QuantaSmart™
Tri-Carb®
Model 2810TR, 2910TR, 3110TR, 3180TR/SL
1
1
1
Online Help 1
5
5
6
Library 12
2
15
15
16
17
17
18
18
Getting Started 19
3
IPA 21
21
21
IPA 21
21
IPA 23
IPA 29
4
CPM 33
CPM 33
CPM 34
Assay Definition 35
Assay Parameters 36
Count Conditions 38
Count Corrections 41
Report Definition 43
Report Output 46
Special Files 47
Worklist 49
5
50
50
51
52
52
52
Output 53
6
54
54
54
55
56
Assay Definition 57
Assay Parameters 58
Count Conditions 60
Count Corrections 63
Report Definition 65
Report Output 68
Special Files 69
Worklist 71
7
DPM 73
DPM 73
DPM 74
Assay Definition 75
Assay Parameters 76
Count Conditions 78
Count Corrections 83
Report Definition 85
Report Output 88
Special Files 89
Worklist 91
QuantaSmart
Operation manual 1
1
QuantaSmart Tri-Carb
Windows Xp
Output Report Spectra View
Replay
Nuclide Library
QuantaSmart
Online Help
QuantaSmart
QuantaSmart Help
Contents, Index, search help text link
QuantaSmart Help
QuantaSmart
Operation manual 2
Contents
Contents
Figure 1-1. Contents
QuantaSmart
Operation manual 3
Index
Index
Figure 1-2. Index
QuantaSmart
Operation manual 4
Find “Word” “Words”
“Word” Word
Note “Word” “Phrase” “Help”
Find
Figure 1-3. Find
QuantaSmart
Operation manual 5
Assay
QuantaSmart
Assay Definition
Protocol
QuantaSmart 60
60
QuantaSmart
Operation manual 6
QuantaSmart
File Run View Libraries Tools IPA Diagnostics
Help
Figure 1-4.
QuantaSmart
Operation manual 7
Alt
File
File
Run
Run
View
View
“Replay” View
Libraries
Libraries “Sample Nuclides” “Quench Standards Libraries”
“Alpha Beta”
“Alpha Beta” “Alpha Beta Standard”
Tool
Tool “Radio nuclide Decay Calculator”
IPA
IPA (Instrument Performance Assessment )
Diagnostics
Diagnostics
QuantaSmart
Operation manual 8
Window
“Spectra View”
Help
Help QuantaSmart
Instrument Status Bar
Status Bar
Protocol Tree
Protocol Tree
Flags
“Priostat ”
QuantaSmart
Operation manual 9
Report Symbol
Prohibitory Symbols
“Nuclide
Library”
The Replay Tree
“Replay” “Replay Tree”
QuantaSmart
Operation manual 10
SpectraView
1.
2.
3.
4.
Figure 1-5. SpectraView .
QuantaSmart
Operation manual 11
Sample Number
Count time
Pre-count Delay
Note
Acquisition Time
Apply AEC
tSIE AEC
AEC Automatic Efficiency Correction
AEC
KeV Full Scale
“Auto”
Count Full Scale
Y
“Auto”
Y
Log keV Scale
Log keV
QuantaSmart
Operation manual 12
Linear keV Scale
keV
Region
RegionA,B,C
CPM
CPM
CPM
2%S
95% Confidence limits
Assay Definition
Report Definition
Library
“Nuclide Library” “Nuclide Library”
“Alpha Beta”
“Alpha Beta” “Alpha Beta Nuclide
Library”
“Quench Standard Library”
“DPM Assay” DPM Disintegration Per Minute
QuantaSmart
Operation manual 13
“Sample Nuclide Library”
“Alpha Beta Standard” “Alpha Beta Nuclide Library” “Quench Standard”
“Sample Nuclides Library”
“Alpha Beta Assay”
“Library” “Library ”
QuantaSmart
Operation manual 14
- Note -
QuantaSmart
Operation manual 15
2
β
CPM Count Per Minute
DPM Disintegration Per Minute
DPM
QuantaSmart
Operation manual 16
Figure 2-1.
