UNDtROROUND ENCINEFRING & ENVIRONMENTAL SOLUTIONS · (0 026 milligrams per liter) in the composite sample from MW-26C drill cuttings ... Water Quality in Bedrock Assessment Groundwater

H A I I Y & :ALDKICII

t -? Other

10 October 2003File No 29213020

US Environmental Protection Agency Region VIISuperrund Division901 North 5th StreetKansas City Kansas 66101

Attention Ms Mary Peterson

Subject September 2003 Monthly Progress ReportChemical Commodities Inc Olathe Kansas

UNDtROROUNDENCINEFRING &ENVIRONMENTALSOLUTIONS

IfUK700 Monn via

t Smtt J10 AT)[im 4 KS ((,215

F«x 9131995822\v\vi\ HikjAldrichcom

OFFICESHi i h nM i tun ttf-C I \ t ] <i dOhm

M ;»<>i nI J n t t n n lC mm itimt

( os \npthsC ulihniM

Mi IK heaterNrv\t wirkM » I r i \i1 uillandMn nKi h

WStn

rnui

1 r mm

I at 11

Dear Ms Peterson

The September 2003 Monthly Progress Report presents an update of Remedial Investigation(RI) and Feasibility Study (FS) activities conducted at the Chemical Commodities Inc site inOlathe Kansas This report has been prepared pursuant to Section XIV Docket NoCERCLA 7 2000-019

Table 1 specifies the work performed and any problems encountered analytical data receivedduring the reporting period and the developments anticipated during the next reportingperiod including a schedule of actions to be performed anticipated problems and plannedresolutions of past or anticipated problems Table 2 provides water quality data collectedduring groundwater sampling of newly installed bedrock wells and surface water sampling atMill Creek Table 3 summarizes constituents detected in the bedrock assessment groundwatersamples collected from newly installed bedrock wells Copies of the analytical data receivedduring September 2003 are provided as Attachment A Figure 1 identifies the bedrockassessment groundwater sampling locations and Mill Creek sediment and surface watersampling locations

40112332

SUPERFUND RECORDS

RECEIVED

OC1 14 2lWSUPCKFUND DIVISION

IIIIIIIIIIIIIIIIIII

US Environmental Protection Agency Region VII

1 10 October 2003Page 2

Please call Brian Mossman (818 586 6015) or me (913 599 5802) if you have any questionsregarding this progress report

Sincerely yoursHAI EY & ALDRICH INC

Michael D Basel Ph D P EVice President

EnclosuresTable 1 - September 2003 Monthly Progress ReportTable 2 - Water Quality in Bedrock Assessment Groundwater and Mill Creek

Surface WaterTable 3 - Summary of Bedrock Assessment Groundwater Analytical ResultsFigure 1 - Phase II Bedrock Assessment Sampling LocationsAttachment A - Copies of Laboratory Analytical Reports

cc The Boeing Company Attn Brian MossmanKansas Department of Health and Environment Attn Rob WeberGeoSyntec Consultants Attn Mark Schultheis

TABLE 1SEPTEMBER 2003, MONTHLY PROGRESS REPORT

CHEMICAL COMMODITIES, INC SITE, OLATHE, KANSAS

ITEM TO BE ADDRESSED ACCORDING TO SECTION XTV of DOCKET No CERCLA-7-2000-019

Work Performed During Reporting Period and Any Problems Encountered

Remedial Investigation / Feasibility Study (RI/FS) activities conducted during the reporting period includeResponse to Kansas Department of Health and Environment s comments regarding the Phase n Bedrock Assessment (letter dated 3 September2003) was submitted to the U S Environmental Protection Agency (EPA) on 9 September 2003 Verbal approval of these responses werereceived by Mary Peterson in a phone conversation on 10 September 2003 so installation of the final Phase n bedrock well could proceed

Notification of Potassium Permanganate Pilot Testing being conducted by University of Waterloo The Boeing Company and Haley &Aldrich Inc was provided to the EPA on 5 September 2003Additional characterization of the bedrock was conducted from September 8 through September 18 2003 per the Phase II Bedrock AssessmentWorkplan (Haley & Aldnch Inc 23 June 2003) The field event included the following activities• Installation and development of seven bedrock monitoring wells (MW-22B MW-23B MW 26C MW-30B MW-31B MW-32B and MW

33B) Locations are shown m Figure 1 One planned bedrock well (MW-31C) was not installed because bedrock and the contact to theEudora Shale were encountered much shallower than expected while drilling at MW-31B (Figure 1)

• Slug testing on five of the seven newly installed bedrock wells MW-30B was dry after well completion and MW-26C could not be testeddue to extremely slow recovery

• Collection of groundwater samples for VOC analysis from five of the seven newly installed bedrock wells (MW-30B was dry and MW-26Ccould not be sampled due to slow recovery) and one prrvate unused well (Figure 1) Water quality parameters (pH temperature andconductivity) were measured during sampling and are provided in Table 2

• Collection of surface water and sediment samples from Mill Creek for VOC analysis Four surface water samples (MC001 throughMC004) and three sediment samples (MC001 MC002 and MC004 no sample collected from MC003 because Mill Creek has a concretebed at this location) were collected at locations shown in Figure 1 Water quality parameters were measured during sampling and areprovided in Table 2

• Collection of soil samples from drill cuttings from bedrock well installation Sample results will be used for profiling prior to disposal

Page 1 of 2 2003-09 CCI MPR Table I xls

TABLE 1SEPTEMBER 2003, MONTHLY PROGRESS REPORT

CHEMICAL COMMODITIES, INC SITE, OLATHE, KANSAS

ITEM TO BE ADDRESSED ACCORDING TO SECTION XTV of DOCKET No CERCLA-7-20CKMH9

Analytical Data Received During Reporting Penod

Analytical data received from the laboratory during the September reporting penod have been summarized as follows (copies of laboratory data areprovided as Attachment A)

Groundwater samples from five newly installed bedrock wells and one private unused well Detections are summarized in Table 3Sediment and surface water samples from Mill Creek No detectable concentrations were found in the Mill Creek sediment or surface watersamples with the exception of acetone (3 3 J [estimated value] micrograms per liter) in surface water at location MC001Soil samples from drill cuttings No detectable concentrations were found in the drill cuttings samples with the exception of trichloroethene(0 026 milligrams per liter) in the composite sample from MW-26C drill cuttings

Developments Anticipated During the Next Reporting Penod Including Schedule of Actions to be Performed, AnticipatedProblems, and Planned Resolutions of Past or Anticipated Problems_______________________________

