w w w .tes tveritas.com info@ tes tveritas · in tern ational demand for se rvices and p rodu cts for anal ysis. scheme P ro get to Tries te. The main featu res of Proget to Tries

[email protected]

Highlight

20 years of experiences 65 participating countries

Operational Headquarterloc. Padriciano, 9934149 Trieste (TS)Italy Tel: +39 040 3755560

Via Svizzera, 1635127 Padova (PD)ItalyTel: +39 049 8256292Fax: +39 049 21064938

Legal Headquarter

FOOD SAFETY ANALYSIS

Test Veritas S.r.l. was created to satisfy the increasing international demand for services and products for

analysis.

scheme Progetto Trieste.

The main features of Progetto Trieste are:

Screening results are assessed by dedicatedcriteria

Test materials are mainly incurred

often provided

2019

beta-lactams in milk and muscle

List of EN ISO/IEC 17043:2010 accredited scopes

available at

www.accredia.it

1 in cheese

nitrofuran metabolites in shrimps

heavy metals in muscle and milk

ciromazine, macrolides, melamine in eggs

2015-2018 Participanting countries

avermectins and sulphonamides in liver

Details of accreditedschemes available at www.testveritas.com

MO 01COM rev.1 del 06/10/2017, emiss.4 dd 19/03/19 1 of 18

(Cert. PTP N. 0008)

acrylamide in bread

Find out more about

Visit www.testveritas.com

Groups of analytes


Aflatoxins B/G Fumonisins Ochratoxin A Patulin

Synthetic steroids RAL Stilbenes

Corticosteroids

-agonistsRactopamine

Chloramphenicol Tetracyclines Quinolones and fluoroquinolones Nitrofuran metabolites Avermectins Macrolides

Sulphonamides -lactams

Coccidiostatics

Histamine (see page n.7) Illegal dyes

Streptomycin

Heavy metals (see pages n.10-11)

Lead, Cadmium, Mercury, Arsenic

CyromazinFipronil

Other contaminants(see pages n.10-13)

Pesticides(see pages n.10-11)

Aflatoxin M1

DON Zearalenone

and others see the list on page n.11

Mycotoxins(see pages n. 12-15)

Veterinary drug residues(see pages n. 3-9)

MelamineAcrylamide

Nitrates (see pages n.10-11)

Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected] The updated programme is available at www.testveritas.com

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered with the test material.

Progetto Trieste - Veterinary Drug Residues 2019 Programme

Those proficiency tests could distinguish between participations with confirmatory methods (HPLC-GC) or screening methods (ELISA, RIA, biosensors, microbial inhibition assays, lateral flow, etc...).For participating with confirmatory methods the code is A and quantification is requested. Evaluation of performance

For participating with screening methods the code is B and quantification is optional. Qualitative results will be

When the shipment includes 2 test materials, they are at a different concentration of analyte. The laboratory will receive an evaluation for each test material.


will be in z-score terms.

assessed by dedicated criteria (see Evaluation Criteria at www.testveritas.com).

Analytes Matrix Status Code Quantity Euro

E1910 A 30g x 2 Test Materials B

330,00 285,00 Chloramphenicol egg

ROUND of MARCH (see next page too)

spiked 15g x 2 Test Materials

Shipping date: March 18th 2019. Result submission deadline: April 22nd 2019. Final Report available in May 2019. Order deadline: January 31st 2019

MI1911 A 20ml x 2 Test Materials B

3300,00 285,00 Chloramphenicol

10ml x 2 Test Materials


430,00 325,00

Tetracyclines andQuinolones/ 10ml x 2 Test Materials partial participations in MI1913

Only for analysis of Quinolones/Fluoroquinolones: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00

MI1913/Q

Only for analysis of Tetracyclines: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00

MI1913/T

spiked

M1914 A 20g x 2 Test Materials B

330,00 285,00 Nitrofuran metabolites 10g x 2 Test Materials

swine muscle

bovine milk

incurredor spiked

incurred


330,00 285,00 Chloramphenicol 10g x 2 Test Materials rabbit muscle incurred

bovine milk

TECHNICAL ASPECTS

Indicative concentrations

Category

List of moleculesChloramphenicol chloramphenicol eggs, milk: < 2 ppb or blank

muscle: < 3 ppb or blank Tetracyclines oxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers milk: < 300 ppb or blank Quinolones and fluoroquinolones

enrofloxacin, ciprofloxacin, flumequine, marbofloxacin, danofloxacin, sarafloxacin, nalidixic acid, oxolinic acid, norfloxacin

milk: < 200 ppb or blank

Nitrofuran metabolites AOZ, AMOZ, AHD, SEM muscle: < 4 ppb or blank

Each test material may contain one or more substances from the table below. The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.

