AMX/ARX - AVANCEramsey1.chem.uic.edu › nmr › downloads › BASHCD10 › pdf › z31455.… · BRUKER Version AMX/ARX - AVANCE 2H Lockswitch 500MHz Technical Manual 004

AMX/ARX - AVANCE

2H Lockswitch 500MHzTechnical Manual

BRUKER

Version

004

The information in this manual may be altered without notice.

BRUKER accepts no responsibility for actions taken as a resultof use of this manual. BRUKER accepts no liability for any mis-takes contained in the manual, leading to coincidental damage,whether during installation or operation of the instrument. Un-authorised reproduction of manual contents, without writtenpermission from the publishers, or translation into another lan-guage, either in full or in part, is forbidden.

This manual was written by

BARTHELEMY Philippe

© December 15, 1998: Bruker SA

Wissembourg, France

Manual P/N: Z31455DWG-Nr: 1165004

Contents

Contents ............................................................... 3

Index ..................................................................... 5

1 General description ................................................ 71.1 Description .......................................................................... 71.2 Specifications ...................................................................... 81.3 Spectrometer environment ................................................... 91.4 Wiring ................................................................................. 9

2 Control signal & RF signal route...........................112.1 About polarity selection ..................................................... 112.2 Internal polarity selection ................................................... 112.3 Output signal polarities function of selected jumpers .......... 122.4 RF signal of DEC 2H IN route ............................................ 13

3 Applications.......................................................... 153.1 Applications spectra .......................................................... 15

Composit pulse program spectra ....................................163.2 Pulse program ................................................................... 18

Sequence for AMX, ASX and ARX spectrometer ............18Sequence for Avance spectrometer DMX, DRX ..............19

4 2H Lockswitch 500MHZ ........................................ 21

5 Control Board ....................................................... 23

6 Blanking Switch BLMK 32-160MHZ ...................... 29

7 HP Coupler 3dB 62,5-125MHZ .............................. 33

8 Specifications ....................................................... 378.1 2H Lockswitch 500 MHz specifications ............................... 37

Figures ................................................................ 39

Tables .................................................................. 41

Technical Manual Version 004 BRUKER 3 (43)

Contents

4 (43) BRUKER Technical Manual Version 004

Index

Numerics

13C chloroform line ............................................................................................. 152H TX OUT from LOCK TRANSMITER................................................................ 9

A

AMX/ARX polarity ............................................................................................... 11Auxiliary BLK OUT ................................................................................................ 9AVANCE polarity................................................................................................. 11

B

BLK from X Amplifier............................................................................................. 9

F

Frequency range................................................................................................. 37

O

Observation 13C decoupling 2H and 1H............................................................. 15

P

Power requirements ............................................................................................ 37Pulse program for AMX....................................................................................... 18Pulse program for ARX ....................................................................................... 18Pulse program for ASX ....................................................................................... 18Pulse program for DMX....................................................................................... 19Pulse program for DRX....................................................................................... 19

R

RF POWER from X Amplifier ................................................................................ 9RF to 2H Probe ..................................................................................................... 9

S

Software control .................................................................................................. 37Spectra................................................................................................................ 15Spectra with 1H WALTS-16 & 2H GARP............................................................ 16Spectra with 1H WALTS-16 & 2H WALTS-16..................................................... 17


Index

T

TCU OBS 2H selection ......................................................................................... 9TCU programed BLK............................................................................................. 9

W

W4B132147 C..................................................................................................... 22W4D132510 A..................................................................................................... 28W4L132122 G ..................................................................................................... 25W4L132146......................................................................................................... 35W4S132122 G..................................................................................................... 24W4S132144 A ..................................................................................................... 30W4S132146 ........................................................................................................ 34

X

X out...................................................................................................................... 9


1General description 1Description 1.1

The 2H Lockswitch system allows to perform experiments with Lock and Deuteri-um decoupling or just Deuterium observation. It is possible to switch from the Xobservation to Deuterium observation by using only one X amplifier without doingany cable changes. This manipulation is possible because of the internal «rout-ing» that dispatches the source [channel 1 = 13C (2H)] either on the «Deuterium»output (Dec / Lock 2H to HPPR) or on the «X» output (BB Preamplifier).

The commutation for «Lock» and «1H or X» observation is possible with this ac-cessory (automatic).

This system allows also to perform 1 axis «Deuterium Gradient Shiming».

Figure 1.1. Synoptic of 2H Lockswitch

2H LOCKSWITCH

Sel Obs-2H

Lockswitch andHPPR 2H BLKelaboration

TP-FO in

Sel 2H/Dec

TP-FO out

2H TR inTR Switch

Relay SwitchDec 2H in

BB Preamp.

