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TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

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Page 1: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

www.alsglobal.comSalt Lake City Laboratory

TEST CATALOG AND FEE SCHEDULE

Page 2: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing
Page 3: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

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1-800-356-9135

Table of Contents Pages Qualifications and Accreditations, Description of Services, Rush Services ........................ ii Partial Lists of Analyses by Method Alphabetical List by Analysis ............................................................................................. 1 NIOSH 4th Edition Methods ............................................................................................ 13 OSHA Methods .............................................................................................................. 17 Common Industrial Hygiene Analyses Acids (Inorganic) ............................................................................................................. 19 Acids (Organic ................................................................................................................. 19 Aldehydes ...................................................................................................................... 19 Amines ........................................................................................................................... 19 Asbestos/Total Fibers ..................................................................................................... 23 Diesel Particulate (Elemental Carbon) ........................................................................... 23 Gravimetric ..................................................................................................................... 24 ♦ Indoor Air Quality (VOCs) ........................................... Air Analysis ................................ 24 Lead and Beryllium ......................................................................................................... 24 ♦ Light Hydrocarbons ...................................................... Air Analysis ................................ 24 Metals ............................................................................................................................. 24 Methamphetamine, Illicit Drugs and Related Compounds .............................................. 25 Pesticides & Herbicides ................................................................................................. 25 Polychlorinated Biphenyls (PCBs) ................................................................................. 26 Polynuclear Aromatic Hydrocarbons (PAHs) ................................................................. 26 Silica (Crystalline) ........................................................................................................... 26 Solvent Panel—Low Level Indoor Air Quality .............. .................................................. 26 ♦ Sulfur Gases (Mercaptans) .......................................... Air Analysis ................................ 26 ♦ Toxic Organic Methods (EPA) ...................................... Air Analysis ................................ 26 ♦ Vapor Intrusion ............................................................. Air Analysis ................................ 26 Analyte and Panel Lists for Common Industrial Hygiene Analyses ................................... 29 ALS Environmental—Salt Lake City Standard Industrial Hygiene Report Formats .......... 35 Media Available from ALS Environmental—Salt Lake City Sorbent Tubes ................................................................................................................ 37 SKC Industrial Hygiene Filters (Assembled) .................................................................. 38 Industrial Hygiene Filters (Assembled at ALS Environmental) ...................................... 39 Passive Samplers ........................................................................................................... 39 Miscellaneous Media ...................................................................................................... 40 Sampling Pump Rentals from ALS Environmental—Salt Lake City Industrial Hygiene Sampling Pumps .............................................................................. 41 Microbiological Services Mold in Air Non-Viable Fungal Spore Analyses ................................................................................ 43 Bulk/Surface Mold Swab, Tape-Lift, Bulk Analyses ...................................................................................... 43

♦ Direct analysis of air samples collected in SUMMA canisters or Tedlar bags

Industrial Hygiene Test Catalog & Fee Schedule

Page 4: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

NOTES

Page 5: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

ALS Environmental in Salt Lake City, Utah is AIHA LAP, LLC accredited for the specified Field(s) of Testing as documented by the scope of accreditation. These fields include the following:

AIHA LAP, LLC Accreditation (ISO 17025 & AIHA LAP, LLC Policies)

DOECAP—AP

ISO 17025:2017

NIOSH Contract Laboratory for 32 years (1974—2006)

Washington State Methamphetamine Certification (No. C596)

ALS participates in several AIHA LAP, LLC Proficiency Analytical Testing (PAT) Programs:

Industrial Hygiene

Metals, Silica, Asbestos/Fibers, Organic Compounds

Beryllium (BePAT)

Bulk Asbestos Analysis Program

Qualifications and Accreditations

ALS Environmental—Salt Lake City is pleased to offer an extensive array of Industrial Hygiene analyses. Specific analytical tests are listed in this catalog. Partial lists of tests are presented in four sections. The first section is an alphabetical list by analyte. The second section lists NIOSH and OSHA methods numerically. The third section provides a list of methods developed in-house and finally the fourth section provides details pertinent to prominent types of industrial hygiene analyses (e.g., asbestos, silica, metals, particulate). Volume discounts are available depending on the scope of the project. Please call a member of our customer service team for additional information.

When preparing samples for analysis, please note that many analyses require a three sample minimum fee to cover the costs of method setup for non-routine sample analyses. Please inquire as to which analyses require this minimum.

Description of Services

Standard Turnaround Time for Routine IH Analytes - 5 Business Days SURCHARGES WILL BE ADDED TO THE LISTED FEES FOR ROUTINE IH ANALYSES BASED ON THE FOLLOWING SAMPLE TURNAROUND TIMES

Pre-arranged Same Day Results (received by 9:00 am Prevailing MT—reported by 6:00 pm Prevailing MT) Quote

Next Working Day Results—reported by 6:00 pm Prevailing MT 100%

Second Day Results—reported by 6:00 pm Prevailing MT 75%

Third Day Full Report—reported by 6:00 pm Prevailing MT 50%

Fourth Day—reported by 6:00 pm MST 35%

Non-routine analysis TAT & applicable surcharges, along with prior notification to confirm rush analysis capacity (e.g. especially same day & one day results) must be arranged with your ALS Project Manager. A 4:00 pm Prevailing MT sample delivery cutoff applies and any samples received after that time will be logged in as received the follow-ing day.

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1-800-356-9135

“For special criteria parameters like DoD/DOE QSM a surcharge of 10% may apply.”

Page 6: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

NOTES

Page 7: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

Abietic Acid OSHA CSI HPLC GFF (Wipe) 150

Acetaldehyde TO-11A HPLC-UV SKC 226-119 90

Acetic acid NIOSH 1603 GC-FID SKC 226-01 110

Acetic acid NIOSH 2011 (Mod) IC SKC 226-10-03 /Prefilter PTFE 110

Acetone NIOSH 1300 GC-FID SKC 226-01 90/25*

Acetone TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Acetonitrile NIOSH 1606 GC-FID SKC 226-09 65

Acid mist OSHA ID 165SG IC SKC 226-10-03 65/20*

Acids (Inorganic) NIOSH Methods IC Various (pgs 19 & 27)

Acids (Organic) ALS LC-MS SKC 226-10-03 / cotton gauze 165/35*

Acrylamide OSHA 21 (Mod) GC-MS SKC 226-10 165

Acrylic acid OSHA 28 HPLC-UV SKC 226-30-08 (2) 90

Acrylonitrile NIOSH 1604 GC-FID SKC 226-01 55

Acrylonitrile OSHA 37 (Mod) GC-FID SKC 226-01 85

Alcohols I NIOSH 1400 GC-FID SKC 226-01 55/15*

Alcohols II NIOSH 1401 GC-FID SKC 226-01 55/15*

Alcohols III NIOSH 1402 GC-FID SKC 226-01 55/15*

Alcohols IV NIOSH 1403 GC-FID SKC 226-01 55/15*

Aldehyde screen TO-11A HPLC SKC 226-119/UMEX100 Badge

$245† 90/25*

Alkaline dust NIOSH 7401 (Mod) TITRA PTFE filter, 1µm 85

Allyl chloride NIOSH 1000 GC-FID SKC 226-01 85

Allyl glycidyl ether NIOSH 2545 GC-FID SKC 226-35-03 95

Amines (pgs 19 - 21)

Ammonia NIOSH 6015 (Mod) VIS SKC 226-10-06 60

n-amyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25*

Amphetamine NIOSH 9111 LC-MS cotton gauze 110/25

Aniline OSHA 73 (Mod) GC-MS SKC 226-98 110

Anisidine NIOSH 2514 HPLC-UV SKC 226-30-05 110

Aroclors (panel of 9) NIOSH 5503 GC-ECD 37mm GFF plus SKC 226-39 100/35

Aromatic hydrocarbons NIOSH 1501 GC-FID SKC 226-01 55/15*

Arsenic Trioxide + As-compounds NIOSH 7901 (Mod) ICP SKC 225-9001 85

Arsine NIOSH 6001 (Mod) ICP-MS SKC 226-01 100

Asbestos (air) NIOSH 7400 (Mod) PCM MCE filter (SKC 225-321A) 20

Asbestos (bulk) NIOSH 9002 (Mod) PLM Bulk material 30

Aspartame NIOSH 5031 HPLC-UV PTFE filter, 1µm 150

Benzene OSHA 12 (Mod) GC-FID SKC 226-01 55

Benzene NIOSH 1501 GC-FID SKC 226-01 55/15*

Benzene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Benzoyl peroxide NIOSH 5009 HPLC MCE filter, .8µm 90

Benzyl acetate OSHA PV2124 GC-FID SKC 226-78 65

Benzyl alcohol OSHA PV 2009 GG-FID SKC 226-95 80

Benzyl chloride NIOSH 1003 GC-FID SKC 226-01 90/25*

Benzyl chloride TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Bis(2-chloroethyl)ether NIOSH 1004 GC-FID SKC 226-01 110

Bis Chlormethyl ether (BCME) by TD/GC-MS

ALS GC-MS 250mg Tenax TD Tube/SKC 226-157PE

400

Partial Alphabetical List of Analysis by Analyte

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Pg 1

1-800-356-9135

“For special criteria parameters like DoD/DOE QSM a surcharge of 10% may apply.”

Page 8: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

Bis(2-ethylhexyl)phthalate NIOSH 5020 GC-FID MCE filter, .8µm 80/20* Biphenyl NIOSH 2530 GC-FID SKC 226-35-01 80

Bisphenol A/Diglycidyl Ether of BPA NIOSH Draft 9029/9209

HPLC-UV QFF (air) / pre-cleaned cotton gauze

220

Bromochloromethane NIOSH 1003 GC-FID SKC 226-01 90/25*

Bromoform TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Bromoform NIOSH 1003 GC-FID SKC 226-01 90/25*

1– Bromopropane/ 2-bromopropane NIOSH 1025 GC-FID SKC 226-01 85/25*

Bromodichloromethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Bromomethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Bromotrifluoromethane NIOSH 1017 GC-FID SKC 226-09 85

Bromoform NIOSH 1003 GC-FID SKC 226-01 90/25* Bromoxynil NIOSH 5605 GC-MS SKC 226-58 or Cotton gauze 110/30*

1,3-Butadiene NIOSH 1024 GC-FID SKC 226-37 85

1,3-Butadiene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 n-Butane ALS Light Hydrocar- GC-FID SUMMA Canister/Tedlar bag 80/35*

2-Butoxyethanol NIOSH 1403 GC-FID SKC 226-01 55/15*

1,3-Butylene Glycol NIOSH 5523 GC-FID SKC 226-57 85/25*

2-Butoxyethylacetate OSHA 83 GC-FID SKC 226-01 90

n-Butyl Acrylate NIOSH 1450 GC-FID SKC 226-01 90/25* 2-Butoxyethanol OSHA 83 GC-FID SKC 226-01 90

sec-Butyl Acetate NIOSH 1450 GC-FID SKC 226-01 90/25*

t-Butyl Acetate NIOSH 1450 GC-FID SKC 226-01 90/25*

n-Butyldiethanolamine ALS GC-MS SKC 226-95 (pgs 19-23)

n-Butyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25*

n-Butyl alcohol NIOSH 1401 GC-FID SKC 226-01 55/15* sec-Butyl alcohol NIOSH 1401 GC-FID SKC 226-01 55/15*

t-Butyl alcohol NIOSH 1400 GC-FID SKC 226-01 55/15*

2-Butoxyethanol acetate OSHA 83 GC-FID SKC 226-01 90

n-Butyl glycidyl ether NIOSH 1616 GC-FID SKC 226-01 85

Butyric Acid ALS LC-MS SKC 226-10-03 165/35

p-tert-Butyltoluene NIOSH 1501 GC-FID SKC 226-01 55/15*

Capsaicin/Dihydrocapsaicin (Pepper NIOSH 5041 HPLC-UV Cotton gauze wipes 110

Camphor NIOSH 1301 GC-FID SKC 226-01 90/25*

Caprolactam OSHA PV2012 HPLC-UV SKC 226-57 110

Carbaryl (Sevin) OSHA 63 HPLC-UV SKC 226-30-16 90

Carbon black NIOSH 5000 GRAV PVC, 5µm, Preweighed 20

Carbon black OSHA ID 196 GRAV PVC, 5µm, Preweighed 110

Carbon disulfide NIOSH 1622 Draft GC-SCD SKC 226-01/226-44 90

Carbon disulfide TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Carbon tetrachloride TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Carbon tetrachloride NIOSH 1003 GC-FID SKC 226-01 90/25*

3-Carene NIOSH 1552 GC-FID SKC 226-01 55/25*

Carfentanyl ALS LC-MS Cotton Gauze 165

Chloramines NIOSH 7607 Draft IC Treated Silica gel/filter cassette 160

Chlordane NIOSH 5510 GC-ECD 226-107/Prefilter (MCE) 130

Chlorinated terphenyl NIOSH 5014 GC-ECD Glass fiber filter, 1µm 90

Chlorine/Bromine NIOSH 6011 (Mod) IC SKC 225-9006 80/35

Chlorine dioxide OSHA ID 202 (Mod) IC Impinger 90

Chlorobenzene TO-15/TO-17(Mod) GC-MS SUMMA/Carbotrap 300 250/250

Chlorobenzene NIOSH 1003 GC-FID SKC 226-01 90/25*

Page 2 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

Page 9: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

p-Chlorobenzotrifluoride NIOSH 1026 GC-FID SKC 226-01 85

Chloroform TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Chloroform NIOSH 1003 GC-FID SKC 226-01 90/25*

Chloromethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

p-Chlorophenol NIOSH 2014 HPLC-UV SKC 226-10 90

Chloroprene NIOSH 1002 GC-FID SKC 226-01 100

Chloroprene/2,3-Dichlorobutadiene ALS D2 GC-MS SKC 226-196 180/50

Chloroprene NIOSH 1002 GC-FID SKC 226-01 90

Chlorothalonil ALS GC-MS SKC 226-58 or cotton gauze wipe Quote

Chlorpyrifos/Diazinon/Malathion ALS GC-MS SKC 226-58 or cotton gauze wipe Quote

Citric acid ALS LC-MS SKC 226-10-03 or cotton gauze wipe

165/35

Cocaine ALS LC-MS cotton gauze wipe 110

Copper (Fumes/Dust; Soluble/Insoluble)

NIOSH 7029 (Mod) ICP MCE filter, .8µm 50/25

Cresols/Phenols OSHA 32 (Mod) GC-MS SKC 226-95 90/35*

Crotonaldehyde TO-11A HPLC-UV SKC 226-119 90/35*

Cumene NIOSH 1501 GC-FID SKC 226-01 55/15*

Cyclohexane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Cyclohexane NIOSH 1500 GC-FID SKC 226-01 55/15*

Cyclohexanol NIOSH 1402 GC-FID SKC 226-01 55/15*

Cyclohexanone OSHA 01 GC-FID SKC 226-110 55

Cyclohexanone NIOSH 1300 GC-FID SKC 226-01 90/25*

Cyclohexene NIOSH 1500 GC-FID SKC 226-01 55/15*

Cyclohexylamine ALS N2568 GC-MS SKC 226-98 165

1,3-Cyclopentadiene NIOSH 2523 GC-FID Chromosorb 104 tube 85

Cyfluthrin ALS GC-MS SKC 226-58/pre-cleaned cotton gauze

Quote

Cypermethrin ALS GC-MS SKC 226-58/pre-cleaned cotton gauze

Quote

Cytarabine ALS LC-MS SKC 226-57 or cotton gauze wipe Quote

2,4-DNT/2,6-DNT/ 2,4,6-TNT OSHA 44 (Mod) HPLC SKC 226-56 90/35*

n-Decane NIOSH 1500 GC-FID SKC 226-01 55/15*

Decabromodiphenyl Oxide NIOSH 2559 HPLC-UV Quartz fiber filter 175

Deltamethrin ALS GC-MS SKC 226-58 or cotton gauze wipe Quote

Diacetone alcohol NIOSH 1402 GC-FID SKC 226-01 55/15*

Dibutyl phosphate NIOSH 5017 (Mod) GC-MS PTFE filter, 1µm 100

Diisobutyl ketone NIOSH 1300 GC-FID SKC 226-01 90/25*

1,2-Dibromoethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

1,2-Dibromo-3-Chloropropane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Dibromochloromethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Dibutyl phthalate/Di(2-ethylhexyl phthalate

NIOSH 5020 GC-FID MCE filter, .8µm 80/20*

1,1-Dichloroethane NIOSH 1003 GC-FID SKC 226-01 90/25*

1,2-Dichlorobenzene NIOSH 1003 GC-FID SKC 226-01 90/25*

1,2-Dichloroethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

1,2-Dichloroethene (cis/trans) TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

1,2-Dichloroethene (cis/trans) NIOSH 1003 GC-FID SKC 226-01 90/25*

1,4-Dichlorobenzene NIOSH 1003 GC-FID SKC 226-01 90/25*

1,1-Dichloro-1-nitroethane NIOSH 1601 GC-FID SKC 226-81A 85

1-800-356-9135

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 3

Page 10: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

1,2-Dichlorobenzene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250 1,3-Dichlorbenzene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

1,4-Dichlorobenzene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Cis & trans 1,4-Dichloro-2-butene ALS D1 GC-MS SIM SKC 226-73 170/35 2,3-Dichloro-1,3-butadiene ALS D2 GC-MS SIM SKC 226-196 170/35

