-
PPM
86
42
0
1.98
2.00
0.59
5.07
0.91
0.91
1.00
1.01
1.02
1.03
1.00
0.95
8.138.138.118.118.107.777.767.767.757.747.277.277.157.157.147.127.117.117.107.097.067.04
6.31
5.68
4.634.624.624.604.514.514.484.474.244.234.204.19
3.373.353.343.33
2.912.892.882.86
2.332.322.32
1.68
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
170.73
149.94
144.87
136.75
129.19128.60128.44126.87123.96
78.17 77.25 77.00 76.74 74.23
62.41
34.56 34.01
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.00
2.05
3.834.72
1.06
4.07
0.85
0.84
2.01
1.00
1.01
1.00
7.997.987.707.687.387.367.367.357.357.337.337.327.327.317.317.307.267.257.257.237.237.167.157.157.147.127.117.117.097.097.086.35
5.47
4.754.744.734.734.724.694.414.38
3.443.433.413.40
2.982.962.952.94
1.56
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
170.86
149.75
145.18
137.02131.32129.36129.09128.61128.54128.46126.87123.84121.68
86.02 83.41
77.26 77.00 76.75
62.68
34.92 34.52
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.67
2.76
5.248.90
3.35
1.00
1.31
1.29
1.33
1.66
1.28
1.35
8.218.20
7.897.887.397.397.387.377.287.287.277.267.207.197.186.66
5.395.385.37
5.045.035.01
4.364.354.334.324.164.154.124.11
3.353.333.323.303.253.233.223.20
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
175
150
125
100
7550
250
171.33
150.05
144.55137.07136.60135.07129.72129.12128.84128.77128.55127.39125.97124.09
107.75
77.26 77.00 76.75
63.65
43.07
35.86
-0.02
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
2.00
1.972.01
1.041.98
6.56
1.06
1.00
0.981.06
1.00
2.05
8.168.157.877.867.747.727.597.587.577.477.467.447.267.247.247.237.227.207.197.187.18
4.974.964.954.943.833.823.813.803.793.783.663.653.643.633.613.603.563.553.543.533.533.513.513.503.433.423.403.393.223.213.203.193.183.173.173.163.143.133.11
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
210.
020
0.0
190.
018
0.0
170.
016
0.0
150.
014
0.0
130.
012
0.0
110.
010
0.0
90.0
80.0
70.0
60.0
50.0
40.0
30.0
20.0
10.0
0.0
-10.
0
198.32
173.92
149.94
144.73136.22136.04133.61128.96128.86128.71128.46128.04127.26124.08
77.26 77.00 76.74
61.72
40.86 39.44 35.53
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
0.0
2.05
2.12
1.01
6.17
3.02
0.88
2.05
1.00
7.09
1.01
1.00
7.987.967.807.787.267.137.127.117.117.107.097.077.066.446.436.426.416.416.37
5.56
4.754.714.704.694.694.674.404.363.853.833.813.803.783.463.443.433.413.033.013.002.982.75
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
0.0
160.
015
0.0
140.
013
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0.0
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170.98
161.73161.45
149.66
145.27
137.25134.13129.35128.63128.53126.70123.71
104.97103.33
98.46
85.82 82.95 77.26 77.00 76.75
62.85
55.62 55.50
35.55 34.47
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.00
2.13
7.36
2.14
0.95
0.98
2.13
1.08
3.28
1.08
0.79
7.987.987.967.697.677.267.267.197.177.157.147.127.107.097.076.846.83
6.36
5.47
4.754.744.734.724.704.674.384.34
3.83
3.443.433.413.40
2.982.962.952.94
1.57
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
175
150
125
100
7550
250
170.89
160.16
149.70
145.23
137.10
132.85129.37128.58128.46126.82123.80
114.18113.66
88.06
82.05 77.25 77.00 76.74 76.53
62.73
55.35
35.05 34.45
-0.02
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
0.0
2.04
2.13
0.32
10.97
0.93
0.99
2.06
1.00
0.20
1.05
1.01
3.59
0.32
0.46
0.52
7.987.967.697.677.267.267.157.147.127.117.107.097.07
6.37
5.64
4.754.744.734.724.724.684.394.35
3.443.433.413.402.982.962.952.93
2.362.29
2.04
1.63
1.271.261.24
0.000.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
0.0
160.
