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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY v.,..,'« •»- M'v 27 . oREGION m
OFFICE OF ANALYTICAL SERVICES AND QUALITY ASSURANCE201 DEFENSE HIGHWAY
SUITE 20OANNAPOLIS, MARYLAND 21401
DATE : November 26, 1996
SUBJECT: Region III Data QA Review/)/?
FROM : Cynthia E. Caporale ( "&£?Region III ESATRPO (3EPfiO)
TO : Chris CorbettRegional Project Manager (3HW22)
Attached is the inorganic data validation report for the KeystoneSanitation Site (Case? 24906) completed by the Region IIIEnvironmental Services Assistance Team (ESAT) contractor under thedirection of Region III BSD. ,
- • : . . ' ' ' %
If you have any questions regarding this review, please call me at(410) 573-2732.
Attachment •
'cc: Russ Sloboda/Haliburton NUS
WA File: 0396004 TDF:1113
•AR32I7D8-Printed on Recycled Pap-.-r
USEPA REGION! III
MIC IE8IONAL ACCEPTANCE/REJECnON/REDUCEO VALUE RECOMMENDATION FORM
l*XTtlul«t NUMBER OF SAMPLES, i* i ««•«•••—.„„„....... ... .............————•"-————-————————— • tOO HAILDATE •
PARTI. DATA ACCEI ANCE OR REJECTION
INSTRUCTIONS, EPA REOZONS MUST ACCEFT OR iCJECT DATA WITHIN M DAYS. IF DATA ARC 8EZN6 REJECTED, THZS FORMMUST BE ACCOMPANIED BY I.I A SIGHED MEMO FROM THE REGIONAL OFFICIAL OESOtZBIMB THE CONTRACTUAL REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS <OATA REVIEW,TELEPHONE tOCS, ETC.), t.J ALL KJECTED DATA.
A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS S06.
* • ACCEPT ALL :;: '•' . REJECT ALL
B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY RCJECT ALL SAMPLES IN A PARTICULAR FRACTION D4 THZS SD6.ALL FRACTIONS NOT MARKED AS REJECTED ARE ACCEPTED. ,
REJECT ALL, RTTALa CYAMBg
C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVELCHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AMD COMPLETE THE REVERSE SIDEOF THZS FORM. •
___ PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION
PART II. REDUCED VALUE. • A. . .
INSTRUCTIONS! REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE TO BE PROCESSED, THISFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE RE6ZONAL OFFICIAL CZTZNB THE CONTRACTUAL NON-COHPLZANCE;THE DOLLAR AMOUNT FOR REDUCED VALUEJ AND A WRITTEN JUSTIFICATION (NARRATIVE} OF HOW SAMPLE WORTH WASDETERMINED FOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.!
CHECK ONE OF THE FOLLOWING:' ' . • ; ' • ' , . . ' . ' ' • ' • ' ' • • • • , ' ' . ' . - . . ' - . ' .NO REDUCED VALUE B»_» REDUCED VALUE (COMPLETE. REVERSE SIDE) :
IDENTIFY THE SAMPLES/FRACTIONS THAT ARC RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SIDE OF THIS FORM.
••••••••••••••••••••M«WUHHM TKZS FORM CANNOT BE PROCEESSEO WITHOUT A SIGNATURE *••••••*»••••••••••••••«•••• . . . • ' . ' . y - ' . - - ' ' . • I - • . . ' . ; > ' •• • " • • ' ' ' • t i ' " •« NAME OF REGIONAL OFFICIAL, T &l\e VJilolrVC*_____________________________ •
&lfj*r a fj Aj2bi* SIGNATURE! C~\rPj+* a JA S A JefiOCOtV ___________ DATE! 7 * I I 1 tp_____ - •. •
« SEND THIS FORM TOt A BtfH ^ MMM| ^ ^ . •• . • . ' VRHR R R R R R R R R R R R R K ^ • «
«'
AR32I709•••••••••••••••••••••••••••••••••••••••M• SEE LIST OF SAMPLES ON REVERSE SIDE •••••••••••••••••••••••••••••••••••••••••I
I LAB CODE! CHEM . CASE MOli 2490C SDC NO., NCSHOS I
FART III. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE ;
ENTER AN -X" IN THE BLOCK TO THE RIGHT OF THE "V-FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A -D" IN THE BLOCK TO THE RIGHT OF THE "Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE.ALL SAMPLES THAT ARE NOT MARKED WITH AN "JT OR A -0" AXE ACCEPTED. '
SAMPLE
LCSS
MCSMIS
HCSM11
HCSH12
HCSM17
HCSM19
HCSH25
HCSM25D
NCSH25S
HCSM26
HCSM28
HCSM3I
HCSH31
MCSM32
HCSM5S
HCSM34
11
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
FlHI
V
V
Y
Y
Y
Y
Y
V
V
Y
Y
Y
Y
Y
Y
V
IACTETAL
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
IONS 4S I
1
1
1
1
1
1
1
1
1
1
1
1
1
;iii
WALYZED 1CYANIDE
Y '
V 1
V 1
r'JY 1
V I
V 1
V 1
Y I
Y 1
Y r.VY I
Y '
Y 1
v 1
v «
1R32I7IO
USEPA REGION! HII • ' ' ' • " . * , ' ' - - '
' INORGANZC REOZONAL ACCEnANtt/REJeCTION/REOUCED VALUE RECOMKENDATZON FORM
.....-.——....._....*................__„_,_„ .
i LAB CODE, CKEM CASE NoT«m""" """""s"*""*;"I On NAME* KEYSTONE SANITATION NUMBER OF SAMPLES, 23 I •««««,..„.„•.....................................................—__m———M- • SOO HAILOATE
PART Z. DATA ACCEPTANCE OR REJECTION '
ZMSTRUCTIONSi EPA REGIONS MUST ACCEPT OR REJECT DATA WZTHZN SI DAYS, IF DATA ARE BEZNO REJECTED, THZS FORMMUST U ACCOMPANIED BY I.I A SIGNED NEMO FROM THi REGIONAL OFFZCIAL OESCRZBZN6 THE CONTRACTUAL, REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS (DATA tEVZCWS,TCLEFHONE LOGS, ETC.}, t.) ALL REJECTED DATA.
A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS SOG.
.£— ACCEPT ALL _____ REJECT ALL
B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWING IF YOU FULLY REJECT ALL SAMPLES IN A PARTICULAR FRACTION IN THIS SOO.ALL FRACTIONS NOT MARKED AS REJECTED ARE ACCEPTED. /
* ' * . ' i ' • • ** - ' -
REJECT ALL, HfTUA : CYANIM '
C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVEL ACHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AND COMPLETE THE REVERSE SIDE
;. OF THZS FORM. . ' ..• -.': • '- ;;'• • ' ' • . ' ; . ' • -
___. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION
PART IX. REDUCED VALUE
INSTRUCTIONS, REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE TO BE PROCESSED, THZSFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE REGIONAL OFFICIAL CITING THE CONTRACTUAL NON-COMPLIANCE ITHE DOLLAR AMOUNT FOR REDUCED VALUE} AND A WRITTEN JUSTIFICATION (NARRATIVE) OF HOW SAMPLE WORTH WASDETERMINEDFOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.)
CHECK ONE OF THE FOLLOWING!
J NO REDUCED VALUE ;..'.. ': REDUCED VALUE (COMPLETE REVERSE SIDE)
IDENTIFY THE SAMPLES/FRACTIONS THAT ARE RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SIDE OF THIS FORM.
, • ' I : . " ' " ' . ' • ' •
•••••••••••••••••••MHHMMH THZS FORM CANNOT BE FROCEESSEO WITHOUT A SIGNATURE ••••••••••••••••••••••••••••
NAME OF REGIONAL OFFICIAL!
SIGNATURE!
•••••••••••••••••••••••••••••••••••••••IK• SEE LIST OF SAMPLES ON REVERSE SIDE •
I Til
I LAB CODE, CHEM CASE NO. t 24916 S06 NO., HCSM80 |
FART IZZ. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE
ENTER AM "X* IN THE BLOCK TO THE RIGHT OF THE -Y" FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A IT IN THE BLOCK TO .THE RIGHT OF THE -Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE;ALL SAMPLES.THAT ARE NOT MARKED WITH AN "X" OR A -0" ARE ACCEPTED.
SAMPLE
LCSW
HCSMII
HCSMI1
MCSMI2
HCSMM
HCSMI5
NOSH!*
MCSHI7
HCSMM
MCSMI9
HCSMII
Hcsms
HCSM14
MCSH15
HCSH1B
MCSM2I
HCSM21
HCSM24
HCSH24D
NCSM24S
MCSH27
MCSM29
HCSH3S
1 FRACTIONS ANALYZED1 METALS 1 CYANIDE
1 Y I 1 1
1 V 1 IV I
IV 1 1 1
1 V I 1 .Y 1
1 V 1 1 Y 1
1 V I 1 1
1 VI 1 1
1 VI 1 . 1
I v I 1 I
1 Y 1 IV I
1 V 1 1 1
1 V 1 1 V 1
1 V 1 1 1
1 Y 1 1 Y 1
IV 1 1 V 1
1 V 1 1 1
IV 1 1 V 1 V
1 V 1 1 Y 1
1 Y 1 1 V 1
1 Y 1 1 V 1
1 V I IV I
1 Y I I VI
1 V | | I
AR32I7I2
USEPA REGION, III
INORGANIC REGIONAL ACCEnANtt/REJECTION/REDUCEO VALUE RECOMMENDATION FORM
..____1________.__.....i__.__.__________ "»«"»•««»•»«•„•'
I LAB CODE, CKEM CASE«... """"~~~~~£ " "I
-• !.!.i.!!!!I.!!?!.... IMPBIOF t"IM>i * '—————————————.-..-————... ....——......... « SDO MAILDATE •
PARTI. DATA ACCEPTANCE OR REJECTION
INSTRUCTIONS, EPA REGIONS MUST ACCEPT OR REJECT DATA WITHIN SI DAYS. IF DATA ARE BEING REJECTED, THZS FORMMUST BE ACCOMPANIED BY I.) A SIGNED NEMO FROM THE REGIONAL OFFICIAL DESCRIBING THE CONTRACTUAL REASONS FORREJECTION. ATTACH ALL RELATED DOCUMENTS (DATA REVIEW, TELE PHONE LOGS, ETC.), C.) ALL 1CJECTEO DATA.
A. FULL DATA ACCEPTANCE OR REJECTIONCHECK ONE OF THE FOLLOWZNO IF YOU FULLY ACCEPT OR FULLY REJECT ALL SAMPLES IN THIS SOG.
_SL_ ACCEPT ALL ____ REJECT ALL ,
B. REJECTION OF ALL SAMPLES FOR A PARTICULAR FRACTIONCHECK ONE OF THE FOLLOWZNO ZF YOU FULLY REJECT ALL SAMPLES ZN A PARTICULAR FRACTION IN THIS SOG.ALL FRACTIONS NOT MARKED AS REJECTED ARC ACCEPTED.
REJECT ALL, METALS •_:.', CtUftOf
C. REJECTION AT THE SAMPLE AND FRACTIONAL LEVELCHECK THE FOLLOWING TO REJECT SAMPLES AT THE SAMPLE/FRACTIONAL LEVEL AND COMPLETE THE REVERSE SIDEOF THZS FORM. ;
___PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE/FRACTION• • " ' . " , ' * ' • ' . ' . " ' ' . -
PART II. REDUCED VALUE
INSTRUCTIONS: REGION RECOMMENDS REDUCED VALUE AND RETAINS THE DATA. FOR A REDUCED VALUE "TO, BE PROCESSED, THISFORM MUST BE ACCOMPANIED BY A SIGNED NEMO FROM THE REGIONAL OFFICIAL CZTZNG THE CONTRACTUAL NON-COMPLIANCE;THE DOLLAR AMOUNT FOR REDUCED VALUE) AND A WRITTEN JUSTIFICATION (NARRATIVE) OF HOW SAMPLE WORTH WASDETERMINED FOR EACH AFFECTED SAMPLE. ATTACH ALL RELATED DOCUMENTS (DATA REVIEWS, TELEPHONE LOGS, ETC.) .
CHECK ONE OF THE FOLLOWING,
. V NO REDUCED VALUE .___ REDUCED VALUE (COMPLETE REVERSE SZDE)
IDENTIFY THE SAMPLES/FRACTIONS THAT ARC RECOMMENDED FOR REDUCED VALUE ON THE REVERSE SZDE OF THIS FORM.
% - ' • - ; **' ' " "
••••••••••••••••••••••••••••M THIS FORM CANNOT BE PROCEESSEO WITHOUT A SIGNATURE ••••••••••••••••••••x»a*»M*N
• NAME OF REGIONAL OFFICIAL!•• SIGNATURE,
••••••••••••••••••••••••••••••••••••••••I• SEE LIST OF SAMPLES ON REVERSE SIDE « ,
A-R3.2 I 7 1
I LAB CODE, CHEM CASE NO;i 24906 SOG NO., HCSM16 I
PART HI. PARTIAL ACCEPTANCE AND REJECTION BY SAMPLE
ENTER AN -X- IN THE BLOCK TO THE RIGHT OF THE *Y" FOR THE FRACTION RECOMMENDED FOR REJECTIONENTER A -0- IN THE BLOCK TO THE RIGHT OF THE *Y" FOR THE FRACTION RECOMMENDED FOR REDUCED VALUE.ALL SAMPLES THAT ARE NOT HARKED WITH AN>X" OR A "D" ARE ACCEPTED.
SAMPLE
LCSW
HCSHU
MCSMUO
MCSHltS
1 FRACT]1 METAL!
1 V 1
1 V 1
1 V 1
1 V I
EONSi 1
1
1
1
1
ANALYZEDCYANIDE
1
v I
v 1V 1
•{J/)R32I7I1»
LOCKHEED M A R T I N /
LOCKHEED MARTIS Region J, 1419 Forest Drive. Suite 104ENVIRONMENTAL SYSTEMS & TECH\OLOOIES Annapolis. Man-land 21403
Telephone <4 10) 268-7705: Fax 1 4 10) 268-8472
DATE! NOVEMBER 2 5 , 1996 • ' • • • _ .
