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AP42 Section: Background Chapter Reference: Title: 11.19.1 4 15 Emission Test Reports for U.S. Silica, Oceanside, CA, August 1989, September 1990, January 1991, and June 1987, Air Pollution Control District, San Diego, CA.

Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

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Page 1: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

AP42 Section:

Background Chapter Reference:

Title:

11.19.1

4 15

Emission Test Reports for U.S. Silica, Oceanside, CA, August 1989, September 1990, January 1991, and June 1987, Air Pollution Control District, San Diego, CA.

EPA
Text Box
Note: This is a reference cited in AP 42, Compilation of Air Pollutant Emission Factors, Volume I Stationary Point and Area Sources. AP42 is located on the EPA web site at www.epa.gov/ttn/chief/ap42/ The file name refers to the reference number, the AP42 chapter and section. The file name "ref02_c01s02.pdf" would mean the reference is from AP42 chapter 1 section 2. The reference may be from a previous version of the section and no longer cited. The primary source should always be checked.
Page 2: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

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Page 3: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

2DC - 40

A,\$.. . .. _. ..

.;; ?.

i

. I

R. J. Sommerville Air Pollution Control Officer apcd County of Son Diego

,/

3231 Oceanside Blvd. Oceanside. CA 92056

SUBJECT RENEWAL TEST REPORT

The enclosed test report is the result of testing done at your facility.

! j. If you have any questions, please call me at (619) 694-3359. ,

C. W. Ridenour Senior Air Pollution Chemist

Enclosures

AIR POLLUTION CONTROL DISTRICT 9150 Chaapc.ks Drive. Sm Diego, California 92123.1695

(619) 565.5901

Page 4: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.. i” . ‘C

SAN DIEGO AIR POLLUTION CONTROL DISTRICT 9150 CHESAPEAKE DRIVE

SAN DIEGO, CA. 92123

SUMMARY: SOURCE TEST OF PARTICULATE EMISSIONS TO THE ATMOSPHERE

TEST SITE: us. Slllca 3231 Oceanside Bkd. Oceanslde Ca. 92056

TEST W: 89234 P D I : W0236 TEST DATE 22AUQ. 69

EQUIPMENT: FluM bed dryer on a dabs sand process line: crushing. drying, 8 screenlng systems with dust laden air from baQglng & bwer bin areas vented to an antipol wet type air scrubber. 24000 dsctm, w/ 250 gpm of water. (appl. 110658) (appi. YE60749 gea) UNIT TESTED: Venlurl-type scrubber

SITE PERSONNEL Mark Louoh APCD PERSONNEL T. Wood. J. Jacksonand G. hhzls /

REPORT BY: I J.Jackson . DATI18 DEC. 89 APPROVEDBY: DATE a d 9 0

C.W. RIDENOUR SENIOR AIR POLLUTION CHEMIST

PARAMETERS: MEASURED: STACKQAS ROW RATE (DSCFM):

STACK QAS TEMPERATURE ‘F (AVO):

19.61 7

137

PRODUCTION RATE (AVG): 70.8 tonshr.

PERMIT UMIT

RULE 50: General 20 % 1 0 % PASSED

TESREFERPICE: San Diego Air Pollution Control District Quality Assurance Manual Method 5 for Particulate Emissions from Stationary Sources.

SAN DIEGO AIR POLLUTION CONTROL DISTRICT TESTY89234 P/O#OOO236 PAGE 1 OF 6

Page 5: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

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TEST DESCRIPTION

Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at US. Slllca me test wae performed on a Venturi-type scrubber servlng the fluidized bed drver.

System Descrlptlon:

Glass sand is drled In a fluld bed dryer whlch Is flmd by natural gas. The exhaust from thls dryer 1s pulled through a venturl-type scrubber, the emlsslons to the atmosphere from thls scrubber are the subject of thls report.

Procedures: The procedures and equlpment utilized In performlng these tests are based on EPA New Source Performance Standards Method 5. The sampllng traln was modified to exclude the front-end fllter and lnclude a back-end fllter, per the San Dlego Alr Pollution Control Dlstrkt Method 5 testing guldellnes. The calculations were deslgned to Include the impinger catch so that the test resuks can be compared to Rule 54 of SDAPCD.

Veloclly Traverse: Prlor lnformatlon regarding the stack velocity profile ellmlnated the need for a separate exploratory traverse. Temperature and pitot tube data collected during actual sampling were used to calculate stack volume.

Partlcuiate Sampling: Thls sample consisted of 28 traverse polnts, 7 from each of 4 sample ports as shown In Flgure 182. Two of the ports were Inaccessible due to probe interference wlth ralllng. The sample was collected 114 lnche8 below the top of the stack Fleld data aesoclated wlth samF collection has been transferred to computer printout and 1s shown In the report. Calculations were done by computer and are also shown wlthln the repon.

Gas Analysis: An integrated bag sample was collected on slte and measured. The oxygen and cabon dioxide content of the stack gas was measured using a Teledyne model # 32OP-4 serlai # 66676, and an Anared gae analyzer model # AR-400. serial # 305. respectlvely, as per Method 3 In SDAPCD test guidelines.

Comments: Thls repon provides suffklent Information to determlne that the slte Is In compliance despite equlpment problems which prevented sampling in the standard wnfiguratlon.

SAN DIEGO AIR POLLUTION CONTROL DISTRICT TEST#BS234 PK)toMmB PAGE 2 OF 8

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Page 6: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

7 ,' ,.

STTE: US. Slllca OPERATOR: JJackson

rEsT DATE: 22AUG. 89 TEST: 89234

In Wsec. All measurements are actual - uncorrected - values. Average: Vm AP AH 11 12 1s 11 M

41.094 1.54 0.93 94 124 137 55 68.42

SAN DIEGO AIR POLLUTION CONTROL DISTRICT TEST#8I)234 PIOX000236 PAGE 3 OF 8

Page 7: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

DATA SUMk

PRESSURES AVERAOE TEMPERATURES

Pbar 29.9 In Hg ts -- 137 F

P static 3.50 In H20 trn l/Z(eve.tl+ave.lZ) - 109 F

Ps 30.2 In Hg ti - & F

VOLUMES VAPORPRESSURES

Vm, meter 41.094 ft'3

Vlc. lmplngers 109.4 m i Vpw@ Imp - M l n H g

MElER BOX PARAMETERS NOPLEAND PROBE

A M - 2.72 lnH20 Dn--In

AP - 1.64 inH20 An - DnA2'd4 --lnA2

AH - .93 hH20 C p - m

MEER BOX l.D.# D-337 Y - a

STACK MEASUREMENTS STACK PARAMETERS

a02 1.40 Stadc Diameter - 2.50 ft

%co .oo Ao-Area SW - =ftA2

%02 19.50

%NZ 79.10

0 - sampling Urne 98 minutes

mn-particulate collect'd .0249 grams

SAN DIEGO AIR POLLUTION CONTROL DISTRICT TEST089234 P/0#000236 PAGE 4 OF 8

Page 8: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

I . I.

~- ,-

Hzo

O m e n

Carbon monoxlde

Carbon dioxide

N2 + lnens

c A L w u n o N s :

wrr Vwm - ((Vm'Vpw~imp/Ps)'Pm7std)/~m-PsM) - water volume wrrectlon at meter wlo slnca gel - 0.5518 ftA3

- meter volume cotrected to S I P - 37.23 ~3 Vm std - (Vm'Y7std.Pm/(PsM7m))-wrr Vwm

Pm- Pbar+(AW13.8)- wrrected pressure of meter - 29.97 In Hg

Tm- (tl+tZ)R + 460 - meter temperature - 589.3 O R

Ts - W460 - corrected stack temperature - 598.9 O R

Pa- Pbar + (P staUell3.6)- corrected stack pressure - Vw std - Vica'R7std/(Pstd'Md)+rr Vwm

30.18 In Hg

- water volume at STP - 5.72 f t ~ 3

Bws - (Vw std+con Vwm)/(Vw std+@rr Vwm+Vm std)

mn- grams of particulate (from laboratory sheet) - 0.0249 grams

- molslure - 0,1441

.14 I 0.1441 1 8 2.59

.20 0.8559 3 2 5.34

.OO 0.8559 28 0.00

.01 0.8559 44 0.53

.79 0.8559 28 19.09

1 - BwS

EQUATION NUMBW

1

2

3

4

5

6

7

8

9

Cs - 15.43'mnNm etd - graln bdng (dry) - 0.0103 grainsldsct IO

GAS ANALYSIS

SAN DlEQO AIR POLLUTION CONTROL DISTRICT TEST189234 PK)m)Oo238 PAQE 5 OF 8

Page 9: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

A .r-.

Md - Oa2~o2~.449bCo2+o26*(lMF%02-%C02) - average molecular weight, dry (glg'mo1)- 27.55

VS- 85.49'Cp'((TS'AP)/(P8*MS))l.S - stack velodty (W- 68.42

Os - (vs)'Ao'BO - stack flow rate (am)- 25.658

Qstd -17.68'Qs'(l-Brm)'PsTTa -flow rate at m P (dsdm)- 19,617

I - 144'100'Ts'(.002669'VIC+(Vrn~m)*Pm)/(60*Wvs*Ps*An) ilsoklmtic (%) - ,.95.3a ,I

E - (0.00647).(QsM).Cs - partlculate ernlsslon rate ( Ibhr) - 1.71

SUMMARY OF CALCULAlIOHS:

I - % lsoklnetlcs - Cs - graln loading (dry) -

E - partlculate ernlsslon rate - %Co2 -

95.3 %

0.010 gralnsldscf

1.71 lbslhr

1.40 %

SAN D I M 0 AIR POLLUTION CONTROL DISTRICT TESTM9234 PIOM00236 PAQE 6 OF 8

Page 10: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

" R E

* - multlpllcatlon I - divkbn - exponentlatlon Vm - sample gas volume, uncorrected - (fP3) AP - root mean pltot tube dlfferentlal pressure

AH - average dMerenUal pressure across the ornlce - (In H20) 11 - dry gas meter Inlet temperature - ('F) l2 - dry gas meter outlet temperature - ( O F )

ts - stack temperature - ('F) tl - lmplnger out temperature - ("F) vs - stack gas veloclty - 85.49*Cp'~s'AP/(Ps.Ms))~.5 - (fVs) Pbar - barometrlc pressure - (In HQ) Pstatlc - slack staUc pressure - (In Hg) Ps - Absolute stack pressure - Pbar +(PstaW13.8) - (In Hg) m - dry gas meter temperature -(tl+t?)R - ('F) VIc - collected water,lmplngers - (mi) Vpw - Vapor pressure of water - (In Hg) AH @ - odflce pressure dlfferentlal that equates to 0.75 cfm of alr @ 68nF and 29.92 In Hg Dn - nozzle dlameter - (In) An - nozzle area - n'DnW4 - (lnn2) n - the ratlo of drcumference of a clrcle to Its dlameter - 2217 (dlmenslonless) Cp - pltot tuba coeffklent - (dlmenslonless) Y - meter box coeffldent - (dimensionless) C02 - carbon dbxlde - (%) CO - carbon monoxlde - (%) 02 - oxygen - (%) N2 - nltrogen - (%) 0 - sampllnp tlme - (minutes) mn - partkulate found In sample train - (grams) A0 - steck area - stadc dlameterWd4 If round; length 'wldth If rectanglar - (fl"2) Corr Vwm - ((Vm'V~@lmp/Ps)'Pm'Tstd)/~m.Pstd) - (ft"3) Pm - absolute meter pressure - Pbar+(AH113.6) - (In He) Tstd - temperature at standard conditions - (528'R) Tm - dry gas meter temperature -(tl+l2)/2+480 - ('R) Pstd - pressure at standard condltkn - ( 29.02 In. HQ) Vm std - corrected volume of meter - Vm'YT sM*Pm/(Pstd'Tm)-corr Vwm - (W3) Ts - stack temperature - ( O R )

Vw sM - water volume at STP - Vlc*a*RTstd/(PstdWd) - (ftr3)

- (summaUon(press.dlff. acrnas plMt tubesA.5)humber ~nt r les)~2 - (In H20)

SAN DlEQO AIR POLLUTION CONTROL DISTRICT TEST#89234 P/owOo6236 PAQE 7 OF 8

Page 11: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

NOMENCLATURE: CDnt

a - denslly of water a1 STP - 0.002201 - (b/ml) R I Ideal gas conslanl - 21.85 In. Hg'lta3PR'lb'mole Md - dry slack gas molecular welght I 0.32*%02+0.44'%C02+0.28(100%02-%C02)