RX-BLNK out

TX-BLNK out

Coupler

Dec/Lock 2Hto HPPR


General description

Specifications 1.2

- Power supply: 200 V to 240 V AC (rear socket)- Range: 62,5 to 125 MHz- Insertion loss: 4 dB ±1 dB in the range (X channel and 2H channel both)- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM on RF active state) :

20 dB to 30 dB (DEC/LOCK 2H Output 50 Ohms loaded )

- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM desactivated state):greater as 75 dB

- 2H TR IN Input to DEC 2H IN Input Isolation (when BLKM desactivated state) :greater as 75 dB

- 2H TR IN Input to DEC/LOCK 2H Output Isolation (when BLKM desactivatedstate) : greater as 60 dB

- Total switching time : less than 15µs for ’’SEL 2H/DEC & SEL OBS-2H’’ andless than 0,5 µs for TP-FO

- Universal Polarity capability on all logical outputs and TP-FO INSelection (See more details below )

- SEL 2H/DEC & SEL OBS-2H INPUTS OPTO-ISOLATED :Input current > 0,5 mA (1,5 V In) => active levelInput current < 0,3 mA (1,0 V In) => unactive level

- High speed TP-FO INPUT OPTO-ISOLATED :Input current > 5 mA (2,8 V In) => active levelInput current < 2 mA (1,2 V In) => unactive level

➪ Don’t exceed TTL Level; it could cause damage to the Input isolation opto-couplers


Spectrometer environment

Spectrometer environment 1.3

Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer

Wiring 1.4

Figure 1.3. Front panel wiring

HPPR

1st channel

BB

2nd channel

1H

3rd channel

2H

BSMS-lock

BLKy

2H TR

TP-FOTX-BLNK

RX-BLNK

RX-BLNK outTX-BLNK out

TP-FO in

2H TR in

Sel 2H/Dec

Sel Obs 2H

Sel 2H/Dec

Sel Obs 2H

BB Preamp

Dec 2H in

13C pass

2H LOCKSWITCH

Lockswitch andHPPR 2H BLKelaboration

13C

1H

2H

2H stopBB 1H

Receiver

2HReceiver

Dec/Lock 2HHPPR

TP-FO out

Probe

13C

2H

1H

Lock and 2H decouplingfor AMX and AVANCEequiped with BSMS and HPPRusing T-LX with RF blanking

(13C)

TP-FO OUT

2H LOCKSWITCH 500 MHZ

2H TR IN SEL. OBS-2HBB PREAMP. TP-FO INSEL.2H/DEC DEC/LOCK 2Hto HPPRTX-BLNK OUTRX-BLNK OUT DEC 2H IN

2H TX OUT fromLOCK TRANSMITER

X out TCU programedBLK

TCU OBS 2Hselection

BLK fromX Amplifier

(paralle conected)

General

AuxiliaryBLK OUT

(to BSMS L-TX)

RF POWER from X Amplifier

RF to 2H Probe


General description


2Control signal & RF signal route 2About polarity selection 2.1

The 3 switches located on the control board (inside the device) allow to solveproblems about input and output standard polarity.

• AMX/ARX polarity or shows that the validation is done at level 1 to outputand at a current flow in the used optocouplers (from BLK inputs).

• AVANCE polarity or shows that the validation is done at level 0 to out-put and with no current flow in the used optocouplers (from BLK inputs).