015
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013
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011
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0-1
0.0
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0
170.96
149.69
145.20139.36137.05131.21129.37129.26128.57128.44126.81123.80118.56
86.22 82.75 77.26 77.00 76.74
62.73
34.98 34.49
21.47
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
1.073.86
2.23
4.06
5.25
0.99
0.99
3.00
2.04
8.028.008.007.877.877.867.857.857.847.717.717.707.697.697.527.527.517.517.507.507.507.477.477.457.427.407.397.257.167.167.157.147.117.117.107.107.097.096.395.794.864.824.804.794.784.774.594.55
3.483.473.453.443.063.053.033.02
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
170.95
149.62145.20136.90133.09133.01130.65129.54129.31128.67128.48128.38126.96126.88126.63125.50125.08123.82119.31
88.09
84.18
77.26 77.20 77.00 76.74
62.51
35.10 34.76
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.00
2.09
2.19
3.12
4.04
0.98
0.95
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5.71
4.744.734.724.714.694.654.444.40
3.423.413.393.38
2.972.952.942.92
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200
175
150
125
100
7550
250
170.92
149.79
145.05
136.86135.21132.54129.26128.91128.60128.38126.89123.86120.13
84.75 84.43
77.26 77.00 76.74
62.45
34.82 34.54
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
87
65
43
21
0
2.00
2.032.09
2.14
5.26
0.90
0.80
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0.96
8.038.017.707.697.597.587.387.367.267.177.167.167.157.157.117.107.097.09
6.37
5.64
4.744.734.724.714.674.494.45
3.433.423.403.39
2.982.962.952.93
1.64
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200
175
150
125
100
7550
25
170.87
149.84
144.98136.77131.63131.20130.93130.66130.41129.23128.65128.37126.96126.74125.49124.73123.98122.56120.39
85.90 84.37
77.26 77.00 76.74
62.34
34.74 34.61
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
10.0
0.0
2.122.02
1.98
2.12
3.55
5.28
0.94
1.00
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2.57
1.70
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8.218.208.068.047.717.717.697.457.437.267.267.197.177.167.127.107.097.087.06
6.34
5.50
4.734.724.724.704.674.554.514.134.12
3.433.413.403.392.992.972.962.94
2.052.051.571.561.271.261.261.251.250.900.890.87
0.070.000.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
220.
021
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200.
019
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017
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015
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120.
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100.
090
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170.92
149.90147.50144.82
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88.62
83.72 77.26 77.21 77.00 76.75
62.09
34.72 34.66
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
1.95
1.96
4.99
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0.89
1.00
1.00
1.01
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2.952.58
8.098.07
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5.51
4.674.664.654.644.434.424.394.394.144.144.114.10
3.403.393.373.362.922.902.892.87
1.741.731.731.60
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
175
150
125
100
7550
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171.01
149.82
145.20
137.15
129.26128.52128.45126.79123.73
82.42 77.25 77.00 76.74 73.59
62.55
34.67 34.32
3.41
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
2.04
2.03
5.20
0.91
0.92
2.03
1.00
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9.03
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6.37
5.48
4.644.634.624.614.574.524.174.12
3.373.363.343.322.922.902.892.86
1.57
0.160.150.140.000.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
150
100
500
170.75
149.84
145.06
137.16
129.31128.51128.46126.75123.82
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91.32
77.31 77.21 77.00 76.96 76.68
62.99
34.99 34.33
-0.41
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
2.03
2.02
8.141.20
1.11
2.25
1.00
1.01
1.09
1.27
7.87
1.111.13
0.36
0.61
1.02
0.28
8.258.237.947.927.287.277.267.267.247.217.207.087.066.896.466.466.456.446.426.425.205.205.195.014.994.984.394.384.354.344.134.124.114.084.073.843.833.833.823.803.753.373.363.343.333.273.253.243.22
2.05
1.271.261.25
0.070.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
-
PPM
200
150
100
500
170.59
161.80
157.07
149.96
144.62
135.20134.64130.52128.79128.75128.61127.26124.03118.73
109.04
104.75
98.79
77.25 77.20 77.00 76.74
63.48
55.52 55.49
43.17
35.48
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.00
2.04
7.53
2.06
1.00
0.99
2.02
3.15
2.05
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5.305.295.28
4.884.864.85
4.124.114.084.074.064.054.024.013.723.203.193.173.163.143.123.113.09
1.18
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
-
PPM
175
150
125
100
7550
250
171.13
160.60
149.90
144.17
136.91135.25128.84128.75128.62128.47127.37127.27124.02123.99
114.26114.18
106.38106.30
77.26 77.00 76.75
64.18 64.04
55.39 55.27
43.13
36.38
29.59
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
0.0
2.02
2.02
10.12
0.97
1.00
1.00
1.011.12
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3.03
0.17
1.16
0.54
8.218.19
7.907.887.287.267.257.207.197.187.177.177.156.68
5.385.375.375.035.014.99
4.304.294.264.254.154.144.114.103.333.313.303.283.243.223.213.19
2.37
2.04
1.60
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
220.