Milk test materials would contain preservative solutions. It is not requested to research all the molecules of each group.

Fluoroquinolones

LIO

LIO

LIO

LIO

LIO

LIO

or spiked


Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered with the test material.




ROUND of MARCH (see previous page too)

Shipping date: March 18th 2019. Result submission deadline: April 22nd 2019 and April 9th for beta-lactams. Final Report available in May 2019.Order deadline: January 31st 2019

M1891 A 20g x 1 Test Material B

330,00 285,00 -lactams 10g x 1 Test Material

bovine muscle

TECHNICAL ASPECTS


Category

List of molecules

Chloramphenicol chloramphenicol water: < 2 ppb or blank

-lactams penicillin V, penicillin G, amoxicillin, ampicillin muscle: < 200 ppb

Each test material may contain one or more substances from the table below. The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.

It is not requested to research all the molecules of each group.

L1915 A 20g x 1 Test Material B

330,00 285,00 Avermectins 10g x 1 Test Material

bovine liver spiked

Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin liver: < 200 ppb

LIO

LIO

WA1916 A 20ml x 2 Test Materials B

330,00 285,00 Chloramphenicol 10ml x 2 Test Materials

animal watering spiked


330,00 285,00 Macrolides 15g x 1 Test Material

bovine muscle spikedLIO

Macrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin,spiramycin, tilmicosin, tylosin A, tylosin B, virginiamycin

muscle: < 400 ppb

LIO spiked

water

For participating with confirmatory methods (HPLC, GC) the code is A.For participating with screening methods (ELISA, RIA, biosensors, microbial inhibition assay, lateral flow, etc...) the code is B .


Progetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]


Shipping date: May 20th 2019. Result submission deadline : June 24th 2019. Final Report available in July 2019. Order deadline: March 22nd 2019


U1920 A 18ml x 2 Test Materials B

380,00 285,00 Synthetic steroids bovine urine

ROUND of MAY (see next page too)

12ml x 2 Test Materials


380,00 285,00

RAL 6ml x 2 Test Materials


380,00 285,00 Stilbenes 6ml x 2 Test Materials


380,00 285,00

-agonists(ractopamine included) 6ml x 2 Test Materials

partial participations in U1923

Only for analysis of -agonists: A 18ml x 2 Test Materials B 6ml x 2 Test Materials

330,00 245,00 U1923/G

Only for analysis of ractopamine: A 18ml x 2 Test Materials B 6ml x 2 Test Materials

330,00 245,00 U1923/R

incurred orspiked

bovine urine

swine urine incurred or spiked

bovine urine


380,00 285,00 Corticosteroids 6ml x 2 Test Materials

bovine urine

Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.


TECHNICAL ASPECTS


Category

List of moleculesSynthetic steroids 9 nortestosteron

one, methyltestosterone, stanozolol

urine: < 8 ppb or blank RAL zeranol, taleranol Stilbenes diethylstilbestrol (cis-DES and trans-DES), hexestrol, dienestrol

Corticosteroids dexamethasone, betamethasone, flumethasone, prednisolone, prednisone

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.It is not requested to research all the molecules of each group.

-agonists clenbuterol, salbutamol, terbutalineRactopamine ractopamine

The updated programme is available at www.testveritas.com

incurred

incurred orspiked

incurred orspiked

Analysis of synthetic sterois, RAL and stilbenes intended to the homogeneity study have been subcontracted.Test Veritas is responsible of subcrontracted activities.

LIO

LIO

LIO

LIO

LIO

LIO




Shipping date: May 20th 2019. Result submission deadline: June 24th 2019 and June 7th for -lactams. Final Report available in July 2019. Order deadline: March 22nd 2019


ROUND of MAY (see previous page too)


430,00 325,00

Avermectinslactams 10ml x 2 Test Materials

partial participations in MI1925

Only for analysis of avermectins: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1925/I

Only for analysis of -lactams: A 20ml x 2 Test Materials B 10ml x 2 Test Materials

330,00 285,00 MI1925/L

bovine milk


330,00 285,00 Sulphonamides 10ml x 2 Test Materials

bovine milk


Sulphonamides 15g x 2 Test Materials

spiked eggs



TECHNICAL ASPECTS


Category List of molecules

Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin milk: < 30 ppb or blank

Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine,sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazole

milk: < 400 ppb or blankeggs: < 60 ppb or blank

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.



spiked

spiked

-lactams penicillin V, penicillin G, amoxicillin, ampicillin milk: < 30 ppb or blank

