, Alessandro Tona, Srinivasa R. Raghavan, Anne L. Plant and Samuel P. Forry

pp 9239–9246


DOI: 10.1021/ac9013379


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Figure 1 of 6

Monitoring of Biochemical Changes through the C6 Gliomas Progression and Invasion by

Fourier Transform Infrared (FTIR) Imaging

Abdelilah Beljebbar, Sylvain Dukic, Nadia Amharref, Salima Bellefqih and Michel Manfait

pp 9247–9256


DOI: 10.1021/ac901464v

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Figure 1 of 5

Dual Labeling of Metabolites for Metabolome Analysis (DLEMMA): A New Approach for the

Identification and Relative Quantification of Metabolites by Means of Dual Isotope Labeling

and Liquid Chromatography−Mass Spectrometry


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Liron Feldberg, Ilya Venger, Sergey Malitsky, Ilana Rogachev and Asaph Aharoni

pp 9257–9266


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Figure 1 of 7

Fast Determination of Mitochondria Electrophoretic Mobility Using Micro Free-Flow

Electrophoresis

Vratislav Kostal, Bryan R. Fonslow, Edgar A. Arriaga and Michael T. Bowser

pp 9267–9273


DOI: 10.1021/ac901508x


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Figure 1 of 6

Thin-Layer Chromatography/Laser-Induced Acoustic Desorption/Electrospray Ionization

Mass Spectrometry

Sy-Chyi Cheng, Min-Zong Huang and Jentaie Shiea

pp 9274–9281


DOI: 10.1021/ac901514c

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Figure 1 of 7

Identification of Codon-Specific Serine to Asparagine Mistranslation in Recombinant

Monoclonal Antibodies by High-Resolution Mass Spectrometry

X. Christopher Yu, Oleg V. Borisov, Melissa Alvarez, David A. Michels, Yajun Jennifer Wang and Victor Ling

pp 9282–9290


DOI: 10.1021/ac901541h

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Figure 1 of 5

Electrochemical, Photoelectrochemical, and Surface Plasmon Resonance Detection of

Cocaine Using Supramolecular Aptamer Complexes and Metallic or Semiconductor

Nanoparticles

Eyal Golub, Gilad Pelossof, Ronit Freeman, Hong Zhang and Itamar Willner

pp 9291–9298


DOI: 10.1021/ac901551q


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http://pubs.acs.org/doi/abs/10.1021/ac901541hhttp://pubs.acs.org/doi/abs/10.1021/ac901541hhttp://pubs.acs.org/doi/abs/10.1021/ac901541hhttp://pubs.acs.org/doi/full/10.1021/ac901541hhttp://pubs.acs.org/doi/full/10.1021/ac901541hhttp://pubs.acs.org/doi/pdf/10.1021/ac901541hhttp://pubs.acs.org/doi/pdf/10.1021/ac901541hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901541hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901541hhttp://pubs.acs.org/doi/abs/10.1021/ac901551qhttp://pubs.acs.org/doi/abs/10.1021/ac901551qhttp://pubs.acs.org/doi/abs/10.1021/ac901551qhttp://pubs.acs.org/doi/abs/10.1021/ac901551qhttp://pubs.acs.org/doi/suppl/10.1021/ac901551qhttp://pubs.acs.org/doi/full/10.1021/ac901551qhttp://pubs.acs.org/doi/full/10.1021/ac901551qhttp://pubs.acs.org/doi/pdf/10.1021/ac901551qhttp://pubs.acs.org/doi/pdf/10.1021/ac901551qhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901551qhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901551q

Label-Free Electrochemiluminescent Aptasensor with Attomolar Mass Detection Limits

Based on a Ru(phen)32+-Double-Strand DNA Composite Film Electrode

Xue-Bo Yin, You-Ying Xin and Yue Zhao

pp 9299–9305


DOI: 10.1021/ac901609g


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Figure 1 of 8

Detection of Endogenous Dopamine Changes in Drosophila melanogaster Using Fast-Scan

Cyclic Voltammetry

Trisha L. Vickrey, Barry Condron and B. Jill Venton

pp 9306–9313


DOI: 10.1021/ac901638z

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Figure 1 of 6

Biomonitoring of Organophosphorus Agent Exposure by Reactivation of Cholinesterase

Enzyme Based on Carbon Nanotube-Enhanced Flow-Injection Amperometric Detection

Dan Du, Jun Wang, Jordan N. Smith, Charles Timchalk and Yuehe Lin

Abstract

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pp 9314–9320


DOI: 10.1021/ac901673a



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Figure 1 of 8

A Universal Strategy for Development of a Method for Absolute Quantification of Therapeutic

Monoclonal Antibodies in Biological Matrices Using Differential Dimethyl Labeling Coupled

with Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry

Chengjie Ji, Nalini Sadagopan, Yizhong Zhang and Christopher Lepsy

pp 9321–9328


DOI: 10.1021/ac901800f

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Figure 1 of 7

Effective Protocol for Database Similarity Searching of Heteronuclear Single Quantum