Internal polarity selection 2.2

Figure 2.1. AVANCE and AMX/ARX Configurations

➪ For the delivery, the jumpers are setted for «AVANCE» configuration

AM

X/A

RX

AV

AN

CE

J10 J9 J7 J8 J13

OB

S-2

H

SE

L2H

/DE

C

TP

-FO

IN

TP

-FO

OU

T

RX

-TX

AVANCEConfiguration

AMX/ARXConfiguration

AM

X/A

RX

AV

AN

CE

J10 J9 J7 J8 J13

OB

S-2

H

SE

L2H

/DE

C

TP

-FO

IN

TP

-FO

OU

T

RX

-TX


Control signal & RF signal route

Output signal polarities function of selected jumpers 2.3

Table 2.1. For RX-TX Blanking in AVANCE configuration

TP-FO OUTPOL SELECT

SEL 2H/DECPOL IN

TP-FOPOL IN

SEL2H/DEC TP-FO INBLMKState

RX & TXBLNK OUT

TP-FO OUTState for

AMX/ARX

TP-FO OUTState forAVANCE

AMX/ARX AMX/ARX

No SignalCurrent

No SignalCurrent

No SignalNo SignalCurrentCurrent

ThroughIsolatedThroughIsolated

1010

0111

1000

AMX/ARX AVANCE

No SignalCurrent

No SignalCurrent



1010

1101

0010

AVANCE AMX/ARX

No SignalCurrent

No SignalCurrent


IsolatedThroughIsolatedThrough

0101

1011

0100

AVANCE AVANCE

No SignalCurrent

No SignalCurrent



0101

1110

0001

Table 2.2. For RX-TX Blanking in AMX/ARX configuration

TP-FO OUTPOL SELECT

SEL 2H/DECPOL IN

TP-FOPOL IN

SEL2H/DEC TP-FO INBLMKState

RX & TXBLNK OUT

TP-FO OUTState for

AMX/ARX

TP-FO OUTState forAVANCE

AMX/ARX AMX/ARX

No SignalCurrent

No SignalCurrent



0101

0111

1000

AMX/ARX AVANCE

No SignalCurrent

No SignalCurrent



0101

1101

0010

AVANCE AMX/ARX

No SignalCurrent

No SignalCurrent



1010

1011

0100

AVANCE AVANCE

No SignalCurrent

No SignalCurrent



1010

1110

0001


RF signal of DEC 2H IN route

RF signal of DEC 2H IN route 2.4

Table 2.3. For BB PREAMP output device only

SEL OBS 2HPOL IN

SEL OBS 2H Signal from DEC 2H IN routed on

AMX/ARXNo SignalCurrent

BB PREAMP outputDEC/LOCK 2H to HPPR output

AVANCENo SignalCurrent

DEC/LOCK 2H to HPPR outputBB PREAMP output


Control signal & RF signal route


3Applications 3Applications spectra 3.1

Effect on 13C chloroform line of ± n x 1500Hz 2H decoupling offset switchingagainst on resonance frequency.

Figure 3.1. Resonnance spectum

Observation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using «2H LOCK-SWITCH» accessoryDecoupling sequences:- On 1H composit pulse program = WALTZ-16- On 2H composit pulse program = GARP(2H irradiation frequenzy ±1500Hz around on-resonance)

+4500 +3000 +1500 Resonnance -1500 -3000 -4500


Applications

Composit pulse program spectra 3.1.1

Figure 3.2. 1H WALTZ-16 and 2H GARP

Obsevation 13C decoupling 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequence :

- On 1H composit pulse program = WALTZ-16

Obsevation 13C decoupling 2H and 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequences :

- On 1H composit pulse program = WALT-16- On 2H composit pulse program = GARP

(2H irridaition frequency on resonnance)



(2H irridaition frequency +1500Hz off resonnance)



(2H irridaition frequency -1500Hz off resonnance)


Applications spectra

Figure 3.3. 1H WALTZ-16 and 2H WALTZ-16

Obsevation 13C decoupling 1H, lock 2HSample 10% EB in CDC13Using 2H LOCK-SWITCH accessoryDecoupling sequence :

- On 1H composit pulse program = WALTZ-16


- On 1H composit pulse program = WALT-16- On 2H composit pulse program = WALT-16

(2H irridaition frequency on resonnance)



(2H irridaition frequency +1500Hz off resonnance)



(2H irridaition frequency -1500Hz off resonnance)


Applications

Pulse program 3.2

Sequence for AMX, ASX and ARX spectrometer 3.2.1

;zgdc_2h_A;1D sequence for X-nucleus with 1H and 2H decoupling;AMX,ASX and ARX version

d11=30m#define lo_hold_on 45u setf2|9#define lo_hold_off 45u setf2^9#define sel_2h_dec_on 45u setf1^7#define sel_2h_dec_off 45u setf1|7

d11 hl1 cpd dbl0 dbo sel_2h_dec_off1 ze2 d1 dbo lo_hold_off sel_2h_dec_offlo_hold_on sel_2h_dec_ond11 cpdbp1 ph1go=2 ph31lo_hold_off sel_2h_dec_offwr#0d11 do dbo

exit

ph1=0 2 2 0 1 3 3 1ph31=0 2 2 0 1 3 3 1

;hl1: ecoupler power level for CPD decoupling;dbl0: ecoupler power level for CPDB decoupling;p1 : 90 degree transmitter high power pulse;p31: 90 degree pulse for salve timer (cpd-sequence);p30: 90 degree pulse for salve timer (cpdb-sequence);d1 : relaxation delay; 1-5 * T1;d11: delay for disk I/O................[30msec];cpd: cpd-decoupling according to sequence defined by cpdbprg;cpdb: cpdb-decoupling according to sequence defined by cpdbprg


Pulse program

Sequence for Avance spectrometer DMX, DRX 3.2.2

;zgdc_2h_D1D sequence for X-nucleus with H-1 and H-2 decoupling;Avance spectrometer DMX,DRX;jmt SADIS wissembourg

#include

d11=30m

1 zeH2_LOCK.................;define in Avance.incl setnmr8|4d12 setnmr0|8...........;gating 1H HPPR in case of using 5 preamp. units

2 d11 pl13:f2 do:f3d11 cpds2:f2d1 pl14:f3 H2_LOCK......;define in Avance.incl setnmr8|4d11 cpds3:f3 H2_PULSE...;define in Avance.incl setnmr8|4p1 ph1go=2 ph31 cpds2:f2wr#0d11 do:f2d11 do:f3d12 setnmr0^8

exit

ph1=0 2 2 0 1 3 3 1ph11=0 2 2 0 1 3 3 1

;pl13: decoupler power level for decoupling in CDP mode on H-1;pl14: decoupler power level for decoupling in CDP mode on H-2;p1 : 90 degree transmitter high power pulse;p31: 90 degree pulse for salve timer (cpd2:f2-sequence);p30: 90 degree pulse for salve timer (cpd3:f3-sequence);d1 : relaxation delay; 1-5 * T1;d11: delay for disk I/O................[30msec]

;cpd2:f2: f2-decoupling according to sequence defined by cpdprg2:WALTZ16;cpd3:f3: f3-decoupling according to sequence defined by cpdprg3:WALTZ16f3


Applications


42H Lockswitch 500MHZ 4


12

Te

345678

J8

2 1

A

B

C

D

P/N:W1342102

REAR PANELFROM FRAME

N

LINE IN

J3

P

DRAWN:DATE:

APPROV:DATE:

DWG:

VISA:

VISA:

SHEET:

DW

W4B132147

03/12/98

PHB

C

15/12/98

1/1

Figure 4.1.