AOZ, AMOZ, SEM, AHD eggs: < 4 ppb or blank

LIO

LIO

LIO

LIO

incurred or 330,00 285,00


Nitrofuran metabolites 15g x 2 Test Materials

eggs LIO 430,00

325,00 partial participations in E1928

Only for analysis of nitrofuran metabolites: A 30g x 2 Test Materials B 15g x 2 Test Materials

330,00 285,00 E1928/N

Only for analysis of coccidiostatics: A 30g x 2 Test Materials B 15g x 2 Test Materials

330,00 285,00 E1928/C

and coccidiostatics spiked

Nitrofuran metabolites

nicarbazin, robenidine, salinomycin, lasalocid, narasin eggs: < 300 ppb or blank Coccidiostatics

Milk test materials would contain preservatice solutions.

Progetto Trieste - Veterinary Drug Residues and Histamine - 2019 Programme



Shipping date: September 9th 2019. Result submission deadline: October 14th 2019. Final Report available in November 2019. Order deadline: July 26th 2019

ROUND of SEPTEMBER



TECHNICAL ASPECTS


Category

List of moleculesHistamine histamine tuna: 50 ppm < Level 1 < 350 ppm

Level 2 < 350 ppm or blank

Chloramphenicol chloramphenicol fish and shrimps: < 2 ppb or blank Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine,

sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazole muscle: < 300 ppb or blank

Tetracyclines oxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers

Quinolones and fluoroquinolones

enrofloxacin, ciprofloxacin, flumequine, marbofloxacin, danofloxacin, sarafloxacin, nalidixic acid, oxolinic acid, norfloxacin

muscle: < 800 ppb or blank



T1930 A 50g x 2 Test Materials B

295,00 215,00

Histamine(2 levels)

tuna 50g x 2 Test Materials

FI+SH1935 A 20g x 2 Test Materials

B 330,00 285,00 Nitrofuran metabolites

10g x 2 Test Materials

fish and shrimps spiked

incurred


330,00 285,00

Quinolones and fluoroquinoles 10g x 2 Test Materials

turkey muscle


330,00 285,00 Tetracyclines 10g x 2 Test Materials

hen muscle incurred


330,00 285,00 Sulphonamides 10g x 2 Test Materials

turkey or swine muscle

or spiked

FI+SH1934 A 20g x 2 Test Materials

B 330,00 285,00 Chloramphenicol


fish and shrimps

Illegal dyes malachite green, leucomalachite green and the sum of bothcrystal violet

muscle: < 400 ppb or blank

fish: < 12 ppb or blank


FI1936 A 20g x 1 Test Material B

330,00 285,00

Quinolones and fluoroquinoles

10g x 1 Test Material

fish spiked

FI1937 A 20g x 2 Test Materials B

330,00 285,00 Illegal dyes


fish spiked

incurred

incurred or spiked

fish: < 800 ppb

LIO

LIO

LIO

LIO

LIO

LIOLIO

LIO

FI1938 A 20g x 1 Test Material B

330,00 285,00 Sulphonamides


fish spikedLIO


330,00 285,00 Avermectins 10g x 1 Test Materials

bovine muscle spiked

Avermectins ivermectin, abamectin, doramectin, eprinomectin, emamectin, moxidectin muscle: < 300 ppb

spiked

LIO

LIO

fish: < 300 ppb

LIO

Nitrofuran metabolites AOZ, AMOZ, SEM, AHD fish and shrimps: < 4 ppb or blank



Shipping date: November 18th 2019. Result submission deadlinee: December 23rd 2019 and December 13th for honey. Final Report available in February 2020. Order deadline: October 4th 2019


ROUND of NOVEMBER



TECHNICAL ASPECTS


Category

List of molecules

Streptomycin Streptomycin, dihydrostreptomycin honey: < 100 ppb or blank

Sulphonamides sulfamethazine, sulfadimethoxine, sulfaquinoxaline, sulfamerazine, sulfadiazine, sulfamethoxypyridazine, sulfamonometoxine, sulfathiazole

honey: < 100 ppb or blank


L1940 A 20g x 2 Test Materials B

360,00 285,00

-agonists bovine liver 10g x 2 Test Materials

L1941 A 20g x 2 Test Materials B

330,00 285,00 Corticosteroids 10g x 2 Test Materials

H1942 A 30g x 2 Test Materials B

330,00 245,00 Sulphonamides 10g x 2 Test Materials

incurred or spiked

light honey spiked


330,00 245,00 Tetracyclines 10g x 2 Test Materials

incurred or spiked

spiked

bovine liver

light honey

H1948 A 30g x 1 Test Material B

330,00 245,00 Nitrofuran metabolites 10g x 1 Test Material spikedlight honey

(ractopamine included) partial participations in L1940

Only for analysis of -agonists: A 20g x 2 Test Materials B 10g x 2 Test Materials