3,3-Dichloro benzidine OSHA 65 (Mod) GC-MS SIM See method 165

Dichlorodifluoromethane NIOSH 1018 GC-FID SKC 226-01 100

Dichlorodifluoromethane TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

cis-1,3-Dichloropropene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

trans-1,3-Dichloropropene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

1,2-Dichloroethane NIOSH 1003 GC-FID SKC 226-01 90/25*

1,1-Dichloroethane TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

1,1-Dichloroethene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Dichloroethyl ether NIOSH 1004 GC-FID SKC 226-01 110

1,2-Dichloropropane TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Dichlorofluoromethane NIOSH 2516 GC-FID SKC 226-09 (2)/226-25 100

Di-n-butylphthalate NIOSH 5020 GC-FID MCE filter, .8µm 80/20*

Diesel Particulate NIOSH 5040 TOA Quartz fiber filter 70

Diethanolamine OSHA PV2018 HPLC-UV SKC 226-30-18 110

Diethylamine OSHA 41 HPLC SKC 226-96 120 Diethylaminoethanol ALS GC-MS SKC 226-94 or 226-95 165

Diethylenediamine (piperazine) ALS N2568 GC-MS SKC 226-98 165/35*

Diethylene glycol NIOSH 5523 GC-FID SKC 226-57 or cotton gauze wipe

85/25*

Diethylenetriamine (DETA) OSHA 60 HPLC-UV SKC 226-30-18 165/35*

Diethyl ether NIOSH 1610 GC-FID SKC 226-01 55/25*

Difluorodibromomethane NIOSH 1012 GC-FID SKC 226-01 (2) 85

Diisobutyl ketone NIOSH 1300 GC-FID SKC 226-01 90/25*

Dimethyl acetamide/DMF NIOSH 2004 (Mod) GC-FID SKC 226-10 85

2,6-Dimethylpiperidine ALS N2568 GC-MS SKC 226-98 165

Dimethylethanolamine ALS GC-MS SKC 226-94 or 226-95 165

Dimethyl Sulfate NIOSH 2524 GC-SCD or GC- SKC 226-114 100

Dimethylamine OSHA 34 HPLC-UV SKC 226-96 120

N,N-Dimethylpropylamine ALS LC-MS SKC 226-98 165

N,N-Dimethylethylamine ALS LC-MS SKC 226-98 165

2,4-Dinitrotoluene; 2,6-Dinitrotoluene OSHA 44 (Mod) HPLC-UV SKC 226-56 90/35*

Dioxane NIOSH 1602 GC-FID SKC 226-01 55

Diphenyl (Biphenyl) NIOSH 2530 GC-FID SKC 226-35-01 or 03 65

Diphenylamine/Isopropylaniline OSHA 78 HPLC GFF SKC 225-9004 (pg 19-23)

Divinyl benzene/Styrene OSHA 89 GC-FID SKC 226-73 100*

Dodecane NIOSH 1500 GC-FID SKC 226-01 55/15*

Dust, respirable NIOSH 0600 (Mod) GRAV PVC, 5µm, Matched Weight 20

Dust, total NIOSH 0500 (Mod) GRAV PVC, 5µm, Matched Weight 20

Ecstasy (MDMA) NIOSH 9111 (Mod) LC-MS cotton gauze 110/25

EGDN/Nitroglycerin OSHA 43 HPLC-UV SKC 226-35-03 90/35*

Elemental Carbon (See pg 23) NIOSH 5040 TOA Quartz fiber filter 70

Page 4 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

Page 11: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

Epichlorohydrin NIOSH 1010 GC-FID SKC 226-01 85

EPN NIOSH 5600 (Mod) GC-MS SKC 226-58 110

Esters I NIOSH 1450 GC-FID SKC 226-01 90/25*

Ethane ALS Light Hydrocarbons GC FID SUMMA/Tedlar Bag 80/35*

Ethanolamine OSHA PV2111 HPLC-UV SKC 226-30-18 110

2-Ethoxyethanol NIOSH 1403 GC-FID SKC 226-01 55/15*

2-Ethoxyethanol acetate NIOSH 1450 GC-FID SKC 226-01 90/25*

Ethyl acetate NIOSH 1457 GC-FID SKC 226-01 65

Ethyl acetate TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Ethyl acrylate NIOSH 1450 GC-FID SKC 226-01 90/25*

Ethyl alcohol OSHA 100 GC-FID SKC 226-82 (2) 55

Ethyl alcohol NIOSH 1400 GC FID SKC 226-01 55/15*

Ethyl benzene NIOSH 1501 GC-FID SKC 226-01 55/15*

Ethyl benzene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Ethyl bromide NIOSH 1011 GC-FID SKC 226-01 85

Ethyl chloride NIOSH 2519 GC-FID SKC 226-25 100

Ethyl chloride TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

N-Ethyldiethanolamine ALS GC-MS SKC 226-94 or SKC 226-95 (pg 19-23)

Ethyl ether NIOSH 1610 GC-FID SKC 226-01 55

Ethyl formate NIOSH 1452 GC-FID SKC 226-01 65

Ethyl acrylate/Methyl acrylate OSHA 92 GC-FID SKC 226-73 110/25

Ethylene ALS Light Hydrocarbons GC- FID SUMMA/Tedlar bag 80/35*

Ethyl methacrylate NIOSH 2537 GC-FID SKC 226-30-06 65/25*

Ethylamine OSHA 36 GC-FID SKC 226-110 120

Ethylene chlorohydrin NIOSH 2513 GC-FID SKC 226-81A 85

Ethylene dibromide OSHA 02 GC-ECD SKC 226-01 85

Ethylene dichloride OSHA 03 GC-ECD SKC 226-01 GWS 85

Ethylenediamine OSHA 60 HPLC-UV SKC 226-30-18 165

Ethylene glycol NIOSH 5523 GC-FID SKC 226-57 85/25*

Ethylene oxide NIOSH 1614 (Mod) GC-MS SKC 226-178 165

Ethylene thiourea OSHA 95 HPLC-UV Glass fiber filter, 1µm 175

4-Ethyl toluene TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250

Explosives (8330 panel) OSHA 44 (Mod) HPLC-UV SKC 226-56 215

Fentanyl ALS LC-MS Cotton gauze wipe 165

Fenthion ALS GC-MS SKC 226-58/cotton gauze wipe

Quote

Fiberglass NIOSH 7400 (Mod) PCM SKC 225-321A 20

Fipronil ALS GC-MS SKC 226-58/cotton gauze wipe

Quote

Fluorides, particulate/gaseous NIOSH 7902 (Mod) ISE SKC 225-9001 55/20*

Fluorouracil ALS LC-MS SKC 226-57/cotton gauze wipe

Quote

Formaldehyde TO-11A HPLC-UV SKC 226-119 90/35*

Formaldehyde NIOSH 2016 (Mod) HPLC-UV SKC 226-119 90

Formaldehyde NIOSH 2541 GC-FID SKC 226-118 Quote

Formaldehyde OSHA 1007 HPLC-UV SKC UMEX 100 90 Formamide OSHA CSI GC-MS SKC 226-10 165

Formic acid NIOSH 2011 (Mod) IC SKC 226-10-03/Prefilter 110

Ephedrine NIOSH 9111 (Mod) LC-MS cotton gauze 110/25

Enflurane/Isoflurane OSHA 103 GC-FID SKC 226-81A 100/25*

Endrin NIOSH 5519 GC-ECD SKC 226-58 90

1-800-356-9135

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 5

Page 12: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

Freon 11 TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Freon 113 TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Freon 114 TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Furfural OSHA 72 GC-FID SKC 226-81A 85 Furfuryl alcohol NIOSH 2505 GC-FID SKC 226-115 55 Fumaric acid ALS LC-MS SKC 226-10-03 165/35 Glutaraldehyde NIOSH 2532 HPLC-UV SKC 226-119 100 Glutaraldehyde OSHA 64 HPLC-UV SKC 225-9003 100 Glycidol NIOSH 1608 GC-FID SKC 226-01 85 Glycolic acid ALS LC-MS SKC 226-10-03 165/35 Glycol ethers NIOSH 2554 GC-FID SKC 226-81A 55/15* Glycols NIOSH 5523 GC-FID SKC 226-57 85/25* Glyphosate ALS LC-MS Quartz fiber filter 275 Halogenated hydrocarbons NIOSH 1003 GC-FID SKC 226-01 90/15* HDI, 2,4-TDI, 2,6-TDI OSHA 5002 (Mod) LC-MS SKC 225-9002 90/35* Heptane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Heptane NIOSH 1500 GC-FID SKC 226-01 55/15* Heroin ALS LC-MS Cotton gauze wipe 110/25 2-Hexanone TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 2-Hexanone NIOSH 1300 GC-FID SKC 226-01 90/25* Hexachlorobutadiene NIOSH 2543 GC-ECD SKC 226-30-04 85 Hexachloro 1,3-butadiene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Hexachlorocyclopentadiene NIOSH 2518 GC-ECD SKC 226-116 (2) 105 n-Hexane NIOSH 1500 GC-FID SKC 226-01 55/15* n-Hexane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Hexachloroethane NIOSH 1003 GC-FID SKC 226-01 90/25* Hexafluoropropylene ALS D3 LC-MS HDS 245 Hexavalent chromium OSHA ID 215 IC PVC filter, 5µm 90 Hexavalent chromium (Painting Operations) OSHA ID 215 IC PVC filter, 5µm 120 Hexylene glycol OSHA PV 2101 GC-FID SKC 226-01 80/25* Hydrazine OSHA 108 HPLC-UV SKC 225-9012 90 Hydrocarbons NIOSH 1500 GC-FID SKC 226-01 55/15* Hydrocarbons NIOSH 1500 GC-FID SKC 575-001/575-002 55/15* Hydrocarbons (light) ALS GC-FID SUMMA or Tedlar bag (pg 29) Hydrogen cyanide NIOSH 6010 (Mod) VIS SKC 226-210 55/20 Hydrogen peroxide OSHA 1019 VIS SKC 225-9030 110 Hydrogen Peroxide/Peroxyacetic Acid OSHA 1019/NON 57 VIS/HPLC-

UV SKC 225-9030/SKC 226-193UC

110/190

Hydrogen sulfide NIOSH 6013 (Mod) IC ORBO 34/Prefilter (PTFE) 85 Hydroquinone NIOSH 5004 HPLC-UV MCE filter, .8µm + 1% acetic

acid 90

2-Hydroxypropyl acrylate OSHA PV2078 GC-FID SKC 226-73 90 Imidacloprid ALS LC-MS SKC 226-58 or cotton gauze 200 Inorganic acids NIOSH Methods IC Various (pgs 19 & 29) Iodine NIOSH 6005 IC SKC 226-67 85 Isocyanates (monomer/each oligomer) Supelco LC-MS ASSET NCO Sampler 165/50

Isobutane ALS Light Hydrocar-bons

GC-FID SUMMA Canister/Tedlar bag 80/35*

Isopentane ALS Light Hydrocar-bons

GC-FID SUMMA Canister/Tedlar bag 80/35*

Isoamyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25* Isoamyl alcohol NIOSH 1402 GC-FID SKC 226-01 55/15* Isobutyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25* Isobutyl alcohol NIOSH 1405 GC-FID SKC 226-01 90/25*

Isocyanates (select monomers) OSHA 5002 (Mod) LC-MS SKC 225-9002 90/35*

Page 6 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Isophorone NIOSH 2508 GC-FID SKC 226-81A 60 Isophorone diisocyanate (IPDI) OSHA 5002 (Mod) LC-MS SKC 225-9002 130 Isopropyl alcohol OSHA 109 (Mod) GC-FID SKC 226-82 (2) 100 Isopropyl alcohol NIOSH 1400 GC-FID SKC 226-01 55/15* Isopropyl acetate NIOSH 1454 GC-FID SKC 226-01 65 Isopropyl acetate NIOSH 1460 GC-FID SKC 226-01 85 Isopropyl ether NIOSH 1618 GC-FID SKC 226-01 85 Lactic acid ALS LC-MS SKC 226-10-03 165/35 Lead 40CFR50APPG ICP GFF, 8x10 50 LSD ALS LC-MS Cotton gauze wipe 110/25 Limonene NIOSH 1522 LC-MS SKC 226-01 55/25 Maleic anhydride OSHA 25 HPLC-UV SKC 226-30-07/226-30 220 Maleic anhydride OSHA 86 HPLC-UV SKC 225-9021 140 Malonic acid ALS LCMS SKC 226-10-03 165/35 MDMA (ecstasy) ALS LC-MS Cotton gauze wipe 110/25 Mercury NIOSH 6009 (Mod) CVAA SKC 226-17-1A 65 Mercury OSHA ID 140 (Mod) CVAA SKC 520-02 (passive badge) 90 Mercury, particulate OSHA ID 145 (Mod) CVAA MCE filter, .8µm 65 Mercury on wipe NIOSH 9103 (Mod) CVAA Wipe 65 Mesityl oxide NIOSH 1301 GC-FID SKC 226-01 90/25* Metals NIOSH 7300 (Mod) ICP MCE filter, .8µm 50/20* (Complete panel of 27 elements pgs 24 & 29) Metals OSHA ID 125G (Mod) ICP MCE filter, .8µm 50/20* (Complete panel of 27 elements pgs 24 & 29) Metals NIOSH 7303 (Mod) MCE filter, .8um 50/20* Metals on wipe NIOSH 9102 (Mod) ICP Ghost Wipe 50/20* Methamphetamine NIOSH 9111 (Mod) LC-MS Cotton gauze wipe 50 Methamphetamine and other com- ALS LC-MS Cotton gauze wipe (pgs 25 & 30)

Methane ALS Light Hydrocar- GC-FID SUMMA/Tedlar Bag 80/35*

Methanol NIOSH 2000 GC-FID SKC 226-51 55 2-Methoxyethanol/2-Ethoxyethanol OSHA 79 GC-FID SKC 226-01 55/15* n-Methyl-2-pyrrolidinone NIOSH 1302 GC-FID SKC 226-01 65 Methyl acetate NIOSH 1458 GC-FID SKC 226-01 65 Methyl acrylate NIOSH 1459 GC-FID SKC 226-01 65 Methyl cellosolve OSHA 53 GC-FID SKC 226-01 55/15* Methyl cellosolve acetate NIOSH 1451 GC-FID SKC 226-01 65 Methyl chloride NIOSH 1001 GC-FID SKC 226-09 100 Methyl chloride TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Methyl cyclohexane NIOSH 1500 GC-FID SKC 226-01 55/15* Methyl cyclohexanone NIOSH 2521 GC-FID SKC 226-115 85 Methyl ethyl ketone NIOSH 2500 GC-FID SKC 226-81A 65 Methyl ethyl ketone TO-15/TO-17 GC-MS SUMMA/Carbotrap 300 250/250 Methyl iodide NIOSH 1014 GC-FID SKC 226-01 85 Methyl isobutyl ketone TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Methyl isobutyl ketone NIOSH 1300 GC-FID SKC 226-01 90/25* Methyl isoamyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25* Methyl isocyanate ALS LC-MS Supelco NCO Asset Sampler Quote Methyl methacrylate NIOSH 2537 GC-FID SKC 226-30-06 65/25* Methyl methacrylate OSHA 94 GC-FID SKC 226-73 85 Methyl n-amyl ketone NIOSH 1301 GC-FID SKC 226-01 90/25* Methyl tert-butyl ether NIOSH 1615 GC-FID SKC 226-37 55 Methyl tert-butyl ether TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Analyte(s) Method Instrument Sample Medium Fee ($)*

1-800-356-9135

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 7

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Analyte(s) Method Instrument Sample Medium Fee ($)*

Methylal NIOSH 1611 GC-FID SKC 226-01 85

Methylamine OSHA 40 HPLC SKC 226-96 120

N-Methylcyclohexylamine ALS GC-MS SKC 226-98 110

N-Methyldiethanolamine ALS LC-MS SKC 226-95 (pgs 19-23)

Methylene bisphenyl disocyanate (MDI) OSHA 5002 (Mod) LC-MS SKC 225-9002 90

Methylene chloride NIOSH 1005 GC-FID SKC 226-01 (2) 70

Methylene chloride TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Methylene chloride OSHA 59 (Mod) GC-FID SKC 226-09-02 70 4,4- Methylenedianiline (MDA) NIOSH 5029 HPLC-UV SKC 225-9004 110

alpha-Methylstyrene NIOSH 1501 GC-FID SKC 226-01 55/15*

Methylstyrene NIOSH 1501 GC-FID SKC 226-01 55/15*

MOCA/o-Dianisidine/o-Tolidine OSHA 71 (Mod) GC-MS SKC 225-9004 100/35*

Monoethanolamine OSHA PV2111 HPLC-UV SKC 226-30-18 110

Morpholine ALS N2568 GC-MS SKC 226-98 165

Naphthalene OSHA 35 (Mod) GC-FID SKC 226-110 90

Naphthalene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Naphthas NIOSH 1550 GC-FID SKC 226-01 55