Bws - fractlonal sta& gas molsture content I (Vw sld+Con Vwm)/(Vwstd+Con Vwm+Vm sld

Cs - graln loading I 15.430'mnNm sld - (gralnddscf) Mw - molecular welghl - (gIg'mole) Ms I we1 slacic gas molecular welghl - Mb(l-Bws)+Bws'l8 - (Wmole ) Qs - fbw rate - vS'A0'60 - (a&) Qstd - flow rate a1 standard condillons - 17.68'Qs'(l-Bws)'PsTs - (dsch) I I Isoklnetlcs - 144'100'Ts'(.002869'Vlc+VmTTm)'Pm/(60*0*vs'Ps*An) - (%) E - particulate emkslons rate - 0.0084TCs'Osld - (Ibshr)

CONSTANTS:

- (g/g'mole)

- ( W l 00)

0.00847 Ib/(gr'mln/hr) - 1 lb/7000gralns'60 mln/hr 13.6 In H20An Hg 17.68 W l n Hg 60 sedmln 32 g/g'mole - 0 2 molecular welghl 44 g/g'mole - COZ molecular welghl 28 g/g'mole - N2 molecular weight 18 g/g*mole I H20 molecular wIgM 85.48 (Wsec)'(lb'ln Hg/(lb'mole'"R'ln H20))".5 0.04707 - n w n ~ 460 (demensbnless) - comersbn "F lo 'R 144 lnA2/ft%? 15.43 gr/g 0.002669 In Hg'RA3/(OR'mi)

SAN DlEGO AIR POLLUTION CONfROL DISTRICT TEST189234 P / W W 2 3 6 PAGE 8 OF 8

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Page 12: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

Ports E&F f

Page 5

SAN DIEGO AIR POLLUTION CONTROL .DISTRICT

TRAVERSE POINTS

CRYSTAL SILICA

EXHAUST FROM FLUID BE0 DRYER

-- -9 + t t + + + t

+ + + + +

A

B

C

D

E

F

,or&. -

. I6 '. 14 a" . *

23 V i D 1

21 *!4* . were not unaccessible, thus not traversed.

FIgure 1

.

Page 13: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

. ..

I

- . . +.. I '

. Y. .. .

Page 14: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at
Page 15: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

? -.

. . . . . . . . . .

,.i. / Z*.-wnlhci mm- pf9

. 6 m .. . . wu3 tdcmbru:

rClD -.a hi:, w... . b .

4 3 ......... _.

, . I W - #,3 140 -83

9 3 I zq &-?

. . 3 0 . . . . . I 2 5 ,eo..:. . . . . . . . . . . . . . . . . . . . . . .

190 - * 3 * . , 12-5 SLS. . . . . . . .

- * 3 9 . . I 9 . . 'W . . (70. . . . . . . . . . . .

- a 3 m \'30 5% . . . ,4 0 - .3 5 6 130 5t-O ITa - *3 ! G-5 130 s"l5 ' . . . . . . . . . . . . . . . . . . . .

- 3 5 2 6 . 'W. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . .

.!F= .: .!.9 . . . . . . . . . . . . . . . . . . . . . . . 555 - . . - . . . w . . . .Y.

5w. . . . . I ' fo ' ' . . . . . . . . . . . 170. ...... .- . . . . .+

555 . . . . . . . . . . . . . . . . . . . 1% . . . . . . . . -. - . 4.. !5m (70 s a . . . . . . . . . . . . . 1% . . . . . . . . . . ___. . . . . . . . . . . . . . . . . . t

sbs I3 . . . . 5 6 170 & . 4T sa' . . . . . . . 'P . . . . . . . . qo. . . . . . . . . .I E- . . . . . . . . . . . . . . . . . . .

675 I 9 . 5%- . . . . . . . _c_ . . . . . . . . . . . . . .

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5537: I 3 D

....

. . . . . . .

. . e o . 1% . .

I

5% 1 %

1% . . . ... . . . . . . . . . . . . . 55s . . lclo , . ~ ........ ........ &.... m - - . . . . . . . . . I@ .....

&: a I 2Q

$!?WSe.mp ~ P ~ o V f l i . / z P - a 8 F

-rk-*.e#- &wm l7- _c_ ?==V?.EC~-=) . . . . . . . . . . . . . . . . . . .

@?m4 = w - ~ ~ .. w T , 2 3 . . . . . . . . . -. .

&-4 = &IC 6 4 9 Ty,s,(. . . . . .

- ' u r n & 6-k r3rw . . we = I rJ m... . ~. . .. TlD)ll,fL

. . . . . . . . . . . . . . . 6. -.

Page 16: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

........ .... ...

z

- .. ........... -. .... - .............. -

. . . . . . . . . . . . . . . . . . . . . ....

(9 tA5’IeE =MI=%fUs. . . . . . k3fajEO w. O-/O% ,. ,., . . . . . .

Page 17: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

~~~~~~~~~~~ ~ ~~

, __

.__ _--- ...... ~ __

_._ _- - ........... -. .. __ ..... - ... . --_ ...... - ... - .................... ._ ...... ........... .. -

-.____...__.__....---.I .. ........... ........

. . . .

. . . . . . . . . . . . . . . . . . . . . . . . . ..... .. ...... .... ...... -. . . . . . . . . . . . . . . . . . . . . . . . ................

. . . _. . .- _ _ ....... -. . . . . . . . . . . . . .- . . . . . . . . . . . . . . . . . . - ..... .............. ...............

. . . .- .. .- .- .- -. . ....... . -- - . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .........

- -. ... ._ ... ... ............. ._ . _ _ _ ._ ........... -. .. ..

__ ..... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .- - -. - . .

. . . .......... ....... ._ ............. . . . . . . . . . . . . . .

. . . . - . . .

. . . . . . . . . . . . . . . . . ..... ._ ... . . . . . . . . . . . . . . . . ........

Page 18: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

SITE - u. s. Slllca Test Date - 8-22-89

TEST d - 89234 VOLUMES

(1) IMPINGER VOLUMES flnal Inltlal" A

6 1 644.7 ml 539.4 ml - 105.3 1 2 542.6 ml 540.0 ml - 2.6 1 3 457.3 ml 456.2 ml I 1.1 1 4 441.7 ml 441.3 ml - 0.4

TOTAL W M E UQUD COLLECTED - 109.4

comments: Impingem were weighed In gms. Used 1 gWml to convert to mts. Rlnses for front half end badc hall wwe wmblned. Partlculate was whne and chaky.

(2)SOLVENTSADDEOWRffiNOFlECOMRY

ACETONE

BKR ID - 89

m w w WASH - 4 0 0 ml

WASH - ml BACK HALF

rr(ANSER RINSE - 30 ml

totalacetone - I 430.0 1 ml

WATER

BKR ID - 7 6

FRONTHAU: WASH - 4 1 0 ml

BACK HALF WASH - ml

TRANSFER RINSE - 3 2 ml

IMPINQERS - 200 ml

total water - 1 642.0 I ml

* All data and calculatbns may be found on flle at the San Diego County Alr Pollution Control DIstrW.

U.S. Slllca 689234 \ Page 1 T. Wood 9/12/89

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TEST C - 89234

STANDARD CONCENTRATIONS

volume Ac D 5 1 5 rnl volume water - 1010 rnl

Pmas WATER

BKR ID - 7 0 BKR ID - 7 1

1: 60.9329 g 1: 49.4106 g

I : 50.9326 g I : 49.4100 g

A: 0.0003 Q A: 0.0006 Q

Llrnits: llmlt for scetone is 7.9 pglml (7.9 10’4 g/ml) llrnlt for water Is 4 pg/mi (4 10“-6 g/rnl)

TheAcatone PASSED The Water PASSED

5.83E-07 g/ml 5.94E-07 glrni

(3) CORRECTIONS- (volume used)’(std wt)

ACETONE

FRONTHALF- 0.0002 Q

BACKHALF- 0.0000 g

BKR RINSES- 1.7476E-05 g

total gnrm from aotvents I] g

WATER

m H A L F - 0.0002 g

BACKHALF- 0.0000 g

BKRRINSES- 1.901E-05 0

U.S. Silica 189234 \ Page 2 T. Wood 9/12/89

_ -

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TEST I - 89234

SAMPLE WEIGHTS

FRONTHALF BACKHALF

ACErONE

BKR ID I 69 BKR ID - 1: 49.9289 0 1: 9

I : 49.9118 g I : 9

A: 0.0171 9 A: 0.0000

WATER

BKR ID - 7 6 BKR ID - t: 49.2255 0 1: 0

I: 48.2173 0 I: 9

A: 0.0082 Q A: 0.0000 Q

ORGANIC

BKR ID - BKR ID - 1: Q 1: Q

i: 0 I: Q

A: 0.0000 Q A: 0.0000 Q

FILTERS

ID- 89016 ID - 1: 0.1208 g 1: 0

I: 0.1207 g I: B

A: 0.0001 Q A: 0.0000 9

T. Wood 9/12/89

_____

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.. . I.

TEST X - 89234

(4) FINAL WEIGHTS

(total wight galned)

m0NTHAI.F- 0.0253 BAcKHALh 0.0000 oRcu\NK; 0.0000 (front and back)

WEIGHT QAINED D 7 1 0

correction for solvents (acetone and water)

WEIGHT QAINED FROM SOLVENlS I

WEIGHT QAINED (CORRECTED) = I 0.0 2 4 e]g

(6) FILTERS

FRONTHALF- 0.0001 BACKHALF- 0.0000

TOTAL WEIGHT QAINED E I 0 . 0 2 4 9 jg

Comments - Flller - llgM badiw of light grey particulates noted.

U.S. Silica X89234 page4 T. Wood 9/12/89

. -

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TEST I 8 23+

I .. \correction factor

12%

Page 23: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

t4- h/\ pr C ..

. I *

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. . . . .

___ __ ._-..____- .......... . . . .... . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . , . ..+

. ....

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I

.. . . %- 43

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...... .._ .................................... -. ................ . . . . . . . . . . . . . . . . . . . . . .

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w-4f -I

Page 30: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

:-.

R. J. Sommenille Air Pollution Control Officer

May 13. 1991

'U S Silica Co. Attention: PLant Engineer 3231 Oceanside Blvd.

Oceanside, CA 92056

SUBJECT: RENEWAL TEST REPORT

The enclosed test report is the result of testing done at your facility.

If you have any questions, please call me at (619) 694-3359.

M& C. W. Ridenour

Senior Air Pollution Chemist

CWR:jo

Enclosures

AIR POLLVnON CONTROL DISTRICT 9150 Chlcrapcplu DIITC, S.n Diego, c.llbmL 921u-1095

(619) 694-XWl FAX (6l9) 694-'2lS

Page 31: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

W DIEGO AIR F'OUUTION CONTROL DISTRICT 9150 CHESAPEAKE DRIVE SAN DIEGO, CA. 92123

SUMMARY: SOURCE TEST OF PARTICULATE EMISSIONS TO THE ATMOSPHERE

TEST

TEST SITE:

PERMIT UMiT MEASURED P E R " c E

U. S. Silica 3231 Oceanside Bivd. PO BOX 1280 Oceanside, CA 92054.0243

RULE54 DUST AND FUME 40.00 ibhr

TEST#: 90257 P.04 236 TESTDATE 9/14 /90

c 2.00 ibshr PASSED

EQUIPMENT: Fluid bed dryer on a glass sand process line: crushing, drying, 8 screenlng systems with dust laden air lrom bagging & lower bin areas vented to an antipoi we1 type air scrubber, 24000 dscfm. w/ 250 gpm of water. (appi. #lossE) (appi. YE60749 gea)

Venturi-type scrubber UNK TESTED

STE PERSONNEL: TED- APCD PERSONNEL: REPORT BY: J. CAWYER DATE 1/2/91

J. CAWYER. T. PREVO

APPROVED B Y L%&&QuulL DATE& C.W. RIDENOUR

~~~~~~

SENIOR AIR POLLUTION CHEMIST

PARAMETEAS: MEASURED: STACKGAS FLOW RATE (DSCFM): 22640

STACK GAS TEMPERATURE O F (AVG): 131

PRODUCTION RATE (AVG): tonSRlr 74

SAN DIEGO APCD U.S. SILICA PAGE 1 OF 14

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TEST DESCRIPTION

Introduction: This report presents the results of particulate loading and gas volume tests at U. S. Silica the fluidized bed dryer.

System Description: Glass sand is dried In a fluid bed dryer which is fired by natural gas. The exhaust from this dryer is pulled through a venturi-type scrubber, the emissions to the atmosphere from this scrubber are the subject of this report.

