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APPENDIX A
SITE PHOTOGRAPHS
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-1
PHOTOS 1 AND 2
Photo 1: Facing southeast, Drum 1 can be seen in the partially buried drum area. Behind it is the earthen berm, and Monitoring Well B5MW can be seen in the left foreground. (6/9/2011)
Photo 2: The drum with liquid contents (Drum 1) was placed in an overpack drum. (6/9/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-2
PHOTOS 3 AND 4
Photo 3: Facing south, the location of the potentially-damaged Monitoring Well MW16 is circled. (9/1/2011)
Photo 4: Facing north, the lid of the dry well is circled. (9/6/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-3
PHOTOS 5 AND 6
Photo 5: The dry well consisted of a 4-foot diameter perforated concrete pipe. (9/6/2011)
Photo 6: Facing east, the exposed portions of the log crib are shown. (9/6/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-4
PHOTOS 7 AND 8
Photo 7: The process tank was found in the eastern portion of the excavation. (9/7/2011)
Photo 8: The process tank placard indicates that the tank is “dry cleaning and laundry equipment.” (9/13/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-5
PHOTOS 9 AND 10
Photo 9: Facing north, fans provided ventilation during the excavation to reduce organic vapor concentrations. (9/2/2011)
Photo 10: Facing east, a pump on a truck-mounted water tank was used to apply the oxidant mixture to the base of the first lift of the treatment cell. (9/8/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC.Geotechnical & Environmental Consultants
A-6
PHOTOS 11 AND 12
Photo 11: Facing south, the deep horizontal vapor extraction piping was bedded in pea gravel and wrapped in geotextile fabric at 10 feet bgs to allow air flow, protect the pipe, and prevent silting. (9/10/2011)
Photo 12: Facing northwest, the VES array was completed with vertical riser pipes. Rubber slips caps were installed on the north array. (9/16/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-7
PHOTOS 13 AND 14
Photo 13: Facing north, the vapor horizontal vapor extraction system components include a 4-inch slotted PVC pipe which was bedded in pea gravel and enclosed in a geotextile. (9/13/2011)
Photo 14: Facing north, BCX completed the VES installation by shoveling pea gravel on the horizontal pipe, closing geotextile, and placing soil over the assembly to prevent the geotextile from opening. (9/13/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-8
PHOTOS 15 AND 16
Photo 15: Facing east, the north consolidation area is shown, with the soil pile with >1,000 ppm screening results on the left, and soil with <100 ppm screening results on the right. (9/6/2011)
Photo 16: Facing east, BCX removes the 6-mil liner from northeast consolidation area. Soil was segregated in piles, with soil with the lowest screening results (<1 ppm and <5 ppm) in piles on the right. (9/2/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-9
PHOTOS 17 AND 18
Photo 17: Facing southeast, BCX is conducting the targeted additional excavation. Gray ash-like material indicative of impacted soil is below the excavator bucket. (9/7/2011)
Photo 18: Facing east, the south VES risers can be seen. To the right (south) of the risers, the property slopes down, and trees and a fence are present. (9/15/2011)
32-1-17172-011
4501 Lake Otis Parkway Anchorage, Alaska
PHOTOS 1 AND 2
December 2011
SHANNON & WILSON, INC. Geotechnical & Environmental Consultants A-10
PHOTOS 19 AND 20
Photo 19: Facing west, the location of the bituminous fiber pipe on the west wall of the excavation is circled. (9/7/2011)
Photo 20: Facing south, the root wad on the south edge of the excavation prior to removal. (9/2/2011)
32-1-17172-011
APPENDIX B
RESULTS OF ANALYTICAL TESTING BY
SGS OF NORTH AMERICA INC.
OF ANCHORAGE, ALASKA AND
ADEC LABORATORY DATA REVIEW CHECKLISTS
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SGS North America Environmental Services – Alaska DivisionClient Services/Continuous Improvement Lead
Heather L. Hall 2011.07.0115:31:51 -08'00'
CASE NARRATIVE Print Date: 7/1/2011
Workorder No.: 1112835
Project Name: 32-1-17172-006 4115 Lake Otis
Client Name: Shannon & Wilson, Inc.
Lab Sample ID
Sample Comments
Sample Type Client Sample ID
Refer to the sample receipt form for information on sample condition.
1035306
8260B - LCS recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCS LCS for HBN 1216746 [VXX/22361*
1035307
8260B - LCSD recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCSD LCSD for HBN 1216746 [VXX/2236*
1035312
8260B - CCV recovery for multiple analytes does not meet QC criteria (biased high). These analytes were not detected
above the LOQ in the associated samples.
CCV CCV for HBN 1216748 [VMS/12198*
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
SG S N o rth A m eric a Inc . En vir onm enta l D ivis ion 200 W e st Pot ter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs .com M em ber of SG S Group
32-1-17172-006 4115 Lake Otis
Project Manager
Steve Crupi
T: (907) 561-2120 F:
Attn: Jake Gano
5430 Fairbanks St., Ste. 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1112835
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SG S Group
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 7/1/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-006 4115 Lake Otis
Workorder No.: 1112835
Analytical Methods
Method Description Analytical Method
Volatile Organic Compounds (W) FULL SW8260B
Print Date: 7/1/2011 2:31 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1112835001 17172-006-DS1
1112835002 17172-006-WTB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Print Date: 7/1/2011 2:31 pmDetectable Results Summary
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L912Toluene
ug/L0.800JEthylbenzene
ug/L6.12n-Butylbenzene
ug/L1081,3,5-Trimethylbenzene
ug/L23.54-Isopropyltoluene
ug/L0.660Jn-Propylbenzene
ug/L0.330JStyrene
ug/L1.59sec-Butylbenzene
ug/L15.8P & M -Xylene
ug/L2.21Naphthalene
ug/L26.9o-Xylene
ug/L42.7Xylenes (total)
ug/L98.0J1,2,4-Trimethylbenzene
ug/L1.66tert-Butylbenzene
ug/L0.840JIsopropylbenzene (Cumene)
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L4.15JMethylene chloride
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 98.0J 100 ug/L VMS12198 VXX2236131.0 100
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 108 100 ug/L VMS12198 VXX2236131.0 100
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 23.5 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.800J 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.840J 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 2.00 U 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 2.21 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 6.12 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.660J 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 26.9 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 15.8 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 1.59 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.330J 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 1.66 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 912 100 ug/L VMS12198 VXX2236131.0 100
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 42.7 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 99.7 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 103 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 100 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:55
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 1 Analyst: JPI
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 18:15
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 100 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 4.15J 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 105 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 92.7 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 98.7 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:28
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835002-A
Dilution Factor: 1 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,1-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,2-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 06/30/110.620
1,2-Dibromoethane 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichloropropane 0.240 U 0.400 ug/L 06/30/110.120
1,4-Dichlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
2,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
2-Butanone (MEK) 6.20 U 10.0 ug/L 06/30/113.10
2-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
2-Hexanone 6.20 U 10.0 ug/L 06/30/113.10
4-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Isopropyltoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 06/30/113.10
Benzene 0.240 U 0.400 ug/L 06/30/110.120
Bromobenzene 0.620 U 1.00 ug/L 06/30/110.310
Bromochloromethane 0.620 U 1.00 ug/L 06/30/110.310
Bromodichloromethane 0.300 U 0.500 ug/L 06/30/110.150
Bromoform 0.620 U 1.00 ug/L 06/30/110.310
Bromomethane 1.88 U 3.00 ug/L 06/30/110.940
Carbon disulfide 1.24 U 2.00 ug/L 06/30/110.620
Carbon tetrachloride 0.620 U 1.00 ug/L 06/30/110.310
Chlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
Chloroethane 0.620 U 1.00 ug/L 06/30/110.310
Chloroform 0.600 U 1.00 ug/L 06/30/110.300
Chloromethane 0.620 U 1.00 ug/L 06/30/110.310
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 06/30/110.150
Dibromochloromethane 0.300 U 0.500 ug/L 06/30/110.150
Dibromomethane 0.620 U 1.00 ug/L 06/30/110.310
Dichlorodifluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Ethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Hexachlorobutadiene 0.620 U 1.00 ug/L 06/30/110.310
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 06/30/110.310
Methylene chloride 2.00 U 5.00 ug/L 06/30/111.00
Methyl-t-butyl ether 3.00 U 5.00 ug/L 06/30/111.50
Naphthalene 1.24 U 2.00 ug/L 06/30/110.620
n-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
n-Propylbenzene 0.620 U 1.00 ug/L 06/30/110.310
o-Xylene 0.620 U 1.00 ug/L 06/30/110.310
P & M -Xylene 1.24 U 2.00 ug/L 06/30/110.620
sec-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Styrene 0.620 U 1.00 ug/L 06/30/110.310
tert-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Tetrachloroethene 0.620 U 1.00 ug/L 06/30/110.310
Toluene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
Trichloroethene 0.620 U 1.00 ug/L 06/30/110.310
Trichlorofluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Vinyl chloride 0.620 U 1.00 ug/L 06/30/110.310
Xylenes (total) 1.88 U 3.00 ug/L 06/30/110.940
Surrogates
1,2-Dichloroethane-D4 <surr> 109 70-120 % 06/30/11
4-Bromofluorobenzene <surr> 94.3 75-120 % 06/30/11
Toluene-d8 <surr> 99.4 85-120 % 06/30/11
Instrument
Method
Batch VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane LCS 33.7 112 ( 80-130 ) 30 ug/L 06/30/2011
LCSD 34.5 115 2 (< 20 ) 30 ug/L 06/30/2011
1,1,1-Trichloroethane LCS 35.1 117 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 35.9 120 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2,2-Tetrachloroethane LCS 28.8 96 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 29.4 98 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2-Trichloroethane LCS 30.2 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.8 103 2 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethane LCS 33.5 112 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 33.8 113 1 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethene LCS 35.4 118 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.5 125 6 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloropropene LCS 33.5 112 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 34.4 115 3 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichlorobenzene LCS 31.4 105 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 33.0 110 5 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichloropropane LCS 30.0 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 0 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trichlorobenzene LCS 31.9 106 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trimethylbenzene LCS 30.2 101 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromo-3-chloropropane LCS 29.3 98 ( 50-130 ) 30 ug/L 06/30/2011
LCSD 29.6 99 1 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromoethane LCS 33.1 110 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 0 (< 20 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,2-Dichlorobenzene LCS 29.9 100 ( 70-120 ) 30 ug/L 06/30/2011
LCSD 30.9 103 3 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloroethane LCS 33.5 112 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 33.7 112 0 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloropropane LCS 32.1 107 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 32.5 108 1 (< 20 ) 30 ug/L 06/30/2011
1,3,5-Trimethylbenzene LCS 29.9 100 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 3 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichlorobenzene LCS 29.8 99 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.0 103 4 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichloropropane LCS 30.1 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 1 (< 20 ) 30 ug/L 06/30/2011
1,4-Dichlorobenzene LCS 30.4 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
2,2-Dichloropropane LCS 37.5 125 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 39.0 130 4 (< 20 ) 30 ug/L 06/30/2011
2-Butanone (MEK) LCS 102 114 ( 30-150 ) 90 ug/L 06/30/2011
LCSD 118 131 14 (< 20 ) 90 ug/L 06/30/2011
2-Chlorotoluene LCS 29.1 97 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.1 100 3 (< 20 ) 30 ug/L 06/30/2011
2-Hexanone LCS 86.5 96 ( 55-130 ) 90 ug/L 06/30/2011
LCSD 93.0 103 7 (< 20 ) 90 ug/L 06/30/2011
4-Chlorotoluene LCS 28.9 96 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 30.3 101 5 (< 20 ) 30 ug/L 06/30/2011
4-Isopropyltoluene LCS 31.7 106 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
4-Methyl-2-pentanone (MIBK) LCS 111 123 ( 60-135 ) 90 ug/L 06/30/2011
LCSD 113 125 2 (< 20 ) 90 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Benzene LCS 32.8 109 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.2 111 1 (< 20 ) 30 ug/L 06/30/2011
Bromobenzene LCS 30.6 102 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 3 (< 20 ) 30 ug/L 06/30/2011
Bromochloromethane LCS 36.6 122 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 37.1 124 1 (< 20 ) 30 ug/L 06/30/2011
Bromodichloromethane LCS 33.9 113 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 34.0 113 0 (< 20 ) 30 ug/L 06/30/2011
Bromoform LCS 36.5 122 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.6 125 3 (< 20 ) 30 ug/L 06/30/2011
Bromomethane LCS 45.1 150 ( 30-145 )* 30 ug/L 06/30/2011
LCSD 45.2 151 * 0 (< 20 ) 30 ug/L 06/30/2011
Carbon disulfide LCS 49.4 110 ( 35-160 ) 45 ug/L 06/30/2011
LCSD 49.7 110 1 (< 20 ) 45 ug/L 06/30/2011
Carbon tetrachloride LCS 36.1 120 ( 65-140 ) 30 ug/L 06/30/2011
LCSD 36.6 122 2 (< 20 ) 30 ug/L 06/30/2011
Chlorobenzene LCS 32.3 108 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 3 (< 20 ) 30 ug/L 06/30/2011
Chloroethane LCS 32.5 108 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 32.7 109 1 (< 20 ) 30 ug/L 06/30/2011
Chloroform LCS 33.6 112 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.0 113 1 (< 20 ) 30 ug/L 06/30/2011
Chloromethane LCS 31.3 104 ( 40-125 ) 30 ug/L 06/30/2011
LCSD 31.5 105 1 (< 20 ) 30 ug/L 06/30/2011
cis-1,2-Dichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.7 119 0 (< 20 ) 30 ug/L 06/30/2011
cis-1,3-Dichloropropene LCS 35.5 118 ( 70-130 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 35.5 118 0 (< 20 ) 30 ug/L 06/30/2011
Dibromochloromethane LCS 34.3 114 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 34.9 116 2 (< 20 ) 30 ug/L 06/30/2011
Dibromomethane LCS 33.5 112 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.6 112 0 (< 20 ) 30 ug/L 06/30/2011
Dichlorodifluoromethane LCS 38.0 127 ( 30-155 ) 30 ug/L 06/30/2011
LCSD 36.2 121 5 (< 20 ) 30 ug/L 06/30/2011
Ethylbenzene LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.8 113 2 (< 20 ) 30 ug/L 06/30/2011
Hexachlorobutadiene LCS 32.7 109 ( 50-140 ) 30 ug/L 06/30/2011
LCSD 34.6 115 6 (< 20 ) 30 ug/L 06/30/2011
Isopropylbenzene (Cumene) LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.9 113 2 (< 20 ) 30 ug/L 06/30/2011
Methylene chloride LCS 30.9 103 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 30.7 102 1 (< 20 ) 30 ug/L 06/30/2011
Methyl-t-butyl ether LCS 51.8 115 ( 65-125 ) 45 ug/L 06/30/2011
LCSD 50.7 113 2 (< 20 ) 45 ug/L 06/30/2011
Naphthalene LCS 31.7 106 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.3 108 2 (< 20 ) 30 ug/L 06/30/2011
n-Butylbenzene LCS 30.1 100 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 31.5 105 5 (< 20 ) 30 ug/L 06/30/2011
n-Propylbenzene LCS 30.2 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
o-Xylene LCS 33.7 112 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 34.1 114 1 (< 20 ) 30 ug/L 06/30/2011
P & M -Xylene LCS 66.9 112 ( 75-130 ) 60 ug/L 06/30/2011
LCSD 67.3 112 1 (< 20 ) 60 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
sec-Butylbenzene LCS 30.4 101 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 4 (< 20 ) 30 ug/L 06/30/2011
Styrene LCS 34.1 114 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.6 115 2 (< 20 ) 30 ug/L 06/30/2011
tert-Butylbenzene LCS 30.4 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
Tetrachloroethene LCS 34.7 116 ( 45-150 ) 30 ug/L 06/30/2011
LCSD 35.4 118 2 (< 20 ) 30 ug/L 06/30/2011
Toluene LCS 31.8 106 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 31.9 106 0 (< 20 ) 30 ug/L 06/30/2011
trans-1,2-Dichloroethene LCS 34.7 116 ( 60-140 ) 30 ug/L 06/30/2011
LCSD 36.1 120 4 (< 20 ) 30 ug/L 06/30/2011
trans-1,3-Dichloropropene LCS 32.7 109 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.8 109 0 (< 20 ) 30 ug/L 06/30/2011
Trichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.9 120 1 (< 20 ) 30 ug/L 06/30/2011
Trichlorofluoromethane LCS 37.1 124 ( 60-145 ) 30 ug/L 06/30/2011
LCSD 36.6 122 1 (< 20 ) 30 ug/L 06/30/2011
Vinyl chloride LCS 34.4 115 ( 50-145 ) 30 ug/L 06/30/2011
LCSD 33.7 112 2 (< 20 ) 30 ug/L 06/30/2011
Xylenes (total) LCS 101 112 ( 80-120 ) 90 ug/L 06/30/2011
LCSD 101 113 1 (< 20 ) 90 ug/L 06/30/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 104 ( 70-120 ) 06/30/2011
LCSD 102 2 06/30/2011
4-Bromofluorobenzene <surr> LCS 95 ( 75-120 ) 06/30/2011
LCSD 94 0 06/30/2011
Toluene-d8 <surr> LCS 99 ( 85-120 ) 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 98 1 06/30/2011
Batch
Method
Instrument
VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: July 1, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1112835 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments:
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 9.5° C
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO,
BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No discrepancies noted.
e. Data quality or usability affected? (Please Explain.)
Comments: The sample was collected approximately 30 minutes before the temperature was measured at the laboratory. It is our opinion that because the samples was collected shortly before being submitted, the temperature does not affect the quality or usability of the data.
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: LCS and LSCD recoveries for bromomethane and methyl iodide are outside QC criteria (biased high). CCV recoveries for several analytes do not meet QC criteria (biased high).
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: Case narrative does not comment on data quality or usability.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments:
b. All applicable holding times met? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 3 of 6
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.)
Comments:
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection level for the project? Yes / No / NA (Please explain.) Comments: LODs are greater than the ADEC groundwater standard for several VOC analytes. However, the results are used for disposal characterization; the results are still usable for this purpose.
e. Data quality or usability affected? (Please explain.) Comments: The data are usable for the purposed of disposal characterization.
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments:
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments:
iii. If above LOQ, what samples are affected? NA
Comments:
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments:
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: Data quality or usability is not affected.
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments:
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.)
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 4 of 6
Comments:
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments: LCS/LCSD recoveries for bromomethane are outside of QC criteria (biased high). Also, according to the case narrative LCS/LCSD recoveries for methyl iodide are biased high, although the results of this analyte are not included with the suite of VOCs on this report.
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments: The analytes were not detected in the project samples.
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: Data quality or usability is not affected.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory samples? Yes / No / NA (Please explain.) Comments:
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments:
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 5 of 6
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Methylene chloride was detected at a concentration less than the LOQ.
iv. If above LOQ, what samples are affected? NA Comments:
v. Data quality or usability affected? . Comments: Methylene chloride is a common lab contaminant and was not detected in the project sample. It is our opinion that the detection was likely due to contamination at the lab. Data quality or usability is not affected.
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.) Comments: Field duplicates were not submitted for disposal characterization samples.
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 6 of 6
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Not decontamination or equipment blank submitted due to our use of disposable sampling equipment.
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments:
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SGS North America Environmental Services – Alaska DivisionProject Manager
Steven Crupi 2011.06.22 17:11:06 -08'00'
CASE NARRATIVE Print Date: 6/22/2011
Workorder No.: 1112386
Project Name: 32-1-17172-6 4501 Lake Otis
Client Name: Shannon & Wilson, Inc.
Lab Sample ID
Sample Comments
Sample Type Client Sample ID
Refer to the sample receipt form for information on sample condition.
1112386001
AK102/103 - Unknown hydrocarbon with several peaks is present.
PS 17172-6-D1S3
1112386002
AK103 - Unknown hydrocarbon with several peaks is present.
PS 17172-6-D2S3
1112386003
AK103 - Unknown hydrocarbon with several peaks is present.
PS 17172-6-D3S2
1112386004
AK102/103 - Unknown hydrocarbon with several peaks is present.
PS 17172-6-D3S4
1032210
8270D SIM - Anthracene was detected in the MB at 6.25 ug/Kg. Anthracene concentrations detected in the associated
samples are either below the LOQ or greater than ten times the amount found in the blank.
MB MB for HBN 1214836 [XXX/24925]*
1032214
8270D SIM - MS recoveries for multiple analytes are outside of QC criteria because the PAH concentrations present in the
sample are significantly greater than the amounts spiked for this QC sample. Refer to the LCS for accuracy information.
MS 11UNA-25D-TS2...(1112492085MS)*
1032215
8270D SIM - MSD recoveries for multiple analytes are outside of QC criteria because the PAH concentrations present in the
sample are significantly greater than the amounts spiked for this QC sample. Refer to the LCS for accuracy information.
8270D SIM- MS/MSD RPDs for multiple analytes do not meet QC criteria. Results for these analytes are estimated in the
original sample, where detected.
MSD 11UNA-25D-TS...(1112492085MSD)*
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
SG S N o rth A m eric a Inc . En vir onm enta l D ivis ion 200 W e st Pot ter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs .com M em ber of SG S Group
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Print Date: 6/22/2011 5:04 pmReport of Manual Integrations
Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason
1112386003 17172-6-D3S2 XMS6007 8270D SIMS (PAH)Benzo[b]Fluoranthene SP
1112386003 17172-6-D3S2 XMS6007 8270D SIMS (PAH)Benzo[k]fluoranthene PNF
Manual Integration Reason Code Descriptions
Code Description
O Original Chromatogram
M Modified Chromatogram
SS Skimmed surrogate
BLG Closed baseline gap
RP Reassign peak name
PIR Pattern integration required
IT Included tail
SP Split peak
RSP Removed split peak
FPS Forced peak start/stop
BLC Baseline correction
PNF Peak not found by software
All DRO/RRO analysis are integrated per SOP.
