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1 Supporting Information Mussel-inspired functionalization of graphene for synthesizing Ag-polydopamine-graphene nanosheets as antibacterial materials Zhe Zhang, Jing Zhang, Bailin Zhang, and Jilin Tang * State Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, (P. R. China) Electronic Supplementary Material (ESI) for Nanoscale This journal is © The Royal Society of Chemistry 2012

Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Page 1: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

1

Supporting Information

Mussel-inspired functionalization of graphene for synthesizing

Ag-polydopamine-graphene nanosheets as antibacterial

materials

Zhe Zhang, Jing Zhang, Bailin Zhang, and Jilin Tang*

State Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied

Chemistry, Chinese Academy of Sciences, Changchun 130022, (P. R. China)

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 2: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S1. FTIR spectra of GO (1) and PDA-GNS (2).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 3: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S2. AFM images of Ag-PDA-GNS-30 (a), Ag-PDA-GNS-40 (b), and

Ag-PDA-GNS-50 (c). In right the cross-sections identified by the lines in (a), (b), and

(c) show the heights of Ag-PDA-GNS, respectively.

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 4: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S3. XRD patterns of Ag-PDA-GNS-30 (1), Ag-PDA-GNS-40 (2), and

Ag-PDA-GNS-50 (3).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 5: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S4. TEM images of Ag-PDA-GNS-30 (a, b), Ag-PDA-GNS-40 (c, d), and

Ag-PDA-GNS-50 (e, f).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 6: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S5. TEM images of Ag-PDA-GNS synthesized by the PDA layer on the surface

of GNS as a reducing agent with 50 mg AgNO3 added.

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 7: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S6. UV-vis absorption spectra of Ag-PDA-GNS-30 (1), Ag-PDA-GNS-40 (2),

and Ag-PDA-GNS-50 (3).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 8: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S7. Raman spectra of Ag-PDA-GNS-30 (1), Ag-PDA-GNS-40 (2), and

Ag-PDA-GNS-50 (3).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 9: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S8. XPS general spectra of GO (1), PDA-GNS (2), and Ag-PDA-GNS-50 (3).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 10: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S9. C 1s XPS spectra of GO (a) and PDA-GNS (b).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

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Fig. S10. TGA curves of Ag-PDA-GNS-30 (1), Ag-PDA-GNS-40 (2), and

Ag-PDA-GNS-50 (3).

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012

Page 12: Supporting Information Mussel-inspired functionalization ... · 12 . Fig. S11. Bacterial growth curves in LB media with the -PDA-GNS. 1% (v/v) Ag active substances of Ag-PDA-GNS was

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Fig. S11. Bacterial growth curves in LB media with the Ag-PDA-GNS. 1% (v/v)

active substances of Ag-PDA-GNS was added to the culture of E.coli (A) and

B.subtilis (B). The growth of the bacteria was measured by the OD at 600 nm

wavelength. The initial addition of Ag-PDA-GNS to the LB bacterium suspension

was regarded as the starting point.

Electronic Supplementary Material (ESI) for NanoscaleThis journal is © The Royal Society of Chemistry 2012