SUBJECTS IKORGANIC DATA VALIDATION (ZK2 LEVEL)SITE: KEYSTONE SANITATION CASE 24906SDGS MCSMOO, MCSM03, MCSM16
' '.PROMl BAR! PRASADVV? MAHBOOBEH HECANIC __
DATA REVIEWER SENIOR OVERSIGHT CHEMIST
TOt CYNTHIA E. CAPORALEESAT REGIONAL PROJECT OFFICER,
THROUGH! DALE S. BOSHARTESAT TEAM MANAGER
•( j Case 24906 consisted of a total of thirty-four (34)x~— . samples in three Sample Delivery Groups (SDGs) analyzed
for metals and cyanide (CN) by the Chemtech ConsultingGroup (CHEM) . The samples were analyzed according to theContract Laboratory Program (CLP) Statement of Work (SOW)
. . ILH04.0, through the Routine Analytical Services (RAS)program. The specifics about the samples in this caseare listed below. ,SDG Matrix .- Sample (s)
HCSMOO Aqueous (unfiltered) 12
Aqueous (filtered) 8
HCSM03 ;4oli 13
MCSM16 Aqueous (unfiltered) 1
The sample set included one (1) each of the following:rinsate blank, unfiltered field blank, filtered fieldblank, unfiltered field duplicate pair, soil fieldduplicate; pair.
. . . - ' . ' , . ' i ' . . - ' ' • . - . ' • • ; 'SUMMARY
All analytes were successfully analyzed in all samples.. The. samples vere analyzed by the laboratory and validated
AR321715
Page 2 of 5
by the reviewer on an SDG basis. The results for therinsate blank were used for qualifying all samples*Areas of concern with respect to data usability arelisted below.MINOR ISSUES .
The continuing calibration (CCB), rinsata (RB) and field(FB) blanks had reported results greater than theInstrument Detection Limits. (IDLs) for the analyteslisted below. The reported results for these analytes inthe affected samples which are less than five times(< 5x) the blank concentrations may be biased high andhave been qualified "B".SDG Blank Type Analyta(3>MCSMOO CCB Magnesium (Mg)
RB Manganese (Mn), Zinc (Zn)FB (filtered) Mn, Zn
MCSM16 RB 2n
The percent difference (% D) for the ICP serial dilution ^analysis was outsida the control limit for the potassium(K) analyte in SDG MCSMO?. ' The'reported results for thisanalyte in the affected samples are estimated and havebeen qualified "Jn *
The initial and final Contract Required Detection Limit(CRDL) standard recoveries were mixed for the arsenic(As) and thallium (Td) analytes in SDG MCSMOO. Thequantitation limits for these analytes are estimated dueto opposing bias effects and have been qualified "UJW.The CRDL standard recovery was high for the chromium (Cr)analyte in SDG MCSMOO. The continuing calibration blankfor this analyte had a negative result with an absolutevalue > IDL. The reported results for the Cr analyte insamples MCSM20 and MCSM29, which are < 2x .CRDL and < 2xthe absolute value of the blank, ara estimated due toopposing bias effects and have been qualified "J".
The CRDL standard recovery was low for the As analyte inSDG MCSMOO. The quantitation limits for this analyte inthe affected samples may be biased low and have beenqualified "UL11.
The CRDL standard recoveries were high for the analytes j.listed below. The reported results for these analytas in "—-
AR32I7I6
. . - ' . : . Pages of 5the affected samples which are < 2x CRDL may be biasedhigh and have been qualified "Kn, unless superseded bythe "B«! qualifier.SDG Analytes
MCSMOO Cobalt (Co), Copper (Cu) ,, Lead (Pb) , Hn,Nickel (Ni), Zn
HCSM03 As, Cadmium (Cd) , Selenium (Se)
MCSM16 Co, Ni^
The preparation and continuing calibration blanks inSDG MCSMOO had negative results with absolute values> IDL for the analytes listed below. The reportedresults for these analytes in the affected samples,which are < 2x absolute value of the blank, and thequantitation limits may be biased low and have beenqualified "L" and "UL'Y respectively, unlesssuperseded by the "B" qualifier.
Blank Type Analvtes '
PB Aluminum (Al) , Calcium (Ca) , Cu,Iron (Fe) , Magnesium (Mg) , K,Sodium (Na) ,
NOTES ' '.';'•'. •'•;". .• • • . _• _ ' • . ••The As, Pb, Se and Tl analytes were analyzed using theICP method and had IDLs less than the CRDLs.
The sample shipment, designated for the CN analysis ofunfiltered sample MCSM01, was not received by the .laboratory. Hence, the CN analysis for sample MCSM01was not performed by the laboratory. See phone logby the laboratory dated 8/1/96 in Appendix B.The laboratory incorrectly reported on Form 2B ofSDG MCSMOO that tihe CRDL standard recovery for themercury (Hg) analyte was 0.0% instead of 99.0%. Thisdiscrepancy has been rectified during the validation.
The field duplicate results were outside the controllimits (20% RPD, ± CRDL) for several analytes in theaqueous sample pair MCSM27/MCSM29. The field duplicateresults were within the control limits (35% RPD,± 2x CRDL) for all analytes, except Zn, in the soilsample pair MCSM26/MCSM28. The concentrations for the
AR32I7I7
. Page 4 of 5outliers and their precision* estimates are reported inTable 4.The filtered aqueous sample MCSM08 had several analytesdetected at concentrations greater than those in itsunfiltered aliquot (sample MCSM02). The filtered aqueoussample MCSM20 had the Pb analyte detected at aconcentration greater than the CRDL while the Pb analytewas not detected in its unfiltered aliquot (sampleMCSM18). The concentrations for the outliers and theirprecision estimates are reported in Table 5. (Theprecision criteria for the laboratory duplicates havebeen applied to the field duplicates also.)Soil sample concentrations are calculated on the basis ofthe raw data values (in 0g/L), the gram weight of sampleused, the volume of the digestate/distillate, and the %solids according to the following equation:
mg/Kg = (raw value. uo/L)fdiaeatata volume. LV(weight,g)(% solids/100)
To obtain the quantitation limit, insert the IDL (Form X)for the raw value; refer to Forms XIII to obtain eachsample preparation weight and volume used. The •quantitation limits thus obtained are specific for eachsample and preparation method.The data were reviewed in accordance with the NationalFunctional Guidelines for Evaluating Inorganic Analyses,with modifications for use within Region III.
INFORMATION REGARDING REPORT CONTENT
Table 1A is a summary of qualifiers added to the results from thelaboratory during validation.ATTACHHBNTa
TABLE 1A SUMMARY OF QUALIFIERS ON DATA SUMMARY FORMAFTER DATA VALIDATION
TABLE IB CODES USED IN COMMENTS COLUMN
TABLE 2 GLOSSARY OF DATA QUALIFIER CODES
TABLE 3 DATA SUMMARY FO RMS < '
TABLE 4 SUMMARY OF FIELD DUPLICATE OUTLIERS
TABLE 5 SUMMARY OF UNFILTERED/FILTERED OUTLIERS
AR32I7I8
.11 nil .11 ...j I.
. . ' . . ' Page 5 of 5•' - ' ' V; *. . • - . - ; • •
ATTACHMENTS fContd.i ,
APPENDIX A RESULTS REPORTED BY LABORATORY FORM Is
APPENDIX B SUPPORT DOCUMENTATION
DCN: HP9611KEY.NAR
AR32I7I9
• ' . - • • • Page 1 of 3/
TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY ,
FORM AFTER DATA VALIDATION
• ' . . ' - - . . ' ' ' . - . • ' ' NON- ' . • - . - . • ' „POSITIVE DETECTED
ANALYTB 8EK3 SAMPLES AFFECTED* VALUES VALUES BIAS COMMENTS*
Al MCSMOO 07,10,13-15,18,20, L UL Low PBN(-65.630g/L)21,24,27,35
As MCSMOO 14,20,21,27,29,35 UJ Low/ CRM(88.5%, .High 142.8%) •
00-02,04-07,09,10, UL Low CRL(83.5%) ,13,15,13
MCSM03 03,31,34 K High CRH( 123%) . . _ • • '
25 K High CRH(123%,117.8%) '
Cd MCSM03 03,11,12,19,33,34 K High CRH(111%).
Ca MCSMOO 13,15,21 L UL LoW
Cr MCSMOO 20,29 J High/ CBM(110.9%, .Low -1.2jug/L)
14,21,27,35 , UL, LOW CCN(-1.2/ig/L) '
Co MCSMOO 08 K High CRH(115.3%,' : 116.8%)
29,35 K High CRH(115.3%)
MCSM16 16 K High CRH(116.8%,' 111.9%)
Cu MCSMOO 00-02,04-07,09',10, K High CRH(117.1%,18 .. 115.8%)
08 K High CRH(121%,125.5%)
20,29 K High CRH(115.8%,•-.••••- :. '. ' ' ' ' / ..-121%)
13-15,21,24,27,35 UL Low PBN(-i.61jig/L) •
-«• All samples begin with the prefix "MCSM".* See explanation of Comments on table IB.
flR32l720
/ Y - • ' ' '- . ' - ".- :; • , ••'. ' "' , . ' • '• Page 2 of 3 ••^ TABLE 1A
SUMMARY OF QUALIFIERS ON DATA SUMMARYFORM AFTER DATA VALIDATION
' . ' ' • . ' • • • ' : • • • . . ' • : : • . ' - " • ; NON- .• .POSITIVE DETECTED
ANALYTB SDQ SAMPLES AFFECTED* VALUES VALUES BIAS COMMENTS*
Fe MCSMOO 06,10,13-15,21,27 L UL Low PBN(-53.78/jg/L)
Pb MCSMOO 01,02 K High CRH(126.8%,
08 K High CRH(130.7%) .
20,29 K High CRH(117.S%)
Mg MCSMOO 14 B . High CCB(20.8Mg/L) ', PBN(-66.64pg/L)
13,15,21 UL Low PBN(-66.64/ig/L)* ' " - • . • - . ' » • ' ' , , .
Mn MCSMOO 01,18 B High RB(2.10g/L)-CRH(114.9%)
05-07 B High FB(2.8/*g/L) ,CRH(114.9%)
00,02,04,10,15 K High CRH(114.9%)
14,20 K High CRH(113.1%).. ' ' ' , • • . . • ' ' . • ' . • - , '
,24 K High CRH(113.1%,* 115%)
Ni MCSMOO 02704,05,10 K High CRH( 114.6% )•' : ' • • ' • : - ' . . . ' • . ' - • I
29,35 K High CRH(114.7%) v-
MCSM16 16 K High CRH(117.5%,112.2%)
K MCSMOO 13-15,21 OL Low PBN(-79.44/ig/L)
MCSM03 All samples J . SD(17.2%) .
Se MCSM03 28 K High CRH(117.2%,. . , . : . ; - t . • • : • • > . . 135%) , • • • • • • • .
-H AH samples begin with the prefix "MCSM".* See explanation of Comments on Table IB. .
flR32!72l
Page 3 of 3 , iTABLB 1A
SUMMARY OF QUALIFIERS ON DATA SUMMARYFORM AFTER DATA VALIDATION
.•• ' • ' • ' •••-.- NON-. •' • •'• ' . -POSITIVE DETECTED
ANALYTB 3DQ SAMPLES Ag?ECTED+ VALUES VALUES BIAS COMMENTS*
Na MCSMOO 13,15,21 UL Low PBN(-74.66/ig/L) '
Tl MCSMOO 00-02,04-07,09,10, UJ High/ CRM(123.2%, -13,15,18 Low 75.4%)
14,20,21,27,29,35 UJ Low/ CRM(75.4%,High 147.4%)
Zn MCSMOO 00-02,04-07,09,10, B High RB(24.2pg/L)18 - CRH(115.4%)
20,27,29,35 B High RB(24.2pg/L)".-i CRH(112%)
• • , ' • • - . ' /
* 08 B High RB(24.2 g/L) .
1 4 , . • K High CRH(112%) • i J .
15 K High CRH(115.4%) •
MCSM16 16 B. High RB(24.2Mg/L)CRH(116.4%143.5%)
• ' I • ' • ' ' ' . • ' .
+ All samples begin with tha prefix "MCSM*1.* See explanation of Comments on Table IB.
AR32I722
' ' - . - ' . ; TABLE IB '.'.'• ' ..
CODES USED IN COMMENTS COLUMN
PBN . = The preparation blank had a negative result with absolutevalue > IDL (the blank result is in parenthesis). Thereported results which are < 2x the absolute value of theblank and the quantitation limits may be biased low.
CRN = The initial and final CRDL standard recoveries were mixed(> 110% or < 90%) [% recoveries are in parenthesis]. Thequantitation limits are estimated.
, . , . ' .,! * -.. ..... ^ , • - ^
CRL •* .The CRDL standard recovery .was low .(% recovery is inparenthesis). The quantitation limits may be biased low.
CRH « The CRDL standard recovery was high (% recovery is inparenthesis). The reported results which are < 2x CRDL maybe biased high. v
CBM «= The CRDL standard recovery was high and CCB had negativeresult with absolute value > IDL (recovery and blank valuesare in parenthesis)* The reported results, which are < 2x
' CRDL and < 2x absolute value of the blank, are estimated.CCN = The CCB had a negative result with absolute value > IDL
(the blank result is in parenthesis). The quantitationlimits may be biased low.
CCB •«= The continuing calibration blank had a result > IDL (theresult is in parenthesis). The reported results which are
: < 5x the blank concentration may be biased high.RB «= The rinsate blank had a result > IDL (the result is in
parenthesis). The reported results which are < 5x theblank concentration may be biased high.
FB «* The field blank had a result > IDL (the result is inparenthesis). The reported results which are < 5x theblank concentration may be biased high. .
SD «= The ICP serial dilution results were outside the controllimit (10% D) (% D is in parenthesis]. The reportedresults are estimated.
/5R32I723
' • ; • • . ' . . - ' -TABLE 2 • . ' • , - . - . ' • • ' i
' GLOSSARY 07 DATA QUALIFIER CODES (INORGANIC)
CODES RELATED TO IDENTIFICATION(confidence concerning presence or absence of analytes):
U = Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.
(NO CODE) =» confirmed identification.
B •> Not detected substantially above the level reportedin laboratory or field blanks.
' '. - , • .. . ' /
R =» Unusable result. Analyte may or may not be presentin the sample. Supporting data necessary toconfirm result.
CODES RELATED TO QUANTITATION(can be used for both positive results and sample quantitationl i m i t s ) : . . ' . ' '
J » Analyte Present. Reported value may not beaccurate or precise.
K 3 Analyte present. Reported valua may be biased v^Xhigh. Actual value is expected to be lower.
L =• Analyte present. Reported value may be biased low., Actual value is expected to be higher.
[] = Analyte present. As values approach the IDL thequantitation may not be accurate.
UJ = Not detected, quantitation limit may ba inaccurateor imprecise.