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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32-1-17172-6 4501 Lake Otis
Project Manager
Steve Crupi
T: (907) 561-2120 F:
Attn: Jake Gano
5430 Fairbanks St., Ste. 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1112386
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SGS Group
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Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 6/22/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-6 4501 Lake Otis
Workorder No.: 1112386
Analytical Methods
Method Description Analytical Method
8270 PAH SIM Semi-Volatiles GC/MS 8270D SIMS (PAH)
Diesel/Residual Range Organics AK102
Diesel/Residual Range Organics AK103
Gasoline Range Organics (S) AK101
Percent Solids SM2540G SM20 2540G
VOC 8260 (S) Field Extracted SW8260B
Print Date: 6/22/2011 5:04 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1112386001 17172-6-D1S3
1112386002 17172-6-D2S3
1112386003 17172-6-D3S2
1112386004 17172-6-D3S4
1112386005 17172-6-STB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Print Date: 6/22/2011 5:04 pmDetectable Results Summary
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Result UnitsParameter
Semivolatile Organic Fuels Department
mg/Kg68.8Diesel Range Organics
mg/Kg211Residual Range Organics
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Result UnitsParameter
Semivolatile Organic Fuels Department
mg/Kg42.8Residual Range Organics
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Result UnitsParameter
Semivolatile Organic Fuels Department
mg/Kg19.7JDiesel Range Organics
mg/Kg101Residual Range Organics
Polynuclear Aromatics GC/MS
ug/Kg5.38Phenanthrene
ug/Kg1.60JAnthracene
ug/Kg8.43Fluoranthene
ug/Kg9.09Pyrene
ug/Kg10.8Benzo(a)Anthracene
ug/Kg14.7Chrysene
ug/Kg12.0Benzo[b]Fluoranthene
ug/Kg2.55JBenzo[k]fluoranthene
ug/Kg12.3Benzo[a]pyrene
ug/Kg4.36JIndeno[1,2,3-c,d] pyrene
ug/Kg1.84JDibenzo[a,h]anthracene
ug/Kg8.03Benzo[g,h,i]perylene
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Result UnitsParameter
Semivolatile Organic Fuels Department
mg/Kg23.8Diesel Range Organics
mg/Kg136Residual Range Organics
Client Sample ID: 17172-6-STB
SGS Ref. #: 1112386005 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/Kg50.6JCarbon disulfide
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Fuels Department
DL DF
Gasoline Range Organics 2.54 U 4.25 mg/Kg VFC105141.27 1
4-Bromofluorobenzene <surr> 100 50-150 % VFC105141
Batch Information
Initial Prep Wt./Vol.: 40.614 gAnalytical Batch: VFC10514
Analytical Method: AK101
Analysis Date/Time: 06/10/11 17:16 Container ID:1112386001-B
Dilution Factor: 1 Analyst: EAB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Semivolatile Organic Fuels Department
DL DF
Diesel Range Organics 68.8 22.6 mg/Kg XFC9853 XXX248766.99 1
Residual Range Organics 211 22.6 mg/Kg XFC9853 XXX248766.99 1
5a Androstane <surr> 87.4 50-150 % XFC9853 XXX248761
n-Triacontane-d62 <surr> 96 50-150 % XFC9853 XXX248761
Batch Information
Initial Prep Wt./Vol.: 30.455 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK102
Analysis Date/Time: 06/13/11 20:38
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386001-A
Dilution Factor: 1 Analyst: MCS
Initial Prep Wt./Vol.: 30.455 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK103
Analysis Date/Time: 06/13/11 20:38
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386001-A
Dilution Factor: 1 Analyst: MCS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,1,1-Trichloroethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,1,2,2-Tetrachloroethane 51.0 U 84.9 ug/Kg VMS1214125.5 1
1,1,2-Trichloroethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,1-Dichloroethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,1-Dichloroethene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,1-Dichloropropene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2,3-Trichlorobenzene 51.0 U 84.9 ug/Kg VMS1214125.5 1
1,2,3-Trichloropropane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2,4-Trichlorobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2,4-Trimethylbenzene 51.0 U 84.9 ug/Kg VMS1214125.5 1
1,2-Dibromo-3-chloropropane 105 U 170 ug/Kg VMS1214152.7 1
1,2-Dibromoethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2-Dichlorobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2-Dichloroethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,2-Dichloropropane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,3,5-Trimethylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,3-Dichlorobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,3-Dichloropropane 26.4 U 42.5 ug/Kg VMS1214113.2 1
1,4-Dichlorobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
2,2-Dichloropropane 26.4 U 42.5 ug/Kg VMS1214113.2 1
2-Butanone (MEK) 264 U 425 ug/Kg VMS12141132 1
2-Chlorotoluene 26.4 U 42.5 ug/Kg VMS1214113.2 1
2-Hexanone 264 U 425 ug/Kg VMS12141132 1
4-Chlorotoluene 26.4 U 42.5 ug/Kg VMS1214113.2 1
4-Isopropyltoluene 26.4 U 42.5 ug/Kg VMS1214113.2 1
4-Methyl-2-pentanone (MIBK) 264 U 425 ug/Kg VMS12141132 1
Benzene 13.2 U 21.2 ug/Kg VMS121416.62 1
Bromobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Bromochloromethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
Bromodichloromethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
Bromoform 26.4 U 42.5 ug/Kg VMS1214113.2 1
Bromomethane 210 U 340 ug/Kg VMS12141105 1
Carbon disulfide 105 U 170 ug/Kg VMS1214152.7 1
Carbon tetrachloride 26.4 U 42.5 ug/Kg VMS1214113.2 1
Chlorobenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 210 U 340 ug/Kg VMS12141105 1
Chloroform 26.4 U 42.5 ug/Kg VMS1214113.2 1
Chloromethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
cis-1,2-Dichloroethene 26.4 U 42.5 ug/Kg VMS1214113.2 1
cis-1,3-Dichloropropene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Dibromochloromethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
Dibromomethane 26.4 U 42.5 ug/Kg VMS1214113.2 1
Dichlorodifluoromethane 51.0 U 84.9 ug/Kg VMS1214125.5 1
Ethylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Hexachlorobutadiene 51.0 U 84.9 ug/Kg VMS1214125.5 1
Isopropylbenzene (Cumene) 26.4 U 42.5 ug/Kg VMS1214113.2 1
Methylene chloride 105 U 170 ug/Kg VMS1214152.7 1
Methyl-t-butyl ether 105 U 170 ug/Kg VMS1214152.7 1
Naphthalene 51.0 U 84.9 ug/Kg VMS1214125.5 1
n-Butylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
n-Propylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
o-Xylene 51.0 U 84.9 ug/Kg VMS1214125.5 1
P & M -Xylene 51.0 U 84.9 ug/Kg VMS1214125.5 1
sec-Butylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Styrene 26.4 U 42.5 ug/Kg VMS1214113.2 1
tert-Butylbenzene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Tetrachloroethene 13.2 U 21.2 ug/Kg VMS121416.62 1
Toluene 51.0 U 84.9 ug/Kg VMS1214125.5 1
trans-1,2-Dichloroethene 26.4 U 42.5 ug/Kg VMS1214113.2 1
trans-1,3-Dichloropropene 26.4 U 42.5 ug/Kg VMS1214113.2 1
Trichloroethene 13.2 U 21.2 ug/Kg VMS121416.62 1
Trichlorofluoromethane 51.0 U 84.9 ug/Kg VMS1214125.5 1
Vinyl chloride 26.4 U 42.5 ug/Kg VMS1214113.2 1
Xylenes (total) 105 U 170 ug/Kg VMS1214152.7 1
1,2-Dichloroethane-D4 <surr> 98.3 80-117 % VMS121411
4-Bromofluorobenzene <surr> 92.4 68-136 % VMS121411
Toluene-d8 <surr> 98.9 85-121 % VMS121411
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
11 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 40.614 gAnalytical Batch: VMS12141
Analytical Method: SW8260B
Analysis Date/Time: 06/12/11 20:14 Container ID:1112386001-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
12 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D1S3
SGS Ref. #: 1112386001 Collection Date/Time: 06/09/11 09:30
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 87.4
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Solids
DL DF
Total Solids 87.4 % SPT83971
Batch Information
Initial Prep Wt./Vol.: 1 mLAnalytical Batch: SPT8397
Analytical Method: SM20 2540G
Analysis Date/Time: 06/11/11 13:30 Container ID:1112386001-A
Dilution Factor: 1 Analyst: DDR
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
13 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Fuels Department
DL DF
Gasoline Range Organics 1.91 U 3.19 mg/Kg VFC105140.956 1
4-Bromofluorobenzene <surr> 107 50-150 % VFC105141
Batch Information
Initial Prep Wt./Vol.: 49.562 gAnalytical Batch: VFC10514
Analytical Method: AK101
Analysis Date/Time: 06/10/11 17:34 Container ID:1112386002-B
Dilution Factor: 1 Analyst: EAB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
14 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Semivolatile Organic Fuels Department
DL DF
Diesel Range Organics 13.5 U 21.7 mg/Kg XFC9853 XXX248766.73 1
Residual Range Organics 42.8 21.7 mg/Kg XFC9853 XXX248766.73 1
5a Androstane <surr> 87.6 50-150 % XFC9853 XXX248761
n-Triacontane-d62 <surr> 95.5 50-150 % XFC9853 XXX248761
Batch Information
Initial Prep Wt./Vol.: 30.086 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK102
Analysis Date/Time: 06/13/11 19:56
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386002-A
Dilution Factor: 1 Analyst: MCS
Initial Prep Wt./Vol.: 30.086 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK103
Analysis Date/Time: 06/13/11 19:56
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386002-A
Dilution Factor: 1 Analyst: MCS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
15 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,1,1-Trichloroethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,1,2,2-Tetrachloroethane 38.2 U 63.8 ug/Kg VMS1214119.1 1
1,1,2-Trichloroethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,1-Dichloroethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,1-Dichloroethene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,1-Dichloropropene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2,3-Trichlorobenzene 38.2 U 63.8 ug/Kg VMS1214119.1 1
1,2,3-Trichloropropane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2,4-Trichlorobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2,4-Trimethylbenzene 38.2 U 63.8 ug/Kg VMS1214119.1 1
1,2-Dibromo-3-chloropropane 79.0 U 128 ug/Kg VMS1214139.5 1
1,2-Dibromoethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2-Dichlorobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2-Dichloroethane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,2-Dichloropropane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,3,5-Trimethylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,3-Dichlorobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
1,3-Dichloropropane 19.9 U 31.9 ug/Kg VMS121419.95 1
1,4-Dichlorobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
2,2-Dichloropropane 19.9 U 31.9 ug/Kg VMS121419.95 1
2-Butanone (MEK) 199 U 319 ug/Kg VMS1214199.5 1
2-Chlorotoluene 19.9 U 31.9 ug/Kg VMS121419.95 1
2-Hexanone 199 U 319 ug/Kg VMS1214199.5 1
4-Chlorotoluene 19.9 U 31.9 ug/Kg VMS121419.95 1
4-Isopropyltoluene 19.9 U 31.9 ug/Kg VMS121419.95 1
4-Methyl-2-pentanone (MIBK) 199 U 319 ug/Kg VMS1214199.5 1
Benzene 9.94 U 15.9 ug/Kg VMS121414.97 1
Bromobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
Bromochloromethane 19.9 U 31.9 ug/Kg VMS121419.95 1
Bromodichloromethane 19.9 U 31.9 ug/Kg VMS121419.95 1
Bromoform 19.9 U 31.9 ug/Kg VMS121419.95 1
Bromomethane 158 U 255 ug/Kg VMS1214179.1 1
Carbon disulfide 79.0 U 128 ug/Kg VMS1214139.5 1
Carbon tetrachloride 19.9 U 31.9 ug/Kg VMS121419.95 1
Chlorobenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
16 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 158 U 255 ug/Kg VMS1214179.1 1
Chloroform 19.9 U 31.9 ug/Kg VMS121419.95 1
Chloromethane 19.9 U 31.9 ug/Kg VMS121419.95 1
cis-1,2-Dichloroethene 19.9 U 31.9 ug/Kg VMS121419.95 1
cis-1,3-Dichloropropene 19.9 U 31.9 ug/Kg VMS121419.95 1
Dibromochloromethane 19.9 U 31.9 ug/Kg VMS121419.95 1
Dibromomethane 19.9 U 31.9 ug/Kg VMS121419.95 1
Dichlorodifluoromethane 38.2 U 63.8 ug/Kg VMS1214119.1 1
Ethylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
Hexachlorobutadiene 38.2 U 63.8 ug/Kg VMS1214119.1 1
Isopropylbenzene (Cumene) 19.9 U 31.9 ug/Kg VMS121419.95 1
Methylene chloride 79.0 U 128 ug/Kg VMS1214139.5 1
Methyl-t-butyl ether 79.0 U 128 ug/Kg VMS1214139.5 1
Naphthalene 38.2 U 63.8 ug/Kg VMS1214119.1 1
n-Butylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
n-Propylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
o-Xylene 38.2 U 63.8 ug/Kg VMS1214119.1 1
P & M -Xylene 38.2 U 63.8 ug/Kg VMS1214119.1 1
sec-Butylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
Styrene 19.9 U 31.9 ug/Kg VMS121419.95 1
tert-Butylbenzene 19.9 U 31.9 ug/Kg VMS121419.95 1
Tetrachloroethene 9.94 U 15.9 ug/Kg VMS121414.97 1
Toluene 38.2 U 63.8 ug/Kg VMS1214119.1 1
trans-1,2-Dichloroethene 19.9 U 31.9 ug/Kg VMS121419.95 1
trans-1,3-Dichloropropene 19.9 U 31.9 ug/Kg VMS121419.95 1
Trichloroethene 9.94 U 15.9 ug/Kg VMS121414.97 1
Trichlorofluoromethane 38.2 U 63.8 ug/Kg VMS1214119.1 1
Vinyl chloride 19.9 U 31.9 ug/Kg VMS121419.95 1
Xylenes (total) 79.0 U 128 ug/Kg VMS1214139.5 1
1,2-Dichloroethane-D4 <surr> 96.3 80-117 % VMS121411
4-Bromofluorobenzene <surr> 99.1 68-136 % VMS121411
Toluene-d8 <surr> 94.2 85-121 % VMS121411
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
17 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 49.562 gAnalytical Batch: VMS12141
Analytical Method: SW8260B
Analysis Date/Time: 06/12/11 19:43 Container ID:1112386002-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
18 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D2S3
SGS Ref. #: 1112386002 Collection Date/Time: 06/09/11 09:50
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 91.9
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Solids
DL DF
Total Solids 91.9 % SPT83971
Batch Information
Initial Prep Wt./Vol.: 1 mLAnalytical Batch: SPT8397
Analytical Method: SM20 2540G
Analysis Date/Time: 06/11/11 13:30 Container ID:1112386002-A
Dilution Factor: 1 Analyst: DDR
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
19 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Fuels Department
DL DF
Gasoline Range Organics 1.75 U 2.91 mg/Kg VFC105140.873 1
4-Bromofluorobenzene <surr> 101 50-150 % VFC105141
Batch Information
Initial Prep Wt./Vol.: 49.617 gAnalytical Batch: VFC10514
Analytical Method: AK101
Analysis Date/Time: 06/10/11 17:53 Container ID:1112386003-B
Dilution Factor: 1 Analyst: EAB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
20 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Semivolatile Organic Fuels Department
DL DF
Diesel Range Organics 19.7J 21.0 mg/Kg XFC9853 XXX248766.50 1
Residual Range Organics 101 21.0 mg/Kg XFC9853 XXX248766.50 1
5a Androstane <surr> 87.6 50-150 % XFC9853 XXX248761
n-Triacontane-d62 <surr> 96.1 50-150 % XFC9853 XXX248761
Batch Information
Initial Prep Wt./Vol.: 30.089 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK102
Analysis Date/Time: 06/13/11 20:17
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386003-A
Dilution Factor: 1 Analyst: MCS
Initial Prep Wt./Vol.: 30.089 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK103
Analysis Date/Time: 06/13/11 20:17
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386003-A
Dilution Factor: 1 Analyst: MCS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
21 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,1,1-Trichloroethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,1,2,2-Tetrachloroethane 35.0 U 58.2 ug/Kg VMS1214117.5 1
1,1,2-Trichloroethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,1-Dichloroethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,1-Dichloroethene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,1-Dichloropropene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2,3-Trichlorobenzene 35.0 U 58.2 ug/Kg VMS1214117.5 1
1,2,3-Trichloropropane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2,4-Trichlorobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2,4-Trimethylbenzene 35.0 U 58.2 ug/Kg VMS1214117.5 1
1,2-Dibromo-3-chloropropane 72.2 U 116 ug/Kg VMS1214136.1 1
1,2-Dibromoethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2-Dichlorobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2-Dichloroethane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,2-Dichloropropane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,3,5-Trimethylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,3-Dichlorobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
1,3-Dichloropropane 18.2 U 29.1 ug/Kg VMS121419.08 1
1,4-Dichlorobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
2,2-Dichloropropane 18.2 U 29.1 ug/Kg VMS121419.08 1
2-Butanone (MEK) 182 U 291 ug/Kg VMS1214190.8 1
2-Chlorotoluene 18.2 U 29.1 ug/Kg VMS121419.08 1
2-Hexanone 182 U 291 ug/Kg VMS1214190.8 1
4-Chlorotoluene 18.2 U 29.1 ug/Kg VMS121419.08 1
4-Isopropyltoluene 18.2 U 29.1 ug/Kg VMS121419.08 1
4-Methyl-2-pentanone (MIBK) 182 U 291 ug/Kg VMS1214190.8 1
Benzene 9.08 U 14.6 ug/Kg VMS121414.54 1
Bromobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
Bromochloromethane 18.2 U 29.1 ug/Kg VMS121419.08 1
Bromodichloromethane 18.2 U 29.1 ug/Kg VMS121419.08 1
Bromoform 18.2 U 29.1 ug/Kg VMS121419.08 1
Bromomethane 144 U 233 ug/Kg VMS1214172.2 1
Carbon disulfide 72.2 U 116 ug/Kg VMS1214136.1 1
Carbon tetrachloride 18.2 U 29.1 ug/Kg VMS121419.08 1
Chlorobenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
22 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 144 U 233 ug/Kg VMS1214172.2 1
Chloroform 18.2 U 29.1 ug/Kg VMS121419.08 1
Chloromethane 18.2 U 29.1 ug/Kg VMS121419.08 1
cis-1,2-Dichloroethene 18.2 U 29.1 ug/Kg VMS121419.08 1
cis-1,3-Dichloropropene 18.2 U 29.1 ug/Kg VMS121419.08 1
Dibromochloromethane 18.2 U 29.1 ug/Kg VMS121419.08 1
Dibromomethane 18.2 U 29.1 ug/Kg VMS121419.08 1
Dichlorodifluoromethane 35.0 U 58.2 ug/Kg VMS1214117.5 1
Ethylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
Hexachlorobutadiene 35.0 U 58.2 ug/Kg VMS1214117.5 1
Isopropylbenzene (Cumene) 18.2 U 29.1 ug/Kg VMS121419.08 1
Methylene chloride 72.2 U 116 ug/Kg VMS1214136.1 1
Methyl-t-butyl ether 72.2 U 116 ug/Kg VMS1214136.1 1
Naphthalene 35.0 U 58.2 ug/Kg VMS1214117.5 1
n-Butylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
n-Propylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
o-Xylene 35.0 U 58.2 ug/Kg VMS1214117.5 1
P & M -Xylene 35.0 U 58.2 ug/Kg VMS1214117.5 1
sec-Butylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
Styrene 18.2 U 29.1 ug/Kg VMS121419.08 1
tert-Butylbenzene 18.2 U 29.1 ug/Kg VMS121419.08 1
Tetrachloroethene 9.08 U 14.6 ug/Kg VMS121414.54 1
Toluene 35.0 U 58.2 ug/Kg VMS1214117.5 1
trans-1,2-Dichloroethene 18.2 U 29.1 ug/Kg VMS121419.08 1
trans-1,3-Dichloropropene 18.2 U 29.1 ug/Kg VMS121419.08 1
Trichloroethene 9.08 U 14.6 ug/Kg VMS121414.54 1
Trichlorofluoromethane 35.0 U 58.2 ug/Kg VMS1214117.5 1
Vinyl chloride 18.2 U 29.1 ug/Kg VMS121419.08 1
Xylenes (total) 72.2 U 116 ug/Kg VMS1214136.1 1
1,2-Dichloroethane-D4 <surr> 91.6 80-117 % VMS121411
4-Bromofluorobenzene <surr> 92.4 68-136 % VMS121411
Toluene-d8 <surr> 93.4 85-121 % VMS121411
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
23 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 49.617 gAnalytical Batch: VMS12141
Analytical Method: SW8260B
Analysis Date/Time: 06/12/11 19:12 Container ID:1112386003-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
24 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Polynuclear Aromatics GC/MS
DL DF
1-Methylnaphthalene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
2-Methylnaphthalene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