021
0.0
200.
019
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180.
017
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015
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090
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171.22
150.00144.43139.94136.74135.10133.96129.73128.79128.77128.55127.34125.81124.07
107.00
77.25 77.00 76.74
63.76
43.09
36.06
21.16
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.07
4.62
1.342.47
1.33
7.70
0.92
0.99
0.95
1.04
1.00
0.981.06
8.208.187.847.837.707.697.507.497.497.487.437.417.417.407.277.267.257.257.227.217.206.74
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4.144.144.104.10
3.443.433.413.403.333.313.303.28
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
171.76
149.90144.94135.64134.87133.66130.27129.73128.86128.70128.62128.41127.37127.01126.54126.45125.17124.16124.09
109.90
77.26 77.20 77.00 76.74
62.75
42.66
34.39
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
-
PPM
86
42
0
1.89
1.94
0.312.03
5.342.10
0.96
0.96
0.96
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0.90
2.00
8.188.168.167.847.837.357.337.267.257.257.247.247.237.237.237.167.157.147.146.99
5.405.395.38
4.974.954.954.94
4.324.314.294.274.154.144.114.10
3.293.283.263.253.203.183.173.15
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
171.45
149.98
144.28135.77135.63135.35134.99129.26129.15128.76128.64128.43127.34124.10
108.33
77.25 77.00 76.74
63.82
43.03
35.78
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
98
76
54
32
10
2.02
2.03
2.13
2.44
3.542.24
1.09
0.94
0.94
2.00
2.04
8.188.167.837.827.827.657.637.447.437.267.257.247.247.157.147.147.147.137.057.03
5.455.445.44
4.984.974.964.954.414.404.384.374.174.164.134.13
3.303.283.273.203.183.173.15
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
171.65
150.03144.37140.57135.38134.91132.00131.74131.47131.25128.85128.68128.42127.43126.87126.57126.07126.04124.70124.10122.54120.40109.73
77.26 77.00 76.74
63.62
43.04
35.54
29.66
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
2.02
2.00
1.02
1.041.00
1.45
1.04
1.01
1.02
3.060.72
3.34
11.81
8.188.188.178.168.167.797.777.777.267.237.227.227.147.137.137.12
6.36
4.954.944.934.924.824.314.304.274.263.913.913.903.883.873.293.283.263.253.123.103.093.07
2.181.751.551.431.311.301.261.241.230.940.920.910.900.880.870.85
0.070.00-0.01
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
175
150
125
100
7550
250
171.89
135.00130.31128.81128.62128.41127.32123.88
105.36
77.26 77.00 76.74
62.80
42.39
34.77
29.69
23.53
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
1.00
2.221.01
2.142.03
3.11
6.99
0.98
1.00
2.07
0.93
2.00
8.668.658.088.078.007.987.877.867.837.827.677.657.607.597.577.557.537.527.497.487.467.267.237.227.19
4.93
3.85
3.633.613.363.243.163.14
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
176.75
135.22131.13124.29122.72122.53122.24119.47118.56118.47118.43118.26118.08118.01117.17116.66115.89114.92114.62
77.21 77.00 76.80
49.26 48.03
43.65
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
2.02
2.00
3.192.15
0.64
0.63
1.09
2.41
1.03
1.93
1.07
3.15
8.118.118.098.097.617.617.597.597.297.267.257.237.137.127.117.107.097.076.976.956.95
4.614.594.584.57
3.743.733.62
2.992.83
2.18
1.571.531.531.531.521.501.261.261.241.23
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
225
200
175
150
125
100
7550
25
206.36
171.92
149.79
144.51
136.32
128.95128.72127.87126.94124.19
77.26 77.00 76.74
61.15
43.30
39.72
33.77
30.09