UL « Not detected, quantitation limit is probablyhigher. . ;
CODES
Q a No analytical result.
flR32!72i»
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( • ' ' ' ': - ' '. : , ' • ' ••,'•••'•,;• TABLE 4 '!' \'\ '. ' •
SUMMARY OP FIELD DUPLICATE OUTLIERS
SDG MCSMOO
Analvte HCSM27 MCSM29 Difference
Al ND 940 , 940
Fe 39.3 2260 2220.7
Pb ND 3.2 3.2
Mn 93.4 179 62. 8+
.'•/ SDG MCSM03
Analvte MCSM26 MCSM28 Rpp
Zn 213 83.8 87.1
ND B Not detected.+ «= RPD instead of difference.
ft'R 321-731
TABLB 5 ' .
SUMMARY OF UNPILTERED/ FILTERED OUTLIERS
Analvta HCSM02 MCSM03 Diffarenea
Al 177 553. 376
Cr 1,6 258 256.4
Fe 425 1330 905
Mn 19.2 39.2 20.0
Hi 11^0 193 182
Zn 22.8 49.1 -•- 26.3
Analvta MCSH18 MCSM2Q Diffarenea
Pb ND 3.1 3.1
ND. « Not detected.+ a RPD instead of difference.
AR32I732
APPENDIX A
RESULTS REPORTED BY LABORATORY
i J , ' ' \ ' • • / -' . . \v'.;>; FORM IS - -
BR32I733
8DO MCSMOO
i!R32l73lt
U.S. EPA - CLP •. . " " ' ' ' . ' ' ' • • ' ' l
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET " '
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166MCSMOO
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8739S
Level (low/med): LOW ; Date Received: 08/01/96
% Solids: 0.0 • ;.
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39^37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron ,LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide ,• . f >
Concent rat ion
5759.0 ,9.0
22.81.0 '1.0
36200' 19.3
1.012.0
10303.0
289012.30.20
: 3.03120
' 5.02.0
231009.01.0
25.69.0
C
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Color After: CLOUDY Clarity After: CLEAR Artifacts:
Comments: • ' ' " .
FORM I - IN 003 ILM04.0
AR32 I 735
U.S. EPA .- CLP ', .- 1- ' ... '. . ' ' .
• EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET ' •
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166MCSM01
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 87473 .
Level (low/med): LOW . Date Received: 03/01/96* . - / - ' -
% Solids: 0.0 ' . .
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration•
13909.09.016.11.01.0
331002.01.015.5139
• 4.62230
7.20.203.0
21905.02.0
10600 .9.01.017.1
C
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Color Before: 'BROWN .( Clarity Before: CLEAR Texture:
Color After: CLOUDY Clarity After: CLEAR Artifacts:
Comments: .
FORM I - IN Minji ILM04.0004
AR32I736
U;S. EPA - CLP/;r •" 1- / . '
'' EPA SAMPLE NO.INORGANIC -ANALYSIS DATA SHEET
MCSM02Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.i 24906 SAS No. : SDG No. :.MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8742S
Level (low/med): LOW • Date Received: 08/01/96
% Solidst 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS NO.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-26-07440-62-27440-66-6
. ;
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmium /CalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium'ThalliumVanadiumZincCyanide
Concent rat ion
1779.09.016.4.1.0,1.0
326001..61,026:44253.3
236019.20.20
. 11,01640
5.0, • 2.0
71909.01.022.89.0
C
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Comments: • v
FORM I - IN A-* ILM04.0005AR32I737
U.S.. EPA - CLP• r . ' ' - v • . •• ' •" * . •
EPA SAMPLEINORGANIC ANALYSIS DATA SHEET ..
MCSM04Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: ., SDG No.: MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8741S
Level (low/med): LOW Date Received: 08/01/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43^97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc'Cyanide .
Concentration
2539.09.026.3
- . 1.01.0
256005.21.017.16523.0
452019.30.20'3.4
37305.02.0
100009.01.018.09.0
C
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Comments : . ' '
Clarity Before : CLEAR Texture :
Clarity After: CLEAR Artifacts:
- \ • • . ' . .
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FORM I - IN ILMO.4.0OOG
AR32I738
U.S. EPA - CLP";..v. . •!•-• •. ': '• " . .. • /
- '"'. . • ' - ' -:i'' 'i '. " - - '
* " EPA SAMPLE NO.
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
INORGANIC ANALYSIS DATA SHEET • _____^___
MCSM09
Lab Code: CHEM Case No. :-24906 SAS No. : SDG No.: MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8740S .
Level (low/med):' LOW , Date Received: 08/01/96
% Solids: , 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-36-27440-39-37440*41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmium -Calcium ;ChromiumCobaltCopper 'Iron, •.;••LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
3849.0
. 9.015.0•1.01.0
344001.71.0
13.44503.0
227041.20.203.0
2740• , 5.0
2.06050
."•.. 9.01.0
16.39.0
C
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Color Before: COLORLESS Clarity Before: CLEAR texture:
Color After': . CLOUDY - Clarity After: CLEAR Artifacts:'' _ • ' , * • : • ' • ' " ' • • • *
Comments: - ' ?•,
FORM I -. IN ILM04.0Oil
(5R32I739
U.S. EPA T CLP: ! . • . . _ . . . -' . 'V.'
EPA SAMPLEINORGANIC ANALYSIS DATA SHEET
MCSM13Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSMOO
Matrix {soil/water): WATER - Lab Sample ID: 3743S
Level (low/med) : LOW . Date Received; 08/01/96
* Solids: 0.0 - ' • '
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-4 '7440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
11.09.09.0
, . 1.01.0
. l.-Oi10.01.01 . 01.027.03.011.01.00.203.039.05.02.013.0
. < 9.01.02.09.0
C
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Color Before:'BROWN Clarity Before: CLEAR • Texture:
Color After: COLORLESS Clarity After: CLEAR Artifacts:
Comments: ' . .FIELD QC SAMPLE
FORM I - IN ' ILM04.0013
U.S. EPA - CLP"-'-'.'"'.v ' ' ' ' i - ' ' ' • ' ,•
t .,".'" . : • > • ? ' •' . •.' • '
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET .. . .
MCSM15Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code.: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO• ' • . . ' ' " . . . , . ' ""- . ' *
Matrix (soil/water): WATER Lab Sample ID: 8744S
Level (low/med): LOW ; Date Received: 08/01/96
% Solids: 0.0
Concentration Units.(ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-9S-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6 ,
•• •
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmium 'CalciumChromiumCobaltCopperIronLead 'MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concent rat ion
11.09.09.01.01.01.0
20.71.01.01.0
• 27.03.0
•11. 02.10.203.039.05.02.018.09.01.024.29.0
C
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Color Before: -COLORLESS Clarity Before: CLEAR Texture:
Color After: COLORLESS Clarity After: CLEAR Artifacts:
Comments: .FIELD,QC SAMPLE .
FORM I - IN ' ILM04.0
015
,U.S... EPA - CLP
EPA SAMPLE N'INORGANIC ANALYSIS DATA SHEET ___ \
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166MCSM18
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSMOO
Matrix (soil/water): WATER ' Lab Sample ID: 8745S
Level (low/med): LOW Date Received: 08/01/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
-
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinccyanide
Concentration
1269.09.011.71.01.0
244001.31.0
-' 13.42233.0
20703.10.203 . 0
2360; 5.0
2.07670
9.01.0
' 11.39.0
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Comments: ' , .
FORM I. - IN ILM04.0
016,rtR32l7l>2
U.S. EPA - CLP•.-''•'• 1 - , . -. . ' ' _ '
V' ' •' ' -• - , " " . . . '. ,V :v • ! ' ' ' " • ' -
EPA SAMPLE NO,INORGANIC ANALYSIS DATA SHEET
MCSM21Lab Name: CHEMTECH CONSULTING,GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 9005S
Level (low/med): LOW , Date Received: 08/09/96, • - * '
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
' •'
AnalyteAluminumAntimonyArsenicBarium •BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
11.09.0
- 9.01.0.1.01.010.01.01.01.0
27.03.0
11.01.00.203.0
39.0•" • 5.0
2.018.09.01.02.09.0
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: Clarity Before: CLEAR Texture:
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FORM I - IN ' nift ILM04.0
• A R 32 I 71* 3
U.S. EPA - CLP '. • , 1 . . . - . ' • '
EPA SAMPLE N(INORGANIC ANALYSIS DATA SHEET
MCSM24Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Co.de: CHEM Case NO.: 24906 -"SASNO.: SQG No. : MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 9000S
Level (low/med): LOW ' Date Received: 08/09/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
30.49.0
- 9.010.21.01.0
123001.01.01.0
1533.0
348026.40.203.0
23105.0
, 2.02180
9.01.02.09.0
C
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Comments:
FORM I - IN . ILM04.0019
U.S. EPA- - CLP. . . , - . . 1 . • • ' ' • .
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM27Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 9003S
Level (low/med): LOW . ; Date Received: 08/09/96
\ Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
;
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
11.0, • 9.0
9.0; 74.0. 1.0
1.018400
1.01.01.0
39.33.0
1190093.40.203.0
70005.02.0
93809.0; i.o6.19.0
C
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Comments: • ••. ; <
FORM I - IN ILM04.0020
A R 321?;!* 5-
U.S. EPA - CLP1 ' ' '
EPA SAMPLEINORGANIC ANALYSIS DATA SHEET
MCSM29Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case NO.: 24906 SAS No.: SDG No. : MCSMOO
Matrix (soil/water) : WATER , Lab Sample ID: 90043
Level (low/med): LOW Date Received: 03/09/96• * •
% Solids: 0 . 0 - . ' . , .
. Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLead .MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
9409.09.0
93.41.01.0
231002.31.8
13.72260
3.214800179
0.20• • 6 . 8
83005.02.0
119009.01.0
23.8. 9.0
C
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Color Before: COLORLESS Clarity Before: CLEAR - Texture:
Color After: COLORLESS Clarity After: CLEAR • Artifacts:
Comments: '
FORM I - IN ' ILM04.0021
iVR32l7t»6
U.S. EPA - CLP• : • : " • ' • ' 1
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM05Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8750S
Level {low/med): LOW Date Received: 08/01/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95 47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium -ThalliumVanadiumZincCyanide
Concent rat ion
1679.09.014.91.01.0
237005.31.07.4
1673.0
42308.10.20
. 9.13700
5.0• . 2.0
97309.01.0
34.7
C
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Color Before: .BROWN Clarity Before: CLEAR Texture:
Color After: CLOUDY .Clarity After: CLEAR Artifacts:. • - . ' , . - - ' ' - ' s
Comments:• ' • . -
FORM I - IN , j*nn ILM04.011137
A R 32 I 71* 7
U.S. EPA - CLP '• 1
EPA SAMPLE NO,INORGANIC ANALYSIS DATA SHEET
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166MCSM06
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No,: MCSMOO, ' • - . • • " • '
Matrix (soil/water): WATER •• . . Lab Sample ID: 8746S
Level (low/med): LOW Date Received: 08/01/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS NO.
7429-90-57440-36-07440-33-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-3,7439-89-67439-92-17439-95-47439-96-57439-97-67440-02-0 '7440-09-77732-49-27440-22-47440-23-57440-28-07440-62-27440-65-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper ,IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium .VanadiumZincCyanide
Concentration
1499.09.018.91.0 '1.0
311002.71.0
. ' 3. 9 :. 73.5
3.02460
4.50.203.0
28005.02.0
205009.01.025.4
. . . •
C
3UUBUU
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Color Before: BROWN Clarity Before: CLEAR Texture:
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Comments: - •
FORM I - IN ILM04.0008 v
U.S. EPA - CLP•' :. ...." 'I ' - • .. - ' . '• '
'EPA SAMPLE NO.INORGANIC ANALYSIS DATA . SHEET
MCSM07Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: ,24906 SAS.No.: SDG No.: MCSMOO
Matrix (soil/water): WATER Lab Sample ID: 8748S
Level (low/med): LOW I Date Received: 08/01/96
% Solids: 0.0 : -•.' ' • , ' • '''.' " ' " '' *
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
74 29 -SO -57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenic ,,BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMerCuryNickel .••••PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
1239.0
• 9.013.81.01.0
.291001.0
: i, o11.81693.0
19204.70.203.0
20605.0
W 2.09800
• ' . ' , - 9 . 01.0
12.2
C
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Color After: CLOUDY
Comments i . ' , . . . ' • .
; Clarity Before: CLEAR . Texture:
Clarity After: CLEAR ... Artifacts:
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• • • ' •FORM I - IN An**' ILM04 . 0"09
AR32I7V9
U.S. EPA - CLP, ., ' 1 - _ .- .
: • . , EPA SAMPLEINORGANIC ANALYSIS DATA SHEET •'
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166MCSM03
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSMOO
Matrix (soil/water): WATER Lab Sample-ID: 8751S
Level (low/med): LOW , Date Received: 08/01/96
% Solids: 0.0
Concentration Units (ug/L;or mg/Kg dry weight): UG/Lf-
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-43-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
5539.09.018.51.01.0
31600 •2534.5
21.31330
4.42390
39.2. 0.20
193'1370
• 5.02.0
81009.01.0
-49.11
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Clarity Before: CLEAR Texture:
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- • • • • • - ' « . - • .• • • • -
FORM I - IN _ ILM04.0010
4R32I750
U.S. EPA - CLP... : i
' ' * ' - ' • EPA SAMPLE NO./ . INORGANIC ANALYSIS DATA SHEET
MCSM10Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO
Matrix (soil/water): WATER * Lab Sample ID: 8749S
Level (low/med): LOW Date Received: 08/01/96
% Solids: 0.0 ,
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
' 1279.09.011. L1.01.0
296006.1
- 1.09.973.43.0
188020.90.205.0
2480•' 5.0
2.05550
9.01.0
: 10.4
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Comments: -
FORM I - IN *? ' ' • ILM04.0
VR 32 I 75 I
U.S. EPA - CLP'1 ' ' '
• ; EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET '
MCSM14Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No. : .; SDG No.: MCSMOO1 • ' '. . ' •
• ' - "
Matrix (soil/water): WATER Lab Sample ID: 8752S• r ' •
Level (low/med): LOW Date Received: 08/01/96
* Solids: 0.0 '
Concentration Units (ug/L or mg/Kg dry weight): UG/L ,
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-8 -7439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77732-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
V
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel 'PotassiumSeleniumSilverSodiumThalliumVanadiumZiricCyanide
Concentration
11.09.29.01.01.01.0
3151.01.0
. ' 1.027.03.022.42.80.20
. 3.039*05.0
. 2.04939.0
"1.0.2.3
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Color Before: "COLORLESS Clarity Before: CLEAR Texture:
Color After: COLORLESS Clarity After: CLEAR Artifacts:
Comments: " . .FIELD QC SAMPLE
FORM I .- IN ILM04.0
0144R32I752
tf.S. EPA - CLP .•"•'••.• ; * ' • '•• - • •' '.