Acenaphthene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
Acenaphthylene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
Anthracene 1.60J 5.24 ug/Kg XMS6007 XXX249251.57 1
Benzo(a)Anthracene 10.8 5.24 ug/Kg XMS6007 XXX249251.57 1
Benzo[a]pyrene 12.3 5.24 ug/Kg XMS6007 XXX249251.57 1
Benzo[b]Fluoranthene 12.0 5.24 ug/Kg XMS6007 XXX249251.57 1
Benzo[g,h,i]perylene 8.03 5.24 ug/Kg XMS6007 XXX249251.57 1
Benzo[k]fluoranthene 2.55J 5.24 ug/Kg XMS6007 XXX249251.57 1
Chrysene 14.7 5.24 ug/Kg XMS6007 XXX249251.57 1
Dibenzo[a,h]anthracene 1.84J 5.24 ug/Kg XMS6007 XXX249251.57 1
Fluoranthene 8.43 5.24 ug/Kg XMS6007 XXX249251.57 1
Fluorene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
Indeno[1,2,3-c,d] pyrene 4.36J 5.24 ug/Kg XMS6007 XXX249251.57 1
Naphthalene 3.14 U 5.24 ug/Kg XMS6007 XXX249251.57 1
Phenanthrene 5.38 5.24 ug/Kg XMS6007 XXX249251.57 1
Pyrene 9.09 5.24 ug/Kg XMS6007 XXX249251.57 1
2-Fluorobiphenyl <surr> 84.1 45-105 % XMS6007 XXX249251
Terphenyl-d14 <surr> 92.7 30-125 % XMS6007 XXX249251
Batch Information
Initial Prep Wt./Vol.: 22.586 g
Prep Extract Vol.: 1 mL
Analytical Batch: XMS6007
Analytical Method: 8270D SIMS (PAH)
Analysis Date/Time: 06/18/11 05:16
Prep Batch: XXX24925
Prep Method: SW3550C
Prep Date/Time: 06/16/11 12:00 Container ID:1112386003-A
Dilution Factor: 1 Analyst: RTS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
25 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S2
SGS Ref. #: 1112386003 Collection Date/Time: 06/09/11 10:20
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 95.0
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Solids
DL DF
Total Solids 95.0 % SPT83971
Batch Information
Initial Prep Wt./Vol.: 1 mLAnalytical Batch: SPT8397
Analytical Method: SM20 2540G
Analysis Date/Time: 06/11/11 13:30 Container ID:1112386003-A
Dilution Factor: 1 Analyst: DDR
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
26 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Fuels Department
DL DF
Gasoline Range Organics 1.83 U 3.05 mg/Kg VFC105140.916 1
4-Bromofluorobenzene <surr> 102 50-150 % VFC105141
Batch Information
Initial Prep Wt./Vol.: 48.307 gAnalytical Batch: VFC10514
Analytical Method: AK101
Analysis Date/Time: 06/10/11 18:11 Container ID:1112386004-B
Dilution Factor: 1 Analyst: EAB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
27 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Semivolatile Organic Fuels Department
DL DF
Diesel Range Organics 23.8 21.0 mg/Kg XFC9853 XXX248766.52 1
Residual Range Organics 136 21.0 mg/Kg XFC9853 XXX248766.52 1
5a Androstane <surr> 82.7 50-150 % XFC9853 XXX248761
n-Triacontane-d62 <surr> 90.2 50-150 % XFC9853 XXX248761
Batch Information
Initial Prep Wt./Vol.: 30.297 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK102
Analysis Date/Time: 06/13/11 20:59
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386004-A
Dilution Factor: 1 Analyst: MCS
Initial Prep Wt./Vol.: 30.297 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC9853
Analytical Method: AK103
Analysis Date/Time: 06/13/11 20:59
Prep Batch: XXX24876
Prep Method: SW3550C
Prep Date/Time: 06/13/11 09:10 Container ID:1112386004-A
Dilution Factor: 1 Analyst: MCS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
28 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,1,1-Trichloroethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,1,2,2-Tetrachloroethane 36.6 U 61.1 ug/Kg VMS1214118.3 1
1,1,2-Trichloroethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,1-Dichloroethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,1-Dichloroethene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,1-Dichloropropene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2,3-Trichlorobenzene 36.6 U 61.1 ug/Kg VMS1214118.3 1
1,2,3-Trichloropropane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2,4-Trichlorobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2,4-Trimethylbenzene 36.6 U 61.1 ug/Kg VMS1214118.3 1
1,2-Dibromo-3-chloropropane 75.8 U 122 ug/Kg VMS1214137.9 1
1,2-Dibromoethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2-Dichlorobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2-Dichloroethane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,2-Dichloropropane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,3,5-Trimethylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,3-Dichlorobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
1,3-Dichloropropane 19.1 U 30.5 ug/Kg VMS121419.53 1
1,4-Dichlorobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
2,2-Dichloropropane 19.1 U 30.5 ug/Kg VMS121419.53 1
2-Butanone (MEK) 191 U 305 ug/Kg VMS1214195.3 1
2-Chlorotoluene 19.1 U 30.5 ug/Kg VMS121419.53 1
2-Hexanone 191 U 305 ug/Kg VMS1214195.3 1
4-Chlorotoluene 19.1 U 30.5 ug/Kg VMS121419.53 1
4-Isopropyltoluene 19.1 U 30.5 ug/Kg VMS121419.53 1
4-Methyl-2-pentanone (MIBK) 191 U 305 ug/Kg VMS1214195.3 1
Benzene 9.52 U 15.3 ug/Kg VMS121414.76 1
Bromobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
Bromochloromethane 19.1 U 30.5 ug/Kg VMS121419.53 1
Bromodichloromethane 19.1 U 30.5 ug/Kg VMS121419.53 1
Bromoform 19.1 U 30.5 ug/Kg VMS121419.53 1
Bromomethane 151 U 244 ug/Kg VMS1214175.7 1
Carbon disulfide 75.8 U 122 ug/Kg VMS1214137.9 1
Carbon tetrachloride 19.1 U 30.5 ug/Kg VMS121419.53 1
Chlorobenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
29 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 151 U 244 ug/Kg VMS1214175.7 1
Chloroform 19.1 U 30.5 ug/Kg VMS121419.53 1
Chloromethane 19.1 U 30.5 ug/Kg VMS121419.53 1
cis-1,2-Dichloroethene 19.1 U 30.5 ug/Kg VMS121419.53 1
cis-1,3-Dichloropropene 19.1 U 30.5 ug/Kg VMS121419.53 1
Dibromochloromethane 19.1 U 30.5 ug/Kg VMS121419.53 1
Dibromomethane 19.1 U 30.5 ug/Kg VMS121419.53 1
Dichlorodifluoromethane 36.6 U 61.1 ug/Kg VMS1214118.3 1
Ethylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
Hexachlorobutadiene 36.6 U 61.1 ug/Kg VMS1214118.3 1
Isopropylbenzene (Cumene) 19.1 U 30.5 ug/Kg VMS121419.53 1
Methylene chloride 75.8 U 122 ug/Kg VMS1214137.9 1
Methyl-t-butyl ether 75.8 U 122 ug/Kg VMS1214137.9 1
Naphthalene 36.6 U 61.1 ug/Kg VMS1214118.3 1
n-Butylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
n-Propylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
o-Xylene 36.6 U 61.1 ug/Kg VMS1214118.3 1
P & M -Xylene 36.6 U 61.1 ug/Kg VMS1214118.3 1
sec-Butylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
Styrene 19.1 U 30.5 ug/Kg VMS121419.53 1
tert-Butylbenzene 19.1 U 30.5 ug/Kg VMS121419.53 1
Tetrachloroethene 9.52 U 15.3 ug/Kg VMS121414.76 1
Toluene 36.6 U 61.1 ug/Kg VMS1214118.3 1
trans-1,2-Dichloroethene 19.1 U 30.5 ug/Kg VMS121419.53 1
trans-1,3-Dichloropropene 19.1 U 30.5 ug/Kg VMS121419.53 1
Trichloroethene 9.52 U 15.3 ug/Kg VMS121414.76 1
Trichlorofluoromethane 36.6 U 61.1 ug/Kg VMS1214118.3 1
Vinyl chloride 19.1 U 30.5 ug/Kg VMS121419.53 1
Xylenes (total) 75.8 U 122 ug/Kg VMS1214137.9 1
1,2-Dichloroethane-D4 <surr> 93.6 80-117 % VMS121411
4-Bromofluorobenzene <surr> 92.2 68-136 % VMS121411
Toluene-d8 <surr> 92.3 85-121 % VMS121411
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
30 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 48.307 gAnalytical Batch: VMS12141
Analytical Method: SW8260B
Analysis Date/Time: 06/12/11 18:41 Container ID:1112386004-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
31 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-D3S4
SGS Ref. #: 1112386004 Collection Date/Time: 06/09/11 10:25
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Percent Solids: 94.2
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Solids
DL DF
Total Solids 94.2 % SPT83971
Batch Information
Initial Prep Wt./Vol.: 1 mLAnalytical Batch: SPT8397
Analytical Method: SM20 2540G
Analysis Date/Time: 06/11/11 13:30 Container ID:1112386004-A
Dilution Factor: 1 Analyst: DDR
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
32 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-STB
SGS Ref. #: 1112386005 Collection Date/Time: 06/09/11 09:00
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Fuels Department
DL DF
Gasoline Range Organics 1.51 U 2.52 mg/Kg VFC105140.755 1
4-Bromofluorobenzene <surr> 94.7 50-150 % VFC105141
Batch Information
Initial Prep Wt./Vol.: 49.681 gAnalytical Batch: VFC10514
Analytical Method: AK101
Analysis Date/Time: 06/10/11 18:47 Container ID:1112386005-A
Dilution Factor: 1 Analyst: EAB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
33 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-STB
SGS Ref. #: 1112386005 Collection Date/Time: 06/09/11 09:00
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,1,1-Trichloroethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,1,2,2-Tetrachloroethane 30.2 U 50.3 ug/Kg VMS1214115.1 1
1,1,2-Trichloroethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,1-Dichloroethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,1-Dichloroethene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,1-Dichloropropene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2,3-Trichlorobenzene 30.2 U 50.3 ug/Kg VMS1214115.1 1
1,2,3-Trichloropropane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2,4-Trichlorobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2,4-Trimethylbenzene 30.2 U 50.3 ug/Kg VMS1214115.1 1
1,2-Dibromo-3-chloropropane 62.4 U 101 ug/Kg VMS1214131.2 1
1,2-Dibromoethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2-Dichlorobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2-Dichloroethane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,2-Dichloropropane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,3,5-Trimethylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,3-Dichlorobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
1,3-Dichloropropane 15.7 U 25.2 ug/Kg VMS121417.85 1
1,4-Dichlorobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
2,2-Dichloropropane 15.7 U 25.2 ug/Kg VMS121417.85 1
2-Butanone (MEK) 157 U 252 ug/Kg VMS1214178.5 1
2-Chlorotoluene 15.7 U 25.2 ug/Kg VMS121417.85 1
2-Hexanone 157 U 252 ug/Kg VMS1214178.5 1
4-Chlorotoluene 15.7 U 25.2 ug/Kg VMS121417.85 1
4-Isopropyltoluene 15.7 U 25.2 ug/Kg VMS121417.85 1
4-Methyl-2-pentanone (MIBK) 157 U 252 ug/Kg VMS1214178.5 1
Benzene 7.86 U 12.6 ug/Kg VMS121413.93 1
Bromobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
Bromochloromethane 15.7 U 25.2 ug/Kg VMS121417.85 1
Bromodichloromethane 15.7 U 25.2 ug/Kg VMS121417.85 1
Bromoform 15.7 U 25.2 ug/Kg VMS121417.85 1
Bromomethane 125 U 201 ug/Kg VMS1214162.4 1
Carbon disulfide 50.6J 101 ug/Kg VMS1214131.2 1
Carbon tetrachloride 15.7 U 25.2 ug/Kg VMS121417.85 1
Chlorobenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
34 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-STB
SGS Ref. #: 1112386005 Collection Date/Time: 06/09/11 09:00
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 125 U 201 ug/Kg VMS1214162.4 1
Chloroform 15.7 U 25.2 ug/Kg VMS121417.85 1
Chloromethane 15.7 U 25.2 ug/Kg VMS121417.85 1
cis-1,2-Dichloroethene 15.7 U 25.2 ug/Kg VMS121417.85 1
cis-1,3-Dichloropropene 15.7 U 25.2 ug/Kg VMS121417.85 1
Dibromochloromethane 15.7 U 25.2 ug/Kg VMS121417.85 1
Dibromomethane 15.7 U 25.2 ug/Kg VMS121417.85 1
Dichlorodifluoromethane 30.2 U 50.3 ug/Kg VMS1214115.1 1
Ethylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
Hexachlorobutadiene 30.2 U 50.3 ug/Kg VMS1214115.1 1
Isopropylbenzene (Cumene) 15.7 U 25.2 ug/Kg VMS121417.85 1
Methylene chloride 62.4 U 101 ug/Kg VMS1214131.2 1
Methyl-t-butyl ether 62.4 U 101 ug/Kg VMS1214131.2 1
Naphthalene 30.2 U 50.3 ug/Kg VMS1214115.1 1
n-Butylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
n-Propylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
o-Xylene 30.2 U 50.3 ug/Kg VMS1214115.1 1
P & M -Xylene 30.2 U 50.3 ug/Kg VMS1214115.1 1
sec-Butylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
Styrene 15.7 U 25.2 ug/Kg VMS121417.85 1
tert-Butylbenzene 15.7 U 25.2 ug/Kg VMS121417.85 1
Tetrachloroethene 7.86 U 12.6 ug/Kg VMS121413.93 1
Toluene 30.2 U 50.3 ug/Kg VMS1214115.1 1
trans-1,2-Dichloroethene 15.7 U 25.2 ug/Kg VMS121417.85 1
trans-1,3-Dichloropropene 15.7 U 25.2 ug/Kg VMS121417.85 1
Trichloroethene 7.86 U 12.6 ug/Kg VMS121413.93 1
Trichlorofluoromethane 30.2 U 50.3 ug/Kg VMS1214115.1 1
Vinyl chloride 15.7 U 25.2 ug/Kg VMS121417.85 1
Xylenes (total) 62.4 U 101 ug/Kg VMS1214131.2 1
1,2-Dichloroethane-D4 <surr> 92.2 80-117 % VMS121411
4-Bromofluorobenzene <surr> 86.5 68-136 % VMS121411
Toluene-d8 <surr> 91.7 85-121 % VMS121411
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
35 of 62
Shannon & Wilson, Inc. Print Date: 6/22/2011 5:04 pm
Client Sample ID: 17172-6-STB
SGS Ref. #: 1112386005 Collection Date/Time: 06/09/11 09:00
Receipt Date/Time: 06/09/11 12:24Project ID: 32-1-17172-6 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 49.681 gAnalytical Batch: VMS12141
Analytical Method: SW8260B
Analysis Date/Time: 06/12/11 17:39 Container ID:1112386005-A
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
36 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1030937 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004, 1112386005
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Fuels Department
Gasoline Range Organics 1.50 U 2.50 mg/Kg 06/10/110.750
Surrogates
4-Bromofluorobenzene <surr> 99.1 50-150 % 06/10/11
Instrument
Method
Batch VFC10514
AK101
Agilent 7890 PID/FID
37 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1030944 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Solids
Total Solids 100 % 06/11/11
Instrument
Method
Batch SPT8397
SM20 2540G
38 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1030951 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24876
SW3550C
06/13/2011
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Semivolatile Organic Fuels Department
Diesel Range Organics 12.4 U 20.0 mg/Kg 06/13/116.20
Surrogates
5a Androstane <surr> 82.8 60-120 % 06/13/11
Instrument
Method
Batch XFC9853
AK102
HP 7890A FID SV E F
Residual Range Organics 12.4 U 20.0 mg/Kg 06/13/116.20
Surrogates
n-Triacontane-d62 <surr> 94.6 60-120 % 06/13/11
Instrument
Method
Batch XFC9853
AK103
HP 7890A FID SV E F
39 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1031024 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004, 1112386005
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
40 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1031024 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,1,1-Trichloroethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,1,2,2-Tetrachloroethane 30.0 U 50.0 ug/Kg 06/12/1115.0
1,1,2-Trichloroethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,1-Dichloroethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,1-Dichloroethene 15.6 U 25.0 ug/Kg 06/12/117.80
1,1-Dichloropropene 15.6 U 25.0 ug/Kg 06/12/117.80
1,2,3-Trichlorobenzene 30.0 U 50.0 ug/Kg 06/12/1115.0
1,2,3-Trichloropropane 15.6 U 25.0 ug/Kg 06/12/117.80
1,2,4-Trichlorobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
1,2,4-Trimethylbenzene 30.0 U 50.0 ug/Kg 06/12/1115.0
1,2-Dibromo-3-chloropropane 62.0 U 100 ug/Kg 06/12/1131.0
1,2-Dibromoethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,2-Dichlorobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
1,2-Dichloroethane 15.6 U 25.0 ug/Kg 06/12/117.80
1,2-Dichloropropane 15.6 U 25.0 ug/Kg 06/12/117.80
1,3,5-Trimethylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
1,3-Dichlorobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
1,3-Dichloropropane 15.6 U 25.0 ug/Kg 06/12/117.80
1,4-Dichlorobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
2,2-Dichloropropane 15.6 U 25.0 ug/Kg 06/12/117.80
2-Butanone (MEK) 156 U 250 ug/Kg 06/12/1178.0
2-Chlorotoluene 15.6 U 25.0 ug/Kg 06/12/117.80
2-Hexanone 156 U 250 ug/Kg 06/12/1178.0
4-Chlorotoluene 15.6 U 25.0 ug/Kg 06/12/117.80
4-Isopropyltoluene 15.6 U 25.0 ug/Kg 06/12/117.80
4-Methyl-2-pentanone (MIBK) 156 U 250 ug/Kg 06/12/1178.0
Benzene 7.80 U 12.5 ug/Kg 06/12/113.90
Bromobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
Bromochloromethane 15.6 U 25.0 ug/Kg 06/12/117.80
Bromodichloromethane 15.6 U 25.0 ug/Kg 06/12/117.80
Bromoform 15.6 U 25.0 ug/Kg 06/12/117.80
Bromomethane 124 U 200 ug/Kg 06/12/1162.0
Carbon disulfide 62.0 U 100 ug/Kg 06/12/1131.0
Carbon tetrachloride 15.6 U 25.0 ug/Kg 06/12/117.80
Chlorobenzene 15.6 U 25.0 ug/Kg 06/12/117.80
Chloroethane 124 U 200 ug/Kg 06/12/1162.0
Chloroform 15.6 U 25.0 ug/Kg 06/12/117.80
Chloromethane 15.6 U 25.0 ug/Kg 06/12/117.8041 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1031024 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
cis-1,2-Dichloroethene 15.6 U 25.0 ug/Kg 06/12/117.80
cis-1,3-Dichloropropene 15.6 U 25.0 ug/Kg 06/12/117.80
Dibromochloromethane 15.6 U 25.0 ug/Kg 06/12/117.80
Dibromomethane 15.6 U 25.0 ug/Kg 06/12/117.80
Dichlorodifluoromethane 30.0 U 50.0 ug/Kg 06/12/1115.0
Ethylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
Hexachlorobutadiene 30.0 U 50.0 ug/Kg 06/12/1115.0
Isopropylbenzene (Cumene) 15.6 U 25.0 ug/Kg 06/12/117.80
Methylene chloride 62.0 U 100 ug/Kg 06/12/1131.0
Methyl-t-butyl ether 62.0 U 100 ug/Kg 06/12/1131.0
Naphthalene 30.0 U 50.0 ug/Kg 06/12/1115.0
n-Butylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
n-Propylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
o-Xylene 30.0 U 50.0 ug/Kg 06/12/1115.0
P & M -Xylene 30.0 U 50.0 ug/Kg 06/12/1115.0
sec-Butylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
Styrene 15.6 U 25.0 ug/Kg 06/12/117.80
tert-Butylbenzene 15.6 U 25.0 ug/Kg 06/12/117.80
Tetrachloroethene 7.80 U 12.5 ug/Kg 06/12/113.90
Toluene 30.0 U 50.0 ug/Kg 06/12/1115.0
trans-1,2-Dichloroethene 15.6 U 25.0 ug/Kg 06/12/117.80
trans-1,3-Dichloropropene 15.6 U 25.0 ug/Kg 06/12/117.80
Trichloroethene 7.80 U 12.5 ug/Kg 06/12/113.90
Trichlorofluoromethane 30.0 U 50.0 ug/Kg 06/12/1115.0
Vinyl chloride 15.6 U 25.0 ug/Kg 06/12/117.80
Xylenes (total) 62.0 U 100 ug/Kg 06/12/1131.0
Surrogates
1,2-Dichloroethane-D4 <surr> 85 80-117 % 06/12/11
4-Bromofluorobenzene <surr> 90.4 68-136 % 06/12/11
Toluene-d8 <surr> 91.8 85-121 % 06/12/11
Instrument
Method
Batch VMS12141
SW8260B
HP 5890 Series II MS5 VLA
42 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Prep
1032210 Method Blank
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24925
SW3550C
06/16/2011
QC results affect the following production samples:
1112386003
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Polynuclear Aromatics GC/MS
1-Methylnaphthalene 3.00 U 5.00 ug/Kg 06/16/111.50
2-Methylnaphthalene 3.00 U 5.00 ug/Kg 06/16/111.50
Acenaphthene 3.00 U 5.00 ug/Kg 06/16/111.50
Acenaphthylene 3.00 U 5.00 ug/Kg 06/16/111.50
Anthracene 6.25 5.00 ug/Kg 06/16/11* 1.50
Benzo(a)Anthracene 3.00 U 5.00 ug/Kg 06/16/111.50
Benzo[a]pyrene 3.00 U 5.00 ug/Kg 06/16/111.50
Benzo[b]Fluoranthene 3.00 U 5.00 ug/Kg 06/16/111.50
Benzo[g,h,i]perylene 3.00 U 5.00 ug/Kg 06/16/111.50
Benzo[k]fluoranthene 3.00 U 5.00 ug/Kg 06/16/111.50
Chrysene 3.00 U 5.00 ug/Kg 06/16/111.50
Dibenzo[a,h]anthracene 3.00 U 5.00 ug/Kg 06/16/111.50
Fluoranthene 3.00 U 5.00 ug/Kg 06/16/111.50
Fluorene 3.00 U 5.00 ug/Kg 06/16/111.50
Indeno[1,2,3-c,d] pyrene 3.00 U 5.00 ug/Kg 06/16/111.50
Naphthalene 2.36J 5.00 ug/Kg 06/16/111.50
Phenanthrene 3.00 U 5.00 ug/Kg 06/16/111.50
Pyrene 3.00 U 5.00 ug/Kg 06/16/111.50
Surrogates
2-Fluorobiphenyl <surr> 76.3 45-105 % 06/16/11
Terphenyl-d14 <surr> 125 30-125 % 06/16/11
Instrument
Method
Batch XMS6005
8270D SIMS (PAH)
HP 6890/5973 MS SVQA
43 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
DateOriginal
PrepShannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Duplicate1030945
Soil/Solid (dry weight)
1118385004
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004
ParameterQC
Result
Analysis
DateRPDRPD
LimitsOriginal
ResultUnits
Solids
88.0 92.0 % 4 (< 15 ) 06/11/2011Total Solids
Batch
Method
Instrument
SPT8397
SM20 2540G
44 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1030940 Lab Control Sample
1030941 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004, 1112386005
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Fuels Department
Gasoline Range Organics LCS 10.4 104 ( 60-120 ) 10.0 mg/Kg 06/10/2011
LCSD 10.5 105 1 (< 20 ) 10.0 mg/Kg 06/10/2011
Surrogates
4-Bromofluorobenzene <surr> LCS 101 ( 50-150 ) 06/10/2011
LCSD 102 1 06/10/2011
Batch
Method
Instrument
VFC10514
AK101
Agilent 7890 PID/FID
45 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1030952 Lab Control Sample
1030953 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24876
SW3550C
06/13/2011
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Semivolatile Organic Fuels Department
Diesel Range Organics LCS 154 92 ( 75-125 ) 167 mg/Kg 06/13/2011
LCSD 158 95 2 (< 20 ) 167 mg/Kg 06/13/2011
Surrogates
5a Androstane <surr> LCS 85 ( 60-120 ) 06/13/2011
LCSD 86 2 06/13/2011
Batch
Method
Instrument
XFC9853
AK102
HP 7890A FID SV E F
Residual Range Organics LCS 162 97 ( 60-120 ) 167 mg/Kg 06/13/2011
LCSD 163 98 1 (< 20 ) 167 mg/Kg 06/13/2011
Surrogates
n-Triacontane-d62 <surr> LCS 93 ( 60-120 ) 06/13/2011
LCSD 95 3 06/13/2011
Batch
Method
Instrument
XFC9853
AK103
HP 7890A FID SV E F
46 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1031025 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004, 1112386005
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
47 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1031025 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane LCS 721 96 ( 80-125 ) 750 ug/Kg 06/12/2011
1,1,1-Trichloroethane LCS 693 92 ( 80-127 ) 750 ug/Kg 06/12/2011
1,1,2,2-Tetrachloroethane LCS 707 94 ( 80-124 ) 750 ug/Kg 06/12/2011
1,1,2-Trichloroethane LCS 732 98 ( 80-124 ) 750 ug/Kg 06/12/2011
1,1-Dichloroethane LCS 676 90 ( 77-125 ) 750 ug/Kg 06/12/2011
1,1-Dichloroethene LCS 675 90 ( 65-150 ) 750 ug/Kg 06/12/2011
1,1-Dichloropropene LCS 685 91 ( 76-134 ) 750 ug/Kg 06/12/2011
1,2,3-Trichlorobenzene LCS 769 102 ( 68-125 ) 750 ug/Kg 06/12/2011
1,2,3-Trichloropropane LCS 702 94 ( 78-123 ) 750 ug/Kg 06/12/2011
1,2,4-Trichlorobenzene LCS 798 106 ( 76-122 ) 750 ug/Kg 06/12/2011
1,2,4-Trimethylbenzene LCS 735 98 ( 80-122 ) 750 ug/Kg 06/12/2011
1,2-Dibromo-3-chloropropane LCS 735 98 ( 71-128 ) 750 ug/Kg 06/12/2011
1,2-Dibromoethane LCS 731 98 ( 80-124 ) 750 ug/Kg 06/12/2011
1,2-Dichlorobenzene LCS 708 94 ( 80-120 ) 750 ug/Kg 06/12/2011
1,2-Dichloroethane LCS 697 93 ( 80-122 ) 750 ug/Kg 06/12/2011
1,2-Dichloropropane LCS 742 99 ( 80-120 ) 750 ug/Kg 06/12/2011
1,3,5-Trimethylbenzene LCS 718 96 ( 80-123 ) 750 ug/Kg 06/12/2011
1,3-Dichlorobenzene LCS 702 94 ( 80-122 ) 750 ug/Kg 06/12/2011
1,3-Dichloropropane LCS 681 91 ( 80-124 ) 750 ug/Kg 06/12/2011
1,4-Dichlorobenzene LCS 724 97 ( 80-122 ) 750 ug/Kg 06/12/2011
2,2-Dichloropropane LCS 691 92 ( 80-129 ) 750 ug/Kg 06/12/2011
48 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1031025 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
2-Butanone (MEK) LCS 1960 87 ( 61-140 ) 2250 ug/Kg 06/12/2011
2-Chlorotoluene LCS 718 96 ( 80-123 ) 750 ug/Kg 06/12/2011
2-Hexanone LCS 2180 97 ( 74-129 ) 2250 ug/Kg 06/12/2011
4-Chlorotoluene LCS 711 95 ( 80-123 ) 750 ug/Kg 06/12/2011
4-Isopropyltoluene LCS 719 96 ( 80-123 ) 750 ug/Kg 06/12/2011
4-Methyl-2-pentanone (MIBK) LCS 2180 97 ( 76-126 ) 2250 ug/Kg 06/12/2011
Benzene LCS 647 86 ( 80-123 ) 750 ug/Kg 06/12/2011
Bromobenzene LCS 673 90 ( 80-123 ) 750 ug/Kg 06/12/2011
Bromochloromethane LCS 681 91 ( 72-125 ) 750 ug/Kg 06/12/2011
Bromodichloromethane LCS 756 101 ( 80-123 ) 750 ug/Kg 06/12/2011
Bromoform LCS 774 103 ( 74-125 ) 750 ug/Kg 06/12/2011
Bromomethane LCS 721 96 ( 60-149 ) 750 ug/Kg 06/12/2011
Carbon disulfide LCS 933 83 ( 45-160 ) 1130 ug/Kg 06/12/2011
Carbon tetrachloride LCS 722 96 ( 80-126 ) 750 ug/Kg 06/12/2011
Chlorobenzene LCS 702 94 ( 80-123 ) 750 ug/Kg 06/12/2011
Chloroethane LCS 700 93 ( 59-154 ) 750 ug/Kg 06/12/2011
Chloroform LCS 673 90 ( 72-125 ) 750 ug/Kg 06/12/2011
Chloromethane LCS 699 93 ( 62-140 ) 750 ug/Kg 06/12/2011
cis-1,2-Dichloroethene LCS 737 98 ( 76-125 ) 750 ug/Kg 06/12/2011
cis-1,3-Dichloropropene LCS 763 102 ( 80-125 ) 750 ug/Kg 06/12/2011
49 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1031025 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Dibromochloromethane LCS 734 98 ( 80-125 ) 750 ug/Kg 06/12/2011
Dibromomethane LCS 664 89 ( 80-119 ) 750 ug/Kg 06/12/2011
Dichlorodifluoromethane LCS 704 94 ( 51-155 ) 750 ug/Kg 06/12/2011
Ethylbenzene LCS 715 95 ( 80-123 ) 750 ug/Kg 06/12/2011
Hexachlorobutadiene LCS 810 108 ( 78-124 ) 750 ug/Kg 06/12/2011
Isopropylbenzene (Cumene) LCS 758 101 ( 80-123 ) 750 ug/Kg 06/12/2011
Methylene chloride LCS 692 92 ( 73-125 ) 750 ug/Kg 06/12/2011
Methyl-t-butyl ether LCS 1020 91 ( 79-124 ) 1130 ug/Kg 06/12/2011
Naphthalene LCS 748 100 ( 68-122 ) 750 ug/Kg 06/12/2011
n-Butylbenzene LCS 734 98 ( 80-124 ) 750 ug/Kg 06/12/2011
n-Propylbenzene LCS 721 96 ( 80-125 ) 750 ug/Kg 06/12/2011
o-Xylene LCS 733 98 ( 80-123 ) 750 ug/Kg 06/12/2011
P & M -Xylene LCS 1470 98 ( 80-125 ) 1500 ug/Kg 06/12/2011
sec-Butylbenzene LCS 732 98 ( 80-122 ) 750 ug/Kg 06/12/2011
Styrene LCS 778 104 ( 80-124 ) 750 ug/Kg 06/12/2011
tert-Butylbenzene LCS 719 96 ( 80-121 ) 750 ug/Kg 06/12/2011
Tetrachloroethene LCS 733 98 ( 79-128 ) 750 ug/Kg 06/12/2011
Toluene LCS 731 98 ( 80-125 ) 750 ug/Kg 06/12/2011
trans-1,2-Dichloroethene LCS 645 86 ( 76-126 ) 750 ug/Kg 06/12/2011
trans-1,3-Dichloropropene LCS 778 104 ( 80-124 ) 750 ug/Kg 06/12/2011
Trichloroethene LCS 712 95 ( 80-123 ) 750 ug/Kg 06/12/2011
50 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1031025 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Trichlorofluoromethane LCS 732 98 ( 62-149 ) 750 ug/Kg 06/12/2011
Vinyl chloride LCS 791 106 ( 68-139 ) 750 ug/Kg 06/12/2011
Xylenes (total) LCS 2210 98 ( 86-124 ) 2250 ug/Kg 06/12/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 87 ( 80-117 ) 06/12/2011
4-Bromofluorobenzene <surr> LCS 91 ( 68-136 ) 06/12/2011
Toluene-d8 <surr> LCS 88 ( 85-121 ) 06/12/2011
Batch
Method
Instrument
VMS12141
SW8260B
HP 5890 Series II MS5 VLA
51 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1032211 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24925
SW3550C
06/16/2011
QC results affect the following production samples:
1112386003
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Polynuclear Aromatics GC/MS
52 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1032211 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24925
SW3550C
06/16/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Polynuclear Aromatics GC/MS
1-Methylnaphthalene LCS 18.0 81 ( 44-107 ) 22.2 ug/Kg 06/17/2011
2-Methylnaphthalene LCS 17.3 78 ( 45-105 ) 22.2 ug/Kg 06/17/2011
Acenaphthene LCS 17.6 79 ( 45-110 ) 22.2 ug/Kg 06/17/2011
Acenaphthylene LCS 17.1 77 ( 45-105 ) 22.2 ug/Kg 06/17/2011
Anthracene LCS 17.1 77 ( 55-105 ) 22.2 ug/Kg 06/17/2011
Benzo(a)Anthracene LCS 19.7 89 ( 50-110 ) 22.2 ug/Kg 06/17/2011
Benzo[a]pyrene LCS 15.4 69 ( 50-110 ) 22.2 ug/Kg 06/17/2011
Benzo[b]Fluoranthene LCS 20.4 92 ( 45-115 ) 22.2 ug/Kg 06/17/2011
Benzo[g,h,i]perylene LCS 18.9 85 ( 40-125 ) 22.2 ug/Kg 06/17/2011
Benzo[k]fluoranthene LCS 20.6 93 ( 45-125 ) 22.2 ug/Kg 06/17/2011
Chrysene LCS 19.6 88 ( 55-110 ) 22.2 ug/Kg 06/17/2011
Dibenzo[a,h]anthracene LCS 18.2 82 ( 40-125 ) 22.2 ug/Kg 06/17/2011
Fluoranthene LCS 21.1 95 ( 55-115 ) 22.2 ug/Kg 06/17/2011
Fluorene LCS 18.1 81 ( 50-110 ) 22.2 ug/Kg 06/17/2011
Indeno[1,2,3-c,d] pyrene LCS 18.9 85 ( 40-120 ) 22.2 ug/Kg 06/17/2011
Naphthalene LCS 22.3 100 ( 40-105 ) 22.2 ug/Kg 06/17/2011
Phenanthrene LCS 19.8 89 ( 50-110 ) 22.2 ug/Kg 06/17/2011
Pyrene LCS 20.3 91 ( 45-125 ) 22.2 ug/Kg 06/17/2011
Surrogates
2-Fluorobiphenyl <surr> LCS 79 ( 45-105 ) 06/17/2011
Terphenyl-d14 <surr> LCS 97 ( 30-125 ) 06/17/2011
53 of 62
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 06/22/2011 17:04
Batch
Method
Date
Prep
1032211 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-6 4501 Lake Otis
Soil/Solid (dry weight)
XXX24925
SW3550C
06/16/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Polynuclear Aromatics GC/MS
Batch
Method
Instrument
XMS6007
8270D SIMS (PAH)
HP 6890/5973 MS SVQA
54 of 62
Matrix
SGS Ref.# Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Original
Prep1031030 Matrix Spike
1031031 Matrix Spike Duplicate
1031029
Solid/Soil (Wet Weight)
QC results affect the following production samples:
1112386001, 1112386002, 1112386003, 1112386004, 1112386005
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane MS (16.1) U 755 97 ( 80-125 ) 776 ug/Kg 06/12/2011
MSD 725 93 4 (< 20 ) 776 ug/Kg 06/12/2011
1,1,1-Trichloroethane MS (16.1) U 714 92 ( 80-127 ) 776 ug/Kg 06/12/2011
MSD 726 94 2 (< 20 ) 776 ug/Kg 06/12/2011
1,1,2,2-Tetrachloroethane MS (31.0) U 739 95 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 727 94 2 (< 20 ) 776 ug/Kg 06/12/2011
1,1,2-Trichloroethane MS (16.1) U 730 94 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 721 93 1 (< 20 ) 776 ug/Kg 06/12/2011
1,1-Dichloroethane MS (16.1) U 700 90 ( 77-125 ) 776 ug/Kg 06/12/2011
MSD 713 92 2 (< 20 ) 776 ug/Kg 06/12/2011
1,1-Dichloroethene MS (16.1) U 781 101 ( 65-150 ) 776 ug/Kg 06/12/2011
MSD 751 97 4 (< 20 ) 776 ug/Kg 06/12/2011
1,1-Dichloropropene MS (16.1) U 720 93 ( 76-134 ) 776 ug/Kg 06/12/2011
MSD 689 89 4 (< 20 ) 776 ug/Kg 06/12/2011
1,2,3-Trichlorobenzene MS (31.0) U 750 97 ( 68-125 ) 776 ug/Kg 06/12/2011
MSD 723 93 4 (< 20 ) 776 ug/Kg 06/12/2011
1,2,3-Trichloropropane MS (16.1) U 717 92 ( 78-123 ) 776 ug/Kg 06/12/2011
MSD 683 88 5 (< 20 ) 776 ug/Kg 06/12/2011
1,2,4-Trichlorobenzene MS (16.1) U 770 99 ( 76-122 ) 776 ug/Kg 06/12/2011
MSD 771 99 0 (< 20 ) 776 ug/Kg 06/12/2011
1,2,4-Trimethylbenzene MS (31.0) U 733 95 ( 80-122 ) 776 ug/Kg 06/12/2011
MSD 730 94 0 (< 20 ) 776 ug/Kg 06/12/2011
1,2-Dibromo-3-chloropropane MS (64.2) U 807 104 ( 71-128 ) 776 ug/Kg 06/12/2011
MSD 815 105 1 (< 20 ) 776 ug/Kg 06/12/2011
1,2-Dibromoethane MS (16.1) U 749 97 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 726 94 3 (< 20 ) 776 ug/Kg 06/12/2011
1,2-Dichlorobenzene MS (16.1) U 730 94 ( 80-120 ) 776 ug/Kg 06/12/2011
MSD 725 93 1 (< 20 ) 776 ug/Kg 06/12/2011
1,2-Dichloroethane MS (16.1) U 718 93 ( 80-122 ) 776 ug/Kg 06/12/2011
MSD 730 94 2 (< 20 ) 776 ug/Kg 06/12/2011
1,2-Dichloropropane MS (16.1) U 794 102 ( 80-120 ) 776 ug/Kg 06/12/2011
MSD 760 98 4 (< 20 ) 776 ug/Kg 06/12/2011
1,3,5-Trimethylbenzene MS (16.1) U 717 92 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 721 93 1 (< 20 ) 776 ug/Kg 06/12/2011
1,3-Dichlorobenzene MS (16.1) U 703 91 ( 80-122 ) 776 ug/Kg 06/12/2011
MSD 709 91 1 (< 20 ) 776 ug/Kg 06/12/2011
1,3-Dichloropropane MS (16.1) U 708 91 ( 80-124 ) 776 ug/Kg 06/12/2011
55 of 62
Matrix
SGS Ref.# Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Original
Prep1031030 Matrix Spike
1031031 Matrix Spike Duplicate
1031029
Solid/Soil (Wet Weight)
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
MSD 691 89 2 (< 20 ) 776 ug/Kg 06/12/2011
1,4-Dichlorobenzene MS (16.1) U 761 98 ( 80-122 ) 776 ug/Kg 06/12/2011
MSD 752 97 1 (< 20 ) 776 ug/Kg 06/12/2011
2,2-Dichloropropane MS (16.1) U 717 92 ( 80-129 ) 776 ug/Kg 06/12/2011
MSD 663 85 8 (< 20 ) 776 ug/Kg 06/12/2011
2-Butanone (MEK) MS (161) U 1970 84 ( 61-140 ) 2330 ug/Kg 06/12/2011
MSD 2080 89 5 (< 20 ) 2330 ug/Kg 06/12/2011
2-Chlorotoluene MS (16.1) U 707 91 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 704 91 0 (< 20 ) 776 ug/Kg 06/12/2011
2-Hexanone MS (161) U 2320 100 ( 74-129 ) 2330 ug/Kg 06/12/2011
MSD 2230 96 4 (< 20 ) 2330 ug/Kg 06/12/2011
4-Chlorotoluene MS (16.1) U 700 90 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 718 93 3 (< 20 ) 776 ug/Kg 06/12/2011
4-Isopropyltoluene MS (16.1) U 734 95 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 719 93 2 (< 20 ) 776 ug/Kg 06/12/2011
4-Methyl-2-pentanone (MIBK) MS (161) U 2180 94 ( 76-126 ) 2330 ug/Kg 06/12/2011
MSD 2180 94 0 (< 20 ) 2330 ug/Kg 06/12/2011
Benzene MS (8.08) U 704 91 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 819 106 15 (< 20 ) 776 ug/Kg 06/12/2011
Bromobenzene MS (16.1) U 702 90 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 712 92 1 (< 20 ) 776 ug/Kg 06/12/2011
Bromochloromethane MS (16.1) U 710 91 ( 72-125 ) 776 ug/Kg 06/12/2011
MSD 683 88 4 (< 20 ) 776 ug/Kg 06/12/2011
Bromodichloromethane MS (16.1) U 762 98 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 782 101 3 (< 20 ) 776 ug/Kg 06/12/2011
Bromoform MS (16.1) U 780 100 ( 74-125 ) 776 ug/Kg 06/12/2011
MSD 774 100 1 (< 20 ) 776 ug/Kg 06/12/2011
Bromomethane MS (128) U 751 97 ( 60-149 ) 776 ug/Kg 06/12/2011
MSD 735 95 2 (< 20 ) 776 ug/Kg 06/12/2011
Carbon disulfide MS (64.2) U 1140 98 ( 45-160 ) 1160 ug/Kg 06/12/2011
MSD 1130 97 1 (< 20 ) 1160 ug/Kg 06/12/2011
Carbon tetrachloride MS (16.1) U 772 99 ( 80-126 ) 776 ug/Kg 06/12/2011
MSD 757 98 2 (< 20 ) 776 ug/Kg 06/12/2011
Chlorobenzene MS (16.1) U 721 93 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 689 89 4 (< 20 ) 776 ug/Kg 06/12/2011
Chloroethane MS (128) U 663 85 ( 59-154 ) 776 ug/Kg 06/12/2011
MSD 646 83 3 (< 20 ) 776 ug/Kg 06/12/2011
Chloroform MS (16.1) U 688 89 ( 72-125 ) 776 ug/Kg 06/12/2011
MSD 656 85 5 (< 20 ) 776 ug/Kg 06/12/2011
Chloromethane MS (16.1) U 636 82 ( 62-140 ) 776 ug/Kg 06/12/201156 of 62
Matrix
SGS Ref.# Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Original
Prep1031030 Matrix Spike
1031031 Matrix Spike Duplicate
1031029
Solid/Soil (Wet Weight)
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
MSD 622 80 2 (< 20 ) 776 ug/Kg 06/12/2011
cis-1,2-Dichloroethene MS (16.1) U 763 98 ( 76-125 ) 776 ug/Kg 06/12/2011
MSD 698 90 9 (< 20 ) 776 ug/Kg 06/12/2011
cis-1,3-Dichloropropene MS (16.1) U 772 100 ( 80-125 ) 776 ug/Kg 06/12/2011
MSD 777 100 1 (< 20 ) 776 ug/Kg 06/12/2011
Dibromochloromethane MS (16.1) U 735 95 ( 80-125 ) 776 ug/Kg 06/12/2011
MSD 736 95 0 (< 20 ) 776 ug/Kg 06/12/2011
Dibromomethane MS (16.1) U 700 90 ( 80-119 ) 776 ug/Kg 06/12/2011
MSD 671 86 4 (< 20 ) 776 ug/Kg 06/12/2011
Dichlorodifluoromethane MS (31.0) U 617 80 ( 51-155 ) 776 ug/Kg 06/12/2011
MSD 558 72 10 (< 20 ) 776 ug/Kg 06/12/2011
Ethylbenzene MS (16.1) U 750 97 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 719 93 4 (< 20 ) 776 ug/Kg 06/12/2011
Hexachlorobutadiene MS (31.0) U 879 113 ( 78-124 ) 776 ug/Kg 06/12/2011
MSD 860 111 2 (< 20 ) 776 ug/Kg 06/12/2011
Isopropylbenzene (Cumene) MS (16.1) U 778 100 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 762 98 2 (< 20 ) 776 ug/Kg 06/12/2011
Methylene chloride MS (64.2) U 739 95 ( 73-125 ) 776 ug/Kg 06/12/2011
MSD 728 94 2 (< 20 ) 776 ug/Kg 06/12/2011
Methyl-t-butyl ether MS (64.2) U 1050 91 ( 79-124 ) 1160 ug/Kg 06/12/2011
MSD 1060 91 1 (< 20 ) 1160 ug/Kg 06/12/2011
Naphthalene MS (31.0) U 762 98 ( 68-122 ) 776 ug/Kg 06/12/2011
MSD 739 95 3 (< 20 ) 776 ug/Kg 06/12/2011
n-Butylbenzene MS (16.1) U 724 93 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 719 93 1 (< 20 ) 776 ug/Kg 06/12/2011
n-Propylbenzene MS (16.1) U 711 92 ( 80-125 ) 776 ug/Kg 06/12/2011
MSD 722 93 2 (< 20 ) 776 ug/Kg 06/12/2011
o-Xylene MS (31.0) U 758 98 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 718 92 6 (< 20 ) 776 ug/Kg 06/12/2011
P & M -Xylene MS (31.0) U 1530 99 ( 80-125 ) 1550 ug/Kg 06/12/2011
MSD 1520 98 1 (< 20 ) 1550 ug/Kg 06/12/2011
sec-Butylbenzene MS (16.1) U 734 95 ( 80-122 ) 776 ug/Kg 06/12/2011
MSD 730 94 1 (< 20 ) 776 ug/Kg 06/12/2011
Styrene MS (16.1) U 781 101 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 772 99 1 (< 20 ) 776 ug/Kg 06/12/2011
tert-Butylbenzene MS (16.1) U 738 95 ( 80-121 ) 776 ug/Kg 06/12/2011
MSD 709 91 4 (< 20 ) 776 ug/Kg 06/12/2011
Tetrachloroethene MS (8.08) U 767 99 ( 79-128 ) 776 ug/Kg 06/12/2011
MSD 716 92 7 (< 20 ) 776 ug/Kg 06/12/2011
Toluene MS (31.0) U 767 99 ( 80-125 ) 776 ug/Kg 06/12/201157 of 62
Matrix
SGS Ref.# Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Original
Prep1031030 Matrix Spike
1031031 Matrix Spike Duplicate
1031029
Solid/Soil (Wet Weight)
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
MSD 761 98 1 (< 20 ) 776 ug/Kg 06/12/2011
trans-1,2-Dichloroethene MS (16.1) U 742 96 ( 76-126 ) 776 ug/Kg 06/12/2011
MSD 726 94 2 (< 20 ) 776 ug/Kg 06/12/2011
trans-1,3-Dichloropropene MS (16.1) U 783 101 ( 80-124 ) 776 ug/Kg 06/12/2011
MSD 777 100 1 (< 20 ) 776 ug/Kg 06/12/2011
Trichloroethene MS (8.08) U 749 97 ( 80-123 ) 776 ug/Kg 06/12/2011
MSD 738 95 2 (< 20 ) 776 ug/Kg 06/12/2011
Trichlorofluoromethane MS (31.0) U 699 90 ( 62-149 ) 776 ug/Kg 06/12/2011
MSD 698 90 0 (< 20 ) 776 ug/Kg 06/12/2011
Vinyl chloride MS (16.1) U 742 96 ( 68-139 ) 776 ug/Kg 06/12/2011
MSD 700 90 6 (< 20 ) 776 ug/Kg 06/12/2011
Xylenes (total) MS (64.2) U 2290 98 ( 86-124 ) 2330 ug/Kg 06/12/2011
MSD 2230 96 3 (< 20 ) 2330 ug/Kg 06/12/2011
Surrogates
1,2-Dichloroethane-D4 <surr> MS 635 82 ( 80-117 ) 06/12/2011
MSD 651 84 3 06/12/2011
4-Bromofluorobenzene <surr> MS 1800 87 ( 68-136 ) 06/12/2011
MSD 1830 89 2 06/12/2011
Toluene-d8 <surr> MS 704 91 ( 85-121 ) 06/12/2011
MSD 681 88 3 06/12/2011
Batch
Method
Instrument
VMS12141
SW8260B
HP 5890 Series II MS5 VLA
58 of 62
Matrix
SGS Ref.# Printed Date/Time 06/22/2011 17:04Batch
Method
Date
Original
Prep1032214 Matrix Spike
1032215 Matrix Spike Duplicate
1112492085
Soil/Solid (dry weight)
XXX24925
Sonication Extraction Soil 8270 PAH SIM
06/16/2011
QC results affect the following production samples:
1112386003
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Polynuclear Aromatics GC/MS
1-Methylnaphthalene MS 1320 425 -1,680* ( 44-107 ) 53.2 ug/Kg 06/17/2011
MSD 677 -1,200* 46 (< 30 ) 53.0 ug/Kg 06/17/2011*
2-Methylnaphthalene MS 1910 550 -2,560* ( 45-105 ) 53.2 ug/Kg 06/17/2011
MSD 873 -1,950* 46 (< 30 ) 53.0 ug/Kg 06/17/2011*
Acenaphthene MS 1870 727 -2,140* ( 45-110 ) 53.2 ug/Kg 06/17/2011
MSD 1241 -1,190* 52 (< 30 ) 53.0 ug/Kg 06/17/2011*
Acenaphthylene MS 753 357 -745* ( 45-105 ) 53.2 ug/Kg 06/17/2011
MSD 459 -555* 25 (< 30 ) 53.0 ug/Kg 06/17/2011
Benzo[b]Fluoranthene MS 5550 2802 -5,170* ( 45-115 ) 53.2 ug/Kg 06/17/2011
MSD 4118 -2,690* 38 (< 30 ) 53.0 ug/Kg 06/18/2011*
Benzo[k]fluoranthene MS (66.6) U 0.00 0* ( 45-125 ) 53.2 ug/Kg 06/17/2011
MSD 0.00 0* 0 (< 30 ) 53.0 ug/Kg 06/17/2011
Dibenzo[a,h]anthracene MS 1080 507 -1,070* ( 40-125 ) 53.2 ug/Kg 06/17/2011
MSD 771 -575* 41 (< 30 ) 53.0 ug/Kg 06/17/2011*
Fluoranthene MS 9080 4246 -9,130* ( 55-115 ) 53.2 ug/Kg 06/17/2011
MSD 6791 -4,330* 46 (< 30 ) 53.0 ug/Kg 06/18/2011*
Phenanthrene MS 11700 4952 -12,700* ( 50-110 ) 53.2 ug/Kg 06/17/2011
MSD 7904 -7,130* 46 (< 30 ) 53.0 ug/Kg 06/18/2011*
Pyrene MS 9810 4642 -9,750* ( 45-125 ) 53.2 ug/Kg 06/17/2011
MSD 7380 -4,590* 46 (< 30 ) 53.0 ug/Kg 06/18/2011*
Surrogates
2-Fluorobiphenyl <surr> MS 42.8 81 ( 45-105 ) 06/17/2011
MSD 42.4 80 1 06/17/2011
Terphenyl-d14 <surr> MS 56.0 105 ( 30-125 ) 06/17/2011
MSD 61.2 115 9 06/17/2011
Batch
Method
Instrument
XMS6005
8270D SIMS (PAH)
HP 6890/5973 MS SVQA
59 of 62
60 of 62
61 of 62
62 of 62
Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: July 1, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1112386 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments: Sample D2S1 was inadvertently mislabeled as Sample D2S3 on the chain of custody, but is correctly identified in the report tables.