2H Locksw

itch 500MH

Z B

lock Diagram

chn

ical Man

ual V

ersion

004B

RU

KE

R22 (43)

8 7 6 5 4 3

D

C

B

A

P3

J7

DEC 2H IN

DEC/LOCK 2Hto HPPR

J9

BB PREAMP

J1

J3

P1 J2 P2

RELAY SWITCHP/N:73705

COUPLER HP 3dBP/N:W1345141

P2 J2

J3 P3

P1 J1

J2 P2

F1

BLANKING SWITCHBLMK

P/N:W1345135

P1 J1

CP1

J10

2H TR IN

P/N:W1341016FRONT PANEL

J11SEL OBS-2H

TP5 TP6 J3

F1

+15V

220V

POWERSUPPLY

TP1

J1SEL 2H/DEC

J2TP-FO IN

J4TP-FO OUT

J6TX-BLNK OUT

J5RX-BLNK OUT

CONTROL BOARDP/N:W1346044

TP20V

P/N:O56541

F2

TP3

LD1POWERSTATUS

TP4

NOTE :

J8 = 59053 : SMA CONNECTORJ7 = 14848 : N CONNECTOR

LD1 = 32510 : POWER STATUS LED

J3 = 52666 : LINE IN CONNECTOR

J9 = 14848 : N CONNECTORJ10 = 59053 : SMA CONNECTOR

BLOCK DIAGRAM

ART: W1345010

2H LOCKSWITCH UNIT500MHZ

EC: 04

5Control Board 5


12

24 (4

345678

2 1

A

B

C

D

2

A04

J3BLKM BLK

OUT

J4TP-FO OUT

R26100

R947.5

J5RX-BLNK OUT

R27100

R5100

4

B04

6

C04

8

D04

10

E04

J6TX-BLNK OUT

R6100

R28100

D21N4007

+15V

TP5+REL

R29100

12

F04

D31N4007

TP6-REL

J12PIN DIODE

SWITCHR2147.5

R1933.2

+5V +5V

C6100NF

U5

CE322UF35V

U3

5V

C5100NF

DRAWN:DATE:

APPROV:DATE:

DWG:

VISA:

VISA:

SHEET:

DW

W4S132122

PHB

12/11/97

13/11/97

G 1/1

S.a.d.i.s

SPECTROSPIN

Figure 5.1.

Control B

oard Schem

atic

3)B

RU

KE

RT

echn

ical Man

ual V

ersion

004

8 7 6 5 4 3

D

C

B

A

+5V

23456

1

RS14.7K

+5V

23456789

1

RS24.7K

J11SEL OBS-2H

R1470

R23.32K

J1SEL 2H/DEC

1

2

8

7

3

4 6

5

U1HCPL-2731

R3470

R43.32K

+5V R22100

R23100

R24100

+5V

IN1 1

IN2 2

IN3 3

IN4 4

IN5 5

IN6 6

IN7 7

IN8 8

IN9 9

GND 10

VCC 20

I/O8 19

I/O7 18

I/O6 17

I/O5 16

I/O4 15

I/O3 14

I/O2 13

I/O1 12

IN10 11

U2EP330

HLS04/01

1

U374HC

R1047.5

3

U374HC

5

U374HC

R1147.5

R25100

R17100

+5V+5V

R201K

1

27

5

8U5A

HCPL-2630J2

TP-FO IN

R161K

R15332

R14100

9

U374HC

11

U374HC

R1247.5

13

U374HC

1 2 3

J8OUT

R13100

RX-TX

R30100

1 2 3

J13SEL

123

J7IN

123

J9SEL

2H/DEC TP-FO

123

J10SEL

OBS-2H

1-2 : AVANCE2-3 : AMX / ARX

T1BS170

R18100

+5V+5V +

C2100NF

U2 U3

C1100NF

U1

+5V

CE222UF35V

C4100NF

C3100NF

R7121

CE122UF35V

R31121

R32121

VI1 VO 2GND

3

U4MC7805CT

TP2DGND

D11N4007

TP3LED K

TP1+15V

+15V

L110UH

TP4LED A +5V

R8470

VCC

ART: W1346044

2H LOCKSWITCHCONTROL BOARD

EC: 09

12

Te

345678

+15V

DGND

P2P1

J6

2 1

A

B

C

D

VISA:

VISA:

G SHEET: 1/1

S.a.d.i.s

SPECTROSPIN

Figure 5.2.