330,00 260,00 L1940/G

Only for analysis of ractopamine: A 20g x 2 Test Materials B 10g x 2 Test Materials

330,00 260,00 L1940/R

Corticosteroids dexamethasone, betamethasone, flumethasone, prednisolone, prednisone

-agonists clenbuterol, salbutamol, terbutalineRactopamine ractopamine

liver: < 7 ppb or blank

The updated programme is available at www.testveritas.comProgetto Trieste c/o Test Veritas Srl (Italy) Tel. +39 049 8256292 [email protected]

L1946 A 20g x 1 Test Material B

330,00 285,00 Sulphonamides 10g x 1 Test Material

incurred or spiked

bovine or swineliver

Tetracyclines oxytetracycline, chlortetracycline, doxycycline, tetracycline and epimers honey: < 100 ppb or blank Coccidiostatics nicarbazin, robenidine, salinomycin, lasalocid, narasin muscle: < 100 ppb

E1947 A 30g x 1 Test Material B

330,00 285,00 Macrolides 10g x 1 Test Material spikedeggs

LIO

LIO

LIO

LIO


330,00 245,00 Streptomycin 10g x 2 Test Materials spikedlight honey


330,00 285,00 Coccidiostatics 10g x 1 Test Material

incurred or spiked

chicken or henmuscle

LIO

liver: < 8 ppb or blank

Macrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin, spiramycin,tilmicosin, tylosin A, tylosin B, virginiamycin

eggs: < 300 ppb

Nitrofuran metabolites AOZ, AMOZ, AHD, SEM honey: < 8 ppb

liver: < 300 ppb

LIO


Progetto Trieste - Veterinar

P

ry Drug Residues

We want to evidence you in this prewiew some proficiency testing that were not present in the 2019 programme but will be present in 2020.


ROUND OF MARCH 2020

In this round there will be proposed similar codes to the ones proposed in 2019 and in addition:

Analytes Matrix

Quinolones and fluoroquinolones eggsTetracyclines eggs

ROUND OF SEPTEMBER 2020

ROUND OF NOVEMBER 2020

and much more....

Avermectins fish


Analytes Matrix

Tetracyclines fish and shrimps

and much more....

-lactams fish


Analytes Matrix

Tetracyclines liverChloramphenicol honey

and much more....

Quinolones and fluoroquinolones honey

Tylosin honey


Progetto Trieste - Pesticide Residues, Heavy Metals and Nitrates - 2019


Shipping date: October 14th 2019. Result submission deadline: November 18th 2019. Final Report available in January 2020. Order deadline: September 13th 2019

ROUND of OCTOBER


M1976 50g x 1 Test Material 220,00

bovine muscle

VF1970 60g x 1 Test Material

220,00 Pesticides

tomato

The quantification with chromatographic method is requested. Evaluation will be in z-score terms.

spiked

spiked

For orders of 2 of the above codes: 2 Test Materials 300, 00


In each participation they are included the evaluations of 2 technicians.

Heavy Metals

LIO

LIO

ROUND of FEBRUARY 2020 (preview)

Glyphosate honey

In 2020 similiar proficiency testing than above will be proposed and in addition there will be the following:

Analytes Matrix

ROUND of FEBRUARY


E1900 40g x 1 Test Material

250,00 Cyromazin, Melamine andFipronil (all molecules will be present)

egg spiked

Shipping date: February 18th 2019. Result submission deadline: March 25th 2019. Final Report available in April 2019. Order deadline: December 31st 2018.

LIO

20g x 1 Test Material 190,00 AB

VF1973 50g x 1 Test Material 220,00 Heavy Metals tomato spikedLIO

VF1972 70g x 1 Test Material 220,00 Nitrates lettuce spikedLIO

Combined orders

VF1970blank 60g x 1 Test Material 50,00 Pesticides (blank sample) tomato blankLIO

FI1971 50g x 1 Test Material

220,00 Pesticides

fish spiked


LIO

FI1975 50g x 1 Test Material 220,00 Heavy Metals fish spikedLIO

Combined orders

FI1971blank 50g x 1 Test Material 50,00

Pesticides (blank sample) fish blankLIO

Pesticides milkPesticides pistachio

LIO Lyophilized material. Quantity regards the final quantity after reconstitution. Instructions for reconstitution will be delivered withthe test material.

Analysis of pesticides, heavy metals, nitrate, cyromazin and its metabolites (melamine), fipronil and fipronil-sulfone intended tothe homogeneity study have been subcontracted.Test Veritas is responsible of subcrontracted activities.