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 3.0° C
Work Order Number: 1112386
32-1-17172-011 Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO, BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No discrepancies noted.
e. Data quality or usability affected? (Please Explain.)
Comments:
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: Anthracene was detected in the method blank at 6.25 mg/kg. MS/MSD recoveries for multiple analytes are outside QC criteria. MS/MSD RPDs do not meet QC criteria.
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: Analytes with MS/MSD RPD failures are estimated in the original sample, where detected.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments:
b. All applicable holding times met? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1112386
32-1-17172-011 Former Peacock Cleaners Page 3 of 6
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.)
Comments:
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection level for the project? Yes / No / NA (Please explain.) Comments: LODs are greater than the ADEC migration to groundwater standard for non-detect results in the following analytes: 1,2-dichloroethane, 1,2-dichloropropane, 1,2-dibromoethane, methylene chloride,
1,1,2,2-tetrachloroethane, 1,1,2-trichloroethane, 1,2,3-tricloropropane, and vinyl chloride in project Samples D1S3, D2S3, D3S2, and D3S4
Carbon tetrachloride and bromomethane in project Sample D1S3.
e. Data quality or usability affected? (Please explain.) Comments: The potential presence of these analytes at concentrations greater than the ADEC migration to groundwater cleanup standard but less than the LOD cannot be determined.
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments:
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments: Anthracene was detected at 6.25 mg/kg.
iii. If above LOQ, what samples are affected?
Comments: Sample D3S2.
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments: The results are flagged in the report tables.
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: The detection is potentially attributable to lab contamination. The result is an estimate.
Work Order Number: 1112386
32-1-17172-011 Former Peacock Cleaners Page 4 of 6
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples?
(LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments:
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.) Comments:
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments: For PAH analysis by EPA 8270 SIMS and VOC analysis by EPA 8260B, MS/MSD RPDs are evaluated. Eight of the ten reported PAH analytes had RPDs outside of QC criteria.
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments: Sample D3S2.
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: It is our opinion that the RPD failure was the result of concentrations of PAH analytes in the spiked sample, which was not one of the project samples. Therefore, the MS/MSD RPD failures do not indicate a precision failure in our samples. Because the precision of the project sample/duplicate is within the DQOs, it the results are not flagged.
Work Order Number: 1112386
32-1-17172-011 Former Peacock Cleaners Page 5 of 6
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory
samples? Yes / No / NA (Please explain.) Comments:
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments:
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Carbon disulfide was detected at a concentration less than the LOQ.
iv. If above LOQ, what samples are affected? NA Comments: Carbon disulfide was not detected in the project samples.
v. Data quality or usability affected? Comments: Data quality or usability is not affected.
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.)
Work Order Number: 1112386
32-1-17172-011 Former Peacock Cleaners Page 6 of 6
Comments: Sample D3S4 is a duplicate of Sample D3S2
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments: For analytes detected in both samples, the RPDs were 18.9 percent (DRO) and 29.5 percent (RRO)
iv. Data quality or usability affected? Explain. Comments:
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Not decontamination or equipment blank submitted due to our use of disposable sampling equipment.
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments:
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SGS North America Environmental Services – Alaska DivisionClient Services/Continuous Improvement Lead
Heather L. Hall 2011.07.0115:31:51 -08'00'
CASE NARRATIVE Print Date: 7/1/2011
Workorder No.: 1112835
Project Name: 32-1-17172-006 4115 Lake Otis
Client Name: Shannon & Wilson, Inc.
Lab Sample ID
Sample Comments
Sample Type Client Sample ID
Refer to the sample receipt form for information on sample condition.
1035306
8260B - LCS recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCS LCS for HBN 1216746 [VXX/22361*
1035307
8260B - LCSD recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCSD LCSD for HBN 1216746 [VXX/2236*
1035312
8260B - CCV recovery for multiple analytes does not meet QC criteria (biased high). These analytes were not detected
above the LOQ in the associated samples.
CCV CCV for HBN 1216748 [VMS/12198*
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
SG S N o rth A m eric a Inc . En vir onm enta l D ivis ion 200 W e st Pot ter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs .com M em ber of SG S Group
32-1-17172-006 4115 Lake Otis
Project Manager
Steve Crupi
T: (907) 561-2120 F:
Attn: Jake Gano
5430 Fairbanks St., Ste. 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1112835
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SG S Group
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 7/1/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-006 4115 Lake Otis
Workorder No.: 1112835
Analytical Methods
Method Description Analytical Method
Volatile Organic Compounds (W) FULL SW8260B
Print Date: 7/1/2011 2:31 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1112835001 17172-006-DS1
1112835002 17172-006-WTB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Print Date: 7/1/2011 2:31 pmDetectable Results Summary
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L912Toluene
ug/L0.800JEthylbenzene
ug/L6.12n-Butylbenzene
ug/L1081,3,5-Trimethylbenzene
ug/L23.54-Isopropyltoluene
ug/L0.660Jn-Propylbenzene
ug/L0.330JStyrene
ug/L1.59sec-Butylbenzene
ug/L15.8P & M -Xylene
ug/L2.21Naphthalene
ug/L26.9o-Xylene
ug/L42.7Xylenes (total)
ug/L98.0J1,2,4-Trimethylbenzene
ug/L1.66tert-Butylbenzene
ug/L0.840JIsopropylbenzene (Cumene)
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L4.15JMethylene chloride
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 98.0J 100 ug/L VMS12198 VXX2236131.0 100
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 108 100 ug/L VMS12198 VXX2236131.0 100
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 23.5 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.800J 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.840J 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 2.00 U 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 2.21 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 6.12 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.660J 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 26.9 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 15.8 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 1.59 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.330J 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 1.66 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 912 100 ug/L VMS12198 VXX2236131.0 100
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 42.7 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 99.7 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 103 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 100 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:55
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 1 Analyst: JPI
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 18:15
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 100 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 4.15J 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 105 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 92.7 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 98.7 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:28
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835002-A
Dilution Factor: 1 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,1-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,2-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 06/30/110.620
1,2-Dibromoethane 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichloropropane 0.240 U 0.400 ug/L 06/30/110.120
1,4-Dichlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
2,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
2-Butanone (MEK) 6.20 U 10.0 ug/L 06/30/113.10
2-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
2-Hexanone 6.20 U 10.0 ug/L 06/30/113.10
4-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Isopropyltoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 06/30/113.10
Benzene 0.240 U 0.400 ug/L 06/30/110.120
Bromobenzene 0.620 U 1.00 ug/L 06/30/110.310
Bromochloromethane 0.620 U 1.00 ug/L 06/30/110.310
Bromodichloromethane 0.300 U 0.500 ug/L 06/30/110.150
Bromoform 0.620 U 1.00 ug/L 06/30/110.310
Bromomethane 1.88 U 3.00 ug/L 06/30/110.940
Carbon disulfide 1.24 U 2.00 ug/L 06/30/110.620
Carbon tetrachloride 0.620 U 1.00 ug/L 06/30/110.310
Chlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
Chloroethane 0.620 U 1.00 ug/L 06/30/110.310
Chloroform 0.600 U 1.00 ug/L 06/30/110.300
Chloromethane 0.620 U 1.00 ug/L 06/30/110.310
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 06/30/110.150
Dibromochloromethane 0.300 U 0.500 ug/L 06/30/110.150
Dibromomethane 0.620 U 1.00 ug/L 06/30/110.310
Dichlorodifluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Ethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Hexachlorobutadiene 0.620 U 1.00 ug/L 06/30/110.310
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 06/30/110.310
Methylene chloride 2.00 U 5.00 ug/L 06/30/111.00
Methyl-t-butyl ether 3.00 U 5.00 ug/L 06/30/111.50
Naphthalene 1.24 U 2.00 ug/L 06/30/110.620
n-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
n-Propylbenzene 0.620 U 1.00 ug/L 06/30/110.310
o-Xylene 0.620 U 1.00 ug/L 06/30/110.310
P & M -Xylene 1.24 U 2.00 ug/L 06/30/110.620
sec-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Styrene 0.620 U 1.00 ug/L 06/30/110.310
tert-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Tetrachloroethene 0.620 U 1.00 ug/L 06/30/110.310
Toluene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
Trichloroethene 0.620 U 1.00 ug/L 06/30/110.310
Trichlorofluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Vinyl chloride 0.620 U 1.00 ug/L 06/30/110.310
Xylenes (total) 1.88 U 3.00 ug/L 06/30/110.940
Surrogates
1,2-Dichloroethane-D4 <surr> 109 70-120 % 06/30/11
4-Bromofluorobenzene <surr> 94.3 75-120 % 06/30/11
Toluene-d8 <surr> 99.4 85-120 % 06/30/11
Instrument
Method
Batch VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane LCS 33.7 112 ( 80-130 ) 30 ug/L 06/30/2011
LCSD 34.5 115 2 (< 20 ) 30 ug/L 06/30/2011
1,1,1-Trichloroethane LCS 35.1 117 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 35.9 120 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2,2-Tetrachloroethane LCS 28.8 96 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 29.4 98 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2-Trichloroethane LCS 30.2 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.8 103 2 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethane LCS 33.5 112 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 33.8 113 1 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethene LCS 35.4 118 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.5 125 6 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloropropene LCS 33.5 112 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 34.4 115 3 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichlorobenzene LCS 31.4 105 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 33.0 110 5 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichloropropane LCS 30.0 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 0 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trichlorobenzene LCS 31.9 106 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trimethylbenzene LCS 30.2 101 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromo-3-chloropropane LCS 29.3 98 ( 50-130 ) 30 ug/L 06/30/2011
LCSD 29.6 99 1 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromoethane LCS 33.1 110 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 0 (< 20 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,2-Dichlorobenzene LCS 29.9 100 ( 70-120 ) 30 ug/L 06/30/2011
LCSD 30.9 103 3 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloroethane LCS 33.5 112 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 33.7 112 0 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloropropane LCS 32.1 107 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 32.5 108 1 (< 20 ) 30 ug/L 06/30/2011
1,3,5-Trimethylbenzene LCS 29.9 100 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 3 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichlorobenzene LCS 29.8 99 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.0 103 4 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichloropropane LCS 30.1 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 1 (< 20 ) 30 ug/L 06/30/2011
1,4-Dichlorobenzene LCS 30.4 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
2,2-Dichloropropane LCS 37.5 125 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 39.0 130 4 (< 20 ) 30 ug/L 06/30/2011
2-Butanone (MEK) LCS 102 114 ( 30-150 ) 90 ug/L 06/30/2011
LCSD 118 131 14 (< 20 ) 90 ug/L 06/30/2011
2-Chlorotoluene LCS 29.1 97 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.1 100 3 (< 20 ) 30 ug/L 06/30/2011
2-Hexanone LCS 86.5 96 ( 55-130 ) 90 ug/L 06/30/2011
LCSD 93.0 103 7 (< 20 ) 90 ug/L 06/30/2011
4-Chlorotoluene LCS 28.9 96 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 30.3 101 5 (< 20 ) 30 ug/L 06/30/2011
4-Isopropyltoluene LCS 31.7 106 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
4-Methyl-2-pentanone (MIBK) LCS 111 123 ( 60-135 ) 90 ug/L 06/30/2011
LCSD 113 125 2 (< 20 ) 90 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Benzene LCS 32.8 109 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.2 111 1 (< 20 ) 30 ug/L 06/30/2011
Bromobenzene LCS 30.6 102 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 3 (< 20 ) 30 ug/L 06/30/2011
Bromochloromethane LCS 36.6 122 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 37.1 124 1 (< 20 ) 30 ug/L 06/30/2011
Bromodichloromethane LCS 33.9 113 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 34.0 113 0 (< 20 ) 30 ug/L 06/30/2011
Bromoform LCS 36.5 122 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.6 125 3 (< 20 ) 30 ug/L 06/30/2011
Bromomethane LCS 45.1 150 ( 30-145 )* 30 ug/L 06/30/2011
LCSD 45.2 151 * 0 (< 20 ) 30 ug/L 06/30/2011
Carbon disulfide LCS 49.4 110 ( 35-160 ) 45 ug/L 06/30/2011
LCSD 49.7 110 1 (< 20 ) 45 ug/L 06/30/2011
Carbon tetrachloride LCS 36.1 120 ( 65-140 ) 30 ug/L 06/30/2011
LCSD 36.6 122 2 (< 20 ) 30 ug/L 06/30/2011
Chlorobenzene LCS 32.3 108 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 3 (< 20 ) 30 ug/L 06/30/2011
Chloroethane LCS 32.5 108 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 32.7 109 1 (< 20 ) 30 ug/L 06/30/2011
Chloroform LCS 33.6 112 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.0 113 1 (< 20 ) 30 ug/L 06/30/2011
Chloromethane LCS 31.3 104 ( 40-125 ) 30 ug/L 06/30/2011
LCSD 31.5 105 1 (< 20 ) 30 ug/L 06/30/2011
cis-1,2-Dichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.7 119 0 (< 20 ) 30 ug/L 06/30/2011
cis-1,3-Dichloropropene LCS 35.5 118 ( 70-130 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 35.5 118 0 (< 20 ) 30 ug/L 06/30/2011
Dibromochloromethane LCS 34.3 114 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 34.9 116 2 (< 20 ) 30 ug/L 06/30/2011
Dibromomethane LCS 33.5 112 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.6 112 0 (< 20 ) 30 ug/L 06/30/2011
Dichlorodifluoromethane LCS 38.0 127 ( 30-155 ) 30 ug/L 06/30/2011
LCSD 36.2 121 5 (< 20 ) 30 ug/L 06/30/2011
Ethylbenzene LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.8 113 2 (< 20 ) 30 ug/L 06/30/2011
Hexachlorobutadiene LCS 32.7 109 ( 50-140 ) 30 ug/L 06/30/2011
LCSD 34.6 115 6 (< 20 ) 30 ug/L 06/30/2011
Isopropylbenzene (Cumene) LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.9 113 2 (< 20 ) 30 ug/L 06/30/2011
Methylene chloride LCS 30.9 103 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 30.7 102 1 (< 20 ) 30 ug/L 06/30/2011
Methyl-t-butyl ether LCS 51.8 115 ( 65-125 ) 45 ug/L 06/30/2011
LCSD 50.7 113 2 (< 20 ) 45 ug/L 06/30/2011
Naphthalene LCS 31.7 106 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.3 108 2 (< 20 ) 30 ug/L 06/30/2011
n-Butylbenzene LCS 30.1 100 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 31.5 105 5 (< 20 ) 30 ug/L 06/30/2011
n-Propylbenzene LCS 30.2 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
o-Xylene LCS 33.7 112 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 34.1 114 1 (< 20 ) 30 ug/L 06/30/2011
P & M -Xylene LCS 66.9 112 ( 75-130 ) 60 ug/L 06/30/2011
LCSD 67.3 112 1 (< 20 ) 60 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
sec-Butylbenzene LCS 30.4 101 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 4 (< 20 ) 30 ug/L 06/30/2011
Styrene LCS 34.1 114 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.6 115 2 (< 20 ) 30 ug/L 06/30/2011
tert-Butylbenzene LCS 30.4 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
Tetrachloroethene LCS 34.7 116 ( 45-150 ) 30 ug/L 06/30/2011
LCSD 35.4 118 2 (< 20 ) 30 ug/L 06/30/2011
Toluene LCS 31.8 106 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 31.9 106 0 (< 20 ) 30 ug/L 06/30/2011
trans-1,2-Dichloroethene LCS 34.7 116 ( 60-140 ) 30 ug/L 06/30/2011
LCSD 36.1 120 4 (< 20 ) 30 ug/L 06/30/2011
trans-1,3-Dichloropropene LCS 32.7 109 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.8 109 0 (< 20 ) 30 ug/L 06/30/2011
Trichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.9 120 1 (< 20 ) 30 ug/L 06/30/2011
Trichlorofluoromethane LCS 37.1 124 ( 60-145 ) 30 ug/L 06/30/2011
LCSD 36.6 122 1 (< 20 ) 30 ug/L 06/30/2011
Vinyl chloride LCS 34.4 115 ( 50-145 ) 30 ug/L 06/30/2011
LCSD 33.7 112 2 (< 20 ) 30 ug/L 06/30/2011
Xylenes (total) LCS 101 112 ( 80-120 ) 90 ug/L 06/30/2011
LCSD 101 113 1 (< 20 ) 90 ug/L 06/30/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 104 ( 70-120 ) 06/30/2011
LCSD 102 2 06/30/2011
4-Bromofluorobenzene <surr> LCS 95 ( 75-120 ) 06/30/2011
LCSD 94 0 06/30/2011
Toluene-d8 <surr> LCS 99 ( 85-120 ) 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 98 1 06/30/2011
Batch
Method
Instrument
VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: July 1, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1112835 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments:
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 9.5° C
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO,
BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No discrepancies noted.
e. Data quality or usability affected? (Please Explain.)
