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PDF, Dental waxes ,Origin, Composition, Properties, Classification , Applications.
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5/5/2014
1
DENTAL WAXESPRESENTED BY
DR.HASHMAT GUL
DEMONSTRATOR
DENTAL MATERIALS DEPT.
INTRODUCTION
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WAXES
� DEFINATION
Waxes are thermoplastic materials which are normally solids at room
temperature but melt without decomposition, to form mobile liquids.
� ORIGIN OF WAXES
MINERAL ANIMAL PLANT
1) Paraffin 1) Bees 1) Carnauba
2) Microcrystalline 2) Candela
DENTAL WAXES
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DENTAL WAXES
� DEFINATION : Dental waxes are thermoplastic moldable materials
that are solids at room temperature.
� GENERAL COMPOSITION OF DENTAL WAXES
• Hydrocarbon (e.g. Paraffin )* or Ester types
• High or low MW Acc.to desired properties
•Constitute the main bulk
Base wax
• Hydrocarbon or Ester type
• High or low MW Acc.to desired properties
• Traces To impart the desired properties in the final product
Modifier
Colorant
DENTAL WAXES-BASE WAX
BASE WAX
� Paraffin
� Microcrystalline
� PARAFFIN
� The major component of almost all dental waxes
� Obtained by fractional distillation of petroleum.
� Linear hydrocarbon
� Low MW (a couple dozen carbon atoms long) just high enough that it is
solid at room temperature.
� Not pure as a mixture of hydrocarbons
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DENTAL WAXES-MODIFIERS
MODIFIERS� Normally Dental waxes consist of two or more components which
may be natural or synthetic waxes, resins, oils, fats and pigments.
� Blending is carried out to produce a material with the desired properties for a
specific application e.g.
Wax Desired Property imparted by the Modifier wax
1). Bees Wax � Less brittle
� Increase stickiness
2). Carnauba wax &
Candelilla wax
� Control the softening temperature.
� Carnauba tend to increase the hardness and water resistance.
3).Micro- crystalline
wax
� Raise melting point.
� Lower the softening temperature
� Lower brittleness.
PROPERTIES OF DENTAL WAXES
� THERMAL PROPERTIES
� The softening temperature
� Melting point
� The coefficient of thermal expansion which affect
� Accuracy
� Dimensional stability
� MECHANICAL PROPERTIES
� Flow & Creep
� Brittleness & Toughness
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�THERMAL PROPERTIES
THE SOFTENING TEMPERATURE
� Also called SOLID-SOLID TRANSITION TEMPERATURE
� All the waxes used in dentistry have
� a predominantly crystalline structure
� a well-defined melting point
� On heating, a second endothermic peak exists at a temperature somewhat lower than the melting point. This peak is indicative of a solid– solid transition involving
� Change in crystalline structure of the wax , accompanied by a change in
mechanical properties i.e.
Brittle solid Softer, moldable material
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MELTING POINT: It is the temperature at which the wax converts into liquid-state & began to flow.
METHODS OF SOFTENING WAX PRIOR
TO MOULDING INCLUDE :
� A Bunsen burner
� A water bath
� An infra-red lamp
� A Wax Annealer
� Waxes are very poor thermal conductors and must be maintained
above the solid-solid transition temperature for long enough to allow
thorough softening to occur throughout the material. *
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THE COEFFICIENT OF THERMAL
EXPANSION
� DEFINATION : The fractional change in size per degree change in temperature at a constant pressure.
� Waxes exhibit high values of The coefficient of thermal expansion which affect
� Accuracy
� Dimensional stability
� PROBLEMS
� On cooling waxes undergo thermal contraction.
Low thermal conductivity values uneven Cooling* internal stresses Dimensional changes.*
� Greater stresses may also be incorporated if the wax is not properly softened before moulding
� MECHANICAL PROPERTIES
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FLOW & CREEP
� A major factor which determines the moldability and stability of a wax is
its flow value. This property is related to creep. *
� To prevent distortion , Waxes should, ideally, exhibit
� considerable flow at the molding temperature.
� little or no flow at mouth temperature or room temperature .