Control B

oard Location

chn

ical Man

ual V

ersion

004B

RU

KE

R25 (43)

W4P132122GLED

A

K

AV

AN

CE

AM

X/A

RX

TP

-FO

IN

TP

-FO

OU

T

SE

L2H

/DE

C

OB

S-2

H

-REL+

RX

-TX

J3 J12TP4

TP3

TT

TP6 TP5

U1 U5

U2

J8J7J9J10 J13

R1

R2

R3

R4 R

5

R7

R8

R11

R10

R9

R6

R13

R19

R16

R18

R17R14

R15

R21

R20

R25

R24R23R22

R12

R29

R28R

27

R26

R30

R32

R31C1

C2

C3

C4

C5

C6

D1D3 D2

L1

CE1

CE2

CE3

RS

1

T1

U3

RS

2

J1 J2 J4 J5J11

U4

8 7 6 5 4 3

D

C

B

A ART:

2H LOCKSWITCH

W1346044 DRAWN:DATE:

APPROV:DATE:

DWG:

EC: RC05/01/98

W4L132122

05/01/98PhBCONTROL BOARD

CI : W4P132122G

Control Board

Value Table

+------------------------------------------------------------------------------+¦ Part:W1346044 Drawing:W4S132122G Copy In Part: Draw: ¦¦ Desc:2H LOCKSWITCH CIRCUIT CONTROL ECL:9 Modified:03/12/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ C01 37167 COND CERM 100N 100V 10% X7R ¦¦ C02 37167 COND CERM 100N 100V 10% X7R ¦¦ C03 37167 COND CERM 100N 100V 10% X7R ¦¦ C04 37167 COND CERM 100N 100V 10% X7R ¦¦ C05 37167 COND CERM 100N 100V 10% X7R ¦¦ C06 37167 COND CERM 100N 100V 10% X7R ¦¦ CE01 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CE02 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CE03 10017 COND CHIMI RAD 22U 35V 6.3X7 ¦¦ CI01 W1356617 CI CONTROL 2H LOCKSWITCH ¦¦ D01 355 DIODE 1N4007 ¦¦ D02 355 DIODE 1N4007 ¦¦ D03 355 DIODE 1N4007 ¦¦ ICSU01 4285 IC SUPPORT DIL8 TULIPE ¦¦ ICSU02 9276 IC SUPPORT DIL20 TULIPE ¦¦ ICSU03 4284 IC SUPPORT DIL14 TULIPE ¦¦ ICSU05 4285 IC SUPPORT DIL8 TULIPE ¦¦ J01 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J02 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J03 8747 ACCBL PICOT FOURCHE D1.3MM ¦¦ J03' 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ J04 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J05 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J06 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J07 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J07' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J08 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J08' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J09 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J09' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J10 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J10' 3033 ACCBL CAVALIER F 2.54MM ¦¦ J11 22656 CN COAX SMA F C PRT L=29.5MM ¦¦ J12 8747 ACCBL PICOT FOURCHE D1.3MM ¦¦ J12' 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ J13 W1204337 CN M 3 D PRT BARSIL R2.54 H8 ¦¦ J13' 3033 ACCBL CAVALIER F 2.54MM ¦¦ L01 30609 SELF 10UH 0.33A ¦¦ R01 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R02 1016 RES MET 3.32K 1% 0.6W 50PPM ¦¦ R03 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R04 1016 RES MET 3.32K 1% 0.6W 50PPM ¦¦ R05 998 RES MET 100 1% 0.6W 50PPM ¦¦ R06 998 RES MET 100 1% 0.6W 50PPM ¦¦ R07 999 RES MET 121 1% 0.6W 50PPM ¦¦ R08 2741 RES MET 470 1% 0.6W 50PPM ¦¦ R09 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R10 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R11 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R12 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R13 998 RES MET 100 1% 0.6W 50PPM ¦¦ R14 998 RES MET 100 1% 0.6W 50PPM ¦¦ R15 1004 RES MET 332 1% 0.6W 50PPM ¦¦ R16 1010 RES MET 1K 1% 0.6W 50PPM ¦