Comments: The sample was collected approximately 30 minutes before the temperature was measured at the laboratory. It is our opinion that because the samples was collected shortly before being submitted, the temperature does not affect the quality or usability of the data.
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: LCS and LSCD recoveries for bromomethane and methyl iodide are outside QC criteria (biased high). CCV recoveries for several analytes do not meet QC criteria (biased high).
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: Case narrative does not comment on data quality or usability.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments:
b. All applicable holding times met? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 3 of 6
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.)
Comments:
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection level for the project? Yes / No / NA (Please explain.) Comments: LODs are greater than the ADEC groundwater standard for several VOC analytes. However, the results are used for disposal characterization; the results are still usable for this purpose.
e. Data quality or usability affected? (Please explain.) Comments: The data are usable for the purposed of disposal characterization.
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments:
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments:
iii. If above LOQ, what samples are affected? NA
Comments:
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments:
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: Data quality or usability is not affected.
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments:
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.)
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 4 of 6
Comments:
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments: LCS/LCSD recoveries for bromomethane are outside of QC criteria (biased high). Also, according to the case narrative LCS/LCSD recoveries for methyl iodide are biased high, although the results of this analyte are not included with the suite of VOCs on this report.
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments: The analytes were not detected in the project samples.
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: Data quality or usability is not affected.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory samples? Yes / No / NA (Please explain.) Comments:
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments:
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 5 of 6
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Methylene chloride was detected at a concentration less than the LOQ.
iv. If above LOQ, what samples are affected? NA Comments:
v. Data quality or usability affected? . Comments: Methylene chloride is a common lab contaminant and was not detected in the project sample. It is our opinion that the detection was likely due to contamination at the lab. Data quality or usability is not affected.
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.) Comments: Field duplicates were not submitted for disposal characterization samples.
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
Work Order Number: 1112835
32-1-17172-011 Former Peacock Cleaners Page 6 of 6
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: Not decontamination or equipment blank submitted due to our use of disposable sampling equipment.
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments:
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SGS North America Environmental Services – Alaska DivisionProject Manager
Steven Crupi 2011.10.26 16:54:16 -08'00'
CASE NARRATIVE Print Date: 7/1/2011
Workorder No.: 1112835
Project Name: 32-1-17172-006 4115 Lake Otis
Client Name: Shannon & Wilson, Inc.
Lab Sample ID
Sample Comments
Sample Type Client Sample ID
Refer to the sample receipt form for information on sample condition.
1035306
8260B - LCS recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCS LCS for HBN 1216746 [VXX/22361*
1035307
8260B - LCSD recovery for bromomethane and methyl iodide does not meet QC criteria (biased high). These analytes were
not detected above the LOQ in the associated samples.
LCSD LCSD for HBN 1216746 [VXX/2236*
1035312
8260B - CCV recovery for multiple analytes does not meet QC criteria (biased high). These analytes were not detected
above the LOQ in the associated samples.
CCV CCV for HBN 1216748 [VMS/12198*
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
SG S N o rth A m eric a Inc . En vir onm enta l D ivis ion 200 W e st Pot ter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs .com M em ber of SG S Group
32-1-17172-006 4115 Lake Otis
Project Manager
Steve Crupi
T: (907) 561-2120 F:
Attn: Jake Gano
5430 Fairbanks St., Ste. 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1112835
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SG S Group
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 7/1/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-006 4115 Lake Otis
Workorder No.: 1112835
Analytical Methods
Method Description Analytical Method
Volatile Organic Compounds (W) FULL SW8260B
Print Date: 7/1/2011 2:31 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1112835001 17172-006-DS1
1112835002 17172-006-WTB
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Print Date: 7/1/2011 2:31 pmDetectable Results Summary
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L912Toluene
ug/L0.800JEthylbenzene
ug/L6.12n-Butylbenzene
ug/L1081,3,5-Trimethylbenzene
ug/L23.54-Isopropyltoluene
ug/L0.660Jn-Propylbenzene
ug/L0.330JStyrene
ug/L1.59sec-Butylbenzene
ug/L15.8P & M -Xylene
ug/L2.21Naphthalene
ug/L26.9o-Xylene
ug/L42.7Xylenes (total)
ug/L98.0J1,2,4-Trimethylbenzene
ug/L1.66tert-Butylbenzene
ug/L0.840JIsopropylbenzene (Cumene)
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/L4.15JMethylene chloride
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 98.0J 100 ug/L VMS12198 VXX2236131.0 100
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 108 100 ug/L VMS12198 VXX2236131.0 100
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 23.5 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.800J 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.840J 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 2.00 U 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 2.21 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 6.12 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.660J 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 26.9 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 15.8 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 1.59 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.330J 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 1.66 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 912 100 ug/L VMS12198 VXX2236131.0 100
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 42.7 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 99.7 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 103 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 100 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-DS1
SGS Ref. #: 1112835001 Collection Date/Time: 06/30/11 12:10
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:55
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 1 Analyst: JPI
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 18:15
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835001-A
Dilution Factor: 100 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,1-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,1,2-Trichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,1-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,3-Trichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
1,2-Dibromoethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,2-Dichloroethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
1,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichlorobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
1,3-Dichloropropane 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
1,4-Dichlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
2,2-Dichloropropane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Butanone (MEK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
2-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
2-Hexanone 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
4-Chlorotoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Isopropyltoluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L VMS12198 VXX223613.10 1
Benzene 0.240 U 0.400 ug/L VMS12198 VXX223610.120 1
Bromobenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromochloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromodichloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Bromoform 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Bromomethane 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
Carbon disulfide 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
Carbon tetrachloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chlorobenzene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Chloroethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Chloroform 0.600 U 1.00 ug/L VMS12198 VXX223610.300 1
Chloromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromochloromethane 0.300 U 0.500 ug/L VMS12198 VXX223610.150 1
Dibromomethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Dichlorodifluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Ethylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Hexachlorobutadiene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Methylene chloride 4.15J 5.00 ug/L VMS12198 VXX223611.00 1
Methyl-t-butyl ether 3.00 U 5.00 ug/L VMS12198 VXX223611.50 1
Naphthalene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
n-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
n-Propylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
o-Xylene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
P & M -Xylene 1.24 U 2.00 ug/L VMS12198 VXX223610.620 1
sec-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Styrene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
tert-Butylbenzene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Tetrachloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Toluene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichloroethene 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Trichlorofluoromethane 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Vinyl chloride 0.620 U 1.00 ug/L VMS12198 VXX223610.310 1
Xylenes (total) 1.88 U 3.00 ug/L VMS12198 VXX223610.940 1
1,2-Dichloroethane-D4 <surr> 105 70-120 % VMS12198 VXX223611
4-Bromofluorobenzene <surr> 92.7 75-120 % VMS12198 VXX223611
Toluene-d8 <surr> 98.7 85-120 % VMS12198 VXX223611
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Shannon & Wilson, Inc. Print Date: 7/1/2011 2:31 pm
Client Sample ID: 17172-006-WTB
SGS Ref. #: 1112835002 Collection Date/Time: 06/30/11 12:00
Receipt Date/Time: 06/30/11 12:31Project ID: 32-1-17172-006 4115 Lake Otis
Matrix: Water (Surface, Eff., Ground)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Batch Information
Initial Prep Wt./Vol.: 5 mL
Prep Extract Vol.: 5 mL
Analytical Batch: VMS12198
Analytical Method: SW8260B
Analysis Date/Time: 06/30/11 16:28
Prep Batch: VXX22361
Prep Method: SW5030B
Prep Date/Time: 06/30/11 13:22 Container ID:1112835002-A
Dilution Factor: 1 Analyst: JPI
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,1-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1,2,2-Tetrachloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,1,2-Trichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethane 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
1,1-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,3-Trichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2,4-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dibromo-3-chloropropane 1.24 U 2.00 ug/L 06/30/110.620
1,2-Dibromoethane 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,2-Dichloroethane 0.300 U 0.500 ug/L 06/30/110.150
1,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
1,3,5-Trimethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichlorobenzene 0.620 U 1.00 ug/L 06/30/110.310
1,3-Dichloropropane 0.240 U 0.400 ug/L 06/30/110.120
1,4-Dichlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
2,2-Dichloropropane 0.620 U 1.00 ug/L 06/30/110.310
2-Butanone (MEK) 6.20 U 10.0 ug/L 06/30/113.10
2-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
2-Hexanone 6.20 U 10.0 ug/L 06/30/113.10
4-Chlorotoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Isopropyltoluene 0.620 U 1.00 ug/L 06/30/110.310
4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 ug/L 06/30/113.10
Benzene 0.240 U 0.400 ug/L 06/30/110.120
Bromobenzene 0.620 U 1.00 ug/L 06/30/110.310
Bromochloromethane 0.620 U 1.00 ug/L 06/30/110.310
Bromodichloromethane 0.300 U 0.500 ug/L 06/30/110.150
Bromoform 0.620 U 1.00 ug/L 06/30/110.310
Bromomethane 1.88 U 3.00 ug/L 06/30/110.940
Carbon disulfide 1.24 U 2.00 ug/L 06/30/110.620
Carbon tetrachloride 0.620 U 1.00 ug/L 06/30/110.310
Chlorobenzene 0.300 U 0.500 ug/L 06/30/110.150
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31Batch
Method
Date
Prep
1035305 Method Blank
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
Chloroethane 0.620 U 1.00 ug/L 06/30/110.310
Chloroform 0.600 U 1.00 ug/L 06/30/110.300
Chloromethane 0.620 U 1.00 ug/L 06/30/110.310
cis-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
cis-1,3-Dichloropropene 0.300 U 0.500 ug/L 06/30/110.150
Dibromochloromethane 0.300 U 0.500 ug/L 06/30/110.150
Dibromomethane 0.620 U 1.00 ug/L 06/30/110.310
Dichlorodifluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Ethylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Hexachlorobutadiene 0.620 U 1.00 ug/L 06/30/110.310
Isopropylbenzene (Cumene) 0.620 U 1.00 ug/L 06/30/110.310
Methylene chloride 2.00 U 5.00 ug/L 06/30/111.00
Methyl-t-butyl ether 3.00 U 5.00 ug/L 06/30/111.50
Naphthalene 1.24 U 2.00 ug/L 06/30/110.620
n-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
n-Propylbenzene 0.620 U 1.00 ug/L 06/30/110.310
o-Xylene 0.620 U 1.00 ug/L 06/30/110.310
P & M -Xylene 1.24 U 2.00 ug/L 06/30/110.620
sec-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Styrene 0.620 U 1.00 ug/L 06/30/110.310
tert-Butylbenzene 0.620 U 1.00 ug/L 06/30/110.310
Tetrachloroethene 0.620 U 1.00 ug/L 06/30/110.310
Toluene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,2-Dichloroethene 0.620 U 1.00 ug/L 06/30/110.310
trans-1,3-Dichloropropene 0.620 U 1.00 ug/L 06/30/110.310
Trichloroethene 0.620 U 1.00 ug/L 06/30/110.310
Trichlorofluoromethane 0.620 U 1.00 ug/L 06/30/110.310
Vinyl chloride 0.620 U 1.00 ug/L 06/30/110.310
Xylenes (total) 1.88 U 3.00 ug/L 06/30/110.940
Surrogates
1,2-Dichloroethane-D4 <surr> 109 70-120 % 06/30/11
4-Bromofluorobenzene <surr> 94.3 75-120 % 06/30/11
Toluene-d8 <surr> 99.4 85-120 % 06/30/11
Instrument
Method
Batch VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
QC results affect the following production samples:
1112835001, 1112835002
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,1,1,2-Tetrachloroethane LCS 33.7 112 ( 80-130 ) 30 ug/L 06/30/2011
LCSD 34.5 115 2 (< 20 ) 30 ug/L 06/30/2011
1,1,1-Trichloroethane LCS 35.1 117 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 35.9 120 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2,2-Tetrachloroethane LCS 28.8 96 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 29.4 98 2 (< 20 ) 30 ug/L 06/30/2011
1,1,2-Trichloroethane LCS 30.2 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.8 103 2 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethane LCS 33.5 112 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 33.8 113 1 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloroethene LCS 35.4 118 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.5 125 6 (< 20 ) 30 ug/L 06/30/2011
1,1-Dichloropropene LCS 33.5 112 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 34.4 115 3 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichlorobenzene LCS 31.4 105 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 33.0 110 5 (< 20 ) 30 ug/L 06/30/2011
1,2,3-Trichloropropane LCS 30.0 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 0 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trichlorobenzene LCS 31.9 106 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
1,2,4-Trimethylbenzene LCS 30.2 101 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromo-3-chloropropane LCS 29.3 98 ( 50-130 ) 30 ug/L 06/30/2011
LCSD 29.6 99 1 (< 20 ) 30 ug/L 06/30/2011
1,2-Dibromoethane LCS 33.1 110 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 0 (< 20 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
1,2-Dichlorobenzene LCS 29.9 100 ( 70-120 ) 30 ug/L 06/30/2011
LCSD 30.9 103 3 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloroethane LCS 33.5 112 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 33.7 112 0 (< 20 ) 30 ug/L 06/30/2011
1,2-Dichloropropane LCS 32.1 107 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 32.5 108 1 (< 20 ) 30 ug/L 06/30/2011
1,3,5-Trimethylbenzene LCS 29.9 100 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 3 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichlorobenzene LCS 29.8 99 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.0 103 4 (< 20 ) 30 ug/L 06/30/2011
1,3-Dichloropropane LCS 30.1 100 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 29.9 100 1 (< 20 ) 30 ug/L 06/30/2011
1,4-Dichlorobenzene LCS 30.4 101 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.8 106 5 (< 20 ) 30 ug/L 06/30/2011
2,2-Dichloropropane LCS 37.5 125 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 39.0 130 4 (< 20 ) 30 ug/L 06/30/2011
2-Butanone (MEK) LCS 102 114 ( 30-150 ) 90 ug/L 06/30/2011
LCSD 118 131 14 (< 20 ) 90 ug/L 06/30/2011
2-Chlorotoluene LCS 29.1 97 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 30.1 100 3 (< 20 ) 30 ug/L 06/30/2011
2-Hexanone LCS 86.5 96 ( 55-130 ) 90 ug/L 06/30/2011
LCSD 93.0 103 7 (< 20 ) 90 ug/L 06/30/2011
4-Chlorotoluene LCS 28.9 96 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 30.3 101 5 (< 20 ) 30 ug/L 06/30/2011
4-Isopropyltoluene LCS 31.7 106 ( 75-130 ) 30 ug/L 06/30/2011
LCSD 32.8 109 3 (< 20 ) 30 ug/L 06/30/2011
4-Methyl-2-pentanone (MIBK) LCS 111 123 ( 60-135 ) 90 ug/L 06/30/2011
LCSD 113 125 2 (< 20 ) 90 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Benzene LCS 32.8 109 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.2 111 1 (< 20 ) 30 ug/L 06/30/2011
Bromobenzene LCS 30.6 102 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 3 (< 20 ) 30 ug/L 06/30/2011
Bromochloromethane LCS 36.6 122 ( 65-130 ) 30 ug/L 06/30/2011
LCSD 37.1 124 1 (< 20 ) 30 ug/L 06/30/2011
Bromodichloromethane LCS 33.9 113 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 34.0 113 0 (< 20 ) 30 ug/L 06/30/2011
Bromoform LCS 36.5 122 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 37.6 125 3 (< 20 ) 30 ug/L 06/30/2011
Bromomethane LCS 45.1 150 ( 30-145 )* 30 ug/L 06/30/2011
LCSD 45.2 151 * 0 (< 20 ) 30 ug/L 06/30/2011
Carbon disulfide LCS 49.4 110 ( 35-160 ) 45 ug/L 06/30/2011
LCSD 49.7 110 1 (< 20 ) 45 ug/L 06/30/2011
Carbon tetrachloride LCS 36.1 120 ( 65-140 ) 30 ug/L 06/30/2011
LCSD 36.6 122 2 (< 20 ) 30 ug/L 06/30/2011
Chlorobenzene LCS 32.3 108 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 33.1 110 3 (< 20 ) 30 ug/L 06/30/2011
Chloroethane LCS 32.5 108 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 32.7 109 1 (< 20 ) 30 ug/L 06/30/2011
Chloroform LCS 33.6 112 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.0 113 1 (< 20 ) 30 ug/L 06/30/2011
Chloromethane LCS 31.3 104 ( 40-125 ) 30 ug/L 06/30/2011
LCSD 31.5 105 1 (< 20 ) 30 ug/L 06/30/2011
cis-1,2-Dichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.7 119 0 (< 20 ) 30 ug/L 06/30/2011
cis-1,3-Dichloropropene LCS 35.5 118 ( 70-130 ) 30 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 35.5 118 0 (< 20 ) 30 ug/L 06/30/2011
Dibromochloromethane LCS 34.3 114 ( 60-135 ) 30 ug/L 06/30/2011
LCSD 34.9 116 2 (< 20 ) 30 ug/L 06/30/2011
Dibromomethane LCS 33.5 112 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.6 112 0 (< 20 ) 30 ug/L 06/30/2011
Dichlorodifluoromethane LCS 38.0 127 ( 30-155 ) 30 ug/L 06/30/2011
LCSD 36.2 121 5 (< 20 ) 30 ug/L 06/30/2011
Ethylbenzene LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.8 113 2 (< 20 ) 30 ug/L 06/30/2011
Hexachlorobutadiene LCS 32.7 109 ( 50-140 ) 30 ug/L 06/30/2011
LCSD 34.6 115 6 (< 20 ) 30 ug/L 06/30/2011
Isopropylbenzene (Cumene) LCS 33.3 111 ( 75-125 ) 30 ug/L 06/30/2011
LCSD 33.9 113 2 (< 20 ) 30 ug/L 06/30/2011
Methylene chloride LCS 30.9 103 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 30.7 102 1 (< 20 ) 30 ug/L 06/30/2011
Methyl-t-butyl ether LCS 51.8 115 ( 65-125 ) 45 ug/L 06/30/2011
LCSD 50.7 113 2 (< 20 ) 45 ug/L 06/30/2011
Naphthalene LCS 31.7 106 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.3 108 2 (< 20 ) 30 ug/L 06/30/2011
n-Butylbenzene LCS 30.1 100 ( 70-135 ) 30 ug/L 06/30/2011
LCSD 31.5 105 5 (< 20 ) 30 ug/L 06/30/2011
n-Propylbenzene LCS 30.2 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
o-Xylene LCS 33.7 112 ( 80-120 ) 30 ug/L 06/30/2011
LCSD 34.1 114 1 (< 20 ) 30 ug/L 06/30/2011
P & M -Xylene LCS 66.9 112 ( 75-130 ) 60 ug/L 06/30/2011
LCSD 67.3 112 1 (< 20 ) 60 ug/L 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
sec-Butylbenzene LCS 30.4 101 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 31.6 105 4 (< 20 ) 30 ug/L 06/30/2011
Styrene LCS 34.1 114 ( 65-135 ) 30 ug/L 06/30/2011
LCSD 34.6 115 2 (< 20 ) 30 ug/L 06/30/2011
tert-Butylbenzene LCS 30.4 101 ( 70-130 ) 30 ug/L 06/30/2011
LCSD 31.0 103 2 (< 20 ) 30 ug/L 06/30/2011
Tetrachloroethene LCS 34.7 116 ( 45-150 ) 30 ug/L 06/30/2011
LCSD 35.4 118 2 (< 20 ) 30 ug/L 06/30/2011
Toluene LCS 31.8 106 ( 75-120 ) 30 ug/L 06/30/2011
LCSD 31.9 106 0 (< 20 ) 30 ug/L 06/30/2011
trans-1,2-Dichloroethene LCS 34.7 116 ( 60-140 ) 30 ug/L 06/30/2011
LCSD 36.1 120 4 (< 20 ) 30 ug/L 06/30/2011
trans-1,3-Dichloropropene LCS 32.7 109 ( 55-140 ) 30 ug/L 06/30/2011
LCSD 32.8 109 0 (< 20 ) 30 ug/L 06/30/2011
Trichloroethene LCS 35.7 119 ( 70-125 ) 30 ug/L 06/30/2011
LCSD 35.9 120 1 (< 20 ) 30 ug/L 06/30/2011
Trichlorofluoromethane LCS 37.1 124 ( 60-145 ) 30 ug/L 06/30/2011
LCSD 36.6 122 1 (< 20 ) 30 ug/L 06/30/2011
Vinyl chloride LCS 34.4 115 ( 50-145 ) 30 ug/L 06/30/2011
LCSD 33.7 112 2 (< 20 ) 30 ug/L 06/30/2011
Xylenes (total) LCS 101 112 ( 80-120 ) 90 ug/L 06/30/2011
LCSD 101 113 1 (< 20 ) 90 ug/L 06/30/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 104 ( 70-120 ) 06/30/2011
LCSD 102 2 06/30/2011
4-Bromofluorobenzene <surr> LCS 95 ( 75-120 ) 06/30/2011
LCSD 94 0 06/30/2011
Toluene-d8 <surr> LCS 99 ( 85-120 ) 06/30/2011
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 07/01/2011 14:31
Batch
Method
Date
Prep
1035306 Lab Control Sample
1035307 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-006 4115 Lake Otis
Water (Surface, Eff., Ground)
VXX22361
SW5030B
06/30/2011
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
LCSD 98 1 06/30/2011
Batch
Method
Instrument
VMS12198
SW8260B
HP 5890 Series II MS1 VJA
Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: October 25, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1114353 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments:
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 2.4° C
Work Order Number: 1114353
32-1-17172-011 Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO,
BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No discrepancies noted.
e. Data quality or usability affected? (Please Explain.)