� CREEP AND FLOW ARE BOTH MEASURED by applying a load (2 kg) to a
cylindrical specimen (10 mm diameter by 6 mm height) and measuring
the extent to which the specimen becomes compressed after a given
time(10 min).
� The flow is recorded as the percentage change in the height of the
cylinder.
BRITTLENESS & TOUGHNESS*
� BRITTLENESS & TOUGHNESS are the important properties which the
manufacturers can, to some extent, control.
� EXAMPLES
� FOR DENTURE WAXES, toughness is required since the wax denture
base may have to be removed from a slightly undercut cast many
times without fracturing.
� FOR INLAY WAXES, brittleness is preferred in order that the wax will
fracture rather than distort on removal from an undercut cavity. This
will indicate to the dental surgeon that a modification to the cavity
shape is required
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CLASSIFICATION OF DENTAL WAXES
1. PATTERN WAXES
�Are used in the construction of metal
castings & bases for dentures through lost
wax technique.*
� TYPES
1) Inlay wax
2) Casting wax
3) Baseplate wax/Modeling wax
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PATTERN WAXES-Inlay wax
� COMPOSITION
� Paraffin + Carnauba + Ceresin + Beeswax + Colorant.
a) 60% Paraffin (and Microcrystalline) Wax = BASE Wax
b) 25% Carnuba (and Candelilla) Wax = MODIFIER Wax
c) 10% Ceresin = MODIFIER Wax
d) 5% Beeswax = MODIFIER Wax
e) < 1% Colorants = COLORANT
� USED to produce patterns for metal casting using the lost wax tech.e.g. inlays, onlays , crowns & pontics
PATTERN WAXES-Inlay wax
� SUPPLIED IN:
�Several forms: sticks, pellets & tins.
�Dark colours : blue or green.
�They are labelled : hard, medium & soft (acc. to their
melting ranges).
�They are not sticky to touch
� REQUIREMENTS :
a) Good adaptation to dies .
b) Thermal stability at low temperatures.
c) Complete pyrolysis at high temperatures.
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PATTERN WAXES-Inlay wax
� TYPES : There are two types:
� Type 1 Soft Indirect tech
� Type 2 Hard Direct tech
PATTERN WAXES-Inlay wax
a). TYPE II INLAY WAX:
� Used directly in the mouth , softened & placed into
the prepared tooth in the direct waxing technique.*
� Has a lower melting range for the comfort of the
patient & the accuracy of the wax on removal.
� Has a softening point slightly higher than the mouth
temp.
�All the limitations of the mouth must be considered.
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PATTERN WAXES-Inlay wax
b). Type I INLAY wax:
� More frequently used, where wax is melted onto a die outside the mouth in the indirect technique.*
� Softening temp. lower than mouth temp. for indirect tech.
� Most dentists prefer to use this & have a dental laboratory technician produce the wax pattern and casting.
INLAY WAXPhysical Properties – Melting Range
COMPOSITION (%)
TE
MP
ER
AT
UR
E (
C)
Paraffin Carnuba
40
30
20
60
50
70
80
90
25 50 75 100
LIQUID
LIQUID + SOLID
SOLID
Melting Onset (Solidus)
Melting Completion (Liquidus)
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INLAY WAXPhysical Properties – Thermal Expansion of Components
250ppm/°°°°C
0 25 30 40 4535 50
0
1.2
1.0
0.8
0.6
0.4
0.2
TEMPERATURE (C)
EX
PA
NS
ION
(%
)
KERRHARDWAX
INLAY WAXMechanical Properties & Chemical Properties
� MECHANICAL PROPERTIES:
1) Flow < 1%
2) Ductility = moderate
3) Residual Stress = none
� CHEMICAL PROPERTIES:
1) Homogeneity = good
2) Contact Angle = low
3) Oxidation = complete
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PATTERN WAXES-CASTING WAXES
� USED to construct the metal framework
of partial and complete dentures.
�Comes in sheets & preformed shapes.
� The physical properties are similar to
inlay wax except the melting range.
� The melting range is only important for
laboratory procedures, because
these waxes are not softened in mouth.