4ml
12 15 20ml 18
6 7ml
ID ID
PID Positive Sample Identification
Toward
QuantaSmart
Operation manual 17
DPM
Run
Pause Stop
Start Resume
Next Protocol
End Protocol
Forward
Reverse
QuantaSmart
Operation manual 18
QuantaSmart “Assay Definition”
“Reports”
Protocol
Protocol
Output
File Print
Assay Select Assay
OK
QuantaSmart
Operation manual 19
Getting Started
Alpha Beta, Alpha Beta Standards, CPM Assay, DPM
Single, DPM Dual, DPM Triple, FS DPM, Direct DPM, Quench Standards,
Single Photo Counting
Direct DPM DPM
3 7
QuantaSmart
Operation manual 20
- Note -
QuantaSmart
Operation manual 21
IPA
(IPA)
PMT
14
C
β
14C QIP Quench Indicating
Parameter SIE transformed Spectral Index of the External Standard
1000 tSIE
1000
IPA
IPA Instrument Performance Assessment3H
14C
Figure of Merit2
Chi-Square
IPA
SNC Self-Normalization & Calibration IPA
SNC 23
QuantaSmart
Operation manual 22
Note BGO
IPA 23 SNC
23
SNC IPA
23 SNC IPA
IPA 23
IPA
23
QuantaSmart
Operation manual 23
IPA
IPA
IPA IPA Definition
IPA Definition
Figure 3-1. IPA Definition
3H Standard DPM
3H DPM
( ) DPM
QuantaSmart
Operation manual 24
3H Reference Date
3H
14C -14 Standard DPM
14C DPM
DPM
14C
Background Count Time
14C
3H
60
3H E
2B Figure of Merit Threshold
E2
B E2
B
IPA
14C -14 E
2B Figure of Merit Threshold
14C E
2B E
2
IPA
Do Chi Square Test for 3H
20
QuantaSmart
Operation manual 25
Do Chi Square Test for 14C -14
-14
14C 20
RS 232 Transmit IPA Data
IPA RS 232
of Datapoints to Establish Baseline
14C IPA
99
3H Background Mean and Limit
IPA
4SE
14C -14 Background Mean and Limit
IPA14
C
4SE
3H Efficiency Mean and Limit
IPA
3%
14C -14 Efficiency Mean and Limit
IPA -14
3%
QuantaSmart
Operation manual 26
Reset Baselines
IPA
Establish Baseline 99
Super Low Level SNC
IPA
SNC
Note SNC
Figure 3-2. Super Low Level Tri-Carb SNC
-14
High Sensitivity Low Level super Low Level
QuantaSmart
Operation manual 27
“IDLE”
SNC
IPA
“ ”
Super Low Level BGO SNC
IPA
SNC
Note SNC
QuantaSmart
Operation manual 28
Figure 3-3. Super Low Level Tri-Carb SNC
2. 14
C
3.
4. 3H
5.
