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Appendix I Laboratory Certificates

Appendix - Department of Defence

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Page 1: Appendix - Department of Defence

AECOM RAAF Base RichmondDetailed Site Investigation

Revision 0 – 05-Jun-2018Prepared for – Department of Defence – ABN: 68706814312

Appendix ILaboratory Certificates

Page 2: Appendix - Department of Defence

AECOM RAAF Base RichmondDetailed Site Investigation

Revision 1 – 13-Jun-2018Prepared for – Department of Defence – ABN: 68706814312

I

Appendix I Laboratory Certificates

Page 3: Appendix - Department of Defence

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : EN1704797

:: LaboratoryClient Environmental Division NewcastleAECOM Australia Pty Ltd

: :ContactContact MR CLAYTON COWPER Hayley Worthington

:: AddressAddress PO BOX Q410 QVB POST OFFICE

SYDNEY NSW, AUSTRALIA 2000

5/585 Maitland Road Mayfield West

NSW Australia 2304

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone 02 8264 5100 +612 4014 2500

:: FacsimileFacsimile 02 8264 5111 +61 2 4967 7382

::Project 60547028, task 3.2 Page 1 of 3

:Order number 60547028 task 3.2 :Quote number ES2017AECOMAU0002 (SY/308/17)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : NSW_0902_PFAS (RAAF Richmond)

Sampler : JR

DatesDate Samples Received : Issue Date : 23-Nov-201723-Nov-2017 11:17

Scheduled Reporting Date: 30-Nov-2017:Client Requested Due

Date

30-Nov-2017

Delivery DetailsMode of Delivery : :Undefined Not AvailableSecurity Seal

No. of coolers/boxes : :---- Temperature ----

: : 1 / 1Rebatch of ES1728217Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 4: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : EN1704797 Amendment 02 of 3:Page

23-Nov-2017:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Any sample identifications that cannot be displayed entirely in the analysis summary table will be listed below.

EN1704797-001 : [ 08-Nov-2017 ] : 0902_MW92_20.5_081117

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

componentS

OIL

- E

A150

H

Pa

rtic

le S

ize A

na

lysi

s b

y H

ydro

me

ter:

AS

12

89

EN1704797-001 08-Nov-2017 00:00 0902_MW92_20.5_081117 ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Page 5: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : EN1704797 Amendment 03 of 3:Page

23-Nov-2017:Issue Date

Requested Deliverables

60547028

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

BEN HUNTER

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CATHERINE HANSEN

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CLAYTON COWPER

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

DERP LAB REPORTS

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

DIRK SANDERSON

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

Page 6: Appendix - Department of Defence

0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 3EN1704797

:: LaboratoryClient AECOM Australia Pty Ltd Environmental Division Newcastle

: :ContactContact MR CLAYTON COWPER Hayley Worthington

:: AddressAddress PO BOX Q410 QVB POST OFFICE

SYDNEY NSW, AUSTRALIA 2000

5/585 Maitland Road Mayfield West NSW Australia 2304

:Telephone 02 8264 5100 :Telephone +612 4014 2500

:Project 60547028, task 3.2 Date Samples Received : 23-Nov-2017 11:17

:Order number 60547028 task 3.2 Date Analysis Commenced : 29-Nov-2017

:C-O-C number ---- Issue Date : 30-Nov-2017 18:07

Sampler : JR

Site : NSW_0902_PFAS (RAAF Richmond)

Quote number : SY/308/17

1:No. of samples received

1:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Dianne Blane Laboratory Coordinator (2IC) Newcastle - Inorganics, Mayfield West, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 7: Appendix - Department of Defence

2 of 3:Page

Work Order :

:Client

EN1704797

60547028, task 3.2:Project

AECOM Australia Pty Ltd

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing

purposes.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

EA150H: Soil Particle Density required for Hydrometer analysis according to AS 1289.3.5.1 2006 was not requested by the client. Typical sediment SPD values used for calculations and consequently NATA

endorsement does not apply to hydrometer results.

l

Page 8: Appendix - Department of Defence

3 of 3:Page

Work Order :

:Client

EN1704797

60547028, task 3.2:Project

AECOM Australia Pty Ltd

Analytical Results

----------------0902_MW92_20.5_08

1117

Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------08-Nov-2017 00:00Client sampling date / time

--------------------------------EN1704797-001UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EA150: Particle Sizing

97 ---- ---- ---- ----%1----+75µm

96 ---- ---- ---- ----%1----+150µm

89 ---- ---- ---- ----%1----+300µm

74 ---- ---- ---- ----%1----+425µm

60 ---- ---- ---- ----%1----+600µm

52 ---- ---- ---- ----%1----+1180µm

48 ---- ---- ---- ----%1----+2.36mm

45 ---- ---- ---- ----%1----+4.75mm

42 ---- ---- ---- ----%1----+9.5mm

30 ---- ---- ---- ----%1----+19.0mm

<1 ---- ---- ---- ----%1----+37.5mm

<1 ---- ---- ---- ----%1----+75.0mm

EA150: Soil Classification based on Particle Size

1 ---- ---- ---- ----%1----Clay (<2 µm)

<1 ---- ---- ---- ----%1----Silt (2-60 µm)

50 ---- ---- ---- ----%1----Sand (0.06-2.00 mm)

49 ---- ---- ---- ----%1----Gravel (>2mm)

<1 ---- ---- ---- ----%1----Cobbles (>6cm)

Page 9: Appendix - Department of Defence

ALS Environmental

Newcastle, NSW

CLIENT: DATE REPORTED: 29-Nov-2017

COMPANY: DATE RECEIVED: 23-Nov-2017

ADDRESS: REPORT NO: EN1704797-001 / PSD

001PROJECT: SAMPLE ID:

Particle Size Distribution Particle Size (mm)Percent Passing

150 100%

75 100%

37.5 100%

19.0 70%

9.50 58%

4.75 55%

2.36 52%

1.18 48%

0.600 40%

0.425 26%

0.300 11%

0.150 4%

0.075 3%

Particle Size (microns)

75 2%

55 1%

39 1%

19 1%

10 1%

5 1%

1 1%

Median Particle Size (mm)* 1.770

0.00 17

Sample Comments: Analysed:

Loss on Pretreatment NA Limit of Reporting: 1%

Sample Description: Dispersion Method Shaker

Test Method: Hydrometer Type ASTM E100TRUE

Soil Particle Density (<2.36mm) #N/A g/cm3

Dianne BlaneLaboratory CoordinatorAuthorised Signatory

Certificate of Analysis

Clayton Cowper

0902_MW92_20.5_081117

27-Nov-17

AECOM Australia Pty Ltd

Median Particle Size is not covered under the current scope of ALS's NATA accreditation.

60547028, Task 3.2

Samples analysed as received.* Insufficient sample provided for Soil Particle Density analysis according to AS 1289.3.5.1—2006. * Soil Particle Density required for Hydrometer analysis according to AS 1289.3.5.1—2006 was not requested by the client . Typical sediment SPD values used for calculations and consequently, NATA endorsement does not apply to hydrometer results

SAND, GRAVEL

AS1289.3.6.3 2003

AS1289.3.6.3 states that this method is not applicable for samples containing <10% fines (<75um). Results should be assessed accordingly

PO BOX Q410 QVB POST OFFICE SYDNEY NSW, AUSTRALIA 2000

NATA Accreditation: 825 Site: NewcastleThis document is issued in accordance with NATA’s accreditation requirements.Accredited for compliance with ISO/IEC 17025. This document shall not be reproduced, except in full.

ALS Laboratory Group Pty Ltd5/585 Maitland RoadMayfield West, NSW 2304pH 02 4014 2500fax 02 4968 [email protected]

Clay | Silt | Sand | Gravel |

0%

10%

20%

30%

40%

50%

60%

70%

80%

90%

100%

0.00

1

0.00

4

0.01

6

0.06

4

0.25

6

1.02

4

4.09

6

16.3

84

65.5

36

262.

144

Grain Size (mm)

Template Version PKV7a-170725 Page 1 of 1

Page 10: Appendix - Department of Defence

False

1 1.00True

Environmental

QUALITY CONTROL REPORTWork Order : EN1704797 Page : 1 of 3

:: LaboratoryClient Environmental Division NewcastleAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER :Contact Hayley Worthington

:Address PO BOX Q410 QVB POST OFFICE

SYDNEY NSW, AUSTRALIA 2000

Address : 5/585 Maitland Road Mayfield West NSW Australia 2304

::Telephone 02 8264 5100 +612 4014 2500:Telephone

:Project 60547028, task 3.2 Date Samples Received : 23-Nov-2017

:Order number 60547028 task 3.2 Date Analysis Commenced : 29-Nov-2017

:C-O-C number ---- Issue Date : 30-Nov-2017

Sampler : JR

Site : NSW_0902_PFAS (RAAF Richmond)

Quote number : SY/308/17

No. of samples received 1:

No. of samples analysed 1:

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Dianne Blane Laboratory Coordinator (2IC) Newcastle - Inorganics, Mayfield West, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 11: Appendix - Department of Defence

2 of 3:Page

Work Order :

:Client

EN1704797

AECOM Australia Pty Ltd

60547028, task 3.2:Project

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.

l No Laboratory Duplicate (DUP) Results are required to be reported.

Page 12: Appendix - Department of Defence

3 of 3:Page

Work Order :

:Client

EN1704797

AECOM Australia Pty Ltd

60547028, task 3.2:Project

Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

l No Method Blank (MB) or Laboratory Control Spike (LCS) Results are required to be reported.

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

l No Matrix Spike (MS) or Matrix Spike Duplicate (MSD) Results are required to be reported.

Page 13: Appendix - Department of Defence

True

Environmental

QA/QC Compliance Assessment to assist with Quality ReviewWork Order : EN1704797 Page : 1 of 4

:: LaboratoryClient Environmental Division NewcastleAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER Telephone : +612 4014 2500

:Project 60547028, task 3.2 Date Samples Received : 23-Nov-2017

Site : NSW_0902_PFAS (RAAF Richmond) Issue Date : 30-Nov-2017

JR:Sampler No. of samples received : 1

:Order number 60547028 task 3.2 No. of samples analysed : 1

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l NO Laboratory Control outliers occur.

l NO Matrix Spike outliers occur.

l For all regular sample matrices, NO surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

l NO Analysis Holding Time Outliers exist.

Outliers : Frequency of Quality Control Samples

l NO Quality Control Sample Frequency Outliers exist.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 14: Appendix - Department of Defence

2 of 4:Page

Work Order :

:Client

EN1704797

AECOM Australia Pty Ltd

60547028, task 3.2:Project

Analysis Holding Time Compliance

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.

This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA150: Particle Sizing

Snap Lock Bag: Separate bag received (EA150H)

0902_MW92_20.5_081117 07-May-2018---- 29-Nov-2017----08-Nov-2017 ---- üEA150: Soil Classification based on Particle Size

Snap Lock Bag: Separate bag received (EA150H)

0902_MW92_20.5_081117 07-May-2018---- 29-Nov-2017----08-Nov-2017 ---- ü

Page 15: Appendix - Department of Defence

3 of 4:Page

Work Order :

:Client

EN1704797

AECOM Australia Pty Ltd

60547028, task 3.2:Project

Quality Control Parameter Frequency Compliance

l No Quality Control data available for this section.

Page 16: Appendix - Department of Defence

4 of 4:Page

Work Order :

:Client

EN1704797

AECOM Australia Pty Ltd

60547028, task 3.2:Project

Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

Particle Size Analysis by Hydrometer according to AS1289.3.6.3 - 2003Particle Size Analysis by Hydrometer EA150H SOIL

Page 17: Appendix - Department of Defence
Page 18: Appendix - Department of Defence
Page 19: Appendix - Department of Defence

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1716547

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8503

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60547028, TASK 3.1 Page 1 of 5

:Order number 60547028, TASK 3.1 :Quote number ES2017AECOMAU0002 (SY/308/17)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : RAAF RICHMOND

Sampler : DIRK SANDERSON

DatesDate Samples Received : Issue Date : 12-Jul-201705-Jul-2017 13:15

Scheduled Reporting Date: 18-Jul-2017:Client Requested Due

Date

18-Jul-2017

Delivery DetailsMode of Delivery : :Undefined Not intact.Security Seal

No. of coolers/boxes : :3 Temperature 0.1' C - Ice present

: : 45 / 45Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l 6/7/17: This is an updated SRA which indicates additional analysis.

l Samples 0902_QC205_040717 and 0902_QC206_040717 to be forwarded to Envirolab.l EP071: Results of sample 0902_SD011_040717 have been confirmed by re-extraction and re-analysis.

l EP231X: Poor Matrix Spike (MS) recoveries is due to target and non-target sample matrix interferences. Confirmed by

re-analysis.

l EG020: Bromine quantification may be unreliable due to its low solubility in acid, leading to variable volatility during measurement

by ICPMS.

l EP075: LOR for samples raised due to high amount of moisture present.

l EP071: Positive results for samples ES1716547_001 &021 has been confirmed by re-extraction and re-analysis.

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l TOC analysis will be conducted by ALS Brisbane.l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.

l Preliminary results will be available on the scheduled reporting date listed in this report. However the final report with

1,4-dioxane analysis will be complete on 18/7/17.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 20: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716547 Amendment 02 of 5:Page

12-Jul-2017:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

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ES1716547-025 03-Jul-2017 00:00 0902_SD001_030717 ü ü ü ü

ES1716547-033 03-Jul-2017 00:00 0902_SD009_030717 ü ü ü ü

ES1716547-035 04-Jul-2017 00:00 0902_SD011_040717 ü ü ü ü

ES1716547-036 03-Jul-2017 00:00 0902_SD012_030717 ü ü ü ü

ES1716547-038 03-Jul-2017 00:00 0902_SD014_030717 ü ü ü ü

ES1716547-045 03-Jul-2017 00:00 0902_QC108_030717 ü ü ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

SO

IL -

EA

055-1

03

Mois

ture

Conte

nt

SO

IL -

EP

003

Tota

l Org

anic

Carb

on

(T

OC

) in

So

il

SO

IL -

EP

231X

(so

lids)

PF

AS

- F

ull

Suite

(2

8 a

na

lyte

s)

SO

IL -

S-1

2

OC

/OP

Pest

icid

es

SO

IL -

S-2

3

SV

OC

/VO

C

ES1716547-025 03-Jul-2017 00:00 0902_SD001_030717 ü ü ü ü ü

ES1716547-026 04-Jul-2017 00:00 0902_SD002_040717 ü ü

ES1716547-027 04-Jul-2017 00:00 0902_SD003_040717 ü ü

ES1716547-028 04-Jul-2017 00:00 0902_SD004_040717 ü ü

ES1716547-029 04-Jul-2017 00:00 0902_SD005_040717 ü ü

ES1716547-030 04-Jul-2017 00:00 0902_SD006_040717 ü ü

ES1716547-031 04-Jul-2017 00:00 0902_SD007_040717 ü ü

ES1716547-032 03-Jul-2017 00:00 0902_SD008_030717 ü ü

ES1716547-033 03-Jul-2017 00:00 0902_SD009_030717 ü ü ü ü ü

ES1716547-034 03-Jul-2017 00:00 0902_SD010_030717 ü ü

ES1716547-035 04-Jul-2017 00:00 0902_SD011_040717 ü ü ü ü ü

ES1716547-036 03-Jul-2017 00:00 0902_SD012_030717 ü ü ü ü ü

ES1716547-037 03-Jul-2017 00:00 0902_SD013_030717 ü ü

ES1716547-038 03-Jul-2017 00:00 0902_SD014_030717 ü ü ü ü ü

ES1716547-039 03-Jul-2017 00:00 0902_SD015_030717 ü ü

ES1716547-040 03-Jul-2017 00:00 0902_SD016_030717 ü ü

ES1716547-041 03-Jul-2017 00:00 0902_SD017_030717 ü ü

ES1716547-042 04-Jul-2017 00:00 0902_SD018_040717 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 21: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716547 Amendment 03 of 5:Page

12-Jul-2017:Issue Date

SO

IL -

EA

05

5-1

03

Mo

istu

re C

onte

nt

SO

IL -

EP

00

3

Tota

l Org

an

ic C

arb

on

(T

OC

) in

Soil

SO

IL -

EP

23

1X

(so

lids)

PF

AS

- F

ull

Suite

(28 a

naly

tes)

SO

IL -

S-1

2

OC

/OP

Pe

stic

ides

SO

IL -

S-2

3

SV

OC

/VO

C

ES1716547-043 04-Jul-2017 00:00 0902_SD019_040717 ü ü

ES1716547-044 03-Jul-2017 00:00 0902_QC106_030717 ü ü

ES1716547-045 03-Jul-2017 00:00 0902_QC108_030717 ü ü ü ü ü

WA

TE

R -

EA

01

5H

To

tal D

isso

lve

d S

olid

s -

Hig

h L

eve

l

WA

TE

R -

EK

05

5G

Am

mo

nia

as

N B

y D

iscr

ete

An

aly

ser

WA

TE

R -

EP

11

6

1.4

-Dio

xan

e

WA

TE

R -

EP

23

1X

PF

AS

- F

ull

Su

ite (

28

an

aly

tes)

