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Page 1: Introduction

IntroductionIntroduction

Chapter 1Chapter 1

Page 2: Introduction
Page 3: Introduction

Instrumental MeasurementInstrumental Measurement

Page 4: Introduction

FluorimeterFluorimeter

Page 5: Introduction

Properties employed in Properties employed in Instrumental MethodsInstrumental Methods

Page 6: Introduction

Examples of Instrumental Examples of Instrumental ComponentsComponents

Page 7: Introduction

Selecting Analytical MethodSelecting Analytical Method

Page 8: Introduction

Method Choice (continued)Method Choice (continued)

Page 9: Introduction

Dynamic RangeDynamic Range

Page 10: Introduction

Signal to NoiseSignal to Noise

Page 11: Introduction

Precision and AccuracyPrecision and Accuracy

Page 12: Introduction

Uncertainty vs. Uncertainty vs. ConcentrationConcentration

Page 13: Introduction

Precision of Analytical Precision of Analytical MethodsMethods

Page 14: Introduction

AccuracyAccuracyPrecisionPrecisionDeterminate ErrorDeterminate Error(systematic)(systematic)Indeterminate Error Indeterminate Error (Random)(Random)

Page 15: Introduction

Method of Standard Method of Standard AdditionsAdditions

Page 16: Introduction

Problem 1-11Problem 1-11

Page 17: Introduction

Fluormetric Determination of Phenobarbital

y = 3.164x + 3.246

R2 = 0.9999

-4

-2

0

2

4

6

8

10

12

-2 -1.5 -1 -0.5 0 0.5 1 1.5 2 2.5

Volume (mL)

Fluo

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