6. IDLE
SNC
IPA
“ ”
Note BGO
IPA 23 SNC
QuantaSmart
Operation manual 29
IPA
IPA IPA IPA
IPA
IPA
IPA
IPA
IPA
14C -14 Background
-14 IPA
SD
SD IPA
14C -14 Background Baseline
-14
“IPA Definition”
14C -14 Chi-Square
-14 IPA
30 20
7.63 36.19
SD IPA
14C -14 Efficiency
-14
SD IPA
QuantaSmart
Operation manual 30
14C -14 Efficiency Baseline
IPA Definition
14C -14 Figure of Merit
FOM Figure of Merit
14 SD
IPA
3H Background
IPA
SD Standard Deviation
SD IPA
3H Background Baseline
IPA Deviation
SD Standard Deviation
3H Chi Square
IPA
30 20
7.63 36.19
SD IPA
3H Efficiency
SD IPA
QuantaSmart
Operation manual 31
3H Efficiency Baseline
IPA Definition
3H Figure of Merit
FOM Figure of Merit
SD
IPA
IPA
IPA
IPA
Figure 3-4. IPA Charts & Tables Window
QuantaSmart
Operation manual 32
- Note -
QuantaSmart
Operation manual 33
CPM
CPM
QuantaSmart
CPM
CPM
1 2 3
CPM Count Per
Minute
CPM
3
QuantaSmart
Operation manual 34
CPM
CPM File New Assay
Select Assay Type (Figure 4-1)
Figure 4-1. Select Assay Type
Select Assay Type CPM OK Assay
Definition (Figure 4-2)
Note: QuantaSmart
QuantaSmart
Operation manual 35
Assay Definition
Assay Definition Assay Parameters, Count Conditions, Count
Corrections, Report Definition, Report Output, Special Files, Worklist
Assay Definition
CPM
■
■ Sample Nuclides library
■
■
■
■ Worklist
QuantaSmart
Operation manual 36
Assay Parameters
Assay Parameters
Figure 4-2. Assay Parameters Tab
Password
Lock Assay
Note
Lock Assay
Password
QuantaSmart
Operation manual 37
Author
Assay Description
Note: ”Assay Parameters”
QuantaSmart
Operation manual 38
Count Conditions
Count Conditions
Figure 4-3. Count Conditions Tab
Name
Sample Nuclide Library
(Figure 4-4)
QuantaSmart
Operation manual 39
Figure 4-4. Sample Nuclides Library
Note:
Sample Nuclide Library
Sample Nuclide Library
DPM
OK
Assay Count Cycles
Count Time
2 Sigma% Low Count Reject (LCR)
QuantaSmart
Operation manual 40
Background Subtract
CPM
st
10 CPM
IPA IPA
IPA
CPM
Note: Count Conditions ”Count
Conditions”
QuantaSmart
Operation manual 41
Count Corrections
Count Corrections
Figure 4-5. Count Corrections Tab
Static Controller
-
■ 40%
■ (PPN 7000901)
■
Pre-Count delay
QuantaSmart
Operation manual 42
Luminescence Correction
Apply Half-life Correction
Sample Nuclide Library
Reference Date Time Reference Date Time
Note: Count Correction ”Count Correction”
QuantaSmart
Operation manual 43
Report Definition
Report Definition
Figure 4-6. Report Definition Tab
Report Name
Report Name
Note: /,@,
QuantaSmart
Operation manual 44
Report Fields
Report Fields
Report Fields
Report Fields Block
Data
Add
Report Fields custom
Delete
Note: (Custom) Custom
Format
Equation…
custum
Note Delete Note
QuantaSmart
Operation manual 45
Figure 4-7. Equation
QuantaSmart
Operation manual 46
Report Output
Report Output
Figure 4-8. Report Output
Report Output
RS-232
Note: QuantaSmart
Delimited Text ASCII Excel Lotus 1-2-3
QuantaSmart
Operation manual 47
Special Files
Special Files
Figure 4-9. Special Files
■ Spectra File (composite) 1
■ Spectrum File (Individual) 1
■ IPA Data File
■ Prot.dat file
■ 2000ca.dat file
Data Output Path
QuantaSmart
Operation manual 48
Assay Parameter Assay Definition OK
5
QuantaSmart
Operation manual 49
Worklist :
Assay Definition Worklist ( 4-10) Positive Identification (PID#)
Sample List Library
Note Worklist
Note Worklist 2810TR, 2910TR 3110TR, 3180TR
Figure 4-10. Worklist Tab.
QuantaSmart
Operation manual 50
1. 3
2. Assay Definition 5
4,6,7
3.
QuantaSmart
Associate
Assay… File Associate Assay
Figure 5-1.