WA

TE

R -

NT

-01

& 0

2A

Ca

, M

g, N

a, K

, C

l, S

O4

, A

lka

linity

& F

luo

ride

WA

TE

R -

W-2

3

SV

OC

/VO

C

WA

TE

R -

W-2

6

TR

H/B

TE

XN

/PA

H/8

Me

tals

ES1716547-001 03-Jul-2017 00:00 0902_SW001_030717 ü ü ü ü ü ü

ES1716547-002 04-Jul-2017 00:00 0902_SW002_040717 ü

ES1716547-003 04-Jul-2017 00:00 0902_SW003_040717 ü

ES1716547-004 04-Jul-2017 00:00 0902_SW004_040717 ü

ES1716547-005 04-Jul-2017 00:00 0902_SW005_040717 ü

ES1716547-006 04-Jul-2017 00:00 0902_SW006_040717 ü

ES1716547-007 04-Jul-2017 00:00 0902_SW007_040717 ü

ES1716547-008 03-Jul-2017 00:00 0902_SW008_030717 ü

ES1716547-009 03-Jul-2017 00:00 0902_SW009_030717 ü ü ü ü ü ü

ES1716547-010 03-Jul-2017 00:00 0902_SW010_030717 ü

ES1716547-011 04-Jul-2017 00:00 0902_SW011_040717 ü ü ü ü ü ü ü

ES1716547-012 03-Jul-2017 00:00 0902_SW012_030717 ü ü ü ü ü ü

ES1716547-013 03-Jul-2017 00:00 0902_SW013_030717 ü

ES1716547-014 03-Jul-2017 00:00 0902_SW014_030717 ü ü ü ü ü ü

ES1716547-015 03-Jul-2017 00:00 0902_SW015_030717 ü

ES1716547-016 03-Jul-2017 00:00 0902_SW016_030717 ü

ES1716547-017 03-Jul-2017 00:00 0902_SW017_030717 ü

ES1716547-018 04-Jul-2017 00:00 0902_SW018_040717 ü

ES1716547-019 04-Jul-2017 00:00 0902_SW019_040717 ü

ES1716547-020 03-Jul-2017 00:00 0902_QC105_030717 ü

ES1716547-021 03-Jul-2017 00:00 0902_QC107_030717 ü ü ü ü ü ü

ES1716547-022 03-Jul-2017 00:00 0902_QC504_030717 ü ü ü ü

ES1716547-023 04-Jul-2017 00:00 0902_QC505_040717 ü ü ü ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 22: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716547 Amendment 04 of 5:Page

12-Jul-2017:Issue Date

WA

TE

R -

EK

07

1G

Rea

ctiv

e P

hosp

ho

rus

by

Dis

cre

te a

naly

ser

WA

TE

R -

NT

-04

Nitr

ite a

nd N

itrate

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

ES1716547-011 04-Jul-2017 00:00 0902_SW011_040717 ü ü

ES1716547-024 04-Jul-2017 00:00 0902_QC506_040717 ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Page 23: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716547 Amendment 05 of 5:Page

12-Jul-2017:Issue Date

Requested Deliverables

60547028

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

BEN HUNTER2

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CATHERINE HANSEN

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CLAYTON COWPER

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

DIRK SANDERSON

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

Page 24: Appendix - Department of Defence

0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 93ES1716547

:: LaboratoryClient AECOM Australia Pty Ltd Environmental Division Sydney

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield NSW Australia 2164

:Telephone +61 02 8934 0000 :Telephone +61 2 8784 8503

:Project 60547028, TASK 3.1 Date Samples Received : 05-Jul-2017 13:15

:Order number 60547028, TASK 3.1 Date Analysis Commenced : 06-Jul-2017

:C-O-C number ---- Issue Date : 17-Jul-2017 10:35

Sampler : DIRK SANDERSON

Site : RAAF RICHMOND

Quote number : SY/308/17

45:No. of samples received

45:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Dian Dao Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Sanjeshni Jyoti Senior Chemist Volatiles Sydney Organics, Smithfield, NSW

Satishkumar Trivedi Acid Sulfate Soils Supervisor Brisbane Acid Sulphate Soils, Stafford, QLD

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 25: Appendix - Department of Defence

2 of 93:Page

Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When no sampling time is provided, the sampling time will default 00:00 on the date of sampling. If no sampling date is provided, the sampling date will be assumed by the laboratory and displayed in brackets without a

time component.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

EG020: Bromine quantification may be unreliable due to its low solubility in acid, leading to variable volatility during measurement by ICPMS.l

EP075: LOR for samples raised due to high amount of moisture present.l

EP071: Positive results for samples ES1716547_001 &021 has been confirmed by re-extraction and re-analysis.l

EP071: Results of sample 0902_SD011_040717 have been confirmed by re-extraction and re-analysis.l

EP231X: Poor Matrix Spike (MS) recoveries is due to target and non-target sample matrix interferences. Confirmed by re-analysis.l

EP231: Particular samples required dilution due to the presence of high level contaminants. LOR values have been adjusted accordingly.l

EP075: 'Sum of PAH' is the sum of the USEPA 16 priority PAHsl

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero, for 'TEQ 1/2LOR' are treated as half the reported LOR, and for 'TEQ LOR' are treated as being equal to the reported LOR.

Note: TEQ 1/2LOR and TEQ LOR will calculate as 0.6mg/Kg and 1.2mg/Kg respectively for samples with non-detects for all of the eight TEQ PAHs.

l

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero.

l

ED007 and ED008: When Exchangeable Al is reported from these methods, it should be noted that Rayment & Lyons (2011) suggests Exchange Acidity by 1M KCl - Method 15G1 (ED005) is a more suitable method

for the determination of exchange acidity (H+ + Al3+).

l

Page 26: Appendix - Department of Defence

3 of 93:Page

Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EA055: Moisture Content (Dried @ 105-110°C)

24.0 64.2 41.8 49.1 39.5%1----Moisture Content

ED007: Exchangeable Cations

2.9 ---- ---- ---- ----meq/100g0.1----Exchangeable Calcium

3.0 ---- ---- ---- ----meq/100g0.1----Exchangeable Magnesium

0.3 ---- ---- ---- ----meq/100g0.1----Exchangeable Potassium

0.2 ---- ---- ---- ----meq/100g0.1----Exchangeable Sodium

6.4 ---- ---- ---- ----meq/100g0.1----Cation Exchange Capacity

EG005T: Total Metals by ICP-AES

10700Iron ---- ---- ---- ----mg/kg507439-89-6

<5Arsenic ---- ---- ---- ----mg/kg57440-38-2

<1Cadmium ---- ---- ---- ----mg/kg17440-43-9

8Chromium ---- ---- ---- ----mg/kg27440-47-3

5Copper ---- ---- ---- ----mg/kg57440-50-8

8Lead ---- ---- ---- ----mg/kg57439-92-1

4Nickel ---- ---- ---- ----mg/kg27440-02-0

36Zinc ---- ---- ---- ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

<0.1Mercury ---- ---- ---- ----mg/kg0.17439-97-6

EP003: Total Organic Carbon (TOC) in Soil

0.22 ---- ---- ---- ----%0.02----Total Organic Carbon

EP068A: Organochlorine Pesticides (OC)

<0.05alpha-BHC ---- ---- ---- ----mg/kg0.05319-84-6

<0.05Hexachlorobenzene (HCB) ---- ---- ---- ----mg/kg0.05118-74-1

<0.05beta-BHC ---- ---- ---- ----mg/kg0.05319-85-7

<0.05gamma-BHC ---- ---- ---- ----mg/kg0.0558-89-9

<0.05delta-BHC ---- ---- ---- ----mg/kg0.05319-86-8

<0.05Heptachlor ---- ---- ---- ----mg/kg0.0576-44-8

<0.05Aldrin ---- ---- ---- ----mg/kg0.05309-00-2

<0.05Heptachlor epoxide ---- ---- ---- ----mg/kg0.051024-57-3

<0.05^ ---- ---- ---- ----mg/kg0.05----Total Chlordane (sum)

<0.05trans-Chlordane ---- ---- ---- ----mg/kg0.055103-74-2

<0.05alpha-Endosulfan ---- ---- ---- ----mg/kg0.05959-98-8

<0.05cis-Chlordane ---- ---- ---- ----mg/kg0.055103-71-9

<0.05Dieldrin ---- ---- ---- ----mg/kg0.0560-57-1

Page 27: Appendix - Department of Defence

4 of 93:Page

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:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP068A: Organochlorine Pesticides (OC) - Continued

<0.054.4`-DDE ---- ---- ---- ----mg/kg0.0572-55-9

<0.05Endrin ---- ---- ---- ----mg/kg0.0572-20-8

<0.05beta-Endosulfan ---- ---- ---- ----mg/kg0.0533213-65-9

<0.05^ Endosulfan (sum) ---- ---- ---- ----mg/kg0.05115-29-7

<0.054.4`-DDD ---- ---- ---- ----mg/kg0.0572-54-8

<0.05Endrin aldehyde ---- ---- ---- ----mg/kg0.057421-93-4

<0.05Endosulfan sulfate ---- ---- ---- ----mg/kg0.051031-07-8

<0.24.4`-DDT ---- ---- ---- ----mg/kg0.250-29-3

<0.05Endrin ketone ---- ---- ---- ----mg/kg0.0553494-70-5

<0.2Methoxychlor ---- ---- ---- ----mg/kg0.272-43-5

<0.05^ Sum of Aldrin + Dieldrin ---- ---- ---- ----mg/kg0.05309-00-2/60-57-1

<0.05^ Sum of DDD + DDE + DDT ---- ---- ---- ----mg/kg0.0572-54-8/72-55-9/5

0-2

EP068B: Organophosphorus Pesticides (OP)

<0.05Dichlorvos ---- ---- ---- ----mg/kg0.0562-73-7

<0.05Demeton-S-methyl ---- ---- ---- ----mg/kg0.05919-86-8

<0.2Monocrotophos ---- ---- ---- ----mg/kg0.26923-22-4

<0.05Dimethoate ---- ---- ---- ----mg/kg0.0560-51-5

<0.05Diazinon ---- ---- ---- ----mg/kg0.05333-41-5

<0.05Chlorpyrifos-methyl ---- ---- ---- ----mg/kg0.055598-13-0

<0.2Parathion-methyl ---- ---- ---- ----mg/kg0.2298-00-0

<0.05Malathion ---- ---- ---- ----mg/kg0.05121-75-5

<0.05Fenthion ---- ---- ---- ----mg/kg0.0555-38-9

<0.05Chlorpyrifos ---- ---- ---- ----mg/kg0.052921-88-2

<0.2Parathion ---- ---- ---- ----mg/kg0.256-38-2

<0.05Pirimphos-ethyl ---- ---- ---- ----mg/kg0.0523505-41-1

<0.05Chlorfenvinphos ---- ---- ---- ----mg/kg0.05470-90-6

<0.05Bromophos-ethyl ---- ---- ---- ----mg/kg0.054824-78-6

<0.05Fenamiphos ---- ---- ---- ----mg/kg0.0522224-92-6

<0.05Prothiofos ---- ---- ---- ----mg/kg0.0534643-46-4

<0.05Ethion ---- ---- ---- ----mg/kg0.05563-12-2

<0.05Carbophenothion ---- ---- ---- ----mg/kg0.05786-19-6

<0.05Azinphos Methyl ---- ---- ---- ----mg/kg0.0586-50-0

EP074A: Monocyclic Aromatic Hydrocarbons

<0.5Styrene ---- ---- ---- ----mg/kg0.5100-42-5

Page 28: Appendix - Department of Defence

5 of 93:Page

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:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP074A: Monocyclic Aromatic Hydrocarbons - Continued

<0.5Isopropylbenzene ---- ---- ---- ----mg/kg0.598-82-8

<0.5n-Propylbenzene ---- ---- ---- ----mg/kg0.5103-65-1

<0.51.3.5-Trimethylbenzene ---- ---- ---- ----mg/kg0.5108-67-8

<0.5sec-Butylbenzene ---- ---- ---- ----mg/kg0.5135-98-8

<0.51.2.4-Trimethylbenzene ---- ---- ---- ----mg/kg0.595-63-6

<0.5tert-Butylbenzene ---- ---- ---- ----mg/kg0.598-06-6

<0.5p-Isopropyltoluene ---- ---- ---- ----mg/kg0.599-87-6

<0.5n-Butylbenzene ---- ---- ---- ----mg/kg0.5104-51-8

EP074B: Oxygenated Compounds

<5Vinyl Acetate ---- ---- ---- ----mg/kg5108-05-4

<52-Butanone (MEK) ---- ---- ---- ----mg/kg578-93-3

<54-Methyl-2-pentanone (MIBK) ---- ---- ---- ----mg/kg5108-10-1

<52-Hexanone (MBK) ---- ---- ---- ----mg/kg5591-78-6

EP074C: Sulfonated Compounds

<0.5Carbon disulfide ---- ---- ---- ----mg/kg0.575-15-0

EP074D: Fumigants

<0.52.2-Dichloropropane ---- ---- ---- ----mg/kg0.5594-20-7

<0.51.2-Dichloropropane ---- ---- ---- ----mg/kg0.578-87-5

<0.5cis-1.3-Dichloropropylene ---- ---- ---- ----mg/kg0.510061-01-5

<0.5trans-1.3-Dichloropropylene ---- ---- ---- ----mg/kg0.510061-02-6

<0.51.2-Dibromoethane (EDB) ---- ---- ---- ----mg/kg0.5106-93-4

EP074E: Halogenated Aliphatic Compounds

<5Dichlorodifluoromethane ---- ---- ---- ----mg/kg575-71-8

<5Chloromethane ---- ---- ---- ----mg/kg574-87-3

<5Vinyl chloride ---- ---- ---- ----mg/kg575-01-4

<5Bromomethane ---- ---- ---- ----mg/kg574-83-9

<5Chloroethane ---- ---- ---- ----mg/kg575-00-3

<5Trichlorofluoromethane ---- ---- ---- ----mg/kg575-69-4

<0.51.1-Dichloroethene ---- ---- ---- ----mg/kg0.575-35-4

<0.5Iodomethane ---- ---- ---- ----mg/kg0.574-88-4

<0.5trans-1.2-Dichloroethene ---- ---- ---- ----mg/kg0.5156-60-5

<0.51.1-Dichloroethane ---- ---- ---- ----mg/kg0.575-34-3

<0.5cis-1.2-Dichloroethene ---- ---- ---- ----mg/kg0.5156-59-2

<0.51.1.1-Trichloroethane ---- ---- ---- ----mg/kg0.571-55-6

Page 29: Appendix - Department of Defence

6 of 93:Page

Work Order :

:Client

ES1716547

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Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<0.51.1-Dichloropropylene ---- ---- ---- ----mg/kg0.5563-58-6

<0.5Carbon Tetrachloride ---- ---- ---- ----mg/kg0.556-23-5

<0.51.2-Dichloroethane ---- ---- ---- ----mg/kg0.5107-06-2

<0.5Trichloroethene ---- ---- ---- ----mg/kg0.579-01-6

<0.5Dibromomethane ---- ---- ---- ----mg/kg0.574-95-3

<0.51.1.2-Trichloroethane ---- ---- ---- ----mg/kg0.579-00-5

<0.51.3-Dichloropropane ---- ---- ---- ----mg/kg0.5142-28-9

<0.5Tetrachloroethene ---- ---- ---- ----mg/kg0.5127-18-4

<0.51.1.1.2-Tetrachloroethane ---- ---- ---- ----mg/kg0.5630-20-6

<0.5trans-1.4-Dichloro-2-butene ---- ---- ---- ----mg/kg0.5110-57-6

<0.5cis-1.4-Dichloro-2-butene ---- ---- ---- ----mg/kg0.51476-11-5

<0.51.1.2.2-Tetrachloroethane ---- ---- ---- ----mg/kg0.579-34-5

<0.51.2.3-Trichloropropane ---- ---- ---- ----mg/kg0.596-18-4

<0.5Pentachloroethane ---- ---- ---- ----mg/kg0.576-01-7

<0.51.2-Dibromo-3-chloropropane ---- ---- ---- ----mg/kg0.596-12-8

EP074F: Halogenated Aromatic Compounds

<0.5Chlorobenzene ---- ---- ---- ----mg/kg0.5108-90-7

<0.5Bromobenzene ---- ---- ---- ----mg/kg0.5108-86-1

<0.52-Chlorotoluene ---- ---- ---- ----mg/kg0.595-49-8

<0.54-Chlorotoluene ---- ---- ---- ----mg/kg0.5106-43-4

<0.51.2.3-Trichlorobenzene ---- ---- ---- ----mg/kg0.587-61-6

EP074G: Trihalomethanes

<0.5Chloroform ---- ---- ---- ----mg/kg0.567-66-3

<0.5Bromodichloromethane ---- ---- ---- ----mg/kg0.575-27-4

<0.5Dibromochloromethane ---- ---- ---- ----mg/kg0.5124-48-1

<0.5Bromoform ---- ---- ---- ----mg/kg0.575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.5Naphthalene ---- ---- ---- ----mg/kg0.591-20-3

<0.5Acenaphthylene ---- ---- ---- ----mg/kg0.5208-96-8

<0.5Acenaphthene ---- ---- ---- ----mg/kg0.583-32-9

<0.5Fluorene ---- ---- ---- ----mg/kg0.586-73-7

<0.5Phenanthrene ---- ---- ---- ----mg/kg0.585-01-8

<0.5Anthracene ---- ---- ---- ----mg/kg0.5120-12-7

<0.5Fluoranthene ---- ---- ---- ----mg/kg0.5206-44-0

Page 30: Appendix - Department of Defence

7 of 93:Page

Work Order :

:Client

ES1716547

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AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<0.5Pyrene ---- ---- ---- ----mg/kg0.5129-00-0

<0.5Benz(a)anthracene ---- ---- ---- ----mg/kg0.556-55-3

<0.5Chrysene ---- ---- ---- ----mg/kg0.5218-01-9

<0.5Benzo(b+j)fluoranthene ---- ---- ---- ----mg/kg0.5205-99-2 205-82-3

<0.5Benzo(k)fluoranthene ---- ---- ---- ----mg/kg0.5207-08-9

<0.5Benzo(a)pyrene ---- ---- ---- ----mg/kg0.550-32-8

<0.5Indeno(1.2.3.cd)pyrene ---- ---- ---- ----mg/kg0.5193-39-5

<0.5Dibenz(a.h)anthracene ---- ---- ---- ----mg/kg0.553-70-3

<0.5Benzo(g.h.i)perylene ---- ---- ---- ----mg/kg0.5191-24-2

<0.5^ ---- ---- ---- ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

0.6^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

1.2^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP075A: Phenolic Compounds

<0.5Phenol ---- ---- ---- ----mg/kg0.5108-95-2

<0.52-Chlorophenol ---- ---- ---- ----mg/kg0.595-57-8

<0.52-Methylphenol ---- ---- ---- ----mg/kg0.595-48-7

<0.63- & 4-Methylphenol ---- ---- ---- ----mg/kg0.51319-77-3

<0.52-Nitrophenol ---- ---- ---- ----mg/kg0.588-75-5

<0.52.4-Dimethylphenol ---- ---- ---- ----mg/kg0.5105-67-9

<0.52.4-Dichlorophenol ---- ---- ---- ----mg/kg0.5120-83-2

<0.52.6-Dichlorophenol ---- ---- ---- ----mg/kg0.587-65-0

<0.54-Chloro-3-methylphenol ---- ---- ---- ----mg/kg0.559-50-7

<0.52.4.6-Trichlorophenol ---- ---- ---- ----mg/kg0.588-06-2

<0.52.4.5-Trichlorophenol ---- ---- ---- ----mg/kg0.595-95-4

<1Pentachlorophenol ---- ---- ---- ----mg/kg187-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<0.52-Methylnaphthalene ---- ---- ---- ----mg/kg0.591-57-6