Nickel Carbonyl NIOSH 6007 (Mod) ICP ORBO 304 100

Nicotine NIOSH 2551 (Mod) GC-MS SKC 226-93 / cotton gauze 85

Nitric oxide/Nitrogen dioxide NIOSH 6014 VIS SKC 226-40A 90/45*

Nitrogen dioxide/Sulfur dioxide ALS IC SKC UMEX 200 85/25

p-Nitroaniline NIOSH 5033 HPLC-UV MCE filter, .8µm 90

Nitrobenzene OSHA 44 (Mod) HPLC SKC 226-56 56

Nitroethane NIOSH 2526 GC-FID SKC 226-30-02 85

Nitrogen Dioxide NIOSH 6014 IC SKC 226-40-2 90

Nitroglycerin/EGDN OSHA 43 HPLC SKC 226-35-03 90/35*

Nitromethane NIOSH 2527 GC-FID SKC 226-111A 85

1-Nitropropane OSHA 46 GC-FID SKC 226-93 85

Nitrotoluene (isomers) OSHA 44 (Mod) HPLC SKC 226-56 90

2-Nitropropane NIOSH 2528 GC-FID SKC 226-110 85

Nitrous Oxide (N2O) ALS GC-ECD Tedlar Bag 165 n-Nonane NIOSH 1500 GC-FID SKC 226-01 55/15*

OCBM (tear gas) P&CAM 304 HPLC-UV SKC 226-56 / cotton gauze 90

n-Octane NIOSH 1500 GC-FID SKC 226-01 55/15*

1-Octanethiol NIOSH 2510 GC-SCD SKC 226-81A 65

Organic Carbon/Elemental Carbon NIOSH 5040 TOA Treated Quartz Fiber Filter 70

Organic vapors OSHA 07 GC-FID SKC 226-01 55/15*

Organochlorine Pesticides (pgs 25, 31) NIOSH 5605 (Mod) GC-ECD/GC-MS

SKC 226-58 / pre-cleaned cotton gauze

Quote

Organophosphorus Pesticides (pgs 25, 31) NIOSH 5600 (Mod) GC-MS SKC 226-58 / pre-cleaned cotton gauze

Quote

Organosulfur Compounds(see Sulfur Gases) ALS GC-SCD SUMMA or Tedlar bag Quote

4,4'-Oxydianiline (ODA) ALS D4 GC-MS SKC 225-9004 165

Oxalic acid OSHA PV2115 IC Glass fiber filter 110

Ozone OSHA ID 214 IC SKC 225-9014 90

Paraquat NIOSH 5003 HPLC-UV PTFE filter, 1µm 150

OCBM (tear gas) P&CAM 304 HPLC-UV SKC 226-56 / cotton gauze 90

n-Octane NIOSH 1500 GC-FID SKC 226-01 55/15*

1-Octanethiol NIOSH 2510 GC-SCD SKC 226-81A 65

Page 8 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Pentanoic acid ALS LC-MS SKC 226-57/cotton gauze 165/35*

Pentane NIOSH 1500 GC-FID SKC 226-01 55/15* Pentane ALS Light Hydrocar- GC-FID SUMMA or Tedlar bag 80

Pentachloroethane NIOSH 2517 GC-ECD SKC 226-59-04 85 Pentachlorophenol OSHA 39 HPLC-UV SKC 226-97 (2) 140 2-Pentanone NIOSH 1300 (Mod) GC-FID SKC 226-01 90/25* Peracetic acid/H2O2 NON 57 / OSHA

1019 HPLC-UV/VIS SKC 226-193UC / SKC 225-

9030 190/110

Permethrin ALS GC-MS SKC 226-58/cotton gauze (pgs 25; 31) Peroxyacetic Acid NON 57 HPLC-UV SKC 226-193UC / 225-9030 190 Pesticides (pgs 25; 31) NIOSH 5601 (Mod) LC-MS SKC 226-58 Quote Pesticides or Herbicides NIOSH 5605 Draft GC-MS SKC 226-58 Quote

Pesticides or Herbicides List (pg 25) Quote Pesticide Surface Residues NIOSH 9201 GC-MS Pre-cleaned cotton gauze Quote Pesticide Surface Residues NIOSH 9202 GC-MS Pre-cleaned cotton gauze Quote Piperonyl butoxide ALS GC-MS SKC 226-58 Quote Phenol/Cresol OSHA 32 (Mod) GC-MS SKC 226-95 90/45* Phenyl propanol amine ALS LC-MS Cotton gauze wipe 110 Phenylene diamine OSHA 87 HPLC-UV SKC 225-9004 (pgs 19-23) Phosgene NON 40 GC-MS SKC 226-153 165 Phosphine OSHA 1003 (Mod) ICP SKC 225-9018 70 Phosphoric acid OSHA ID 111 IC MCE filter, .8µm 65 Phthalates OSHA 104 GC-FID SKC 226-56 90/35* Phthalic anhydride OSHA 90 HPLC-UV Glass fiber filter (treated) 90 Polychlorinated biphenyls (PCBs) NIOSH 5503 GC-ECD SKC 226-39 / Prefilter (GFF) 100 Polynuclear aromatic hydrocarbons (PAH)

NIOSH 5528 Draft GC-MS SIM SKC 226-57 255

Propene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Propionic acid ALS LC-MS SKC 226-10-03 165/35* n-Propyl acetate NIOSH 1450 GC-FID SKC 226-01 90/25* n-Propyl alcohol NIOSH 1401 GC-FID SKC 226-01 55/15* Propylene dichloride NIOSH 1013 GC-FID SKC 226-81A 85 Propylene glycol NIOSH 5523 GC-FID SKC 226-57 85/25* Propylene oxide NIOSH 1612 GC-FID SKC 226-01 100 Pseudoephedrine ALS LC-MS Cotton gauze wipe 110 Pyridine NIOSH 1613 (Mod) GC-MS SKC 226-01 100 Pyridine NIOSH 1613 GC-FID SKC 226-01 65 Quartz & Cristobalite OSHA ID 142 (Mod) XRD PVC filter, 5µm 70 Silica (Crystalline) NIOSH 7500 (Mod) XRD PVC filter, 5µm (pg 26) Solvent Panel (pgs 26 & 30) Sodium azide (Gaseous/Particulate) OSHA ID 211 (Mod) IC 226-55/Prefilter (PVC) 90/90* Solder metals OSHA ID 206 (Mod) ICP MCE filter, .8µm 50/20* Stoddard solvent NIOSH 1550 GC-FID SKC 226-01 55 Strychnine NIOSH 5016 HPLC-UV Glass fiber filter, 1µm 90 Styrene OSHA 09 (Mod) GC-FID SKC 226-01 55 Styrene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Styrene NIOSH 1501 GC-FID SKC 226-01 55/15* Succinic acid ALS LC-MS SKC 226-10-03 165/35* Sulfur dioxide OSHA ID 200 IC SKC 226-80 65 Sulfur dioxide/Sulfate NIOSH 6004 (Mod) IC SKC 225-9005 85/35* Sulfur dioxide/Nitrogen dioxide OSHA ID 182 IC SKC UMEX-200 Badges 85/30 Sulfur gases (panels) ALS GC-SCD SUMMA or Tedlar bag (pgs 26 & 30)

Analyte(s) Method Instrument Sample Medium Fee ($)*

1-800-356-9135

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 9

Page 16: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Analyte(s) Method Instrument Sample Medium Fee ($)*

Sulfur hexafluoride ALS GC-ECD SUMMA or Tedlar bag 220 Sulfuric acid OSHA ID 113 IC MCE filter, .8µm 65 Sulfuryl fluoride NIOSH 6012 (Mod) IC SKC 226-16 100 2,4-TDI OSHA 5002 (Mod) LC-MS SKC 225-9002 90/35* 2,6-TDI OSHA 5002 (Mod) LC-MS SKC 225-9002 90/35* Tear Gas (OCBM) P&CAM 304 HPLC-UV SKC 226-56 90 Temephos ALS GC-MS SKC 226-58 / cotton gauze (pgs 25; 31) Tartaric acid ALS LC-MS Cotton gauze wipe 165/35* o-Terphenyl NIOSH 5021 GC-FID PTFE filter, 2µm 65 1,1,2,2-Tetrabromoethane NIOSH 2003 GC-FID SKC 226-10 85 Tetrachlorodifluoroethane NIOSH 1016 GC-FID SKC 226-01 85 Tetrachloroethene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Tetrachloroethene NIOSH 1003 GC-FID SKC 226-01 90/25* 1,1,2,2-Tetrachloroethane NIOSH 1019 GC-FID SKC 226-81A 85 1,1,2,2-Tetrachloroethane TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Tetraethylene glycol NIOSH 5523 GC-FID SKC 226-57 85/25* Tetraethyl lead (TEL)/Tetramethyl lead (TML)

NIOSH 2533 (Mod) GC-MS SKC 226-30-04/226-30-06 100/35*

Tetrahydrofuran NIOSH 1609 GC-FID SKC 226-01 55 Tetrahydrocannabinol (THC) ALS LC-MS Wipe 85 Thiram NIOSH 5005 HPLC-UV PTFE filter, 1µm 90 o,m,p-Toluidine OSHA 73 (Mod) GC-MS SKC 225-9004 (pg IH-21) Toluene TO-15/ TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Toluene NIOSH 1501 GC-FID SKC 226-01 55/15* Total fibers NIOSH 7400 (Mod) PCM SKC 225-321A 20 Total Petroleum Hydrocarbons NIOSH 1550 GC-FID SKC 226-01 55 Tributyl phosphate NIOSH 5600 (Mod) GC-MS SKC 226-58 100 Trichloramine NIOSH 7607 IC Treated silica gel/filter cassette 160 1,1,2-Trichloro-1,2,2-trifluoroethane NIOSH 1020 GC-FID SKC 226-01 85 1,1,2-Trichloroethane OSHA 11 GC-FID SKC 226-01 55 1,1,2-Trichloroethane NIOSH 1003 GC-FID SKC 226-01 90/25* 1,1,1-Trichloroethane OSHA 14 GC-FID SKC 226-01 55 Trichloroethene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Trichloroethene NIOSH 1022 GC-FID SKC 226-01 55 Trifluorobromomethane NIOSH 1017 GC-FID SKC 226-01 85 1,2,3-Trichloropropane NIOSH 1003 GC-FID SKC 226-01 55/25* Triethanolamine ALS GC-MS SKC 225-709 165 Triethylamine ALS LC-MS SKC 226-98 165 Triethylene tetramine (TETA) OSHA 60 HPLC-UV SKC 226-30-18 165 1,2,4-Trimethylbenzene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250 Trimethylamine ALS LC-MS SKC 226-98 165/35* Triphenyl phosphate ALS GC-MS SKC 226-58 Quote Turpentine NIOSH 1551 GC-FID SKC 226-01 55

Valeraldehyde TO-11A HPLC-UV SKC 226-119 90/20* Vanadium pentoxide NIOSH 7504 (Mod) XRD PVC filter, 5µm 140 Vapor intrusion TO-15 GC-MS Tedlar bag or SUMMA Can 250 Vinyl bromide OSHA 08 GC-FID SKC 226-01 100 Vinyl chloride NIOSH 1007 GC-FID SKC 226-01 (2) 100 Vinyl chloride OSHA 75 GC-FID ORBO 92 Tube 100

Terpenes Scan ALS GC-MS SKC 226-58 Quote

Page 10 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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1-800-356-9135

Analyte(s) Method Instrument Sample Medium Fee ($)*

Vinylidene chloride NIOSH 1015 GC-FID SKC 226-01 100

Vinylidene chloride OSHA 19 GC-FID SKC 226-01 100

Warfarin NIOSH 5002 HPLC-UV PTFE filter, 1µm 110

Xylene TO-15/TO-17 (Mod) GC-MS SUMMA/Carbotrap 300 250/250

Xylene NIOSH 1501 GC-FID SKC 226-01 55/15*

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 11

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NOTES

Page 19: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

1-800-356-9135

NIOSH 4th Edition Methods

Fourth Edition NIOSH Method

Analytes(s) Instrument Sample Medium Fee ($)*

0500 (Mod) Dust, total GRAV PVC, 5µm, Matched Weight 20 0600 (Mod) Dust, respirable GRAV PVC, 5µm, Matched Weight 20 1000 Allyl chloride GC-FID SKC 226-01 85 1001 Methyl chloride GC-FID SKC 226-09 90 1002 Chloroprene GC-FID SKC 226-01 90 1003 Halogenated hydrocarbons GC-FID SKC 226-01 90/25* 1004 Dichloroethyl ether GC-FID SKC 226-01 85 1005 Methylene chloride GC-FID SKC 226-01 (2) 70 1007 Vinyl chloride GC-FID SKC 226-01 (2) 100 1010 Epichlorohydrin GC-FID SKC 226-01 85 1011 Ethyl bromide GC-FID SKC 226-01 85 1012 Difluorodibromomethane GC-FID SKC 226-01 (2) 85 1013 Propylene dichloride GC-FID SKC 226-81A 85 1014 Methyl iodide GC-FID SKC 226-01 85 1015 Vinylidene chloride GC-FID SKC 226-01 100 1016 Tetrachlorodifluoroethane GC-FID SKC 226-01 85 1017 Bromotrifluoromethane GC-FID SKC 226-09 85 1018 Dichlorodifluoromethane GC-FID SKC 226-01 100 1019 1,1,2,2-Tetrachloroethane GC-FID SKC 226-81A 85 1020 1,1,2-Trichloro-1,2,2-trifluoroethane GC-FID SKC 226-01 85 1022 Trichloroethylene GC-FID SKC 226-01 55 1024 1,3-Butadiene GC-FID SKC 226-37 85 1025 1-bromopropane/ 2-bromopropane GC-FID SKC 226-01 85/25* 1026 p-Chlorobenzotrifluoride GC-FID SKC 226-01 85 1300 Ketones I GC-FID SKC 226-01 90/15* 1301 Ketones II GC-FID SKC 226-01 90/15* 1302 n-Methyl-2-pyrrolidinone GC-FID SKC 226-01 65 1400 Alcohols I GC-FID SKC 226-01 55/15* 1401 Alcohols II GC-FID SKC 226-01 55/15* 1402 Alcohols III GC-FID SKC 226-01 55/15* 1403 Alcohols IV GC-FID SKC 226-01 55/15* 1450 Esters I GC-FID SKC 226-01 90/25* 1451 Methyl cellosolve acetate GC-FID SKC 226-01 65 1452 Ethyl formate GC-FID SKC 226-01 65 1454 Isopropyl acetate GC-FID SKC 226-01 65 1457 Ethyl acetate GC-FID SKC 226-01 65 1458 Methyl acetate GC-FID SKC 226-01 65 1459 Methyl acrylate GC-FID SKC 226-01 65 1460 Isopropyl Acetate GC-FID SKC 226-01 85 1500 Hydrocarbons GC-FID SKC 226-01 55/15* 1501 Aromatic hydrocarbons GC-FID SKC 226-01 55/15* 1550 Naphthas/Stoddard solvents/Mineral spirits GC-FID SKC 226-01 55/15* 1551 Turpentine GC-FID SKC 226-01 55 1601 1,1-Dichloro-1-nitroethane GC-FID SKC 226-81A 85 1602 Dioxane GC-FID SKC 226-01 55 1603 Acetic acid GC-FID SKC 226-01 110 1604 Acrylonitrile GC-FID SKC 226-01 55

“For special criteria parameters like DoD/DOE QSM a surcharge of 10% may apply.”

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 13

Page 20: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Fourth Edition NIOSH Method

Analytes(s) Instrument Sample Medium Fee ($)*

1606 Acetonitrile GC-FID SKC 226-09 65 1608 Glycidol GC-FID SKC 226-01 85 1609 Tetrahydrofuran GC-FID SKC 226-01 55 1610 Ethyl ether GC-FID SKC 226-01 55 1611 Methylal GC-FID SKC 226-01 85 1612 Propylene oxide GC-FID SKC 226-01 100 1613 (Mod) Pyridine GC-MS SKC 226-01 100 1613 Pyridine GC-FID SKC 226-01 65 1614 (Mod) Ethylene oxide GC-MS SKC 226-178 165 1615 Methyl tert-butyl ether GC-FID SKC 226-37 55 1616 n-Butyl glycidyl ether GC-FID SKC 226-01 85 1618 Isopropyl ether GC-FID SKC 226-01 85 1622 Draft Carbon Disulfide GC-SCD SKC 226-01/226-09 90 2000 Methanol GC-FID SKC 226-51 55 2002 (Mod) Aromatic Amines LC-MS SKC 226-10 (pgs 19-23) 2003 1,1,2,2-Tetrabromoethane GC-FID SKC 226-10 85 2004 (Mod) Dimethyl acetamide/ DMF GC-FID SKC 226-10 85 2005 Nitrobenzene/Nitrotoluene isomers (by OSHA 44mod) HPLC SKC 226-56 90/35* 2010 (Mod) Aliphatic Amines (pgs 19-23) 2011 (Mod) Formic acid / Acetic acid IC 226-10-03/Prefilter

(PTFE) 110/35*

2014 p-Chlorophenol HPLC-UV SKC 226-10 90 2016 (Mod) Formaldehyde HPLC-UV SKC 226-119 90 2500 Methyl ethyl ketone GC-FID SKC 226-81A 65 2505 Furfuryl alcohol GC-FID SKC 226-115 55

2507 Nitroglycerin/EGDN (by OSHA 43) HPLC SKC 226-35-03 90/35* 2508 Isophorone GC-FID SKC 226-81A 60 2510 (Mod) 1-Octanethiol GC-SCD SKC 226-35-03 65 2513 Ethylene chlorohydrin GC-FID SKC 226-81A 85 2514 Anisidine HPLC-UV SKC 226-30-05 110 2516 Dichlorofluoromethane GC-FID SKC 226-09 (2)/226-25 100 2517 Pentachloroethane GC-ECD SKC 226-59-04 85 2518 Hexachlorocyclopentadiene GC-ECD SKC 226-116 (2) 105 2519 Ethyl chloride GC-FID SKC 226-25 100 2521 Methyl cyclohexanone GC-FID SKC 226-115 85 2523 1,3-Cyclopentadiene GC-FID Chromosorb 104 tube 85 2524 Dimethyl Sulfate GC-MS or GC-