QuantaSmart
Operation manual 51
Associate Assay
Data Paths User ID Additional Header
OK Protocol
Figure 5-2.
forward
QuantaSmart
Operation manual 52
QuantaSmart Figure
5-1
Output Figure 5-3
QuantaSmart
Operation manual 53
Output
Output Figure 5-3
Assay Definition 5
Assay Definition Output
Figure 5-3. Output
QuantaSmart
Operation manual 54
QuantaSmart
2
(QIP) SIS, tSIE
%Efficiency vs QIP DPM
(Disintegration Per Minute) DPM CPM Efficiency
QuantaSmart
Operation manual 55
1
DPM
DPM=CPM/Efficiency
3 ”Calibration”
QuantaSmart
Operation manual 56
File New Assay
Assay
Type
Figure 6-1. Select Assay Type
Assay Type Quench Standards OK Assay
Definition
Note: QuantaSmart
QuantaSmart
Operation manual 57
Assay Definition
Assay Definition Assay Parameters, Count Conditions, Count
Corrections, Report Definition, Report Output, Special Files Worklist
Assay Definition
CPM
■
■ Sample Nuclides Library
■
■
■
■ Worklist
QuantaSmart
Operation manual 58
Assay Parameters
Assay Parameters
Figure 6-2. Assay Parameters Tab
Password
Lock Assay
Lock Assay
Password
Author
QuantaSmart
Operation manual 59
Assay Description
Note: ”Assay Parameters”
QuantaSmart
Operation manual 60
Count Conditions
Count Conditions
Figure 6-3. Count Conditions Tab
Name
Quench Standard Library
(Figure 6-4)
QuantaSmart
Operation manual 61
Figure 6-4. Quench Standards Library
Quench Standard Quench Standard Library
Quench Standard Library
DPM DPM
DPM DPM
( )
DPM Reference Date
QuantSmart DPM
OK
Note:
Quench Standard Library Quench Curve
”Quench Curve”
QuantaSmart
Operation manual 62
Count Time
2 Sigma% Low Count Reject (LCR)
Background Subtract
CPM
st
10 CPM
IPA IPA
IPA
CPM
Note: Count Conditions ”Count
Conditions”
QuantaSmart
Operation manual 63
Count Corrections
Count Corrections
Figure 6-5. Count Corrections Tab
Static Controller
-
■ 40%
■ (PPN 7000901)
■
Pre-Count delay
QuantaSmart
Operation manual 64
Apply Half-life Correction
Quench Standard Library
Reference Date Time Reference Date
Time
DPM
DPM
Note: Count Correction ”Count Correction”
QuantaSmart
Operation manual 65
Report Definition
Report Definition
Figure 6-6. Reports Tab
Report Name
Report Name
Note: /,@,
QuantaSmart
Operation manual 66
Report Fields
Report Fields
Report Fields
Report Fields Block
Data
Add
Report Fields custom
Delete
Note: (Custom) Custom
Format
Equation…
custum
Note Delete Note
QuantaSmart
Operation manual 67
Figure 6-7. Equation
QuantaSmart
Operation manual 68
Report Output
Report Output
Figure 6-8. Report Output
Report Output
RS-232
QuantaSmart
Operation manual 69
Special Files
Special Files
Figure 6-9. Special Files
■ Spectra File (composite) 1
■ Spectrum File (Individual) 1
■ IPA Data file
■ Prot.dat file
■ 2000ca.dat file
Data Output Path
QuantaSmart
Operation manual 70
Quench Standard
Library DPM
Assay Parameter Assay Definition OK
5
QuantaSmart
Operation manual 71
Worklist :
Assay Definition Worklist ( 6-10) Positive Identification (PID#)
Sample List Library
Note Worklist
Note Worklist 2810TR, 2910TR 3110TR, 3180TR
Figure 6-10. Worklist Tab.