<0.52-Chloronaphthalene ---- ---- ---- ----mg/kg0.591-58-7

<0.5N-2-Fluorenyl Acetamide ---- ---- ---- ----mg/kg0.553-96-3

<0.57.12-Dimethylbenz(a)anthracene ---- ---- ---- ----mg/kg0.557-97-6

<0.53-Methylcholanthrene ---- ---- ---- ----mg/kg0.556-49-5

EP075C: Phthalate Esters

<0.5Dimethyl phthalate ---- ---- ---- ----mg/kg0.5131-11-3

Page 31: Appendix - Department of Defence

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:Client

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Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<0.5Diethyl phthalate ---- ---- ---- ----mg/kg0.584-66-2

<0.5Di-n-butyl phthalate ---- ---- ---- ----mg/kg0.584-74-2

<0.5Butyl benzyl phthalate ---- ---- ---- ----mg/kg0.585-68-7

<5.0bis(2-ethylhexyl) phthalate ---- ---- ---- ----mg/kg5117-81-7

<0.5Di-n-octylphthalate ---- ---- ---- ----mg/kg0.5117-84-0

EP075D: Nitrosamines

<0.5N-Nitrosomethylethylamine ---- ---- ---- ----mg/kg0.510595-95-6

<0.5N-Nitrosodiethylamine ---- ---- ---- ----mg/kg0.555-18-5

<1.0N-Nitrosopyrrolidine ---- ---- ---- ----mg/kg1930-55-2

<0.5N-Nitrosomorpholine ---- ---- ---- ----mg/kg0.559-89-2

<0.5N-Nitrosodi-n-propylamine ---- ---- ---- ----mg/kg0.5621-64-7

<0.5N-Nitrosopiperidine ---- ---- ---- ----mg/kg0.5100-75-4

<0.5N-Nitrosodibutylamine ---- ---- ---- ----mg/kg0.5924-16-3

<1.0N-Nitrosodiphenyl &

Diphenylamine

---- ---- ---- ----mg/kg186-30-6 122-39-4

<0.5Methapyrilene ---- ---- ---- ----mg/kg0.591-80-5

EP075E: Nitroaromatics and Ketones

<0.52-Picoline ---- ---- ---- ----mg/kg0.5109-06-8

<0.5Acetophenone ---- ---- ---- ----mg/kg0.598-86-2

<0.5Nitrobenzene ---- ---- ---- ----mg/kg0.598-95-3

<0.5Isophorone ---- ---- ---- ----mg/kg0.578-59-1

<1.02.6-Dinitrotoluene ---- ---- ---- ----mg/kg1606-20-2

<1.02.4-Dinitrotoluene ---- ---- ---- ----mg/kg1121-14-2

<0.51-Naphthylamine ---- ---- ---- ----mg/kg0.5134-32-7

<0.54-Nitroquinoline-N-oxide ---- ---- ---- ----mg/kg0.556-57-5

<0.55-Nitro-o-toluidine ---- ---- ---- ----mg/kg0.599-55-8

<1Azobenzene ---- ---- ---- ----mg/kg1103-33-3

<0.51.3.5-Trinitrobenzene ---- ---- ---- ----mg/kg0.599-35-4

<0.5Phenacetin ---- ---- ---- ----mg/kg0.562-44-2

<0.54-Aminobiphenyl ---- ---- ---- ----mg/kg0.592-67-1

<0.5Pentachloronitrobenzene ---- ---- ---- ----mg/kg0.582-68-8

<0.5Pronamide ---- ---- ---- ----mg/kg0.523950-58-5

<0.5Dimethylaminoazobenzene ---- ---- ---- ----mg/kg0.560-11-7

<0.5Chlorobenzilate ---- ---- ---- ----mg/kg0.5510-15-6

Page 32: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP075F: Haloethers

<0.5Bis(2-chloroethyl) ether ---- ---- ---- ----mg/kg0.5111-44-4

<0.5Bis(2-chloroethoxy) methane ---- ---- ---- ----mg/kg0.5111-91-1

<0.54-Chlorophenyl phenyl ether ---- ---- ---- ----mg/kg0.57005-72-3

<0.54-Bromophenyl phenyl ether ---- ---- ---- ----mg/kg0.5101-55-3

EP075G: Chlorinated Hydrocarbons

<0.51.3-Dichlorobenzene ---- ---- ---- ----mg/kg0.5541-73-1

<0.51.4-Dichlorobenzene ---- ---- ---- ----mg/kg0.5106-46-7

<0.51.2-Dichlorobenzene ---- ---- ---- ----mg/kg0.595-50-1

<0.5Hexachloroethane ---- ---- ---- ----mg/kg0.567-72-1

<0.51.2.4-Trichlorobenzene ---- ---- ---- ----mg/kg0.5120-82-1

<0.5Hexachloropropylene ---- ---- ---- ----mg/kg0.51888-71-7

<0.5Hexachlorobutadiene ---- ---- ---- ----mg/kg0.587-68-3

<2.5Hexachlorocyclopentadiene ---- ---- ---- ----mg/kg2.577-47-4

<0.5Pentachlorobenzene ---- ---- ---- ----mg/kg0.5608-93-5

<1.0Hexachlorobenzene (HCB) ---- ---- ---- ----mg/kg1118-74-1

EP075H: Anilines and Benzidines

<0.5Aniline ---- ---- ---- ----mg/kg0.562-53-3

<0.54-Chloroaniline ---- ---- ---- ----mg/kg0.5106-47-8

<1.02-Nitroaniline ---- ---- ---- ----mg/kg188-74-4

<1.03-Nitroaniline ---- ---- ---- ----mg/kg199-09-2

<0.5Dibenzofuran ---- ---- ---- ----mg/kg0.5132-64-9

<0.54-Nitroaniline ---- ---- ---- ----mg/kg0.5100-01-6

<0.5Carbazole ---- ---- ---- ----mg/kg0.586-74-8

<0.53.3`-Dichlorobenzidine ---- ---- ---- ----mg/kg0.591-94-1

EP075I: Organochlorine Pesticides

<0.5alpha-BHC ---- ---- ---- ----mg/kg0.5319-84-6

<0.5beta-BHC ---- ---- ---- ----mg/kg0.5319-85-7

<0.5gamma-BHC ---- ---- ---- ----mg/kg0.558-89-9

<0.5delta-BHC ---- ---- ---- ----mg/kg0.5319-86-8

<0.5Heptachlor ---- ---- ---- ----mg/kg0.576-44-8

<0.5Aldrin ---- ---- ---- ----mg/kg0.5309-00-2

<0.5Heptachlor epoxide ---- ---- ---- ----mg/kg0.51024-57-3

<0.5alpha-Endosulfan ---- ---- ---- ----mg/kg0.5959-98-8

<0.54.4`-DDE ---- ---- ---- ----mg/kg0.572-55-9

Page 33: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<0.5Dieldrin ---- ---- ---- ----mg/kg0.560-57-1

<0.5Endrin ---- ---- ---- ----mg/kg0.572-20-8

<0.5beta-Endosulfan ---- ---- ---- ----mg/kg0.533213-65-9

<0.54.4`-DDD ---- ---- ---- ----mg/kg0.572-54-8

<0.5Endosulfan sulfate ---- ---- ---- ----mg/kg0.51031-07-8

<1.04.4`-DDT ---- ---- ---- ----mg/kg150-29-3

EP075J: Organophosphorus Pesticides

<0.5Dichlorvos ---- ---- ---- ----mg/kg0.562-73-7

<0.5Dimethoate ---- ---- ---- ----mg/kg0.560-51-5

<0.5Diazinon ---- ---- ---- ----mg/kg0.5333-41-5

<0.5Chlorpyrifos-methyl ---- ---- ---- ----mg/kg0.55598-13-0

<0.5Malathion ---- ---- ---- ----mg/kg0.5121-75-5

<0.5Fenthion ---- ---- ---- ----mg/kg0.555-38-9

<0.5Chlorpyrifos ---- ---- ---- ----mg/kg0.52921-88-2

<0.5Pirimphos-ethyl ---- ---- ---- ----mg/kg0.523505-41-1

<0.5Chlorfenvinphos ---- ---- ---- ----mg/kg0.5470-90-6

<0.5Prothiofos ---- ---- ---- ----mg/kg0.534643-46-4

<0.5Ethion ---- ---- ---- ----mg/kg0.5563-12-2

EP080/071: Total Petroleum Hydrocarbons

<10 ---- ---- ---- ----mg/kg10----C6 - C9 Fraction

<50 ---- ---- ---- ----mg/kg50----C10 - C14 Fraction

<100 ---- ---- ---- ----mg/kg100----C15 - C28 Fraction

<100 ---- ---- ---- ----mg/kg100----C29 - C36 Fraction

<50^ ---- ---- ---- ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction ---- ---- ---- ----mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

---- ---- ---- ----mg/kg10C6_C10-BTEX

<50 ---- ---- ---- ----mg/kg50---->C10 - C16 Fraction

<100 ---- ---- ---- ----mg/kg100---->C16 - C34 Fraction

<100 ---- ---- ---- ----mg/kg100---->C34 - C40 Fraction

<50^ ---- ---- ---- ----mg/kg50---->C10 - C40 Fraction (sum)

<50^ ---- ---- ---- ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

Page 34: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

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AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP080: BTEXN

<0.2Benzene ---- ---- ---- ----mg/kg0.271-43-2

<0.5Toluene ---- ---- ---- ----mg/kg0.5108-88-3

<0.5Ethylbenzene ---- ---- ---- ----mg/kg0.5100-41-4

<0.5meta- & para-Xylene ---- ---- ---- ----mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene ---- ---- ---- ----mg/kg0.595-47-6

<0.2^ ---- ---- ---- ----mg/kg0.2----Sum of BTEX

<0.5^ Total Xylenes ---- ---- ---- ----mg/kg0.51330-20-7

<1Naphthalene ---- ---- ---- ----mg/kg191-20-3

EP116: 1.4-Dioxane

<0.05ø1.4-Dioxane ---- ---- ---- ----mg/kg0.05123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.0003Perfluorobutane sulfonic acid

(PFBS)

0.0023 0.0022 <0.0002 <0.0002mg/kg0.0002375-73-5

0.0005Perfluoropentane sulfonic acid

(PFPeS)

0.0032 0.0027 <0.0002 <0.0002mg/kg0.00022706-91-4

0.0175Perfluorohexane sulfonic acid

(PFHxS)

0.237 0.0947 0.0012 0.0004mg/kg0.0002355-46-4

0.0052Perfluoroheptane sulfonic acid

(PFHpS)

0.0157 0.0054 <0.0002 <0.0002mg/kg0.0002375-92-8

2.05Perfluorooctane sulfonic acid

(PFOS)

1.68 0.936 0.0119 0.0068mg/kg0.00021763-23-1

0.0329Perfluorodecane sulfonic acid

(PFDS)

0.0177 0.0212 <0.0002 <0.0002mg/kg0.0002335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

0.002Perfluorobutanoic acid (PFBA) 0.002 0.001 <0.001 <0.001mg/kg0.001375-22-4

0.0032Perfluoropentanoic acid (PFPeA) 0.0059 0.0029 <0.0002 <0.0002mg/kg0.00022706-90-3

0.0139Perfluorohexanoic acid (PFHxA) 0.0097 0.0077 0.0003 <0.0002mg/kg0.0002307-24-4

0.0071Perfluoroheptanoic acid (PFHpA) 0.0076 0.0031 <0.0002 <0.0002mg/kg0.0002375-85-9

0.0348Perfluorooctanoic acid (PFOA) 0.0298 0.0082 0.0004 <0.0002mg/kg0.0002335-67-1

0.228Perfluorononanoic acid (PFNA) 0.0133 0.0073 0.0002 <0.0002mg/kg0.0002375-95-1

1.12Perfluorodecanoic acid (PFDA) 0.0026 0.0148 0.0003 <0.0002mg/kg0.0002335-76-2

1.03Perfluoroundecanoic acid

(PFUnDA)

0.0060 0.0110 <0.0002 <0.0002mg/kg0.00022058-94-8

0.150Perfluorododecanoic acid

(PFDoDA)

0.0114 0.0039 <0.0002 <0.0002mg/kg0.0002307-55-1

Page 35: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

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Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

0.0121Perfluorotridecanoic acid

(PFTrDA)

0.0017 0.0011 <0.0002 <0.0002mg/kg0.000272629-94-8

0.0031Perfluorotetradecanoic acid

(PFTeDA)

0.0032 0.0006 <0.0005 <0.0005mg/kg0.0005376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.0104Perfluorooctane sulfonamide

(FOSA)

0.0378 0.0174 <0.0002 <0.0002mg/kg0.0002754-91-6

<0.0005N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

<0.0005N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2

<0.0005N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7

<0.0005N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2

<0.0002N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9

<0.0002N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.00054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4

0.5086:2 Fluorotelomer sulfonic acid

(6:2 FTS)

0.0742 0.0084 <0.0005 <0.0005mg/kg0.000527619-97-2

4.738:2 Fluorotelomer sulfonic acid

(8:2 FTS)

0.0424 0.0125 <0.0005 <0.0005mg/kg0.000539108-34-4

0.039010:2 Fluorotelomer sulfonic acid

(10:2 FTS)

0.0023 0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

10.0 2.21 1.16 0.0143 0.0072mg/kg0.0002----Sum of PFAS

2.07Sum of PFHxS and PFOS 1.92 1.03 0.0131 0.0072mg/kg0.0002355-46-4/1763-23-

1

7.37 2.09 1.08 0.0138 0.0072mg/kg0.0002----Sum of PFAS (WA DER List)

EP068S: Organochlorine Pesticide Surrogate

Page 36: Appendix - Department of Defence

13 of 93:Page

Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD005_0407170902_SD004_0407170902_SD003_0407170902_SD002_0407170902_SD001_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-029ES1716547-028ES1716547-027ES1716547-026ES1716547-025UnitLORCAS NumberCompound

Result Result Result Result Result

EP068S: Organochlorine Pesticide Surrogate - Continued

110Dibromo-DDE ---- ---- ---- ----%0.0521655-73-2

EP068T: Organophosphorus Pesticide Surrogate

96.9DEF ---- ---- ---- ----%0.0578-48-8

EP074S: VOC Surrogates

92.31.2-Dichloroethane-D4 ---- ---- ---- ----%0.517060-07-0

92.0Toluene-D8 ---- ---- ---- ----%0.52037-26-5

93.64-Bromofluorobenzene ---- ---- ---- ----%0.5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

82.9Phenol-d6 ---- ---- ---- ----%0.513127-88-3

86.42-Chlorophenol-D4 ---- ---- ---- ----%0.593951-73-6

91.12.4.6-Tribromophenol ---- ---- ---- ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

80.92-Fluorobiphenyl ---- ---- ---- ----%0.5321-60-8

85.9Anthracene-d10 ---- ---- ---- ----%0.51719-06-8

90.64-Terphenyl-d14 ---- ---- ---- ----%0.51718-51-0

EP075S: Acid Extractable Surrogates

75.12-Fluorophenol ---- ---- ---- ----%0.5367-12-4

77.5Phenol-d6 ---- ---- ---- ----%0.513127-88-3

70.12-Chlorophenol-D4 ---- ---- ---- ----%0.593951-73-6

77.72.4.6-Tribromophenol ---- ---- ---- ----%0.5118-79-6

EP075T: Base/Neutral Extractable Surrogates

75.0Nitrobenzene-D5 ---- ---- ---- ----%0.54165-60-0

56.11.2-Dichlorobenzene-D4 ---- ---- ---- ----%0.52199-69-1

81.12-Fluorobiphenyl ---- ---- ---- ----%0.5321-60-8

86.9Anthracene-d10 ---- ---- ---- ----%0.51719-06-8

87.84-Terphenyl-d14 ---- ---- ---- ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

94.81.2-Dichloroethane-D4 ---- ---- ---- ----%0.217060-07-0

95.5Toluene-D8 ---- ---- ---- ----%0.22037-26-5

96.84-Bromofluorobenzene ---- ---- ---- ----%0.2460-00-4

EP116S: 1.4-Dioxane Surrogate

92.3ø1.4-Dioxane-d8 ---- ---- ---- ----%0.0117647-74-4

EP231S: PFAS Surrogate

106 96.0 111 112 107%0.0002----13C4-PFOS

Page 37: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EA055: Moisture Content (Dried @ 105-110°C)

43.6 46.6 51.7 32.7 89.6%1----Moisture Content

ED007: Exchangeable Cations

---- ---- ---- 5.3 ----meq/100g0.1----Exchangeable Calcium

---- ---- ---- 4.0 ----meq/100g0.1----Exchangeable Magnesium

---- ---- ---- 0.1 ----meq/100g0.1----Exchangeable Potassium

---- ---- ---- 3.0 ----meq/100g0.1----Exchangeable Sodium

---- ---- ---- 12.4 ----meq/100g0.1----Cation Exchange Capacity

EG005T: Total Metals by ICP-AES

----Iron ---- ---- 10000 ----mg/kg507439-89-6

----Arsenic ---- ---- <5 ----mg/kg57440-38-2

----Cadmium ---- ---- <1 ----mg/kg17440-43-9

----Chromium ---- ---- 11 ----mg/kg27440-47-3

----Copper ---- ---- 14 ----mg/kg57440-50-8

----Lead ---- ---- 14 ----mg/kg57439-92-1

----Nickel ---- ---- 10 ----mg/kg27440-02-0

----Zinc ---- ---- 70 ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

----Mercury ---- ---- <0.1 ----mg/kg0.17439-97-6

EP003: Total Organic Carbon (TOC) in Soil

---- ---- ---- 0.38 ----%0.02----Total Organic Carbon

EP068A: Organochlorine Pesticides (OC)