SCD SKC 226-114 100

2526 Nitroethane GC-FID SKC 226-30-02 85 2527 Nitromethane GC-FID SKC 226-111A 85 2528 2-Nitropropane GC-FID SKC 226-110 85 2530 Diphenyl (biphenyl) GC-FID SKC 226-35-01 65 2532 Glutaraldehyde HPLC-UV SKC 226-119 100 2533 (Mod) Tetraethyl Lead/Tetramethyl Lead GC-MS SKC 226-30-04/226-30-06 100/35* 2536 Valeraldehyde (by EPA TO-11A) HPLC-UV SKC 226-119 90 2537 Ethyl methacrylate/Methyl methacrylate GC-FID SKC 226-30-06 65/25* 2540 Ethylenediamine (by OSHA 60) HPLC-UV SKC 226-30-18 165 2541 Formaldehyde GC-FID SKC 226-118 Quote

2543 Hexachlorobutadiene GC-ECD SKC 226-30-04 85 2545 Allyl glycidyl ether GC-FID SKC 226-35-03 95 2551 (Mod) Nicotine GC-MS SKC 226-93 110 2554 Glycol Ethers GC-FID SKC 226-81A 55/15* 2555 (Mod) Ketones I GC-FID SKC 226-81A 85/20* 2559 Decabromodiphenyl Oxide HPLC-UV Quartz fiber filter 175

Page 14 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

Page 21: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Fourth Edition NIOSH Method

Analytes(s) Instrument Sample Medium Fee ($)*

5000 Carbon black GRAV PVC, 5µm, Matched Weight 20 5003 Paraquat/Diquat HPLC-UV PTFE filter, 1µm 150/35* 5004 Hydroquinone HPLC-UV MCE filter, .8µm 90 5005 Thiram HPLC-UV PTFE filter, 1µm 90 5009 Benzoyl peroxide HPLC-UV MCE filter, .8µm 90 5010 Bromoxynil (by NIOSH 5605 GCMS) GC-MS SKC 226-58 Quote 5014 Chlorinated terphenyl GC-ECD Glass fiber filter, 1µm 90 5016 Strychnine HPLC Glass fiber filter, 1µm 90 5017 (Mod) Dibutyl phosphate GC-MS PTFE filter, 1µm 100 5020 Dibutyl phthalate/Di(2-ethylhexyl)phthalate GC-FID MCE filter, .8µm 80/20* 5021 o-Terphenyl GC-FID PTFE filter, 2µm 65 5029 4,4-Methylenedianiline (MDA) HPLC-UV SKC 225-9004 110

5038 Triphenyl phosphate (by NIOSH 5600 mod) GC-MS SKC 226-58 Quote 5039 Toxaphene (or NIOSH 5605) GC-ECD SKC 226-58 100/35* 5040 Diesel Particulate (Elemental carbon) TOA SKC 225-401 70 5041 Capsaicin HPLC PTFE or GFF 110 5502 Aldrin/Lindane (by NIOSH 5605) GC-ECD SKC 226-58 110/35* 5503 Polychlorinated biphenyls GC-ECD 37 mm GFF/SKC 226-39 100 5509 Benzidine/3,3-Dichlorobenzidine HPLC-UV Glass fiber filter, 1µm 90/35*

5510 Chlordane GC-ECD 226-107/Prefilter (MCE) 130 5523 Glycols GC-FID SKC 226-57 85/25* 5528 Draft Polynuclear Aromatic Hydrocarbons (PAH) GC-MS SIM SKC 226-57 255 5600 (Mod) Organophosphorus pesticides GC-MS SKC 226-58 Quote 5601 (Mod) Pesticides (pgs 24; 31) LC-MS SKC 226-58 Quote 5602 (Mod) Organochlorine pesticides and herbicides (pgs 24;

31) GC-MS SKC 226-58 Quote

5605 Draft Pesticides or Herbicides GC-MS/GC- SKC 226-58 Quote 6001 (Mod) Arsine ICP-MS SKC 226-01 100 6004 (Mod) Sulfur dioxide/Sulfate IC SKC 225-9005 85/35* 6005 Iodine IC SKC 226-67 85 6007(Mod) Nickel Carbonyl ICP ORBO 304 100 6009 (Mod) Mercury CVAA SKC 226-17-1A 65 6010 (Mod) Hydrogen cyanide VIS SKC 226-210 55/20 6011 (Mod) Chlorine/Bromine IC SKC 225-9006 150/50* 6012 (Mod) Sulfuryl fluoride IC SKC 226-16 175 6013 (Mod) Hydrogen sulfide IC ORBO 34Prefilter (PTFE) + o-

ring 85

6014 Nitric oxide/Nitrogen dioxide VIS SKC 226-40A 90/45* 6015 (Mod) Ammonia VIS SKC 226-10-06 60 7029 (Mod) Copper, or other metals (Dust/Fume) ICP MCE filter, .8µm 50/25* 7300 (Mod) Metals ICP MCE filter, .8µm 50/20* (Complete panel-27 elements ) pg 24 7303 (Mod) Metals ICP MCE filter, .8 um 50/20* 7400 (Mod) Total Fibers PCM SKC 225-321A 20 7401 (Mod) Alkaline dust TITRA PTFE filter, 1µm 85 7500 (Mod) Silica (crystalline) XRD PVC filter, 5µm (pg 26) 7504 (Mod) Vanadium pentoxide XRD PVC filter, 5µm 140 7607 (Mod) Chloramine compounds IC Silica gel/filter cassette 160 7901 (Mod) Arsenic trioxide ICP SKC 225-9001 85 7902 (Mod) Fluorides, particulate/gaseous ISE SKC 225-9001 55/20*

1-800-356-9135

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 15

Page 22: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

FourthEdition NIOSH Method

Analytes(s) Instrument Sample Medium Fee ($)*

7906 Hydrofluoric acid IC SKC 225-9031 110 7907 Hydrochloric, Hydrobromic, Nitric acids IC SKC 225-9032 110/35* 7908 Sulfuric, Phosphoric acids IC SKC 225-9033 110/35* 9002 (Mod) Asbestos bulk PLM Bulk material 30 9029 Draft Bisphenol A and Diglycidyl Ether of BPA in

air HPLC-UV QFF 220

9102 (Mod) Metals on wipe ICP Wipe 50/20* 9103 (Mod) Mercury on wipe CVAA Wipe 65 9111 (Mod) Methamphetamine LC-MS Cotton gauze (pgs 25 & 31) 9201 (Mod) Pesticide Surface Residues, scan GC-MS Pre-cleaned cotton gauze Quote 9202 (Mod) Pesticide Surface Residues, scan GC-MS Pre-cleaned cotton gauze Quote 9204 (Draft) Pesticide Surface Residues, scan GC-MS Pre-cleaned cotton gauze Quote 9209 (Draft) Bisphenol A and Diglycidyl Ether of BPA HPLC-UV Pre-cleaned cotton gauze 220

Page 16 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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OSHA Method Analytes(s) Instrument Sample Medium Fee ($)* 01 Cyclohexanone GC-FID SKC 226-110 55 02 Ethylene dibromide GC-ECD SKC 226-01 85 03 Ethylene dichloride GC-ECD SKC 226-01 GWS 85 05 Chloroform (by NIOSH 1003) GC-FID SKC 226-01 90 07 Organic vapors GC-FID SKC 226-01 55/15* 08 Vinyl bromide GC-FID SKC 226-01 100 09 (Mod) Styrene GC-FID SKC 226-01 55 11 (Mod) 1,1,2-Trichloroethane GC-FID SKC 226-01 55 12 (Mod) Benzene GC-FID SKC 226-01 or 226-09 55/15* 14 (Mod) 1,1,1-Trichloroethane GC-FID SKC 226-01 55 19 Vinylidene chloride GC-FID SKC 226-01 100 21 (Mod) Acrylamide GC-MS SKC 226-10 or 226-57 165 25 Maleic anhydride HPLC-UV SKC 226-30-07 or 226-30 220 28 Acrylic acid HPLC-UV SKC 226-30-08 (2) 90 29 Enflurane/Halothane GC-FID SKC 226-01 (2) Quote 32 (Mod) Phenol /Cresol GC-MS SKC 226-95 90/35* 34 Dimethylamine HPLC SKC 226-96 120 35 (Mod) Naphthalene GC-FID SKC 226-110 90 36 Ethylamine HPLC SKC-226-96 120 37 (Mod) Acrylonitrile GC-FID SKC 226-01 85 39 Pentachlorophenol HPLC-UV SKC 226-97 (2) 140 40 Methylamine HPLC SKC 226-96 120 41 Diethylamine HPLC SKC 226-96 120 42 HDI/2,4-TDI/2,6-TDI (by OSHA 5002mod) LC-MS SKC 225-9002 90/35* 42 Isophorone diisocyanate (by OSHA 5002mod) LC-MS SKC 225-9002 130 43 EGDN/Nitroglycerin HPLC-UV SKC 226-35-03 90/35* 44 (Mod) 2,4-DNT/2,6-DNT/2,4,6-TNT HPLC-UV SKC 226-56 90/35* 46 1-Nitropropane GC-FID SKC 226-93 85 47 Methylene bis-phenyl diisocyanate (MDI) (by LC-MS SKC 225-9002 90

50 Ethylene oxide (by NIOSH 1614mod) GC-MS SKC 226-178 165 53 Methyl cellosolve GC-FID SKC 226-01 55/15* 54 Methyl isocyanate (by LCMS on ASSET) LCMS ASSET EZ4-NCO Quote 57 4,4-Methylenedianiline (MDA) (by NIOSH 5029) GC-MS SKC 225-9004 110 59 (Mod) Methylene chloride GC-FID SKC 226-09-02 70 63 (Mod) Carbaryl (Sevin) HPLC-UV SKC 226-30-16 90 64 Glutaraldehyde HPLC-UV SKC 225-9003 100 65 Benzidine (by ALS method) GC-MS SKC 225-9004 (pg IH-20) 65 3,3-Dichlorobenzidine (by ALS method) GC-MS SKC 225-9004 (pg IH-20) 71 MOCA/o-Dianisidine/o-Tolidine GC-MS SKC 225-9004 (pg IH-20) 72 Furfural GC-FID SKC 226-81A 85 73 o,m,p-Toluidine (by ALS method) GC-MS SKC 225-9004 (pg IH-20) 75 Vinyl chloride GC-FID ORBO 92 Tube 100 78 Diphenylamine/Isopropylaniline HPLC GFF SKC 225-9004 (pg IH-20) 79 2-Methoxyethanol/2-Ethoxyethanol GC-FID SKC 226-01 55/15* 83 2-Butoxyethanol GC-FID SKC 226-01 90 86 Maleic anhydride HPLC-UV SKC 225-9021 140

OSHA Methods

1-800-356-9135

“For special criteria parameters like DoD/DOE QSM a surcharge of 10% may apply.”

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 17

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OSHA Method Analytes(s) Instrument Sample Medium Fee ($)*

89 Divinyl benzene/Styrene GC-FID SKC 226-73 100/35 90 Phthalic anhydride HPLC-UV Glass fiber filter (treated) 90 92 Ethylacrylate/Methylacrylate GC-FID SKC 226-73 110/25* 94 Methyl methacrylate GC-FID SKC 226-73 85 95 Ethylene thiourea HPLC-UV Glass fiber filter, 1µm 170 98 Trimellitic anhydride (TMA) HPLC-UV Glass fiber filter (treated) 175 100 Ethyl alcohol GC-FID SKC 226-82 (2) 55 103 Enflurane / Isoflurane GC-FID SKC 226-81A 100/25* 104 Phthalates GC-FID SKC 226-56 90/35* 106 Desflurane GC-FID SKC 226-81A 110 108 Hydrazine HPLC-UV SKC 225-9012 90 109 (Mod) Isopropyl alcohol GC/FID SKC 226-82(2) 100 1003 (Mod) Phosphine ICP SKC 225-9018 70 1007 Formaldehyde HPLC-UV SKC UMEX100 90 1019 Hydrogen peroxide VIS SKC 225-9030 110 ID 111 Phosphoric acid (by NIOSH 7908) IC SKC 225-9033 110 ID 112 Formic acid (by NIOSH 2011mod) IC SKC 226-10-03/Prefilter (PTFE) 110 ID 113 Sulfuric acid IC MCE filter, .8µm 65 ID 125G (Mod) Metals (pgs 24 & 29) ICP MCE filter, .8µm (Full Panel – $125) 50/20* ID 140 (Mod) Mercury CVAA SKC-520-02 90 ID 142 (Mod) Quartz & Cristobalite (pg 26) XRD PVC filter, 5µm 70 ID 145 (Mod) Mercury, particulate CVAA MCE filter, .8µm 65 ID 174SG Hydrochloric Acid IC SKC 226-10-03 65 ID 182 Sulfur dioxide / Nitrogen dioxide IC SKC UMEx 500-200 Badge 85/30* ID 165SG Acid mist IC SKC 226-10-03 65/20* ID 200 Sulfur dioxide IC SKC 226-80 65 ID 202 (Mod) Chlorine dioxide IC Fritted bubbler 90 ID 206 (Mod) Solder metals ICP MCE filter, .8µm 50/20* ID 211 (Mod) Sodium Azide (Gaseous/ Particulate) IC 226-55/Prefilter (PVC) 90/90* ID 214 Ozone IC SKC 225-9014 90 ID 215 Hexavalent Chromium IC PVC filter, 5µm 90 ID 215 Hexavalent Chromium (painting operation) IC PVC filter, 5µm 120

PV2115 Oxalic acid IC SKC 226-10-03 110

Page 18 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Common Industrial Hygiene Analyses

Analyte Method Instrument Medium Fee($) Hydrofluoric acid NIOSH 7906 IC SKC 225-9031

37mm treated filter 110

Hydrochloric, Hydrobromic, Nitric acids

NIOSH 7907 IC SKC 225-9032 37mm treated filter

110/35*

Sulfuric, Phosphoric acids NIOSH 7908 IC SKC 225-9033 37mm treated filter

110/35*

Acids (Inorganic) Analyte List (pg 29)

Aldehydes Analyte List (Pg 22)

Analyte Method Instrument Medium Fee($) Aldehydes (Panel of 15—pg 29) TO-11A HPLC-UV SKC 226-119 or UMEX100 Badge 225

Test Catalog & Fee Schedule Page 19

1-800-356-9135

Analyte Method Instrument Medium Fee($) Organic acids (Acetic, Formic) NIOSH 2011 (Mod) IC SKC 226-10-03 / Prefilter PTFE 110/35*

Organic acids (Panel of 3) ALS LC-MS SKC 226-10-03 Wipes cotton gauze

165/35*

Organic acids (Panel of 8) ALS LC-MS SKC 226-10-03 Wipes cotton gauze

165/35*

Organic Acids (Semiquantitative Panel)

ALS IC/LC-MS SKC 226-10-03 Wipes cotton gauze

350

Oxalic acid OSHA PV2115 IC Glass fiber filter 110

Acids (Organic) Analyte List (pg 29)

Aldehydes

3 sample minimum

Amines

SECTION 1: NBD-chloride Treated XAD-7 Sampler Volatile Amines

The NBD-chloride treated XAD-7 treated SKC 226-96 sampler can be used for volatile C1-C4 primary or secondary alkyl amines. All four analytes listed below can be analyzed together as the Amines-VOA Aliphatic VAA-1 panel.

Table 1. NBD-Chloride treated XAD-7 and LC analysis

Analyte Method Instrument Medium Notes Fee($)

Methylamine OSHA 40 HPLC-UV 226-96 120/35*

Ethylamine OSHA 36 HPLC-UV 226-96 120/35*

Diethylamine (DEA) OSHA 41 HPLC-UV 226-96 120/35*

Dimethylamine (DMA) OSHA 34 HPLC-UV 226-96 120/35*

SECTION 2: NITC Treated XAD-2 Sampler and LC-UV or LC-MS Amines

The NITC treated XAD-2 sampler, SKC 226-30-18, works for primary and secondary amines. Most of the amines listed in sec-tion 3 below may also be analyzed using the SKC 226-30-18 sampler and LC analysis upon request.

Table 2. NITC treated XAD-2 and LC-UV analysis

Analyte Method Instrument Medium Notes Fee($)

(Mono-) Ethanolamine (MEA) PV2111 HPLC-UV 226-30-18 1 110/35*

1-Amino-2-propanol PV2122 HPLC-UV 226-30-18 110/35*

2-Amino-2-methyl-1-propanol PV2145 HPLC-UV 226-30-18 110/35*

Aminoethylethanolamine (AEEA) PV2116 HPLC-UV 226-30-18 165/35*

Diethanolamine (DEA) PV2018 HPLC-UV 226-30-18 110/35*

Isopropylamine PV2126 HPLC-UV 226-30-18 165/35*

7 working day TAT 3 sample minimum

Note: See Footnotes on Page 27

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Page 20 Test Catalog & Fee Schedule

Analyte Method Instrument Medium Notes Fee($)

Ethylenediamine (EDA) OSHA 60 HPLC-UV 226-30-18 165/35*

Diethylenetriamine (DETA) OSHA 60 HPLC-UV 226-30-18 165/35*

Triethylenetetramine (TETA) OSHA 60 HPLC-UV 226-30-18 165/35*

Tetraethylenepentamine OSHA 60 Modified HPLC-UV 226-30-18 165/35*

Hexamethylenediamine (1,6-Hexanediamine) OSHA 60 Modified HPLC-UV 226-30-18

165/35*

Diethylamine OSHA 60 Modified HPLC-UV 226-30-18 2 165/35*

Piperazine (diethylenediamine) OSHA 60 Modified HPLC-UV 226-30-18 3 165/35*

Morpholine OSHA 60 Modified HPLC-UV 226-30-18 3 165/35*

1. Mono-ethanolamine has been determined by ALS method N2568 which offers an alternative method to analyze mono-ethanolamine with other N2568 analytes such as N,N-dimethyl-ethanolamine on 226-95 media.