Procedures: The procedures and equipment utilized In performing these tests are based on EPA New Source Performance Standards Method 5. The sampling train was modified lo exclude the front-end filter and Include a back-end filter. per the San Diego Air Pollution Control District Method 5 testing guidelines. The calculations were designed to include the impinger catch so that the test resuits can be compared to Rule 54 of SDAPCD.

Velocity Traverse: Prellmlnary calculations were based upon data from previous tests. Temperature and pitot tube data collected during actual sampling were used to calculate stack volume.

particulate sampling: This sample consisted of 42 traverse points, 7 from each of 8 sample ports as shown in Figure 1. The sample was collected 114 Inches below the top of the stack. Field data as- sociated wilh sample c~liectlon has been transferred to computer printout and Is shown in the report. Calculations were done by computer and are also shown within the report.

Gas Analysis: An integrated bag sample was collected on site and measured. The oxygen and carbon dioxide content of the stack gas was measured using electronic instrumentation.

. The lest was performed on a Venturi-type scrubber serving the

SAN DIEGO APCD US. SILICA PAGE 2 0 F 14

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i

r 4

SITE: U. S. Slllca Report version I1

TEST DATE: 9114190 DATA SUMMARY: # RAVERS GASMETER PRESS.

Vm It3 ACROSS

BES .oo .oo .oo - - -

0 -Pn 1- 12

,* . I

.82

.BO

.20

.50

.BO

.90

.20

.65

.75

- - - - - - - -

25 0.80

27 I I 1.35

.85

.70

9 c '&

- - ",.

L " , 1 ,

SAN DIEGO APCD

OPERATOF J. CAWYER

TEST 90257

mEss. DRYGASMETER STACK IMP. STACK DIFF. TEMPERATURE T E w T E M P m

U.S. SILICA PAGE 3 OF 14

. _

Page 34: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

3 9 0.05 0.10 89 120 132 40 0.10 0.10 88 120 131 4 1 0.15 0.20 8 9 120 131

SAN DiEGO APCD US. SILICA

64 12.95 68 18.30 6 3 22.42

PAGE 4 OF 14

42 660.365 0.05 0.10 90 124 115 6 2 12.77

A

,

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CALCULATIONS:

UNITS EOUATlON

corr Vwm - ((Vm"Vpw@lmp/Ps)'Pm'Tstd)l(Tm'Psld) MlMBw - water volume correction at meter w/o slllca gel - 1.13 IF3 1

- dry meler volume corrected lo STP - 72.88 n ~ 3 2

Pm- Pbar+(AH/l3.6)- corrected pressure of meter - 30.03 in Hg 3

Tm- (11 +12)R + 480 - meter temperature I 566.6 O R 4

Ts - ts+460 - corrected slack temperature - 590.5 O R 5

Vm sld - (Vm"Tsld'Pm/(Pstd7m))-corr Vwm

Ps- Pbar + (P slatid13.6)- corrected slack pressure = 30.08 In Hg 6

Vw sld - Vlc'a'R7std/(Pstd'MwH2O)+corr Vwm -water volume at STP - 7.63 It"3 7

Bws = (Vw std)/(Vw std+Vm s1d)'lOO - percent molslure - 9.48 % 0

mn- grams of particulate (from laboratory sheet) - 0.0338 grams 9

Cs - 15.43'mnNm std - grain loading (dry) - 0.007 gralnslddscf 10

Vm'- Vm'Y - Corrected dry gas meter volume - 79.13 11'3 11

Md-0.440(%C02)+0.320*(%02)+0.280( N2+lnerts+CO) Dry gas molecular weight - 28.96g/g'mole 12

Ms-Md'( 1 -BWS)+l B.O'(BwS) = 27.92 g/g'mole 13 Stack gas molecular weighbwel bask

SAN DlEGO APCD US. SILICA PAGE5OF14

. .-

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. -.

vs- 85.49'Cp'(lr~'AP)/(Ps'Ms))~.5 - stack velocity

Qs - (vs)'A0'60 - stack flow rate

Qstd -17.64'(3~'(1-Bws)'PsTTs -flow rate at STP

I - 144'100'Ts'(.002669'Vicc(Vm'~m)~Pm)/ (60'0'vs'Ps'An) -isokinetic

E - (O.O0857)'(Qstd)'Cs - particulate emission rate

SUMMARY OF CALCULATIONS:

I - % isokinetics - 97.8 %

Cs - grain loading (dry) = 0.007 gralnsldscf

E - particulate emission rate - 1.39 lbslhr

%Co2 - 1.20 K

SAN DlEGO APCD US. SILICA

EQUATION UNITS MJMBW

74.22 (Ws) 1 4

27834 (acfm) 15

22640 (dsclm) 16

97.76 (%) 17

1.39 (Ibslhr) 1 8

PAGE 6 OF 14

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SITE: U. S. Silica Report version #2 OPERATOF J. CAWYER

31668 1 /2 /04 TEST: 90257 DATA SUMMARY: t

SAN DIEGO APCD US. SILICA PAGE 7 OF 14

-.

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38 0.05 0.10 90 120 133 39 0.05 0.10 89 120 132 40 0.10 0.10 88 120 131 41 0.15 0.20 89 120 131 42 660.365 0.05 0.10 90 124 115

Vm, meter 80.782 W3

Vlc. impingers 137.7 m i Vpw@ imp - 0.459 inHg

METER BOX PARAMETERS

w- 2.61 inH20 Dn- 0.173 i n

AP - 3.90 iflH20 An - DnA2'n/4 - .0235 in%?

NOZLE AND PROBE

AH - 2.27 inH20 Cp- 0.807

62 12.96 64 12.95 68 18.30 63 22.42 62 12.77

METER BOX I.D.# D337 Y - .9796 STACK MEASUREMENTS STACK PARAMETERS

? a 0 2 1.20 Slack Diameter - 2.50 It

%co 0.00 Ao-Area stack - 6.25 11V

%02 19.10

%NZ 79.70

0 - sampling Ume 126 mlnutes

mn-particulate coliect'd 0.0338 grams

SAN DIEGO AFCD U.S. SILICA PAGE 8 OF 14

._

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CALCULATIONS:

UNITS

Corr Vwm - ((Vm"Vpw@imp/Ps)'Pm'Tstd)/(Tm'Pstd) EQUATION NuMaw - water volume correction at meter wlo silica gel - 1.13 It"3 1

- dry meter volume corrected to STP - 72.88 w 3 2

Pm- Pbar+(AH/l3.6)- corrected pressure of meter - 30.03 in Hg 3

Tm- (11 +tZ)L? + 460 - melw temperalure - 566.6 O R 4

Ts - ts+460 - corrected stadc temperature - 590.5 'R 5

Vm sId - (Vm'7std'Pm/(Pstd7m))-co~ Vwm

Ps- Pbar + (P static113.6)- corrected stack pressure - 30.08 in Hg 6

Vw std - VIca'R7std/(PsM'MwHZO)+corr Vwm - water volume at STP P 7.63 1tA3 7

Bws - (Vw std)l(Vw std+Vm std)'100 I percent moisture - 9.48 % 8

mn- grams of particulate (Irom laboratory sheet) - 0.0338 grams 9

Cs - 15.43'mnNm std - grain loading (dry) - 0.007 grainsld dscl 10

Vm'- Vm'Y - Corrected dry gas meter volume - 79.13 ft"3 11

Md-0.440(%C02)+0.320*(%02)+0.280(N2+1nerts+C0) Dry gas molecular weight - 28.96 glg'mole 12

Ms-Md'(l-BwS)+l B.O'(Bws) - 27.92 glg'mole 13 Slack gas molecular weight-wet basis

SAN DIEGO APCD US. SIUCA PAGE9OF14

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VS- 85.49.Cp'((TS'AP)/(PS'MS))'.5 - stack velocity

Qs - (vs)'A0'60 - stack flow rate

Qstd -17.64'Qs'(l-Bws)'P~s -flow rate at STP

I - 144*10D'Ts'(.00266s'Vic+(Vm'/lm)'Pm)/ (W'Wvs'Ps'An) -1soklnetic

E - (O.O0857)'(Qstd)'Cs - particulate ernlsslon rate

SUMMARY OF CALCULATlONS

I - % lsokinetlcs - Cs - grain loadlng (dry) I

E - particulate emission rate - %Co2 -

Corrected Cs -CS (llioo) -

81.0 %

0.007 gralnsldscl

1.68 lbslhr

1.20 %

0.006 gralnsldscf

EQUATION UNITS W B W

89.61 (fVS) 14

33605 (acfm) 15

27333 (dscfm) 16

80.97 (%) 17

1.68 (Ibslhr) 1 8

Corrected E - 0.00857'Qstd'Cs corr = 1.36 lbslhr

SAN DiEGO APCD U.S. SILICA PAGE 10 OF 14

-

Page 41: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

NOMENCLATURE

muitlpiicatlon I division A exponentlath Vm Vm AP

AH 11 dry gas meter inlet temperature - (OF) 12 dry gas meter outlet temperature - (OF) 1s stack temperature - (OF) ti lmpinger out temperature - ('F) vs Pbar - barometric pressure - (in Hg) Pstatic - stack static pressure - (in Hg) Ps - Absolute stack pressure - Pbar +(Pstatic/13.6) - (in Hg) tm - dry gas meter temperature -(titG?)L? - (OF) Vic - collected water.impingers - (mi) Vpw - Vapor pressure of water - (in Hg) AH @ - orifice pressure differential that equates to 0.75 cfrn of air @ 68QF and 29.92 in HQ Dn - nozzle diameter - (In) An - nozzle area - x'DnW4 - (InV) II - the ratio of circumference of a circle to Its diameter - 22i7 (dimensionless) Cp - pitot tube coefficient - (dimensionless) Y - meter box coefficient - (dimensionless) CO2 - carbOn dioxide - (96) CO - calbon monoxide - (%) 02 -oxygen - (%) N2 - nitrogen - (%) 0 - sampling time D (minutes) mn - particulate found in sample train - (grams) A0 - stack area - stack diameterWd4 i f round; length 'width if rectangiar = (1162) Corr Vwm - ((Vm"Vpw@imp/Ps)'Pm'Tstd)/(Trn'Pstd) - (ft"3) Pm - absolute meter pressure I Pbart(AW13.6) - (in Hg) Tstd - temperature at standard conditions - (528OR) Tm - dry gas meter temperature -(t1+12)12+460 - (OR) Pstd - pressure at standard condition - ( 29.92 in. Hg) Vm std - dry corrected volume of meter - Vm'T std'Pml(Pstd'Tm)-corr Vwm - (ft"3) Ts - stack temperature - (OR) Vw std - water volume at STP - Vlc'a'R'Tstdl(Pstd'MwH20) - (ftfi3)

sample gas volume. uncorrected - (fta3) sample gas volume, corrected - Vm'Y - ftA3 root mean pilot tube differentlal pressure

average differential pressure across the orifice - (in H20) - (summatlon(press.dlff. across pitot tubesA.5)lnumbsr entries)V - (in H20)

stack gas velocity - 85.49'Cp'(Ts'APl(Ps'M~))~.5 - (fVs)

SAN DIEGO APCD US. SILICA PAGE 11 OF 14

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NOMENCLATURE w n t

a - denslly of water at STP - 0.002201 - (Iblml) R - Ideal gas constant - 21.65 In. Hg'ftA3PR'lb'rnole

Bws - fractional stack gas rnolsture content - (Vw std+Corr Vwrn)/(Vwstd+Corr Vwrn+Vrn std)

Cs - grain loading - 15.430'mnNm std - (gralns/dscf) Mw - molecular weight - (g/g'rnole) MS - wet stack gas molecular weight - Md'(l-Bws)+Bws'l8 - (glg'mole) as - flow rate - vs'Ao'6O - (acfm) Qstd - flow rate at standard condltlons - 17.68'Qs'(l-Bws)'PsTTs - (dscfm) I - lsoklnetlcs - 144'1 00'Ts'(.002669'Vlc+Vm'~1n~Pm/(60'0'vs'Ps'An) - ( O h )

E - particulate emlsslons rate - O.W847*Cs*Qstd I (Ibshr) MwH20 - molecular weight of water - 17.98 (g/g'mole)

CONSTANIS:

Md - dry Stack gas molecular weight - 0.32'%02+0.44'%C02+0.28(100-%02-%C02) - (glg'mole) - (Wt 00)

0.00847 Ib/(gr'mlnhr) - 1 lb/7000gralns'60 mlnlhr 13.6 In H 2 0 h Hg 17.68 W n Hg 60 sedmln 32 g/g'mole 02 molecular weight 44 glg'rnole - CO2 molecular welght 26 s/g'mole - N2 molecular welght 18 glg'rnole - H20 molecular welght 85.49 (ft/sec)'(lb'ln Hg/(lb'rnole'oR'ln H20))".5 0.04707 - ftA3/ml 460 (demenslonless) - wnverslon O F to O R

144 lnA2/ftA2 15.43 gr/g 0.002669 In Hg'ftA3/(DR'ml)

SAN DIEGO APCD U.S. SILICA PAGE12OF14

-.