. - ' . ' ' " ' " - " • " * . • • '
' • EPA SAMPLE NO.'INORGANIC ANALYSIS DATASHEETo -. •• ..:..:
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166MCSM20
Lab Code: CHEM. Case No. : 24906 SAS No. : SDG No.:, MCSMOO" • • i ' . ' ' " . , - " " . • " ' •
Matrix (soil/water): WATER Lab Sample ID: 8753S
Level (low/med): • LOW . Date Received: 08/01/96
t JSolids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70 -27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28 07440-62-27440-66-6
Analyte /
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel ;.PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
84.89.09.0
• 12.41.01.0
222001.71.08.9
1283 . 1
2070 .15.50.203.0
2450•' ' 5.0
2.07990
9.01.08.1
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Comments:
FORM I - IN ILM04.0
017AR32I753
• N ' U.S. EPA - CLP' . . 1 • ' • , . - • ' • . . . ' s
EPA SAMPLE NO ~• , INORGANIC ANALYSIS DATASHEET , ..'''________' )
I M C S M 3 5
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSMOO
Matrix (soil/water): WATER , Lab Sample ID: 9006S
Level (low/med): LOW Date Received: 08/09/96
% Solids: 0.0
Concentration Units (ug/L or mg/Kg dry weight): UG/L
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-37439-39-67439-92-17439-95-47439-96r57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCoppe^IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
11.09.09.0
60.31.01.0
5130I'.O1.21.0
4233 . 0
44102470.203.3
7545.02.0
59009.0l.'O
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FORM I - IN ftnrt ILM04.0022
AR32l75l»-
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U.S. EPA - CLP.'"•••• : i - ' '
- v '^ EPA SAMPLE NO.U ..-_•• INORGANIC ANALYSIS DATA SHEET''• ' -' . ' > '• .•'.•••••.• - , • • •' ~
MCSM33Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSM03
Matrix (soil/water): SOIL ' Lab Sample ID: 8991S
Level (Idw/medK: LOW Date Received: 08/09/96i • • ' ' ' . ' • ' • • ' . - • ' . ' ' ' - / - • •
* Solids: 52.2
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-9a-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-67439-89-67439-92-17439-95-47439-96-57439-97-r67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver-SodiumThalliumVanadiumZincCyanide
Concentration21800
3.39.4
1060.650.48
194016720.229.6
3960054.9
3030936
0.1926.2801
f 1.80.74
157.3.3
25.7187 :
0.85
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Comments: - '
FORM I - IN ILM04.0
AR32I756
U.S. EPA - CLP• . " 1 • • •• - '
EPA SAMPLEINORGANIC ANALYSIS DATA SHEET .
MCSM32Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM ' Case No. : 24906 SAS No. : SDG No. : MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 89903
Level (low/med): LOW Date Received: 08/09/96% Solids: 66.8 ' ..
Concentration Units (ug/L or mg/Kg dry weight): MG/Kd
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-43-47440-5a-87439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09*77732-49-27440-22-47440-23-57440-28-0,7440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration20400
2.66,0
1580.650.29
130032.119.721.6
2320014.3
• 21604190.1522.4947
v 1.40.53
168, -. ' 2.6
22.335.9'0.65
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EPA SAMPLE NO,INORGANIC ANALYSIS DATA SHEET
MCSM31Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.; 24906 SAS No.: SDG No. : MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 8989S
Level (low/med): LOW Date Received: 08/09/96
% Solids: 59.3
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440 -23- S7440-26-07440-62-27440-66-6
,
AnalyteAluminumAntimonyArsenicBarium'BerylliumCadmiumCalciumChromiumCobaltCopperIron'LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
196003.05.3
73.50.33.0.33
80230.114.518.4
3410011.2
35203000.1625.54791.70.66
1083.016.4
106 •'0.74
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AR32I758
U.S. EPA - CLP• •• •' 1 • . '_ •' ' •...'-.. '.
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET _
MCSM30Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
- . . • .Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 89883
Level (low/med) : LOW Date Received: 08/09/96
% Solids: 33.1- • j • . • -
Concentration Units (ug/L or mg/Kg dry weight): MO/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440*70r27440-47-37440-43-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-29-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenic .BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver .Sodium iThalliumVanadiumZincCyanide
Concentration13300
5.310.483.40.590.59
201034.616.058.2
2320034.0
1510371
0.2735.35103.01.2
148-.-• ' 5.3
17.9140 '.1.3
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AR32 I 759
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•- EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM28Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.': MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 8987S
Level (low/med): , LOW Date Received: 08/09/96
* Solids: 59.7 ; •
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-4 ,'7440-23-57440-28-07440-62-27440-66-6
Analvte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper'IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration16700
3.0•7.696.20.680.33
145042.724.523.4
4050027.6
1780936
0.1718.8947
•*' 1.70.66
148: 3.0
27.8. 83.8 :
0.70
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AR321760
U.S. EPA - CLP ,. : • 1 ' - . ' • •
EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET
Lab Name:,CHEMTECH CONSULTING GROUP Contractt 68-D5-0166MCSM26
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 39933
Level (low/med): LOW Date Received: 08/09/96
% Solids: 58.1.. . . • " - ' • . - - / •
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90--57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-S2-2 .7440-66.-6
•
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration15900
3.0.: ) 7.6
89.70.610.34
1700-43.924.321.7
3610026.6
1670•• .* 895
0.1721.4366
* 1.7. 0.53IS!
-. 3.024.7213 :
0.77
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FORM I -IN ' ILM04.0
AR32I76I
U.S. EPA - CLP -'•-"•' X ' ' •. ' : • • • • • ' •
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM25Lab Name:. CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM ' Case No.: 24906 SAS No.: SDG No.: MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 8983S
Level (low/med): LOW , Date Received: 08/09/96
% Solids: • , -. 45.6 :':••';/ ; . . • • . ' .. • .
Concentration Unite (ug/L or mg/Kg dry weight): MG/KG ,
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-7'7440-43-97440-70-27440-47-37440-48-47440-50-87439-69-67439-92-17439-95-47439-96-S7439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6••
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganese,MercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
170003.95.9
1240.500..43
120031.010.412.2
2150019.5
21102160.2215.7947
* 2.20.87
104: " • ' • • • 3 . 9
21.684. o:0.94
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FORM I - IN - ILM04.0
AR32f762
U.S. EPA - CLP' • 1 , • .
EPA SAMPLE NOINORGANIC ANALYSIS DATA SHEET
MCSM19Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166
Lab Code: CHEM Case No.: 24906. SAS No.: SDG No.: MCSM03' ' , ' ' ' '
Matrix (soil/water) : SOIL Lab Sample ID: 37333
Level (low/med): LOW Date Received: 03/01/96
% Solids: . 70.0
Concentration Units (ug/L or mg/Kg dry weight); MG/KG
CAS No. .
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-rl7439-95-47439-96-57439-97-67440-02-07440-09-77732-49-27440-22-4744 0-23'- 57440-28-07440-S2-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury.NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration14600
2.52.5
55.90.70'0.46
2050036.519.326.2
4010023.1.
9920584
0.1314 . 9727
.* 1.46.57
1622.5
22.4106 '•:
0.64
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Comments: .
FORM I - IN UDM006 ILM04-°
AR32I763
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EPA SAMPLE NO..INORGANIC ANALYSIS DATA SHEET
MCSM17Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case Nb.,:_ 24906 SAS No.: SDG No. : MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 8966S
Level (low/med): LOW Date Received: 08/09/96
% Solids: ; • ' • • - . S4-.0: ,'/•/—..';"•,.:"• ' • ' . • • " ' • •
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-67439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimony :ArsenicBarium 'BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
• ' • • ; • " : - . .
Concentration
161003.33.3
1270.770.36
84830.814.512.0
2650019.6
2050537
0.1717.8
. 952• .1.8
0.731183.3
26.9' 69.2*
0.79
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POEMI-™ ,,01,005
U.S. EPA -' CLP: ' X • . . " ' • . " .
EPA SAMPLEINORGANIC ANALYSIS DATA SHEET
MCSM12Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-P5-0166
Lab Code^ CHEM Case No.: 24906 , SAS Noi : SDG No.: MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 87373
Level (low/med): LOW Date Received: 08/01/96
% Solids: 61.8
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS NO.
7429-90-57440-36-07440-38-2 ,7440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-37439-39-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron •LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration13000
2.92.9
36.30.320.39
120035.227.627.4
-. 4590017.3
16404900.1520.9537
• 1.60.63
1042,9
• . 13.197.6-0.66
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FORM I - IN IKM'004 ILM04.0
' i\R32l765
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EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM11Lab Name: CHEMTECH CONSULTING GROUP • Contract: 68-D5-0166
Lab Code: CHEM -Case No. : 24906 SAS No.: SDG No.: MCSM03
Matrix (soil/water): SOIL ' Lab Sample ID: 8735S
Level (low/med): LOW , Date Received: 08/01/96
% Solids: 63.0 ; '/.,
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-38'-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1-'.7439-95-47439-96-57439-97-67440-02 -0 .7440-09-77782-49-27440-22-47440-23 -S7440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalcium ;ChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
189002.82.881.20.720.48
286045.618.4
' 30.842600
33.513406650 . 1417.0
1030* ' • 1.6
0.63175
: 2.825.61360.67
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FORM I - IN ILM04.0
AR32I766
U.S. EPA - CLP' •• 1 ' . - . - ' • - ' ' ' . " • • "
: EPA SAMPLEINORGANIC ANALYSIS DATA SHEET
\JLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
MCSM03
Lab Code: CHEM Case No,: 24906 SAS No.: SDG No.: MCSM03
Matrix (soil/water) : SOIL ' Lab Sample ID: 373'6S
Level (low/med) : LOW Date Received: 08/01/96
* Solids: 49.3 - ,
Concentration-Units. (ug/L or mg/Kg dry weight): MG/KG
CAS No.
7429-90-57440-36-07440-33-27440-39-37440-41-7.7440-43-97440-70-27440-47-37440-48-47440-50-37439-89-67439-92-17439-95-47439-96-57439-97-57440-02-07440-09-77782-49-27440-22-47440-23-57440-23-07440-62-27440-66-6
• _ m
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration19500
3.46.7
1070.910.53
361077.523.320.7
4730042.7
1300999
0.1920.1
1140.1.90.76
1873.4
31.3154 •
0.90
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FORM I - IN tJl)'»002 ILM04
\R32I767
U.S. EPA - CLP: ' ' '•• 1 . •.. ' '' ' : ' , . ' ' •. •-
EPA SAMPLE NO.INORGANIC ANALYSIS DATA SHEET
MCSM34Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM . Case No. : 24906 SAS No. : SDG No.: MCSM03
Matrix (soil/water): SOIL Lab Sample ID: 8992S
Level (low/med): LOW Date Received: 08/09/96* • ' ! . " ' • ' • • . ' •
* Solids: 81.9 , ^
Concentration Units (ug/L or mg/Kg dry weight): MG/KG
CAS NO.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96--S7439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentrationi . • ' ••
167002.14.886.20.710.37
425039.214.826.5
3990029.7
16207580.1218.2
1080' 1.2
0.47124
': 2.125.5100 '0.54
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MCSM16.Lab Name: CHEMTECH. CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No&. : 24906 SAS No. : . SDG No. : MCSM16
Matrix, (soil/water): WATER • Lab Sample ID: 9008S
Level (low/med): LOW Date Received: 08/09/96
% Solids: 0 . 0 . ' , ' • '
Concentration Units (ug/L;or mg/Kg dry weight): UG/L
.o-
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIron <LeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium 'ThalliumVanadiumZincCyanide
Concent rat ion
2149.09.0
53.71.01.0
43501.01.51.0
8463.0
34402380.209.4
21405.02.0
21000009.01.0
28.0-9.0
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AR32 1770
APPENDIX B' ; . - ' •
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COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 '
Lab Code: CHEM Case No. : 24906 ~ SAS No. : SDG No. : MCSMOO
SOW No.: ILM04.0 , .
- EPA SAMPLE NO. Lab Sample ID. ,MCSMOO 8739SMCSM01 8747S'MCSM02 8742SMCSM04 8741S ,MCSM05 8750S • .MCSM06 ' 8746SMCSM07 8748SMCSM08 '8751SMCSM09 8740S ' ' ' " f?MCSM10 8749SMCSM13 8743SMCSM14 8752SMCSM15 8744S.MCSM18 874SSMCSM20 8753S .MCSM21 9005SMCSM24 9000SMCSM24D 9001S2MCSM24S 9002DSMCSM27 9003S
Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES
If yes-were raw data generated beforeapplication of background corrections? Yes/No NO
Comments; '* .
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee. a«--verified by the following signature.
Signature: \S=±J&P&F<K Name: PARVEEN HASAN, • • ' . — . t \ s T — : ———— ~ — ~ — ' . • ' . -Date: ______ tfff2/4t> _______ Title: QA/QC OFFICER
COVER PAGE - IN ILM04-°C\T\
AR32I782
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-01S6
Lab Code: CHEM - Case No..: 24906 SAS No. : SDG No.: MCSMOO• •
SOW No.: ILM04.0
EPA SAMPLE NO. Lab Sample ID.MCSM29 9004S 'MCSM35 900SS -
Were ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? • Yes/No YES
If yes-were raw data generated beforeapplication of background corrections? ' Yes/No NO
Comments: ' ', • , '
• • • •I certify that this data package ia in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as_verified by the following signature. ,
Signature: *4- &W* -~_____ Name: PARVEEN HASAN
Date: ^r&ft&_______ Title: QA/QC OFFICER ••' . • . - • * , ' • • " .
COVER PAGE - IN . . ILM04.0£02
AR,32I783.
In Reference to Case Ncfc):
REGIONAL/LABORATORY COMMUNICATION SYSTEMTelephone Record Log
Date of Call:
Laboratory Name:Lab Contact: '
Region:Regional Contact:" - -' ''••/Call Initiated By: * Laboratory ___ Region
In reference to data for the following sample numbers):
Summary of Queations/bsues Discussed:
;s
Summary of Resolution:
: g,.Signature •. ••;••• ~ ~[ ' ; Date
» ; - ' , " * • • . . ' • . " ,
Distribution: (1) Lab Copy, (2) Region Copy, 0) ^ Copy R QM n J c r 7 8 M
U.S. EPA - CLP
.'•••• '. : " 2B 'CRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO
AA CRDL Standard Source: INOR-VEN
ICP CRDL Standard Source: INOR-VEN '.
. Concentration'Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium,VanadiumZinc
.
CRDL Standard for AA
True Found %R• <
f~ " .
0.2
-•- -
' .
- '.*
o.oo"Oil 8".•
'•.:•-'"."..