----alpha-BHC ---- ---- <0.05 ----mg/kg0.05319-84-6

----Hexachlorobenzene (HCB) ---- ---- <0.05 ----mg/kg0.05118-74-1

----beta-BHC ---- ---- <0.05 ----mg/kg0.05319-85-7

----gamma-BHC ---- ---- <0.05 ----mg/kg0.0558-89-9

----delta-BHC ---- ---- <0.05 ----mg/kg0.05319-86-8

----Heptachlor ---- ---- <0.05 ----mg/kg0.0576-44-8

----Aldrin ---- ---- <0.05 ----mg/kg0.05309-00-2

----Heptachlor epoxide ---- ---- <0.05 ----mg/kg0.051024-57-3

----^ ---- ---- <0.05 ----mg/kg0.05----Total Chlordane (sum)

----trans-Chlordane ---- ---- <0.05 ----mg/kg0.055103-74-2

----alpha-Endosulfan ---- ---- <0.05 ----mg/kg0.05959-98-8

----cis-Chlordane ---- ---- <0.05 ----mg/kg0.055103-71-9

----Dieldrin ---- ---- <0.05 ----mg/kg0.0560-57-1

Page 38: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP068A: Organochlorine Pesticides (OC) - Continued

----4.4`-DDE ---- ---- <0.05 ----mg/kg0.0572-55-9

----Endrin ---- ---- <0.05 ----mg/kg0.0572-20-8

----beta-Endosulfan ---- ---- <0.05 ----mg/kg0.0533213-65-9

----^ Endosulfan (sum) ---- ---- <0.05 ----mg/kg0.05115-29-7

----4.4`-DDD ---- ---- <0.05 ----mg/kg0.0572-54-8

----Endrin aldehyde ---- ---- <0.05 ----mg/kg0.057421-93-4

----Endosulfan sulfate ---- ---- <0.05 ----mg/kg0.051031-07-8

----4.4`-DDT ---- ---- <0.2 ----mg/kg0.250-29-3

----Endrin ketone ---- ---- <0.05 ----mg/kg0.0553494-70-5

----Methoxychlor ---- ---- <0.2 ----mg/kg0.272-43-5

----^ Sum of Aldrin + Dieldrin ---- ---- <0.05 ----mg/kg0.05309-00-2/60-57-1

----^ Sum of DDD + DDE + DDT ---- ---- <0.05 ----mg/kg0.0572-54-8/72-55-9/5

0-2

EP068B: Organophosphorus Pesticides (OP)

----Dichlorvos ---- ---- <0.05 ----mg/kg0.0562-73-7

----Demeton-S-methyl ---- ---- <0.05 ----mg/kg0.05919-86-8

----Monocrotophos ---- ---- <0.2 ----mg/kg0.26923-22-4

----Dimethoate ---- ---- <0.05 ----mg/kg0.0560-51-5

----Diazinon ---- ---- <0.05 ----mg/kg0.05333-41-5

----Chlorpyrifos-methyl ---- ---- <0.05 ----mg/kg0.055598-13-0

----Parathion-methyl ---- ---- <0.2 ----mg/kg0.2298-00-0

----Malathion ---- ---- <0.05 ----mg/kg0.05121-75-5

----Fenthion ---- ---- <0.05 ----mg/kg0.0555-38-9

----Chlorpyrifos ---- ---- <0.05 ----mg/kg0.052921-88-2

----Parathion ---- ---- <0.2 ----mg/kg0.256-38-2

----Pirimphos-ethyl ---- ---- <0.05 ----mg/kg0.0523505-41-1

----Chlorfenvinphos ---- ---- <0.05 ----mg/kg0.05470-90-6

----Bromophos-ethyl ---- ---- <0.05 ----mg/kg0.054824-78-6

----Fenamiphos ---- ---- <0.05 ----mg/kg0.0522224-92-6

----Prothiofos ---- ---- <0.05 ----mg/kg0.0534643-46-4

----Ethion ---- ---- <0.05 ----mg/kg0.05563-12-2

----Carbophenothion ---- ---- <0.05 ----mg/kg0.05786-19-6

----Azinphos Methyl ---- ---- <0.05 ----mg/kg0.0586-50-0

EP074A: Monocyclic Aromatic Hydrocarbons

----Styrene ---- ---- <0.5 ----mg/kg0.5100-42-5

Page 39: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP074A: Monocyclic Aromatic Hydrocarbons - Continued

----Isopropylbenzene ---- ---- <0.5 ----mg/kg0.598-82-8

----n-Propylbenzene ---- ---- <0.5 ----mg/kg0.5103-65-1

----1.3.5-Trimethylbenzene ---- ---- <0.5 ----mg/kg0.5108-67-8

----sec-Butylbenzene ---- ---- <0.5 ----mg/kg0.5135-98-8

----1.2.4-Trimethylbenzene ---- ---- <0.5 ----mg/kg0.595-63-6

----tert-Butylbenzene ---- ---- <0.5 ----mg/kg0.598-06-6

----p-Isopropyltoluene ---- ---- <0.5 ----mg/kg0.599-87-6

----n-Butylbenzene ---- ---- <0.5 ----mg/kg0.5104-51-8

EP074B: Oxygenated Compounds

----Vinyl Acetate ---- ---- <5 ----mg/kg5108-05-4

----2-Butanone (MEK) ---- ---- <5 ----mg/kg578-93-3

----4-Methyl-2-pentanone (MIBK) ---- ---- <5 ----mg/kg5108-10-1

----2-Hexanone (MBK) ---- ---- <5 ----mg/kg5591-78-6

EP074C: Sulfonated Compounds

----Carbon disulfide ---- ---- <0.5 ----mg/kg0.575-15-0

EP074D: Fumigants

----2.2-Dichloropropane ---- ---- <0.5 ----mg/kg0.5594-20-7

----1.2-Dichloropropane ---- ---- <0.5 ----mg/kg0.578-87-5

----cis-1.3-Dichloropropylene ---- ---- <0.5 ----mg/kg0.510061-01-5

----trans-1.3-Dichloropropylene ---- ---- <0.5 ----mg/kg0.510061-02-6

----1.2-Dibromoethane (EDB) ---- ---- <0.5 ----mg/kg0.5106-93-4

EP074E: Halogenated Aliphatic Compounds

----Dichlorodifluoromethane ---- ---- <5 ----mg/kg575-71-8

----Chloromethane ---- ---- <5 ----mg/kg574-87-3

----Vinyl chloride ---- ---- <5 ----mg/kg575-01-4

----Bromomethane ---- ---- <5 ----mg/kg574-83-9

----Chloroethane ---- ---- <5 ----mg/kg575-00-3

----Trichlorofluoromethane ---- ---- <5 ----mg/kg575-69-4

----1.1-Dichloroethene ---- ---- <0.5 ----mg/kg0.575-35-4

----Iodomethane ---- ---- <0.5 ----mg/kg0.574-88-4

----trans-1.2-Dichloroethene ---- ---- <0.5 ----mg/kg0.5156-60-5

----1.1-Dichloroethane ---- ---- <0.5 ----mg/kg0.575-34-3

----cis-1.2-Dichloroethene ---- ---- <0.5 ----mg/kg0.5156-59-2

----1.1.1-Trichloroethane ---- ---- <0.5 ----mg/kg0.571-55-6

Page 40: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

----1.1-Dichloropropylene ---- ---- <0.5 ----mg/kg0.5563-58-6

----Carbon Tetrachloride ---- ---- <0.5 ----mg/kg0.556-23-5

----1.2-Dichloroethane ---- ---- <0.5 ----mg/kg0.5107-06-2

----Trichloroethene ---- ---- <0.5 ----mg/kg0.579-01-6

----Dibromomethane ---- ---- <0.5 ----mg/kg0.574-95-3

----1.1.2-Trichloroethane ---- ---- <0.5 ----mg/kg0.579-00-5

----1.3-Dichloropropane ---- ---- <0.5 ----mg/kg0.5142-28-9

----Tetrachloroethene ---- ---- <0.5 ----mg/kg0.5127-18-4

----1.1.1.2-Tetrachloroethane ---- ---- <0.5 ----mg/kg0.5630-20-6

----trans-1.4-Dichloro-2-butene ---- ---- <0.5 ----mg/kg0.5110-57-6

----cis-1.4-Dichloro-2-butene ---- ---- <0.5 ----mg/kg0.51476-11-5

----1.1.2.2-Tetrachloroethane ---- ---- <0.5 ----mg/kg0.579-34-5

----1.2.3-Trichloropropane ---- ---- <0.5 ----mg/kg0.596-18-4

----Pentachloroethane ---- ---- <0.5 ----mg/kg0.576-01-7

----1.2-Dibromo-3-chloropropane ---- ---- <0.5 ----mg/kg0.596-12-8

EP074F: Halogenated Aromatic Compounds

----Chlorobenzene ---- ---- <0.5 ----mg/kg0.5108-90-7

----Bromobenzene ---- ---- <0.5 ----mg/kg0.5108-86-1

----2-Chlorotoluene ---- ---- <0.5 ----mg/kg0.595-49-8

----4-Chlorotoluene ---- ---- <0.5 ----mg/kg0.5106-43-4

----1.2.3-Trichlorobenzene ---- ---- <0.5 ----mg/kg0.587-61-6

EP074G: Trihalomethanes

----Chloroform ---- ---- <0.5 ----mg/kg0.567-66-3

----Bromodichloromethane ---- ---- <0.5 ----mg/kg0.575-27-4

----Dibromochloromethane ---- ---- <0.5 ----mg/kg0.5124-48-1

----Bromoform ---- ---- <0.5 ----mg/kg0.575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

----Naphthalene ---- ---- <0.5 ----mg/kg0.591-20-3

----Acenaphthylene ---- ---- <0.5 ----mg/kg0.5208-96-8

----Acenaphthene ---- ---- <0.5 ----mg/kg0.583-32-9

----Fluorene ---- ---- <0.5 ----mg/kg0.586-73-7

----Phenanthrene ---- ---- <0.5 ----mg/kg0.585-01-8

----Anthracene ---- ---- <0.5 ----mg/kg0.5120-12-7

----Fluoranthene ---- ---- <0.5 ----mg/kg0.5206-44-0

Page 41: Appendix - Department of Defence

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Work Order :

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ES1716547

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

----Pyrene ---- ---- <0.5 ----mg/kg0.5129-00-0

----Benz(a)anthracene ---- ---- <0.5 ----mg/kg0.556-55-3

----Chrysene ---- ---- <0.5 ----mg/kg0.5218-01-9

----Benzo(b+j)fluoranthene ---- ---- <0.5 ----mg/kg0.5205-99-2 205-82-3

----Benzo(k)fluoranthene ---- ---- <0.5 ----mg/kg0.5207-08-9

----Benzo(a)pyrene ---- ---- <0.5 ----mg/kg0.550-32-8

----Indeno(1.2.3.cd)pyrene ---- ---- <0.5 ----mg/kg0.5193-39-5

----Dibenz(a.h)anthracene ---- ---- <0.5 ----mg/kg0.553-70-3

----Benzo(g.h.i)perylene ---- ---- <0.5 ----mg/kg0.5191-24-2

----^ ---- ---- <0.5 ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

----^ ---- ---- <0.5 ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

----^ ---- ---- 0.6 ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

----^ ---- ---- 1.2 ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP075A: Phenolic Compounds

----Phenol ---- ---- <0.5 ----mg/kg0.5108-95-2

----2-Chlorophenol ---- ---- <0.5 ----mg/kg0.595-57-8

----2-Methylphenol ---- ---- <0.5 ----mg/kg0.595-48-7

----3- & 4-Methylphenol ---- ---- <0.6 ----mg/kg0.51319-77-3

----2-Nitrophenol ---- ---- <0.5 ----mg/kg0.588-75-5

----2.4-Dimethylphenol ---- ---- <0.5 ----mg/kg0.5105-67-9

----2.4-Dichlorophenol ---- ---- <0.5 ----mg/kg0.5120-83-2

----2.6-Dichlorophenol ---- ---- <0.5 ----mg/kg0.587-65-0

----4-Chloro-3-methylphenol ---- ---- <0.5 ----mg/kg0.559-50-7

----2.4.6-Trichlorophenol ---- ---- <0.5 ----mg/kg0.588-06-2

----2.4.5-Trichlorophenol ---- ---- <0.5 ----mg/kg0.595-95-4

----Pentachlorophenol ---- ---- <1 ----mg/kg187-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