Coherence Spectra

Gregory K. Pierens, Mehdi Mobli and Viktor Vegh

pp 9329–9335


DOI: 10.1021/ac901616t


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Figure 1 of 5

Use of Single Particle Aerosol Mass Spectrometry for the Automated Nondestructive

Identification of Drugs in Multicomponent Samples

Audrey N. Martin, George R. Farquar, Paul T. Steele, A. Daniel Jones and Matthias Frank

pp 9336–9342


DOI: 10.1021/ac901208h


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Figure 1 of 6

Multiple Reaction Monitoring Cubed for Protein Quantification at the Low Nanogram/Milliliter

Level in Nondepleted Human Serum

T. Fortin, A. Salvador, J. P. Charrier, C. Lenz, F. Bettsworth, X. Lacoux, G. Choquet-Kastylevsky and J. Lemoine

pp 9343–9352


DOI: 10.1021/ac901447h


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Figure 1 of 4

Chiral Sensing Using a Complementary Metal−Oxide Semiconductor-Integrated Three- Abstract



http://pubs.acs.org/doi/abs/10.1021/ac901208hhttp://pubs.acs.org/doi/abs/10.1021/ac901208hhttp://pubs.acs.org/doi/abs/10.1021/ac901208hhttp://pubs.acs.org/doi/suppl/10.1021/ac901208hhttp://pubs.acs.org/doi/full/10.1021/ac901208hhttp://pubs.acs.org/doi/full/10.1021/ac901208hhttp://pubs.acs.org/doi/pdf/10.1021/ac901208hhttp://pubs.acs.org/doi/pdf/10.1021/ac901208hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901208hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901208hhttp://pubs.acs.org/doi/abs/10.1021/ac901447hhttp://pubs.acs.org/doi/abs/10.1021/ac901447hhttp://pubs.acs.org/doi/abs/10.1021/ac901447hhttp://pubs.acs.org/doi/suppl/10.1021/ac901447hhttp://pubs.acs.org/doi/full/10.1021/ac901447hhttp://pubs.acs.org/doi/full/10.1021/ac901447hhttp://pubs.acs.org/doi/pdf/10.1021/ac901447hhttp://pubs.acs.org/doi/pdf/10.1021/ac901447hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901447hhttp://pubs.acs.org/doi/pdfplus/10.1021/ac901447hhttp://pubs.acs.org/doi/abs/10.1021/ac9017007http://pubs.acs.org/doi/abs/10.1021/ac9017007

Transducer Microsensor System

Petra Kurzawski, Volker Schurig and Andreas Hierlemann

pp 9353–9364


DOI: 10.1021/ac9017007

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Figure 1 of 7

Online Hydrogen/Deuterium Exchange Performed in the Ion Mobility Cell of a Hybrid Mass

Spectrometer

Korn l Nagy, Karine Redeuil and Serge Rezzi

pp 9365–9371


DOI: 10.1021/ac901736j


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Figure 1 of 4

Microarrays of Ring-Recessed Disk Electrodes in Transient Generator-Collector Mode:

Theory and Experiment

Denis Menshykau, Aoife M. O’Mahony, F. Javier del Campo, Francesc Xavier Mun z and Richard G. Compton

pp 9372–9382


DOI: 10.1021/ac9017633

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Coulometric d-Fructose Biosensor Based on Direct Electron Transfer Using d-Fructose

Dehydrogenase

Seiya Tsujimura, Akiko Nishina, Yuji Kamitaka and Kenji Kano

pp 9383–9387


DOI: 10.1021/ac901771t

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Colorimetric, High-Throughput Assay for Screening Angiotensin I-Converting Enzyme

Inhibitors

V. K. Jimsheena and Lalitha R. Gowda

pp 9388–9394


DOI: 10.1021/ac901775h

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Figure 1 of 5

Analysis of Phosphorylated Peptides by Double Pseudoneutral Loss Extraction Coupled with Abstract



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Derivatization Using N-(4-Bromobenzoyl)aminoethanethiol

Nariyasu Mano, Sayaka Aoki, Takuma Yamazaki, Yoko Nagaya, Masaru Mori, Kohei Abe, Miki Shimada, Hiroaki

Yamaguchi, Takaaki Goto and Junichi Goto

pp 9395–9401


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MALDI Mass Spectrometric Imaging Using the Stretched Sample Method to Reveal

Neuropeptide Distributions in Aplysia Nervous Tissue

Tyler A. Zimmerman, Stanislav S. Rubakhin, Elena V. Romanova, Kevin R. Tucker and Jonathan V. Sweedler

pp 9402–9409


DOI: 10.1021/ac901820v


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Electrochemical Oxidation of Benzothiazole Dyes for Monitoring Amyloid Formation Related

to the Alzheimer’s Disease

Anthony Joseph Veloso, Vinci Wing Sze Hung, Guneet Sindhu, Andrea Constantinof and Kagan Kerman

pp 9410–9415


DOI: 10.1021/ac901940a


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Poly[hydroxyethyl acrylate-co-poly(ethylene glycol) diacrylate] Monolithic Column for