MI1974 40g x 1 Test Material 220,00

milk spikedHeavy Metals LIO


Progetto Trieste - Pesticide Residues, HeavyMetals, Nitrite and Nitrate - 2019 Programme


TECHNICAL ASPECTS


Category

List of moleculesPesticides 2-Phenylphenol (ortho-phenylphenol), Acephate, Acetamiprid, Acetochlor, Acrinathrin, Aldicarb,

Aldicarb-sulfone (aldoxycarb), Aldicarb-sulfoxide, Allethrin, Ametoctradin, Atrazine, Azinphos-ethyl, Azinphos-methyl, Azoxystrobin, Benalaxyl, Bendiocarb, Bifenthrin, Biphenyl, Bitertanol, Boscalid, Bromophos-ethyl, Bromopropylate, Bromuconazole, Bupirimate, Buprofezin, Cadusafos, Captan, Carbaryl, Carbendazim, Carbofuran, Carbofuran(3-hydroxy), Carboxin, Chlorantraniliprole (rynaxypyr), Chlordane (cis e trans), Chlorfenapyr, Chlorfenvinphos, Chloridazon, Chlorobenzilate, Chlorothalonil, Chlorpropham, Chlorpyrifos (ethyl), Chlorpyrifos-methyl, Chlorthal-dimethyl, Clofentezine, Clomazone, Clothianidin, Cyazofamid, Cyflufenamid, Cyfluthrin (sum of constituent isomers), Cyhalothrin-lambda Cimoxany, Cypermethrin (sum of constituent isomers), Cyproconazole, Cyprodinil, Cyromazine, Cumaphos, Demeton-s-methyl, Demeton-S-methyl-sulfon, Desmethyl-pirimicarb, Diafenthiuron, Diazinon, Dichlorvos, Dicloran, Dicofol, Diclobutrazol, Dicrotophos, Dieldrin, Diethofencarb, Difenoconazole, Diflubenzuron, Dimethenamid, Dimethoato, Dimehtomorph, Diniconazole, Diphenylamine, Disulfoton, Disulfoton-sulfoxide, Disulfoton-sulfone, Dodine, Diuron, Endosulfan I e II (alpha e beta), Endosulfan-sulfate, Endrin, Epoxiconazole, Hexaconazole, Ethiofencarb, Etofenprox, Ethion, Ethirimol, Ethoprophos, Etoxazole, Etrimfos, Famoxadone, Fenamidone, Fenamiphos, Fenamiphos-sulfoxide, Fenamiphos-sulfone, Fenarimol, Fenitrothion, Fenazaquin, Fenbuconazole, Fenhexamid, Fenoxaprop-p-ethyle, Fenoxycarb, Fenpropathrin, Fenpropidin, Fenpropimorph, Fenpyroximate, Fensulfothion, Fention, Fenvalerate, Fipronil-sulfone, Flonicamid, Flucythrinate, Fluazifop-p-butyl, Fluazinam, Fludioxonil, Flufenoxuron, Fluopicolide, Fluopyram, Fluquinconazol, Flusilazole, Flutriafol, Fluvalinate (tau), Fosetyl-aluminium, Formothion, Fosthiazate,Fuberidazole, Flufenacet, Fosfamidon, Furathiocarb, HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), Heptachlor, Heptachlor-epoxide (cis e trans), Heptenophos, Hexaconazole, Haloxyfop-2 ethoxyethyl, Haloxyfop-p-methyl, Hexythiazox, Imazalil, Imidacloprid, Indoxacarb, Iprodion, Iprovalicarb, Isofenphos-ethyl, Isofenphos-methyl, Isoproturon, Isoxaben, Kresoxim-methyl, Lenacil, Linuron, Lufenuron, Malaoxon, Malathion, Mandipropamid, Mecarbam, Mepanipyrim, Metalaxyl, Methamidophos, Metamitron, Metconazole,Metazachlor, Methiocarb, Methiocarb sulfoxide, Methomyl, Methoxychlor, Methoxyfenozide, Metolachlor, Metrafenone, Metribuzin, Mevinphos, Monocrotophos, Monolinuron, Myclobutanil, Nuarimol, Omethoate Oxadiazon, Oxadixyl, Oxamyl, Oxyfluorfen, Oxycarboxin, Oxydemeton-methyl, Paclobutrazol, Pencycuron, Penconazole, Pendimethalin, Permethrin, Phenthoate, Phorate, Phosalone, Phosmet, Phosphamidon, Piperonyl-butoxide, Pyraclostrobin, Pyridaben, Pyrifenox, Pyrimethanil, Pirimicarb, Pirimiphos-ethyl, Pirimiphos-methyl, Pyriproxyfen, Prochloraz, Procymidone, Profenofos, Promecarb, Prometon, Prometryn, Propamocarb, Propargite, Propaquizafop, Propazine, Propiconazole, Propyzamide, Propoxur, Prosulfocarb, Prothiofos, Pymetrozine, Quinalphos,Quinoxyfen, Quintozene, Quizalofop-ethyl, Spinetoram, Spinosad (A and D), Spirodiclofen, Spiromesifen, Spirotetramat, Spiroxamine, Sulfotep, Tebuconazole, Tebufenozide, Tebufenpyrad, Tecnazene, Teflubenzuron, Tefluthrin, Terbufos, Terbumeton, Terbuthylazine, Terbutryn, Tetraconazole, Tetrachlorvinphos, Tetradifon, Tetramethrin, Thiabendazole, Thiacloprid, Thiamethoxam, Thiodicarb, Tolclofos-methyl, Tolylfluanid, Thiophanate methyl, Triadimenol, Triazophos, Tricyclazole,Trichlorphon, Triadimefon, Trifloxystrobin, Triflumuron, Trifluralin, Triticonazole,Vamidotion, Vinclozolin, Zoxamide.