----2-Methylnaphthalene ---- ---- <0.5 ----mg/kg0.591-57-6

----2-Chloronaphthalene ---- ---- <0.5 ----mg/kg0.591-58-7

----N-2-Fluorenyl Acetamide ---- ---- <0.5 ----mg/kg0.553-96-3

----7.12-Dimethylbenz(a)anthracene ---- ---- <0.5 ----mg/kg0.557-97-6

----3-Methylcholanthrene ---- ---- <0.5 ----mg/kg0.556-49-5

EP075C: Phthalate Esters

----Dimethyl phthalate ---- ---- <0.5 ----mg/kg0.5131-11-3

Page 42: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

----Diethyl phthalate ---- ---- <0.5 ----mg/kg0.584-66-2

----Di-n-butyl phthalate ---- ---- <0.5 ----mg/kg0.584-74-2

----Butyl benzyl phthalate ---- ---- <0.5 ----mg/kg0.585-68-7

----bis(2-ethylhexyl) phthalate ---- ---- <5.0 ----mg/kg5117-81-7

----Di-n-octylphthalate ---- ---- <0.5 ----mg/kg0.5117-84-0

EP075D: Nitrosamines

----N-Nitrosomethylethylamine ---- ---- <0.5 ----mg/kg0.510595-95-6

----N-Nitrosodiethylamine ---- ---- <0.5 ----mg/kg0.555-18-5

----N-Nitrosopyrrolidine ---- ---- <1.0 ----mg/kg1930-55-2

----N-Nitrosomorpholine ---- ---- <0.5 ----mg/kg0.559-89-2

----N-Nitrosodi-n-propylamine ---- ---- <0.5 ----mg/kg0.5621-64-7

----N-Nitrosopiperidine ---- ---- <0.5 ----mg/kg0.5100-75-4

----N-Nitrosodibutylamine ---- ---- <0.5 ----mg/kg0.5924-16-3

----N-Nitrosodiphenyl &

Diphenylamine

---- ---- <1.0 ----mg/kg186-30-6 122-39-4

----Methapyrilene ---- ---- <0.5 ----mg/kg0.591-80-5

EP075E: Nitroaromatics and Ketones

----2-Picoline ---- ---- <0.5 ----mg/kg0.5109-06-8

----Acetophenone ---- ---- <0.5 ----mg/kg0.598-86-2

----Nitrobenzene ---- ---- <0.5 ----mg/kg0.598-95-3

----Isophorone ---- ---- <0.5 ----mg/kg0.578-59-1

----2.6-Dinitrotoluene ---- ---- <1.0 ----mg/kg1606-20-2

----2.4-Dinitrotoluene ---- ---- <1.0 ----mg/kg1121-14-2

----1-Naphthylamine ---- ---- <0.5 ----mg/kg0.5134-32-7

----4-Nitroquinoline-N-oxide ---- ---- <0.5 ----mg/kg0.556-57-5

----5-Nitro-o-toluidine ---- ---- <0.5 ----mg/kg0.599-55-8

----Azobenzene ---- ---- <1 ----mg/kg1103-33-3

----1.3.5-Trinitrobenzene ---- ---- <0.5 ----mg/kg0.599-35-4

----Phenacetin ---- ---- <0.5 ----mg/kg0.562-44-2

----4-Aminobiphenyl ---- ---- <0.5 ----mg/kg0.592-67-1

----Pentachloronitrobenzene ---- ---- <0.5 ----mg/kg0.582-68-8

----Pronamide ---- ---- <0.5 ----mg/kg0.523950-58-5

----Dimethylaminoazobenzene ---- ---- <0.5 ----mg/kg0.560-11-7

----Chlorobenzilate ---- ---- <0.5 ----mg/kg0.5510-15-6

Page 43: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP075F: Haloethers

----Bis(2-chloroethyl) ether ---- ---- <0.5 ----mg/kg0.5111-44-4

----Bis(2-chloroethoxy) methane ---- ---- <0.5 ----mg/kg0.5111-91-1

----4-Chlorophenyl phenyl ether ---- ---- <0.5 ----mg/kg0.57005-72-3

----4-Bromophenyl phenyl ether ---- ---- <0.5 ----mg/kg0.5101-55-3

EP075G: Chlorinated Hydrocarbons

----1.3-Dichlorobenzene ---- ---- <0.5 ----mg/kg0.5541-73-1

----1.4-Dichlorobenzene ---- ---- <0.5 ----mg/kg0.5106-46-7

----1.2-Dichlorobenzene ---- ---- <0.5 ----mg/kg0.595-50-1

----Hexachloroethane ---- ---- <0.5 ----mg/kg0.567-72-1

----1.2.4-Trichlorobenzene ---- ---- <0.5 ----mg/kg0.5120-82-1

----Hexachloropropylene ---- ---- <0.5 ----mg/kg0.51888-71-7

----Hexachlorobutadiene ---- ---- <0.5 ----mg/kg0.587-68-3

----Hexachlorocyclopentadiene ---- ---- <2.5 ----mg/kg2.577-47-4

----Pentachlorobenzene ---- ---- <0.5 ----mg/kg0.5608-93-5

----Hexachlorobenzene (HCB) ---- ---- <1.0 ----mg/kg1118-74-1

EP075H: Anilines and Benzidines

----Aniline ---- ---- <0.5 ----mg/kg0.562-53-3

----4-Chloroaniline ---- ---- <0.5 ----mg/kg0.5106-47-8

----2-Nitroaniline ---- ---- <1.0 ----mg/kg188-74-4

----3-Nitroaniline ---- ---- <1.0 ----mg/kg199-09-2

----Dibenzofuran ---- ---- <0.5 ----mg/kg0.5132-64-9

----4-Nitroaniline ---- ---- <0.5 ----mg/kg0.5100-01-6

----Carbazole ---- ---- <0.5 ----mg/kg0.586-74-8

----3.3`-Dichlorobenzidine ---- ---- <0.5 ----mg/kg0.591-94-1

EP075I: Organochlorine Pesticides

----alpha-BHC ---- ---- <0.5 ----mg/kg0.5319-84-6

----beta-BHC ---- ---- <0.5 ----mg/kg0.5319-85-7

----gamma-BHC ---- ---- <0.5 ----mg/kg0.558-89-9

----delta-BHC ---- ---- <0.5 ----mg/kg0.5319-86-8

----Heptachlor ---- ---- <0.5 ----mg/kg0.576-44-8

----Aldrin ---- ---- <0.5 ----mg/kg0.5309-00-2

----Heptachlor epoxide ---- ---- <0.5 ----mg/kg0.51024-57-3

----alpha-Endosulfan ---- ---- <0.5 ----mg/kg0.5959-98-8

----4.4`-DDE ---- ---- <0.5 ----mg/kg0.572-55-9

Page 44: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

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AECOM Australia Pty Ltd

Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

----Dieldrin ---- ---- <0.5 ----mg/kg0.560-57-1

----Endrin ---- ---- <0.5 ----mg/kg0.572-20-8

----beta-Endosulfan ---- ---- <0.5 ----mg/kg0.533213-65-9

----4.4`-DDD ---- ---- <0.5 ----mg/kg0.572-54-8

----Endosulfan sulfate ---- ---- <0.5 ----mg/kg0.51031-07-8

----4.4`-DDT ---- ---- <1.0 ----mg/kg150-29-3

EP075J: Organophosphorus Pesticides

----Dichlorvos ---- ---- <0.5 ----mg/kg0.562-73-7

----Dimethoate ---- ---- <0.5 ----mg/kg0.560-51-5

----Diazinon ---- ---- <0.5 ----mg/kg0.5333-41-5

----Chlorpyrifos-methyl ---- ---- <0.5 ----mg/kg0.55598-13-0

----Malathion ---- ---- <0.5 ----mg/kg0.5121-75-5

----Fenthion ---- ---- <0.5 ----mg/kg0.555-38-9

----Chlorpyrifos ---- ---- <0.5 ----mg/kg0.52921-88-2

----Pirimphos-ethyl ---- ---- <0.5 ----mg/kg0.523505-41-1

----Chlorfenvinphos ---- ---- <0.5 ----mg/kg0.5470-90-6

----Prothiofos ---- ---- <0.5 ----mg/kg0.534643-46-4

----Ethion ---- ---- <0.5 ----mg/kg0.5563-12-2

EP080/071: Total Petroleum Hydrocarbons

---- ---- ---- <10 ----mg/kg10----C6 - C9 Fraction

---- ---- ---- <50 ----mg/kg50----C10 - C14 Fraction

---- ---- ---- <100 ----mg/kg100----C15 - C28 Fraction

---- ---- ---- <100 ----mg/kg100----C29 - C36 Fraction

----^ ---- ---- <50 ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

----C6 - C10 Fraction ---- ---- <10 ----mg/kg10C6_C10

----^ C6 - C10 Fraction minus BTEX

(F1)

---- ---- <10 ----mg/kg10C6_C10-BTEX

---- ---- ---- <50 ----mg/kg50---->C10 - C16 Fraction

---- ---- ---- <100 ----mg/kg100---->C16 - C34 Fraction

---- ---- ---- <100 ----mg/kg100---->C34 - C40 Fraction

----^ ---- ---- <50 ----mg/kg50---->C10 - C40 Fraction (sum)

----^ ---- ---- <50 ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

Page 45: Appendix - Department of Defence

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Work Order :

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP080: BTEXN

----Benzene ---- ---- <0.2 ----mg/kg0.271-43-2

----Toluene ---- ---- <0.5 ----mg/kg0.5108-88-3

----Ethylbenzene ---- ---- <0.5 ----mg/kg0.5100-41-4

----meta- & para-Xylene ---- ---- <0.5 ----mg/kg0.5108-38-3 106-42-3

----ortho-Xylene ---- ---- <0.5 ----mg/kg0.595-47-6

----^ ---- ---- <0.2 ----mg/kg0.2----Sum of BTEX

----^ Total Xylenes ---- ---- <0.5 ----mg/kg0.51330-20-7

----Naphthalene ---- ---- <1 ----mg/kg191-20-3

EP116: 1.4-Dioxane

----ø1.4-Dioxane ---- ---- <0.05 ----mg/kg0.05123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

<0.0002Perfluorobutane sulfonic acid

(PFBS)

<0.0002 <0.0002 <0.0002 0.0039mg/kg0.0002375-73-5

<0.0002Perfluoropentane sulfonic acid

(PFPeS)

<0.0002 <0.0002 <0.0002 0.0043mg/kg0.00022706-91-4

0.0008Perfluorohexane sulfonic acid

(PFHxS)

0.0015 0.0019 0.0067 0.107mg/kg0.0002355-46-4

<0.0002Perfluoroheptane sulfonic acid

(PFHpS)

<0.0002 0.0003 0.0010 0.0079mg/kg0.0002375-92-8

0.0074Perfluorooctane sulfonic acid

(PFOS)

0.0146 0.0385 0.183 1.10mg/kg0.00021763-23-1

<0.0002Perfluorodecane sulfonic acid

(PFDS)

<0.0002 0.0008 0.0029 0.0216mg/kg0.0002335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 0.006mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 <0.0002 0.0005 0.0025mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 <0.0002 0.0006 0.0083mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 <0.0002 0.0004 0.0037mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) 0.0003 <0.0002 0.0016 0.0169mg/kg0.0002335-67-1

<0.0002Perfluorononanoic acid (PFNA) 0.0003 0.0002 0.0008 0.0050mg/kg0.0002375-95-1

<0.0002Perfluorodecanoic acid (PFDA) 0.0003 0.0003 0.0007 0.0064mg/kg0.0002335-76-2

<0.0002Perfluoroundecanoic acid

(PFUnDA)

<0.0002 0.0002 0.0007 0.0112mg/kg0.00022058-94-8

<0.0002Perfluorododecanoic acid

(PFDoDA)

<0.0002 <0.0002 0.0006 0.0118mg/kg0.0002307-55-1

Page 46: Appendix - Department of Defence

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Work Order :

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.0002Perfluorotridecanoic acid

(PFTrDA)

<0.0002 <0.0002 0.0002 0.0103mg/kg0.000272629-94-8

<0.0005Perfluorotetradecanoic acid

(PFTeDA)

<0.0005 <0.0005 <0.0005 0.0075mg/kg0.0005376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.0002Perfluorooctane sulfonamide

(FOSA)

<0.0002 <0.0002 0.0010 0.0238mg/kg0.0002754-91-6

<0.0005N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.000531506-32-8

<0.0005N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00054151-50-2

<0.0005N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00052448-09-7

<0.0005N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00051691-99-2

<0.0002N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9

<0.0002N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.00054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4

<0.00056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

0.0017 0.0008 <0.0005 0.0056mg/kg0.000527619-97-2

<0.00058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.0005 <0.0005 <0.0005 0.0292mg/kg0.000539108-34-4

<0.000510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.0005 <0.0005 <0.0005 0.0062mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0082 0.0187 0.0430 0.201 1.40mg/kg0.0002----Sum of PFAS

0.0082Sum of PFHxS and PFOS 0.0161 0.0404 0.190 1.21mg/kg0.0002355-46-4/1763-23-

1

0.0082 0.0181 0.0412 0.193 1.28mg/kg0.0002----Sum of PFAS (WA DER List)

EP068S: Organochlorine Pesticide Surrogate

Page 47: Appendix - Department of Defence

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Analytical Results

0902_SD010_0307170902_SD009_0307170902_SD008_0307170902_SD007_0407170902_SD006_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-034ES1716547-033ES1716547-032ES1716547-031ES1716547-030UnitLORCAS NumberCompound

Result Result Result Result Result

EP068S: Organochlorine Pesticide Surrogate - Continued

----Dibromo-DDE ---- ---- 115 ----%0.0521655-73-2

EP068T: Organophosphorus Pesticide Surrogate

----DEF ---- ---- 103 ----%0.0578-48-8

EP074S: VOC Surrogates

----1.2-Dichloroethane-D4 ---- ---- 74.3 ----%0.517060-07-0

----Toluene-D8 ---- ---- 76.5 ----%0.52037-26-5

----4-Bromofluorobenzene ---- ---- 85.2 ----%0.5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

----Phenol-d6 ---- ---- 90.0 ----%0.513127-88-3

----2-Chlorophenol-D4 ---- ---- 88.5 ----%0.593951-73-6

----2.4.6-Tribromophenol ---- ---- 78.9 ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

----2-Fluorobiphenyl ---- ---- 80.9 ----%0.5321-60-8

----Anthracene-d10 ---- ---- 93.0 ----%0.51719-06-8

----4-Terphenyl-d14 ---- ---- 80.8 ----%0.51718-51-0

EP075S: Acid Extractable Surrogates

----2-Fluorophenol ---- ---- 81.1 ----%0.5367-12-4

----Phenol-d6 ---- ---- 85.2 ----%0.513127-88-3

----2-Chlorophenol-D4 ---- ---- 76.2 ----%0.593951-73-6

----2.4.6-Tribromophenol ---- ---- 87.2 ----%0.5118-79-6

EP075T: Base/Neutral Extractable Surrogates

----Nitrobenzene-D5 ---- ---- 80.4 ----%0.54165-60-0

----1.2-Dichlorobenzene-D4 ---- ---- 58.2 ----%0.52199-69-1

----2-Fluorobiphenyl ---- ---- 90.2 ----%0.5321-60-8

----Anthracene-d10 ---- ---- 99.2 ----%0.51719-06-8

----4-Terphenyl-d14 ---- ---- 99.2 ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

----1.2-Dichloroethane-D4 ---- ---- 74.9 ----%0.217060-07-0

----Toluene-D8 ---- ---- 79.3 ----%0.22037-26-5

----4-Bromofluorobenzene ---- ---- 87.5 ----%0.2460-00-4

EP116S: 1.4-Dioxane Surrogate

----ø1.4-Dioxane-d8 ---- ---- 106 ----%0.0117647-74-4

EP231S: PFAS Surrogate

105 113 106 109 98.8%0.0002----13C4-PFOS

Page 48: Appendix - Department of Defence

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Work Order :

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EA055: Moisture Content (Dried @ 105-110°C)

57.8 59.3 44.9 38.6 73.1%1----Moisture Content

ED007: Exchangeable Cations

6.7 5.2 ---- 7.2 ----meq/100g0.1----Exchangeable Calcium

0.8 1.6 ---- 2.0 ----meq/100g0.1----Exchangeable Magnesium

0.2 0.4 ---- 0.3 ----meq/100g0.1----Exchangeable Potassium

0.2 0.3 ---- 0.2 ----meq/100g0.1----Exchangeable Sodium

8.0 7.5 ---- 9.8 ----meq/100g0.1----Cation Exchange Capacity

EG005T: Total Metals by ICP-AES

14000Iron 9990 ---- 12900 ----mg/kg507439-89-6

<5Arsenic <5 ---- <5 ----mg/kg57440-38-2

7Cadmium 2 ---- <1 ----mg/kg17440-43-9

45Chromium 22 ---- 11 ----mg/kg27440-47-3

57Copper 40 ---- 9 ----mg/kg57440-50-8

52Lead 58 ---- 11 ----mg/kg57439-92-1

12Nickel 11 ---- 7 ----mg/kg27440-02-0

906Zinc 161 ---- 54 ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

<0.1Mercury <0.1 ---- <0.1 ----mg/kg0.17439-97-6

EP003: Total Organic Carbon (TOC) in Soil

0.46 0.22 ---- 0.18 ----%0.02----Total Organic Carbon

EP068A: Organochlorine Pesticides (OC)

<0.05alpha-BHC <0.05 ---- <0.05 ----mg/kg0.05319-84-6

<0.05Hexachlorobenzene (HCB) <0.05 ---- <0.05 ----mg/kg0.05118-74-1

<0.05beta-BHC <0.05 ---- <0.05 ----mg/kg0.05319-85-7

<0.05gamma-BHC <0.05 ---- <0.05 ----mg/kg0.0558-89-9

<0.05delta-BHC <0.05 ---- <0.05 ----mg/kg0.05319-86-8

<0.05Heptachlor <0.05 ---- <0.05 ----mg/kg0.0576-44-8

<0.05Aldrin <0.05 ---- <0.05 ----mg/kg0.05309-00-2

<0.05Heptachlor epoxide <0.05 ---- <0.05 ----mg/kg0.051024-57-3

<0.05^ <0.05 ---- <0.05 ----mg/kg0.05----Total Chlordane (sum)

<0.05trans-Chlordane <0.05 ---- <0.05 ----mg/kg0.055103-74-2

<0.05alpha-Endosulfan <0.05 ---- <0.05 ----mg/kg0.05959-98-8

<0.05cis-Chlordane <0.05 ---- <0.05 ----mg/kg0.055103-71-9

0.14Dieldrin <0.05 ---- <0.05 ----mg/kg0.0560-57-1

Page 49: Appendix - Department of Defence

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP068A: Organochlorine Pesticides (OC) - Continued

<0.054.4`-DDE <0.05 ---- <0.05 ----mg/kg0.0572-55-9

<0.05Endrin <0.05 ---- <0.05 ----mg/kg0.0572-20-8

<0.05beta-Endosulfan <0.05 ---- <0.05 ----mg/kg0.0533213-65-9

<0.05^ Endosulfan (sum) <0.05 ---- <0.05 ----mg/kg0.05115-29-7

<0.054.4`-DDD <0.05 ---- <0.05 ----mg/kg0.0572-54-8

<0.05Endrin aldehyde <0.05 ---- <0.05 ----mg/kg0.057421-93-4

<0.05Endosulfan sulfate <0.05 ---- <0.05 ----mg/kg0.051031-07-8

<0.24.4`-DDT <0.2 ---- <0.2 ----mg/kg0.250-29-3

<0.05Endrin ketone <0.05 ---- <0.05 ----mg/kg0.0553494-70-5

<0.2Methoxychlor <0.2 ---- <0.2 ----mg/kg0.272-43-5

0.14^ Sum of Aldrin + Dieldrin <0.05 ---- <0.05 ----mg/kg0.05309-00-2/60-57-1

<0.05^ Sum of DDD + DDE + DDT <0.05 ---- <0.05 ----mg/kg0.0572-54-8/72-55-9/5

0-2

EP068B: Organophosphorus Pesticides (OP)

<0.05Dichlorvos <0.05 ---- <0.05 ----mg/kg0.0562-73-7

<0.05Demeton-S-methyl <0.05 ---- <0.05 ----mg/kg0.05919-86-8

<0.2Monocrotophos <0.2 ---- <0.2 ----mg/kg0.26923-22-4

<0.05Dimethoate <0.05 ---- <0.05 ----mg/kg0.0560-51-5

<0.05Diazinon <0.05 ---- <0.05 ----mg/kg0.05333-41-5

<0.05Chlorpyrifos-methyl <0.05 ---- <0.05 ----mg/kg0.055598-13-0

<0.2Parathion-methyl <0.2 ---- <0.2 ----mg/kg0.2298-00-0

<0.05Malathion <0.05 ---- <0.05 ----mg/kg0.05121-75-5

<0.05Fenthion <0.05 ---- <0.05 ----mg/kg0.0555-38-9

<0.05Chlorpyrifos <0.05 ---- <0.05 ----mg/kg0.052921-88-2

<0.2Parathion <0.2 ---- <0.2 ----mg/kg0.256-38-2

<0.05Pirimphos-ethyl <0.05 ---- <0.05 ----mg/kg0.0523505-41-1

<0.05Chlorfenvinphos <0.05 ---- <0.05 ----mg/kg0.05470-90-6

<0.05Bromophos-ethyl <0.05 ---- <0.05 ----mg/kg0.054824-78-6

<0.05Fenamiphos <0.05 ---- <0.05 ----mg/kg0.0522224-92-6

<0.05Prothiofos <0.05 ---- <0.05 ----mg/kg0.0534643-46-4

<0.05Ethion <0.05 ---- <0.05 ----mg/kg0.05563-12-2

<0.05Carbophenothion <0.05 ---- <0.05 ----mg/kg0.05786-19-6

<0.05Azinphos Methyl <0.05 ---- <0.05 ----mg/kg0.0586-50-0

EP074A: Monocyclic Aromatic Hydrocarbons

<0.5Styrene <0.5 ---- <0.5 ----mg/kg0.5100-42-5

Page 50: Appendix - Department of Defence

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP074A: Monocyclic Aromatic Hydrocarbons - Continued

<0.5Isopropylbenzene <0.5 ---- <0.5 ----mg/kg0.598-82-8

<0.5n-Propylbenzene <0.5 ---- <0.5 ----mg/kg0.5103-65-1

<0.51.3.5-Trimethylbenzene <0.5 ---- <0.5 ----mg/kg0.5108-67-8

<0.5sec-Butylbenzene <0.5 ---- <0.5 ----mg/kg0.5135-98-8

<0.51.2.4-Trimethylbenzene <0.5 ---- <0.5 ----mg/kg0.595-63-6

<0.5tert-Butylbenzene <0.5 ---- <0.5 ----mg/kg0.598-06-6

<0.5p-Isopropyltoluene <0.5 ---- <0.5 ----mg/kg0.599-87-6

<0.5n-Butylbenzene <0.5 ---- <0.5 ----mg/kg0.5104-51-8

EP074B: Oxygenated Compounds

<5Vinyl Acetate <5 ---- <5 ----mg/kg5108-05-4

<52-Butanone (MEK) <5 ---- <5 ----mg/kg578-93-3

<54-Methyl-2-pentanone (MIBK) <5 ---- <5 ----mg/kg5108-10-1

<52-Hexanone (MBK) <5 ---- <5 ----mg/kg5591-78-6

EP074C: Sulfonated Compounds

<0.5Carbon disulfide <0.5 ---- <0.5 ----mg/kg0.575-15-0

EP074D: Fumigants

<0.52.2-Dichloropropane <0.5 ---- <0.5 ----mg/kg0.5594-20-7

<0.51.2-Dichloropropane <0.5 ---- <0.5 ----mg/kg0.578-87-5

<0.5cis-1.3-Dichloropropylene <0.5 ---- <0.5 ----mg/kg0.510061-01-5

<0.5trans-1.3-Dichloropropylene <0.5 ---- <0.5 ----mg/kg0.510061-02-6

<0.51.2-Dibromoethane (EDB) <0.5 ---- <0.5 ----mg/kg0.5106-93-4

EP074E: Halogenated Aliphatic Compounds

<5Dichlorodifluoromethane <5 ---- <5 ----mg/kg575-71-8

<5Chloromethane <5 ---- <5 ----mg/kg574-87-3

<5Vinyl chloride <5 ---- <5 ----mg/kg575-01-4

<5Bromomethane <5 ---- <5 ----mg/kg574-83-9

<5Chloroethane <5 ---- <5 ----mg/kg575-00-3

<5Trichlorofluoromethane <5 ---- <5 ----mg/kg575-69-4

<0.51.1-Dichloroethene <0.5 ---- <0.5 ----mg/kg0.575-35-4

<0.5Iodomethane <0.5 ---- <0.5 ----mg/kg0.574-88-4

<0.5trans-1.2-Dichloroethene <0.5 ---- <0.5 ----mg/kg0.5156-60-5

<0.51.1-Dichloroethane <0.5 ---- <0.5 ----mg/kg0.575-34-3

<0.5cis-1.2-Dichloroethene <0.5 ---- <0.5 ----mg/kg0.5156-59-2

<0.51.1.1-Trichloroethane <0.5 ---- <0.5 ----mg/kg0.571-55-6

Page 51: Appendix - Department of Defence

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AECOM Australia Pty Ltd

Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<0.51.1-Dichloropropylene <0.5 ---- <0.5 ----mg/kg0.5563-58-6