+------------------------------------------------------------------------------+¦ Part:W1346044 Drawing:W4S132122G Copy In Part: Draw: ¦¦ Desc:2H LOCKSWITCH CIRCUIT CONTROL ECL:9 Modified:03/12/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ R17 998 RES MET 100 1% 0.6W 50PPM ¦¦ R18 998 RES MET 100 1% 0.6W 50PPM ¦¦ R19 992 RES MET 33.2 1% 0.6W 50PPM ¦¦ R20 1010 RES MET 1K 1% 0.6W 50PPM ¦¦ R21 994 RES MET 47.5 1% 0.6W 50PPM ¦¦ R22 998 RES MET 100 1% 0.6W 50PPM ¦¦ R23 998 RES MET 100 1% 0.6W 50PPM ¦¦ R24 998 RES MET 100 1% 0.6W 50PPM ¦¦ R25 998 RES MET 100 1% 0.6W 50PPM ¦¦ R26 998 RES MET 100 1% 0.6W 50PPM ¦¦ R27 998 RES MET 100 1% 0.6W 50PPM ¦¦ R28 998 RES MET 100 1% 0.6W 50PPM ¦¦ R29 998 RES MET 100 1% 0.6W 50PPM ¦¦ R30 998 RES MET 100 1% 0.6W 50PPM ¦¦ R31 999 RES MET 121 1% 0.6W 50PPM ¦¦ R32 999 RES MET 121 1% 0.6W 50PPM ¦¦ RS01 9818 RES RES 4.7KX5 2% SIL6 ¦¦ RS02 7223 RES RES 4.7KX8 2% SIL9 ¦¦ T01 34607 TRANS BS170 N VMOS TO92 ¦¦ TP01 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP02 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP03 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP04 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP05 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ TP06 59995 ACCBL PICOT FOURCHE D1.1MM ¦¦ U01 14820 OPTO COUP HCPL-2731 DIL8 2-FOI ¦¦ U02 W1356676 IC 220/2H LOCKSWITCH CONTROL ¦¦ U03 10812 IC 7404/MM74HC04N PDIP 14 ¦¦ U04 446 IC 7805/VREG MC7805CT TO220 ¦¦ U05 5941 IC HCPL 2630 ¦+------------------------------------------------------------------------------+


Figure 5.3. Pal HLS01/01 Schematic

8 7 6 5 4 3 2 1

A

B

C

D

12345678

D

C

B

A

VCC

TPFOOUT

TXBLNKRXBLNK

BLKMOUTIN1 1

IN2 2

IN3 3

IN4 4

IN5 5

IN6 6

IN7 7

IN8 8

IN9 9

GND 10

VCC 20

I/O8 19

I/O7 18

I/O6 17

I/O5 16

I/O4 15

I/O3 14

I/O2 13

I/O1 12

IN10 11

EP330PC-12

SEL2HDEC

GND

TPINPOLTPOUTPOL

SELOBS2H

HLS04/0111/09/96

GND

TPFOINSELPOL

OBS2HPOLRXTXSEL

GND

RESERVEDRESERVEDRESERVED

RELAYOUT

SEL2HDEC 3

9 RXTXSEL

NOT

XOR

NOT

XOR

NOT

NOT

BLKMOUT

RXBLNK

TXBLNK 16

17

19

NOT

NOT

TPFOOUT 18

NOTXOROR2

XOR

NOT

NOT

SELPOL

TPFOIN

TPINPOL

TPOUTPOL

6

7

4

5

SELOBS2H

OBS2HPOL

2

8

XOR NOT

15 RELAYOUT

ART:

HLS04/01PAL 2H LOCKSWITCH

W1356676 EC: DRAWN:DATE:

APPROV:DATE:

DWG:

DW11/09/96

W4D132510

11/09/96PHB

VISA:

VISA:

SHEET: 1/1A

S.a.d.i.s

SPECTROSPIN


6Blanking Switch BLMK 32-160MHZ 6


12345678

30 (4

2 1

A

B

C

D

J2RF OUT

8F

C72PF

CI1

VISA:

VISA:

SHEET: 1/1A

Figure 6.1.

Blanking S

witch B

LMK

32-160MH

Z S

chematic

3)B

RU

KE

RT

echn

ical Man

ual V

ersion

004

8 7 6 5 4 3

D

C

B

A

R250

TT40C3

6.8NFC4

6.8NF

R551.1

C64.7PF

1

3

2

4

SW2DH80050

C1N

L41.5UH

1.

R4392

L31.5UH

C51NFL2

1.5UHR3392

L11.5UH

1

3

2

4SW1

DH80050

C21NF

CL150R

J1RF IN

C11NF

R11K

R9470

L51.5UH

R7392

C10390PF

R61K

C96.8NF

R8470

CE122UF

50V

NC1

IA2

GND3

IB4

NC 8

OA 7

V+ 6

OB 5

U1TSC428CPA

R104.7K

CP1BLK1\

F1+15V

ART:

2H LOCKSWITCHBLANKING SWITH BLKMSWITCH 10W / 32-160MHZ

W1345135 DRAWN:DATE:

APPROV:DATE:

DWG:

EC: 01 DW06/11/98

W4S132144

15/12/98PHB

Value Table

+------------------------------------------------------------------------------+¦ Part:W1345135 Drawing:W4S132144A Copy In Part: Draw: ¦¦ Desc:COMMUTATEUR BLKM 32-160MHZ ECL:1 Modified:09/11/98 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ C1 30424 COND CMS CDR14 1N 50V 20% ¦¦ C2 30424 COND CMS CDR14 1N 50V 20% ¦¦ C3 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C4 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C5 30424 COND CMS CDR14 1N 50V 20% ¦¦ C6 30396 COND CMS CDR14 4.7P 500V 0.25P ¦¦ C7 30389 COND CMS CDR14 1.2P 500V 0.25P ¦¦ C8 30424 COND CMS CDR14 1N 50V 20% ¦¦ C9 56276 COND CERM 6.8N 500V 5% X7R ¦¦ C10 30419 COND CMS CDR14 390P 200V 20% ¦¦ CE1 1983 COND CHIMI RAD 22U 50V 7X7 ¦¦ CI1 W1356240 CI B-LKM BLANKING SWITCH 10W ¦¦ CP1 56154 COND PAS FILTRE 100P 100V 10A ¦¦ ICSU1 4285 IC SUPPORT DIL8 TULIPE ¦¦ J1 33011 CN COAX SMA F D EMB PLATINE ¦¦ J2 33011 CN COAX SMA F D EMB PLATINE ¦¦ L1 51528 SELF 1.5UH 0.56A ¦¦ L2 51528 SELF 1.5UH 0.56A ¦¦ L3 51528 SELF 1.5UH 0.56A ¦¦ L4 51528 SELF 1.5UH 0.56A ¦¦ L5 51528 SELF 1.5UH 0.56A ¦¦ R1 20737 RES CMS 1K 1% 0.25W 1206 ¦¦ R2 30863 RES HF 50 40W ¦¦ R3 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R4 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R5 20765 RES CMS 51.1 1% 0.25W 1206 ¦¦ R6 20737 RES CMS 1K 1% 0.25W 1206 ¦¦ R7 20731 RES CMS 392 1% 0.25W 1206 ¦¦ R8 51288 RES CMS 475 1% 0.25W 1206 ¦¦ R9 51288 RES CMS 475 1% 0.25W 1206 ¦¦ R10 20745 RES CMS 4.7K 1% 0.25W 1206 ¦¦ RAD1 W1305665 BLAH RADIAT BLANKING SWITCH ¦¦ SW1 30636 DIODE PIN SW 10W ¦¦ SW2 30636 DIODE PIN SW 10W ¦¦ U1 56292 IC 428/DRV TSC428CPA DIP8 ¦+------------------------------------------------------------------------------+


Blanking Switch BLMK 32-160MHZ


7HP Coupler 3dB 62,5-125MHZ 7


Figure 7.1. HP Coupler 3dB 62,5-125MHZ Schematic

8 7 6 5 4 3 2 1

A

B

C

D

12345678

D

C

B

A

IN 1

0

2

ISO3

90

4

AN110261-3

J1RF IN 1

J2RF IN 2

R150

150W

CI1

J3RF OUT

HP COUPLER 3dB62.5-125MHZ

2H LOCKSWITCH

ART: W1345141 EC: 01 DRAWN:DATE:

APPROV:DATE:

DWG:

DW31/05/95

W4S132146

31/05/95PHB

VISA:

VISA:

SHEET: 1/1

S.a.d.i.s

SPECTROSPIN


12345678

Te

2 1

A

B

C

D

VISA:

VISA:

- SHEET: 1/1

S.a.d.i.s

SPECTROSPIN

Figure 7.2.

HP

Coupler 3dB

62,5-125MH

Z Location

chn

ical Man

ual V

ersion

004B

RU

KE

R35 (43)

J1

J3

J2

8 7 6 5 4 3

D

C

B

A ART: W1345141 DRAWN:DATE:

APPROV:DATE:

DWG:

EC: DW10/11/98

W4L132146

10/11/98PhBCOUPLEUR HP 3dB 62.5-125MHz

CI : W4P132448

W4P132448

INIS

O

R1

90°

AN1

0°

HP Coupler 3dB 62,5-125MHZ

Value Table

+------------------------------------------------------------------------------+¦ Part:W1345141 Drawing:W4S132146 Copy In Part: Draw: ¦¦ Desc:COUPLEUR HP 3DB / 62.5-125MHZ ECL:1 Modified:22/04/96 By:DW ¦+-- Value Tab ---------------------------------------------------------------+¦ Pos. Component Local Description ¦¦ AN01 56522 IC 10261/COUPL.HF 62.5-125MHZ ¦¦ CI01 W1340016 CI 3DB HP COUPLEUR 62.5-125MHZ ¦¦ J01 6194 CN COAX N F D EMB PLATINE ¦¦ J02 6194 CN COAX N F D EMB PLATINE ¦¦ J03 6194 CN COAX N F D EMB PLATINE ¦¦ R01 20138 RES HF CHARGE 50 OHMS 5% 150W ¦+------------------------------------------------------------------------------+


8Specifications 82H Lockswitch 500 MHz specifications 8.1

Table 8.1. General requirements

Power requirements 220 V ±10%, 50/60 Hz

Power consumption 15 W

Weight 4 Kg

Dimensions445 / 484 mm width (cabinet / front panel)1 Unit height280 mm depth

Software control XWINNMR or UXNMR

Table 8.2. Insertion loss

Decoupling channel 4 dB ±1dB

Lock channel 4 dB ±1dB

BB channel 1dB maximum

BLK 2H isolation 50 dB Typical

DEC 2H IN / 2H TR IN directivity 20 dB Typical

Table 8.3. Switching time

SEL 2H/DEC 15 µs typical (minimum current for level 1 INPUT : 0,5 mA)