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.001.91
3.92
1.95
0.79
1.02
1.02
1.02
0.97
0.97
0.97
0.99
6.27
8.268.258.178.15
7.357.337.327.307.297.287.277.277.197.187.17
6.32
5.77
4.694.654.484.464.454.354.31
1.891.871.861.851.831.621.611.611.591.581.581.571.431.421.400.830.810.80
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
171.71
150.08
145.59
131.22128.93128.88128.46124.00121.72
85.37 83.45
77.25 77.00 76.74
58.38
37.69 34.75
24.66 22.55 22.01
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.00
2.07
3.86
2.04
0.97
1.02
1.99
1.09
1.08
3.14
3.17
8.238.228.168.14
7.327.317.297.287.277.267.197.187.17
6.27
5.77
4.64
3.913.88
2.342.322.322.30
0.980.960.750.74
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
171.20
149.95
145.98
131.26128.86128.79128.40123.93121.90
85.15 83.71
77.26 77.00 76.75
66.20
34.26
27.68
19.93 19.46
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
87
65
43
21
0
2.00
1.91
4.66
2.02
0.93
1.00
1.99
1.02
3.16
8.278.258.158.13
7.347.337.327.297.287.277.267.197.17
6.42
5.78
4.624.604.604.59
4.264.22
1.70
1.371.36
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
175
150
125
100
7550
250
172.02
150.15
145.16
131.25129.06128.84128.45124.21121.53
86.18
82.99
77.25 77.00 76.74
56.13
35.26
13.94
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
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0.0
1.98
6.53
7.03
0.94
0.95
2.00
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2.94
0.33
0.13
7.607.597.337.317.317.297.287.287.277.277.267.257.167.167.157.147.127.087.087.077.066.39
5.47
4.684.664.654.634.594.364.32
3.513.493.483.46
2.852.842.822.81
2.36
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
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015
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013
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143.79137.34136.43131.44129.54129.27128.52128.42128.23127.51126.46122.26
85.20 84.13 77.26 77.21 77.00 76.75
61.59
34.66 34.50
21.46
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
0.0
11.26
0.97
1.00
1.04
0.44
0.46
0.99
0.47
1.03
1.51
0.17
6.82
0.09
7.367.307.297.287.277.267.20
6.336.25
5.955.89
5.024.96
4.724.574.534.294.26
3.893.85
3.46
3.25
1.98
1.351.281.23
0.89
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
0.0
160.
015
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013
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0
172.97172.76
155.41154.77
138.11137.63131.60131.52129.00128.66128.43128.28126.64126.55122.39121.91
84.80 77.26 77.20 77.00 76.74 70.33 69.88
62.14 61.14
38.38 36.32 34.79 34.44
22.06 21.80
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
16.58
1.00
1.00
2.17
0.57
1.46
0.57
2.56
7.367.317.307.297.287.267.247.237.217.207.08
6.256.16
5.76
5.265.245.205.195.165.134.714.554.524.374.33
3.923.893.443.433.393.353.293.273.243.213.19
2.03
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
150
100
500
172.54172.40
155.57155.14137.83137.43136.11135.62131.60129.05128.96128.65128.51128.39128.32128.25128.05127.66126.61122.25
84.64 84.09 77.25 77.20 77.00 76.74 68.11 67.69 62.06 61.40
38.45 36.54 34.79 34.40
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
0.0
12.46
1.00
0.98
0.39
0.56
0.95
0.39
1.08
1.010.45
9.91
7.387.367.307.297.277.277.267.21
6.336.27
6.015.91
4.704.574.53
4.234.19
3.843.80
3.443.243.223.143.10
1.501.471.261.22
0.88
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
0.0
160.
015
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140.