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NOTE:

Note concerning compliance test #go257 for U.S. Silica performed on 9/16/90.

1) Velocity Data:

It was found during the process of this test that the stack flow velocity had a large amount of variation, The delta p readings varied from zero to above five inches of water. The magnahelic that was used during this test measures to only five inches of water. Therefore, for the first five readings of this test the delta p value is unknown. Two calculations have been generated. The first uses a value of 5.00 inches of H20 for the unkown points and the second calculation uses and arbitrary maximum value of 20.0 inches of H20. Using 20.0 inches of H20, the %I is 81.0%. Correcting for this low %I the emission rate is 1.36 Ib/hr. Using the 5.00 inches of water pressure readings the %I is 97.8% and the emission rate is 1.39 Iblhr. Higher values of delta p would decrease the o/ol, thus indicating oversampling. Therefore, this test shows compliance for a limit of 40 Ib/hr however, this data is not accurate and should not be used to determine emissior inventory data or other data which necessitates precise and accurate data.

2) Production Data:

The production data taken for this test was data that was requested from site personnel. This data, besides not having any corollation with APCD engineers or sourcetesting crew, is based upon estimated monthly tonnage and monthly operating hours. during the testing, I was informed that that information was not available.

When asked for specific tonnages and hours

SAN DIEGOAPCD US. SILICA PAQE 13 OF 14

~

1 ~

!

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NOTE: con't

3) Site Platform Condition:

Improvements to the site platform are recommended before any further testing be performed. The angle of the platform side guards as they extend from the stack to the walkway are at such an angle that makes it necessary to use only a 3 ft probe. Even with a 3 ft probe it is a tight fit. Also, a 6 ft support board is needed to support the impingers at a proper level. During this particulate test it was noticed by T. Prevo that the platform was decaying in several areas and that he considered it to be unsafe. It is my recomendation that the platform be rebuilt and that the angle extending from the stack to the walkway be reevaluated so as to make it more accessible for the sourcetest team.

Janet E. Cawyer Acting Assistant Chemist San Diego Air Pollution Control District

SAN DlEGO APCD US. SILICA PAGE 14 OF 14

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> .. . I ,-, P.

SAN DIEGO AIR POLLUTION COXTZOL DISTRICT

TRAVERSE POINTS

U. S: SILICA

EXHAUST FROM FLUID BED DRYER

BO" 1 . . __

Figure 1

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-. Page 6 _<

-- i ':I -.

I !

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a

.

- b

s In c 2

E a? E

a? c I- t

i

Page 48: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

1

m

E 0

E

P

i

N

Page 49: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

0 0 In

e

i P a

.. -

I

i z

I .. c

0 ID In m

% p"

a a w

L .. m e

- E w w w

?- In 01 0 m 0

(0 In

I

P I - - a .. ..

Q 9 m

0

f 3 *

Page 50: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

0 0 0 0 B g g

t a

0 0 0

0 0

3 s 0 x

i

0

0

Page 51: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

i

b In N 0 al

I a Li w I-

I - - a .. .. P 9 m

I

{! i

I ..;.a E 9 m

In

.. ::a I

!!i z

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0 0 0 N O N r r o N N O 7 7

m 0 0 0 2 m m

0 0 -

? z

i

0 0 0

8

0 0 0

5 x s z b z

m

u) N 0

o w 0 0 0 0

8

o w w

Page 53: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

i

h

Page 54: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

la:

FROM:

COMPANY NAME

LOCATION ATIENTIOM # OF PACES (XNC. COVER)

FACSIMILE MESSAGE

FACSIMILE TELEPHONE NUMBER (619) 433-9615

. :. . . . .:.. . . . . . . . . '. .

. . . . :.

# M E

LOCATION

DATE

wxh - U. S. SILICA - OCEANSIDE. CA -

Phons (619) 757-2b30 if ,problem with thir transmittal . . Dryer throughput :

Auy. 32,70 1 394.8 SepD. - Dee. 104,623 1,392.8

Sun. - 4. 23B,269 3,225 Sepi . (Est.) 2 ~ 0 0 6 3%

1940 -

. .'

. . . .

. . : :

, . .

. . . .

!

U.S.'Silica Company - 3231 Oceanside Blvd. - Omanside, CA 920S6 - (619) 757-2630

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I

I 5DC-47

METHOD 5 PRELIMINARY DATA SHEET

PRELIMINARY TRAVERSE DATA Stack Temperature: aveSqL.4 min I 13 max f7'/ previous test r e p o r t : z Stack velocity Delta P ave 1.64 min , lo max Y . m (ChedcoffSOurceOf data) % moisture \q.b\ I GasMD(Dry) 17 . rS Nozzle Diameter used: , I 7 3 Traverse Point Layout (attach sketch): Nomograph AHH/AP ratio:_LL_.

OUTSIDE REQUESTS: APCD engineer-- Barometric Request:

a v e m min- max- on site traverse:=

Optimum nozzle Dia:&I

J

/

PRE$TEST CiiiCKS: Traverse Points M a r k e d 2 I Sample Time at Traverse Point: 2 !ob "A)&.

PortsCleaned - Port S k z ledlar Bag Leak Checked-/ Temperatke Sensors (at ambient temperature) ts 7 v p tbox 7 ydF ti 7 Y - F

SDAPCD FIGURE 5 3 A

. .

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PRETEST LEAK CHECKS: MeterOrificeCheck J Sample Line r e 7 dm I min Limit: 0.02u-m !

PitotTubes High Y . 4 inmo I S sec . LOW 3.0 inH20 L s e c

SAMPLING CHECKS: Hot Box Heater O n : - Probe Heater On. - ImpingersIced - Static Pressure: f.00

POSlTEsT LEAK CHEKS Meter Orifice C h e c k L Sample Line nav dm I min Limit 0.02dm PitotTubes High 3 . 0 inmo

LOW 7 . 0 inmo

,. . . x

FIGURE 5-3A

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SAN DIEGO AIR POLLUTION CONTROL DISTRICT . h us- 51.l.I L A . . h

ORIFICE CHECK 4 l w l s s . .

Yc = (0*(0.0319'Tm/bar)A0.5)/Vm

Pretest check

(run at &i@ for 0 minutes)

..

TIME T1 T2 V M start: n *. ao 7 g " P 4 7 O F 5 1 7 I % g

T o q 76°F I n",; -7 . cvio finish:

PBar

average: i Y Z - L & 2 2 F +460

; (0.97 5 Yc/Ym S 1.03)

-I-- --_- -

Post test check

TIME '11. TI VM PBai start: 0:ob S F I = 79-r 0 7 . 7 3 g

finish: y: e0 / I f 0,- gp/r &

net: XxsL 2&%25 J+UlB.GL z.tLu

Yc= .'?%SO Ym= .47?6 Yc/Ym=

(0.97 5 Yc/Ym S 1.03)

average: 9sof 75S°F +460

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FIELD DATA SHEET #Z:CO"T

Ps. absolute - Tm, absolute fi0%3?) 7 6 9 .3a a ~ @ across meter 2. c 123

% moisture . I33 L

correction factor 9 &= s.56 h6°f= )

Ts, absolute 5 7 b . 4 .aP stack I . 2 - v

Ideal nozzle dlam l f 7 f / 7 3 . t73 nozzle used

test differential pressure

K 3 I . O @

CLILP K'= \ , \

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Poua3b. . . Sample No.

AmDlmtof Imp. Tip lmpinger No SoutionUsed Solution (ml) Configuration Weight (prams)

I --- m vq9.75

2

3

4

5

6

- him Wt. Gain - hila Wt.Gain .

GAS ANALYSF RESULTS

Gar Fractional Part

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. . ..__..._.... .__._._.. * _._.__. M .._.-. .. . .. .-.... .-. ...-- --... .-.. -

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.

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Page 67: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.+ .n

TEST

RULE 54 DUST AND FUME

SAN DIEGO AIR POLLUTION CONTROL DISTRICT 9150 CHESAPEAKE DRIVE

SAN DIEGO. CA. 92123

SUMMARY SOURCE TEST OF PARTlCUlATE EMISSIONS TO THE ATMOSPHERE

40.00 Ib/hr 1.68 lbshr PASSED

TEST SITE U.S. SILICA

TEST #: P.0.b TEST DATE:

EQUIPMENT.

UNIT TESTED

SITE ENGINNER: SITE PERSONNEL: APCD ENGINEER: APCD PERSONNEL REPORT BY: DATE: APPROVED B Y DATE:

C.W. RIDENOUR SENIOR AIR POLLUTION CHEMIST

PARAMETERS: STACK GAS FLOW RATE (OSCmn):

STACK GAS TEMPERATUREeF (AVO):

PRODUCTION RATE (AVO): tonshr

MEASURU): 27307

131

RESULTS Based upon APCD Method 5 Standards relating to the entire impinger catch. I PERMITLIMIT I MEASURED

TEST REFERENCE San Diego Alr Pollullon Control Dlstrlcl Quality Assurance Manual Method 5 for Particulate Emlssions from Stationary Sources.

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.O.# 870054 PAGE 1 OF 8

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, ' .

TEST DESCRIPTION

Introduction: This report presents the results 01 particulate loading and gas volume tests at 0 . The test was performed on the baghouse exhaust.

System Description: The crushed rock, sand, and hot asphalt oil are heated and mixed in the rotary drum. The rock and sand are dried In a rotary dryer which is heated by natural gas. The exhaust from this dryer is vented through a baghouse. the emissions to the atmosphere from this rotary dryer are the subject of this report.

Procedures: The procedures and equipment utilized In performing these tests are based on EPA New Source Performance Standards Method 5. The sampling train was modified to exclude the front-end filter and include a back-end filter. per the San Diego Air Pollution Control District Method 5 testing guidelines. The calculations were designed to Include the lmplnger catch so that the test results can be compared to Rule 54 of SDAPCD.

Veloclty Traverse: Preliminary caicuiatlons were based upon data from previous tests. Temperature and pilot tube data collected during actual sampling were used to calculate stack volume.

Particulate Sampling: This sample consisted of 20 traverse points, 10 from each of 2 sample ports as shown in Figure 1. The sample was collected 24 inches below the top of the stack. FieM data as- sociated with sample wilectlon has been transferred to computer printout and is shown In the report. Calculations were done by computer and are also shown within the report.

Qas Analysis: An Integrated bag sample was wllected on site and measured. The oxygen and carbon dioxide content of the stack gas was measured using electronic instrumentation.

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.0.W 870054 PAQE 2 OF 8

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SITE 0 OPERATOR:

TEST DATE TEST: 0

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.0.I 870054 PAGE 3 OF 8

.

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# Pressures are In Inches of water. temperatures are In degrees Fahrenheit, velocltles ere in ftlsec. All measurements are actual - uncorrected - values.

80.782 3.90 2.27 s o 123 131 5 7 89.63 Average: Vm AP AH 11 12 1s t i VS

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.O.# 870054 PAQE 4 OF 8

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DATA SUMMARY:

PRESSURES AVERAGETEMPERAWRES

P bar 29.86 in Hg ts - 131 F

P static 3.00 in H20 tm 1/2(avg.tl+avg.l2) - 107 F

PS 30.08 in Hg ti - 5 7 F

VOLUMES VAPORPRESSURES

Vm, meter 80.782 ft"3

Vlc. impingers 137.7 m i Vpw@ imp - 0.4688 inHg

METER BOX PARAMETERS

A N 3 - 2.6123 inH20 Dn- 0.173 in

AP - 3.90 inH20 An - DnA2*d4 - .0235 inA2

NOZZLE AND PROBE

AH - . 2.27 inH20 Cp- 0.8070

METER BOX 1.D.t D337 Y - ,9796

STACKMEASUREMENTS STACK PARAMETERS

%02 1.20 Slack Diameter - 2.50 It

Y d x 0.00 Ao-Area stack - 6.25 ftA2

%02 19.10

%N2 79.70

0 - sampling tlma 126 mlnutas

mn-particulate coiiect'd 0.0338 grams

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.0.t 870054 PAGE 5 OF 8

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..a . .