<0.5Carbon Tetrachloride <0.5 ---- <0.5 ----mg/kg0.556-23-5

<0.51.2-Dichloroethane <0.5 ---- <0.5 ----mg/kg0.5107-06-2

<0.5Trichloroethene <0.5 ---- <0.5 ----mg/kg0.579-01-6

<0.5Dibromomethane <0.5 ---- <0.5 ----mg/kg0.574-95-3

<0.51.1.2-Trichloroethane <0.5 ---- <0.5 ----mg/kg0.579-00-5

<0.51.3-Dichloropropane <0.5 ---- <0.5 ----mg/kg0.5142-28-9

<0.5Tetrachloroethene <0.5 ---- <0.5 ----mg/kg0.5127-18-4

<0.51.1.1.2-Tetrachloroethane <0.5 ---- <0.5 ----mg/kg0.5630-20-6

<0.5trans-1.4-Dichloro-2-butene <0.5 ---- <0.5 ----mg/kg0.5110-57-6

<0.5cis-1.4-Dichloro-2-butene <0.5 ---- <0.5 ----mg/kg0.51476-11-5

<0.51.1.2.2-Tetrachloroethane <0.5 ---- <0.5 ----mg/kg0.579-34-5

<0.51.2.3-Trichloropropane <0.5 ---- <0.5 ----mg/kg0.596-18-4

<0.5Pentachloroethane <0.5 ---- <0.5 ----mg/kg0.576-01-7

<0.51.2-Dibromo-3-chloropropane <0.5 ---- <0.5 ----mg/kg0.596-12-8

EP074F: Halogenated Aromatic Compounds

<0.5Chlorobenzene <0.5 ---- <0.5 ----mg/kg0.5108-90-7

<0.5Bromobenzene <0.5 ---- <0.5 ----mg/kg0.5108-86-1

<0.52-Chlorotoluene <0.5 ---- <0.5 ----mg/kg0.595-49-8

<0.54-Chlorotoluene <0.5 ---- <0.5 ----mg/kg0.5106-43-4

<0.51.2.3-Trichlorobenzene <0.5 ---- <0.5 ----mg/kg0.587-61-6

EP074G: Trihalomethanes

<0.5Chloroform <0.5 ---- <0.5 ----mg/kg0.567-66-3

<0.5Bromodichloromethane <0.5 ---- <0.5 ----mg/kg0.575-27-4

<0.5Dibromochloromethane <0.5 ---- <0.5 ----mg/kg0.5124-48-1

<0.5Bromoform <0.5 ---- <0.5 ----mg/kg0.575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.8Naphthalene <0.8 ---- <0.5 ----mg/kg0.591-20-3

<0.8Acenaphthylene <0.8 ---- <0.5 ----mg/kg0.5208-96-8

<0.8Acenaphthene <0.8 ---- <0.5 ----mg/kg0.583-32-9

<0.8Fluorene <0.8 ---- <0.5 ----mg/kg0.586-73-7

3.1Phenanthrene <0.8 ---- <0.5 ----mg/kg0.585-01-8

<0.8Anthracene <0.8 ---- <0.5 ----mg/kg0.5120-12-7

7.9Fluoranthene <0.8 ---- <0.5 ----mg/kg0.5206-44-0

Page 52: Appendix - Department of Defence

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:Client

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

6.0Pyrene <0.8 ---- <0.5 ----mg/kg0.5129-00-0

1.9Benz(a)anthracene <0.8 ---- <0.5 ----mg/kg0.556-55-3

3.3Chrysene <0.8 ---- <0.5 ----mg/kg0.5218-01-9

4.8Benzo(b+j)fluoranthene <0.8 ---- <0.5 ----mg/kg0.5205-99-2 205-82-3

1.4Benzo(k)fluoranthene <0.8 ---- <0.5 ----mg/kg0.5207-08-9

2.0Benzo(a)pyrene <0.8 ---- <0.5 ----mg/kg0.550-32-8

2.1Indeno(1.2.3.cd)pyrene <0.8 ---- <0.5 ----mg/kg0.5193-39-5

<0.8Dibenz(a.h)anthracene <0.8 ---- <0.5 ----mg/kg0.553-70-3

3.1Benzo(g.h.i)perylene <0.8 ---- <0.5 ----mg/kg0.5191-24-2

35.6^ <0.5 ---- <0.5 ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

3.1^ <0.5 ---- <0.5 ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

3.3^ 0.6 ---- 0.6 ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

3.6^ 1.2 ---- 1.2 ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP075A: Phenolic Compounds

<0.6Phenol <0.6 ---- <0.5 ----mg/kg0.5108-95-2

<0.62-Chlorophenol <0.6 ---- <0.5 ----mg/kg0.595-57-8

<0.62-Methylphenol <0.6 ---- <0.5 ----mg/kg0.595-48-7

<1.23- & 4-Methylphenol <1.2 ---- <0.6 ----mg/kg0.51319-77-3

<0.62-Nitrophenol <0.6 ---- <0.5 ----mg/kg0.588-75-5

<0.62.4-Dimethylphenol <0.6 ---- <0.5 ----mg/kg0.5105-67-9

<0.62.4-Dichlorophenol <0.6 ---- <0.5 ----mg/kg0.5120-83-2

<0.62.6-Dichlorophenol <0.6 ---- <0.5 ----mg/kg0.587-65-0

<0.64-Chloro-3-methylphenol <0.6 ---- <0.5 ----mg/kg0.559-50-7

<0.62.4.6-Trichlorophenol <0.6 ---- <0.5 ----mg/kg0.588-06-2

<0.62.4.5-Trichlorophenol <0.6 ---- <0.5 ----mg/kg0.595-95-4

<1Pentachlorophenol <1 ---- <1 ----mg/kg187-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<0.62-Methylnaphthalene <0.6 ---- <0.5 ----mg/kg0.591-57-6

<0.62-Chloronaphthalene <0.6 ---- <0.5 ----mg/kg0.591-58-7

<0.6N-2-Fluorenyl Acetamide <0.6 ---- <0.5 ----mg/kg0.553-96-3

<0.67.12-Dimethylbenz(a)anthracene <0.6 ---- <0.5 ----mg/kg0.557-97-6

<0.63-Methylcholanthrene <0.6 ---- <0.5 ----mg/kg0.556-49-5

EP075C: Phthalate Esters

<0.6Dimethyl phthalate <0.6 ---- <0.5 ----mg/kg0.5131-11-3

Page 53: Appendix - Department of Defence

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Work Order :

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ES1716547

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<0.6Diethyl phthalate <0.6 ---- <0.5 ----mg/kg0.584-66-2

2.8Di-n-butyl phthalate <0.6 ---- <0.5 ----mg/kg0.584-74-2

<0.6Butyl benzyl phthalate <0.6 ---- <0.5 ----mg/kg0.585-68-7

<5.0bis(2-ethylhexyl) phthalate <5.0 ---- <5.0 ----mg/kg5117-81-7

<0.6Di-n-octylphthalate <0.6 ---- <0.5 ----mg/kg0.5117-84-0

EP075D: Nitrosamines

<0.6N-Nitrosomethylethylamine <0.6 ---- <0.5 ----mg/kg0.510595-95-6

<0.6N-Nitrosodiethylamine <0.6 ---- <0.5 ----mg/kg0.555-18-5

<1.0N-Nitrosopyrrolidine <1.0 ---- <1.0 ----mg/kg1930-55-2

<0.6N-Nitrosomorpholine <0.6 ---- <0.5 ----mg/kg0.559-89-2

<0.6N-Nitrosodi-n-propylamine <0.6 ---- <0.5 ----mg/kg0.5621-64-7

<0.6N-Nitrosopiperidine <0.6 ---- <0.5 ----mg/kg0.5100-75-4

<0.6N-Nitrosodibutylamine <0.6 ---- <0.5 ----mg/kg0.5924-16-3

<1.2N-Nitrosodiphenyl &

Diphenylamine

<1.2 ---- <1.0 ----mg/kg186-30-6 122-39-4

<0.6Methapyrilene <0.6 ---- <0.5 ----mg/kg0.591-80-5

EP075E: Nitroaromatics and Ketones

<0.62-Picoline <0.6 ---- <0.5 ----mg/kg0.5109-06-8

<0.6Acetophenone <0.6 ---- <0.5 ----mg/kg0.598-86-2

<0.6Nitrobenzene <0.6 ---- <0.5 ----mg/kg0.598-95-3

<0.6Isophorone <0.6 ---- <0.5 ----mg/kg0.578-59-1

<1.02.6-Dinitrotoluene <1.0 ---- <1.0 ----mg/kg1606-20-2

<1.02.4-Dinitrotoluene <1.0 ---- <1.0 ----mg/kg1121-14-2

<0.61-Naphthylamine <0.6 ---- <0.5 ----mg/kg0.5134-32-7

<0.64-Nitroquinoline-N-oxide <0.6 ---- <0.5 ----mg/kg0.556-57-5

<0.65-Nitro-o-toluidine <0.6 ---- <0.5 ----mg/kg0.599-55-8

<1Azobenzene <1 ---- <1 ----mg/kg1103-33-3

<0.61.3.5-Trinitrobenzene <0.6 ---- <0.5 ----mg/kg0.599-35-4

<0.6Phenacetin <0.6 ---- <0.5 ----mg/kg0.562-44-2

<0.64-Aminobiphenyl <0.6 ---- <0.5 ----mg/kg0.592-67-1

<0.6Pentachloronitrobenzene <0.6 ---- <0.5 ----mg/kg0.582-68-8

<0.6Pronamide <0.6 ---- <0.5 ----mg/kg0.523950-58-5

<0.6Dimethylaminoazobenzene <0.6 ---- <0.5 ----mg/kg0.560-11-7

<0.6Chlorobenzilate <0.6 ---- <0.5 ----mg/kg0.5510-15-6

Page 54: Appendix - Department of Defence

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Work Order :

:Client

ES1716547

60547028, TASK 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP075F: Haloethers

<0.6Bis(2-chloroethyl) ether <0.6 ---- <0.5 ----mg/kg0.5111-44-4

<0.6Bis(2-chloroethoxy) methane <0.6 ---- <0.5 ----mg/kg0.5111-91-1

<0.64-Chlorophenyl phenyl ether <0.6 ---- <0.5 ----mg/kg0.57005-72-3

<0.64-Bromophenyl phenyl ether <0.6 ---- <0.5 ----mg/kg0.5101-55-3

EP075G: Chlorinated Hydrocarbons

<0.61.3-Dichlorobenzene <0.6 ---- <0.5 ----mg/kg0.5541-73-1

<0.61.4-Dichlorobenzene <0.6 ---- <0.5 ----mg/kg0.5106-46-7

<0.61.2-Dichlorobenzene <0.6 ---- <0.5 ----mg/kg0.595-50-1

<0.6Hexachloroethane <0.6 ---- <0.5 ----mg/kg0.567-72-1

<0.61.2.4-Trichlorobenzene <0.6 ---- <0.5 ----mg/kg0.5120-82-1

<0.6Hexachloropropylene <0.6 ---- <0.5 ----mg/kg0.51888-71-7

<0.6Hexachlorobutadiene <0.6 ---- <0.5 ----mg/kg0.587-68-3

<2.5Hexachlorocyclopentadiene <2.5 ---- <2.5 ----mg/kg2.577-47-4

<0.6Pentachlorobenzene <0.6 ---- <0.5 ----mg/kg0.5608-93-5

<1.0Hexachlorobenzene (HCB) <1.0 ---- <1.0 ----mg/kg1118-74-1

EP075H: Anilines and Benzidines

<0.6Aniline <0.6 ---- <0.5 ----mg/kg0.562-53-3

<0.64-Chloroaniline <0.6 ---- <0.5 ----mg/kg0.5106-47-8

<1.02-Nitroaniline <1.0 ---- <1.0 ----mg/kg188-74-4

<1.03-Nitroaniline <1.0 ---- <1.0 ----mg/kg199-09-2

<0.6Dibenzofuran <0.6 ---- <0.5 ----mg/kg0.5132-64-9

<0.64-Nitroaniline <0.6 ---- <0.5 ----mg/kg0.5100-01-6

0.6Carbazole <0.6 ---- <0.5 ----mg/kg0.586-74-8

<0.63.3`-Dichlorobenzidine <0.6 ---- <0.5 ----mg/kg0.591-94-1

EP075I: Organochlorine Pesticides

<0.6alpha-BHC <0.6 ---- <0.5 ----mg/kg0.5319-84-6

<0.6beta-BHC <0.6 ---- <0.5 ----mg/kg0.5319-85-7

<0.6gamma-BHC <0.6 ---- <0.5 ----mg/kg0.558-89-9

<0.6delta-BHC <0.6 ---- <0.5 ----mg/kg0.5319-86-8

<0.6Heptachlor <0.6 ---- <0.5 ----mg/kg0.576-44-8

<0.6Aldrin <0.6 ---- <0.5 ----mg/kg0.5309-00-2

<0.6Heptachlor epoxide <0.6 ---- <0.5 ----mg/kg0.51024-57-3

<0.6alpha-Endosulfan <0.6 ---- <0.5 ----mg/kg0.5959-98-8

<0.64.4`-DDE <0.6 ---- <0.5 ----mg/kg0.572-55-9

Page 55: Appendix - Department of Defence

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Work Order :

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AECOM Australia Pty Ltd

Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<0.6Dieldrin <0.6 ---- <0.5 ----mg/kg0.560-57-1

<0.6Endrin <0.6 ---- <0.5 ----mg/kg0.572-20-8

<0.6beta-Endosulfan <0.6 ---- <0.5 ----mg/kg0.533213-65-9

<0.64.4`-DDD <0.6 ---- <0.5 ----mg/kg0.572-54-8

<0.6Endosulfan sulfate <0.6 ---- <0.5 ----mg/kg0.51031-07-8

<1.04.4`-DDT <1.0 ---- <1.0 ----mg/kg150-29-3

EP075J: Organophosphorus Pesticides

<0.6Dichlorvos <0.6 ---- <0.5 ----mg/kg0.562-73-7

<0.6Dimethoate <0.6 ---- <0.5 ----mg/kg0.560-51-5

<0.6Diazinon <0.6 ---- <0.5 ----mg/kg0.5333-41-5

<0.6Chlorpyrifos-methyl <0.6 ---- <0.5 ----mg/kg0.55598-13-0

<0.6Malathion <0.6 ---- <0.5 ----mg/kg0.5121-75-5

<0.6Fenthion <0.6 ---- <0.5 ----mg/kg0.555-38-9

<0.6Chlorpyrifos <0.6 ---- <0.5 ----mg/kg0.52921-88-2

<0.6Pirimphos-ethyl <0.6 ---- <0.5 ----mg/kg0.523505-41-1

<0.6Chlorfenvinphos <0.6 ---- <0.5 ----mg/kg0.5470-90-6

<0.6Prothiofos <0.6 ---- <0.5 ----mg/kg0.534643-46-4

<0.6Ethion <0.6 ---- <0.5 ----mg/kg0.5563-12-2

EP080/071: Total Petroleum Hydrocarbons

<10 <10 ---- <10 ----mg/kg10----C6 - C9 Fraction

<50 <50 ---- <50 ----mg/kg50----C10 - C14 Fraction

520 <100 ---- <100 ----mg/kg100----C15 - C28 Fraction

380 <100 ---- <100 ----mg/kg100----C29 - C36 Fraction

900^ <50 ---- <50 ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction <10 ---- <10 ----mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

<10 ---- <10 ----mg/kg10C6_C10-BTEX

80 <50 ---- <50 ----mg/kg50---->C10 - C16 Fraction

750 <100 ---- <100 ----mg/kg100---->C16 - C34 Fraction

200 <100 ---- <100 ----mg/kg100---->C34 - C40 Fraction

1030^ <50 ---- <50 ----mg/kg50---->C10 - C40 Fraction (sum)

80^ <50 ---- <50 ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

Page 56: Appendix - Department of Defence

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP080: BTEXN

<0.2Benzene <0.2 ---- <0.2 ----mg/kg0.271-43-2

0.7Toluene <0.5 ---- <0.5 ----mg/kg0.5108-88-3

<0.5Ethylbenzene <0.5 ---- <0.5 ----mg/kg0.5100-41-4

<0.5meta- & para-Xylene <0.5 ---- <0.5 ----mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene <0.5 ---- <0.5 ----mg/kg0.595-47-6

0.7^ <0.2 ---- <0.2 ----mg/kg0.2----Sum of BTEX

<0.5^ Total Xylenes <0.5 ---- <0.5 ----mg/kg0.51330-20-7

<1Naphthalene <1 ---- <1 ----mg/kg191-20-3

EP116: 1.4-Dioxane

<0.05ø1.4-Dioxane <0.05 ---- <0.05 ----mg/kg0.05123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.0003Perfluorobutane sulfonic acid