2. The preferred method for diethylamine is OSHA 41, analysis by HPLC on the 226-96 sampler. Diethylamine has also been determined by ALS method N2568 by GC-MS in the past.

3. Morpholine and piperazine are sometimes sampled together on SKC 226-30-18, but the NITC derivatives have problems separating on the LC column. Therefore it is preferable to sample these on SKC 226-98 and determining these by GC-MS using N2568.

SECTION 3: Alkyl Amines Using ALS Method, N2568.

ALS method N2568 is applicable to a wide range of primary and secondary alkyl amines and other compounds. The preferred sampler for alkyl amines is the SKC 226-98, a phosphoric acid treated XAD-7 tube. It takes the place of silica gel, acid treated silica gel samplers, and impingers previously recommended for various amines. Most of the amines listed in section 2 above may also be analyzed using ALS N2568 provided they are sampled on the 226-98 sampler.

Table 2. NITC treated XAD-2 and LC-UV analysis cont.

Table 3. Alkyl Amines using N2568 with meta-toluoyl chloride derivatization

Analyte Method Instrument Medium Notes Fee($)

Aniline (OSHA PV 2079) ALS N2568 GC-MS 226-98 1 165/35*

Benzylamine ALS N2568 GC-MS 226-98 165/35*

Butylamine ALS N2568 GC-MS 226-98 165/35*

Cyclohexylamine (PV2016) ALS N2568 GC-MS 226-98 165/35*

Dibutylamine ALS N2568 GC-MS 226-98 165/35*

Diethylamine ALS N2568 GC-MS 226-98 2 165/35*

2,6-Dimethylpiperidine ALS N2568 GC-MS 226-98 165/35*

Di-n-propylamine ALS N2568 GC-MS 226-98 165/35*

2-Ethylhexylamine ALS N2568 GC-MS 226-98 165/35*

1-Hexylamine ALS N2568 GC-MS 226-98 165/35*

3-Methoxypropylamine ALS N2568 GC-MS 226-98 165/35*

N-Methylcyclohexylamine ALS N2568 GC-MS 226-98 165/35*

Morpholine ALS N2568 GC-MS 226-98 3 165/35*

Phenethylamine ALS N2568 GC-MS 226-98 165/35*

Piperidine ALS N2568 GC-MS 226-98 165/35*

Piperazine (diethylenediamine) ALS N2568 GC-MS 226-98 3 165/35* 1. The preferred method for Aniline is OSHA 73 Modified (section 5). Upon request, the ALS N2568 alternative uses the same sampler but

derivatizes the analyte with m-toluoyl chloride. 2. The preferred method for diethylamine is OSHA 41, analysis by HPLC on the 226-96 sampler. 3. Morpholine and piperazine can be sampled on SKC 226-30-18, but the NITC derivatives may have problems separating on the LC column.

Therefore it is preferable to sample these on SKC 226-98 with analysis by ALS N2568.

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7 working day TAT 3 sample minimum

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Test Catalog & Fee Schedule Page 21

SECTION 4: Alcoholamines Using ALS Method, N2568.

ALS recommends most alcoholamines be collected separate from the alkyl amines listed in table 3. If collected on 226-95 samplers, MBTSTFA (a silylating reagent) derivatization can be used, an easier and faster procedure to prepare samples for analysis. If 226-98 samplers must be used, meta-toluoyl chloride derivatization will be performed (see section 3).

Table 4. Alcoholamines using ALS method N2568

Analyte Method Instrument Medium Notes Fee($)

(Mono-) Ethanolamine (MEA) ALS N2568 GC-MS 226-95 1 150/35*

N,N-Dimethylaminoethanol (DMAE) (NIOSH 2561) ALS N2568 GC-MS 226-95 2 150/35*

N,N-Diethylaminoethanol (DEAE) (NIOSH 2007) ALS N2568 GC-MS 226-95 2 150/35*

N,N-Dibuylaminoethanol (DBAE) (NIOSH 2007) ALS N2568 GC-MS 226-95 2 150/35*

N,N-Dimethylaminopropanol (DMAP) (NIOSH 2561) ALS N2568 GC-MS 226-95 2 150/35*

N-Methyldiethanolamine (NMDEA) ALS N2568 GC-MS 226-95 3 150/35*

N-Ethyldiethanolamine (NEDEA) ALS N2568 GC-MS 226-95 3 150/35*

N-Butyldiethanolamine (NBDEA) ALS N2568 GC-MS 226-95 3 150/35*

Piperazine, N-(2-hydroxyethyl) ALS N2568 GC-MS 226-98 4 165/35*

N,N-Dimethylaminoethoxyethanol, 2- (DMAEE) ALS N2568 GC-MS 226-95 2 150/35*

1. The preferred media for mono-ethanolamine is the 226-30-18 sampler with analysis by LC. Mono-ethanolamine has been successfully determined by ALS method N2568 with meta-toluoyl chloride in the past.

2. These ethanolamines have been analyzed by N2568 using meta-toluoyl chloride. But their vapor pressures are compatible with the 226-95 sampler, which allows derivati-zation with MTBSTFA.

3. These ethanolamines have been analyzed by N2568 using meta-toluoyl chloride. Their vapor pressures are compatible with the 226-95 sampler, which allows desorption with ACN and derivatization with MSTFA, same as for triethanolamine (table 9) by OSHA PV2141 modified. However, MTBSTFA is the preferred derivatization reagent.

4. Piperazine, N-(2-hydroxyethyl) contains a secondary amine and requires derivatization by meta-toluoyl chloride, but can be collected on the 226-95 sampler if necessary.

SECTION 5: Aromatic Amines

Aromatic amines have been determined at ALS by both HPLC-UV/MS and GC-MS procedures. GC-MS analysis usually in-volves derivatization with heptafluorobutyric anhydride (HFBA).

Table 5. Mono-aromatic amines and diamines by OSHA 73 modified

Analyte Method Instrument Medium Notes Fee($)

2-, 3-, 4-Aminopyridines OSHA 73 modified * GC-MS 225-9004 1 110/35*

Aniline (OSHA PV2079) OSHA 73 modified * GC-MS 226-98 2 110/35*

Anisidines OSHA 73 modified * GC-MS 226-98 110/35*

Chloroanilines (OSHA PV2109) OSHA 73 modified * GC-MS 225-9004 110/35*

Dichloroanilines OSHA 73 modified * GC-MS 225-9004 110/35*

Diethylanilines OSHA 73 modified * GC-MS 225-9004 110/35*

Dimethoxyanilines OSHA 73 modified * GC-MS 226-98 3 110/35*

Dimethylanilines (Xylidines) OSHA 73 modified * GC-MS 225-9004 110/35*

Diethylmethylphenylenediamine (mixed iso-mers)

OSHA 73 modified * GC-MS 225-9004 110/35*

2-Ethyl aniline OSHA 73 modified * GC-MS 225-9004 110/35*

N-Ethyl-aniline OSHA 73 modified * GC-MS 225-9004 110/35*

N-Isopropylaniline OSHA 73 modified * GC-MS 225-9004 110/35*

Methylanilines (Toluidines) (OSHA 73) OSHA 73 modified * GC-MS 225-9004 110/35*

N-Methylaniline OSHA 73 modified * GC-MS 225-9004 110/35*

5-Methyl-ortho-anisidine (p-Cresidine) OSHA 73 modified * GC-MS 226-98 3 110/35*

7 working day TAT 3 sample minimum

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Page 22 Test Catalog & Fee Schedule

Table 5. Mono-aromatic amines and diamines by OSHA 73 modified cont.

Analyte Method Instrument Medium Notes Fee($)

Toluenediamine, 2,4-, 2,6- (OSHA 65) OSHA 73 modified * GC-MS 225-9004 1 110/35*

2,4,6-Trimethylphenylenediamine OSHA 73 modified * GC-MS 225-9004 110/35*

Xylenediamine, meta-, para- (OSHA 105) OSHA 73 modified * GC-MS 226-98 3, 4 110/35* * OSHA 73 modified does not require samples be transferred to vials containing water. In general, aromatic amines with one benzene ring are stable in the cassettes for shipment and storage. 1. The toluene-diamines and aminopyridines require a high ionic strength aqueous phase for extraction. See OSHA 65 for an example. These analytes should be sampled

separately from the other analytes in table 5 and 6. 2. Aniline can also be determined by ALS method N2568 on 226-98 media if requested. 3. SKC 226-98 media is preferred for this analyte. OSHA 73 modified replaces NIOSH 2514 or OSHA CSI recommended media. 4. The preferred method for xylene-diamines is OSHA 105, analysis by HPLC as found in table 7 below. OSHA 73 modified can be used as an alternative method using 226-

98 media if necessary.

Table 6. Poly-aromatic amines and diamines by ALS ODA method

Analyte Method Instrument Medium Notes Fee($)

4-Aminobiphenyl (OSHA 93) ALS ODA method * GC-MS 225-9004 110/35*

Benzidine (OSHA 65) ALS ODA method * GC-MS 225-9004 110/35*

ortho-Dianisidine (OSHA 71) ALS ODA method * GC-MS 225-9004 110/35*

3,3’-Dichlorobenzidine (OSHA 65) ALS ODA method * GC-MS 225-9004 110/35*

Methylene-bis(2-chloroaniline) (MOCA) ALS ODA method * GC-MS 225-9004 110/35*

4,4’-Methylenedianiline (MDA) (OSHA 57) ALS ODA method * GC-MS 225-9004 110/35*

Methylene-bis(ortho-ethylaniline) (MBOEA) ALS ODA method * GC-MS 225-9004 110/35*

Naphthylamines, alpha-, beta- (OSHA 93) ALS ODA method * GC-MS 225-9004 110/35*

4,4’-Oxydianiline (ODA) ALS ODA method * GC-MS 225-9004 110/35*

ortho-Tolidine (OSHA 71) ALS ODA method * GC-MS 225-9004 110/35*

* ALS ODA method is a modified OSHA 65 method, requiring filters to be transferred from cassettes to vials containing 2 mL of water within 10 hours of sampling.

Table 7. Aromatic amines NOT analyzed using OSHA 73 modified or ALS ODA method

Analyte Method Instrument Medium Notes Fee($)

Nitroanilines N5033 HPLC-UV SKC 225-3-01 (MCE) Quote

Phenylenediamine, ortho-meta OSHA 87 HPLC 225-9004 1 120/35

Diphenylamine n-Isopropylaniline

OSHA 78 modified GC-MS SKC 225-9004 2

100/35

N,N-Dialkyl Aromatics: N,N-Dimethylaniline N,N-Dimethyl-p-toluidine

OSHA PV2064 modi-fied replacing OSHA PV 2064 and NIOSH

GC-MS SKC 226-98 2

100/35

N-Phenyl-1-naphthylamine N-Phenyl-2-naphthylamine

OSHA 96

HPLC-Fluorescence

SKC 225-9015 ascorbic acid treated GFF

3 Quote

2,5-Dimethyl pyrrole ALS Method GC-MS 226-153 4 Quote

1. The phenylene-diamines are easily oxidized in alkaline solutions and has to be desorbed with acidic solutions containing EDTA to remove metals that promote oxidation. These solutions are best determined by HPLC as described in OSHA 87. 2. The media is desorbed with an alkaline solution and extracted into toluene to be analyzed with GC-MS without derivatization. 3. Easily oxidized; protect from UV light 4. The 226-98 phosphoric acid treated sampler cannot be used for pyrroles because the acid catalyzes breakdown and/or polymerization of this highly electrophilic com-pound. The di-n-butyl amine on the 226-153 sampler acts as a stabilizer. Pyrrole and its alkyl derivatives do not need derivatization and can be desorbed directly in ethyl acetate and analyzed as-is.

7 working day TAT 3 sample minimum

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1-800-356-9135

Analyte Method Instrument Medium TAT Fee($) Bulk Asbestos NIOSH 9002

(Mod) PLM Bulk 30

Bulk Asbestos NIOSH 9002 (Mod)

PLM Bulk 60

Asbestos in Air NIOSH 7400 (Mod)

PCM MCE Filter 20

Asbestos in Air NIOSH 7400 (Mod)

PCM MCE Filter 40

Asbestos/Total Fibers

Diesel Particulate (Elemental Carbon)

Analyte Method Instrument Medium Fee($)

Organic Carbon/Elemental Carbon NIOSH 5040 TOA Treated Quartz Fiber Filter 70

Organic Carbon/Elemental Carbon (Acid treatment for removal of carbo-naceous material)

NIOSH 5040 TOA Treated Quartz Fiber Filter 120

SECTION 6: Quaternary Amines

ALS analyzes benzyl and ethylbenzyl ammonium chloride as well as di-alkyl-dimethylammonium chloride quaternary amine classes by GC-MS using on-column pyrolysis. Table 8 is not inclusive, please inquire about other quaternary amines. Wipe sampling should be done in 2”x2” Cotton gauze, pre-extracted, wetted with Methanol and shipped in polypropylene or glass containers,. Table 8. Quaternary amines by GC-MS

Analyte Method Instrum Medium Notes Fee($)

Benzalkonium Chloride ALS Method GC-MS 37mm QFF, 2”x2” cot- * Quote

Ethylbenzalkonium Chloride ALS Method GC-MS 37mm QFF, 2”x2” cot- * Quote

Didecyldimethylammonium chlo-ride (DDAC)

ALS Method GC-MS 37mm QFF, 2”x2” cot-ton gauze

* Quote

* Please contact ALS for information on sampling and analytical capability

SECTION 7: Other Amines

Table 9. Amines analyzed by procures that do not fit in other sections

Analyte Method Instrument Medium Notes Fee($)

Triethanolamine PV2141 Mod. GC-MS SKC 225-701 150

Nicotine NIOSH 2551 Mod. GC-MS SKC 226-93 1 85

Cotinine NIOSH 2551 Mod. GC-MS SKC 226-93 1 Quote

N-Methyl morpholine ALS Method GC-FID SKC 226-98 Quote

N-Ethyl morpholine ALS Method GC-FID SKC 226-98 Quote

Trimethylamine OSHA PV2060 LC-MS SKC 226-98 165/35*

Triethylamine OSHA PV2060 LC-MS SKC 226-98 165/35*

N,N-Dimethylethylamine OSHA PV2096 LC-MS SKC 226-98 2 165/35*

1. Nicotine and Cotinine are cyclic alkyl amines analyzed by NIOSH 2551 modified. 2. PV2096 calls for alumina tube samplers which ALS substitutes with the 226-98 sampler.

7 working day TAT 3 sample minimum

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 23

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Gravimetric

Analyte Method Instrument Medium Fee($)

Total Dust NIOSH 0500 Microbalance PVC, 5µm, matched weight 20

Respirable Dust NIOSH 0600 Microbalance PVC, 5µm, matched weight 20

PM 10 40 CFR 50 APP Microbalance QFF, 8”x10”, pre-weighed 40

Indoor Air Quality (VOCs) Analyte List (pg 29)

Analyte Method Instrument Medium Fee($)

Volatile Organics EPA TO-15 GC-MS SUMMA/Tedlar Bag/HDS 250

Media rental fees See pg 40

Volatile Organics1 EPA TO-17 (Mod) Semi-quantitative

GC-MS Supelco Carbotrap 300 Tube 250

Media rental fees See pg 40

Volatile Organics2 (Passive Monitoring)

EPA TO-17 (Mod) Semi-quantitative

GC-MS Supelco Radiello -145 passive sam-pler

250

Note: For gravimetric determinations, ALS recommends matched weight filters. If tared filters are used ALS recommends that filters be utilized within six months of their tare weight determination.

1 In addition to the compounds listed above, a National Institute of Standards and Technology (NIST) database search will be performed and significant TICs (Tentatively Identified Compounds) will be reported from a library of over 75,000 com-pounds. Contact ALS customer service for more information.

2 Sampling rates for passive monitors not determined for all compounds.

Lead and Beryllium

Analyte Method Instrument Medium Fee($) Lead NIOSH 7300 (Mod) ICP MCE Cassette/Paint/Wipe/Bulk 20

Lead 40 CFR 50 APP G ICP 8 X 10 Glass Fiber Filter 50

Beryllium NIOSH 7300/7303 ICP MCE Cassette/Wipe 50

Beryllium Oxide NIOSH 7300 (Mod) ICP MCE Cassette/Wipe 70

Light Hydrocarbons (GC-FID) Analyte List (pg 29)

Analyte Method Instrument Medium Fee($)

Light Hydrocarbons (9 Analyte Panel) ALS GC-FID Tedlar Air Bag or Summa 220

Single Analyte/Additional Analyte ALS GC-FID Tedlar Air Bag or Summa 80/50*

Fixed Gas Scan (5 Analyte Panel) ALS GC-FID Tedlar Air Bag or Summa 220

Analyte Method Instrument Medium Fee($)

Metals Panel A (15 Metals) NIOSH 7300/7303 (Mod) ICP MCE Cassette/Wipe/Bulk 105

Metals Panel B (27 Metals, full list) NIOSH 7300/7303 (Mod) ICP MCE Cassette/Wipe/Bulk 125

Metals Panel C (7 RCRA Metals) NIOSH 7300/7303 (Mod) ICP MCE Cassette/Wipe/Bulk 105

Metals Panel D (8 Metals, welding fume specific)

NIOSH 7300/7303 (Mod) ICP MCE Cassette/Wipe/Bulk 105

Specific Metals from full list ( Panel B) NIOSH 7300/7303 (Mod) ICP MCE Cassette/Wipe/Bulk 50/20*

Metals ALS ICP-MS MCE Cassette/Wipe/Bulk Quote

Metals Analyte List (pg 29)

Note: Additional fee may be charged for non-routine mediums. Please call 1-800-356-9135 for information about recommended media types.