CALCULATIONS:

UNITS EQUATION

corr Vwm - ((Vm"Vpw~imp/Ps)'Pm'Tstd)/(Tm'Pstd) VJMem - water volume correction at meter w/o silica gel = 1.15 ft.3 1

- dry meter volume corrected to STP - 72.86 1tA3 2

Pm- Pbar+(AH/l3.6)- corrected pressure of meter - 30.03 In Hg 3

Tm- (11 +tZ)L? + 460 - meter temperature I 566.6 "R 4

Ts - 0+460 - corrected stack temperature I 591.0 O R 5

Vm std - (Vm"Tstd'Pm/(Pstd'Tm))-corr Vwm

Ps- Pbar + (P staIidl3.6)- corrected stack pressure - 30.08 in Hg 6

Vw std - Vlc*a'R7std/(Pstd'MwH2O)+corr Vwm - water volume at STP - 7.65 11'3 7

Bws - (Vw std)/(Vw std+Vm std)'lOO - percent molsture - 9.51 % 8

mn- grams of particulate (trom laboratory sheet) - 0.0338 grams 9

Cs - 15.43'mnNm std - Orain loading (dry) P 0.007 grains/dsc, 10

Vm'- Vm'Y - Corrected dry gas meter volume - 79.13 11'3 11

Md-0.440(%C02)+0.320'(%02)+0.280(N2+inerts+C0) Dry gas molecular weight - 28.96 g/g'mole 12

Ms-Md'(1 -Bws)+l E.O'(BwS) - 27.91 g/g'moie 13 Stack gas molecular weight-wet basis

vS- 85.49*Cp*((Ts*AP)/(P~'Ms))~.5 I stack velocity 89.63 (ft/s) 14

Qs - (vs)'Ao'GO D stadc flow rate 33610 (acfm) 1 5

Qstd -17.64'Qs'(l-Bws)'Pfls -flow rate at STP 27307 (dscfm) 1 6

I - 144'100'Ts'(.00266S'Vlc+(Vm'~m)'Pm)/ (60'0'vs'Ps'An) -isoklnetic

E - (O.O0857)'(Qstd)'Cs - particulate emission rate 1.68 (Ibs/hr) 1 8

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.O.# 870054 PAGE 6 OF 8

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,- h

SUMMARY OF CAiCULATIONS:

Enter the type of plant. (AsphaltCombusUon)

I - % lsoklnatlcs - 81.0 %

Cs - graln loading (dry) - 0.007 gralnsldscf

E - partlculate ernlssion rate - 1.68 Ibslhr

%Co2 - 1.20 %

Corrected Cs- Cs * ( l / lOO)= 0.006 Oralnsldscf

Corrected E- 0.00857'Qstd'Cs Cor1 1.36 lbslhr

SAN DlEGO AIR POLLUTION CONTROL DISTRICT P.O.% 870054 PAGE 7 OF 8

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.* , . .

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.O.# 870054 PAGE 4 OF 8

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DC- 44 . I

-. P

# Pressures are in inches of water. temperatures are in degrees Fahrenheit, velocities are in ftlsec. All measurements are actual - uncorrected . values.

Average: Vm AP AH 11 12 t S t i 80.782 2.1 1 2.27 90 123 131 5 7

vs 74.24

SAN DlEGO AIR POLLUTION CONTROL DISTRICT P.O.# 870054 PAGE 5 OF 8 ~

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DATA SUMMARY:

PRESSURES

P bar 29.86 in Hg

P 8tatlc 3.00 In H20

PS 30.08 In Hg

VOLUMES

Vm, meter 80.782 f t ~ 3

VIc, implngers 137.7 m i

METER BOX PARAMEERS

AH@ = 2.6123 lnH20

AP - 2.11 lnH20

AH - . 2.27 Inti20

METER BOX 1.D.X 0337

STACKMEASUREMENTS

%c02 1.20

%co 0.00

%02 19.10

%N2 79.70

0 - sampling time 126 minutes

mn-particulate coiiecrd 0.0338 grams

AVERAGETEMPERATURES

ts 131 F

bn - lL?(avg.tl+avg.t?) - 107 F

ti - 5 7 F

VAPOR PRESSURES

Vpw@ Imp I 0.4686 InHg

NOZZLE AND PROBE

Dn= 0.173 In

An - DnA2'n/4 - .0235 in"2

Cp- 0.8070

Y - .9796

STACKPARAMETERS

Stack Diameter - 2.50 ft

Ao-Area stack = 6.25 W 2

SAN DIEGO AIR POLLUTION CONTROL DISTRICT P.0.X 870054 PAGE 6 OF 8

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CALCULATIONS:

corr Vwm - ((Vm"Vpw@lmp/Ps)'Pm'Tstd)/(Tm'Pstd) - water volume correctlon at meter w/o sllica gel - Vm std - (Vm'7std'Pm/(Pstd7m))-corr Vwm - dry meter volume wrrecied to STP

Pm- Pbar+(AH/l3.6)- corrected pressure of meter

Tm- (tl+t?)R + 460 - meter temperature

TS - ls+460 - corrected stack temperature

P

- I

- Ps- Pbar + (P statW13.6)- corrected stack pressure -

VW std - Vlc'a'R7std/(Pstd'MwH2O)+corr VWm - water volume a1 STP - Bws - (Vw std)/(Vw std+Vm std)'lOO - percent moisture -

mn- grams of particulate (from laboratory sheet)

Cs 15.43'mnNm std - grain loading (dry) - .I

Vm'- Vm'Y - Corrected dry gas meter volume I

Md-0.440(%C02)+0.320'(%02)+0.280(N2+1nerts+CO) Dry gas molecular welght I

Ms-Md'(l -BWS)+l B.O'(Bws) I

Stack gas molecular welght-wet basis

vs- 85.49'Cp'(Cr~.AP)/(Ps'Ms))~.5 - slack velocity

Qs - (vs)'A0'60 - stack flow rate

Qstd -17.64'Qs*(l-Bws)'PslTs -flow rate at STP

I = 144'400'Ts*(.002669'Vlc+(Vm'TTm).Pm)l (GO'O'vs'Ps'An) -1soklnetlc

E - (O.O0857)'(Qstd)'Cs I partlculate emission rate

UNITS EQUATION NllMBw

1.15 n ~ 3 1

72.86 It"3 2

30.03 in Hg 3

566.6 O R 4

591.0 'R 5

30.08 In Hg 6

7.65 n ~ 3 7

9.51 % 8

0.0338 grams 9

0.007 grainsldsc 10

79.13 11'3 11

SAN DlEGO AIR POLLUTION CONTROL DISTRICT P.0.I 870054 PAGE 7 OF 8

28.96 g/g'mole 12

27.91 g/g'mole 13

74.24 (ft/s) 14

27840 (aclm) 15

22618 (dscfm) 16

97.83 (W 17

1.39 (Ibslhr) 18

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SUMMARY OF CALCULATIONS

Enter the type of plant. (Asphalt/Combustion) lAsphaltI

I - % isoklnetlC8 - 97.8 %

C8 - grain loading (dry) - 0.007 grainsldscf

E - particulate emission rate - 1.39 lbslhr

%Co2 - 1.20 Ye

SAN DlEGO AIR POLLUTlON COMROL DISTRICT P.O.# 870054 PAGE 7 OF 8

...

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i

Q

t

Page 80: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

E E E E

.

- E

6 c1

c m v)

E E E E E

- Z ' E E E E

U

m

c 0

E

i

N

3 P

Page 81: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

0

11 0

m m m

ll

.. ' ; : ; a P

m a Y

m o w

L

I m

s m e

i

m

n 9

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. .,< i

0 0 0 0 0 x

m m

P 0

0

0

0 e

m m m

m m m

# ? E x 4

i

U

Page 83: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

i

f. 0 N

m a w 0 0 0

0 9

U , . ~ a Q

m 5

a m w

.. - = a U

P

w w w

t Y ._

Lo

P P

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SAN DIEGO A I R POLLUTION CONTROL D I S T R I C T 9150 CHESAPEAKE D R I V F - SAN OIEGO, CALIFORNIA

TEST NO.: 87163

P.O. NO.: 0236

TEST DATE: JUNE 12, 1987 '

SOURCE TESTED: U. S. S I L I C A CO. 3231 OCEANSIDE BLVO. OCEANSIDE, CA 92056

U N I T TESTED: F L U I D B E 0 DRYER

PERFORMED BY: P. JARMAN G. CARRIER

REPORT PREPARED BY: P. JARMAN

c. RIOENOUR A. SEGAL (ENG)

'APPROVED By: C.M. RIDENOUR

SENIOR A I R POLLUTION CHEMIST

3/9/87 DATE

INDEX

SUMMARY OF RESULTS . . . . . . . . . . . . 1

TEST DESCRIPTION . . . . . . . . . . . . . 2

F I N A L CALCULATIONS . . . . . . . . . . . . 3

TRAVERSE POINTS, FIGURE 1 . . . . . . . . 5

S I T E DESCRIPTION, FIGURE 2 . . . . . . . 6

PARTICULATE SAMPLING TRAIN, FIGURE 3 . . . 7

SAMPLE COLLECTION DATA . . . . . . . . . . 8

LABORATORY DATA 10

U N I T OPERATION DbTA . . . . . . . . . . . 1 1

. . . . . . . . . . . . .

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SAN DIEGO COUNTY AIR POLLUTION CONTROL D I S T R I C T

PAGE 1 TEST DATE1 J u n e 12. 1987

TEST NO. : 87163

P.O. NO. : 0 2 3 6

SUMMARY: EMISSIONS TO ATMOSPHERE

NAME OF FIRM: U. 5. S i l i c a Company

LOCATION OF PLANT: 3231 O c e a n s i d e B l v d .

TYPE OF OPERATION: P r o c e s s i n g a n d B a g g i n g Sand

U N I T TESTED: F l u i d B e d D r y e r

MEASURED EMISSIONS ALLOWABLE EMISSIONS

RULE 5 2 PARTICULATE G r a i n s G r a i n s MATTER, DRY p e r SCF p e r SCF

RULE 53A SULFUR COMPDS AS SO-2, DRY X b y VOL. % b y VOL.

RULE 5 3 8 COMBUSTION G r a i n s p e r G r a i n s p e r SCF 012% COZ SCF 012% CO2 CONTAMINANTS

G r a i n s p e r G r a l n s p e r RULE 53C INCINERATORS SCF 812% coz SCF eizx coz

L b s / H r 40 L b s l H r RULE 5 4 DUST 6 FUMES 3.68

EMISSION RATES

GAS FLOW RATE. DSCFM 25.742 PARTICULATES: 3*68 L b s / H r

GAS TEMPERATURE. ‘F 121.0 CAVE) OXIDES OF

PRODUCTION RATE 70.3 T o n s / h r

NITROGEN : L b s l H r

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L ,.-” h

TEST NO. 87163 PAGE 2 P.0. NO. 0236

TEST DESCRIPTION

Introduct ion This report presents the resul ts o f part iculate loading and gas volume tests performed a t U.S. S i l i c a Co., on June 12, 1987. The tests were performed on the exhaust stack o f the water scrub- ber serving the F lu id Bed Dryer. while production averaged 70.3 tons per hour.

System Description Glass sand I s dried i n a natural gas f i r e d F lu id Bed Dryer. The exhaust from the dryer i s pul led through a venturi-type scrubber. This report shows the emissions i n t o the atnosphere frm t h i s scrubber.

Procedures The procedures and equipment u t i l i z e d I n performing these tests were based on EPA New Source Performance Standards Method 5. t r a i n was modified as shown cm Page 7. The calculat ions were de- signed to include the lmplnger catch so t h a t the t e s t resul ts can be cunpared to Rule 54 o f SDAPCD.

Velocity Traverse P r i o r Information regarding the stack veloci ty p ro f i le eliminated the need for a separate exploratory traverse. Temperature and p i t o t tube data col lected during actual sampling was used t o calculate actual stack volume.

Par t icu la te Sampling This sample consisted of 42 traverse points, 7 frm each sample p o r t as shown I n Figure 1. on page 5. The sample was col lected a t 3 minutes per po int for a t o t a l t e s t time of 84 minutes. The sample was col- lected 7 feet frun the exhaust ou t le t of the stack. F ie ld data as- soclated with sample col lect ion has been transferred to computer p r in tou t and I s shown on Page 8 and 9. Calculattons were performed by computer and are shorn on Pages 3 and 4. Though the Isoklnet lc Sampling ra te I s outslde the usual recunnmnded range, the emission I s acceptable I n accordance with c r i t e r i o n contalned i n Appendix A, Part 10. SDAPCb Quali ty Assurance Guidllnes and Operattonal Procedures. The isok inet ic variance was caused by the assumed moisture content being 5% lower than previously measured.