•e-re-«tc>,oflj-V\5PuVi pk
•• ' \ "'' •:'. l
CRDL Standard for ICPInitial Final
True Found VR Found .^ VR
120:020.0
10.010.0
20.0100.050.0
6.0
30.0
80.0• .•"• .
10.020.0
20.0100.040.0
'.' .
\130.6019.02
11.4011.52
21.92116.9858.54
7.61
34.48
91.66,x '
14.1821.31
25.64113.. 8646.18
108 . 895.1
114.0115.2
109.6117.0<£17.jr
ff26.§y
CT4T
T14.|/
141.8106.6
(£2B .2113 .5IS JU
129.04V 17.70
9.9710.74
21.29108.3757.90
7.05
32.50
84.47
14.2223.29
15.07109. OS41.37
1
i07.5(gtTTS99.7107.4
106.4108.4Q."S".j£__j.i7r|7108.3
105.6
142.2116.4
<g5 . JL
109.0103.4
'
,
Sft wrtU, fr t«4« ' KcSMco-oi. oH-°"T \O}
• ' : , : : . ' "028 ' / - :FORM II (PART 2) - IN ILM04.0
flR32(785
UvS. EPA - CLP
" : ' • ' " • • . ' . •' ' v 2B • ' •, '( . . . CRDL STANDARD FOR AA AND ICP
' • " . ' " ." *\ " ' " ~ " . " • ' ~
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO
AA CRDL Standard Source: ' .
ICP CRDL Standard Source: INOR-VEN• ' • • ' • • •• • ' / ' . • • ' •' " •-
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmium -CalciumChromiumCobaltCopperIronLead ,MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard f or AA
True Found %R
-. '.
-•
• • '>
' . . ' ' •
1 • ' /•
'' .
"
- —— rrr"
CRDL Standard for ICPInitial Final
True Found %R Found . %R
1 120.020.0
10.010.0
20.0100. 050.0
6.0
; 30.0
eo:o.• •• •10.020.0
20.0100.040.0
.
128 . 0428.56
li.2211.18
• 22.18115.8360.48
6.32.33.94
91.74
9.2223.53
29.47113.5444.79
\
106.742. j««— ; — -^112.2111.8
'vSUl&15 .ITiii.65*v»_ — -**
105.3
( 13 . l]
fl4 .7*^ ^92.2117.6
J7 '."4"113.5112 .0
—\i/
, • : : i V : . 029 •'.- •-FORM II (PART 2) - IN ILM04.0
AR3J2I786
U.S. EPA- - CLP
' : ' 2BCRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 2490S SAS No. : SDG No. : MCSMOO
AA CRDL Standard Source: .
ICP CRDL Standard Source: INOR-VEN •I / • - • ' . " • .
Concentration Units: ug/L •
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found %R
/
1
•
CRDL Standard for ICPInitial Final
True Found %R Found %R(*+)
•' 120.020.0
10 . 010 . 0
20:0100.050.0
6.0
30.0
80.0
10.020.0
20.0100.040.0
.
. •
131.3322.93
11.93-11.52
22.09' 116.75, 62 . 73
7.84
34.49
93.97
11.4523 . 34
19 . 93115.9346.56
\
109.5114.9
119.3115.2
llOi^*?gyg30.7]
liiTo8117 . 5
114 . 5116.7
99.5115.9116.4
>b
FORM II (PART 2) - IN 030 ILM04.0
AR32I787
1 ,'••'. U.S. EPA - CLP
, ' . ' , . ' ' '.. ;';"; :' '3: ' ' " - . • ' ' ' ' ' •
I i . . BLANKS
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166- - ' . " • • ' . ' ' * • "
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSMOO
Preparation Blank Matrix (soil/Water): WATER
Preparation Blank Concentration Units (ug/L or mg/kg): UG/L
•
1 Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium .VanadiumZincCyanide
InitialCalib.Blank(ug/L) C
• -82.99-.09.01.01.01.0
-60.6-1.11.0-2.0-46.33.0
-81.01.00.23.0
-75.55 .0-2.3
-78.59.0-1.02.09.0
BUUUUUBBUBBUBUUUBUBBUBUU
•
Continuing Calibration*Blank (ug/L) ,
1 C 2 C 3 C
. -54.39.09.01.01.01.0
-37.61.01.0-1.6-53.53.0
-59.81.00.23.0
-70.85.02.0
-71.59.01.02.09.0
BUUUUUBUUBBUBUUUBUUBUUUu-
-55.49.09.01.01.01.0
-48.21.01.0-1.1
, -53.03.0
-68.1..00.23.0
-64.65.0
•' v 2.0-62.5; 9.01.0
• 2.09.0
/
BUUUUUBUUBBUBUUUBUUBUUUU
-53.09.09.01 . 01.01.0
-47.71.01.0-1.3-44.33.0
-71.61.00.23.0
-77.15.02.0
-63.2^9.01.02.09.0
1V \^
BUUUUUBUUBBUBUUUBUUBUUUU—
Prepa-rationBlank c
665.6309.0009.0001.0001.000l.OQO
£r39 .31031.0001.000Q..61D1
(-53 .-78p3J . 000
C*66.640i.ooo"0.2003.000
,6"79 . 44S5.0002.000
74 . 66(£— 9". Oocf1.0002.000
' 9.000
BUUUUUBUUBBUBUUUBUUBUUUU
M
PPPP 'PPPPPPPPPPCVPPPPPPPPCA
FORM III - IN ILM04.0
033AR32I788
U.S. EPA - CLP :. • . • ' • . ' . • i - >. . • • •• /. , -: . . / , • -S ' . . . . • .
. ' .. '•' BLANKS '. .-.: •" '~ " ' ' , " . " ' • • ' • " •
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSMOO
Preparation Blank Matrix (soil/water):/ . . . . . - • _ ' . . . . .
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBarium.BerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide.
InitialCalib.Blank(ug/L) C
•1 V .
• ' .^
• •
Continuing CalibrationBlank (ug/L)
4. _ C 2. C 3. r-»C(& >& >.V
-52.99.09.01.21.01 .0
-45.2<3l£TTtT
. -29^03,0
-75.61.00.23.0
-33.45.02.0
-63.59.01.02.09.0
V
.-. V
BUUBUUBBU>B3UBUUUBUUBUUUU—
13.09.09.01.01.01.0
25.01.01.01.027.03.0
<rgcL-y1.00.23.039.05.02.018.09.01.02.0
——— I ———— —— _
3UUUuu3Uuuuu3Uuuuuuuuuu
11.09.09.01.01.0,1.010.01.01.01.027.03.011.01.0
3.039.05.02.018.09.01.02.0
1•V' ^
UUUUUuuuuuuuuuuuuuuuuu
—
Prepa-ration
. Blank C•
.•
. ' - " •
i
•
.''
_
,
M
P~PPPPPPP-
MppppcvppppppppCA
•
•
FORM III - IN ' > . , ILM04.0
/1R32I789
U*S. EPA - CLP
•' '/'/''';- 5A '••.';' " • -: • ' . " rEPA SAMPLE NO.
SPIKE SAMPLE RECOVERY
_ MCSM24SLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSMOO/ ' • . ' • ; , . ' ' , ' ' "
Matrix (soil/water); WATER Level (low/med): LOW1 " • " , " ' • • • ' - ' ,-'• •
V Solids for Sample: 0.0 .
Concentration Units (ug/L or mg/kg dry weight): UG/L
. •
u
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimitVR
75-12575-12575-12575-12575-12575-125
75-12575-12575-12575-12575-125
75-12575-12575-125
- /
75-12575-125
75-12575-12575-12575-125
Spiked SampleResult (SSR) C
2124.7800501.180041.5700
1989.260049.200049.7400
200.5500503.4400237.70001239.710021.4000
529.06000.9360
500.6200
9.420044.1800
56.5800500.4600512.4400100.3000
: '
T..
•
1 •
SampleResult (SR) C
80.35009.00009.000010.19001.00001.0000
1.00001.00001.0000
153.00003.0000
•
26.40000.20003.0000
' • , • ' •' 5. 00002.0000
9.00001.00002.00009.0000
BUUBUU
UUU
u
uuuuuuuu
•
SpikeAdded (SA)
2000.00500.0040.00
2000.0050.0050.00
200.00500.00250.001000.0020.00
500.001.00
500.00
10.0050.00
50 . 00, 500.00500.00100.00
%R
102.2100.2103.999.098.499.5
100.3100.7
. 95 . 1108.7107.0
100.593.6100.1
94.288.4
113 .2100.1102.5100.3
Q""M
PPPPPPNRPPPPPNRPCVPNRPPNRPPPCA
Comments:
FORM V (Part 1) - IN ILM04.0
AR32 I 790
U.S. EPA - CLP
. . ..EPA SAMPLE W
DUPLICATES > • • \
MCSM24DLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSMOO
Matrix (soil/water) t WATER , ' Level (low/med) :* LOW
% Solids for Sample: 0.0 . % solids for Duplicate: 0.0
Concentration Units (ug/L or mg/kg dry weight): UG/L
I s.
Analyte
AluminumAntimony (ArsenicBariumBerylliumCadmiumCalciumChromium 'CobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit
,
5000.0
100.0
15.0
^ - • .
Sample (S) C
80.3500. 9.00009.000010.19001.00001.0000
12273.57001.00001.00001.0000
153.00003.0000
3476.060026.40000.20003.0000
2311.20005.00002.0000
2180.76009.00001.00002.00009.0000
3UU3UU
uuuu3
Uu3UU3UUUu
Duplicate (D) C
77.42009,00009.000010.23001.00001.0000
12353.90001.00001.00001.0000
." 152.14003.0000
3505.730026.54000.20003.0000
2330.80005.00002,0000
2194.67009.00001.00002.0000.9.0000
BUU3UU
UUU
u3
Uu3UuBUuuu
RPD
3.7
0.4
0.7
0.6
0.9o:s
0.3
j0.6
Q M
P-PPPPPPPPPPPPPCVPPPPPPPPCA
FORM'vi-- IN ; 040 ILM04-°
SR32I79I
U.S. EPA - CLP
. ; ' $ • y • .. . • . . - •, ' ' EPA SAMPLE NO.
ICP SERIAL DILUTIONS
MCSM24LLab Name: CHEMTECH CONSULTING GROUP, Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No;: SDG No.: MCSMOO
Matrix (soil/water):^WATER Level (low/med): LOW" ' - • • . ' ' ' . . ' • • • • • • . . ' ' - ; • , ' *
, Concentration Units: ug/L
\j
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver vSodiumThalliumVanadiumZinc
":••• - ' .'"•
Initial SampleResult (I) C
80.359.009.0010.191.001.00
12273.571.001.001.00
153.003.00
3476.0626.40
3.002311.20
5.002.00
2180.769.001.002.00
IUUBUU
UuU
uB
UBUUBUUU
SerialDilutionResult (S) C
79.5045.0045.0012 . 005.005.00
12463.60.: 5.00
5.005.00
135.0015.00
3532.7526.90
15.002141.5025.0010.00
2026.4045.00
. 5.0010.00
BUUBUUBUUUUUBB
UBUUBUUU
VDiffer-ence
1.1
17.8
1..5
100.0
1.61.9
7.3
7.1
Q M
PPPPPPPPPPPPPPNRPPPPPP-PP
, . . . .FORM IX - IN 043 ILM04-°
- - ' * ' , . . ' . ' * " •
/1R32I792
U.S. 'EPA' - CLP ' . - : • • •
' • . - - • . .-10 • . • • • - . • • • • 'INSTRUMENT DETECTION LIMITS (QUARTERLY) .
- . • • ; ->.' • . ' - • • • • • - : " • • . . ' • ' . ' • ' 'Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
- • * • , • . .
Lab Code: CHEM , Case No.: 24906 SAS No.: SDG No.: MCSMOO- • • • ' . ) • • • - • • •
ICP ID Number: Date: 07/15/96 .
Flame AA ID Number: CN- ' . . X .
Furnace AA ID Number: ' -
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Wave-length(nm)
578 . 00
Back-ground
.
.
.
•*
CRDL(ug/L)
200501020055
50001050251003
5000150.240
5000510
500010502010
IDL(ug/L)
1
• • •
9.0
M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRCA
Comments: • "CN: SP-E LAMBDA-1.(UV/VIS) SPECTROMETER
044FORM X - IN. ILM04.0
AR321793
\ U.S. EPA - CLP
;•••' ^ - .- • • '< : ' 10 -i • ••". •' .•"INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: CHEMTECH "CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM . Case No.: 24906 SAS No.: SDG No..: MCSMOO
ICP ID Number: PO ; Date: 07/15/96 •
Flame AA ID Number: ' ' '. ,
Furnace AA ID Number:
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Wave-length(nm)
306.20206.80189.00493.40313.00226 . 50317.90267.70228.60324.70271.40220.40279.00257.60
231.60766.50
, 196.00328.00588.90190.90292.40206 .20
'• " ... • ;' .'/-
Back-ground
.
..
V
. ' ' •
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
500010502010
IDL(ug/L)
11.09.09.01.01.01.010.01.01.01.027.03.011.01.0
3.039.05.02.018.09.01.02.0
M
PPPPPPPPPPPPPPNRPPPPPPPPNR
Comments: •PO: ICP 6lfe TRACE ANALYZER
FORM X - IN 046 , ILM04.0
AR32I791*
U.S. EPA - CLP
10 '•• . • -' • • ' ' ' 'INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: CHEMTECH "CONSULTING GROUP Contract: 58-D5-0166 - ^
Lab Code: CHEM Case No.: 24906 SAS No.; SDG No..: MCSMOO
ICP, ID Number: Date; 07/15/96
Flame AA ID Number: CV
?urnace AA ID Number:
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Wave-,length(nm)
.-
253.70
." • ,
Back-ground m
' '
- \ : - .
•*
' •
-
CRDL'(ug/D
200601020055
50001050251003
5000150.240
5000510
500010502010
IDL(ug/L)
0.2
M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNRNR
C o m m e n t s : ' • - . . 'CV: SPECTRO-PRODUCTS MERCURY ANALYZER
FORM X - IN ' ' ILM04.0045
AR32I795
: • ' '/ U.S. EPA - CLP • '' '"','' • " ' • • • - ' • • . • |
. • • ' . ; . . '-:•"•" 13. • ' f ' • • . - " ••PREPARATION LOG : , i
Lab Name: CHEMTECH-CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No, : 24906 SAS No.: SDG No. : MCSMOO
Method: CA ' -'•';• ; , ; ' • , •
EPASample No.
MCSMOOMCSM02MCSM04MCSM09MCSM13MCSM15MCSM18 ;MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29PBW
^
• S "
PreparationDate
08/09/9608/09/96
. 08/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/9608/09/96
. " . • • •
. • ' • , v •' . •
.'.:'.