tomato and fish: < 300 ppb

(8 molecules will be present) Nitrate nitrate lettuce: < 8000 ppm

Heavy metals milk and tomato: lead, cadmium, mercury (all molecules will be present)fish and muscle: lead, cadmium, mercury, arsenic (all molecules will be present)

milk: < 120 ppbtomato: < 800 ppbfish and muscle: < 2 ppm

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.


Cyromazin cyromazin (all molecules will be present) eggs: < 100 ppb

Melamine

Fipronil

melamine (all molecules will be present)

fipronil and fipronil-sulfone (all molecules will be present)

eggs: < 200 ppb

eggs: < 80 ppb

(all molecules will be present)

Milk test materials would contain preservative solutions.


Progetto Trieste - Mycotoxins2019 Programme






TECHNICAL ASPECTS


Category

List of moleculesAflatoxins B/G aflatoxins B1, B2, G1, G2 and/or total aflatoxins maize: < 60 ppb or blank

Fumonisins fumonisin B1, B2 and/or sum (B1+B2) maize: < 6000 ppb or blank Ochratoxin A ochratoxin A maize: < 30 ppb or blank


Shipping date: June 24th 2019. Result submission deadline: July 29th 2019. Final Report available in September 2019. Order deadline: April 26th 2019

ROUND of JUNE (see next page too)


sMaterial has been irradied. The irradiation process has been subcontracted.

MA1950 +

MA1956 A 2 Test Materials B

750,00 600,00

Aflatoxins B/G, DON,

2 Test Materials

maize flour incurredZON, Fumonisins s

When the shipment includes 2 test materials , the laboratory will receive an evaluation for each test material.

Analysis of aflatoxins B&G and fumonisins intended to the homogeneity study have been subcontracted.

Test Veritas is responsible of subcrontracted activities.

Ochratoxin A

DON deoxynivalenol maize: < 6000 ppb or blank

ZON zearalenone maize: < 500 ppb or blank

MA1950 A 80g x 1 Test Material B

420,00 370,00

Aflatoxins B/G

40g x 1 Test Material partial participations in MA1950

Only for the analysis of fumonisins:

A 80g x 1 Test Material B 40g x 1 Test Material

260,00 190,00 MA1950/YOnly for the analysis of aflatoxins:


MA1950/F

maize flour incurred

260,00190,00

Fumonisins sOchratoxin A

Only for the analysis of ochratoxin A: A 80g x 1 Test Material B 40g x 1 Test Material

MA1950/O 260,00

190,00

For the analysis of aflatoxins and fumonisins: A 80g x 1 Test Material B 40g x 1 Test Material MA1950/YF 330,00

250,00

For the analysis of aflatoxins and ochratoxin A: A 80g x 1 Test Material B 40g x 1 Test Material MA1950/YO 330,00

250,00

For the analysis of fumonisins and ochratoxin A: A 80g x 1 Test Material B 40g x 1 Test Material MA1950/FO 330,00

250,00

MA1956 A 55g x 1 Test Material B

330,00 250,00

DON and ZON

55g x 1 Test Material partial participations in MA1956

Only for the analysis of ZON:


260,00 190,00 MA1956/DOnly for the analysis of DON:


MA1956/Z

maize flour incurred

260,00190,00

s


Progetto Trieste - Mycotoxins and Acrylamide2019 Programme






Shipping date: June 24th 2019. Result submission deadline: July 29th 2019. Final Report available in September 2019. Order deadline: April 26th 2019

ROUND of JUNE (see previous page too)



When the shipment includes 2 test materials , they are at a different concentration of analyte. The laboratory

Analysis of patuline and aflatoxins B&G intended to the homogeneity study have been subcontracted.

will receive an evaluation for each test material.