Gas analysis Carbon dioxide and oxygen content of the stack gas was measured by Orsat. according to EPA NSPS W h o d 3. The resul ts of t h i s analysis are on Page 4. 4.

Canaents The s i t e I s I n disrepair compared to l a s t year. There are substantial holes and leaks i n the ducttng. These were t m p o r a r l l y sealed during the t e s t but should be repaired.

The sampling

.

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c .-.

PAQE 3

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF SAN DIEQO

TEST NO. 67163 U.S. S I L I C A RUN 1

A. V METER VOLUME, UNCORRECTED+FACTOR

E. P METER PRESSURE, P + H/13.6

C. T METER TEMPERATURE, 46O+(T +T ) / 2

m

m . . b a r

m 1 2 D. T IMPINQER TEMPERATURE

i

TEST DATE JUNE 12. 1967

- E. T AVERAGE STACH TEMPERATURE, 460+DEG. F =

F. P STACK PREBSURE. P + P /13.6 = S

9 b a r g

i a 4 0. VP MAX.H 0 VP PERMITTED AT T (SEE APPENDIX) =

H. v VOLUME OF CONDENSED H o ( ~ E E LAE SHEET) 3

I C 2

c a l c a I. V H 0 VAPOR METER COND.8 H W I E i 0 . 0 0 2 6 7 P

J. V MOISTURE METERED AT METER COND. 8 A i Q / E - K. V SAMPLE VOLUME AT METER COND. I DRY, A-J D

wv

d v L. %M PER CENT MOISTURE CALC.. 1 0 0 r ( I + J ) / ( A + I ) D

M. VP MAX. H 0 VP PERMITTED AT T (SEE APPENDIX) - C

0 a S N. %M PER CENT MOISTURE PERMITTEDo M/F*lOO P

B ENTER LOWER O F L OR N - 0. M.C. MOISTURE CORRECTION FACTOR, (100-L OR N)/IOO-

P. V SAMPLE VOL. 3 STD COND. (DRY K*326 /29 . 92*E/C E

S

ws

m( a t d )

n 9. m WEIQHT O F PARTICULATE MATTER COLLECTED =

1. c QRAIN LOADINQ (DRY). 15.43rS/P = S

P 38.45 C U Qt

P 29.9s . i n H g

D 539. DEQ. R

= 4s. DEQ. F

sal. DEQ. R

30.09 i n Hg

.32 i n Hg

119. m l

3.93 cu f t

. b 3 cu Qt

97.82 cu t t

10.19 x

3.94 i n Hg

11.8 x

' 10.2 x

.e98

94.615 eu f t

.os9 g

017 g r a i n s l s c 9

Page 88: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAQE 4

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF 8 A N DIEGO

TEST NO. 87163 U.S. S I L I C A

TEST DATE JUNE 12, 1987

RUN 1

DD. C P I T O T TUBE CORRECTION FACTOR 3

P EE. V 'STACK VELOCITY AT STACK COND. (SEE SAMPLE DATA)-

5 FF. V STACK VEL. AT STD COND. (DRY).EE*529/29.92+F/E,O =

s ( 6 t d ) 00. DURATION OF SAMPLING P

HH. AVERAQE SAMPLINQ RATE (DRY),P/QG P

11. SELECTED NOZZLE DIAMETER =

JJ. SAMPLING VELOCITY AT STD COND.,HH/I1+*~*144/60*4/3.-

KK. I I SOK I NET I C VAR I AT I ON. J J IFF* 100 E

LL. A AREA OF STACK E

MM. Q FLOW RATE AT STD. COND. (DRY), FF*LL*6O P

5

sd

,922

83. 71 f t / n c c

6 8 . 6 5 f t / s c c

124. min

,433 scfrn

. 149 in 61.30 f t / s e c

89. x

6.23 o q Pt

29742. a c f m

NN. Q FLOW RATE AT STACK COND., EE*LL*bO 9

31391. a c f m

3.48 l b / h c VU. PARTICULATE E f l I S S I O N RATE, 0.00847*T*MM D

,

Page 89: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

-7

SAN D I E M AIR POLLUTION CONTROL DISTRICT

TRAVERSE POINTS

CRYSTAL SILICA

EXHAUST FROM FLUID BED DRYER

B

SAMPLING PORTS C

D

E

F

L.

:+ ..+ .+. + . . .

+ + + +

. + + + + . .

+ + + + + +

+ + +

+

+

+

f.

+

+ + +

+ I

'i

, .' IO.*" '' , I6 . .

1 9 a-

.. . "\ ' . . . 23 V i .

1

t 27*4*

Figure 1

Page 90: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

' FIQJIIF, 2 '

3 .

Page 91: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

- .- '

~

SAN DIEW C O W AIR WLLUTION CONTROL DISTRICT

STACK Sensor W A L L

Page 7

Umbilical IIIPINGERS Cord I

O r i

Dry Cu Ueter Vacuum Pmp

LEGEND FIEU) DATA ABBREVIATIONS Green-th lrpe Ispingera

No. 1 Mod- 100 ML Deionized Mater PT = Point Number

No. 2 Std- 100 MI. Deionized Water - Stack Temperature. OF 3 = Pitot Tube Pressure Differential, in.H20

VEL- Stack Velocity, fps H = Orifice Meter Pressure D&p. in. HzO . TI = Eleter In l e t Temperature, OF T2 = Neter Outlet Temperature, OF P, = Pump Vacuum, in. Hg Ti = Impinget Temperature, OF Pbar = Bsmmstric Pressure. in. Hg

NO. 3 Fbd- D r y

No. 4 Mod- Dry

Ebd - Wodifidd Type Std - Standard Type

FIGURE 3: PARTICUUTE NATTER SAMPLING TRAIN

Page 92: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

- - PACE 8

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF SAN DIEQO

TEST NO. 87163 U.S. SILICA RUN 1

PT

A1 A2 A3 A4 A 5 A 6 A7 El E2 E3 E4 E5 E6 E7 c1 c2 c3 c4 cs Cd c7 D1 D2 D3 D4 D5 D6 D7 El

T

123. 127. 123. 122. 125. 123. 128. 123. 124. 122. 121. 130. 128. 128. 125. 123. 123. 123. 127. 123. 122. 124. 121. 123. 122. 125. 128. 125. 120.

s P

1.500 1. 500 1.300 1.300 1.200 1.300 1.300 1.400 1.600 1.300 1.300 1.400 1.900 1. 500 1.500 2.000 1.500 1.600 1.600 1.800 1.800 1.000 2.000 1. eo0 1. 800 2.000 2.300 2.300 1.800

VEL

71. 6 71. 9 66. 7 66. 6 64. 2 66. 7 66. 9 69. 2 74. 0 71. 5 66. 5 69. 6 71. 9 71.9 71. 7 82. 7 71. 6 74. 0 74 .2 78. 4 78. 4 58. 5 82. 5 78. 4 78.4 82. 8 89. 0 88 .8

n

. 7 9

. 7 9

. 60

. 60

. 9 5

.60

. 60

. 6 5

. 7 5

. 70

.60

. 6 5

. 70

. 70

. 7 0

. 9 0

. 7 0

. 7 5

. 7 s

. 8 0

. B O

. so

. 90

. 8 0

. 8 0

. 90 1. 0 5 1. 0 5

78.2 . e a

TEST DATE JUNE 12. 1987

T T P T cn 1

78. 0 78. 0 78.0 78. 0 78. 0 78. 0 78. 0 BO. 0 80. 0 BO. 0 80. 0 84.0 102.0 82 .0 112.0

a 96. 0

100.0 104.0 108.0 108.0 110.0 110.0 108.0 112.0 114. 0 114.0

82.0 116.0 84.0 100.0 84.0 114.0 84.0 116.0 84.0 118.0 84.0 118.0 84.0 120.0 84.0 120.0 86.0 110.0 86.0 118.0 86 .0 120.0 86.0 120.0 86.0 120.0 8 6 . 0 122.0 8 6 . 0 122.0 08. Q 112.0

m . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00 . 00

i 44.00 43.00 43.00 42.00 42.00 42.00 42.00 42.00 44.00 44.00 44.00 46.00 44.00

._ 2

1. 30 1. 30 1.30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1.30 1. 30 1. 30

.OO 44.00 1.30

.OO 46.00 1.30

. 00 44.00 1. 30

. o o 44.00 1.30

. 00 44.00 1. 30

.OO 42.00 1.30 . 00 43.00 1.30

. O O 43.00 1.30

.M) 42.00 1.30

. O O 44.00 1.30

. 00 44.00 1.30

. 00 44.00 1.30

. 00 44.00 1.30 . 00 43.00 1.30 . 00 45.00 1.30

.OO 44.00 1.30

Page 93: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.- _- PAQE 9

A I R POLLUTION CONTROL DEPARTMENT - COUNTY O F BAN DIEQO

TEST NO, 87163 U.S. S I L I C A RUN 1

P T

E2 E3 E4 E5 E6 E7 F I F2 F3 F4 F5 F6 F7

AVO

T

115. 11s. 114. 123. 120. 123. 111. 107. 111. 114. 115. 116. 117.

9

121.

P

2.500 2.600 2.900 3.000 3.200 3.500 3.200 3.200 3. 500 4.000 4. 200 4.000 3. 800

2. 058

VEL

91. 8 93. 6 98. 8

101.3 104.3 109.4 103. 5 103. 1 108.3 116.0 1iV. 0 116.2 113.4

TEST DATE JUNE 12, 1987

SAMPLE COLLECTION DATA

H

1. 1s 1.20 1.35 1. 40 1.45 1. 60 1.45 1.45

T

as. 0 88. 0 89. 0 90. 0 88. 0 sa. 0 86. 0 66. 0

I T P T

2 m 1 iao.0 .oo 44.00 122.0 .oo 44.00 116.0 .OO 44.00 114.0 .OQ 46.00 118.0 .OQ 47.00 120.0 1.00 47.00 110.0 1 . 0 0 47.00 120.0 1.00 47.00

1.60 86.0 120.0 1 .00 47.00 1.80 86.0 122.0 2.00 48.00 1.90 86 .0 122.0 2.00 49.00 1. so 86.0 122.0 2.00 48.00 1. 70 86. 0 124.0 2.00 48.00

co 2

1. 30 1.30 1. 30 1. 30 1. 30 1. 30 1.30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30

03 .7 .98 83.9 114.6 . Z 9 44. 69 1.30

AVERAQE DELTA P = 2.1429

DRY QAS METER VOLUME UNCORRECTED 96.470 P = 29.88in ng b a r

METER CORRECTION FACTOR * 1.0390 P (STACK PRESSURE) P 2 . 8 in water 5

NOTES - 1. AVO P IS THE BGUARE OF THE MEAN ( 8 G . R T ) 2. (VEL) VEL*COS(ANQ) 3. AVO CO IS THE VELOCITY WEIQHTED AUERAQE

2

Page 94: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

,A - TEST NO. 8 3 I b 3 h

.AGE 19 COUNTY OF SAN OIEGO - A I R POLLUTION CONTROL DISTRICT

PARTICULATE M A T E R LABORATORY DATA

PARTICULATES

A. ACETONE WASH Final -/.OC2Dg Net W t . (o~LC~ NOZZLE, PROBE IHPINGERS.

Pan c a Tare I 0 I lb-g

8 . WATER WASH Final 024s Net W t . &/7 L g NOZZLE, PROBE, IHPINGERS. IMP- INGER CATCH-

Pan I Tare /.&?-3g

C. BACK-UP FILTER Flnal / , l Z 3 : Z , Net Ut. r o o / B g

Pan I && Tare I t D l Y I 4 F i l t e r I fi Tare ~1D?3 g

D. BLANKS

-1 Water g/100ml .-& Water Correction

-1 Acetone *pm/ g/100nl .-g k e t o n e Correction

Water Pant &-3 B-S’g Net Weight Acetone Pan# - tu-& Total Weight o f Par t i cu la te Hatter

Condensed Molsture Final -1 Wash Volumes

(A + 8 + C - D)

Impinger t a r e -1 Acetone 171 m l

Net Galn &ml F i 1 tered 0.1, Water ? g l

Imp. Tare 260 ,III

Total Water 278 m l

Page 95: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

. . . . . . . . . . . .

I. %D"CVQN b4m . . . . . .

0907. (&-4tz~-~&r>... - .- .. ...