' ' . ' • • . . •' :
.'
Weight(gram)
.
•
.• • .
--
Volume(mL>
5050505050505050505050505050
,• *
FORM XIII - IN ,. ILM04.0053
AR32I796:
.••.-.'. • . ' ';•- ' u-s. EPA,'- CLP ;.'•. i • - . ' ' - '
' ' ' - . • . 13 . , ,PREPARATION LOG
Lab Name: CHEMTECH'CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSMOO
Method: CV . '
EPASample No.
MCSMOO '..MCSM01MCSM02MCSM04MCSM05MCSM06MCSM07MCSM03MCSM09MCSM10MCSM13MCSM14MCSM15' MCSM18MCSM20MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM35PBW
-
. .
PreparationDate08/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9608/14/9608/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/9608/14/96
• - *•
' •
. Weight(gram)
• '
- ''
• '
.
Volume(mL)
100100100100100100100100100100100100100100100100100100100100100100100
T'
FORM XI11 - IN ' ' "54 ILMQ4.0
AR32I797
U.S.' EPA - CLP .
' • -'• ' . " ' . ' . ' " • - ^ '13 : . :j- •' - ' . ' . ' • " • • •
• - PREPARATION LOG•* • ' ' '- ^ ' ' • { : • ' ' ' ' • ' ' ' .
ab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : ' SDG No. : MCSMOO
Method: P .
u
EPASample No .
LCSWMCSMOOMCSM01MCSM02MCSM04MCSM05MCSM06MCSM07MCSM08MCSM09MCSM10MCSM13MCSM14MCSM1SMCSM18MCSM20MCSM21MCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM35PBW
. PreparationDate08/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/96OB/16/9608/16/9608/16/96OB/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/9608/16/96
- ' - • !
:-.',."•
Weight(gram)
•
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. - . :
•
Volume(mL)
100100100100100100100100100100100100100100100100100100100100100100100100
*.
-055FORM XIII - IN ILM04.0
AR32I798
U.S. EPA - CLP
- • ' - ' '.' . ' "'' " "- 14' •• ' " • • , ' "ANALYSIS RUN LOG , ' .
Lab. Name: CHEMTECH "CONSULTING GROUP Contract: 63-D5-0166 .
Lab Code: CHEM Case No.: 24906 SAS No. : . SDG No. : MCSMOO* • - • "
Instrument ID Number: PO Method: P . >
Start date: 09/01/96 . End date: 09/01/96 ,
EPASampleNo.
SOSSSSICVICVICVICVICBCRI-\ICSAICSABccvCCB:— IPBWZZZZZZLCSWZZZZZZMCSMOOMCSM09MCSM04MCSM02MCSM13MCSM15CCVCCB— 2-^MCSM18MCSM06MCSM01MCSM07MCSM10
D/F
1.001.001.001.001.001.001.001.00liOO1.001.001.001.001.001.001.001.00
,•• i.oo1.001.001.001.001.001.001.001.001.00
» 1.001.001.001.001.00
Time
09030919092109230926092709340940094409430954100310061009101210161022102510301035103910431046104910531056105911031106110911131116
J
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FORM XIV - IN V ILM04/
' 060
ft R 3-21.7 9 9
IT
U.S. EPA - CLP , .
. ' '.X--' 14 : |fANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: "\ SDG No.;. MCSMOO
Instrument ID Number: PO- Method: P .
Start date: 09/01/96 v End date: 09/01/96
EPASampleNo.
MCSM05CRI— 7-ICSAICSABCCVCCB -3MCSM27MCSM29MCSM21MCSM35ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB-M-ZZZZZZZZZZZZMCSM14MCSM20CRI— 3ICSAICSABCCVCCB— fMCSM24MCSM24DMCSM24SMCSM24LZZZZZZ
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001 .001.001.001.001.001.001.001.001.001.001.001.001.001 . 001.00.1.0.0-1 . 005.001.00
Time
11191124112711301133113611391144114711511211121512181223122812351238124112441253131713231327133513401343134613501353135914031415
* K
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<1
u FORM KIV - IN - ILM04.0
OG1
. ..:HR32I800-."
. U . S . EPA - CLP
. ' .' • ' ' 14 . ' • . ' . '• ' • , . . '. • '. ".ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSMOO
Instrument ID Number: PO Method: P
Start date: 09/01/96 . End date: 09/01/96
EPASampleNo.
ZZZZZZZZZZZZZZZZZZMCSM08ZZZZZZCCVCCB— feZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCRI— U'ICSAICSABccv-CCB-''ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB -? •ZZZZZZ
D/F
1.001.005.001.001.001.001.001.001.001.005.001.001.001.001.00
. 1.001.001.001.001.001.001.005.001.001.001.005.001.00
10.00- 1.001.001.00
Time
14181421142314321439144214451452145514591504151015141517152115321544154715501602160516031614162216251630163616451657170017031709
% ft
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FORM XIV - IN . I-LM04
062
AR32I80I
U.S. EPA - CLP
• . . . • ' ' ' • - ' " ' ; • • • - ' ' • ' ' ' • • ' • ' 1 4 - 'il' ' • ' 'ANALYSIS RUN LOG ?
Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No.: MCSMOO/ . - • - - • .
- ' ' ' • • , ' ' • • . ' , ! ' . .
Instrument ID Number:- CN Method: CA
Start date: 08/09/96 • End date: 08/09/96
EPASampleNo.
SOS10.0S100.0S500.0S1000.0ICVICBCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZ -ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZMCSMOOPBWMCSM09MCSM04MCSM02MCSM13MCSM15MCSM18CCV
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00•1.001.001.001.001 . 001.001.001.001.00.1.001.001.00
Time
20002002200420062008201020122014201620182020202220242026202820302032203420362038204020422044204620482050205220542056205821002102
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FORM XIV - IN • . ILM04.0
05H
AR32I802"
U.S. EPA - CLP
' • • • ' ' " ' . " . • • '' ' ' ' ' . 14- .'••'• • '• 'ANALYSIS RUN LOG '• - . , - • • • • • . - . - • , • •
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSMOO
Instrument ID Number: CN Method: CA1 • • ,' •
Start date: 03/09/96 End date: 03/09/96
EPASampleNo.
CCBMCSM24MCSM24DMCSM24SMCSM27MCSM29MCSM21CCVCCB
. .
D/F
1.001.001.0.01.001.001.001.001.001.00
.
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Time
210421062103211021122114211621132120
% R ALS3AS
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FORM XIV » IN ' '* ILM04
, OS?
'rtR'321803
'•', r . • . u,s. EPA - CLP.' '• -. ,'..; • ' .• • ' '':":•>• -r": •' •'•./'.-..; 14 . . .•.'.'j . : -• , ". .
ANALYSIS RUN LOG
Lab Name; CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: ' SDG No.: MCSMOO
Instrument ID Number: CV Method: CV
Start date: 08/14/96 End date: 08/14/96
EPASampleNo.
SOSO. 2SO. 5Sl.OS5.0S10.0ICVICBCCVCCBCRAPBWMCSMOOMCSM09MCSM04MCSM02MCSM13MCSM15MCSM18MCSM06CCVCCBMCSM01MCSM07MCSM10MCSM05MCSM08MCSM14MCSM20MCSM24MCSM24DMCSM24S
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001 . 0.01.001.00•1.001.001.001.00•1.001.001.00i
Time
15071509151115131515151715191521152315251527152915311533153515371539154115431545154715491551155315551557155916011603160516071609
% R
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FORM XIV - IN « ILM04.0
058
AR32f80l*
U.S. EPA - CLP .
. . •' . • 14ANALYSIS ;RDN LOG • .
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No.': MCSMOO
Instrument ID Number: CV Method: CV
Start date: 08/14/96 End date: 03/14/96
EPASampleNo.
CCVCCBMCSM27MCSM29MCSM21MCSM35ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.00
,1.00i.oo1.001.001.001.001.001.00
f
.
Time
161116131615161716191621162316251627162916311633163516371639164116431645164716491651
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Analytes •:
ALS3AS
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FORM-XIV - IN . , • ILM04
059
AR32I805
MERCURYX .. ColdVaporAAicremiECH^ ™ ^ — — . — - _ — _^ ****** mm, «ktf*6S3UP. WC.
b: o.
Std. Name .
•
mLused
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Std. Ret £ From Logbook
- , . •' :'•''
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Chemical Used j Lotfc
£,C/, 1 <fc3*r-Na.a.-Hit*y*il r fleJfct .
v 1• . • • • • 1 . v ,
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ot Hj100 eL 1000 oL
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r*Corre!anon Coefficient yHOi.
Rev.12/95 AR32I806''t
Page f efJL-
P ^_ -L——v— ;.... —-F=--1i : j -
.... .—••• •- ;.:. : :i.~-~ '-—T:._..., ..... -j .. :.. .....:_.......—„,.....——.————rj——— ~.i • —— rTTTtti——*S. . ......' ;•::-.. ...;: • :• Ij.;!..-..
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•1R32I807
8DO MCSM03
U.S. EPA - CLP' . ' " / • _ ' ' -
• • •' •*
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE| ,
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: .SDG No.: MCSM03
SOW NO.: ILM04.0
EPA SAMPLE NO. Lab Sample ID.MCSM03 8736SMCSM11 8735S .MCSMl'2 8737S xMCSM17 8986S .MCSM19 8738SMCSM25 ' 8983SMCSM25D - 8984S2MCSM25S 8985DSMCSM26 8993S -MCSM28 8987SMCSM30. 8988S ,MCSM31 ,•: 8989SMCSM32 8990S •MCSM33 ' 8991SMCSM34 8992S
UWere ICP interelement corrections applied? Yes/No YESWere ICP background corrections applied? Yes/No YES
If yes-were raw data generated beforeapplication of background corrections? Yes/No NO
Comments: '"The "E" qualifier on Form I and IX for the Potassium indicates
a chemical or a physical interference, which was suspected during thePotassium analysis only. •. -
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee*—ae yerified by the following signature.
Signature: ' ~t*S;r . Name: PARVEEN HASAN
Date: ______<H*2>foc, Title: QA/QC OFFICER
COVER PAGE - IN -- * ILM04.0
AR32I809
U.S. EPA * CLP'
• • 23CRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: • SDG No.: MCSM039 ' . ' •
AA CRDL Standard Source: INOR-VEN
ICP CRDL Standard Source: INOR-VEN
Concentration Units: ug/L •
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper'IronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilver .SodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found *R
0.2 0.22 110.0
CRDL Standard for ICPInitial Final
True Found , %R Found J^R
120.020.0
10.010.0
20.0100.050.0
6.0
30.0
30.0*
10.020.0
20.0100.040.0
131.44,20.73
10.3511.10
21.32103.0351.99
6.40
32.12
86.72
11.7222.23
25.97105 . 2044.30
109.5103.6
103.5
106.6103.1104 . 0
106.7
107.1
108.4
111.4
129.3106.2110.3
123.4024.59
10.3410.63
19.95100.3043.33
4.90
30.23
31.44
13.50C20.52
23.9699.4243.30
1
102.3£237$103.4106.3
100W97.3
31.7
lOO. 9
101.8
3:35. 3103.1
119.899.4103.2
/ 1
FORM II (PART 2) - IN UO'tOlS ILM04.0
AR32I8IQ "'.
, U.S. EPA - CLP'
• • ' • ' - ' • ' ' ' - • ' • . • ' ' • • • . • " ' V ' . ' 2 B ' . . • • .I j : CRDL STANDARD FOR AA AND ICP
' " ' < - ' •
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No. : SDG No. : MCSM03
AA CRDL Standard Source: • , .
ICP CRDL Standard Source: INOR-VEN
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA• • . • • . :. . i
True Found AR
-
*
%
^
. •• ./ . ;. •
CRDL Standard for ICPInitial Final
True Found %R Found >$£•'• ' - ' . ' ^ y120.020.0
/'•.'•10.010.0
20.0100.050.0
•6.0
30.0
80.0*
:10.020 . 0
.- .20.0
100.040.0
' v
.
*
-
129.0423.56
11.0011.19
19.94102.4449.32
7.47•31.14
62.92
10.0020.23
' ,21 . 07101.6647.06
107.5tfi7~a— —110.0111.9
99.7102.498.6
124.5
103.8
103.6
100.0101.2
105.4101.7117.6
4y
FORM II (PART 2) - IN 'V |,tj| |A<f« ILM04.0
; A R 3 2 I 8 I I
'. . • • ; •••••' ' t U.S. EPA.- CLP. .'. • . • - ' . .
.••'.' '' . 23 ' -. • . _•CRDL STANDARD FOR AA AND ICP
•-• •-• ' ;. • •••- ' •• • ' • ' ^ . - •: ' ...." • . - . \JLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 249.06 SAS No.: SDG No.: MCSM03
AA CRDL Standard Source:
ICP CRDL Standard Source: INOR-VENv . •, . ' '. . ' • •
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found %R
'•
•
x
CRDL Standard, for ICPInitial Final
True Found %R Found . _%Rtfft
120.020*. 0
10.010.0
20.0100.050.0
6.0
30.0
30.0**,
10 . 020.0
. • r
20.0100.040.0
'
125.4321.52
9.3410.82
19.30102.3650.46
7.22
30.79
32.21
111 1520 . 19
19.72101.4742.44
104.5107.6
93.4108.2
99102x 4100.9
120.3
102.5
102.3
111.5101.0
98.6101.5106.1
FORM II (PART 2) - IN
AR32I8I2
UiS. EPA - CLP: • - . . - ' • • ' ' ' ( • ' '• • - ' . . - . . . ' • • • ; • , ' • ' • . • ? 3 • ' ' . - . - • ; ;
' . . -. ' : '. •••'.; ;.:';'BLANKS' ••'" •' '• ••' • : •-', .: '.. '..-Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
. . " • - ' - . : " ' > - • ' ' • •
Lab Code: CHEM Case No.;:. 24906 SAS No.: SDG No.: MCSM03
Preparation Blank Matrix (soil/water): SOIL
Preparation Blank Concentration Units (ug/L or mg/kg): MG/KG
t
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium ,ThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
11 . 09.09.01.01.01.010. 01.01.01.0
27.03.0
ll.O1.00.23.0
39.05.02.0
18.09.01.02.09.0
UUUUUUUUUUUUUUUUUUUUuuuu
Continuing CalibrationBlank (ug/L)
1 , C 2 C 3 C
11.09.09.01.01.01.010.0
- 1.01.01.0
27.03.011 . 01.00.23.0
39.05.02.0
18.09.01.02.09.0
UUUUUUUUDU0uuuuuuuu.uuuuu
11.09.09.01.01.01.0
10.01.01.01.0
27.03.0
11.01.00.23.0
39.05,0
' ? •• 2.018.09.0
:•' 1.02.09.0
1
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11.09.09.01.01.01.010 . 01.01.01.0
27.03.0
11.01.00.23.0
39.05.02.0
18.09.01.02.09.0
UUUUUUUUUUUUUUUUUUUUuuuu
Prepa-rationBlank C
-2.7621.8001.8000.2000.2000.2002.0000.2000.2000.2005.4000.600-2.3860.2000.1000.6007.8001.0000.4003.6001.8000.2000.4000.450
BUUUuuuuuuuuBUuuuuuuuuuu
MppppppppppppppCVppppppppCA
( £f $*~-$*. e fe J'.McSMO-S IMi.