SEL OBS 2H 15 µs typical (minimum current for level 1 INPUT : 0,5 mA)

TP-FO IN 300 ns typical (minimum current for level 1 INPUT : 5 mA)

Polarity selection DMX and AMX for all IN and OUT logical compatible

Table 8.4. Logic fan out

TP-FO OUT & RX BLNK / TX BLNKLevel 0 : 5 mA sink for 0,7 V outLevel 1 : 10 mA source for 1,5 V out

’’2H’’ Frequency range 70 to 80 MHz

DEC 2H IN power capability 600 W


Specifications


Figures

1 General description 7Figure 1.1. Synoptic of 2H Lockswitch .....................................................7Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer ......................9Figure 1.3. Front panel wiring ..................................................................9

2 Control signal & RF signal route 11Figure 2.1. AVANCE and AMX/ARX Configurations ............................... 11

3 Applications 15Figure 3.1. Resonnance spectum ..........................................................15Figure 3.2. 1H WALTZ-16 and 2H GARP ...............................................16Figure 3.3. 1H WALTZ-16 and 2H WALTZ-16 .........................................17

4 2H Lockswitch 500MHZ 21Figure 4.1. 2H Lockswitch 500MHZ Block Diagram ................................22

5 Control Board 23Figure 5.1. Control Board Schematic .....................................................24Figure 5.2. Control Board Location ........................................................25Figure 5.3. Pal HLS01/01 Schematic .....................................................28

6 Blanking Switch BLMK 32-160MHZ 29Figure 6.1. Blanking Switch BLMK 32-160MHZ Schematic ....................30

7 HP Coupler 3dB 62,5-125MHZ 33Figure 7.1. HP Coupler 3dB 62,5-125MHZ Schematic ...........................34Figure 7.2. HP Coupler 3dB 62,5-125MHZ Location ..............................35

8 Specifications 37


Figures


Tables

1 General description 7

2 Control signal & RF signal route 11Table 2.1. For RX-TX Blanking in AVANCE configuration ................ 12Table 2.2. For RX-TX Blanking in AMX/ARX configuration .............. 12Table 2.3. For BB PREAMP output device only ............................... 13

3 Applications 15

4 2H Lockswitch 500MHZ 21

5 Control Board 23

6 Blanking Switch BLMK 32-160MHZ 29

7 HP Coupler 3dB 62,5-125MHZ 33

8 Specifications 37Table 8.1. General requirements .................................................... 37Table 8.2. Insertion loss ................................................................. 37Table 8.3. Switching time ............................................................... 37Table 8.4. Logic fan out .................................................................. 37


Tables



Lastpage

ContentsIndexGeneral descriptionDescription 1.1Figure 1.1. Synoptic of 2H Lockswitch

Specifications 1.2Spectrometer environment 1.3Figure 1.2. Synoptic of 2H Lockswitch in the Spectrometer

Wiring 1.4Figure 1.3. Front panel wiring

Control signal & RF signal routeAbout polarity selection 2.1Internal polarity selection 2.2Figure 2.1. AVANCE and AMX/ARX Configurations

Output signal polarities function of selected jumpers 2.3Table 2.1. For RX-TX Blanking in AVANCE configurationTable 2.2. For RX-TX Blanking in AMX/ARX configuration

RF signal of DEC 2H IN route 2.4Table 2.3. For BB PREAMP output device only

ApplicationsApplications spectra 3.1Figure 3.1. Resonnance spectumComposit pulse program spectra 3.1.1Figure 3.2. 1H WALTZ-16 and 2H GARPFigure 3.3. 1H WALTZ-16 and 2H WALTZ-16

Pulse program 3.2Sequence for AMX, ASX and ARX spectrometer 3.2.1Sequence for Avance spectrometer DMX, DRX 3.2.2

2H Lockswitch 500MHZFigure 4.1. 2H Lockswitch 500MHZ Block Diagram

Control BoardFigure 5.1. Control Board SchematicFigure 5.2. Control Board LocationFigure 5.3. Pal HLS01/01 Schematic

Blanking Switch BLMK 32-160MHZFigure 6.1. Blanking Switch BLMK 32-160MHZ Schematic

HP Coupler 3dB 62,5- 125MHZFigure 7.1. HP Coupler 3dB 62,5-125MHZ SchematicFigure 7.2. HP Coupler 3dB 62,5-125MHZ Location

Specifications2H Lockswitch 500 MHz specifications 8.1Table 8.1. General requirementsTable 8.2. Insertion lossTable 8.3. Switching timeTable 8.4. Logic fan out

FiguresTables

Documents

AMX/ARX - AVANCEramsey1.chem.uic.edu › nmr › downloads › BASHCD10 › pdf › z31455.… · BRUKER Version AMX/ARX - AVANCE 2H Lockswitch 500MHz Technical Manual 004