(PFBS)

<0.0002 <0.0002 0.0004 <0.0002mg/kg0.0002375-73-5

0.0005Perfluoropentane sulfonic acid

(PFPeS)

0.0002 0.0002 0.0007 <0.0002mg/kg0.00022706-91-4

0.0479Perfluorohexane sulfonic acid

(PFHxS)

0.0133 0.0064 0.0151 0.0033mg/kg0.0002355-46-4

0.0068Perfluoroheptane sulfonic acid

(PFHpS)

0.0009 0.0003 0.0019 0.0003mg/kg0.0002375-92-8

0.722Perfluorooctane sulfonic acid

(PFOS)

0.0777 0.0416 0.158 0.0367mg/kg0.00021763-23-1

0.0060Perfluorodecane sulfonic acid

(PFDS)

0.0011 0.0005 0.0008 0.0005mg/kg0.0002335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 0.001mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) 0.0005 <0.0002 <0.0002 <0.0002mg/kg0.00022706-90-3

0.0057Perfluorohexanoic acid (PFHxA) 0.0005 0.0005 0.0006 0.0002mg/kg0.0002307-24-4

0.0014Perfluoroheptanoic acid (PFHpA) 0.0004 0.0003 <0.0002 <0.0002mg/kg0.0002375-85-9

0.0066Perfluorooctanoic acid (PFOA) 0.0010 0.0006 0.0008 0.0003mg/kg0.0002335-67-1

0.0042Perfluorononanoic acid (PFNA) 0.0011 0.0002 <0.0002 0.0003mg/kg0.0002375-95-1

0.0041Perfluorodecanoic acid (PFDA) 0.0014 <0.0002 0.0005 0.0003mg/kg0.0002335-76-2

0.0085Perfluoroundecanoic acid

(PFUnDA)

0.0010 <0.0002 0.0011 0.0002mg/kg0.00022058-94-8

0.0152Perfluorododecanoic acid

(PFDoDA)

0.0013 <0.0002 0.0005 <0.0002mg/kg0.0002307-55-1

Page 57: Appendix - Department of Defence

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

0.0078Perfluorotridecanoic acid

(PFTrDA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.000272629-94-8

0.0063Perfluorotetradecanoic acid

(PFTeDA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.0106Perfluorooctane sulfonamide

(FOSA)

<0.0002 <0.0002 0.0020 <0.0002mg/kg0.0002754-91-6

<0.0005N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000531506-32-8

<0.0005N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00054151-50-2

<0.0005N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00052448-09-7

<0.0005N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.00051691-99-2

<0.0002N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9

<0.0002N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.00054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4

0.00406:2 Fluorotelomer sulfonic acid

(6:2 FTS)

0.0006 <0.0005 <0.0005 0.0006mg/kg0.000527619-97-2

0.04638:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.000539108-34-4

0.006510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.911 0.101 0.0506 0.182 0.0437mg/kg0.0002----Sum of PFAS

0.770Sum of PFHxS and PFOS 0.0910 0.0480 0.173 0.0400mg/kg0.0002355-46-4/1763-23-

1

0.834 0.0940 0.0494 0.175 0.0421mg/kg0.0002----Sum of PFAS (WA DER List)

EP068S: Organochlorine Pesticide Surrogate

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Analytical Results

0902_SD015_0307170902_SD014_0307170902_SD013_0307170902_SD012_0307170902_SD011_040717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-039ES1716547-038ES1716547-037ES1716547-036ES1716547-035UnitLORCAS NumberCompound

Result Result Result Result Result

EP068S: Organochlorine Pesticide Surrogate - Continued

101Dibromo-DDE 101 ---- 105 ----%0.0521655-73-2

EP068T: Organophosphorus Pesticide Surrogate

111DEF 95.3 ---- 91.4 ----%0.0578-48-8

EP074S: VOC Surrogates

77.41.2-Dichloroethane-D4 90.8 ---- 77.9 ----%0.517060-07-0

75.0Toluene-D8 94.5 ---- 82.8 ----%0.52037-26-5

77.34-Bromofluorobenzene 93.7 ---- 76.9 ----%0.5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

79.8Phenol-d6 85.7 ---- 88.0 ----%0.513127-88-3

80.02-Chlorophenol-D4 90.4 ---- 87.6 ----%0.593951-73-6

88.82.4.6-Tribromophenol 88.5 ---- 77.1 ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

81.02-Fluorobiphenyl 87.9 ---- 88.0 ----%0.5321-60-8

87.6Anthracene-d10 94.5 ---- 92.1 ----%0.51719-06-8

87.54-Terphenyl-d14 89.6 ---- 82.7 ----%0.51718-51-0

EP075S: Acid Extractable Surrogates

79.62-Fluorophenol 90.0 ---- 87.7 ----%0.5367-12-4

84.7Phenol-d6 90.1 ---- 89.8 ----%0.513127-88-3

76.82-Chlorophenol-D4 82.8 ---- 82.8 ----%0.593951-73-6

93.22.4.6-Tribromophenol 83.1 ---- 79.3 ----%0.5118-79-6

EP075T: Base/Neutral Extractable Surrogates

86.5Nitrobenzene-D5 87.5 ---- 86.2 ----%0.54165-60-0

59.11.2-Dichlorobenzene-D4 71.6 ---- 65.4 ----%0.52199-69-1

84.72-Fluorobiphenyl 91.3 ---- 92.3 ----%0.5321-60-8

94.7Anthracene-d10 98.9 ---- 98.7 ----%0.51719-06-8

96.74-Terphenyl-d14 99.0 ---- 98.4 ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

78.51.2-Dichloroethane-D4 92.6 ---- 79.0 ----%0.217060-07-0

77.8Toluene-D8 98.2 ---- 85.9 ----%0.22037-26-5

78.24-Bromofluorobenzene 95.8 ---- 78.3 ----%0.2460-00-4

EP116S: 1.4-Dioxane Surrogate

108ø1.4-Dioxane-d8 101 ---- 105 ----%0.0117647-74-4

EP231S: PFAS Surrogate

122 117 108 118 109%0.0002----13C4-PFOS

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Analytical Results

0902_QC106_0307170902_SD019_0407170902_SD018_0407170902_SD017_0307170902_SD016_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-044ES1716547-043ES1716547-042ES1716547-041ES1716547-040UnitLORCAS NumberCompound

Result Result Result Result Result

EA055: Moisture Content (Dried @ 105-110°C)

39.0 51.2 67.0 46.6 85.6%1----Moisture Content

EP231A: Perfluoroalkyl Sulfonic Acids

<0.0002Perfluorobutane sulfonic acid

(PFBS)

<0.0002 <0.0002 <0.0002 0.0024mg/kg0.0002375-73-5

<0.0002Perfluoropentane sulfonic acid

(PFPeS)

<0.0002 <0.0002 <0.0002 0.0032mg/kg0.00022706-91-4

<0.0002Perfluorohexane sulfonic acid

(PFHxS)

<0.0002 0.0014 0.0005 0.0787mg/kg0.0002355-46-4

<0.0002Perfluoroheptane sulfonic acid

(PFHpS)

<0.0002 0.0002 <0.0002 0.0052mg/kg0.0002375-92-8

0.0022Perfluorooctane sulfonic acid

(PFOS)

0.0003 0.0235 0.0027 0.605mg/kg0.00021763-23-1

<0.0002Perfluorodecane sulfonic acid

(PFDS)

<0.0002 0.0004 <0.0002 0.0102mg/kg0.0002335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.001Perfluorobutanoic acid (PFBA) <0.001 <0.001 <0.001 0.003mg/kg0.001375-22-4

<0.0002Perfluoropentanoic acid (PFPeA) <0.0002 0.0005 <0.0002 0.0065mg/kg0.00022706-90-3

<0.0002Perfluorohexanoic acid (PFHxA) <0.0002 0.0005 <0.0002 0.0174mg/kg0.0002307-24-4

<0.0002Perfluoroheptanoic acid (PFHpA) <0.0002 0.0005 <0.0002 0.0032mg/kg0.0002375-85-9

<0.0002Perfluorooctanoic acid (PFOA) <0.0002 0.0013 <0.0002 0.0118mg/kg0.0002335-67-1

<0.0002Perfluorononanoic acid (PFNA) <0.0002 0.0011 <0.0002 0.0023mg/kg0.0002375-95-1

<0.0002Perfluorodecanoic acid (PFDA) <0.0002 0.0037 <0.0002 0.0028mg/kg0.0002335-76-2

<0.0002Perfluoroundecanoic acid

(PFUnDA)

<0.0002 0.0012 <0.0002 0.0057mg/kg0.00022058-94-8

<0.0002Perfluorododecanoic acid

(PFDoDA)

<0.0002 0.0003 <0.0002 0.0055mg/kg0.0002307-55-1

<0.0002Perfluorotridecanoic acid

(PFTrDA)

<0.0002 <0.0002 <0.0002 0.0026mg/kg0.000272629-94-8

<0.0005Perfluorotetradecanoic acid

(PFTeDA)

<0.0005 <0.0005 <0.0005 0.0031mg/kg0.0005376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.0002Perfluorooctane sulfonamide

(FOSA)

<0.0002 0.0004 <0.0002 0.0220mg/kg0.0002754-91-6

<0.0005N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.000531506-32-8

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Analytical Results

0902_QC106_0307170902_SD019_0407170902_SD018_0407170902_SD017_0307170902_SD016_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

03-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-044ES1716547-043ES1716547-042ES1716547-041ES1716547-040UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.0005N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00054151-50-2

<0.0005N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00052448-09-7

<0.0005N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.0005 <0.0005 <0.0005 <0.0006mg/kg0.00051691-99-2

<0.0002N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022355-31-9

<0.0002N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.0002 <0.0002 <0.0002 <0.0002mg/kg0.00022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.00054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.0005 <0.0005 <0.0005 <0.0005mg/kg0.0005757124-72-4

<0.00056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.0005 <0.0005 <0.0005 0.0025mg/kg0.000527619-97-2

<0.00058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.0005 <0.0005 <0.0005 0.0123mg/kg0.000539108-34-4

<0.000510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.0005 <0.0005 <0.0005 0.0023mg/kg0.0005120226-60-0

EP231P: PFAS Sums

0.0022 0.0003 0.0350 0.0032 0.808mg/kg0.0002----Sum of PFAS

0.0022Sum of PFHxS and PFOS 0.0003 0.0249 0.0032 0.684mg/kg0.0002355-46-4/1763-23-

1

0.0022 0.0003 0.0277 0.0032 0.743mg/kg0.0002----Sum of PFAS (WA DER List)

EP231S: PFAS Surrogate

115 117 125 112 102%0.0002----13C4-PFOS

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EA055: Moisture Content (Dried @ 105-110°C)

66.7 ---- ---- ---- ----%1----Moisture Content

ED007: Exchangeable Cations

8.7 ---- ---- ---- ----meq/100g0.1----Exchangeable Calcium

2.7 ---- ---- ---- ----meq/100g0.1----Exchangeable Magnesium

0.6 ---- ---- ---- ----meq/100g0.1----Exchangeable Potassium

0.8 ---- ---- ---- ----meq/100g0.1----Exchangeable Sodium

12.7 ---- ---- ---- ----meq/100g0.1----Cation Exchange Capacity

EG005T: Total Metals by ICP-AES

22200Iron ---- ---- ---- ----mg/kg507439-89-6

6Arsenic ---- ---- ---- ----mg/kg57440-38-2

12Cadmium ---- ---- ---- ----mg/kg17440-43-9

62Chromium ---- ---- ---- ----mg/kg27440-47-3

59Copper ---- ---- ---- ----mg/kg57440-50-8

116Lead ---- ---- ---- ----mg/kg57439-92-1

20Nickel ---- ---- ---- ----mg/kg27440-02-0

529Zinc ---- ---- ---- ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

<0.1Mercury ---- ---- ---- ----mg/kg0.17439-97-6

EP003: Total Organic Carbon (TOC) in Soil

0.10 ---- ---- ---- ----%0.02----Total Organic Carbon

EP068A: Organochlorine Pesticides (OC)

<0.05alpha-BHC ---- ---- ---- ----mg/kg0.05319-84-6

<0.05Hexachlorobenzene (HCB) ---- ---- ---- ----mg/kg0.05118-74-1

<0.05beta-BHC ---- ---- ---- ----mg/kg0.05319-85-7

<0.05gamma-BHC ---- ---- ---- ----mg/kg0.0558-89-9

<0.05delta-BHC ---- ---- ---- ----mg/kg0.05319-86-8

<0.05Heptachlor ---- ---- ---- ----mg/kg0.0576-44-8

<0.05Aldrin ---- ---- ---- ----mg/kg0.05309-00-2

<0.05Heptachlor epoxide ---- ---- ---- ----mg/kg0.051024-57-3

<0.05^ ---- ---- ---- ----mg/kg0.05----Total Chlordane (sum)

<0.05trans-Chlordane ---- ---- ---- ----mg/kg0.055103-74-2

<0.05alpha-Endosulfan ---- ---- ---- ----mg/kg0.05959-98-8

<0.05cis-Chlordane ---- ---- ---- ----mg/kg0.055103-71-9

<0.05Dieldrin ---- ---- ---- ----mg/kg0.0560-57-1

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP068A: Organochlorine Pesticides (OC) - Continued

<0.054.4`-DDE ---- ---- ---- ----mg/kg0.0572-55-9

<0.05Endrin ---- ---- ---- ----mg/kg0.0572-20-8

<0.05beta-Endosulfan ---- ---- ---- ----mg/kg0.0533213-65-9

<0.05^ Endosulfan (sum) ---- ---- ---- ----mg/kg0.05115-29-7

<0.054.4`-DDD ---- ---- ---- ----mg/kg0.0572-54-8

<0.05Endrin aldehyde ---- ---- ---- ----mg/kg0.057421-93-4

<0.05Endosulfan sulfate ---- ---- ---- ----mg/kg0.051031-07-8

<0.24.4`-DDT ---- ---- ---- ----mg/kg0.250-29-3

<0.05Endrin ketone ---- ---- ---- ----mg/kg0.0553494-70-5

<0.2Methoxychlor ---- ---- ---- ----mg/kg0.272-43-5

<0.05^ Sum of Aldrin + Dieldrin ---- ---- ---- ----mg/kg0.05309-00-2/60-57-1

<0.05^ Sum of DDD + DDE + DDT ---- ---- ---- ----mg/kg0.0572-54-8/72-55-9/5

0-2

EP068B: Organophosphorus Pesticides (OP)

<0.05Dichlorvos ---- ---- ---- ----mg/kg0.0562-73-7

<0.05Demeton-S-methyl ---- ---- ---- ----mg/kg0.05919-86-8

<0.2Monocrotophos ---- ---- ---- ----mg/kg0.26923-22-4

<0.05Dimethoate ---- ---- ---- ----mg/kg0.0560-51-5

<0.05Diazinon ---- ---- ---- ----mg/kg0.05333-41-5

<0.05Chlorpyrifos-methyl ---- ---- ---- ----mg/kg0.055598-13-0

<0.2Parathion-methyl ---- ---- ---- ----mg/kg0.2298-00-0

<0.05Malathion ---- ---- ---- ----mg/kg0.05121-75-5

<0.05Fenthion ---- ---- ---- ----mg/kg0.0555-38-9

<0.05Chlorpyrifos ---- ---- ---- ----mg/kg0.052921-88-2

<0.2Parathion ---- ---- ---- ----mg/kg0.256-38-2

<0.05Pirimphos-ethyl ---- ---- ---- ----mg/kg0.0523505-41-1

<0.05Chlorfenvinphos ---- ---- ---- ----mg/kg0.05470-90-6

<0.05Bromophos-ethyl ---- ---- ---- ----mg/kg0.054824-78-6

<0.05Fenamiphos ---- ---- ---- ----mg/kg0.0522224-92-6

<0.05Prothiofos ---- ---- ---- ----mg/kg0.0534643-46-4

<0.05Ethion ---- ---- ---- ----mg/kg0.05563-12-2

<0.05Carbophenothion ---- ---- ---- ----mg/kg0.05786-19-6

<0.05Azinphos Methyl ---- ---- ---- ----mg/kg0.0586-50-0

EP074A: Monocyclic Aromatic Hydrocarbons

<0.5Styrene ---- ---- ---- ----mg/kg0.5100-42-5

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP074A: Monocyclic Aromatic Hydrocarbons - Continued

<0.5Isopropylbenzene ---- ---- ---- ----mg/kg0.598-82-8

<0.5n-Propylbenzene ---- ---- ---- ----mg/kg0.5103-65-1

<0.51.3.5-Trimethylbenzene ---- ---- ---- ----mg/kg0.5108-67-8

<0.5sec-Butylbenzene ---- ---- ---- ----mg/kg0.5135-98-8

<0.51.2.4-Trimethylbenzene ---- ---- ---- ----mg/kg0.595-63-6

<0.5tert-Butylbenzene ---- ---- ---- ----mg/kg0.598-06-6

0.5p-Isopropyltoluene ---- ---- ---- ----mg/kg0.599-87-6

<0.5n-Butylbenzene ---- ---- ---- ----mg/kg0.5104-51-8

EP074B: Oxygenated Compounds

<5Vinyl Acetate ---- ---- ---- ----mg/kg5108-05-4

<52-Butanone (MEK) ---- ---- ---- ----mg/kg578-93-3

<54-Methyl-2-pentanone (MIBK) ---- ---- ---- ----mg/kg5108-10-1

<52-Hexanone (MBK) ---- ---- ---- ----mg/kg5591-78-6

EP074C: Sulfonated Compounds

<0.5Carbon disulfide ---- ---- ---- ----mg/kg0.575-15-0

EP074D: Fumigants

<0.52.2-Dichloropropane ---- ---- ---- ----mg/kg0.5594-20-7

<0.51.2-Dichloropropane ---- ---- ---- ----mg/kg0.578-87-5

<0.5cis-1.3-Dichloropropylene ---- ---- ---- ----mg/kg0.510061-01-5

<0.5trans-1.3-Dichloropropylene ---- ---- ---- ----mg/kg0.510061-02-6

<0.51.2-Dibromoethane (EDB) ---- ---- ---- ----mg/kg0.5106-93-4

EP074E: Halogenated Aliphatic Compounds

<5Dichlorodifluoromethane ---- ---- ---- ----mg/kg575-71-8

<5Chloromethane ---- ---- ---- ----mg/kg574-87-3

<5Vinyl chloride ---- ---- ---- ----mg/kg575-01-4

<5Bromomethane ---- ---- ---- ----mg/kg574-83-9

<5Chloroethane ---- ---- ---- ----mg/kg575-00-3

<5Trichlorofluoromethane ---- ---- ---- ----mg/kg575-69-4

<0.51.1-Dichloroethene ---- ---- ---- ----mg/kg0.575-35-4

<0.5Iodomethane ---- ---- ---- ----mg/kg0.574-88-4

<0.5trans-1.2-Dichloroethene ---- ---- ---- ----mg/kg0.5156-60-5

<0.51.1-Dichloroethane ---- ---- ---- ----mg/kg0.575-34-3

<0.5cis-1.2-Dichloroethene ---- ---- ---- ----mg/kg0.5156-59-2

<0.51.1.1-Trichloroethane ---- ---- ---- ----mg/kg0.571-55-6

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP074E: Halogenated Aliphatic Compounds - Continued