FORM III - IN ILM04.0
: AR32I8I3
O.S. EPA - CLP
' -'. • "; - ' ' . . • -'3 •'. • ' . ' ' - '
• ' • • ' . : . • ' . . • ' BLANKS .. . • - - • ' • . „ . • . • • • • • • • • - . . ' ' - - • ' 'Lab Name: CHEMTECH CONSULTING GROUP Contract:.68-05-0166
Lab Code: CHEM . Case, No. : -24906 SAS No.: SDG No.: MCSM03
Preparation Blank Matrix (soil/water):• ' • . ' ' '
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLead ;.MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Initial .Calib.Blank(ug/L) C
•. • • • ' • _
' *
_
. • • • • .- • ' •' i • .Continuing Calibration
Blank (ug/L)M^_ . ' ''tt , . ^ 'V '*m+L f** ^ > *N ^ j* jW J . C *\ V*
11.09.09.01.01.01.045.31.0vl.O
1.034.33;0
11.01.00.23.0
39.05.04.413.09.01.02.09.0
UUUUUUBUUU3Uu0UUUU30Uu00_
12.59.09.01.01.01.010.01.01.01.0
27. Of3.011.01.00.23.0
39.0S.O
•; 2.0•' 13.0
9.0, : 1.0
2.09;0
300000000000000000300000_
11.09.09.01*01.01.0
-10.61.01.01.727.03.0
-13.51.00.23.0
39.05.02.0
13.09.01.02.0
/1 "
00000030B30030000000000
-mm
. -
Prepa.-r at ionBlank C
-
.
^
M
PPP .PPPPP••• .
V
>*pppCVPPPPPPPPCA
. . . .FORM III - IN ''U'1022 ILM04.0
AR32I8U
0.S. EPA - CLP
' : ; . ' ' • 9 ' • : ; : . - • ' ' •SAMPLE NO.ICP SERIAL DIL0TIONS
MCSM25LLab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No.: MCSM03
Matrix (soil/water): SOIL Level (low/med): LOW
Concentration Units: ug/L
• ' 'Analyte
AluminumAntimonyArsenic.BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Initial SampleResult (I) C• 39122.06
9.0013.69285.58• 1.161.00
2755.6071.4723.6427,98
49592.60' 44.84
. 4853.26497.69
36.172181.28
5.002.00
239,239.0649.64±93.40
U
BUB
B
B
B800B0B
SerialDilutionResult (S) C
38731.7045.0045.00295.805.005.00
2729.0072.9527.5030.45
51191.2049.70
4946. OS518.75
37.501805.8025.0010.00167.4545.0052.60207.80
00B00B
BB
B
BB0UBUB
%Differ-ence
1.0
100.03.6
100.0
1.02.115.48.83.210.81.94.2
3.717.2
30.0
6.07.4
, .
Q**
,
E
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PPPPPPPPPPPPPPNRPPPPPPPP
FORM IX - IN 'w.-wfcu ILM04.0
-•'i'R 3 2-1-815
U.S. EPA - CLP
' - ..-'..'...- 13 • • . '• ' ' . • '.•—- .PREPARATION LOG j
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68TD5-0166
Lab Code:-CHEM Case No. : 24906 SAS No. : . SDG No. : MCSM03• ' ' ' .' ' - ; '
Method: CA , . ' ' .
EPASample No.
LCSSMCSM03MCSM11MCSM12MCSM17MCSM19MCSM25MCSM25D ,MCSM25SMCSM25MCSM23MCSM30MCSM31MCSM32MCSM33MCSM34PBS '
PreparationDate
08/12/9603/12/96OB/12/9608/12/9603/12/9603/12/9608/12/9608/12/9608/12/9608/12/9608/12/9608/12/9603/12/9608/12/9608/12/9608/12/9608/12/96
'
ii
-
Weight(gram)
1.001.001.061.101.061.011.051.051.051.001.08
; - 1.031.021.041.021.011.00
. '/ , •
' *
Volume(raL)
5050505050505050505050505050505050
*
--
FORM XIII - IN. UU''039 ILM04.0
AR32I8I6
; U.S. EPA - CLP' • '
- ' ' • ".••••.•••'•'•'•„•.r 13 ! v . . '• . •• ' .PREPARATION LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab.Code: CHEM Case No:: 24906 SAS No.: SDG No.:.MCSM03
Method: CV ••; ;
EPASample No.
LCSSMCSM03MCSM11MCSM12 -MCSM17MCSM19MCSM25MCSM25DMCSM25SMCSM26 •MCSM28MCSM30MCSM31MCSM32MCSM33MCSM34PBS
PreparationDate
08/19/9608/19/9608/19/9608/19/9608/19/9608/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96OB/19/96
V ' • t-
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' > > . ' -
. Weight' (gram)
0.200.210.220.210.220.220.200.200.200.200.200.220.210.200.200.200.20
1 • ' . -
- . • ,
Volume(mL)
100100100100100100100100100100100100100100100100100
UUH040FORM XII1 - IN ILM04.0
AR32I8I7
U.S. EPA - CLP
. 13 .PREPARATION LOG
' • ."•• • ' , ' • . . • > > ' : • • • • ' • ' • • 'Lab Name: CHEMTECH CONSULTING GROUP •' Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: . SDG No.: MCSM03
Method: ? . . ' • . . : - ' ' -
EPA"Sample No.
LCSSMCSM03MCSM11MCSM12MCSM17MCSM19MCSM25MCSM25DMCSM25SMCSM26MCSM23MCSM30MCSM31MCSM32MCSM33MCSM34P3S
•'. • ' . . .
PreparationDate
08/14/9603/14/9608/14/9608/14/9603/14/9608/14/9608/14/9608/14/9603/14/9608/14/9603/14/9603/14/9608/14/9608/14/9603/14/9603/14/9603/14/96
.
i
Weight(gram)
1.001.051.011.021.021.011.01
• '1--031.041.021.021.021.021:041.041.051.00
•
Volume(mL)
200200200200200200200200200200200200200
' 200• 200200200
FORM XII! - IN , | !U,04.0
/1R32I8I8
U.S. EPA - CLP
' • ••[•••* ' ' • ' 1 4 ' • ; • ' • • ' ' ' . - . ' • •ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSM03
Instrument ID Number: PO . Method: P
Start date: 08/20/96 . End date: 08/20/96
EPASampleNo.
SOSS ,ssICVICVICVICVICBCRI— \ICSAICSABCCVCCB-\PBSZZZZZZLCSSZZZZZZMCSM11MCSM03MCSM12MCSM19MCSM17MCSM28CCVCCB -'Z.MCSM30MCSM31MCSM32MCSM33MCSM34
•
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
09560959100110031005100710101022102610311035104110481051105410581101110611121116111911231126113011371140114311471151115511561201
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FORM XIV - IN ' • ILM04.0
iiOM'046• ' " • • . . * ' > t
AR32I8I9
U.S. EPA - CLP
• , ' • • ' . 1 4 . • ' •. ' • ANALYSIS RUN LOG
Lab Name: CHEMTECH" CONSULTING GRO0P Contract: 68-D5-0166
Lab Code: CHEM . Case No.: 24906 SAS No.: SDG No. : MCSM03
Instrument ID Number: PO, . Method: P
Start date: 08/20/96 End date: 03/20/96
EPASampleNo.
MCSM26ZZZZZZCRI— T-ICSAICSA3CCVCCB— 3MCSM25MCSM25DMCSM25SMCSM25LZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— 4-ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCRI— 3ICSA .•ICSABCCVCCB-*5ZZZZZZZZZZZZ
D/F
1.001.001.001.001.001.001.001.001.001.005.001.001.001*005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
12051210121712231236123912421253130213121316132013251331134113451353135613591404140714111417142314271430144514521455145815041507
% R AL
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FORM XIV - IN „ ILMOT
;[R32I820
U.S. EPA - CLP
' • • • ' • . . ,•:. -;. - ;—":''''. ' : '14' ' ;:-:5i;- \: -,. • •• ... , • /. . ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 ,
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSM03
Instrument -ID'Number: PO Method: P x
Start date: 08/20/96 End date: 08/20/96
o
EPASampleNo.
ZZZZZZZZZZZZZZZZZZZZZZZZCRI— H-ICSAICSABCCVCCB-fe
.
f 1
D/F
1.005.001.001.001.001.001.001.001.00
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152115241527153115441553160416071610
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FORM XIV - IN - ILM04.0
AR32I82I
U.S. EPA - CLP
• • " • - - • ; 14 * • ": - .!ANALYSIS RUN LOG
' -.•' ' - - - ••• .-:' - . •: . - •' "• -:.Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03
Instrument ID Number: CN .< Method: CA
Start date: 08/12/96 End date: 08/12/96 ,
EPA •SampleNo.
SOS10.0S100.0S500.0S1000.0ICVICBCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCV
D/F
1.001.001.001.001.001.001.001.0011.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
• 1.001.001.001.00
Time
21002102210421062103211021122114211621132120212221242126212321302132213421362133214021422144214621482150215221542156215322002202
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FORM XIV - IN * - ILM04
UUM042.AR32I822
:•• . • U.S. EPA - CLP ;
' •"' ' ' ' ' ,=;-;\ 14 ' -' ."- •- ' --, .. ::ANALYSIS RUN LOG
b Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
,ab Code: CHEM . Case No.: 24906 SAS No. :> SDG No.: MCSM03
Instrument ID Number: CN , . Method: CA
jtart date: 08/12/96 End date: 08/12/96
i EPA; Sample: NO.
CCBZZZZZZZZZZZZZZZZZZ .PBSLCSS'MCSMllMCSM03MCSM12MCSM19MCSM25CCVCCBMCSM25DMCSM25SMCSM17MCSM28MCSM30MCSM31MCSM32MCSM33MCSM34MCSM26CCVCCB
•
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
1 i
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22042206220822,10221222142216221822202222222422262228223022322234223622382240224222442246224822502252
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FORM XIV - IN - ILM04.0
00*1043
AR32I823
1 . U.S.; EPA - CLP
• • • ' • • ' • • . . - ' 1 4 - ' • • • ' . -ANALYSIS RUN LOG . ">
Lab Name: CHEMTECH CONSULTING GROUP , Contract: 68-D5-0166
Lab Code: CHEM Case* No.: 24906 SAS No.: SDG No. : MCSM03
Instrument ID Number: CV Method: CV
Start date: 08/19/96 , End date: OB/19/96
EPASampleNo .
SOSO. 2SO. 5Sl.'OS5.0S10.0ICVICBCCVCCBCRAP3SLCSS ,MCSM11MCSM03MCSM12MCSM19MCSM25MCSM25DMCSM25SCCVccaMCSM17MCSM23MCSM3 0MCSM31MCSM32MCSM33MCSM34MCSM26ZZZZZZZZZZZZ
• ' • ' •D/F
1.001.001.001.001.001.001.001.001.001.001.001.0010VOO1.001.001.001.001.001.001.001.001.001.001.001.001 . 00.1.001.001%001.001.0010.00
Time
175717591301130313051807180913111313131518171319182113231325132713291331133313351837133913411343184518471349IS?!1353135513571359
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FORM XIV - IN * ,. . ' . ' - . . - ' • : • • - ' - ; • - . . . ' •
W)M044
/JR32I821*
U.S. EPA -'CLP
' - . ' • ' ' • ' . • : - • •' .".'14' •'ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No. : SDG No. : MCSM03
Instrument ID Number: CV Method: CV. ;,
Start date: 08/19/96 End date: 08/19/96
f
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EPASampleNo.
CCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ2ZZZZZ{ZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZCCVCCB
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1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
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Time
19011903190519071909191119131915191719191921192319251927192919,3119331935193"7193919411943194519471949195119531955195719592001
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FORM XIV - IN „ ILM04.0
nO'1045
AR32I825
SDO MCSM16
/5R32I826
o.1 U.S. EPA - CLP
COVER PAGE - /INORGANIC ANALYSES DATA PACKAGE •
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166\ " , ' • ' : • '
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No. : MCSM16
SOW No.: ILM04.0 _ ,'•
EPA SAMPLE NO. Lab Sample ID.•MCSM16 9008SMCSM16D 9009S2MCSM16S 9010DS
Were ICP interelement corrections applied? ' Yes/No YESWere ICP background corrections applied? Yes/No YES
If yes-were raw data generated beforeapplication of background corrections? Yes/No NO
Comments: ' • ."E" qualifiers on Form I and IX for the Barium and the Potassium
indicate a chemical or a physical interferences, which were suspectedduring the Barium and the Potassium analysis only.
I certify that this data package is in compliance with the terms andconditions of the contract, both .technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or the -Manager's desigriee --ets verified by the following signature.
Signature: (tm/J T ^ .Name: PARVEEN HASAN
Date:. _____0?f/$/f£ ,Title: QA/QC OFFICER
COVER PAGE - IN - - ILM04.0001
AR32I827
U.S. EPA - CLP
' 2 3 - . . - • " .CRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING. GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 . SAS No.: SDG No. : MCSM16
AA CRDL Standard Source: INOR-VEN
ICP CRDL Standard Source: INOR-VEN
Concentration Units: ug/L
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found %R
.
0.2 0.21•
105.0
: CRDL Standard for ICPInitial Final
True Found %R Found %RO ro120.020.0
'10 . 0. . 10.0
20.0100.050.0
6 . 0
30.0
80.0
10,020.0
20.0100.040.0
130.6019.02
11.4011.52
,
21.92116.93
. 53.54
7.61
34.43
91.66
14.1321.31
25.64113.8645.13
108.395.1
114.0115.2
,'109.6117.0117.1
126 .3
114 . 9
114 . 6
141.3106.6
128.2113.9115.4
129.0417.70
9.9710.74
§
21.29108.3757.90
7.05
32.50
84.47
14.2223.29
15.07109.0541.37
107.5-.83 . S
99.7107-"
, ,10o -/108.4115.3
117.5
103.3* •
105 . 6
142.2116.4
75.4109.0103.4
FORM II (PART 2) - IN 008 ILM04.0
AR32I828
U.S. EPA - CLP
, . . • . • • • . : - . • . - . .V J • ' . ' ; • CRDL 'STANDARD FOR AA AND ICP
Lab Name: CHEMTECH .CONSULTING GROUP Contract: 68-D5-0166
Lab Code': CHEM Case No. : 24906 SAS No.: SDG No..: MCSM16
,AA CRDL Standard Source: ;
ICP CRDL Standard Source: INOR-VEN
• • " Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA- • ,-"" '
True Found %R
,
. ' .