Haley & Aldrich Inc will conduct a comprehensive round of groundwater sampling per the Phase II Bedrock Assessment Workplan (Haley &Aldnch Inc 23 June 2003)

Page 2 of2 2003-09 CCI MPR Table 1 xls

Table 2Water Quality in Bedrock Assessment Groundwater and Mill Creek Surface Water

Chemical Commodities, Inc SiteOlathe, Kansas

MonitoringLocation

GroundwaterPrivate Unused Welf

MW22BMW23BMW26Cb

MW30BC

MW31BMW32BMW33B

Mill Creek Surface WaterMC001MC002MC003MC004

MonitoringDate

9/9/039/17/039/17/03

NMNM

9/9/039/12/039/12/03

9/10/039/9/039/9/039/9/03

Conductivity(umho/cm)

630822635NMNM813880820

780620550520

pH

7376178NMNM797476

8 1799 799

Temperature(degrees C)

2323523

NMNM202120

22243028

" Private Unused Well is an inactive agricultural well located on property at 505 E Cedarb Groundwater recovery is extremely slow at MW 26C sample has not yet been collected at this locationc MW 30B was a dry after well installation no sample collected

degrees C degrees CelsiusNM Not measuredumho/cm micromhos per centimeter

Table 3Summary of Bedrock Assessment Groundwater Analytical Results

Chemical Commodities Inc SiteOlathe Kansas

MonitoringLocation

Private Unused Well d

MW22BMW23BMW26Cb

MW30BC

MW31BMW32BMW 32B (DUP)MW33B

DateSampled

9/9/20039/17/039/17/03

9/9/20039/12/039/12/039/12/03

Volatile Organic Compounds Results (jig/L) 'Acetone

39J<10<10NSNS<10<10<10<10

Carbon Disulfide

<10068J<10NSNS

<10<10<10<10

cis-1 2-Dichloroethene

047J<10<1 0NSNS

<10<10<10<10

Chloroform

<10<10<10NSNS

<10056J057J<10

2 Butanone

3 7 J<50<50NSNS

<50<50<50<50

Tnchloroethene

52<10<1 0NSNS

<10<10<10<10

Tetrachloroethene

082J<10<10NSNS

<10<10<10<10

a Only analytes detected above the reporting limit are provided in mis tableb Groundwater recovery is extremely slow at MW 26C sample has not yet been collected at this locationc MW 30B was a dry well no sample collectedd Private Unused Well is an inactive agncultural well located on property at 505 E Cedar

jtg/L micrograms per literDUP duplicateJ estimated result result is less than reporting limitNS not sampled

cn•<*•men03CM

oogo

ItoCMCDCM

oo

(JO

'215000 N

«o4.MW31B i^ MW-31C(N<rt Installed)

__ A HILL CSEQCdUng »o UM Cr-K

BASE MAP MOD'FIED FROM MONTGOMERY WATSON HARZA AUGUST 2001G \GRAPH1CS\PROJECTS\CCI\2B954B35 DWG

MC001LEGEND

MW 23B •» BEDROCK MONITORING WELL

® MONrTORING WELL

• SURFACE WATER & SEDIMENT SAMPLE

T GAGE STATION

TR1CHLOROETHYLENE CONCENTRATION (ug/L)DUPLICATE SAMPLES

300

SCALE IN FEET

600

HALEY&ALDRICHCHEMICAL COMMODITIES, INCOLATHE KANSAS

PHASE II BEDROCK ASSESSMENTSAMPLING LOCATIONS

SCALE AS SHOWN OCTOBER 2003

FIGURE 1

IIIIIIIIIIIIIIIIIII

ATTACHMENT A

Copies of Laboratory Analytical Reports

IIIII

IIIIIIIIIIIII

ANALYTICAL REPORT

Boeing/CCI Olathe KS

Lot # E31100190

Haley & Aldrich Inc

SEVERN TRENT LABORATORIES INC

Diane SuzukiProject Manager

September 16 2003

IIIIIIIIIIIIIIIIII

EXECUTIVE SUMMARY - Detection HighlightsE3I100190

REPORTING ANAL YTICALPARAMETER RESULT LIMIT UNITS METHOD

BOHL_WG090903_0001 09/09/03 10 10 001

Acetone 3 9 J 10 ug/L SW846 8260Bcis-1 2 Dichloroethene 0 47 J 10 ug/L SW846 8260B2 Butanone 3 7 J 50 ug/L SW846 8260BTrichloroethene 52 10 ug/L SW846 8260BTetrachloroethene 0 82 J 10 ug/L SW846 8260B

IIIIIIIIIIIIIIIIIII

METHODS SUMMARY631100190

PARAMETERANALYTICALMETHOD

Volatile Organics by GC/MSVolatile Organics by GC/MS

Reference s

SW846 8260BSW846 8260B

PREPARATI ONMETHOD_______

SW846 5030SW846 5030B/826

SW846 Test Methods for Evaluating Solid Waste Physical/ChemicalMethods Third Edition November 1986 and its updates

IIIIIIIIIIIIIIIIIII

SAMPLE SUMMARYE3I100190

SAMPLED SAMPWO # SAMPLED CLIENT SAMPLE ID________________________________________ DATE TIME

FX06JFX064FX07AFX07KFX07MFX07WFX079

NOTE(S)

001002003004005006007

BOHL_MC002MC003MC004

WG09090_WS0909_WS0909_WS0909

MW31B_WG0909MC002MC004

_STS090_STS090

3_000103_03_03_03_903903

0001000100010001_0001_0001

09/09/0309/09/0309/09/0309/09/0309/09/0309/09/0309/09/03

10111314151114

10252030302030

The analytical results of the samples listed above are presented on the following pagesAll calculations are performed before rounding to avoid round off errors in calculated resultsResults noted as ND were not detected at or above the stated limitThis report must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corrosivily density flashpoint Igmtability layers odorpaint filter lest pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight

IIIIIIIIIIIIIIIIIII

HALEY SL ALDRICH INC

Client Sample ID BOHL_WGO90903_0001

GC/MS Volatiles

Lot-Sample #Date Sampled

E31100190 001 Work Order f09/09/03 10 10 Date Recea.'wed

FX06J1AA BBattraa:09/10/03 10 00 MB Hfflum

Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648

PARAMETERDlchlorodlfluoromethaneChloromethaneChloroethaneBromometh aneTrichloro f luoromethane112 Tnchlorotnf luoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert -butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis-1 2 -DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2-Butanone1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene1 1 2 -Tri chloroethane1 2 -Dichl oroethaneTetrachlo roethene2 HexanoneDlbromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Analysis matteAnalysis Tmme

Instrument IDMethod

RESULTNDNDNDNDNDND

NDNDNDND3 9 JNDNDND0 47 JNDNDND3 7 JNDNDNDND5 2NDNDNDNDNDNDND0 82 JNDNDNDND

09/10/0319 06

MSHSW846 826

REPORTINGLIMIT1 02 02 02 02 01 0

1 01 01 01 010)1 01 01 01 a>1 01 01 05 CD1 00 501 01 01 CD1 01 01 05 01 01 00 501 CD5 01 01 01 0

OB

UNITSug/Lug/Lug/Lug/Lug/Lug/L

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

(Continued on next page)

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30

WATER3254202

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID BOHL_WGO90903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 001 Work Order # FX06J1AA Matrix

j Estimated result Result is less than RL

WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Tnmethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro

propane124 Tri chloro

benzeneHexachlor obutadieneNaphthalene1 2 3 -Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate

SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene d8

NOTE(S)

RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

ND

NDNDNDNDNDNDNDNDND

PERCENTRECOVERY10091108

REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)

UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

ug/L

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MC002_WS 090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 -002Date Sampled 09/09/03 11 25Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648

PARAMETERDichlorod if luorome thaneChloromet haneChloroethaneBromomethaneTrichloro f luorome thane112 Trichlorotrifluoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 -Dichloroethene1 1 Dichloroethane2 2 Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2-Butanone1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 DichloropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTet rachlo roe thene2 HexanoneDlbromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order tDate ReceivedAnalysis mateAnalysis TTmme

Instrument IDMethod

RESULTNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

FX0641AA09/10/0309/10/0319 36

MSHSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Wattn10 00 MS Bo

OB



ix WATERam f 325421

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles

Lot-Sample # E3I100190-002 Work Order FX0641AA Matrix WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 T etrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec-Butyl benzenep Isopropyltoluene1 3 -Dichl orobenzene1 4 Dichl orobenzenen Butylbenzene1 2 Dichl orobenzene1 2 Dibromo 3 chloro


benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate

SURROGATEBromofluorobenzene1 2 Dichl oroethane d4Toluene d8

RESULTKDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 0\ 01 01 01 01 01 01 01 01 01 01 01 01 0I 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 401210I 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles


PARAMETERDichlorod if luoromethaneChloromet haneChloroe thaneBromometh aneTrichloro f luoromethane112 Trichlorotrifluoro

ethane1 1 Dichl oroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans-1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 -Dichl oroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order fDate ReceoweedAnalysis matteAnalysis TTnraie

Instrument IDMethod

RESULTNDNDNDNDNDND


FX07A1AA09/10/0309/10/0320 07

MSHSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Mattouc10 00 MB Hftnnni

OB



WATERf 32542i

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MC003_WS090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 003 Work Order # FX07A1AA Matrix WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromofonnIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenzene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen-Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3-chloro


benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate



ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles

Lot-Sample # E3I100190 004Date Sampled 09/09/03 14 30Prep Date 09/10/03Prep Batch # 3254454Dilution Factor 1Analyst ID 004648

PARAMETERDichlorod i f luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrif luoro

ethane1 1 -DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans-1 2 Dichloroethene1 l Dichloroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri Chloroethane2 Butanone1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodlchloromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri Chloroethane1 2 DichloroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order fDate Race owedAnalysis ntatteAnalysis Tnrnie

Instrument IDMethod

RESULTNDNDNDNDNDND


FX07K1AA09/10/0309/10/0320 37

MSHSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Matt10 00 MB

OB



:jnLX WATERSiunm f 325421

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY SL ALDRICH INC


GC/MS Volatiles

Lot-Sample # E3I100190 004 Work Ordeir FX07K1AA Katrajc WATER

PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro


benzeneHexachlor obutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate

SURROGATEBromof luo robenzene1 2 Dichl oroethane d4Toluene d8


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW31B_WG 090903_0001

GC/MS Volatiles


PARAMETERDichlorodif luoromethaneChloromet haneChloroe thaneBromomethaneTnchloro f luoromethane112 Trichlorotnfluoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Trichloroethane2 Butanon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloroethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene1 1 2 -Trichloroethane1 2 Dichl oroethaneTetrachlo roethene2-HexanoneDibromoch loromethaneChlorobenzene1 1 1 2 Tetrachloroethane

Work Order #Date Rece:n.T0ffidAnalysis E&teAnalysis TTmtne

Instrument IDMethod

RESULTNDNDNDNDNDND


FX07M1AA09/10/0309/10/0321 08

MSHSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

KattOLT10 00 MS SBuran

OB



WATERf 3254202

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client San^le ID MW31B_WG090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 005 Work Order # FX07M1AA Hatrxx WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformI sopropyl benzene1 1 2 2 T etrachloroe thane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Tnmethylbenzene2 Chlorotoluene4 -Chlorot oluenetert Butylbenzene124 Tnmethylbenzenesec Butylbenzenep I sopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro


benzeneHexachlor obutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate

SURROGATEBr omo f luo robenz ene1 2 Dichloroethane d4Toluene d8


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)


ug/L


MDL0000000000000000000000

0

00012101222

20308030303040404030203030203030303030303070

30

305040

0000

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MC002_STS090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 -006Date Sampled 09/09/03 11 20Prep Date 09/11/03Prep Batch # 3255091Dilution Factor 1% Moisture

PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochlo romethaneBromodi ch loromethaneBromoformBromomethane2 But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro

propane1 2 Dibromoe thaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 -Dichloroethanecis 1 2 Dichloroethenetrans-1 2 Dichloroethene1 1 Dichloroethene1 2 Dichl oropropane

Work Order tDate Rece:n.T»edAnalysis EtotteAnalysis Tnjme

Analyst IPMethod

RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDND

FX07W1AA09/10/0309/11/0317 12

015590SW846 826

REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010

5 05 05 05 05 0105 05 05 05 05 05 0

Matrix10 00 HE5 Kmnn

SOLID# 3255002

XmsltKiuiineimtJt HD MSDOB

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0

3 01 02 02 02 01 01 01 02 02 02 01 0


1111111111111111111

Client

Lot-Sample # E3I100190 006

PARAMETER2 2 Dichloropropanecis 1 3 Dichloropropenetrans-1 3 Dichloropropene1 1 DichloropropeneEthylbenz eneHexachlor obutadiene2 HexanonelodomethaneIsopropyl benzenep Isopropyl tolueneMethylene chloride4 Methyl -2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Trichlorobenzene124 Trichloro

benzene111 Trichloroethane112 TrichloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane124 Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chlorideXylenes (total)

SURROGATEBromofluorobenzene1 2 Dichloroethane d4Toluene d8

HALEY &

Sample ID

GC/MS

ALDRICH INC

MC002_ST S090903_0001

Volatiles

Work Order # FX07W1AA

RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDND


REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0

5 05 05 0105 05 05 010105 0

RECOVERYLIMITS(60 - 130)(60 140)(60 130)

Matrzx

UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

SOLID

MDL2 01 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0

1 03 02 02 03 02 02 05 02 03 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MC004_STS090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 007Date Sampled 09/09/03 14 30Prep Date 09/11/03Prep Batch # 3255091Dilution Factor 1% Moisture

PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochl o rome thaneBromodich loromethaneBromoformBromomethane2 Butanonen Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromethane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro

propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichl orobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichl oroethane1 2 Dichl oroethanecis 1 2-Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2 Dichl oropropane

Work Order #Date ReceivedAnalysis TTOattreAnalysis TPnrne

Analyst IPMethod



FX0791AA09/10/0309/11/0317 44

015590SW846 826

REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010

5 05 05 05 05 0105 05 05 05 05 05 0

Wattimc10 00 MB Hum

SOLIDt 3255002

irmmlt- mmmmnin- HD MSD

OB



MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0

3 01 02 02 02 01 01 01 02 02 02 01 0


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Bangle ID MC004_STS090903_0001

GC/MS Volatiles

Lot-Sample # E3I100190 007 Work Order FX0791AA Matrix SOLID

PARAMETER2 2 Dichl oropropanecis 1 3 Dichloropropenetrans 1 3 Dichloropropene1 1 DichloropropeneEthylbenzeneHexachlorobutadlene2 HexanonelodomethaneI sopropyl benzenep I sopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro

benzene111 Trichloroethane112 TrichloroethaneTrichloroetheneTrichloro f luoromethane123 Tri chloropropane124 Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chlorideXylenes (total)

SURROGATEBromofluorobenzene1 2 Dichloroethane-d4Toluene d8




REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0

5 05 05 0105 05 05 010105 0

RECOVERYLIMITS(60 - 130)(60 140)(60 130)



MDL2 0\ 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0

1 03 02 02 03 02 02 05 02 03 0


Lot # E31150165

IIIII_ ANALYTICAL REPORT

IIIIIIIIIIIII

Haley & Aldrich Inc



September 29 2003

IIIIIIm

I

I

I

I

I

I

I

I

I

I

I

EXECUTIVE SUMMARY - Detection HighlightsE3I150165

PARAMETER RESULTREPORTINGLIMIT UNITS

MC001_WS100903_0001 09/10/03 11 30 001

Acetone 3 3 J

MW32B_WS091203_0001 09/12/03 15 30 003

Chloroform 0 56 J

MW32B_WS091203_0002 09/12/03 15 30 004

Chloroform 0 57 J

10

1 0

1 0

ug/L

ug/L

ug/L

ANAL YTICALMETHOD

SW846 8260B

SW846 8260B

SW846 8260B

IIIIIIIIIIIIIIIIIII

METHODS SUMMARYE3I150165

PARAMETERANALYTICALMETHOD

Volatile Or games by GC/MSVolatile Organics by GC/MS

Reference s

SW846 8260BSW846 8260B

PREPARATI ONMETHOD______

SW846 5030SW846 5030B/826

SW846 Test Methods for Evaluating Solid Waste Physical/ChemicalMethods Third Edition November 1986 and its updates

IIIIIIIIIIIIIIIIIII

SAMPLE SUMMARYB3I150165

SAMPLED SAMPWO # SAMPLEtf CLIENT SAMPLE ID____________ _______________________________ DATE TIME

FOC4VPOC44FOC46FOC47FOC5HFOC5L

NOTE(S)

001002003004005006

MC001MW33BMW32BMW32BMC001TRIP

_WS1009_WS0912_WS0912_WS0912_STS100BLANK

03_03_03_03_903

0001000100010002_0001

09/10/0309/12/0309/12/0309/12/0309/10/0309/02/03

1112151511

3045303025

The analytical results of the samples listed above are presented on the following pagesAll calculations an performed before rounding to avoid round off errors In calculated resultsResult! noted as NO were not detected at or above the staled limitThis repon must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corroslvlty density flashpoint Igmtabihty layers odorpaint filter test pH porosity pressure reactivity redo* potential specific gravity spot tests solids solubility temperature viscosity and weight

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles


PARAMETERDichlorodif luoromethaneChloromet haneChloroethaneBromome thaneTnchlorof luoromethane112 Tnchlorotrifluoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 Butanone1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTr ichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order #Date Recen̂ ffidAnalysis TUffitreAnalysis Tame

Instrument IDMethod

RESULTNDNDNDNDNDND

NDNDNDND3 3 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

FOC4V1AA09/15/0309/16/0315 17

MSKSW846 826


1 01 01 01 0IdD1 01 01 01 01 01 01 05 01 00 SO1 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Mbitt-im-ir

10 00 MB Sunn

OB



WATERf 32603!

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client San^le ID MC001_WS 100903_0001

GC/MS Volatiles

Lot-Sample # E3I150165 001 Work Order FOC4V1AA Matrix

) Estimated result Result is less than RU

WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorot oluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro

propane124 Tri chloro-

benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTe t r ahydr o fur anVinyl acetate

SURROGATEBromof luo robenzene1 2 Dichl oroethane d4Toluene d8

NOTB(S)


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 50I 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MB33B_WS 091203_0001

GC/MS Volatiles


PARAMETERDichlorodif luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrif luoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichloroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon tetrachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order $Date ReceivedAnalysis matteAnalysis Tame

Instrument IDMethod

RESULTNDNDNDNDNDND


FOC441AA09/15/0309/16/0315 40

MSKSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Matnx10 00 USES Kmm

OB



WATERi 3260331

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW33B_WS 091203_0001

GC/MS Volatiles

Lot-Sample # E3I150165 002 Work Ordeir # FOC441AA Katrxz WATER

PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 T etrachloroethane123 Tri chloropropanen-PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorotoluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyltoluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro


benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate

SURROGATEBromof luo robenzene1 2 Dichloroethane d4Toluene-d8


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW32B_WS 091203_0001

GC/MS Volatiles

Lot-Sample tt E3I150165 -003Date Sampled 09/12/03 15 30Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590

PARAMETERDichlorod i f luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Tnchlorotnfluoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert-butyl etherCarbon diaulfideAcetonetrans 1 2 DichloroetheneI 1 Dichl oroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodi ch lorome thaneDibromome thane4 Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachloroethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order $Date Recei^redAnalysis KtotteAnalysis TTume

Instrument IDMethod

RESULTNDNDNDNDNDND

NDNDNDNDNDNDNDNDND0 56 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

FOC461AA09/15/0309/16/0316 03

MSKSW846 826


1 01 01 01 0101 01 01 01 01 CD1 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

Jtotz10 00 MS I

OB



xx WATERturn $ 32603:

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW32BJHS 091203_0001

GC/MS Volatiles

Lot-Sample # E3I150165-003 Work Order POC461AA Matrix

i Estimated result Result Is less than RL

WATER

PARAMETEREthylbenz eneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene135 Trimethylbenzene2 Chlorot oluene4 Chlorot oluenetert Butylbenzene124 Trimethylbenzenesec Butylbenzenep Isopropyl toluenel 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo 3 chloro-

propane124 Trichloro

benzeneHexachlorobutadleneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate

SURROGATEBromofluorobenzene1 2-Dichloroethane d4Toluene d8

NOTE(S)


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW32BJWS 091203_0002

GC/MS Volatiles

Lot-Sample #Date Sampled

E3I150165 004 Work Order t09/12/03 15 30 Date Received

Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1

Analysis BateAnalysis TTnmie

FOC471AA09/15/03 10 00 MS Hum09/16/0316 26


WATER3260331

Analyst ID 015590

PARAMETERDichlorod if luoromethaneChloromet haneChloroethaneBromome thaneTrichloro f luoromethane112 Tnchlorotnf luoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichl oroethane2 2 Dichl oropropanecis 1 2 DichloroetheneChloroformBromochlo romethane111 Tri chloroethane2 But anon e1 1 Dichl oropropeneCarbon te trachlonde1 2 DibromoethaneBenzeneTrichloro ethene1 2 Dichl oropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 Dichl oroethaneTetrachloroethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Instrument IDMethod

RESULTNDNDNDNDNDND

NDNDNDNDNDNDNDNDND0 57 JNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

MSKSW846 826


1 01 01 01 0101 01 01 01 0i Q>1 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

OB



MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID HW32B_WS 091203_0002

GC/MS Volatiles

Lot-Sample # E3I150165-004 Work Order f FOC471AA Matrix

J Estimated result Result is less than RL

WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 Tetrachloroethane123 Tri chloropropanen PropylbenzeneBromobenz ene1 3 5-Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert-Butylbenzene124 Trimethylbenzenesec Butyl benzenep Isopropyl toluene1 3 Dichlorobenzene1 4 Dichlorobenzenen Butylbenzene1 2 Dichlorobenzene1 2 Dibromo-3 chloro


benzeneHexachlorobutadieneNaphthalene123 Tri chlorobenzeneAcroleinAcrylonitrilelodomethane2 Chloroethyl vinyl etherTetrahydr of uranVinyl acetate


NOTE(S)


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MC001_ST S100903_0001

GC/MS Volatiles

Lot-Sample # E3I150165 005Date Sampled 09/10/03 11 25Prep Date 09/19/03Prep Batch # 3265544Dilution Factor 1% Moisture

PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenz eneBromochlo romethaneBromodich loromethaneBromoformBromomethane2 But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlondeChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo 3-chloro

propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 -DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane

Work Order #Date ReceivedAnalysis matteAnalysis Tame

Analyst IE)Method



FOC5H1AA09/15/0309/19/0317 17

999998SW846 626

REPORTINGLIMIT25100505 05 05 05 05 010255 05 05 05 05 05 05 010105 0105 05 010

5 05 05 05 05 0105 05 05 05 05 05 0

Matrix10 00 MB Stonm

SOLID# 3265309

Innstmnineinitt HD MSDOB



MDL1530402 02 01 01 03 08 0152 02 02 03 01 02 01 02 05 01 03 02 02 03 0

3 01 02 02 02 01 01 01 02 02 02 01 0


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sanqple ID MC001_ST S100903_0001

GC/MS Volatiles

Lot-Sample # E3I150165 005 Work Order FOC5H1AA Matrix

Surrogate recovery is outside slated control limits

SOLID

PARAMETER2 2 Dichloropropanecis 1 3 Dichloropropenetrang 1 3 Dichloropropene1 1 DichloropropeneEthylbenzeneHexachlorobutadiene2-HexanonelodomethaneI sopropyl benzenep IsopropyltolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachloroetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro

benzene111 Tri chloroethane112 Tri chloroethaneTrichloro etheneTrichloro fluoromethane1 2 3-Trichloropropane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)

SURROGATEBromof luorobenzene1 2 Dichloroethane d4Toluene d8

NOTE(S)



PERCENTRECOVERY37 *32 *37 *

REPORTINGLIMIT5 05 05 05 05 05 025105 05 05 0255 05 05 0105 05 05 0205 05 05 0

5 05 05 0105 05 05 010105 0

RECOVERYLIMITS(60 130)(60 140)(60 130)



MDL2 01 03 01 02 02 010102 02 03 0101 02 02 02 03 03 02 02 02 02 02 0

1 03 02 02 03 02 02 05 02 03 0

IIIIIIIIIIIIIIIIIII

HALBY &. ALDRICH INC

Client Sample ID TRIP BLANK

GC/MS Volatiles

Lot-Sample # E3I150165 -006Date Sampled 09/02/03Prep Date 09/16/03Prep Batch # 3259599Dilution Factor 1Analyst ID 015590

PARAMETERDichlorod if luoromethaneChloromet haneChloroethaneBromomethaneTrichloro f luoromethane112 Trichlorotrifluoro

ethane1 1 DichloroetheneMethylene chlorideMethyl tert -butyl etherCarbon disulfideAcetonetrans 1 2 Dichloroethene1 1 Dichloroethane2 2-Dichloropropanecis 1 2 DichloroetheneChloroformBromochlo rome thane111 Tri chloroethane2 Butanone1 1 DichloropropeneCarbon te trachloride1 2 DibromoethaneBenzeneTrichloro ethene1 2 DichloropropaneBromodich loromethaneDibromome thane4 -Methyl 2 pentanoneToluene112 Tri chloroethane1 2 DichloroethaneTetrachlo roethene2 HexanoneDibromoch loromethaneChloroben zene1 1 1 2 Tetrachloroethane

Work Order #Date ReceiiuedAnalysis UtoteAnalysis TTume

Instrument IDMethod

RESULTNDNDNDNDNDND


FOC5L1AA09/15/0309/16/0314 30

MSKSW846 826


1 01 01 01 0101 01 01 01 01 01 01 05 01 00 501 01 01 01 01 01 05 01 01 00 501 05 01 01 01 0

IMIatt-ir-inr

10 00 90S ffifflmt

OB



WATERf 32603:

MDL0 400 300 301 00 300 40

0 300 300 500 303 00 300 200 300 300 300 300 203 00 300 300 300 300 300 300 300 403 00 300 300 400 303 00 400 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID TRIP BLANK

GC/MS Volatiles

Lot-Sample # E3I150165 -006 Work Ordes: FOC5L1AA Matrix WATER

PARAMETEREthylbenzeneVinyl chlorideXylenes (total)StyreneBromoformIsopropyl benzene1 1 2 2 T etrachloroethane1 2 3-Trichloropropanen PropylbenzeneBromobenzene135 Trimethylbenzene2 Chlorotoluene4 Chlorotoluenetert -Buty Ibenzene124 Trimethylbenzenesec Butyl benzenep - 1 soprop yl toluene1 3 Dichlorobenzene1 4 -Dichlorobenzenen Butylbenzene1 2 -Dichlorobenzene1 2 Dibromo 3 chloro-

propane124 Trichloro

benzeneHexachlor obutadieneNaphthalene123 TnchlorobenzeneAcroleinAcrylonit rilelodomethane2 Chloroethyl vinyl etherTetrahydrofuranVinyl acetate

SURROGATEBromofluorobenzene1 2 Dichloroe thane d4Toluene d8


ND

NDNDNDNDNDNDNDNDND


REPORTINGLIMIT1 00 501 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 01 02 0

1 0

1 01 01 020202 05 0105 0

RECOVERYLIMITS(75 130)(65 135)(80 130)


ug/L


MDL0 200 300 800 300 300 300 400 400 400 300 200 300 300 200 300 300 300 300 300 300 300 70

0 30

0 300 500 4012101 02 02 02 0

ANALYTICAL REPORT


Lot # E31180205

Haley & Aldrich Inc



September 24 2003

IEXECUTIVE SUMMARY - Detection Highlights

• B3I180205

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I


MW_22B_WG091703_0001 09/17/03 14 00 001

Carbon disulfide 0 68 J 10 ug/L SW846 8260B

IMETHODS SUMMARY

I E3I180205

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

ANALYTICAL PREPARATI ONPARAMETER ____ ___ ____ METHOD________ METHOD

Volatile Organics by GC/MS SW846 8260B SW846 5030B/826

References

SW846 Test Methods for Evaluating Solid Waste Physical/ ChemicalMethods Third Edition November 1986 and its updates

1SAMPLE SUMMARY

• E3I180205

I WO # SAMPLE* CLIENT SAMPLE ID

FOLQG 001 MW_22B_WG091 703_0001• FOLQR 002 MW_23B_WG091 703_0001• FOLQW 003 TRIP BLANK E3G280120

I NOTB(S)The analytical results of the samples listed above aro presented on the following pagesAll calculations are performed before rounding to avoid round off errors In calculated resultsResults noted as NO were not detected at or above the stated limit

H This report must not be reproduced except In full without the written approval of the laboratoryB Results for the following parameters are never reported on o dry weight basis color corrosivity density flashpoint ignitabihty layers odor

paint filler test pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight

1

1

1

1

1

1

1

1

1

1

1

1

SAMPLED SAMPDATE TIME

09/17/03 14 0009/17/03 14 4009/02/03

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_22B_WG091703_0001

GC/MS Volatiles


PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenzeneBromochlo romethaneBromodich loromethaneBromoformBromomethane2 -But anon en Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon te trachlorideChloroben zeneDlbromoch loromethaneChloroe thane2 Chloroe thyl vinyl etherChloroformChloromethane2 Chlorotoluene4 Chlorotoluene1 2 Dibromo-3 chloro

propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDlchlorodlfluoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 -Dichloroethenetrans-1 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane

Work Order ftDate Recea.T»edAnalysis lateAnalysis Tmme

Instrument IDMethod

RESULTNDNDNDNDNDNDNDNDNDNDNDNDND0 68 JNDNDNDNDNDNDNDNDNDND


FOLQG1AA09/18/0309/19/0314 08

MSHSW846 826

REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 <D0 501 01 02 05 01 02 01 01 02 0

1 01 01 01 01 01 01 00 501 01 01 01 0

Mtali10 00 KB

OB

UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

:nx WATERBnnm i 3262279

MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70

0 300 400 300 300 300 400 200 400 300 300 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles

Lot-Sample # E3I180205 001 Work Order FOLQG1AA Matruc

J Estimated result Result Is less than RL

WATER

PARAMETER2 2 Dichloropropane1 1 Dichl oropropeneEthylbenzeneHexachlorobutadlene2 HexanonelodomethaneIsopropyl benzenep Isopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro

benzene111 Tri chloroethane112 Tri chloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane112 Tri chlorotnf luoro

ethane1 2 4-Tnmethylbenzene135 TnmethylbenzeneVinyl acetateVinyl chl orideXylenes (total)


NOTE(S)

RESULTNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDND

NDNDNDNDND


REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0

1 01 01 02 01 01 0

1 01 05 00 501 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)

UNITSug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

ug/Lug/Lug/Lug/Lug/Lug/L

ug/Lug/Lug/Lug/Lug/L

MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30

0 200 300 300 300 400 40

0 300 202 00 300 80

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC


GC/MS Volatiles


PARAMETERAcetoneAcroleinAcrylonit rileBenzeneBromobenzeneBromochlo romethaneBromodlchloromethaneBromoformBromome thane2 Butanonen Butylbenzenesec Butylbenzenetert ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDibromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2-Chlorotoluene4 Chlorotoluene1 2 Dibromo-3 chloro

propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodif luoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans I 2 Dichloroethene1 1 Dichloroethene1 2 Dichloropropane

Work Order #Date ReceRwedAnalysis DateAnalysis Tmme

Instrument IDMethod



FOLQR1AA09/18/0309/19/0314 39

MSHSW846 826

REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 00 501 01 02 05 01 02 01 01 02 0

1 01 01 01 01 01 01 00 501 01 01 01 0

BBatt-ir-ii -w10 00 MB Pmnrn

OB



WATERf 32622'

MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70

0 300 400 300 300 300 400 200 400 300 300 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sanqale ID MW_23B_WG091703_0001

GC/MS Volatlles

Lot-Sample # E3I180205 002 Work Order FOLQR1AA Matrix WATER

PARAMETER2 2 Dichloropropane1 1 DichloropropeneEthylbenzeneHexachlorobutadlene2 Hexanonelodometha neI sopropyl benzenep IsopropyltolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Trichloro

benzene111 Tnchloroethane112 TnchloroethaneTrichloro etheneTrichloro f luoromethane123 Tri chloropropane112 Tri chlorotrif luoro

ethane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)

SURROGATEBromof luorobenzene1 2 Dichloroethane d4Toluene d8


NDNDNDNDNDND

NDNDNDNDND


REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0

1 01 01 02 01 01 0

1 01 05 00 501 0

RECOVERYLIMITS(75 - 130)(65 - 135)(80 130)




MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30

0 200 300 300 300 400 40

0 300 202 00 300 80

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID TRIP BLANK E3G280120

GC/MS Volatiles

Lot-Sample # E3I180205 003Date Sampled 09/02/03Prep Date 09/19/03Prep Batch # 3262567Dilution Factor 1Analyst ID 015590

PARAMETERAcetoneAcroleinAcrylonitrileBenzeneBromobenz eneBromochlo rome thaneBromodich loromethaneBromoformBromomethane2-Butanonen Butylbenzenesec-Butyl benzenetert-ButylbenzeneCarbon disulfideCarbon tetrachlorideChloroben zeneDlbromoch loromethaneChloroethane2 Chloroethyl vinyl etherChloroformChloromet hane2-Chlorotoluene4 Chlorotoluene1 2 Dibromo 3 chloro

propane1 2 DibromoethaneDibromome thane1 2 Dichlorobenzene1 3 Dichlorobenzene1 4 DichlorobenzeneDichlorodifluoromethane1 1 Dichloroethane1 2 Dichloroethanecis 1 2 Dichloroethenetrans 1 2 Dichloroethene1 1 Dichloroethene1 2-Dichloropropane

Work Order #Date ReceivedAnalysis EtotteAnalysis TTmroe

Instrument IDMethod



FOLQW1AA09/18/0309/19/0315 09

MSHSH846 826

REPORTINGLIMIT1020201 01 01 01 01 02 05 01 01 01 01 00 501 01 02 05 01 02 01 01 02 0

1 01 01 01 01 01 01 00 501 01 01 01 0

Mattmjc10 00 MS ffimnm

OB



WATERf 32622'

MDL3 012100 300 300 300 300 301 03 00 300 300 200 300 300 300 400 302 00 300 300 300 300 70

0 300 400 300 300 300 400 200 400 300 300 300 30


IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID TRIP BLANK E3G280120

GC/MS Volatiles

Lot-Sample # E3I180205 003 Work Order FOLQW1AA Matrix WATER

PARAMETER2 2 Dichloropropane1 1 DichloropropeneEthylbenz eneHexachlorobutadlene2 HexanonelodomethaneI aopropyl benzenep I sopropyl tolueneMethylene chloride4 Methyl 2 pentanoneMethyl tert butyl etherNaphthalenen PropylbenzeneStyrene1 1 1 2 Tetrachloroethane1 1 2 2 TetrachloroethaneTetrachlo roetheneTetrahydrofuranToluene123 Tri chlorobenzene124 Tri chloro

benzene111 Trichloroethane112 TrichloroethaneTrichloro etheneTrichloro f luoromethane1 2 3-Trichloropropane112 Tri chlorotrif luoro

ethane124 Trimethylbenzene135 TrimethylbenzeneVinyl acetateVinyl chlorideXylenes (total)

SURROGATEBromof luo robenzene1 2-Dichloroethane d4Toluene d8


NDNDNDNDNDND

NDNDNDNDND


REPORTINGLIMIT1 01 01 01 05 02 01 01 01 05 01 01 01 01 01 01 01 0101 01 01 0

1 01 01 02 01 01 0

1 01 05 00 501 0

RECOVERYLIMITS(75 130)(65 135)(80 - 130)




MDL0 300 300 200 303 01 00 300 300 303 00 500 500 400 300 300 400 302 00 300 400 30

0 200 300 300 300 400 40

0 300 202 00 300 80


Lot # E31170215

IIIII_ ANALYTICAL REPORT

IIIIIIIIIIIII

Haley & Aldrxch Inc


Diane SuzukxProject Manager

September 24 2003

I1 EXECUTIVE SUMMARY - Detection HighlightsI E3I170215

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I

I


MW_26C_COTTINGS_COMPOSITE 09/16/03 14 30 003

Trichloroethene 0 026 0 025 mg/L SW846 8260B

I• METHODS SUMMARY• E3I170215

I ANALYTICAL PREPARATI ONPARAMETER ___ _______ _____________________ METHOD________ METHOD

I Volatile Organics by GC/MS SW846 8260B SW846 1311/5030

References

• SW846 Test Methods for Evaluating Solid Waste Physical/Chemical™ Methods Third Edition November 1986 and its updates

I

I

I

I

I

I

I

I

I

I

I

I

I

IIIIIIIIIIIIIIIIIII

SAMPLE SUMMARYE3I170215

SAMPLED SAMPWO ft SAMPLEft CLIENT SAMPLE ID ____________________________________ DATE TIME

FOH2TFOH27FOH29FOH3FFOH3HFOH3K

KOTE(S)

001002003004005006

MW_23B_CUTTI NGSMW_22B_CUTTI NGSMW_26C_CUTTI NGS_COMPOSITEMW_30B_CUTTINGSMW_31B_CUTTINGSMW_32B/MW33B _CUTTINGS

09/16/0309/16/0309/16/0309/16/0309/16/0309/16/03

131314131313

503530452505

The analytical results of the samples listed above are presented on the following pagesAll calculations are performed before founding to avoid round off errors In calculated resultsResults noted as NO were not detected at or above the stated limitThis report must not be reproduced except in full without the written approval of the laboratoryResults for the following parameters are never reported on a dry weight basis color corrosivlty density flashpoint Ignitablllty layers odorpaint filter test pH porosity pressure reactivity redox potential specific gravity spot tests solids solubility temperature viscosity and weight