.-T%F . . . .T~.GE.. ... --.-- A z& ..... ,A - ~ ~ E ~ M N s . . ~ & F . . . . / k h & L . . . I_

. ............. ...... '-GAB

. . . . . 09..16 45513.24 . .. .- . . . . . . . . . . . . . . . . . . . . . . . . - . . . . . . . .

$I 8 , .................. . . . . . . . . . . . . . ...... 4 1 q/b . . . . . . .

. . . . . . 09 2 * !.c510 I 20

,, I , . . . . . . . . . . . . . . . . . . . . . . . . . 1.8. ID '5 72! 4

% # 2q 32 7387 ., ., .

0935 4 55356,30 I O I,

. . 1967 4 53- 73; 59

Page 96: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

... -

.... . . . . . . . . . . . . . . . . . . . . .- ... . . . . . . . . . . . . . . . . . . . . . . . . - ..... +

%N.~.L T ; ; N N A G L . . - . ~ ~ ~ = ~ ~ L ~ , ~ ~ ~ . . L . . . . . . . . . . . . . . .......... . . . . . .

4 5664t.06 ...- 4 . S 5 G t Z . q . . . ... ? ....... !.TQc.Y.Z..T;;Y~.. . . . . .. ...

........................... .

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .- ..... - .............. ._ ...... -_ - 0 JE 5 & L . . ~ k @ 4 6 ~ %wcr?orJ. p&i=.= ....... 170 ..I 82 / . . .&43 = .?C?.3 .??'$A& .......

.. . ..... . . . . . . . . . . . . . . . . . . . . . . . ..........

. z.. ~ ~ I . . P ~ E ~ J . _ O P ~ ~ - ~ ~ . o / J , . . . . . . . . . . . . . . . . . . . - . . . . . . . . . . . . . . .

.............. . . . .. ..TEWEIU.TUPE. *K. . ..?&a- 'ki :.- ........... .FTIG ..........

.... 0910.. ...... . . . . . . 7 . h ..2*0. . 'BO . 100 I & -!5 . - 9 . -*45 . . . . 2 5 . .......

093Z~ azl . . . . . . . . . . . . . . . . . . . . . . .

0935 ?@ 223. !&.. . lo0 16 ..? 4 . . . . - 8.8 3 4 5 . . . . . . . 2 5 . .

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

. . . . . . . . . . . . . . . . . . ... .

. . . . . . . . . . . . . . . , .,. 0 43 ...@$ E.e. &.TO %sT. EQdr PM C~ r) e955 ... ....e- 7

Page 97: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

I .., -.

.. . - .... - . .- .... - ...... ... ..... --.AQIZS-:.- c --

-_ ...L ..r.trsrw~L-irrlQ-4 ~1~.3.7~&-- . -. .... ... ~- ............ . .......

............... ................. . ......

...... . . . . . . . . .

.... ... ... . . . . . . . . . . . . . . . . . . . . . . . . ... - .. - -. ....... - . ....... .......

. . . . . . . . . .

Page 98: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

... - . . . . . . . .....

.. -

. . . . . ....... _. ......... ..................

. . . . . ,. . ..................... . .

Page 99: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

DISTUIEL~ONI \MITE - APUI FILE YELLOY - APCD INSPECT^ PIK - aiw

~

.. APCD030587 -- . . . , .. . . .. . .

Page 100: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

W h aiv C,

X

4'

Page 101: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

R. J. Sommewille Air Pollution Control Officer apcd County ot Sm Diego

U. S. S i l i c a Company H r . Dan S t o v e r 3231 Oceanside Blvd. Oceans ide , cn 92056

D e a r S i r :

The e n c l o s e d test r e p o r t i s t h e r e s u l t of t e s t i n g done a t your f a c i l i t y .

If you have any q u e s t i o n s . p l e a s e Cal i me a t ( 6 1 9 ) 565-5911.

C.W. Rldenour Senior Air P o l l u t i o n Chemist

CWR:pj

Enclosures

AIR POLLUTION CONTROL DISTRICT 9150 Chesapeake Drive. San Diego, California 92123-1095

Page 102: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.

f4 P w to

r 8

f e .

a 4

3 Is-, . fi- iJ

k W

f4 k

i

Page 103: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at
Page 104: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.

Page 105: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

< 0

.

I

Page 106: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at
Page 107: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

- . AIR POLLUTION .*ITROL OEPARTMENT - couriv O F ~ I OIESO

.. ORSAT FIELD DATA

m u. 0 to * Q. I9 Dc 8 8.0 - ao.9 Ot 2 0 *‘i 20c7 80.9 ,

I R

co

T e s t No. 83/63

SAYPLE # A . AVERAGE ANALYSIS SAMPLE t

Page 108: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

871631 O U . 8 . S I L I C A 29.88

12. 8 573. 500 ,629. 970 ,3203 3.543 119.0 1.035 1.3 0. 0 18. 8 79. v ,822 6.25 . 147 126.0 . O W 0 0. 0 0. 0 0 . 0 A 1 A2 A 3 A4 A5 A 6 A7 81 82 83 84 85 Q6 87 c1 c2 c3 c4 c5 Cb c7 D I D2 D3 04 D5 D6 D7 E l E2 E3 E4 E5 E6 E7 F1 F2 F3 F4

123. 127. 123. 122. 125. 123. 128. 123. 124. 122. 121. 130. 128. 128. 125. 123. 123. 123. 127. 123. 122. 124. 121. 123. 122. 125. 128. 125. 120. 115. 115. 114. 123. 120. 123. 111. 107. 111. 114.

1 .9 1. 9 1.3 1.3 1. 2 1. 3 1. 3 1 . 4 1.'6 1. 5 1.3 1 . 4 1. 5 1. 5 1 . 5 2.0 1. 3 1.6 1. 6 1. 8 1. 8 1. 2. 1.8 1 . 8 2. 2. 3 2. 3 1. 8 2. 5 2. 6 2. 9 3. 3. 2 3. 5 3 . 2 3. 2 3. 5 4.

. 7 5 78.

. 7 5 78.

. 6 78.

.6 78.

. J S 78.

. 6 78.

. 6 78.

. 6 5 80.

. 7 5 80.

. 7 80.

. 6 80.

. 6 5 84.

. 7 82.

. 7 82.

. 7 84.

. 9 84.

. 7 84.

. 7 5 84.

. e 84.

. 8 84.

. 5 86.

. V 86.

. 8 86.

. 7 5 84.

. a 86.

. v 86. 1. 05 86. 1. 05 86. . e 88. 1. 15 88. 1 .2 88. 1. 35 89. 1. 4 90. 1.45 m. 1. 6 88. 1. 45 86. 1. 45 86. 1. 6 86. 1. 8 ' 86.

I

JUNE 120 1987 ..-.

V6. 100. 104. 108. 108. 110. 110. 108. 112, 114. 114. 102. 112. 116. 100. 114. 116. 1 18. 118. 120. 120. 110. 118. 120. 120. 120. 122. 122. 112. 120. 122. 116. 114. 118. 120. 110. 120. 120. 122.

0. 0 0. 0 0. 0 0 . 0 0. 0 0. 0 0 . 0 0. 0 0 .0 0 . 0 0. 0 0. 0 0. 0 0 . 0 0. 0 0 . 0 0. 0 0. 0 0. 0 0. 0 0. 0 0. 0 0 . 0 0 . 0 0. 0 0. 0 0. 0 0. 0 0 . 0 0. 0 0. 0 0 . 0 0. 0 0 . 0 1. '

1. 1. 1. 2.

44. 43. 43. 42. 42. 42. 42. 42. 44. 44. 44. 46. 44. 44. 4b. 44. 44. 44. 44. 45. 45. 42. 44. 44. 44. 44. 45. 45. 44. 44. 44. 44. 46. 47. 47. 47. 47. 47. 48.

1.3 1.3 1; 3 1.3 1. 3 1.3 1.3 1.3 1.3 1 .3 1. 3 1.3 1.3 1 .3 1.3 1.3 1.3 1.3 1. 3 1.3 1.3 1.3 1 . 3 1 .3 1.3 1.3 1.3 1. 3 1 .3 1.3 1.3 1. 3 1 .3 1.3 1 .3 1.3 1 .3 1.3 1.3

. .

Page 109: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

_- !?5 1.15. 4. 2 1 . 9 86. 122. 2. 49. 1. 3 F6 116. 4. 1. E 86. 12- 2. 48. 1. 3 F7 117. 3.8 1. 7 86. 12 ... 2. 48. 1. 3 END . .42

Page 110: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

- PAGE

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF SAN D I E G O

TEST NO. 87163 U.S. S I L I C A RUN 1

TEST DATE JUNE 12. 1987

SUMMARY F I N A L CALCULATIONS 1. c GRAIN LOADING(DRY) P ,017 grains/acf

VU. PARTICULATE E M I S S I O N RATE P 3.68 l b / h r B

00. XCO (GAS ANALYSIS) a

P 1.30 X

.

Page 111: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

W 3 0 Arrive a t PPCO

o S a 9 Leave APCD

k7 1 port change \\%3 port change Port change

Port change Port change Port change

i\5b End t e s t

Quick 6 leak check cmplete

Equipment dismantle complete

Leave s i t e

Arrive APCD

COMMENTS:

I

Page 112: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

c3 . . *

. . , _i ..., . ~. .. . . . C. ..

,/- 2 +; , ' .; .. . '

. TEST NO.: mIL3 . .

TEST DATE: &ht/87 TEST SITE: 19 ss 6/clc'n4- . .

.',

LOCATION:. b C - < , l c ' h v A ~ L L H \ ; \ i e

SOURCE TEST PERSONNEL: A w . --La* t ' \Cc fl 't i q,n~Ur

FACILITY CONTACT : m%k Lw<

APCD INSPECTOR: . . .

SA)IIPLE-BOY No.: .2

APCO ENGINEER: <-a\ - a . . e

. , ' ,. . .. . .

.. . . . . . . . . . . ?.::& . s'. 3 : ~ 1 ' ' Fo G , , .,. ..: .. ., . . .

Y . . . . . METER BOX N9.: b-3-57 .._.+:;,$.SI' . . . .

/ I 3 i . . .. . . . . . . . .

.. . . . . . FILTER NO.: .

NOZZLE DIAMETER: 0 I v-7 L

STACK SIZE: 3 + 3 0 ' 6. K$! AMBIENT TEW.. OF: &' ASSUME0 IrOISNRE. Z: /a

k *a- . . 9

NO. OF WPLE POINTS:

HINUTES/POINT: ?&/!e STOP TINE: I\ s% TOTAL TEST TIME: (1.b -, FINAL VOLUK. d: 6zq.770

0967 . . . START TI#:

INITIAL VOLUME. F?: '573. <oo

. .

. d ,;" LEAK O(EcKS: INITIAL ' .

6k- 4 O L & f l

'*

1. VAC. LINE (REO):

2. PRESSURE LINE (GREEN):

3. SAMPLE LINE: < ,oz ccm (MUST BE 0 . 0 0 2 FT3/MIN.)

SDAPCO URD 10/17/84

Page 113: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

. . P /'.

SAN UIECO COUNTY AIR POLI.UTION CONTROL DISTRICT

UNIT# b.

ABSOLUTE PRESSURE IN METER:

ABSOLUTE PRESSURE IN STACK: -9 a e 9 2-

ABSOLUTE TEMP. IN METER: - w9= PRESSURE DROP ACROSS METER. 2 ~ 7 Y. MOISTURE OF STACH CAS.

CORRECTION FACTOR: I , 7 L L

AVE. DIFFEREUTIAL PRESSURE: z,qX7 X L - IDEAL NOZZLE DIAMETER.

rlOZZLE USED: b f v

STACK TEMPERTURE: &ooF I I : 1

TEST DIFFERENTIAL PRESSURE:&# '//#W &< ?,f rF z, =Y w\+-* 4559

&%/I.-

-

Page 114: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

-1 . ... ,/-

Page 115: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

. I .

Page 116: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at
Page 117: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

.. ,

-. -. ' 871-631 0 U . S . SILICA . 29, 88

2. 8 573. 300 629.970 ,3203 3.543 119. 1.035 1 .3

... -

- 0 . 0 18. 8 - 79. 9 . a22 6. 25 . 147 126. . 0590 0.0 0 . 0 0. 0 - A 1 123. 1 . 5 . 7 0 78. A2 127. 1.5 .70 78. A 3 123. 1.3 .60 78. A4 122. 1.3 .60 78. A 5 125. 1 . 2 . 5 5 78. A6 123. 1.3 . 6 A 7 128. 1.3 . 6 E1 123. 1.4 . 6 5 E2 124. 1 .6 .75 - E3 122. 1.5 . 7 0 E4 121. 1 .3 . 6 E5 130. 1 . 4 . 6 5 - B6 128. 1.5 .70

78. 78. EO. 80. EO. 80. 84. 82.