Page 24 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Analyte Method Instrument Medium TAT & Fee($)

Methamphetamine (only) wipe

NIOSH 9111 (Mod)

LC-MS Cotton gauze 50 4 day TAT

100 1 day TAT

Methamphetamine (only) water/soil NIOSH 9111 (Mod)

LC-MS Water—250 mL HDPE Soil—4 oz glass

70/95 14 day TAT

Tetrahydrocannabinol (THC active drug)

ALS LC-MS Wipe 85 5 day TAT

Selected Illicit drugs ALS LC-MS or GC-MS

Wipe Quote

Methamphetamine, Illicit Drugs and Related Compounds Analyte List (pg 29)

1-800-356-9135

Option Analyte Method Instrument TAT Fee

1 Pesticides and/or Herbicides NIOSH 5600 (Mod) or NIOSH 5605 GC-MS See Note Quote

2 Pesticides and/or Herbicides NIOSH 5602 GC-MS See Note Quote

3 Pesticides by HPLC NIOSH 5601 HPLC See Note Quote

4 Pesticides and Herbicides NIOSH 5601 (Mod) LC-MS See Note Quote

Note: Comprehensive Pesticide Screen: The classes of pesticides that have a reasonable expectation of being detected by this proce-dure are organophosphorus, organochlorine, pyrethroid, triazole fungicides, most organonitrogen pesticides, and some herbicides such as triazenes (atrazine, propazine, simazine). Pesticides and fungicides that cannot be detected by this procedure include inorganics (arsenic and tin compounds), dithiocarbamates (maneb, mancozeb, etc.), acid herbicides (2,4-D, dicamba, etc.), and most carbamate insecticides. For these classes of compounds, refer to methods listed above or call for quote.

Note: Comprehensive Herbicide Screen: The classes of pesticides that have a reasonable expectation of being detected by this proce-dure are nitro- and chlorinated phenols (e.g., trichlorophenol, pentachlorophenol, dinoseb), most benzoic acid herbicides (e.g., dicamba), and phenoxyacetic acid and related herbicides and their esters (e.g., 2,4-D, 2,4-DB, 2,4,5-T, dichlorprop, MCPA, mecoprop, Silvex, etc.), triazenes (atrazine, propazine, simazine), bromacil, many N-arylcarbamates, and many more. Herbicides that cannot be detected by this procedure include inorganics (arsenic compounds), glyphosate (Roundup™), quaternary amines (paraquat and diquat), sulfonylureas, and most substituted ureas. For these classes of compounds, refer to methods listed above or call for quote.

Analyte Method Instrument Fee($)

Comprehensive Pesticide Screen (semi- ALS Method on SKC 226-58 GC-MS 600

Comprehensive Herbicide Screen (semi- ALS Method on SKC 226-58 GC-MS 600

TAT

14 days

14 days

ALS Sampling Recommendations: Unless otherwise specified in the method, ALS recommends the use of SKC 226-58 OVS-2 tubes for most pesticide and herbicide air sampling. Sample at 0.1 to 1 liter/minute for up to 8 hours. For wipe samples use pre-cleaned cotton gauze moistened with either 100% isopropanol or methanol. Ghost Wipes wetted with water cannot be used for pesticides or drugs.

Note: Prices and TATs quoted are dependent on the complexity of the analysis of the individual Pesticide and/or Herbicide. Analytes can be grouped to be analyzed with like analytes in single runs at a single quoted price. Contact your project manager for more information and to coordinate your sampling plan.

ALS Salt Lake City (ALS-SLC) offers an extensive list of over 600 Pesticides and/or Herbicides for analysis. Many methods of analyses were developed in-house while under contract with the National Institute for Occupational Safety and Health (NIOSH), some fully validated, and many partially evaluated or validated. ALS-SLC’s expertise with pesticides method development is unmatched in the industry.

Pesticides and Herbicides Analyte List (pgs 31-33)

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 25

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Polynuclear Aromatic Hydrocarbons (PAHs) Analyte List (pg 29)

Analyte Method Instrument Medium Fee($)

PCBs NIOSH 5503 GC-ECD Wipe/Filter/Florisil Tube/Oil/Bulk 100

Polychlorinated Biphenyls (PCBs) Analyte List (pg IH - 28)

Analyte Method Instrument Medium Fee($)

PAHs NIOSH 5528 (Draft)3 GC-MS-SIM OVS, XAD-74 SKC 226-57 100/35*; 255†

Analyte Method Instrument Medium Fee($)

Sulfur Gases (Full List of 14 compounds) ALS GC-SCD Tedlar Air Bag or SUMMA/SilcoCan Canister

250

Sulfur Gases (Specific Analytes Chosen from List)

ALS GC-SCD Tedlar Air Bag or SUMMA/SilcoCan Canister

100/50*

SO2 (semi-quantitative) ALS GC-SCD Tedlar Air Bag or SUMMA/SilcoCan Canister

100

Sulfur Gases (Extended List of 20 com-pounds)

ALS GC-SCD Tedlar Air Bag or SUMMA/SilcoCan Canister

320

Analyte Method Instrument Medium Fee($)

Volatiles (Selected list up to 7 com-pounds)

TO-15 GC-MS SIM Tedlar Air Bag or SUMMA Canister 320

Analyte Method Instrument Medium Fee($)

Volatiles (SUMMA/Silco Canisters) Analyte list (pg 29)

GC-MS SUMMA Canister 250

Volatiles (Carbotrap Tubes) Analyte list (pg 29) GC-MS Supelco Carbotrap 300 Tube/ Radiello 145 Pas-sive Badge

250

Sulfur Gases Analyte List (pg 29)

Vapor Intrusion Analyte List (pg 29)

Toxic Organic Methods (EPA)

Solvent Panel-Low Level Indoor Air Quality Analyte List (pg 29)

Analyte Method Instrument Medium Fee($) Quartz6 NIOSH 7500 (Mod) XRD PVC, 5µm 50**

Quartz,6 Cristobalite NIOSH 7500 (Mod) XRD PVC, 5µm 60**

Quartz,6 Cristobalite, Tridymite NIOSH 7500 (Mod) XRD PVC, 5µm 70** Quartz NIOSH 7500 (Mod) XRD Bulk Material 145

15 day TAT Quartz, Cristobalite NIOSH 7500 (Mod) XRD Bulk Material 160

15 day TAT Quartz, Cristobalite, Tridymite NIOSH 7500 (Mod) XRD Bulk Material 175

15 day TAT

Silica (Crystalline)

Analyte Method Instrument Medium Fee($) Full Scan (60) with 5 highest TICs (Tentatively Identified Compounds)

ALS SOP GC-MS Charcoal 226-01 or SKC 575-001 Passive Monitor

195

GC/MS confirmation of GC Analyte ALS SOP GC-MS Quote

GC/MS or LC/MS Custom Analyses ALS SOP GC-MS Quote

Note: Analysis is performed by mass spectrometry which ensures positive identification. Full calibration provides quantitative results for all compounds. Identification of unknown compounds not listed is available at an additional charge of $10 per compound. Contact ALS customer service for information.

Page 26 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Footnotes Legend:

First analyte on a sample/additional analyte on same sample ** Samples collected on non-standard media (i.e. MCE filters) will be subject to a $25 sur-

charge for additional sample preparation fees. Note: Samples having particulate weights that exceed the method-specified maxi-

mum filter loading will be subject to surcharges for additional sample preparation and analysis fees: Filters with

particulate weights exceeding 2 mg will be assessed an additional $25. Filters with par-ticulate weights exceeding 7 mg will be processed as a billable bulk sample at the appli-cable bulk price.

† Fee for complete panel 3 Improved NIOSH method for collection and analysis 4 Validation studies demonstrate excellent retention and no breakthrough for listed PAH compounds 5 Not recommended for naphthalene or other low molecular weight PAH 6 Total weight measurement should also be requested to calculate OSHA PEL

When submitting samples for analysis, please note that many analyses require a three sample minimum fee to cover the costs of method setup. Please inquire as to which analyses require this minimum.

1-800-356-9135

“For special criteria parameters like DoD/DOE QSM a surcharge of 10% may apply.”

Test Catalog & Fee Schedule Page 27

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NOTES

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Analyte & Panel Lists for Common Industrial Hygiene Methods

Acetaldehyde Formaldehyde Isovaleraldehyde Crotonaldehyde m,p-Tolualdehyde Acrolein Acetone Propionaldehyde Benzaldehyde 2,5-Dimethylaldehyde Butyraldehyde Hexanal Valeraldehyde o-Tolualdehyde

Aldehydes

EPA TO-15, 17 (Mod): Indoor Air Quality (VOCs)

Acetone Chloroform cis-1,2-Dichloroethene Hexachloro-1,3-butadiene Toluene Benzene Chloromethane trans-1,2-Dichloroethene n-Hexane 1,2,4-Trichlorobenzene Benzyl chloride Cyclohexane 1,2-Dichloropropane 2-Hexanone 1,1,1-Trichloroethane Bromodichloromethane Dibromochloromethane cis-1,3-Dichlorpropene Methyl t-butyl ether 1,1,2-Trichloroethane Bromoform 1,2-Dibromoethane trans-1,3-Dichloropropene 4-Methyl-2-pentanone (MIBK) Trichloroethene Bromomethane m-Dichlorobenzene Ethyl acetate Methylene chloride 1,2,4-Trimethylbenzene 1,3-Butadiene o-Dichlorobenzene Ethyl benzene Propene 1,3,5-Trimethylbenzene 2-Butanone p-Dichlorobenzene 4-Ethyl toluene Styrene Vinyl acetate Carbon disulfide Dichlorodifluoromethane Freon 11 1,1,2,2-Tetrachloroethane Vinyl chloride Carbon tetrachloride 1,1-Dichloroethane Freon 113 Tetrachloroethene m,p-Xylene Chlorobenzene 1,2-Dichloroethane Freon 114 Tetrahydrofuran o-Xylene Chloroethane 1,1-Dichloroethene Heptane

In addition to the compounds listed above, a National Institute of Standards and Technology (NIST) database search will be performed and significant TICs (Tentatively Identified Compounds) will be reported from a library of over 75,000 compounds. Contact ALS customer service for more information.

Panel A Aluminum Cadmium Copper Manganese Silver Arsenic Calcium Iron Nickel Sodium Beryllium Chromium Lead Selenium Zinc

Panel B Aluminum Chromium Magnesium Silver Yttrium* Arsenic Cobalt Manganese Sodium Zinc Barium Copper Molybdenum Tellurium Zirconium* Beryllium Iron Nickel Thallium Cadmium Lead Phosphorus Titanium Calcium Lithium Selenium Vanadium

Panel C—RCRA Metals

Arsenic Barium

Cadmium Chromium

Lead Selenium

Silver

Panel D—Welding Fumes

Cadmium Copper Manganese Silver

Chromium Iron Nickel Zinc

* not available for ICP-MS analysis

Metals Lists and Panels NIOSH 7300/7303 (Mod): Standard metals panels are offered for analysis by ICP-AES. Analysis by ICP-MS may be available upon request—please consult an ALS Project Manager for a quotation.

Note: Additional fees may be charged for non-routine mediums. Please call 1-800-356-9135 for information about recommended media types.

Light Hydrocarbons (GC-FID)

Methane Propane Propylene

Ethane n-Butane n-Pentane

Isobutene

Isopentane

Ethylene

Acids (Inorganic) Hydrobromic Acid Hydrofluoric Acid Phosphoric Acid Hydrochloric Acid Nitric Acid Sulfuric Acid

1-800-356-9135

Fixed Gas Scan (GC-FID)

Carbon Monoxide Carbon Dioxide Methane Nitrogen Oxygen

Acids (Organic)

LC-MS (panel of 3): Butyric Pentanoic Propanoic LC-MS (panel of 8): Citric Fumaric Malic Succinic Glycolic Lactic Malonic Tartaric

Isocyanates

Monomers

MDI 2.4-TDI 2,6-TDI HDI IPDI HMDI

Oligomers

MDI trimer HDI dimer HDI trimer HDI biuret

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 29

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Analyte & Panel Lists (cont.)

Amphetamine Chlorpheniramine Hydrocodone Methadone Oxazepam Acetaminophen Cocaine Hydromorphone Methamphetamine Oxycodone 6-Acetyl morphine Codeine Ketamine Methaqualone Phencyclidine (PCP) Aminorex Dextromethorphan Lidocaine Methcathinone Phenethylamine Atropine Diazepam LSD 4-Methylaminorex Phentermine Barbiturates Diphenhydramine MBDB Methoxyamphetamine, 4-(PMMA) Pseudoephedrine BDB Ecgonine, methyl ester MDA (ecstasy analog) Methyl phenidate (Ritalin) THC Benzyl piperazine Ephedrine MDEA (ecstasy analog) Morphine Tramadol 4-Bromo-2, 5-DMPEA Fenfluramine MDMA (ecstasy) N-Ethyl amphetamine Trifluoromethylphenyl piperazine Caffeine Fentanyl Melatonin N,N-Dimethyltryptamine Cathine (norpseudoephedrine) Flunitrazepam Meperidine Norephedrine (Phenyl propanol amine) Cathinone Heroin Mescaline Norspseudoephedrine

Methamphetamine, Illicit Drugs and Related

Polychlorinated Biphenyls (PCBs) (Aroclors)

Aroclor 1016 Aroclor 1232 Aroclor 1248 Aroclor 1260 Aroclor 1221 Aroclor 1242 Aroclor 1254 Aroclor 1262

Aroclor 1268

Polynuclear Aromatic Hydrocarbons (PAHs)

Acenaphthene Benzo[b]fluoranthene Chrysene Indeno[1,2,3-cd]pyrene Acenaphthylene Benzo[k]fluoranthene Dibenz[a,h]anthracene Naphthalene Anthracene Benzo[g,h,i]perylene Fluoranthene Phenanthrene Benz[a]anthracene Benzo[a]pyrene Fluorene Pyrene

Solvent Panel-Low Level Indoor Air Quality 1,1,1,2-Tetrachloroethane 2&4-Chlorotoluene Hexachloro-1,3-butadiene m,p-Xylene 1,1,1-Trichloroethane 2-Hexanone Hexachloroethane n-Butylbenzene 1,1,2,2-Tetrachloroethane Benzene Methyl acrylate n-Decane 1,1,2-Trichloroethane Bromobenzene Methyl ethyl ketone n-Hexane 1,2,3-Trichlorobenzene Bromochloromethane Methyl isobutyl ketone n-Octane 1,2,4-Trichlorobenzene Bromoform Naphthalene n-Propylbenzene 1,2,4-Trimethylbenzene Carbon tetrachloride Nitrobenzene n-Undecane 1,2-Dibromo-3-Chloropropane Chlorobenzene Nonane o-Xylene 1,2-Dibromoethane Chloroform Pentachloroethane p-Isopropyltoluene 1,2-Dichlorobenzene Cumene Styrene sec-Butylbenzene 1,2-Dichloroethane Dibromochloromethane Tetrachloroethene tert-Butylbenzene 1,2-Dichloropropane Dibromomethane Tetrahydrofuran trans-1,3-Dichloropropene 1,3,5-Trimethylbenzene Dodecane Toluene 1,3-Dichlorobenzene Ethyl benzene Trichloroethene 1,3-Dichloropropane Ethyl methacrylate cis-1,2-Dichloroethene 1,4-Dichlorobenzene Heptane cis-1,3-Dichloropropene

Sulfur Gases

n-Butyl mercaptan Diethyl sulfide Hydrogen sulfide Tetrahydrothiophene t-Butyl mercaptan Dimethyl sulfide Isopropyl mercaptan Thiophene Carbon disulfide Dimethyl disulfide Methyl mercaptan Carbonyl sulfide Ethyl Mercaptan n-Propyl mercaptan

Additional Sulfur Compounds

Diethyl Disulfide Ethyl methyl sulfide Isobutyl mercaptan

2,5-Dimethylthiophene 2-Ethylthiophene 3-Methylthiophene

1,3-Dinitrobenzene 1,3,5-Trinitrobenzene 2-Amino-4,6-Dinitrotoluene 2-Nitrotoluene 2,4-Dinitrotoluene 2,4,6-Trinitrotoluene

2,6-Dinitrotoluene 3-Nitrotoluene 3, 5-Dinitroaniline 4-Amino-2,6-Dinitrotoluene 4-Nitrotoluene HMX

Nitrobenzene RDX Tetryl Nitroglycerine PETN

Nitroaromatics (8330 list)

Page 30 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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Pesticides and Herbicides (Air and Wipes)