QuantaSmart
Operation manual 72
- Note -
QuantaSmart
Operation manual 73
DPM
DPM
2 DPM
DPM
DPM
DPM DPM
DPM
DPM
■ CPM
■ (QIP)
■ (%Efficiency vs. QIP)
■ DPM CPM Efficiency DPM
DPM
1. 2
”Calibration”
2. DPM
6 ”Quench
Standard Assay”
QuantaSmart
Operation manual 74
DPM
DPM File New Assay
Select Assay Type (Figure 7-1)
Figure 7-1. Select Assay Type
Select Assay Type DPM(Single) OK
Assay Definition
Note: QuantSmart
QuantaSmart
Operation manual 75
Assay Definition
Assay Definition Assay Parameters, Count Conditions, Count
Corrections, Report Definition, Report Output, Special Files Worklist
Assay Definition
CPM
■
■ Sample Nuclides library
■
■
■
■ Worklist
QuantaSmart
Operation manual 76
Assay Parameters
Assay Parameters
Figure 7-2. Assay Parameters Tab
Password
Lock Assay
Lock Assay
Password
Author
QuantaSmart
Operation manual 77
Assay Description
Note: ”Assay Parameters”
QuantaSmart
Operation manual 78
Count Conditions
Count Conditions
Figure 7-3. Count Conditions Tab
Name
Sample Nuclide Library
(Figure 7-4)
QuantaSmart
Operation manual 79
Figure 7-4. Sample Nuclides Library
Note:
Sample Nuclide Library
Sample Nuclide Library
Quench Set
Quench Set 1 1
Low Quench 2
2 Medium Set 3
3 High Set Quench Standard
(Figure 7-5)
QuantaSmart
Operation manual 80
Figure 7-5. Quench Standards Library
DPM OK
Sample Nuclide Library Quench Set
Assay Definition Count Conditions Quench Set
(Figure 7-3)
Sample Nuclide Library OK
QuantaSmart
Operation manual 81
Quench Indicator
Quench Indicator Parameter 3
tSIE(transformed Spectral Index of External standards)
Barium-133
tSIE tSIE
1000 tSIE
10 DPM
160,000 0.5% 2Sigma tSIE
tSIE/AEC AEC
SIS SIS
SIS CPM
Assay Count Cycles
Count Time
2 Sigma% Low Count Reject (LCR)
QuantaSmart
Operation manual 82
Background Subtract
CPM
st
10 CPM
IPA IPA
IPA
CPM
Note: Count Conditions ”Count
Conditions”
QuantaSmart
Operation manual 83
Count Corrections
Count Corrections
Figure 7-6. Count Corrections Tab
Static Controller
-
■ 40%
■ (PPN 7000901)
■
Pre-Count delay
QuantaSmart
Operation manual 84
Luminescence Correction
Apply Half-life Correction
Sample Nuclide Library
Reference Date Time Reference Date
Time
Note: Count Correction ”Count Correction”
QuantaSmart
Operation manual 85
Report Definition
Report Definition
Figure 7-7. Reports Tab
Report Name
Report Name
Note: /,@,
QuantaSmart
Operation manual 86
Report Fields
Report Fields
Report Fields
Report Fields Block
Data
Add
Report Fields custom
Delete
Note: (Custom) Custom
Format
Equation…
custum
Note Delete Note
QuantaSmart
Operation manual 87
Figure 7-8. Equation
Note:
QuantaSmart
Operation manual 88
Report Output
Report Output
Figure 7-9. Report Output
Report Output
RS-232
QuantaSmart
Operation manual 89
Special Files
Special Files
Figure 7-10. Special Files
■ Spectra File (Composite) 1
■ Spectrum File (Individual) 1
■ IPA Data file
■ Prot.dat file
■ 2000ca.dat file
QuantaSmart
Operation manual 90
Assay Parameter Assay Definition OK
5
QuantaSmart
Operation manual 91
Worklist :
Assay Definition Worklist ( 7-11) Positive Identification (PID#)
Sample List Library
Note Worklist
Note Worklist 2810TR, 2910TR 3110TR, 3180TR
Figure 7-11. Worklist Tab.
QuantaSmart
Operation manual 92
― Note
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