Comments: Data quality or usability is not affected.
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: Surrogate recoveries do not meet QC criteria due to matrix interference for the following analysis in the following samples: VOCs (EPA 8260B) for Samples CS2, CS3, CS4, CS5, CS7, and the matrix spike. GRO (AK101) for Samples CS2, CS3, CS4, CS5, CS6, CS6S1, CS7, CS7S5, SWS1,
and SWS4. MSD recovery for naphthalene is outside QC criteria. MS/MSD RPDs for 1,2,3-trichlorobenzene and hexachlororbutadiene are outside QC criteria. CCV recovery for dichlorodifluoromethane does not meet QC criteria (biased high).
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: Case narrative does not comment on data quality or usability.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments: Additional VOCs provided for several samples that were not listed on the COC
Work Order Number: 1114353
32-1-17172-011 Former Peacock Cleaners Page 3 of 6
b. All applicable holding times met? Yes / No / NA (Please explain.)
Comments:
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.) Comments:
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection level for the project? Yes / No / NA (Please explain.) Comments: For non-detect results, the limit of detection (LOD) exceeds the ADEC “migration to groundwater” concentration for several VOC analytes in several samples. However, LODs are less than the interim concentration reduction threshold specified in the QAPP for analytes with a specified threshold.
e. Data quality or usability affected? (Please explain.) Comments: Because the LODs are less than the interim concentration reduction threshold for the previously identified COPCs (including GRO, DRO, PCE, and PCE daughter products), the data are still usable for the purposes of this project.
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments: Multiple method blanks are reported for some analytes due to runs at dilution.
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments:
iii. If above LOQ, what samples are affected? NA
Comments:
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments:
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: Data quality or usability is not affected.
Work Order Number: 1114353
32-1-17172-011 Former Peacock Cleaners Page 4 of 6
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples?
(LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments: LCS only for EPA 8260B and 8270D SIM, per the methods. Refer to MS/MSD RPD for precision.
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.) Comments:
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments: MS/MSD RPDs for 1,2,3-trichlorobenzene and hexachlorobutadiene are outside of QC criteria.
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments: The analytes were not detected in the project samples.
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: Data quality or usability is not affected.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory samples? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1114353
32-1-17172-011 Former Peacock Cleaners Page 5 of 6
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments: Surrogate recoveries were outside of QC criteria for VOCs and GRO for several samples. See section 4.b for a complete list.
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments: The surrogates results are flagged in the lab report. If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments: For GRO analysis, each of the samples with surrogate failures contained hydrocarbon concentrations several orders of magnitude greater than the surrogate spike. Because the surrogate results were within the DQO for the LCS/LCSD and method blank, the failure within the project samples can be attributed to high concentrations of GRO and/or matrix interference, and not to a lab QC failure. For the VOC analytes, the surrogate (toluene-d8) associated with the COPCs, including BTEX, PCE, and PCE daughter products, had recoveries within the DQO. The BFB failures for AK101 and EPA 8260B may be due to inference from other hydrocarbons (i.e. DRO) and/or matrix interference. It is our opinion that the GRO and VOC data for this project are still usable.
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments:
iv. If above LOQ, what samples are affected? NA Comments:
v. Data quality or usability affected? . Comments: Data quality or usability is not affected.
Work Order Number: 1114353
32-1-17172-011 Former Peacock Cleaners Page 6 of 6
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.) Comments: Sample CS3 is a duplicate of Sample CS2.
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments: For analytes detected in both samples, RPDs ranged from 1.8 percent (ethylbenzene) to 43 percent (cis-1,2-DCE).
iv. Data quality or usability affected? Explain. Comments: Data quality or usability not affected.
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: No decontamination or equipment blank collected, as specified in our ADEC- and EPA-approved QAPP.
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments:
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SGS North America Environmental Services – Alaska DivisionProject Manager
Steven Crupi 2011.10.10 15:17:23 -08'00'
Case NarrativeSHANNOT Shannon & Wilson, Inc.
1114824 32-1-17172-009 4501 Lake Otis
Customer:
Project:
SGS North America Inc.
Refer to the sample receipt form for information on sample condition.
1114824001 PS 17172-009-ROOTS-S1Three surrogated methanol vials were needed to preserve the VOC sample portion.
1114824002 PS 17172-009-CONCRETE-S1AK102 - The pattern is consistent with a light weathered middle distillate.AK102 - Diesel range organics result is biased high due to heavier hydrocarbons contributing to the middle distillate range.
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to the associated field samples.
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32-1-17172-009 4501 Lake Otis
Project Manager
Steve Crupi
T: (907)561-2120 F:
Attn: Shayla Marshall
5430 Fairbanks St., Ste 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1114824
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SGS Group
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Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 10/10/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-009 4501 Lake Otis
Workorder No.: 1114824
Analytical Methods
Method Description Analytical Method
Diesel Range Organics (S) AK102
VOC 8260 (S) Field Extracted SW8260B
Print Date: 10/10/2011 3:07 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1114824001 17172-009-ROOTS-S1
1114824002 17172-009-CONCRETE-S1
1114824003 17172-009-STB2
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Print Date: 10/10/2011 3:07 pmDetectable Results Summary
Client Sample ID: 17172-009-ROOTS-S1
SGS Ref. #: 1114824001 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/Kg251Tetrachloroethene
Client Sample ID: 17172-009-CONCRETE-S1
SGS Ref. #: 1114824002 Result UnitsParameter
Semivolatile Organic Fuels Department
mg/Kg275Diesel Range Organics
Volatile Gas Chromatography/Mass Spectroscopy
ug/Kg178cis-1,2-Dichloroethene
ug/Kg1880Tetrachloroethene
ug/Kg55.8Trichloroethene
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 3:07 pm
Client Sample ID: 17172-009-ROOTS-S1
SGS Ref. #: 1114824001 Collection Date/Time: 10/03/11 14:36
Receipt Date/Time: 10/03/11 17:39Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Solid/Soil (Wet Weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Benzene 9.24 U 14.8 ug/Kg VMS124634.62 1
cis-1,2-Dichloroethene 18.5 U 29.6 ug/Kg VMS124639.25 1
Ethylbenzene 18.5 U 29.6 ug/Kg VMS124639.25 1
o-Xylene 18.5 U 29.6 ug/Kg VMS124639.25 1
P & M -Xylene 35.6 U 59.3 ug/Kg VMS1246317.8 1
Tetrachloroethene 251 14.8 ug/Kg VMS124634.62 1
Toluene 18.5 U 29.6 ug/Kg VMS124639.25 1
Trichloroethene 9.24 U 14.8 ug/Kg VMS124634.62 1
Vinyl chloride 18.5 U 29.6 ug/Kg VMS124639.25 1
Xylenes (total) 73.6 U 119 ug/Kg VMS1246336.8 1
1,2-Dichloroethane-D4 <surr> 106 79-118 % VMS124631
4-Bromofluorobenzene <surr> 104 67-138 % VMS124631
Toluene-d8 <surr> 105 85-115 % VMS124631
Batch Information
Initial Prep Wt./Vol.: 42.165 gAnalytical Batch: VMS12463
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 16:24 Container ID:1114824001-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 3:07 pm
Client Sample ID: 17172-009-CONCRETE-S1
SGS Ref. #: 1114824002 Collection Date/Time: 10/03/11 15:42
Receipt Date/Time: 10/03/11 17:39Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Solid/Soil (Wet Weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Semivolatile Organic Fuels Department
DL DF
Diesel Range Organics 275 19.9 mg/Kg XFC10105 XXX258596.18 1
5a Androstane <surr> 85.5 50-150 % XFC10105 XXX258591
Batch Information
Initial Prep Wt./Vol.: 30.095 g
Prep Extract Vol.: 1 mL
Analytical Batch: XFC10105
Analytical Method: AK102
Analysis Date/Time: 10/07/11 01:00
Prep Batch: XXX25859
Prep Method: SW3550C
Prep Date/Time: 10/05/11 20:00 Container ID:1114824002-A
Dilution Factor: 1 Analyst: MCS
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 3:07 pm
Client Sample ID: 17172-009-CONCRETE-S1
SGS Ref. #: 1114824002 Collection Date/Time: 10/03/11 15:42
Receipt Date/Time: 10/03/11 17:39Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Solid/Soil (Wet Weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Benzene 8.62 U 13.8 ug/Kg VMS124634.31 1
cis-1,2-Dichloroethene 178 27.6 ug/Kg VMS124638.61 1
Ethylbenzene 17.2 U 27.6 ug/Kg VMS124638.61 1
o-Xylene 17.2 U 27.6 ug/Kg VMS124638.61 1
P & M -Xylene 33.2 U 55.2 ug/Kg VMS1246316.6 1
Tetrachloroethene 1880 13.8 ug/Kg VMS124634.31 1
Toluene 17.2 U 27.6 ug/Kg VMS124638.61 1
Trichloroethene 55.8 13.8 ug/Kg VMS124634.31 1
Vinyl chloride 17.2 U 27.6 ug/Kg VMS124638.61 1
Xylenes (total) 68.4 U 110 ug/Kg VMS1246334.2 1
1,2-Dichloroethane-D4 <surr> 107 79-118 % VMS124631
4-Bromofluorobenzene <surr> 94 67-138 % VMS124631
Toluene-d8 <surr> 108 85-115 % VMS124631
Batch Information
Initial Prep Wt./Vol.: 45.281 gAnalytical Batch: VMS12463
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 16:58 Container ID:1114824002-B
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 3:07 pm
Client Sample ID: 17172-009-STB2
SGS Ref. #: 1114824003 Collection Date/Time: 10/03/11 14:30
Receipt Date/Time: 10/03/11 17:39Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Solid/Soil (Wet Weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Benzene 7.72 U 12.4 ug/Kg VMS124633.86 1
cis-1,2-Dichloroethene 15.4 U 24.7 ug/Kg VMS124637.71 1
Ethylbenzene 15.4 U 24.7 ug/Kg VMS124637.71 1
o-Xylene 15.4 U 24.7 ug/Kg VMS124637.71 1
P & M -Xylene 29.6 U 49.5 ug/Kg VMS1246314.8 1
Tetrachloroethene 7.72 U 12.4 ug/Kg VMS124633.86 1
Toluene 15.4 U 24.7 ug/Kg VMS124637.71 1
Trichloroethene 7.72 U 12.4 ug/Kg VMS124633.86 1
Vinyl chloride 15.4 U 24.7 ug/Kg VMS124637.71 1
Xylenes (total) 61.4 U 98.9 ug/Kg VMS1246330.7 1
1,2-Dichloroethane-D4 <surr> 103 79-118 % VMS124631
4-Bromofluorobenzene <surr> 103 67-138 % VMS124631
Toluene-d8 <surr> 106 85-115 % VMS124631
Batch Information
Initial Prep Wt./Vol.: 50.552 gAnalytical Batch: VMS12463
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 15:17 Container ID:1114824003-A
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 15:07Batch
Method
Date
Prep
1057072 Method Blank
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
XXX25859
SW3550C
10/05/2011
QC results affect the following production samples:
1114824002
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Semivolatile Organic Fuels Department
Diesel Range Organics 12.4 U 20.0 mg/Kg 10/06/116.20
Surrogates
5a Androstane <surr> 83.4 60-120 % 10/06/11
Instrument
Method
Batch XFC10105
AK102
HP 7890A FID SV E R
11 of 17
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 15:07Batch
Method
Date
Prep
1057083 Method Blank
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1114824001, 1114824002, 1114824003
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
Benzene 7.80 U 12.5 ug/Kg 10/05/113.90
cis-1,2-Dichloroethene 15.6 U 25.0 ug/Kg 10/05/117.80
Ethylbenzene 15.6 U 25.0 ug/Kg 10/05/117.80
o-Xylene 15.6 U 25.0 ug/Kg 10/05/117.80
P & M -Xylene 30.0 U 50.0 ug/Kg 10/05/1115.0
Tetrachloroethene 7.80 U 12.5 ug/Kg 10/05/113.90
Toluene 15.6 U 25.0 ug/Kg 10/05/117.80
Trichloroethene 7.80 U 12.5 ug/Kg 10/05/113.90
Vinyl chloride 15.6 U 25.0 ug/Kg 10/05/117.80
Xylenes (total) 62.0 U 100 ug/Kg 10/05/1131.0
Surrogates
1,2-Dichloroethane-D4 <surr> 102 79-118 % 10/05/11
4-Bromofluorobenzene <surr> 97.1 67-138 % 10/05/11
Toluene-d8 <surr> 106 85-115 % 10/05/11
Instrument
Method
Batch VMS12463
SW8260B
HP 5890 Series II MS5 VLA
12 of 17
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 15:07
Batch
Method
Date
Prep
1057073 Lab Control Sample
1057074 Lab Control Sample Duplicate
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
XXX25859
SW3550C
10/05/2011
QC results affect the following production samples:
1114824002
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Semivolatile Organic Fuels Department
Diesel Range Organics LCS 150 90 ( 75-125 ) 167 mg/Kg 10/06/2011
LCSD 146 87 3 (< 20 ) 167 mg/Kg 10/06/2011
Surrogates
5a Androstane <surr> LCS 86 ( 60-120 ) 10/06/2011
LCSD 84 2 10/06/2011
Batch
Method
Instrument
XFC10105
AK102
HP 7890A FID SV E R
13 of 17
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 15:07
Batch
Method
Date
Prep
1057084 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1114824001, 1114824002, 1114824003
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Benzene LCS 695 93 ( 75-125 ) 750 ug/Kg 10/05/2011
cis-1,2-Dichloroethene LCS 800 107 ( 65-125 ) 750 ug/Kg 10/05/2011
Ethylbenzene LCS 800 107 ( 75-125 ) 750 ug/Kg 10/05/2011
o-Xylene LCS 806 107 ( 75-125 ) 750 ug/Kg 10/05/2011
P & M -Xylene LCS 1580 105 ( 80-125 ) 1500 ug/Kg 10/05/2011
Tetrachloroethene LCS 791 106 ( 65-140 ) 750 ug/Kg 10/05/2011
Toluene LCS 764 102 ( 70-125 ) 750 ug/Kg 10/05/2011
Trichloroethene LCS 799 107 ( 75-125 ) 750 ug/Kg 10/05/2011
Vinyl chloride LCS 855 114 ( 60-125 ) 750 ug/Kg 10/05/2011
Xylenes (total) LCS 2380 106 ( 80-125 ) 2250 ug/Kg 10/05/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 104 ( 79-118 ) 10/05/2011
4-Bromofluorobenzene <surr> LCS 106 ( 67-138 ) 10/05/2011
Toluene-d8 <surr> LCS 108 ( 85-115 ) 10/05/2011
Batch
Method
Instrument
VMS12463
SW8260B
HP 5890 Series II MS5 VLA
14 of 17
Matrix
SGS Ref.# Printed Date/Time 10/10/2011 15:07Batch
Method
Date
Original
Prep1057086 Matrix Spike
1057087 Matrix Spike Duplicate
1057085
Solid/Soil (Wet Weight)
QC results affect the following production samples:
1114824001, 1114824002, 1114824003
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
Benzene MS (11.1) U 984 92 ( 75-125 ) 1070 ug/Kg 10/05/2011
MSD 1020 96 4 (< 20 ) 1070 ug/Kg 10/05/2011
cis-1,2-Dichloroethene MS (22.2) U 1150 107 ( 65-125 ) 1070 ug/Kg 10/05/2011
MSD 1200 112 4 (< 20 ) 1070 ug/Kg 10/05/2011
Ethylbenzene MS (22.2) U 1100 103 ( 75-125 ) 1070 ug/Kg 10/05/2011
MSD 1110 104 1 (< 20 ) 1070 ug/Kg 10/05/2011
o-Xylene MS (22.2) U 1160 108 ( 75-125 ) 1070 ug/Kg 10/05/2011
MSD 1170 110 2 (< 20 ) 1070 ug/Kg 10/05/2011
P & M -Xylene MS (42.8) U 2200 103 ( 80-125 ) 2140 ug/Kg 10/05/2011
MSD 2270 106 3 (< 20 ) 2140 ug/Kg 10/05/2011
Tetrachloroethene MS (11.1) U 1150 108 ( 65-140 ) 1070 ug/Kg 10/05/2011
MSD 1130 105 2 (< 20 ) 1070 ug/Kg 10/05/2011
Toluene MS (22.2) U 1110 104 ( 70-125 ) 1070 ug/Kg 10/05/2011
MSD 1040 97 7 (< 20 ) 1070 ug/Kg 10/05/2011
Trichloroethene MS (11.1) U 1170 109 ( 75-125 ) 1070 ug/Kg 10/05/2011
MSD 1140 106 3 (< 20 ) 1070 ug/Kg 10/05/2011
Vinyl chloride MS (22.2) U 1170 109 ( 60-125 ) 1070 ug/Kg 10/05/2011
MSD 1250 116 6 (< 20 ) 1070 ug/Kg 10/05/2011
Xylenes (total) MS (88.6) U 3350 104 ( 80-125 ) 3220 ug/Kg 10/05/2011
MSD 3450 107 3 (< 20 ) 3220 ug/Kg 10/05/2011
Surrogates
1,2-Dichloroethane-D4 <surr> MS 1100 103 ( 79-118 ) 10/05/2011
MSD 1120 105 2 10/05/2011
4-Bromofluorobenzene <surr> MS 2480 87 ( 67-138 ) 10/05/2011
MSD 2450 86 2 10/05/2011
Toluene-d8 <surr> MS 1230 115 ( 85-115 ) 10/05/2011
MSD 1170 109 5 10/05/2011
Batch
Method
Instrument
VMS12463
SW8260B
HP 5890 Series II MS5 VLA
15 of 17
16 of 17
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Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: October 10, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1114824 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments:
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation
a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 4.6° C
Work Order Number: 1114824
32-1-17172-011, Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO, BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No discrepancies noted.
e. Data quality or usability affected? (Please Explain.)
Comments: Data quality or usability is not affected.
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: Diesel range organics result is biased high for Sample Concrete-S1 due to the presence of heavier hydrocarbon contributing to the middle distillate range.
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: DRO results for this sample are biased high.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments:
b. All applicable holding times met? Yes / No / NA (Please explain.) Comments:
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.) Comments: No soil samples submitted; samples are reported on a wet weight basis.
Work Order Number: 1114824
32-1-17172-011, Former Peacock Cleaners Page 3 of 6
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection
level for the project? Yes / No / NA (Please explain.) Comments:
e. Data quality or usability affected? (Please explain.) Comments:
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments:
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments:
iii. If above LOQ, what samples are affected? NA
Comments:
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments:
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: Data quality or usability is not affected.
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments: LCS only for EPA 8260B, per the method. Refer to MS/MSD RPD for precision.
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1114824
32-1-17172-011, Former Peacock Cleaners Page 4 of 6
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments:
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: Data quality or usability is not affected.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory samples? Yes / No / NA (Please explain.) Comments:
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments:
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1114824
32-1-17172-011, Former Peacock Cleaners Page 5 of 6
iv. Data quality or usability affected? Explain. Comments:
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments:
iv. If above LOQ, what samples are affected? NA Comments:
v. Data quality or usability affected? . Comments: Data quality or usability is not affected.