1-800-356-9135

2,3,5-Trichlorophenol Benomyl (as Carbendazim) Chlorfenapyr DDD, 4,4'- (DDD, p,p'-) (TDE) 2,4,5-T acid and salts Bensulfuron-methyl Chlorfenvinphos (Supona®) DDE, 2,4'- (DDE, o,p'-) 2,4,5-T, Butyl and other esters Bensulide (Betasan) Chlorfurenol DDE, 4,4'- (DDE, p,p'-) 2,4,5-Trichlorophenol Bentazon Chlorfurenol, methyl DDT, 2,4'- (DDT, o,p'-) 2,4,6-Trichlorophenol Benthiazole (TCMBT) Chloridazon, (Pyrazon) DDT, 4,4'- (DDT, p,p'-) 2,4,D, Butyl ester Benzofenap Chlorimuron-ethyl Deltamethrin 2,4,D, Isooctyl ester Benzothiazole Chlorobenzilate (Acaraben) Demeton O&S (Systox) 2,4,D-Acids and salts Bethoxazin Chloroneb (Demosan) Demeton-O-methyl 2,4-D, Butoxyethyl ester BHC Chlorophacinone (Rozol) Demeton-S-methyl 2,4-D, Ethylhexyl ester BHC, alpha- Chlorophene Desmedipham 2,4-D, Isopropyl ester BHC, beta- Chloropicrin (Trichloronitromethane) Dialifos (Torak) 2,4-DB BHC, delta- Chlorothalonil (Daconil®) Diallate (Di-Allate) 2,4-DB butoxyethyl ester Bifenazate Chlorotoluron Diazinon 2.3.4.5-Tetrachlorophenol Bifenox Chloroxuron Dicamba 2-Phenethyl propionate Bifenthrin Chloroxylenol Dichlobenil (Casoron) 3-chloro-p-toluidine hydrochloride Bioallethrin (d-trans-allethrin) Chlorpropham Dichlofenthion 3-Trifluoromethyl-4-nitrophenol Bioresmethrin Chlorpyrifos (Dursban) Dichlofluanid 4-Aminopyridine (Avitrol 200) Biphenyl (Diphenyl) Chlorpyrifos-methyl Dichlone 4-CPA Bispyribac-sodium Chlorsulfuron Dichlorfurenol-methyl Abamectin (Avermectins) Boscalid Chlorthal-dimethyl (Dacthal) Dichlormid Acephate (Orthene) Brodiafcoum Chlozolinate Dichlorprop Acequinocyl Bromacil Cholecalciferol Dichlorprop, isooctyl ester Acetamiprid Bromadiolone Cinmethalin Dichlorvos (DDVP) Acetochlor Bromethalin Citronellol Diclofop-methyl Acibenzolar-S-methyl Bromophos (Bromophos-methyl) Clethodim Dicloran (Botran) (DCNA) Acifluorfen Bromophos-ethyl Clodinafop-propargyl Diclosulam Alachlor (Lasso) Bromopropylate Clofentezine Dicofol (Kelthane®) Aldicarb (Temik) Bromoxynil Clomazone (Dimethazone, Command®) Dicrotophos (Bidrin®) Aldoxycarb Bromoxynil heptanoate Clonitralid Dieldrin Aldrin Bromoxynil octanoate Clopyralid (Lontrel®) Dienochlor (Pentac) Allethrin Bromuconazol Cloransulam-methyl Diethatyl-ethyl Allethrin, D- (Pynamin-forte) Buprofezin Clothianidin Difenacoum

Allidochlor (CDAA) Butachlor (Machete) Coumaphos (Co-Ral) Difenoconazole Ametryn Butralin Crimidine Difenzoquat Amicarbazone (a triazolone) Butylate Crufomate Difethialone Aminocarb Captafol (Difolatan) Curelure, 4-(3-Oxobutyl)phenoxy acetate Diflubenzuron Aminocyclopyrachlor Captan Cyanazine (Bladex) Diflufenzopyr Aminopyralid Carbaryl (Sevin®) Cyanophos Dikegulac sodium, acid Amitraz (look for dimethylamine) Carbendazim Cyazofamid Dimethenamid Amitrole Carbofuran (Furadan) Cybutryne (Irgarol) Dimethirimol Ancymidol Carbophenothion Cyclanilide Dimethoate (Cygon) Anilazine Carbosulfan Cycloate Dimethomorph ANTU Carboxin Cyfluthrin (Baythroid®) Diniconazole Asulam Carfentazone-ethyl Cyhalofop-butyl Dinitramine Atrazine Chinomethionate (Oxythioquinox) Cyhalothrin, gamma Dinocap Azadirachtin Chloramben Cyhalothrin, lambda Dinoseb Azimsulfuron Chlorantraniliprole Cymoxanil Dinotefuran Azinphos methyl (Guthion®) Chlorbenside Cypermethrin Dioxacarb Azinphos-ethyl Chlorbromuron Cyphenothrin Dioxathion (Delnav) Azoxystrobin Chlordane, alpha- (cis-) Cyproconazole Diphacinone Barban Chlordane, gamma- (trans-) Cyprodinil Diphenylamine Benalaxyl Chlordane, technical- Cyromazine Dipropetryn Bendiocarb (Ficam ) Chlordecone (kepone) Dalapon Diquat (Diquat dibromide) Benfluralin (Balan, Benefin) Chlorethoxyfos Daminozide Disulfoton (Di-Syston®) Benodanil Chlorfenac sodium DDD, 2,4'- (DDD, o,p'-) Dithianon

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 31

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Pesticides and Herbicides ( Air and Wipes Cont.)

Dithiopyr Flamprop-methyl Hydroprene Methabenzthiazuron Diuron Flazasulfuron Hydroxyquinoline (Quinolinol) Methacrifos DNOC (Dinitro-o-cresol) Flonicamid Hymexazol (pH 5.92) Methamidophos (Monitor®) Dodemorph Florasulam Imazalil Methazole Emamectin benzoate Fluazifop-p-butyl Imazamethabenz-methyl Methidathion Endosulfan (Thiodan) Fluazinam Imazamox Methiocarb Endosulfan sulfate Flubendiamide Imazapic Methomyl Endosulfan-I (alpha- ) Flucarbazone-sodium Imazapyr Methoprene Endosulfan-II (beta- ) Fluchloralin Imazaquin Methoxychlor, p,p'- Endothall Flucythrinate Imazethapyr Methoxychlor-olefin Endrin Fludioxonil Imazosulfuron Methoxyfenozide Endrin aldehyde Flufenacet Imidacloprid (Admire®) Methyl eugenol Endrin ketone Flufenpyr-ethyl Imiprothrin Metofluthrin EPN Flumetralin Indaziflam Metolachlor (Dual) EPTC (Eptam®) Flumetsulam Indoxacarb Metrafenone Esfenvalerate Flumiclorac-pentyl Iodocarb (Iodopropynyl butylcarbonate) Metribuzin (Sencor) Ethalfluralin (Sonalan) Flumioxazin Iodosulfuron-methyl-sodium Metsulfuron-methyl Ethametsulfuron-methyl Fluometuron Ipconazole Mevinphos (Phosdrin) Ethephon Fluopicolide Iprodione Mexacarbate (Zectran®) Ethion Fluoxastrobin Isazofos MGK-264 (Octacide-264) Ethiprole Flupyrsulfuron-methyl Isodrin MGK-326 (Dipropyl isocinchomeronate) Ethofumasate Flurenol-methyl Isofenphos (Oftanol) Mirex Ethoprop (Ethoprophos, Mocap) Fluridone (Fluridon) Isopropalin Molinate Ethoxyquin Fluroxypyr (Fluoroxypyr) Isoproturon Monocrotophos (Azodrin) Ethylan (Perthane) Fluroxypyr, 1-methylheptyl ester Isoxaben Monolinuron Etofenprox (Ethofenprox) Flurprimidol Isoxaflutole Monuron Etoxazole Flusilazole Kinoprene Myclobutanil Etridiazole (Terrazole™) Fluthiacet-methyl Kresoxim-methyl Naled (Dibrom®) Etrimphos (Etrimfos) Flutolanil Lactofen Naphthalene Eugenol Flutriafol Lenacil Naphthaleneacetamide, 1- Famoxadone Fluvalinate, tau- (Mavrik®) Leptophos (Phosvel) Naphthaleneacetic acid Famphur (Famophos) Folpet Lindane (gamma-BHC) Napropamide Fenamidone Fomesafen Linuron Naptalam Fenamiphos (Nemacur®) Fonofos (Dyfonate®) Lufenuron Neburon Fenarimol Foramsulfuron Malaoxon Nicarbazin Fenazaquin Forchlorfenuron Malathion Niclosamide Fenbuconazol (Fenethanil) Formetanate Maleic hydrazide Nicosulfuron Fenchlorphos (Ronnel) Fosamine, sodium Mandipropamid Nicotine Fenfuram Fosetyl-al MCPA Nitrapyrin Fenhexamide Fosthiazate (OPP) MCPA, ethyhexyl ester Nitrofen Fenitrothion Glufosinate ammonium MCPA, isooctyl ester Nonachlor, cis- Fenoxaprop-ethyl Glyphosate (Round-up) MCPB Nonachlor, trans- Fenoxycarb Halofenozide Mecarbam Norflurazon Fenpropathrin Halosulfuron-methyl Mecoprop (MCPP) Novaluron Fenpropimorph Haloxyfop-methyl Mecoprop-P, as Mecoprop Noviflumuron Fenpyroximate Heptachlor Mefluidide Octhilinone (2-Octyl-4-isothiazolin-3-one) Fensulfothion (Dansanit) Heptachlor endo-epoxide (A) Mercaptobenzothiazole Omethoate Fenthion Heptachlor exo-epoxide (B) Merphos Orthosulfamuron Fenuron Hexachlorobenzene Mesosulfuron-methyl Oryzalin (Surflan®) Fenvalerate Hexachlorophene Mesotrione Oxadiazon Fipronil Hexaconazole Metaflumizone Oxadixyl Fipronil desulfinyl (Fipronil breakdown) Hexaflumuron Metalaxyl (Apron) Oxamyl (Vydate) Fipronil sulfide (Fipronil breakdown) Hexazinone (Velpar®) Metalaxyl-M (Mefenoxam) Oxycarboxin (Plantvax®) Fipronil sulfone (Fipronil breakdown) Hexythiazox Metamitron Oxychlordane Flamprop-isopropyl Hydramethylnon (Amdro) Metconazole Oxydemeton-methyl

Page 32 Test Catalog & Fee Schedule Note: See Footnotes on Page 27

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1-800-356-9135

Oxyfluorfen Propiconazole (Tilt®) Tebufenpyrad Triflumuron Oxytetracycline Propoxur (Baygon®) Tebupirimfos (Phostebupirim) Trifluralin Paclobutrazol Propoxycarbazone-sodium Tebuthiuron Triflusulfuron Paraquat Propyzamide (Pronamide, Kerb) Tecnazene Triflusulfuron-methyl Parathion Prosulfuron Tefluthrin Triforine Parathion-methyl (Methyl Parathion) Prothioconazole Tembotrione Trimethacarb (Landrin) Pebulate Prothioconazole-desthio Temephos (Abate®) Trinexapac-ethyl Pendimethalin (Prowl®) Prothiofos (Tokuthion®) TEPP (Tetraethyl pyrophosphate) Triticonazole Penoxsulam Pymetrozin Tepraloxydim Uniconazole-P Pentachloroaniline Pyraclofos Terbacil Verbenone Pentachlorobenzene Pyraclostrobin Terbufos (Counter®) Vernolate Pentachlorophenol Pyraflufen-ethyl Terbuthylazine Vinclozolin Pentachlorothiophenol Pyrasulfotole Terbutryn Warfarin Perfluidone Pyrazophos Tetrachlorvinphos (Stirofos) E and Z Zoxamide Permethrin (cis- and trans-) Pyrazoxyfen Tetraconazole Permethrin, cis- Pyrethrum ("Pyrethrins") Tetradifon Permethrin, trans- Pyridaben Tetrahydrophthalimide (Captan, Captafol brkdwn) Phenmedipham Pyridalyl Tetramethrin Phenothrin (Sumithrin®) Pyridate Thiabendazole Phenthoate Pyrimethanil Thiacloprid (Calypso) Phenylethyl propionate Pyriproxyfen Thiamethoxam Phenylphenol, ortho- (Hydroxybiphenyl) Pyrithiobac (CAS is for sodium salt) Thiazopyr Phorate (Thimet®) Pyroxsulam Thidiazuron Phosalone (Zolone®) Quinalphos Thiencarbazone-methyl Phosfolan Quinclorac Thifensulfuron-methyl Phosmet (Imidan®) Quinoxyfen Thiobencarb (Benthiocarb) Phosphamidon Quintozene (PCNB) Thiodicarb Picaridin (Icaridin) Quizalofop-ethyl Thionazin (Zinophos®) Picloram (Tordon) Resmethrin Thiophanate Pindone Rimsulfuron Thiophanate-methyl Pinoxaden (Axial) Rotenone Tolclofos-methyl Piperalin (Pipron®) S-421 (Octachlorodipropyl ether) Tolfenpyrad Piperonyl butoxide Saflufenacil Tolyfluanid Pirimicarb (Pirimor) Secbumeton Topramezone Pirimicarb-desmethyl Sethoxydim Toxaphene (Chlorinated camphene) Pirimiphos-ethyl Siduron Tralkoxidim Pirimiphos-methyl Silvex (2,4,5-TP) Tralomethrin Prallethrin Simazine Tralopyril Primisulfuron-methyl Simetryn Transfluthrin Prochloraz Spinetoram Triadimefon (Bayleton®) Procymidone Spinosad (A and D) Triadimenol (Baytan®) Prodiamine Spirodiclofen Tri-allate Profenofos (Curacron®) Spiromesifen Triasulfuron Profluralin Spirotetramat Triazophos Prohexadione calcium Spiroxamine Tribenuron-methyl Promecarb Strychnine Tribufos (DEF) Prometon (Pramitol) Sulfentrazone Trichlorfon (Dylox) Prometryn Sulfluramid Trichloronate Propachlor (Ramrod) Sulfometuron-methyl Triclopyr (acid and salts) Propamocarb Sulfosulfuron Triclopyr, 2-Butoxyethyl ester Propanil Sulfotep (TEDP) Triclosan Propargite (Omite®) Sulprofos (Bolstar®) Tricyclazol Propazine SWEP Trifloxystrobin Propetamphos (Safrotin®) Tebuconazole (Folicur®) Trifloxysulfuron-sodium Propham Tebufenozide Triflumizole

Pesticides and Herbicides ( Air and Wipes Cont.)

Note: See Footnotes on Page 27 Test Catalog & Fee Schedule Page 33

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NOTES

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Test Catalog & Fee Schedule Page 35

Report Level Deliverable

IH1

Report Only

IH2

Report with QC

IH3 Report with Narrative &

QC

IH4 Full Report Raw Data

Case Narrative Required Required

Analytical Results Report with comments

Report with comments

Report with comments Report with comments

Client Documentation (CoC/ARF/Client Instructions) Required Required Required Required

QC Data QC Summary Report(s)

QC Summary Report(s)

QC Summary Report(s)

Instrument QC Summary

Deliverables

All Raw Data

Laboratory Write-ups

Digestion and Extraction Worksheets

Traceability Standards

Cost NA NA NA Quote

ALS Environmental—Salt Lake City Standard Industrial Hygiene Report Formats

1-800-356-9135

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NOTES

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SKC S T (All media is subject to availability and may require a minimum order)

NOTE: If large or 3-stage media collection tubes are selected, the cost of associated analysis doubles.

Tube Number (SKC) Description Treated Sorbent (mg) Cost ($)

226-01 Charcoal tube No 50/100 2

226-01 GWS Charcoal tube, Glass wool separator No 50/100 2

226-09 Charcoal tube No 200/400 2

226-09-02 Charcoal tube No 350/350/350 5

226-10 Silica gel tube No 75/150 2

226-10-03 Silica gel tube (Specially Cleaned) Yes 200/400 3

226-10-04 Silica gel tube No 150/300 3

226-10-06 Silica gel tube (Sulfuric acid) Yes 100/200 4

226-15 GWS Silica gel tube, Glass wool separator No 260/520 4

226-16 Anasorb CSC Charcoal No 800/200 3

226-17-1A Anasorb C300 (Comparable to Hopcalite) No 200 3

226-25 Charcoal (two tubes) No 200 and 400 5

226-27 XAD-2 (2-Hydroxymethyl piperidine) Yes 225/450 7

226-210 Soda Lime No 200/600 5

226-30-02 A XAD-2 (two tubes) No 300 and 600 15

226-30-04 XAD-2 tube No 50/100 3

226-30-05 XAD-2 tube No 75/150 4

226-30-06 XAD-2 tube No 200/400 5

226-30-07 XAD-2 tube (p-Anisidine) Yes 50/100 7

226-30-08 Anasorb 708 No 100 5

226-30-16 OVS (XAD-2, GFF) Yes 140/270 16

226-30-18 XAD-2 (Naphthylisothiocyanate) Yes 40/80 5

226-35-01 Tenax® tube No 10/20 6

226-35-03 Tenax® tube No 50/100 7

226-37 Charcoal (2 tubes) No 200 and 400 4

226-39 Florisil tube No 50/100 2

226-40A Molecular Sieve (2 tubes and oxidizer) Yes 400 ,400, 600 15

226-40-02 Molecular Sieve (triethanolamine) Yes 400/200 4

226-44 Drying tube No 250 3

226-51 Silica gel tube No 50/100 3

226-56 OVS (Tenax, GFF) tube No 70/140 25

226-57 OVS (XAD-7, GFF) tube No 100/200 19

226-58 OVS (XAD-2, QFF) tube No 140/270 20

226-59-04 Porapak-R No 35/70 4

226-67 Charcoal tube (Potassium Hydroxide) Yes 50/100 3

226-73 Charcoal tube (t-Butylcatechol) Yes 50/100 3

226-80 Anasorb 747 (Potassium Hydroxide) Yes 50/100 3

226-81A Anasorb 747 tube No 70/140 6

226-82 Anasorb 747 (2 tubes) No 200 and 400 5

226-55 Silica gel tube (sodium hydroxide) Yes 150/750 4

Media Available Through ALS Environmental—Salt Lake City Listed Media—generally in stock. Contact your Project Manager for ordering details.