Test Veritas is responsible of subcrontracted activities.

N1951 A 50g x 1 Test Material B incurred 50g x 1 Test Material

Aflatoxins B/G pistachio 260,00 190,00

ss

Ochratoxin A A 260,00 incurred

VF1953 A 50ml x 1 Test Material spikedapple juice

(clear)

Patulin 260,00

B 55g x 2 Test Materials 190,00 55g x 2 Test Materials green coffee

and cocoa s

sGC+C1952

Ochratoxin A A 260,00 incurred B 30g x 1 Test Material 190,00

60g x 1 Test Material cured ham

HC1954

TECHNICAL ASPECTS


Category

List of molecules

Aflatoxins B/G aflatoxins B1, B2, G1, G2 and/or total aflatoxins

Ochratoxin A ochratoxin A coffee, cocoa: < 30 ppb or blank

Patulin patulin apple juice: < 150 ppb


pistachio: < 40 ppb

cured ham: < 5 ppb

Acrylamide A 250,00 incurred B 20g x 2 Test Material 190,00

40g x 2 Test Material bread

BF1955

Acrylamide acrylamide bread: < 500 ppb


Progetto Trieste - Mycotoxins2019 Programme

Those proficiency tests could distinguish between the participation with confirmatory methods (HPLC-GC) or screening methods (ELISA, RIA, biosensors, microbial inhibition assays, lateral flow, etc...).For participation with confirmatory methods the code is A and quantification is requested. Evaluation of performance

For participation with screening methods the code is B and quantification is optional. Qualitative results will be




TECHNICAL ASPECTS


Category

List of moleculesAflatoxin M1 aflatoxin M1 milk: < 100 ppt or blank

cheese: < 700 ppt DON deoxynivalenol wheat: < 6000 ppb

T-2 & HT-2 T-2 & HT-2 toxins & as a sum wheat: < 600 ppb

Ochratoxin A ochratoxin A paprika: < 30 ppb; raisin: < 50 ppb

Each test material may contain one or more substances from the table below. Some materials could be “blank”.The proposed concentrations are indicative, specially for incurred matrix (naturally contaminated) with multiple contamination.Milk test materials would contain preservative solutions.It is not requested to research all the molecules of each group.

Shipping date: October 14th 2019. Result submission deadline: November 18th 2019. Final Report available in January 2020. Order deadline: September 13th 2019

ROUND of OCTOBER



SP1964 A 55g x 1 Test Material B

260,00 190,00

Aflatoxins B/G andOchratoxin A 55g x 1 Test Material

paprika

F1962 A 55g x 1 Test Material B

260,00 190,00 55g x 1 Test Material

feedAflatoxins B/G

s

s


260,00 165,00 Aflatoxin M1 bovine milk 20ml x 2 Test Materials

incurred

CE1961 A 50g x 1 Test Material B

260,00 190,00 Aflatoxin M1 fresh cheese

50g x 1 Test Material spiked

WH1963 A 55g x 1 Test Material B

330,00 250,00

DON and T-2 & HT-2


partial participations in WH1963

Only for the analysis of DON: A 55g x 1 Test Material B 55g x 1 Test Material

260,00 190,00 WH1963/D

Only for the analysis of T-2 & HT-2: A 55g x 1 Test Materia B 55g x 1 Test Material

WH1963/T

wheat

260,00190,00

s

Aflatoxins B/G aflatoxins B1, B2, G1, G2 and/or total feed: < 80 ppb; paprika: < 40 ppb

incurred

incurred

incurred


Analysis of aflatoxins B&G, T-2 & HT-2 intended to the homogeneity study have been subcontracted.

When the shipment includes 2 test materials , they are at a different concentration of analyte. The laboratory will receive an evaluation for each test material.

Test Veritas is responsible of subcontracted activities.

LIO

LIO

and spiked

(spreadable cheese or similar)

DF1965 A 55g x 1 Test Material B

260,00 190,00 Ochratoxin A 55g x 1 Test Material

dried vine fruit spiked(raisin)

(water/fruit slurry)


Progetto Trieste - Mycotoxins

We want to evidence you in this prewiew some proficiency testing that were not present in the 2019 programme but will be present in 2020.


ROUND OF FEBRUARY 2020


Analytes Matrix

tomato or

orange

Alternaria toxins ( tenuazonic acid, alternariol,

alternariol monomethyl ether and altenuene)

and much more....