• ".
~~~ • '
'
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•'. --.
^ ,' '
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CRDL Standard for ICP .Initial Final
True Found VR Found iR
120.020.0
10.010.0
20.0100 . 050.0
- 6.0
30.0
80.0
10.020.0
20 . 0100.040.0
. •• .
. '
- 128.0428.56
. 11.2211 . 18
22.18115.8360.46
. %6.32
33.94
91.74
9.2223.53
29.47113.5444.79
^mmmmm ,
106.7142.8
112.2111.8
110.9115.8121.0 *105 . 3
113.1
114.7.
92.2117,6
147.4113.5112.0
. .FORM II (PART 2) - IN . 009 ILM04.0
AR32I829
U.S,' EPA - CLP
23' x . CRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM . Case No. : 24906 SAS No. : SDG No. : MCSM16
AA CRDL Standard Source: .
ICP CRDL Standard Source: INOR-VEN
Concentration Units: ug/L
.Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found %R" . ' ' !
_ . •
CRDL Standard for ICPInitial ;. Final
True Found %R Found, s-S*-
120 . 020.0
10.010.0
20.0100.050.0
6.0
30.0
30.0
10.020,0
20.0100.040.0
•
.
.• -
131.33• 22.98
,11.9311 . 52
22.03116.7562.73
7.84
34.49
93.97^
11.4523.34
19.93115.9346.56
109.5114.9
119.3115 -1
llVjGTSTj)125.5
130.7^
115.0•(£i7TT114.5116.7
99.6115.9€23
- 010FORM II (PART 2) - IN ' ILM04.0
AR32I830
U.S. EPA - CLP
, .' • • ' . , .. 2B • . •• •• -.CRDL STANDARD FOR AA AND ICP
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. :y 24906 SAS No.: SDG No. : MCSM16
AA CRDL Standard Source: ! ,
ICP CRDL Standard Source: INOR-VEN
Concentration Units: ug/L ' .
1
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperironLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL Standard for AA
True Found %R
,
,
- " .
•"• :
'.' i
. x' v :'.. .
• .'. . ' • - ' • _ . . '
1 '",-'• •
CRDL Standard for ICPInitial Final
True Found VR Found %R
120.020.0
10.010.0
20.0100.050.0
6.0
30.0
80.0
10.020.0
•. . .
20.0100.040.0
,- "
.,V
- • ;
•
'
128.2820.58
,
11.9310.78
22.38111.93'59.69
9.60
33.45
89.76*
10.8024.00
- .27.10112.7157.40
4 ———————
MS m
106.9102.9
119.3107.8
111 .9JL11.9;119.4.160.0
111.5••12 ."J?—
108.0120.0
135.5112 . 7ss
M cSf\ i1
FORM II (PART 2) - IN . ' Oil ILM04.0
AR32I83I
U^S. EPA - CLP
' ' .. < '•••'. . ' BLANKS. . -.-. _ ' - . ;
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63 -D5- 0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSM16
Preparation Blank Matrix (soil/water) : WATER
Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium .ThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
-82.99.09.01 . 01.01.0
-60.6-1.11.0-2.0
-46.33.0
' -31.01.00.23.0
-75.55.0-2.350.49.0-1.02.09.0
BUUUuu3BU33U3UU0B0BB0300
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
-54.39.09.01.01.01.0
-37.61.01.0-1.6
-53.53.0
-59.31.00.23.0
-70.85.02.0
46.09.01.02.09.0
BUUUuuBUuBBUBUUU3Uuuuuuu
-55.49.09.01.01.01.0
-48.21.01.0
-1.1-53.03.0
-63.11.00.23.0
-64.6. 5.0
2.046.09.01.02.09.0
30UUUUBUU33UBUUU•3Uuuuuuu
-53.09.0
. 9.01.01.0
, 1.0-47.71.01.0-1.3
-44.33.0
-71.81.00.23.0
-77.15.02.0
46.09 . 01.02.0
3U00003.0033030UU3UUuuuu
Prepa-rationBlank c
11.0009.0009.0001.010
. 1.0001.00014.6201.0001.0001.00027.0003.00011.0001.0000.2003.00039.0005.0002.00046.0009.0001,0002.0009.000
UUUB00300000000000000000
M
PPPPPP ,
i ;
* PPPPPCVPPPPPPPP'CA
Al 9FORM III - IN VA'-ILM04.0
AR32I832
U.S. EPA - CLP
- ', BLANKS
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 •
Lab Code: CHEM Case No. : 24906 SAS No.: , SDG No. : MCSM16
Preparation Blank Matrix (soil/water):
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.'Blank(ug/L) C
•
-
, , /.
.
Continuing CalibrationBlank (ug/L)
*v 0>c *• .'d> - <£> c-52.99.09.01.21.01.0
-45.2-1.21.0
-2.1-29.03.0
-75.61.00.23 .0
-88 4'5.02.0
• 46.09.01.02.0
B00B00BB0BB0BUUUBUUUU0U
13.09.09.01.01.01.0
26.01.01.01.0
27.03.0
20.81.0
3.039.05.0
•' • 2.0
9.01.02.0
BUUUUUBUUUUUBU
UUUU
UUU
11.09.09.01.01.01.010.01.01.01.0
27.03.0
11.01.0
•3.039.05.02.0
9.01.02 . 0
•
UUUuuuuuuuuuuuuuuuuuu
Prepa-rationBlank C
-,
' .
,
'
M
PPPPPPPPPPPPPPCVppppppppNR
FORM III - IN . ' 013 ILM04.0
IVR32I833
. U.S. EPA - CLP
- ' ' .•', ' ' ' • ' . . . - . ' 3 ' . . - . - • • • • :"" ' ' • - - ' . • . . • • . ' " ~x ,
. . • • • - • • v • BLANKS • ' ' - . . : . ' ; /'. ' '. • • - . ' . ' - ' • **^
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166 -
Lab Code:' CHEM 'Case No.: 24906 SAS No.: SDG No.: MCSM16
Preparation Blank. Matrix (soil/water):
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodium .ThalliumVanadiumZincCyanide
InitialCalib.Blank(ugVD C
•
•
•—
' *Continuing Calibration
Blank (ug/L)*• s-~ »C * *e£ '*/T*\ C(3) <£> (&)
15.99.09.01.01.01.024.71.01.01.027.03.022.21.0
3.039.05.02.0
9.01.02.0
3UUUuu3UUUUU3U
UUUU
Uuu
11.09.09.01.41.01.017.31.01.01 . 027.03.011.31. 0
- 3.039.05.02.0
9.01.02.0
\
UUu3UUBUUUUu8U
uuuuuuu
42.69.09.01.01.01 . 046.51.01.01.027.03.039.71.0
3.039.05.02.0
-9.11.04.0
•'
A • •
3UUUUUBUUUuu3U
uuuu3UB
— '
1
Prepa-rationBlank C
1
—
\
M
P,PPPPPPP..
sPPPPNRPPPPNRP-P ,PNR
,
FORM III - IN f\i * ILM04.0
AR32l83lf
U.S. EPA - CLP
• • " . ' . . .'-.:•;• 13 ' . . ' • jr ' / • ' " '• . - '" •'• ''PREPARATION LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No..;: 24906. SAS No.: SDG No.: MCSM16
Method: CA ' "-. v.y.
EPASample No.
MCSM16MCSM16DMCSM16SPBW
• •• •
PreparationDate
08/14/9608/14/9608/14/9608/14/96
-'< • : .:.- -
, ' .,••'.
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. . - .' ' ; •"••>
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Weight(gram)
t
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Volume(mL)
50505050
FORM XIII - IN VT«*w ILM04.0D-4Q
AR32I835
• U.S. EPA - CLP
. • ' ' ; .' ... 13 • . ' '' • • . • • : . - • PREPARATION LOG,
Lab Name: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSM16
Method: C V . . ' • " . ' . ,
EPASample No.
MCSM15MCSM16DMCSM16SPBW
. . !
.
PreparationDate
08/26/9608/26/9603/26/9603/26/96
•
'
.
• ; '• '
Weight(gram).
• •
-
• -:• •• . . . •
•
Volume(mL)
100' 100
100100
, • •
' • '
,
FORM XIII - IN , ILM04.0
AR32I836
0.S. EPA - CLP
• - ' ' : •' • • : : . '13; r .'.••' • • • . - -.'•,. PREPARATION LOG .
LabName: CHEMTECH CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No. : 24906 SAS No.: SDG No.: MCSM16
Method: P .' •.-•.•:••':••••• ' ' '
EPASample No .
LCSWMCSM16MCSM16DMCSM16SPBW
- • : '•-
'
'
PreparationDate
08/23/9608/23/9608/23/96OB/23/96OB/23/96
• • /. ,• .. • ••
' • '.. " •. . . . .,•.;•
' ( * . .
• » - •'- - • ' <
Weight(gram)
%•
•
'. . •
Volume(mL)
10Q100100100100
.
,
•
FORM XIII - IN ftJIO 'ILM°4-°
AR32I837
a ^ u.s. EPA - .CLP v• . ' , : . . ' . • • ' - ' • 1 4 • " . '
. ANALYSIS RUN LOG
Lab Name: CHEMTECli CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No. : MCSM16
Instrument ID Number: PO Method: P
Start date: 09/01/96 Erid date: 09/01/96
EPASampleNo.
SOSSSsICVICVICVICVIC3 :CRI— \ICSAICSABCCVCCB-rNZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB— 2ZZZZZZZZZZZZZZZZZZZZZZZZ .ZZZZZZ
- .'
D/F
1.001.001.001.001.001 . 001.00
, 1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
• i.oo1.001.00
Time
09030919092109230926092709340940094409430954100310061009101210161022102510301035103910431046104910531056105911031106110911131116
' % R -
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.
FORM XIV - IN
046
AR32I838
' U.S. EPA - CLP . .
• V :'^V " . • ' • ; - . - > ' • "-i4 '.al>'"' - . - ' . . ' . ' . - • > - .ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING/GROUP Contract: 68-D5-0166•- , N ' - ' -
Lab Code: CHEM Case No.: 24906 . SAS No.: SDG No.: MCSM16
Instrument ID Number: PO • Method: P
Start date: 09/01/96 ; End date: 09/01/96
EPASampleNo.
ZZZZZZCRI -2-ICSAICSABCCVCCB~3>ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB~H-ZZZZZZZZZZZZZZZZZZZZZZZZCRI -3ICSAICSABCCVCCB-3T"ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00liOO1.001.001.001.001.001.001.00
. 1.005.001.00
Time
11191124112711301133113611391144114711511211121512161223122812351238124112441253131713231327133513401343134613501353135914031415
s. % R
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•-
FORM XIV - IN . ILM04.0
047
AR32I839
U.S. EPA - CLP
. .•' •' ' ' '. 14 ' . ' ,V ANALYSIS RUN LOG
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166
Lab Code: CHEM Case No.: 24906 SAS No.: SDG No.: MCSM16
Instrument ID'Number: PO Method: P
Start date: 09/01/96 '• . ' End date: 09/01/96
EPASampleNo.
ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZccv-CCB— *»ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCRI — 4-ICSAICSABCCVCCB -"7MCSM16MCSM16DMCSM16SMCSM16LZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVccB -2:-PBW
D/F
1.001.005.001.001.00
•'1.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.00'5.001.001.001.005.001.00
•10.00•i.oo1.001.00
Time
14131421142814321439144214451452145514591504151015141517152115321544154715501602160516031614162216251630163616451557170017031709
, .
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FORM XIV - IN " ILMOX J
flR32l8itO
: , , ,;. _ U.S. :EPA - CLP ? ' . . ; ; ,
•'-. - ••• . •'-:-•" 14 . • ' •'" • vANALYSIS RUN LOG
Lab Name: CHEMTECH" CONSULTING GROUP Contract: 68-D5-0166
Lab Code: CHEM Case No i: 24906 SAS No.: SDG No.: MCSM16
Instrument ID Number: CN > . Method: CA . .
Start date: 08/14/96 ' End date: 08/14/96
EPASampleNo.
soS10.0S100.0S500.0S1000.0ICVICBCCVCCBZZZZZZPBWMCSM16MCSM16DMCSM16SZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001,001.001.001.001.001.001.00
f
. . .
Time
13001302130413061308131013121314131613161320132213241326132813301332133413361338
% R AL
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FORM XIV - IN . ILM04.0
1R32/81H
, U.S. EPA - CLP
' . " • ' 14 : ' , •ANALYSIS RUN LOG' • • . • ' • ; • - , . ' . - : . , . • • • . \ J -
Lab Name: CHEMTECH CONSULTING GROUP Contract: 63-D5-0166 •——'
Lab Code: CHEM Case No. :. 24 906 SAS NO.: SDG No. : MCSM16
Instrument ID Number: CV Method: CV
Start date: 08/26/96 End date: OB/26/96
EPASampleNo.
SOSO. 2SO. 5Sl.OS5.0S10.0ICVICBCCVCCBCRA ,.PBW •MCSM16MCSM16DMCSM16SZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ
D/F
1.001.001 . 00I. 001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001 .001.001.001.001.001.001.00.1.001.001.00
Time
15231525152715291531153315351537153915411543154515471549155115531555155715591601160316051607160916111613161516171619162116231625
% R
•
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.
BABECD
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FORM XIV - IN „ ' • ILM04
044
„ U.S. EPA - CLP
'• '' - ' • ' ".-'N '" 14' ' ' ' . : ' , - ' ' 'ANALYSIS RUN LOG
Name: CHEMTECH CONSULTING GROUP .'•'•' \ Contract: 68-D5-0166
Lab Code: CHEM . . Case No.: 24906 SAS No.: SDG No.t MCSM16
Instrument ID Number: CV - Method: CV
Start date: 08/26/96 End date: 08/26/96
EPASampleNo.
CCVCCBZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB
-
D/F
1.001.001.001.001.001.00•1.001.00
-
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Time
16271629163116331635163716391641
• • • -
-,
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SB
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Analytes
ASBA
UECDCA
•
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CuFEPB
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MG
f '
MNHG
XX
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-
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-
FORM XIV - IN ILM04.0
' 045
'!R32I8I*3
Recommended