PATTERN WAXES-BASEPLATE WAX
� Also called Modelling wax.
� They are sheets of wax generally pink in
color to simulate the color of the gingiva.
� USES
1) Occlusal or bite rims *
2) Spacer in custom trays.
3) Pattern for plastic portion of dentures.
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PATTERN WAXES-BASEPLATE WAX
� TYPES
� Type 1 soft wax building contours & veneers.
� Type 2 hard wax Used in Temperate climate.
� Type 3 extra hard most commonly used ‘coz it is hard
at mouth temperature.
� COMPOSITION
� paraffin wax and bees wax
� SOFTENED in Water bath to ensure even thickness of sheets.
PATTERN WAXES-BASEPLATE WAX
� REQUIREMENTS
1) The wax must not distort at mouth temperatures.*
2) Should be tough in order to reduce the chances of fracture/distortion during removal from the stone model or shallow undercuts.
3) They can easily be trimmed with a sharp instrument without tearing, chipping or flaking atroom temperature.
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2.PROCESSING WAXES
� Used primarily to aid in dental procedures both clinically & in laboratory.
� TYPES
� Boxing wax
� Utility wax
� Sticky wax
� Alu wax
� Carding wax
PROCESSING WAXES- BOXING WAX
� USED to form the base portion of a gypsum
model.
The 1.5-inch-wide, red strip of boxing wax is
wrapped around the impression to produce a
form into which the gypsum is poured.
� MANIPULATION
� Easy
� Slightly tacky at room temperature,
allowing it to adhere to itself to secure
the boxed form.
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PROCESSING WAXES-UTILITY WAX
� Also called periphery wax
� Comes in ropes and sheets that are
easily
manipulated at room temp.
� Various colours of pink, white & red.
PROCESSING WAXES-UTILITY WAX
� USES OF WAX ROPES:
1). To adapt the periphery of the impression tray to customize the tray & aid in patient comfort.
Provide a better fit into the vestibule & control the movement of the impression material.
2). To cover sharp brackets and wires in orthodontic patients.
� USE OF WAX SHEETS:
1) May be layered to form a horseshoe shape & used for wax bite registrations
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PROCESSING WAXES-STICKY WAX
� Used to adhere components of metal,
gypsum, or resin together temporarily
during fabrication & repair.
� It comes in orange sticks that are hard &
brittle at room temp, but when heated
under flame become soft & sticky.
� Because it is brittle, even the slightest
torque will fracture the wax.
(Important alert for the operator).
PROCESSING WAXES-ALU WAX
� USED to get occlusal registration.
� Contains aluminium particles and it is brittle.
� Available in thin & thick sheets.
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PROCESSING WAXES-Carding wax
� Used by manufacturers for
attaching denture teeth to
display sheets.
3.IMPRESSION WAXES
� USED
� To obtain impressions of the oral structures.
� TYPES
1) Corrective Impression waxes
2) Bite-Registration waxes
� Bite-wafers
� Occlusal-indicator wax
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IMPRESSION WAXES-Corrective impression wax
� USED to correct small imperfection (e.g. airblows) in other impressions,
especial zinc oxide impressions(edentulous imp).
� Are thermoplastic materials, which flow at mouth temperature and are soft a room temperature. They do not set by chemical reaction.
� CONSIST OF paraffin wax and beeswax in a ratio of approximately 3:1 to ensure the wax flows at mouth temperature.
� DISADVANTAGE: Easily distorted so, A cast should be poured up immediately after taking the impression . These materials are not commonly
used.
� Replaced by ELASTOMERIC IMPRESSION MATERIALS.
IMPRESSION WAXES- BITE REGISTRATION WAX
1- BITE WAFERS:
� It is used to produce wax bite registrations for articulation of models.
� The preformed horseshoe shapes are often reinforced with metal particles to provide stability.
� It is susceptible to distortion at temp slightly higher than mouth temp.
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IMPRESSION WAXES-BITE REGISTRATION WAX
2. OCCLUSAL INDICATOR WAX:
� Used to detect areas of premature occlusal contact.*
�Supplied in scored strips & is dark green, yellow or blue in colour.