P

Progetto Trieste c/o Test Veritas Srl Head Quarter: Via Svizzera 16 – 35127 Padova (PD) - ItalyTel. +39 049 8256292 Fax 049 21064938 [email protected] www.testveritas.com

For order placement...

Progetto Trieste has a Restricted Web Area for participants at www.testveritas.com.

At www.testveritas.com it is available information about how Progetto Triesteworks, advantages,FAQ and examples of FinalReport to show elaborationdata methods.

After login in the Restricted Web Area it is possible to fill in the on-line order form.


All prices are excluding VAT, where applicable, and shipment costs. PRICE FOR ADDITIONAL MATERIAL :

120,00 for codes containing 2 test materials90,00 Euro for codes containing 1 test material

Laboratories that order additional material will receive double quantity of material. Aditional materials will be sold only in combination with "A" or "B" Test Materials

Purchase of "additional material" does not allow to take part into the performance assessment.

PRICE REDUCTIONS (applicable only to orders placed on-line): 5% price reduction for ordering 6 or more Test Materials "A" o "B"

SHIPPING COST (Euro): for mycotoxin rounds

cereals, nuts, feed, coffee, milk: 60,00 EU

130,00 Shipping cost for other destinations will bequote on request.

INVOICING, PAYMENT CONDITIONSThe performance assessment service will start from the registration to the proficiency program. For t

his

reason the invoice will be issued upon the receipt of your order and has to be paid before the test mat

erials

will be shipped.Note: in case your invoice is not paid before the test materials are send, your laboratory would be

cancelled from the participant's list.

Payment can be made by bank credit transfer. Our bank details will be indicated in the order confi

rmation

and in the invoice.


General conditions

water : urine, milk, honey, eggs, tissue:

A fixed bank charge of 20,00 euro will be applied for the orders from all non-EU countries. The orders from non-EU countries would be paid against proforma-invoice; 35,00 euro for the certificate of origin can be charged.

Euro

apple juice, cheese, raisin:

Europe non-EU

90,00 130,00

for veterinary drug residues rounds

60,00 EU

130,00

Europe non-EU

90,00 130,00

In case the provided volume is not enough, it is possible to order additional material.

TAX


QUALITY SYSTEMProficiency Testing Scheme for mycotoxins and veterinary drug residues, histamine and pesticide residues are UNI CEI EN ISO/IEC 17043:2010 accredited by ACCREDIA

schemes at www.testveritas.com.

Scopes of accreditation are available at www.accredia.it.The meaning of the accreditation and the and the details of accredited schemes at www.testveritas.com.

Accreditation excludes, in any case, ACCREDIA from any responsibility regarding the offered service.Progetto Trieste provider, Test Veritas Srl, operates in conformance with UNI EN ISO 9001:2015 (Cert. N. IT12/0502).


JURISDICTIONAny dispute arising from this contract is exclusively competent the Court of Trieste, excluding any competing court. Every business relationship will be settled in Italian language. If there were written communications in English, the only language accepted to the Italian alternative, the interpretation of which was contrary to written communication in Italian always prevail the sense of the latter.

Shipping cost for other destinations will bequote on request.

for pesticides, heavy metals, nitrates, histamine and other compounds rounds

60,00

EU130,00

Europe non-EU

Shipping cost for other destinations will bequote on request.

(Cert. PTP N. 0008) .



Progetto Trieste submitting results

CONFIDENTIALITY OF RESULTSThe identity of partecipants is confidential: every participating laboratory receives a code.Only with specifical authorization from the participant, the Progetto Trieste Secretariat will disclose all or part of the results/evaluation to third parties. In exceptional circumstances, when a regulatory authority requires proficiency testingresults to be directly provided to the autthority by the proficiency testing provider, the affected participants shall benotified of this action in writing.The participants’ list will be published in the Final Report.

RESULTS AND REPORT

Reports will be available on the website inside the Restricted Web Area archive.Participants will be informed by email about the availability of the Final Report.

Results are returned through Progetto Trieste Restricted Web Area.

Hard-copy reports are available for an additional charge.These are sent to participants by post.


CONTROL MATERIALS (AFTER PROFICIENCY TEST CONCLUSION)At the end of the rounds, Test Materials are made available to the participants (until stock lasts) to carry out further investigations or to use them in the control charts of the analytical method. The test materials will be kept for 2 months. Exceeded this time, where possible they will be accompanied by a datasheet which will establish the deadline. The recordings of the tests carried out relating to the test materials will be available for 2 years.

Documents

w w w .tes tveritas.com info@ tes tveritas · in tern ational demand for se rvices and p rodu cts for anal ysis. scheme P ro get to Tries te. The main featu res of Proget to Tries