07 128. 1.5 .70 82. Cl 125. 1.5 .70 84. - ca c3 c4 - C5 C6 c7 DI D2 03 D4 D5 D6

123. 2. 0 123. 1. 5 123. 1. 6 127. 1. 6 123. 1. 8 122. 1 . 8 124. 1. 0 121. 2 . 0 123. 1. 8 122. 1.8 125. 2. 0 128. 2 . 3

.9 84.

.70 84.

.73 84.

. 7 3 84.

. E O 84.

.a0 84.

. 5 86.

.90 86.

. 80 86.

. 80 86.

.90 86. 1. 05 86. - D7 125. 2. 3 1. 05 86.

El 120. 1.8 .a0 88. E2 115. 2. 5 1. 15 88.

I E3 115. 2. 6 1. 2 88. E4 114. 2.9 1. 35 89. E5 123. 3. 0 1. 4 90. - E6 120. 3. 2 1. 45 88. E7 123. 3. 5 1. 6 88. F l i l l . 3.2 1 . 4 5 8 6 . F2 107. 3. 2 1. 45 86. F3 111. 3. 3 1. 6 86. F4 114. 4 . 0 1.8 86.

96. 0. 0 44. 100. 0. 0 43. 104. 0. 0 43. 108. 0. 0 42. 108. 0. 0 42. 110. 0. 0 42. 110. 0. 0 42. 108. 0. 0 42. 112. 0. 0 44. 114. 0. 0 44. 114. 0. 0 44. 102. 0 . 0 44. 112. 0 . 0 44. 116. 0. 0 44. 100. 0. 0 46. 114. 0. 0 44. 116. 0. 0 44. 1lE. 0. 0 44. 118. 0 . 0 45. 120. 0 . 0 45. 120. 0 .0 43. 110. 0 .0 42. 118. 0.0 44. 120. 0 . 0 44. 120. 0 . 0 44. 120. 0 .0 44. 122. 0 .0 43. 122. 0 . 0 45. 112. 0 . 0 44. 120. 0 . 0 44. 122. 0.0 44. 116. 0. 0 44. 114. 0. 0 46. 118. 0 .0 47. 120. 1 .0 47. 110. 1.0 47. 120. 1.0 47. 120. 1.0 47. 122. 2 .0 48.

JUNE 12. R E 7

1 . 3 1. 3 1 .3 1.3 1.3 1.3 1.3 1. 3 1.3 1.3 1.3 1.3 1.3 1 .3 1.3 1.3 1. 3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 Il$ 1.3 1. 3 1. 3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1.3 1. 3 1. 3 1.3

Page 118: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

- ' F S v ' 1 1 5 . 4 . 2 1 . 9 86. 122. 2.0 49. 1 . 3 . F6 116. 4 . 0 1.8 86" 122. 2 . 0 48. 1.3

F7 117. 3. 8 1. 7 Ob. 124. 2 .0 48. 1. 3

42 -. . END

-

Page 119: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAGE

A I R POLLUTION CONTROL DEPARTMENT - COUVTY OF SAN DIEGO

TEST NO. 87163 U.S. SILICA RUN 1

TEST DATE JUNE 12, 1987

PT

A1 A2 A 3 A4 A 5 A6 A7

T

123. 127. 123. 122. 125.

9

P

1 .500 1.900 1.300 1.300 1.200 1.300 1. 300 1. 400 1.600 1. 500 1.300 1.400 1. 500

VEL

71. 6 71. 9 66. 7 66. 6 64. 2 66. 7 66. ? 69.2 74. 0 71. 5 66. 5 6?. 6 71. 9

H

. 7 0

. 70

.60

T T P T m i . 00 44.00

co a

1. 30 I

78. 0 78. 0 78. 0

2 96. 0

100.0 104. 0

. 00 43.00

. 00 43.00 1. 30 1. 30 1. 30 . 60

. 5 5 78. 0 78. 0 78. 0 78. 0 80. 0

108.0 108.0 110.0 110.0 108.0

. O O 42.00

. 00 42.00

. 00 42. 00

. 00 42.00 , 00 42.00 . 00 44.00 . 00 44.00 . 00 44.00 . 00 44.00 . 00 44.00

116.0 . 00 44.00 100.0 . 00 46. 00

. 00 44.00

.oo 44.00

. o o 44.00

1. 30 1. 30 123.

128. .60 . 6 0 . 6 5

1. 30 1. 30 81

82 83

123. 124. 122.

. 7 3

. 70 EO. 0 80. 0

112.0 114.0

1. 30 1. 30 1. 30 84

85 B6 87 c1

121. 130. 128. 128. 125. 123. 123.

.60

. 6 3

. 7 0

. 7 0

.70

. 9 0

. 7 0

. 7 5

. 75

. BO

. 80

. 50

. 90

. 80

. 8 0

80. 0 84. 0 82. 0

114.0 loa. 0 112.0

1. 30 1. 30 1. 30 1. 30 1. 30

1.900 1. so0 2.000 1. 500

71. 9 71. 7 82.7 71. 6

82. 0 84. 0

c2 c3

84. 0 84. 0 84. 0 84. 0 84. 0 84. 0 06. 0 86. 0 86. 0 86. 0 86. 0 86. 0 86. 0 88. 0

114.0 116.0 118.0

1. 30 1. 30 1. 30 1. 30 1 . 30

c4 CS C6 c7 D l

123. 127. 123.

1. 600 1.600 1: 800

74. 0 74. 2 78.4 78. 4 56. 5 82. !3 70. 4 78. 4 82. 8 89. 0

118.0 120.0

.oo 45.00

. o o 43.00 122. 124.

1.800 1.000 2.000 1.800 1.800 2.000 2.300

120.0 110.0 118. 0 120.0 120.0

. 00 45.00

. O O 42.00

. 00 44.00

. 00 44.00

.oo 44.00 120.0 .oo 44.00 122.0 . 00 45.00

. o o 45.00

. 00 44.00

1 . 30 1. 30 D2

D3 121. 123. 122. 125. 128.

1. 30 1.30 D4

D5 D6 D7 El

. 9 0 1. os

1. 30 1. 30 1. 30 1. 30

125. 120.

2.300 1.800

88. 8 78. 2

1. 0 5 , e o

122.0 112.0

Page 120: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAGE

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF 8AN DIEGO

TEST NO. 87163 TEST DATE JUNE 12. 1987 U.S. S I L I C A RUN 1

SAMPLE COLLECTION DATA

PT T

E2 115. E3 115. E4 114. E5 123. E6 120. E7 123. F1 111. F2 107. F3 111. F4 114. F5 115. F6 116. F7 117.

s P VEL H

2. 300 91.8 1. 15 2.600 93.6 1.20 2.900 98.8 1.35 3.000 101.3 1.40 3.200 104.3 1.45 3.500 109.4 1.60 3.200 103.5 1.4Y 3.200 103. 1 1.43 3. 500 108.3 ! . 6 0 4.000 116.0 1.80 4.200 119. 0 1.90 4.000 116.2 1.80 3.800 113.4 1.70

T 1

88.0 88. 0 89. 0 90. 0 88. 0 88 .0 86.0 86. 0 86. 0 86. 0 86. 0 86. 0 86. 0

T 2

120.0 122.0 116.0 114.0 118.0 120.0 110.0 120.0 120.0 122.0 122.0 122.0 124.0

P T m 1 . 00 44.00 .oo 44.00 . 00 44.00 . 00 46.00 .oo 47.00

1.00 47.00 1.00 47.00 1.00 47.00 1.00 47.00 2.00 48.00 2.00 49.00 2. 00 48.'00 a. 00 48.00

co 2

1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30 1. 30

AVO

VEL = 85.48irC +SG. RT. ( ( P I T l / ( P +MI 1 P 5 5 5

AVERAGE DELTA P p 2.1429

DRY GAS METER VOLUME UNCORRECTED 56.470 P - 29.88fn Hg bar

METER CORRECTION FACTOR m 1.0350 P (STACK PRESSURE) = 2.8 i n Uater 5

NOTES - 1. AVG P I 8 THE SQUARE OF THE MEAN (SG.RT) 2. (VEL) = VEL*COS(ANG) 3. AVO co IS THE VELOCITY WEIGHTED AVERAGE

2

Page 121: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAGE

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF BAN DIEGO

TEST NO. E7163 U.S. S I L I C A RUN 1

A. V METER VOLUME, UNCORRECTED*FACTOR m ...

8. P METER PRESSURE, P + Hl13.6

C. T METER TEMPERATURE, 460+(T +T ) / a

D. T IMPINQER TEMPERATURE

E. T AVERAGE STACK TEMPERATURE, 460+DEG. F

F. P STACK PRESSURE, P + P /13.6

C. VP MAX.H 0 VP PERMITTED AT T (SEE APPENDIX)

m b a r

m 1 2

i

5

5 bar g

i 2 i

I C 2

c a l c 2

H. v VOLUHE OF CONDENSED n o (SEE LAB SHEET)

I . V H 0 VAPOR I M T E R COND.4 HK/Br0 .00267

J. V MOISTURE METERED AT METER COND., A+Q/B

K. V SAMPLE VOLUME AT METER COND., DRY, A-J wv

dry L. %M PER CENT tlOISTURE CALC. lOO*(I+J)/(A+I) .a M. VP MAX. H 0 VP PERMITTED AT T (SEE APPENDIX)

N. %M PER CENT MOISTURE PERMITTED, M/F+100

C

S 2 5

6 = E ENTER LOWER OF L OR N

WO

0. H. C. MOISTURE CORRECTION FACTOR, (100-L OR N)/100*

P. V SAMPLE VOL. STD COND. (DRY), K* !528/29,92*EIC P

m t s t d )

n D 9. m WEIGHT OF PARTICULATE MATTER COLLECTED

1. c GRAIN LOADING (DRY). 19.43*S/P = 5

TEST DATE JUNE 120 1987

38.45 cu f t

29.93 in ng

559. DEQ. R

45. DEQ. F

581. DEG. R

30.07 i n Hg

.32 in Hg

119. m l

5.93 cu Q t

.63 cU e t

57.82 cu f t

10.19 x

3. 54 i n Hg

1 l . E X

10.2 x

. 898

54.614 C U f t

. O S 9 9

.017 graine/scP

Page 122: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAQE

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF SAN DIEQO

TEST NO. 87163 U.S. S I L I C A

TEST DATE JUNE 12, 1987

RUN 1

AA. M 9

- - ,822 DD. C P I T O T TUBE CORRECTION FACTOR P E € . V STACK VELOCITY AT STACK COND. (SEE SAMPLE DATA)- 83.71 Pt/eec

68.65 f t l s e c FF. V STACK VEL. AT STD COND. (DRY), EE*528/79,92*F/E*O - QQ. DURATION OF SAHPLING

S

~ ( s t d ) = 126. min

P HH. AVERAQE SAHPLINQ RATE (DRY).PIGG

X I . SELECTED NOZZLE DIAMETER

JJ.

KK. I I S O K I N E T I C VARIATION# JJ /FF* lOO

LL. A AREA OF STACK

HM. G FLOW RATE AT STD. COND. (DRY). FF*LL*6O

P

SAMPLING VELOCITY AT STD COND.,HH/I1+*2*144/60*4/3.= - - =

5 D

Sd

NN. G FLOW RATE AT STACK COND., EE*LL*60 S

P

1 UU. PARTICULATE E M I S S I O N RATE, 0.00847*T*Ml l

.433 s e f m

,147 in

61.30 f t / s e e

89. x

6.23 S q C t

23742. scfm

31391. a c f m

3.68 l b / h r

Page 123: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at

PAGE

A I R POLLUTION CONTROL DEPARTMENT - COUNTY OF SAN DIEQO

TEST NO. E7163 U.S. SILICA RUN 1

TEST DATE JUNE 12. 1987

SUMMARY FINAL CALCULATIONS P .017 grains/scf T. c GRAIN LOADINGCDRY)

W . PARTICULATE EMISSION RATE 3.68 l b l h r 5 E

aa. xca (GAS ANALYSIS) 2

3 1.30 X

Page 124: Title: Emission Test Reports for U.S. Silica, …...I” 1. ,/ ,. ,-- TEST DESCRIPTION Introductlon: Thls report presents the results of partlculate loading and gas VOiume tests at