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.) Comments: No duplicate sample was submitted on this work order.
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: No decontamination or equipment blank collected, as specified in our ADEC- and EPA-approved QAPP.
Work Order Number: 1114824
32-1-17172-011, Former Peacock Cleaners Page 6 of 6
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments:
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1 of 14
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SGS North America Environmental Services – Alaska DivisionProject Manager
Steven Crupi 2011.10.10 16:08:11 -08'00'
CASE NARRATIVE Print Date: 10/10/2011
Workorder No.: 1114835
Project Name: 32-1-17172-009 4501 Lake Otis
Client Name: Shannon & Wilson, Inc.
Lab Sample ID
Sample Comments
Sample Type Client Sample ID
Refer to the sample receipt form for information on sample condition.
1057093
8260B - LCS surrogate recovery for toluene-D8 does not meet QC criteria (biased high). All analytes associated with this
surrogate are within control limit.
LCS LCS for HBN 1271008 [VXX/22844*
* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to
associated field samples.
SG S N o rth A m eric a Inc . En vir onm enta l D ivis ion 200 W e st Pot ter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs .com M em ber of SG S Group
2 of 14
32-1-17172-009 4501 Lake Otis
Project Manager
Steve Crupi
T: (907)561-2120 F:
Attn: Shayla Marshall
5430 Fairbanks St., Ste 3
Anchorage, AK 99518
Certification:
This data package is in compliance with the terms and conditions of the contract, both
technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or
case narrative. This certification applies only to the tested parameters and the specific
sample(s) received at the laboratory. If you have any questions regarding this report, or if we
can be of further assistance, please contact your SGS Project Manager.
1114835
Shannon & Wilson, Inc.
Workorder No.:
Client:
Project:
Laboratory Analytical Report
Contents (Bookmarked in PDF):
Cover Page
Glossary
Sample Summary Forms
Case Narrative
Sample Results Forms
Batch Summary Forms (by method)
Quality Control Summary Forms (by method)
Chain of Custody/Sample Receipt Forms
Attachments (if applicable)
SGS No rth Americ a Inc . En vir onmenta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com Member of SGS Group
3 of 14
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not
responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please
contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions
(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.
SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this
program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for
ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B,
8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all
statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental
Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:
* The analyte has exceeded allowable regulatory or control limits.
! Surrogate out of control limits.
B Indicates the analyte is found in a blank associated with the sample.
CCV Continuing Calibration Verification
CL Control Limit
D The analyte concentration is the result of a dilution.
DF Dilution Factor
DL Detection Limit (i.e., maximum method detection limit)
E The analyte result is above the calibrated range.
F Indicates value that is greater than or equal to the DL
GT Greater Than
ICV Initial Calibration Verification
J The quantitation is an estimation.
JL The analyte was positively identified, but the quantitation is a low estimation.
LCS(D) Laboratory Control Spike (Duplicate)
LOD Limit of Detection (i.e., 2xDL)
LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)
LT Less Than
M A matrix effect was present.
MB Method Blank
MS(D) Matrix Spike (Duplicate)
ND Indicates the analyte is not detected.
Q QC parameter out of acceptance range.
R Rejected
RL Reporting Limit
RPD Relative Percent Difference
U Indicates the analyte was analyzed for but not detected.
Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.
All DRO/RRO analyses are integrated per SOP.
Print Date: 10/10/2011
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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SAMPLE SUMMARY
Client Name: Shannon & Wilson, Inc.
Project Name: 32-1-17172-009 4501 Lake Otis
Workorder No.: 1114835
Analytical Methods
Method Description Analytical Method
VOC 8260 (S) Field Extracted SW8260B
Print Date: 10/10/2011 4:02 pm
Sample ID Cross Reference
Client Sample IDLab Sample ID
1114835001 17172-009-Crib-S1
1114835002 17172-009-STB3
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Print Date: 10/10/2011 4:02 pmDetectable Results Summary
Client Sample ID: 17172-009-Crib-S1
SGS Ref. #: 1114835001 Result UnitsParameter
Volatile Gas Chromatography/Mass Spectroscopy
ug/Kg813Toluene
ug/Kg17700cis-1,2-Dichloroethene
ug/Kg114000Tetrachloroethene
ug/Kg4770Trichloroethene
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 4:02 pm
Client Sample ID: 17172-009-Crib-S1
SGS Ref. #: 1114835001 Collection Date/Time: 10/04/11 09:26
Receipt Date/Time: 10/04/11 10:23Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Solid/Soil (Wet Weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Benzene 95.8 U 153 ug/Kg VMS1246447.9 1
cis-1,2-Dichloroethene 17700 307 ug/Kg VMS1246495.8 1
Ethylbenzene 192 U 307 ug/Kg VMS1246495.8 1
o-Xylene 192 U 307 ug/Kg VMS1246495.8 1
P & M -Xylene 368 U 614 ug/Kg VMS12464184 1
Tetrachloroethene 114000 1530 ug/Kg VMS12464479 10
Toluene 813 307 ug/Kg VMS1246495.8 1
Trichloroethene 4770 153 ug/Kg VMS1246447.9 1
Vinyl chloride 192 U 307 ug/Kg VMS1246495.8 1
Xylenes (total) 762 U 1230 ug/Kg VMS12464381 1
1,2-Dichloroethane-D4 <surr> 102 79-118 % VMS124641
4-Bromofluorobenzene <surr> 102 67-138 % VMS124641
Toluene-d8 <surr> 106 85-115 % VMS124641
Batch Information
Initial Prep Wt./Vol.: 8.145 gAnalytical Batch: VMS12464
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 17:49 Container ID:1114835001-B
Dilution Factor: 1 Analyst: HM
Initial Prep Wt./Vol.: 8.145 gAnalytical Batch: VMS12464
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 22:52 Container ID:1114835001-B
Dilution Factor: 10 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Shannon & Wilson, Inc. Print Date: 10/10/2011 4:02 pm
Client Sample ID: 17172-009-STB3
SGS Ref. #: 1114835002 Collection Date/Time: 10/04/11 09:20
Receipt Date/Time: 10/04/11 10:23Project ID: 32-1-17172-009 4501 Lake Otis
Matrix: Soil/Solid (dry weight)
Analytical
Batch
Prep
BatchLOQ/CL Units QualifiersParameter Result
Volatile Gas Chromatography/Mass Spectroscopy
DL DF
Benzene 7.80 U 12.5 ug/Kg VMS124643.90 1
cis-1,2-Dichloroethene 15.6 U 25.0 ug/Kg VMS124647.79 1
Ethylbenzene 15.6 U 25.0 ug/Kg VMS124647.79 1
o-Xylene 15.6 U 25.0 ug/Kg VMS124647.79 1
P & M -Xylene 30.0 U 49.9 ug/Kg VMS1246415.0 1
Tetrachloroethene 7.80 U 12.5 ug/Kg VMS124643.90 1
Toluene 15.6 U 25.0 ug/Kg VMS124647.79 1
Trichloroethene 7.80 U 12.5 ug/Kg VMS124643.90 1
Vinyl chloride 15.6 U 25.0 ug/Kg VMS124647.79 1
Xylenes (total) 62.0 U 99.9 ug/Kg VMS1246431.0 1
1,2-Dichloroethane-D4 <surr> 108 79-118 % VMS124641
4-Bromofluorobenzene <surr> 108 67-138 % VMS124641
Toluene-d8 <surr> 115 85-115 % VMS124641
Batch Information
Initial Prep Wt./Vol.: 50.061 gAnalytical Batch: VMS12464
Analytical Method: SW8260B
Analysis Date/Time: 10/05/11 16:41 Container ID:1114835002-A
Dilution Factor: 1 Analyst: HM
SGS No rth Am eric a Inc . En vir onm enta l Divis ion 200 W e st Pot ter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs .com M ember of SG S Group
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Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 16:02Batch
Method
Date
Prep
1057092 Method Blank
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1114835001, 1114835002
Parameter Results LOQ/CL UnitsAnalysis
DateDL
Volatile Gas Chromatography/Mass Spectroscopy
Benzene 7.80 U 12.5 ug/Kg 10/05/113.90
cis-1,2-Dichloroethene 15.6 U 25.0 ug/Kg 10/05/117.80
Ethylbenzene 15.6 U 25.0 ug/Kg 10/05/117.80
o-Xylene 15.6 U 25.0 ug/Kg 10/05/117.80
P & M -Xylene 30.0 U 50.0 ug/Kg 10/05/1115.0
Tetrachloroethene 7.80 U 12.5 ug/Kg 10/05/113.90
Toluene 15.6 U 25.0 ug/Kg 10/05/117.80
Trichloroethene 7.80 U 12.5 ug/Kg 10/05/113.90
Vinyl chloride 15.6 U 25.0 ug/Kg 10/05/117.80
Xylenes (total) 62.0 U 100 ug/Kg 10/05/1131.0
Surrogates
1,2-Dichloroethane-D4 <surr> 102 79-118 % 10/05/11
4-Bromofluorobenzene <surr> 103 67-138 % 10/05/11
Toluene-d8 <surr> 108 85-115 % 10/05/11
Instrument
Method
Batch VMS12464
SW8260B
HP 5890 Series II MS5 VLA
9 of 14
Matrix
SGS Ref.#
Client Name
Project Name/#
Printed Date/Time 10/10/2011 16:03
Batch
Method
Date
Prep
1057093 Lab Control Sample
Shannon & Wilson, Inc.
32-1-17172-009 4501 Lake Otis
Soil/Solid (dry weight)
QC results affect the following production samples:
1114835001, 1114835002
ParameterQC
Results
Pct
Recov
Spiked
Amount
Analysis
DateRPDLCS/LCSD
Limits
RPD
Limits
Volatile Gas Chromatography/Mass Spectroscopy
Benzene LCS 766 102 ( 75-125 ) 750 ug/Kg 10/05/2011
cis-1,2-Dichloroethene LCS 829 111 ( 65-125 ) 750 ug/Kg 10/05/2011
Ethylbenzene LCS 826 110 ( 75-125 ) 750 ug/Kg 10/05/2011
o-Xylene LCS 797 106 ( 75-125 ) 750 ug/Kg 10/05/2011
P & M -Xylene LCS 1630 109 ( 80-125 ) 1500 ug/Kg 10/05/2011
Tetrachloroethene LCS 841 112 ( 65-140 ) 750 ug/Kg 10/05/2011
Toluene LCS 808 108 ( 70-125 ) 750 ug/Kg 10/05/2011
Trichloroethene LCS 751 100 ( 75-125 ) 750 ug/Kg 10/05/2011
Vinyl chloride LCS 866 115 ( 60-125 ) 750 ug/Kg 10/05/2011
Xylenes (total) LCS 2430 108 ( 80-125 ) 2250 ug/Kg 10/05/2011
Surrogates
1,2-Dichloroethane-D4 <surr> LCS 105 ( 79-118 ) 10/05/2011
4-Bromofluorobenzene <surr> LCS 111 ( 67-138 ) 10/05/2011
Toluene-d8 <surr> LCS 117 ( 85-115 )* 10/05/2011
Batch
Method
Instrument
VMS12464
SW8260B
HP 5890 Series II MS5 VLA
10 of 14
Matrix
SGS Ref.# Printed Date/Time 10/10/2011 16:03Batch
Method
Date
Original
Prep1057095 Matrix Spike
1057096 Matrix Spike Duplicate
1057094
Solid/Soil (Wet Weight)
QC results affect the following production samples:
1114835001, 1114835002
ParameterQC
Result
Pct
Recov
Spiked
Amount Analysis
Date
MS/MSD
Limits RPDRPD
LimitsOriginal
Result Qualifiers
Volatile Gas Chromatography/Mass Spectroscopy
Benzene MS (9.26) U 895 101 ( 75-125 ) 890 ug/Kg 10/05/2011
MSD 870 98 3 (< 20 ) 890 ug/Kg 10/05/2011
cis-1,2-Dichloroethene MS (18.5) U 861 97 ( 65-125 ) 890 ug/Kg 10/05/2011
MSD 957 108 11 (< 20 ) 890 ug/Kg 10/05/2011
Ethylbenzene MS (18.5) U 928 104 ( 75-125 ) 890 ug/Kg 10/05/2011
MSD 909 102 2 (< 20 ) 890 ug/Kg 10/05/2011
o-Xylene MS (18.5) U 919 103 ( 75-125 ) 890 ug/Kg 10/05/2011
MSD 926 104 1 (< 20 ) 890 ug/Kg 10/05/2011
P & M -Xylene MS (35.6) U 1830 103 ( 80-125 ) 1780 ug/Kg 10/05/2011
MSD 1830 103 0 (< 20 ) 1780 ug/Kg 10/05/2011
Tetrachloroethene MS (9.26) U 834 94 ( 65-140 ) 890 ug/Kg 10/05/2011
MSD 884 99 6 (< 20 ) 890 ug/Kg 10/05/2011
Toluene MS (18.5) U 867 97 ( 70-125 ) 890 ug/Kg 10/05/2011
MSD 881 99 2 (< 20 ) 890 ug/Kg 10/05/2011
Trichloroethene MS (9.26) U 885 99 ( 75-125 ) 890 ug/Kg 10/05/2011
MSD 829 93 7 (< 20 ) 890 ug/Kg 10/05/2011
Vinyl chloride MS (18.5) U 939 106 ( 60-125 ) 890 ug/Kg 10/05/2011
MSD 936 105 0 (< 20 ) 890 ug/Kg 10/05/2011
Xylenes (total) MS (73.6) U 2750 103 ( 80-125 ) 2670 ug/Kg 10/05/2011
MSD 2760 103 0 (< 20 ) 2670 ug/Kg 10/05/2011
Surrogates
1,2-Dichloroethane-D4 <surr> MS 946 106 ( 79-118 ) 10/05/2011
MSD 944 106 0 10/05/2011
4-Bromofluorobenzene <surr> MS 1470 90 ( 67-138 ) 10/05/2011
MSD 1550 95 5 10/05/2011
Toluene-d8 <surr> MS 959 108 ( 85-115 ) 10/05/2011
MSD 970 109 1 10/05/2011
Batch
Method
Instrument
VMS12464
SW8260B
HP 5890 Series II MS5 VLA
11 of 14
12 of 14
13 of 14
14 of 14
Page 1 of 6
LABORATORY DATA REVIEW CHECKLIST CS Report Name: Former Peacock Cleaners, 4501 Lake Otis Parkway, Anchorage, Alaska Date: December 2011 Laboratory Report Date: October 10, 2011 Consultant Firm: Shannon & Wilson, Inc. Completed by: Jake Gano Title: Environmental Engineer Laboratory Name: SGS North America, Inc. Work Order Number: 1114835 ADEC File Number: 2100.38.511 (NOTE: NA = not applicable; Text in italics added by Shannon & Wilson, Inc.)
1. Laboratory a. Did an ADEC CS approved laboratory receive and perform all of the submitted sample
analyses? Yes / No / NA (Please explain.) Comments:
b. If the samples were transferred to another "network" laboratory or sub-contracted to an alternate laboratory, was the laboratory performing the analyses ADEC CS-approved? Yes / No / NA (Please explain.) Comments:
2. Chain of Custody (COC)
a. COC information completed, signed, and dated (including released/received by)? Yes / No / NA (Please explain.) Comments:
b. Correct analyses requested? Yes / No / NA (Please explain.) Comments:
3. Laboratory Sample Receipt Documentation
a. Sample/cooler temperature documented and within range at receipt (4° ± 2° C)?
Yes / No / NA (Please explain.) Comments: Temperature blank = 4.2° C
Work Order Number: 1114835
32-1-17172-011 Former Peacock Cleaners Page 2 of 6
b. Sample preservation acceptable - acidified waters, Methanol-preserved VOC soil (GRO, BTEX, VOCs, etc.)? Yes / No / NA (Please explain.) Comments:
c. Sample condition documented - broken, leaking (soil MeOH), zero headspace (VOC
vials)? Yes / No / NA (Please explain.) Comments: No problems noted
d. If there were any discrepancies, were they documented (e.g., incorrect sample
containers/preservation, sample temperatures outside range, insufficient sample size, missing samples)? Yes / No / NA (Please explain.) Comments: No sand in trip blank. Approved by SGS project manager to proceed with analysis.
e. Data quality or usability affected? (Please Explain.)
Comments: Data quality or usability is not affected.
4. Case Narrative
a. Present and understandable? Yes / No / NA (Please explain.) Comments:
b. Discrepancies, errors or QC failures noted by the lab? Yes / No / NA (Please explain.) Comments: Surrogate recovery (toluene-d8) for the LCS was outside of QC criteria (biased high)
c. Were corrective actions documented? Yes / No / NA (Please explain.) Comments:
d. What is the effect on data quality/usability, according to the case narrative? Comments: All analytes associated with the surrogate are within control limits.
5. Sample Results
a. Correct analyses performed/reported as requested on COC? Yes / No / NA (Please
explain.) Comments:
b. All applicable holding times met? Yes / No / NA (Please explain.) Comments:
c. All soils reported on a dry-weight basis? Yes / No / NA (Please explain.) Comments: No soil samples submitted; wood sample is reported on a wet weight basis.
Work Order Number: 1114835
32-1-17172-011 Former Peacock Cleaners Page 3 of 6
d. Are the reported LOQs less than the Cleanup Level or the minimum required detection level for the project? Yes / No / NA (Please explain.) Comments:
e. Data quality or usability affected? (Please explain.) Comments:
6. QC Samples
a. Method Blank
i. One method blank reported per matrix, analysis, and 20 samples? Yes / No / NA (Please explain.) Comments:
ii. All method blank results less than LOQ? Yes / No / NA (Please explain.) Comments:
iii. If above LOQ, what samples are affected? NA
Comments:
iv. Do the affected sample(s) have data flags? Yes / No / NA (Please explain.) Comments:
If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
v. Data quality or usability affected? (Please explain.)
Comments: Data quality or usability is not affected.
b. Laboratory Control Sample/Duplicate (LCS/LCSD)
i. Organics - One LCS/LCSD reported per matrix, analysis, and 20 samples? (LCS/LCSD required per AK methods, LCS required per SW846) Yes / No / NA (Please explain.) Comments: LCS only for EPA 8260B, per the method. Refer to MS/MSD RPD for precision.
ii. Metals/Inorganics - One LCS and one sample duplicate reported per matrix, analysis and 20 samples? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1114835
32-1-17172-011 Former Peacock Cleaners Page 4 of 6
iii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs, if applicable. (AK petroleum methods: AK101 60%-120%, AK102 75%-125%, AK103 60%-120%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
iv. Precision – All relative percent differences (RPDs) reported and less than method or laboratory limits? And project specified DQOs, if applicable. RPD reported from LCS/LCSD, MS/MSD, and or sample/sample duplicate. (AK Petroleum methods 20%; all other analyses see the laboratory QC pages) Yes / No / NA (Please explain.) Comments:
v. If %R or RPD is outside of acceptable limits, what samples are affected? Comments:
vi. Do the affected samples(s) have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
vii. Data quality or usability affected? Explain. Comments: Data quality or usability is not affected.
c. Surrogates - Organics Only
i. Are surrogate recoveries reported for organic analyses, field, QC and laboratory samples? Yes / No / NA (Please explain.) Comments:
ii. Accuracy – All percent recoveries (%R) reported and within method or laboratory limits? And project specified DQOs if applicable. (AK Petroleum methods 50-150 %R; all other analyses see the laboratory report pages) Yes / No / NA (Please explain.) Comments: Surrogate recoveries were outside of QC criteria for the LCS.
iii. Do the sample results with failed surrogate recoveries have data flags? Yes / No / NA (Please explain.) Comments: If so, are the data flags clearly defined? Yes / No / NA (Please explain.) Comments:
Work Order Number: 1114835
32-1-17172-011 Former Peacock Cleaners Page 5 of 6
iv. Data quality or usability affected? Explain. Comments: Because the LCS results are within the QC criteria, the surrogate failure does not appear to have affected the data quality.
d. Trip Blank - Volatile analyses only (GRO, BTEX, VOCs, etc.) Water and Soil
i. One trip blank reported per matrix, analysis and cooler? Yes / No / NA (Please
explain.) Comments:
ii. Is the cooler used to transport the trip blank and volatile samples clearly indicated on the COC? Yes / No / NA (Please explain if NA or no.) Comments: Only one cooler was used to transport project samples.
iii. All results less than LOQ? Yes / No / NA (Please explain.) Comments:
iv. If above LOQ, what samples are affected? NA Comments:
v. Data quality or usability affected? . Comments: Data quality or usability is not affected.
e. Field Duplicate
i. One field duplicate submitted per matrix, analysis and 10 project samples? Yes / No / NA (Please explain.) Comments: No duplicate sample was submitted on this work order.
ii. Were the field duplicates submitted blind to the lab? Yes / No / NA (Please explain.) Comments:
iii. Precision – All relative percent differences (RPDs) less than specified DQOs? (Recommended: 30% for water, 50% for soil) Yes / No / NA (Please explain.) Comments:
iv. Data quality or usability affected? Explain. Comments:
f. Decontamination or Equipment Blank (if not applicable, a comment stating why must
be entered below)
i. All results less than LOQ? Yes / No / NA (Please explain.) Comments: No decontamination or equipment blank collected, as specified in our ADEC- and EPA-approved QAPP.
Work Order Number: 1114835
32-1-17172-011 Former Peacock Cleaners Page 6 of 6
ii. If results are above LOQ, what samples are affected? NA Comments:
iii. Data quality or usability affected? Explain. Comments:
7. Other Data Flags/Qualifiers (ACOE, AFCEE, Lab-specific, etc.)
a. Are they defined and appropriate? Yes / No / NA (Please explain.) Comments: