80
Unit-III: Extraction

Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

  • Upload
    others

  • View
    32

  • Download
    1

Embed Size (px)

Citation preview

Page 1: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Unit-III: Extraction

hp
Rectangle
hp
Typewriter
hp
Typewriter
hp
Typewriter
hp
Rectangle
hp
Textbox
Extraction, Leaching, Adsorption Concepts and Equipments
Page 2: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 3: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 4: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 5: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 6: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 7: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 8: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 9: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 10: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 11: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 12: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 13: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 14: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 15: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 16: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 17: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 18: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 19: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 20: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 21: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 22: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 23: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 24: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 25: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 26: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 27: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 28: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 29: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Batch Mixer Settler

Page 30: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Continuous Mixer Settler

Page 31: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Spray Tower

Page 32: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 33: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 34: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Packed Tower

Page 35: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 36: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 37: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 38: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 39: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Rotating Disc or Agitated Tower

Page 40: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 41: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

• The Pulse Extraction Process (P.E.P.)

developed by JURA optimise the extraction

time.

• It forces the hot water through the ground

coffee at short intervals.

• This process allows the flavours of the coffee

to fully develop.

Page 42: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 43: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 44: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Unit-III: Leaching

Page 45: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 46: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 47: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 48: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Bollman Extractor

Page 49: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 50: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 51: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 52: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 53: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Unit-IV:Adsorption

Page 54: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 55: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 56: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 57: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 58: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 59: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 60: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 61: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 62: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 63: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 64: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 65: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 66: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 67: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 68: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Freundlich Isotherm:

• For the special case of heterogeneous surface energies

(particularly good for mixed wastes) in which the energy term,

“KF”, varies as a function of surface coverage we use the

Freundlich model.

Langmuir Isotherm:

This model assumes monolayer coverage and constant binding

energy between surface and adsorbate.

Page 69: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 70: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 71: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 72: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 73: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 74: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 75: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 76: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 77: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 78: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid
Page 79: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

Down flow is preferred, up flow might fluidise the particles (attritionand loss of fines)In one column adsorption in the other desorption (regeneration ofadsorbent) takes place.

Page 80: Unit-III: Extraction Extraction, Leaching, Adsorption ... Engineering/MTELACE.… · Liquid-liquid contact e.g. extraction Liquid-solid contact e.g. crystallization, adsorption Gas-solid

• Regeneration is made with

• -steam (if the solvent is not miscible with water) or

• -hot inert gas

• Steam condenses in the bed, raises T of the solid and provides

energy for desorption.

• The solvent is 1. condensed, 2. separated from the water,

3. sometimes dried before reuse.

• After regeneration the bed may be cooled and dried with inert

gas.

• If some water vapour can be in the clean gas the evaporation of

water remaining in the bed helps cool the bed during adsorption.