013
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011
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0-1
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0
173.22173.01
154.82153.97
138.31137.75131.60131.50129.07128.66128.38128.29126.60126.49121.94
85.13 84.70 84.43 81.97 81.27 77.26 77.20 77.00 76.74
62.39 60.76
38.23 36.63 34.78 34.43
28.25
14.06
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
86
42
0
2.04
2.06
3.482.05
0.99
1.00
0.99
1.12
1.52
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0.37
6.99
8.278.068.04
7.347.277.13
6.69
5.22
4.78
4.484.45
4.104.06
1.841.71
1.000.98
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200
175
150
125
100
7550
250
172.36
150.08
144.54
137.16136.16
129.49128.96128.70125.82124.04
107.32
77.25 77.00 76.74
60.72
42.48
38.31
24.28 22.65 21.48
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
86
42
0
2.052.00
5.18
0.90
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3.10
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5.70
8.268.258.048.027.387.377.377.367.287.287.277.277.277.267.04
5.415.405.39
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2.222.212.202.202.192.172.03
1.051.051.041.03
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
175
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125
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170.86
150.04
143.88
137.64136.28
129.65128.96128.89125.93124.00
107.43
77.25 77.00 76.74
69.75
27.48
19.64 19.60
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
86
42
0
2.00
2.07
3.14
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1.00
1.04
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3.73
3.46
1.591.58
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
175
150
125
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7550
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172.32
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144.49
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107.55
77.26 77.00 76.75
58.28
42.78
16.28
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
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5.385.375.365.055.035.02
4.284.274.254.244.084.074.044.043.303.293.273.263.213.193.183.16
2.37
1.61
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
150
100
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171.81
143.68137.33136.32135.76135.36129.51129.37128.91128.77128.68127.46127.10126.04
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77.26 77.00 76.75
63.29
42.84
36.18
21.51
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
108
64
20
11.28
0.96
1.00
2.03
2.02
2.09
6.63
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4.964.954.944.934.914.82
4.254.11
3.32
1.441.291.21
0.88
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
150
100
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172.90
155.40
138.10136.99129.09128.85128.55126.75126.18
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77.26 77.21 77.00 76.75 69.85
62.55
44.28
35.16
22.05 22.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
108
64
20
17.03
1.00
1.95
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2.04
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4.95
4.234.124.11
3.373.29
2.03
1.71
1.271.251.24
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
150
100
500
172.68
155.49
138.03136.58135.81129.15128.86128.76128.55128.46128.35128.17128.06127.94126.81126.18
110.21
77.26 77.20 77.00 76.75
67.81
62.47
44.04
34.98
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
108
64
20
14.91
1.00
1.24
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0.74
1.12
2.57
11.64
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5.38
4.70
4.27
4.02
3.31
2.04
1.611.451.281.261.241.21
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200
150
100
500
173.17
154.90
138.35137.35135.66129.08128.98128.95128.89128.54126.72126.22
110.77
77.32 77.21 77.01 76.69
62.89
44.69
35.25
28.30
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
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0.931.00
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5.645.48
4.764.744.734.514.504.484.484.374.374.34
3.343.333.313.303.093.073.063.04
2.05
1.26
0.89
0.080.01
Electronic Supplementary Material (ESI) for Organic &
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PPM
200
150
100
500
170.65
155.77
141.58135.70133.13128.94128.71128.47128.19127.31126.96
103.54
77.26 77.00 76.74
57.06
46.48
34.77
Electronic Supplementary Material (ESI) for Organic &
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PPM
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0.96
0.981.02
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4.244.234.224.204.194.184.174.163.883.873.863.853.843.783.773.763.753.743.502.822.822.80
2.052.042.042.042.03
Electronic Supplementary Material (ESI) for Organic &
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090
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206.11
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150.93148.04
129.30
124.96
63.76
59.28
52.43
30.26 30.11 29.95 29.80 29.65 29.49 29.33
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
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9.0
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3.01 0.491.97
0.99
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1.051.06
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1.03
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8.288.278.028.007.347.347.347.337.327.317.317.317.307.307.287.287.267.207.207.19
5.675.66
4.484.464.444.414.254.254.244.234.234.223.823.813.803.803.673.673.653.653.61
1.591.58
0.00
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
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019
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128.49128.28128.09127.68124.15
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56.26
52.88
Electronic Supplementary Material (ESI) for Organic &
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PPM
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9.0
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1.98
1.033.03
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2.04
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5.46
8.598.588.348.348.338.328.098.098.078.078.077.497.367.357.347.327.317.307.307.297.287.237.237.227.20
4.394.114.104.084.084.073.573.563.553.543.523.513.503.493.38
2.562.562.56
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
210.
020
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190.