Media Available Through ALS Environmental—Salt Lake City— Page 37

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Page 44: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Tube Number (SKC) Description Treated Sorbent (mg) Cost ($)

226-95 XAD-7 No 50/100 3

226-96 XAD-7 (Plus NBD Chloride) Yes 50/100 4

226-97 XAD-7 (2 tubes + 1 specially cleaned tube) No 175 14

226-98 XAD-7 (Phosphoric acid) Yes 40/80 3

226-107 Chromosorb-102 No 50/100 7

226-110 Chromosorb-106 No 50/100 9

226-111A Chromosorb-106 No 300/600 46

226-114 Porapak-P No 50/100 6

226-115 Porapak-Q No 75/150 5

226-116 A Porapak-T (2 tubes) No 25 and 75 16

226-117♦ XAD-2 tube (2-hydroxymethyl piperidine) Yes 75/150 6

226-118♦ XAD-2 tube (2-hydroxymethyl piperidine) Yes 60/120 6

226-119♦ Silica gel tube (DNPH) Yes 150/300 5

226-153♦ XAD-2 (di-n-Butylamine) Yes 400/200 9

226-178♦ Anasorb 747 (Hydrobromic acid) Yes 100/50 5

226-193 UC♦ Silica Gel (MTSO) Yes 800 10

226-196♦ Charcoal tube (t-butyl catechol) (require 10 working day lead time)

Yes 400/200 6

226-94 XAD-7 Yes 30/60 3

226-93 XAD-4 tube No 40/80 3

SKC I H F (A ) (All media is subject to availability and may require a minimum order)

Filter No. (SKC)

Description (Material, Pore Size, Cassette Type)

Treated

Size (mm)

Cost ($)

225-321A Mixed cellulose ester, 0.8 µm, black polypropylene cassette No 25 2

225-502 MCE, (matched weight), 0.8 µm, 2-piece No 37 5

225-503 MCE, (matched weight), 0.8 µm, 3-piece No 37 5

225-9001 MCE, (sodium carbonate) Yes 37 12

225-9002♦ Glass fiber, (1-(2-pyridyl) piperazine) Yes 37 11

225-9003♦ Glass fiber, 2 filters, (2,4-DNPH) Yes 37 12

225-9004 Glass fiber, (H2SO4) Yes 37 12

225-9005 MCE, cellulose, (sodium carbonate) Yes 37 14

225-9006 Cleaned silver membrane filter, black polypropylene cassette Yes 25 46

225-9014 Glass fiber, 2 filters, nitrite impregnated Yes 37 10

225-9018♦ Glass filter & polyester filter (Mercuric chloride treatment on polyester only)

Yes 37 18

225-9019 Glass fiber, 2 filters, (phosphoric acid & 2,4-dinitrophenylhydrazine) Yes 37 26

225-9020 Glass fiber, 3 filters, (phosphoric acid & 2,4-dinitrophenylhydrazine) Yes 37 23

225-9021 Glass fiber, (veratrylamine) Yes 37 22

225-709 1.0 µm, (binder-free, type AE), 2-piece No 37 3

225-9013 Glass fiber (1-(2-pyridyl) piperazine) Yes 37 12

225-9030♦ Quartz filter, (titanium oxysulfate hydrate) Yes 25 19

225-9031 Cellulose nitrate (Na2C03) Yes 37 27

225-9032 Quartz fiber (Na2C03) Yes 37 25

225-9033 Quartz fiber Yes 37 17

Media Available Through ALS Environmental—Salt Lake City— Page 38

♦ Requires Refrigeration

Page 45: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

I H F (A ALS-S L C ) Filter

Material Description

(Pore Size, Cassette Type, Manufacturer, Catalog #)

Preweighed Size (mm)

Cost ($)

PVC 5.0 µm, 2-piece, Zefon 7P52P No 37 4

PVC 5.0 µm, 3-piece, Zefon 7P53P No 37 4

PVC 5.0 µm, 2-piece (MW), Zefon 7M52P Yes 37 6

PVC 5.0 µm, 3-piece (MW), Zefon 7M53P Yes 37 6

PTFE 1.0 µm, 2-piece, Zefon 721TF No 37 6

PTFE 1.0 µm, 3-piece, SKC 225-1715 No 37 6

PTFE 2.0 µm, 2-piece, SKC 225-1713 No 37 5

MCE 0.8 µm, 2-piece, Zefon 728MCE No 37 2

MCE 0.8 µm, 3-piece, Zefon 738MCE No 37 2

MCE 0.8 µm, 2-piece (MW), SKC 225-502 Yes 37 5

QFF No pore size, heat-treated, 3-piece, SKC 225-401 No 37 6

GFF 1.0 µm, (binder-free, type AE), 2-piece, SKC 225-709 No 37 3

QFF & Tube Chloramine Treated Filter & Tube No 37 30

Respirable PPI (red) 8 L/min with pre-weighed 5.0µm PVC Filter, SKC 225-3841-PW Yes 37 32

Respirable PPI (gold) 2 L/min with pre-weighed 5.0µm PVC Filter, SKC 225-3851-PW Yes 37 32

Respirable PPI (orange) 4 L/min with pre-weighed 5.0µm PVC Filter, SKC 225-3871-PW Yes 37 32

Media Available Through ALS Environmental—Salt Lake City— Page 39

1-800-356-9135

P S Passive Sampler For: Description

(Manufacturer and Sorbent)

Catalog # Cost ($)

Organic Vapors (VOCs) SKC, Charcoal, 350 mg 575-001 16

Organic Vapors (VOCs) SKC, Anasorb 747, 500 mg 575-002 14

Ethylene Oxide SKC, Anasorb 747 treated with hydrobromic acid, 500 mg 575-005 25

Methanol SKC, Anasorb 747, 500 mg, includes secondary diffusion barrier 575-007 18

Mercury SKC, Anasorb C300 (also requires holder SKC 520-03 $40 ea) 520-02 7

Formaldehyde SKC, 2,4-DNPH treated UMEx100 treated tape UMEx 100 18

NO2/SO2 SKC, UMEx200 treated tape UMEx 200 18

Organic Vapors (VOCs) radiello™ Cartridge Adsorbents for sampling BTEX and VOCs (CS2 Desorption)

RAD130 18

Organic Vapors (VOCs) radiello™ Cartridge Adsorbents for sampling BTEX and VOCs (thermal desorption)

RAD145 68

To use with RAD130 radiello™ Diffusive Bodies, white, configured for general use RAD120 14

To use with RAD145 radiello™ Diffusive Bodies yellow, configured for reduced sam-pling rates

RAD1202 18

Required for using any radiello™ radiello™ Triangular Support Plate, rental fee RAD121 25

Optional for using any radiello™ radiello™ Vertical Adapter threaded for standard use, rental fee RAD122 7

Page 46: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

M M

Description Treated Size Cost

SKC 232-01 Tedlar Air Bag No 1 L 11

SKC 232-03 Tedlar Air Bag No 3 L 15

SKC 232-05 Tedlar Air Bag No 5 L 17

Methylene Chloride Extracted Cotton Gauze with Amber Glass Container

Yes 10 cm2 3

Ghost Wipes & Conical Tube (either Methanol wetted for illicit drugs or wetted with DI water for metals)

No wipes 1

SUMMA Canister (7 day rental) Batch Cleaned

Individual Cleaned Silonized 6 L

55

85

Flow Regulator Valve for SUMMA Canister (7 day rental)

NA NA 25

Helium Diffusive Sampler (HDS) (7 day rental) NA NA 30

Supelco Carbotrap 300 tube or SKC Thermal Desorp-tion Tube (7 day rental)

Yes ¾ 40

Cyclone, SKC GS-3 or Aluminum (daily rental) NA NA 15

Supelco ASSET EZ4-NCO Dry Sampler for Isocya-nates

Yes NA 56

Supelco ORBO 34 Activated Coconut Charcoal spe-cially treated (20/40), 400/200 mg

Yes NA 6

Media Available Through ALS Environmental—Salt Lake City— Page 40

1-800-356-9135

Page 47: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

MEDIA

Sampling Pump Rentals

Industrial Hygiene Sampling Pumps

EACH KIT INCLUDES:

(1) Personal Sampling Pump 5 to 4000 ml/min flow range

(1) Low flow Field Rotameter, 5 feet of PVC Tubing

(1) Low flow adapter for sampling in the 5 to 200 ml/min flow range

(1) Sampling Tube Holder and/or Sampling Cassette Holder

RENTAL PRICE:

$125 per week/per pump**

** Additional fees may be applied for non-returned or damaged equipment.

Sampling Pump Rentals From ALS Environmental—Salt Lake City— Page 41

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1-800-356-9135

NOTES

Page 49: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

Microbiological Services Mold in Air

Fungal Spore Trap Spore and Pollen COUNT (Allergenco-D, Air-O-Cell, etc.) Test Code 4 Days 1 Day

Non-viable Fungal Spore Genus Identification and Numeration; Background, Pollen, Fungal Fragment, Skin Cell Density Rating AC1 $35 $70

Non-Viable Fungal Spore Analyses

Bulk/Surface Mold

Swab, Tape-Lift, Bulk Analyses

Fungal Screen Percent ESTIMATE (Swab, Tape-Lift, Bio-Tape, Bulk) Test Code 4 Days 1 Day

Non-viable Fungal G Identification Screen and Relative Density Rating SB1 $35 $70

Test Catalog & Fee Schedule—Page 43

Description Cost ($)

Bio-Tape™ Surface Sampler Bio-Tape™ provides a standardized sampling method for the determination of possible mold, microbial, bioaerosol, and inorganic dust contamination.

2

Air-O-Cell™ Air Sampling Cassette or Allergenco-D The Air-O-Cell and Allergenco-D sampling cassette is specifically designed for the rapid collection and analysis of a wide range of airborne aerosols.

5

M S M

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Periodic Table—Page 15

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ALS Environmental—Salt Lake City provides professional analytical services for all samples submitted. The following statements de-scribe the terms and conditions under which ALS—SLC agrees to operate. Submitting samples to ALS constitutes an agreement to these and the ALS terms published on the ALS Website. https://bit.ly/31solVv

1. GENERAL

1.1 ALS—SLC is not in the position to interpret data as they pertain to regulations, etc. and assumes no responsibility for the quality of samples submitted.

1.2 The Schedule of Fees and Services provides a partial listing of routine analyses performed by ALS—SLC . If you have requirements for analyses not listed, special analytical requirements, or desire information addressing sampling and/or analytical protocols, please contact a member of our project management department.

1.3 Upon request ALS—SLC will supply (at cost plus shipping charges) sampling media and associated supplies.

1.4 Fees are subject to change without notice.

2. ANALYTICAL SERVICE ORDERS

2.1 Requests for analytical services may be made by telephone, FAX, e-mail, or in writing. The client’s authorized representative must confirm all requests for services in writing.

2.2 Chain of Custody (CoC) not provided for Industrial Hygiene analysis unless specifically requested by client.

2.3 ALS—SLC reserves the right to refuse to proceed with an analytical request if the customer fails to provide an acceptable written analytical request or to establish acceptable payment or credit arrangements.

2.4 Prior to submission of environmental samples, the client should develop an appropriate project Quality Assurance/Quality Control (QA/QC) plan. This plan should identify, among other items, the intent of the project, sample collection and preservation require-ments, types of QC samples that are required (e.g. field blanks), laboratory analysis/methods to be performed, minimum data report-ing and deliverable requirements, and required sample turnaround times. This plan should be submitted to ALS prior to sample sub-mission. Unless such a plan is submitted, ALS—SLC is not responsible for project-specific QA/QC requirements. ALS personnel can assist in the preparation of project QA/QC plans.

2.5 ALS—SLC reserves the right to invoke a minimum charge of $100 for each Industrial Hygiene sample project. Each field QC sample will be billed as a regular field sample. Clients will not be charged for laboratory QC samples.

2.6 ALS—SLC reserves the right to add a processing fee for any sample(s) cancellations after work has been initiated.

3. SAMPLE RECEIPT AND PROCESSING

3.1 The client is responsible for the condition and custody of all samples prior to receipt, inspection, and acceptance by ALS—SLC.

3.2 ALS—SLC will use analytical methodologies which have been certified as compliant with requirements published or specified by the U.S. Environmental Protection Agency (EPA), State Environmental or Health Agencies, the National Institute for Occupational Safe-ty and Health (NIOSH), the Occupational Safety and Health Administration (OSHA), or other regulatory agencies. ALS reserves the right to interpret these methodologies when applying them to the analysis of client’s samples based on the reasonable, professional judgment of ALS personnel and recognized standards of the industry.

3.3 All analyses will be monitored under the ALS—SLC Quality Assurance/Quality Control (QA/QC) program. This program includes: instrument calibration, the analysis of spiked samples, quality control samples, laboratory blanks, replicate analyses, comparison of QA/QC data with accepted limits, and monitoring of instrument performance.

3.4 ALS performs Method Detection Limits Studies on a continual basis. Because MDLs change from time to time, projects in progress are subject to new MDL results.

3.5 ALS uses QA/QC protocols which are consistent with current industry standards. It is the responsibility of the client to determine if the proposed QA/QC protocols meet the project or site-specific QA/QC requirements determined by a particular regulatory agent.

Terms & Conditions

Terms and Conditions—Page T&C-1

1-800-356-9135

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3.6 ALS—SLC reserves the right to refuse to proceed with the processing of any sample which is judged by ALS—SLC to be noncom-pliant with quality assurance requirements of a requested regulatory analytical protocol. In such an event, the client shall reimburse ALS—SLC for any costs incurred prior to the stop-work order.

3.7 ALS—SLC will attempt to comply with applicable Federal and State requirements for storage, processing, and analytical holding times. However, unless samples have been scheduled with a ALS—SLC Project Manager prior to delivery, these time limits cannot be guaranteed.

3.8 Should the QA/QC requirements of a requested regulatory method or protocol specify that a sample must be reanalyzed, any addi-tional sample required for the reanalysis will be provided by the client at the client’s expense. Any mandated or requested QA/QC reanalysis, which generates data consistent with original results, will be at the client’s expense.

3.9 ALS—SLC will retain any residual sample for a period of 30 days after data is reported, after which the residual sample will be properly disposed of, unless a written agreement directing ALS otherwise has been established. ALS—SLC reserves the right to return unused portions to the client for disposal.

3.10 ALS—SLC reserves the right to charge $3.00 per sample for handling and disposal. Samples will be disposed of in accordance with current RCRA requirements.

4. ANALYTICAL RESULTS

4.1 ALS—SLC reserves the right to determine the appropriate format in which the analytical results are reported. ALS—SLC will make every effort to honor requests for special hardcopy or electronic report formats where reasonable, advanced notice has been provid-ed by the client. All results are provided for the exclusive use of the client. ALS—SLC accepts no responsibility or liability for the client’s use of such results.

4.2 ALS—SLC requires precise and complete instructions pertaining to parties authorized to receive results of analyses. Any subse-quent request for client results by unauthorized parties will require written permission from the authorized client.

4.3 When requested, ALS—SLC may release verbal, FAX, e-mail (.pdf) results in advance of the written report of results. Such results are tentative and are subject to subsequent confirmation or modification during standard ALS—SLC QA/QC review procedures.

4.4 ALS—SLC will maintain supporting documentation for analytical results for a period of five (5) years, unless a written agreement directing ALS has been otherwise established.

4.5 For Lead analysis on paint, wipe and soil, the client has the right under NLLAP to contact AIHA LAP LLC for any unresolved con-cerns about the quality of reported results, if these concerns cannot be resolved directly with the laboratory.

5. SERVICES OUTSIDE THE SCOPE OF WORK

5.1 In the event the customer requests ALS—SLC to perform extraordinary services which are not included in the scope of work to which the parties agreed, ALS—SLC reserves the right to invoice for the services performed at a minimum rate of $100/hour. Ex-traordinary services include, but are not limited to, the following:

1) Correcting client errors.

2) Request for information or data not required by the original scope of work.

3) Modifications to deliverables not required by the scope of work.

Prior to performing requested extraordinary services, the estimated number of hours required shall be negotiated with the client. ALS shall not proceed with extraordinary services until receiving written authorization from the client.

6. PAYMENT AND TERMS

6.1 Any order less than $500 may require payment at the time of sample delivery prior to sample analysis, unless other payment terms have been established. All major credit cards are accepted.

6.2 Any amounts owing ALS—SLC by the client which are not paid within thirty (30) days after invoicing shall accrue interest at the rate of 1 1/2% per month (18% annually).

6.3 Any taxes local or otherwise are the responsibility of the client and are not deducted from any amount owed to ALS Environmental.

6.4 In the event it becomes necessary for ALS—SLC to proceed with legal action to collect past due amounts, the client agrees to pay court costs and attorneys’ fees.

Terms and Conditions—Page T&C-2

1-800-356-9135

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Page 56: TEST CATALOG AND FEE SCHEDULE - ALS | Laboratory testing

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