Efficient Hydrophobic Interaction Chromatography of Proteins

Yuanyuan Li, H. Dennis Tolley and Milton L. Lee

pp 9416–9424


DOI: 10.1021/ac9020038

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Dynamic Light Scattering as a Powerful Tool for Gold Nanoparticle Bioconjugation and

Biomolecular Binding Studies

Hilde Jans, Xiong Liu, Lauren Austin, Guido Maes and Qun Huo

pp 9425–9432


DOI: 10.1021/ac901822w

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Colorimetric Assay for Lead Ions Based on the Leaching of Gold Nanoparticles

Yi-You Chen, Huan-Tsung Chang, Yen-Chun Shiang, Yu-Lun Hung, Cheng-Kang Chiang and Chih-Ching Huang

pp 9433–9439


DOI: 10.1021/ac9018268


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Multiplexed Determination of Protein Biomarkers Using Metal-Tagged Antibodies and Size

Exclusion Chromatography−Inductively Coupled Plasma Mass Spectrometry

Mattia Terenghi, Lisa Elviri, Maria Careri, Alessandro Mangia and Ryszard Lobinski

pp 9440–9448


DOI: 10.1021/ac901853g

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Highly Sensitive Protein Detection Based on Lanthanide Chelates with Antenna Ligands Abstract | Supporting Info



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Providing a Linear Range of Five Orders of Magnitude

Thole Zuchner, Frank Schumer, Renate Berger-Hoffmann, Katrin M ller, Mathias Lukas, Kornelia Zeckert, J rg

Marx, Horst Hennig and Ralf Hoffmann

pp 9449–9453


DOI: 10.1021/ac902175g

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NanoLC-MS/MS Analyses of Urinary Desmosine, Hydroxylysylpyridinoline and

Lysylpyridinoline as Biomarkers for Chronic Graft-versus-Host Disease

Michel Boutin, Imran Ahmad, Marjo Jauhiainen, Nathalie Lachapelle, Claude Rondeau, Jean Roy and Pierre

Thibault

pp 9454–9461


DOI: 10.1021/ac9018796

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Voltammetric Detection of 5-Hydroxytryptamine Release in the Rat Brain

Parastoo Hashemi, Elyse C. Dankoski, Jelena Petrovic, Richard B. Keithley and R. M. Wightman

pp 9462–9471


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Measuring Low Picogram Per Liter Concentrations of Freely Dissolved Polychlorinated

Biphenyls in Sediment Pore Water Using Passive Sampling with Polyoxymethylene

Steven B. Hawthorne, David J. Miller and Carol B. Grabanski

pp 9472–9480


DOI: 10.1021/ac9019413

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Structural Profiling of Individual Glycosphingolipids in a Single Thin-Layer Chromatogram

by Multiple Sequential Immunodetection Matched with Direct IR-MALDI-o-TOF Mass

Spectrometry

Jamal Souady, Jens Soltwisch, Klaus Dreisewerd, J rg Haier, Jasna Peter-Katalini and Johannes M thing

pp 9481–9492


DOI: 10.1021/ac901948h


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Figure 1 of 9

A Straightforward Method for the Colorimetric Detection of Endogenous Biological Cyanide

Christine M nnel-Crois , Benjamin Probst and Felix Zelder

pp 9493–9498


DOI: 10.1021/ac901977u


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Label-Free Quantitation of a Cancer Biomarker in Complex Media Using Silicon Photonic

Microring Resonators

Adam L. Washburn, L. Cary Gunn and Ryan C. Bailey

pp 9499–9506


DOI: 10.1021/ac902006p


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Figure 1 of 7

Technical Notes

Purification of Nucleic Acids from Whole Blood Using Isotachophoresis

Alexandre Persat, Lewis A. Marshall and Juan G. Santiago

pp 9507–9511

Publication Date (Web): October 15, 2009 (Technical Note)

DOI: 10.1021/ac901965v


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Polymerase Chain Reaction and Immunoassay−Matrix Assisted Laser Desorption Mass

Spectrometry Using Tag-Mass Technology: New Tools to Break Down Quantification Limits

and Multiplexes

J. Stauber, M. El Ayed, M. Wisztorski, R. Day, I. Fournier and M. Salzet

pp 9512–9521


DOI: 10.1021/ac901416s

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Figure 1 of 5

Peptide Retention Standards and Hydrophobicity Indexes in Reversed-Phase High-

Performance Liquid Chromatography of Peptides

Oleg V. Krokhin and Vic Spicer

pp 9522–9530


DOI: 10.1021/ac9016693


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