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170.09
149.20146.96
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56.23
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38.99
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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2.002.01
0.69
3.771.95
0.96
3.96
1.98
9.640.96
2.29
8.218.208.208.198.188.188.098.088.088.078.068.067.527.307.287.287.277.267.257.257.247.247.237.227.227.227.177.177.16
4.624.614.614.604.474.464.434.424.404.404.374.364.364.354.344.313.813.803.793.783.773.763.753.743.343.193.183.18
2.502.492.492.492.48
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
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019
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017
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169.39
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128.87128.04127.70127.50123.98
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74.86 72.14
68.25
58.97
40.00 39.92 39.83 39.76 39.66 39.50 39.33 39.17 38.99 34.50
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
10.0
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3.132.09
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1.00
1.05
3.12
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9.059.048.238.228.228.218.208.208.018.018.007.997.997.987.287.277.267.247.247.237.127.127.115.555.535.535.525.514.894.894.884.884.874.874.864.864.724.714.704.694.394.394.364.364.344.323.843.823.803.803.773.693.683.673.663.32
2.492.492.49
2.07
Electronic Supplementary Material (ESI) for Organic &
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Chemistry 2012
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PPM
200.
019
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017
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170.24
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128.50128.07127.60124.15122.23
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71.84
65.07
61.99
43.14 40.10 40.01 39.93 39.83 39.76 39.67 39.60 39.50 39.34
39.17 39.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
0.0
2.00
2.02
3.03 0.532.00
1.03
0.92
1.071.05
2.07
1.02
3.13
0.78
1.26
0.46
8.258.258.248.248.237.977.967.967.957.957.947.387.377.367.367.357.357.347.347.337.337.327.267.217.207.207.197.187.186.656.65
5.87
4.514.494.394.373.823.813.813.803.793.783.773.433.413.413.40
2.782.77
2.17
1.65
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200.
019
0.0
180.
017
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160.
015
0.0
140.
013
0.0
120.
011
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168.69
150.19
144.77
136.61
128.68128.47128.42128.03124.35
77.26 77.00 76.75 73.63
69.43
55.53
26.53
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
0.0
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3.28
1.99
1.00
1.00
3.95
1.031.02
3.10
0.99
0.33
0.11
7.997.997.977.967.947.947.297.277.267.247.237.237.237.027.016.61
4.664.654.644.634.304.284.244.224.034.024.014.003.893.873.85
2.832.82
2.272.272.26
1.77
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200.
019
0.0
180.
017
0.0
160.
015
0.0
140.
013
0.0
120.
011
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168.18
149.87
144.42
136.66
128.98128.26128.22128.12123.54
77.59 77.25 77.00 76.74 73.83 73.45
66.92
60.10
34.27
26.29
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
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3.44
1.99
0.99
1.00
1.121.93 1.092.02
1.00
0.98
3.05
9.19
5.970.17
7.997.987.987.977.967.957.947.947.307.297.297.287.277.277.267.247.247.237.237.027.027.017.016.606.59
4.654.644.634.624.294.274.254.254.254.234.214.194.184.184.054.044.034.023.873.853.853.83
2.842.83
1.651.65
0.90
0.090.090.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
0.0
180.
017
0.0
160.
015
0.0
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013
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168.26
149.85
144.53
136.76
129.00128.31128.25128.05123.54
84.63
78.25 77.25 77.00 76.74 73.48
67.00
60.17
51.39
34.76
26.37 25.74
18.25
-5.29 -5.33
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
0.0
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1.164.50
3.96
1.95
0.95
1.00
1.961.031.021.031.02
3.01
0.45
7.997.997.997.987.977.977.917.917.907.897.897.887.367.367.367.357.347.347.337.337.337.317.297.297.287.287.277.277.267.267.257.247.247.237.227.227.227.217.217.207.207.197.187.187.186.956.936.936.606.604.734.724.714.704.464.454.324.304.224.204.104.094.084.073.983.963.963.942.832.82
1.58
0.010.00-0.01
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
220.
021
0.0
200.
019
0.0
180.
017
0.0
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013
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144.68136.71131.49129.06128.98128.44128.29128.25128.13123.57121.71
85.91 82.66 77.26 77.21 77.00 76.75 73.63 67.09
60.36
35.25
26.50
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
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1.94
1.940.98
1.001.02
1.021.03
1.01
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3.01
0.33
7.997.997.987.977.977.917.897.377.377.267.257.247.217.197.186.946.936.526.516.486.476.396.386.386.38
4.724.714.704.694.594.554.424.384.304.284.224.204.044.034.024.013.923.903.88
2.842.83
1.61
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
0.0
180.
017
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160.
015
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140.