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_23B_C DTTINGS

TCLP GC/MS Volatiles

Lot-Sample # E3I170215 001Date Sampled 09/16/03 13 50Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1% Moisture

PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlondeTnchloroetheneBenzeneTetrachlo roetheneChloroben zene

SURROGATE4 Bromof luorobenzeneToluene d81 2 -Dichloroethane d4

NOTE(S)

Work Order fDate ReceivedPrep DatePrep BatcBa #

Analyst IE)Method

RESULTNDNDNDNDNDNDNDNDNDND


FOH2T1AA Hattrax09/17/03 10 20 HE S&unm #09/18/03 analysis mate3261563 Analysis THume

015590 TTimmtt-iniiiiiiMiMill HD

SW846 826 OB

REPORTINGLIMIT UNITS MDL0 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0100 12 mg/L 0 0750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0120 025 mg/L 0 0075

RECOVERYLIMITS(80 120)(75 125)(70 135)

SOLID326128509/23/0311 52

MSK

Analysis performed in accordance with USEPA Toxiclty Characteristic Leaching Procedure Method 1311

IIIIIIIIIIIIIIIIIII

HALEY t ALDRICH INC

Client Sample ID MW_22B_CDTTINGS



PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichl oroethane2 ButanoneCarbon te trachlorideTnchloro etheneBenzeneTetrachlo roetheneChloroben zene

SURROGATE4 BromofluorobenzeneToluene d81 2 Dichl oroethane d4

NOTK(S)

Work Order #Date Recer^edPrep DatePrep BatcBn $

Analyst IPMethod



FOH271AA09/17/0309/18/033261563

015590SW846 826

REPORTINGLIMIT0 0250 0250 0250 0250 120 0250 0250 0250 0250 025

RECOVERYLIMITS(80 120)(75 125)(70 135)

MattnLx10 20 MB Baxm f

Amalysasanalysis

mateTCbnrie

Trnijafr miiiin-iinrt- HD

OB

UNITSmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

SOLID326128509/23/0312 15

MSK

MDL0000000000

0075007500750100750075007500750120075

Analysis performed in eccordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_26C_CDTTINGS_C»MPOSITE


Lot-Sample # E3I170215 003Date Sampled 09/16/03 14 30Leach Date 09/18/03Leach Batch # P3 26112Dilution Factor 1% Moisture

PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloro etheneBenzeneTetrachlo roetheneChlorobenzene

SURROGATE4 Bromof 1 uorobenzeneToluene d81 2 Dichloroethane d4

NOTE(S)

Work Order #Date ReceivedPrep DatePrep BatcHu ft

Analyst IPMethod

RESULTNDNDNDNDNDND0 026NDNDND


FOH291AA Matmuc09/17/03 10 20 MS Kmnm #09/18/03 Analysis Usate3261563 Aimalysis TEhrme

015590 1Timn»tt- IT min»»iMitt- HD

SW846 826 OB

REPORTINGLIMIT UNITS MDL0 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0100 12 mg/L 0 0750 025 mg/L 0 0075(ID SD25 mg/L 0 00750 025 mg/L 0 00750 025 mg/L 0 0120 025 mg/L 0 0075

RECOVERYLIMITS(80 120)(75 125)(70 135)

SOLID326128509/23/0312 39

MSK

Analysis performed In accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_30B_COTTINGS



PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 But anon eCarbon tetrachlorideTnchloroetheneBenzeneTetrachlo roetheneChloroben zene

SURROGATE4 BromofluorobenzeneToluene d81 2 Dichloroethane d4

NOTE(S)

Work Order fDate ReceorswsdPrep DatePrep Batcto #

Analyst intMethod



FOH3F1AA Mateuc09/17/03 10 20 MB Hmran09/18/03 Amalysi

*us IBstte

3261563 analysis TEbnrie

015590 lastttwnSW846 826 OB

REPORTINGLIMIT UNITS0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 12 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L

RECOVERYLIMITS(80 120)(75 125)(70 135)

mmtr HD

MDL0 00750 00750 00750 0100 0750 00750 00750 00750 0120 0075

SOLID326128509/23/0313 02

MSK

Analysis performed in iccordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_31B_CDTTINGS


Lot-Sample # E3I170215 005Date Sampled 09/16/03 13 25Leach Date 09/18/03Leach Batch # P326112Dilution Factor 1* Moisture

PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloroetheneBenzeneTetrachloroetheneChloroben zene

SURROGATE4 Bromof luorobenzeneToluene d81 2 Dichloroethane d4

NOTE(S)

Work Order *Date ReceivedPrep DatePrep Batch #

Analyst IBMethod



FOH3H1AA Matin09/17/03 10 20 MS Hn

LK

mm f09/18/03 Analysis mate3261563 Analysis TCbnme

015590 ImstmamEJUitt HDSW846 826 OB

REPORTINGLIMIT UNITS0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 12 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L0 025 mg/L

RECOVERYLIMITS(80 120)(75 125)(70 135)

MDL0 00750 00750 00750 0100 0750 00750 00750 00750 0120 0075

SOLID326128509/23/0313 25

MSK

Analysis performed In accordance with USEPA Toxicity Characteristic Letching Procedure Method 1311

IIIIIIIIIIIIIIIIIII

HALEY & ALDRICH INC

Client Sample ID MW_32B/M W33B_CUTTINGS



PARAMETERVinyl chloride1 1 DichloroetheneChloroform1 2 Dichloroethane2 ButanoneCarbon tetrachlorideTrichloro etheneBenzeneTetrachlo roetheneChloroben zene

SURROGATE4 Bromof luorobenzeneToluene d81 2 Dichloroethane d4

NOTE(S)

Work Order #Date Recex^rodPrep DatePrep BatcBn $

Analyst IPMethod



FOH3K1AA09/17/0309/18/033261563

015590SW846 826

REPORTINGLIMIT0 0250 0250 0250 0250 120 0250 0250 0250 0250 025

RECOVERYLIMITS(80 120)(75 125)(70 135)

Mattntx10 20 MS Hum t

AmaJLysisftmallyraim

XnnsttjnmOB

UNITSmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

nen

natteTriune

att ED

SOLID326128509/23/0313 49

MSK

MDL0000000000

0075007500750100750075007500750120075

Analysis performed In accordance with USEPA Toxlclty Characteristic Leaching Procedure Method 1311

Documents

UNDtROROUND ENCINEFRING & ENVIRONMENTAL SOLUTIONS · (0 026 milligrams per liter) in the composite sample from MW-26C drill cuttings ... Water Quality in Bedrock Assessment Groundwater