013
0.0
120.
011
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100.
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168.18
149.86
144.55144.07
136.72135.74
129.14128.24128.21123.56
115.96
110.96
87.41
77.25 77.20 77.00 76.74 76.09 73.59
67.04
60.45
35.01
26.44
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
0.0
2.00
2.10
3.841.99
1.00
1.98
1.022.02
1.981.04
3.05
1.44
0.51
8.168.157.947.93
7.317.307.307.297.267.167.167.15
5.665.635.004.994.984.974.964.954.954.944.934.454.434.384.353.933.933.923.913.893.883.833.823.813.80
2.82
1.58
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
0.0
180.
017
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160.
015
0.0
140.
013
0.0
120.
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168.75
149.91
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136.84
129.05128.62128.44128.17127.93123.81
109.75
77.26 77.00 76.74 73.11
65.72
62.30
43.60
37.22
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
8.0
7.0
6.0
5.0
4.0
3.0
2.0
1.0
0.0
1.98
2.07
9.40
1.00
0.98
1.021.14
1.981.05
2.09
1.00
3.08
2.97
1.979.42
0.976.071.44
8.368.368.358.348.348.068.058.048.037.357.357.347.327.307.307.297.297.287.287.26
5.705.695.674.894.884.874.864.564.544.494.474.104.084.064.054.033.993.963.793.773.753.743.733.723.713.283.273.263.252.91
2.18
1.62
1.26
0.920.88
0.100.050.050.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
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180.
017
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160.
015
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140.
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167.28
150.30
145.47143.07
137.62
128.94128.38127.82127.74124.40
110.37
77.25 77.20 77.00 76.74 72.92 70.55
64.36 61.90
42.52
31.65
25.73 25.63
18.19
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Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
10.0
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4.0
3.0
2.0
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1.93
1.97
1.104.134.90 0.32
1.00
0.99
2.03
1.00
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1.00
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0.14
8.418.418.418.408.398.398.118.118.108.098.098.097.437.427.427.417.407.407.397.397.377.367.347.337.317.307.307.297.297.287.287.277.265.845.825.814.994.984.974.964.554.524.504.484.254.234.224.213.833.813.793.733.713.713.703.343.333.323.30
2.77
1.63
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200.
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017
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150.36147.93
142.80
137.43134.31129.93129.06128.93128.39127.79127.62127.04124.49
111.99
77.26 77.00 76.74 73.09 70.63
64.24
42.84
34.34
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
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1.021.01
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2.06
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2.22
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3.05
1.38
0.57
8.408.388.098.077.457.337.327.307.297.287.287.267.247.236.446.436.436.436.326.326.046.026.01
4.924.914.904.894.484.464.454.424.244.234.224.203.733.713.703.703.693.693.673.333.313.313.292.94
1.57
1.26
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
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PPM
200.
019
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017
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015
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167.39
150.39147.78
143.99142.89
138.14137.50
128.95128.36127.74127.62124.50
111.74110.52110.50
77.25 77.20 77.00 76.74 73.18 70.78
64.26
42.40
34.72
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
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0.990.95
0.95
2.25
2.070.99
1.151.09
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7.437.437.427.337.327.317.307.307.297.287.277.267.257.256.446.446.446.436.376.376.206.186.17
4.584.564.554.533.873.863.863.853.843.833.823.823.733.723.713.703.523.503.493.483.423.413.403.383.07
2.36
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
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017
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090
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171.93
148.79
143.00
138.09136.60
128.34127.85127.63
115.76
111.40108.92
77.26 77.00 76.75 73.62 70.25
56.44
41.36
33.15
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
10.0
9.0
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1.031.02
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2.14
1.002.01
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3.99
3.06
2.07
1.82
7.447.447.327.327.307.307.297.287.277.267.267.256.456.456.446.446.446.396.386.216.196.18
4.594.574.534.513.883.873.863.863.853.843.713.703.693.683.673.263.253.243.223.093.083.073.063.04
2.35
1.60
0.00
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
-
PPM
200.
019
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180.
017
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160.
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090
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171.16
148.59
143.17
138.02137.59
128.34127.95127.64
113.70111.47109.27
77.26 77.00 76.75 73.51
67.99
62.67
51.62
40.59
33.06
Electronic Supplementary Material (ESI) for Organic &
Biomolecular ChemistryThis journal is © The Royal Society of
Chemistry 2012