<0.51.1-Dichloropropylene ---- ---- ---- ----mg/kg0.5563-58-6

<0.5Carbon Tetrachloride ---- ---- ---- ----mg/kg0.556-23-5

<0.51.2-Dichloroethane ---- ---- ---- ----mg/kg0.5107-06-2

<0.5Trichloroethene ---- ---- ---- ----mg/kg0.579-01-6

<0.5Dibromomethane ---- ---- ---- ----mg/kg0.574-95-3

<0.51.1.2-Trichloroethane ---- ---- ---- ----mg/kg0.579-00-5

<0.51.3-Dichloropropane ---- ---- ---- ----mg/kg0.5142-28-9

<0.5Tetrachloroethene ---- ---- ---- ----mg/kg0.5127-18-4

<0.51.1.1.2-Tetrachloroethane ---- ---- ---- ----mg/kg0.5630-20-6

<0.5trans-1.4-Dichloro-2-butene ---- ---- ---- ----mg/kg0.5110-57-6

<0.5cis-1.4-Dichloro-2-butene ---- ---- ---- ----mg/kg0.51476-11-5

<0.51.1.2.2-Tetrachloroethane ---- ---- ---- ----mg/kg0.579-34-5

<0.51.2.3-Trichloropropane ---- ---- ---- ----mg/kg0.596-18-4

<0.5Pentachloroethane ---- ---- ---- ----mg/kg0.576-01-7

<0.51.2-Dibromo-3-chloropropane ---- ---- ---- ----mg/kg0.596-12-8

EP074F: Halogenated Aromatic Compounds

<0.5Chlorobenzene ---- ---- ---- ----mg/kg0.5108-90-7

<0.5Bromobenzene ---- ---- ---- ----mg/kg0.5108-86-1

<0.52-Chlorotoluene ---- ---- ---- ----mg/kg0.595-49-8

<0.54-Chlorotoluene ---- ---- ---- ----mg/kg0.5106-43-4

<0.51.2.3-Trichlorobenzene ---- ---- ---- ----mg/kg0.587-61-6

EP074G: Trihalomethanes

<0.5Chloroform ---- ---- ---- ----mg/kg0.567-66-3

<0.5Bromodichloromethane ---- ---- ---- ----mg/kg0.575-27-4

<0.5Dibromochloromethane ---- ---- ---- ----mg/kg0.5124-48-1

<0.5Bromoform ---- ---- ---- ----mg/kg0.575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.8Naphthalene ---- ---- ---- ----mg/kg0.591-20-3

<0.8Acenaphthylene ---- ---- ---- ----mg/kg0.5208-96-8

<0.8Acenaphthene ---- ---- ---- ----mg/kg0.583-32-9

<0.8Fluorene ---- ---- ---- ----mg/kg0.586-73-7

<0.8Phenanthrene ---- ---- ---- ----mg/kg0.585-01-8

<0.8Anthracene ---- ---- ---- ----mg/kg0.5120-12-7

<0.8Fluoranthene ---- ---- ---- ----mg/kg0.5206-44-0

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<0.8Pyrene ---- ---- ---- ----mg/kg0.5129-00-0

<0.8Benz(a)anthracene ---- ---- ---- ----mg/kg0.556-55-3

<0.8Chrysene ---- ---- ---- ----mg/kg0.5218-01-9

<0.8Benzo(b+j)fluoranthene ---- ---- ---- ----mg/kg0.5205-99-2 205-82-3

<0.8Benzo(k)fluoranthene ---- ---- ---- ----mg/kg0.5207-08-9

<0.8Benzo(a)pyrene ---- ---- ---- ----mg/kg0.550-32-8

<0.8Indeno(1.2.3.cd)pyrene ---- ---- ---- ----mg/kg0.5193-39-5

<0.8Dibenz(a.h)anthracene ---- ---- ---- ----mg/kg0.553-70-3

<0.8Benzo(g.h.i)perylene ---- ---- ---- ----mg/kg0.5191-24-2

<0.5^ ---- ---- ---- ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

0.6^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

1.2^ ---- ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP075A: Phenolic Compounds

<0.6Phenol ---- ---- ---- ----mg/kg0.5108-95-2

<0.62-Chlorophenol ---- ---- ---- ----mg/kg0.595-57-8

<0.62-Methylphenol ---- ---- ---- ----mg/kg0.595-48-7

<1.23- & 4-Methylphenol ---- ---- ---- ----mg/kg0.51319-77-3

<0.62-Nitrophenol ---- ---- ---- ----mg/kg0.588-75-5

<0.62.4-Dimethylphenol ---- ---- ---- ----mg/kg0.5105-67-9

<0.62.4-Dichlorophenol ---- ---- ---- ----mg/kg0.5120-83-2

<0.62.6-Dichlorophenol ---- ---- ---- ----mg/kg0.587-65-0

<0.64-Chloro-3-methylphenol ---- ---- ---- ----mg/kg0.559-50-7

<0.62.4.6-Trichlorophenol ---- ---- ---- ----mg/kg0.588-06-2

<0.62.4.5-Trichlorophenol ---- ---- ---- ----mg/kg0.595-95-4

<1Pentachlorophenol ---- ---- ---- ----mg/kg187-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<0.62-Methylnaphthalene ---- ---- ---- ----mg/kg0.591-57-6

<0.62-Chloronaphthalene ---- ---- ---- ----mg/kg0.591-58-7

<0.6N-2-Fluorenyl Acetamide ---- ---- ---- ----mg/kg0.553-96-3

<0.67.12-Dimethylbenz(a)anthracene ---- ---- ---- ----mg/kg0.557-97-6

<0.63-Methylcholanthrene ---- ---- ---- ----mg/kg0.556-49-5

EP075C: Phthalate Esters

<0.6Dimethyl phthalate ---- ---- ---- ----mg/kg0.5131-11-3

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP075C: Phthalate Esters - Continued

<0.6Diethyl phthalate ---- ---- ---- ----mg/kg0.584-66-2

<0.6Di-n-butyl phthalate ---- ---- ---- ----mg/kg0.584-74-2

0.6Butyl benzyl phthalate ---- ---- ---- ----mg/kg0.585-68-7

5.7bis(2-ethylhexyl) phthalate ---- ---- ---- ----mg/kg5117-81-7

<0.6Di-n-octylphthalate ---- ---- ---- ----mg/kg0.5117-84-0

EP075D: Nitrosamines

<0.6N-Nitrosomethylethylamine ---- ---- ---- ----mg/kg0.510595-95-6

<0.6N-Nitrosodiethylamine ---- ---- ---- ----mg/kg0.555-18-5

<1.0N-Nitrosopyrrolidine ---- ---- ---- ----mg/kg1930-55-2

<0.6N-Nitrosomorpholine ---- ---- ---- ----mg/kg0.559-89-2

<0.6N-Nitrosodi-n-propylamine ---- ---- ---- ----mg/kg0.5621-64-7

<0.6N-Nitrosopiperidine ---- ---- ---- ----mg/kg0.5100-75-4

<0.6N-Nitrosodibutylamine ---- ---- ---- ----mg/kg0.5924-16-3

<1.2N-Nitrosodiphenyl &

Diphenylamine

---- ---- ---- ----mg/kg186-30-6 122-39-4

<0.6Methapyrilene ---- ---- ---- ----mg/kg0.591-80-5

EP075E: Nitroaromatics and Ketones

<0.62-Picoline ---- ---- ---- ----mg/kg0.5109-06-8

<0.6Acetophenone ---- ---- ---- ----mg/kg0.598-86-2

<0.6Nitrobenzene ---- ---- ---- ----mg/kg0.598-95-3

<0.6Isophorone ---- ---- ---- ----mg/kg0.578-59-1

<1.02.6-Dinitrotoluene ---- ---- ---- ----mg/kg1606-20-2

<1.02.4-Dinitrotoluene ---- ---- ---- ----mg/kg1121-14-2

<0.61-Naphthylamine ---- ---- ---- ----mg/kg0.5134-32-7

<0.64-Nitroquinoline-N-oxide ---- ---- ---- ----mg/kg0.556-57-5

<0.65-Nitro-o-toluidine ---- ---- ---- ----mg/kg0.599-55-8

<1Azobenzene ---- ---- ---- ----mg/kg1103-33-3

<0.61.3.5-Trinitrobenzene ---- ---- ---- ----mg/kg0.599-35-4

<0.6Phenacetin ---- ---- ---- ----mg/kg0.562-44-2

<0.64-Aminobiphenyl ---- ---- ---- ----mg/kg0.592-67-1

<0.6Pentachloronitrobenzene ---- ---- ---- ----mg/kg0.582-68-8

<0.6Pronamide ---- ---- ---- ----mg/kg0.523950-58-5

<0.6Dimethylaminoazobenzene ---- ---- ---- ----mg/kg0.560-11-7

<0.6Chlorobenzilate ---- ---- ---- ----mg/kg0.5510-15-6

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP075F: Haloethers

<0.6Bis(2-chloroethyl) ether ---- ---- ---- ----mg/kg0.5111-44-4

<0.6Bis(2-chloroethoxy) methane ---- ---- ---- ----mg/kg0.5111-91-1

<0.64-Chlorophenyl phenyl ether ---- ---- ---- ----mg/kg0.57005-72-3

<0.64-Bromophenyl phenyl ether ---- ---- ---- ----mg/kg0.5101-55-3

EP075G: Chlorinated Hydrocarbons

<0.61.3-Dichlorobenzene ---- ---- ---- ----mg/kg0.5541-73-1

<0.61.4-Dichlorobenzene ---- ---- ---- ----mg/kg0.5106-46-7

<0.61.2-Dichlorobenzene ---- ---- ---- ----mg/kg0.595-50-1

<0.6Hexachloroethane ---- ---- ---- ----mg/kg0.567-72-1

<0.61.2.4-Trichlorobenzene ---- ---- ---- ----mg/kg0.5120-82-1

<0.6Hexachloropropylene ---- ---- ---- ----mg/kg0.51888-71-7

<0.6Hexachlorobutadiene ---- ---- ---- ----mg/kg0.587-68-3

<2.5Hexachlorocyclopentadiene ---- ---- ---- ----mg/kg2.577-47-4

<0.6Pentachlorobenzene ---- ---- ---- ----mg/kg0.5608-93-5

<1.0Hexachlorobenzene (HCB) ---- ---- ---- ----mg/kg1118-74-1

EP075H: Anilines and Benzidines

<0.6Aniline ---- ---- ---- ----mg/kg0.562-53-3

<0.64-Chloroaniline ---- ---- ---- ----mg/kg0.5106-47-8

<1.02-Nitroaniline ---- ---- ---- ----mg/kg188-74-4

<1.03-Nitroaniline ---- ---- ---- ----mg/kg199-09-2

<0.6Dibenzofuran ---- ---- ---- ----mg/kg0.5132-64-9

<0.64-Nitroaniline ---- ---- ---- ----mg/kg0.5100-01-6

<0.6Carbazole ---- ---- ---- ----mg/kg0.586-74-8

<0.63.3`-Dichlorobenzidine ---- ---- ---- ----mg/kg0.591-94-1

EP075I: Organochlorine Pesticides

<0.6alpha-BHC ---- ---- ---- ----mg/kg0.5319-84-6

<0.6beta-BHC ---- ---- ---- ----mg/kg0.5319-85-7

<0.6gamma-BHC ---- ---- ---- ----mg/kg0.558-89-9

<0.6delta-BHC ---- ---- ---- ----mg/kg0.5319-86-8

<0.6Heptachlor ---- ---- ---- ----mg/kg0.576-44-8

<0.6Aldrin ---- ---- ---- ----mg/kg0.5309-00-2

<0.6Heptachlor epoxide ---- ---- ---- ----mg/kg0.51024-57-3

<0.6alpha-Endosulfan ---- ---- ---- ----mg/kg0.5959-98-8

<0.64.4`-DDE ---- ---- ---- ----mg/kg0.572-55-9

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP075I: Organochlorine Pesticides - Continued

<0.6Dieldrin ---- ---- ---- ----mg/kg0.560-57-1

<0.6Endrin ---- ---- ---- ----mg/kg0.572-20-8

<0.6beta-Endosulfan ---- ---- ---- ----mg/kg0.533213-65-9

<0.64.4`-DDD ---- ---- ---- ----mg/kg0.572-54-8

<0.6Endosulfan sulfate ---- ---- ---- ----mg/kg0.51031-07-8

<1.04.4`-DDT ---- ---- ---- ----mg/kg150-29-3

EP075J: Organophosphorus Pesticides

<0.6Dichlorvos ---- ---- ---- ----mg/kg0.562-73-7

<0.6Dimethoate ---- ---- ---- ----mg/kg0.560-51-5

<0.6Diazinon ---- ---- ---- ----mg/kg0.5333-41-5

<0.6Chlorpyrifos-methyl ---- ---- ---- ----mg/kg0.55598-13-0

<0.6Malathion ---- ---- ---- ----mg/kg0.5121-75-5

<0.6Fenthion ---- ---- ---- ----mg/kg0.555-38-9

<0.6Chlorpyrifos ---- ---- ---- ----mg/kg0.52921-88-2

<0.6Pirimphos-ethyl ---- ---- ---- ----mg/kg0.523505-41-1

<0.6Chlorfenvinphos ---- ---- ---- ----mg/kg0.5470-90-6

<0.6Prothiofos ---- ---- ---- ----mg/kg0.534643-46-4

<0.6Ethion ---- ---- ---- ----mg/kg0.5563-12-2

EP080/071: Total Petroleum Hydrocarbons

<10 ---- ---- ---- ----mg/kg10----C6 - C9 Fraction

<50 ---- ---- ---- ----mg/kg50----C10 - C14 Fraction

<100 ---- ---- ---- ----mg/kg100----C15 - C28 Fraction

<100 ---- ---- ---- ----mg/kg100----C29 - C36 Fraction

<50^ ---- ---- ---- ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction ---- ---- ---- ----mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

---- ---- ---- ----mg/kg10C6_C10-BTEX

<50 ---- ---- ---- ----mg/kg50---->C10 - C16 Fraction

<100 ---- ---- ---- ----mg/kg100---->C16 - C34 Fraction

<100 ---- ---- ---- ----mg/kg100---->C34 - C40 Fraction

<50^ ---- ---- ---- ----mg/kg50---->C10 - C40 Fraction (sum)

<50^ ---- ---- ---- ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP080: BTEXN

<0.2Benzene ---- ---- ---- ----mg/kg0.271-43-2

<0.5Toluene ---- ---- ---- ----mg/kg0.5108-88-3

<0.5Ethylbenzene ---- ---- ---- ----mg/kg0.5100-41-4

<0.5meta- & para-Xylene ---- ---- ---- ----mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene ---- ---- ---- ----mg/kg0.595-47-6

<0.2^ ---- ---- ---- ----mg/kg0.2----Sum of BTEX

<0.5^ Total Xylenes ---- ---- ---- ----mg/kg0.51330-20-7

<1Naphthalene ---- ---- ---- ----mg/kg191-20-3

EP116: 1.4-Dioxane

<0.05ø1.4-Dioxane ---- ---- ---- ----mg/kg0.05123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

<0.0100Perfluorobutane sulfonic acid

(PFBS)

---- ---- ---- ----mg/kg0.0002375-73-5

0.0135Perfluoropentane sulfonic acid

(PFPeS)

---- ---- ---- ----mg/kg0.00022706-91-4

0.671Perfluorohexane sulfonic acid

(PFHxS)

---- ---- ---- ----mg/kg0.0002355-46-4

0.183Perfluoroheptane sulfonic acid

(PFHpS)

---- ---- ---- ----mg/kg0.0002375-92-8

38.9Perfluorooctane sulfonic acid

(PFOS)

---- ---- ---- ----mg/kg0.00021763-23-1

0.318Perfluorodecane sulfonic acid

(PFDS)

---- ---- ---- ----mg/kg0.0002335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.010Perfluorobutanoic acid (PFBA) ---- ---- ---- ----mg/kg0.001375-22-4

0.0135Perfluoropentanoic acid (PFPeA) ---- ---- ---- ----mg/kg0.00022706-90-3

0.508Perfluorohexanoic acid (PFHxA) ---- ---- ---- ----mg/kg0.0002307-24-4

0.105Perfluoroheptanoic acid (PFHpA) ---- ---- ---- ----mg/kg0.0002375-85-9

0.634Perfluorooctanoic acid (PFOA) ---- ---- ---- ----mg/kg0.0002335-67-1

3.25Perfluorononanoic acid (PFNA) ---- ---- ---- ----mg/kg0.0002375-95-1

22.9Perfluorodecanoic acid (PFDA) ---- ---- ---- ----mg/kg0.0002335-76-2

8.38Perfluoroundecanoic acid

(PFUnDA)

---- ---- ---- ----mg/kg0.00022058-94-8

4.46Perfluorododecanoic acid

(PFDoDA)

---- ---- ---- ----mg/kg0.0002307-55-1

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

0.631Perfluorotridecanoic acid

(PFTrDA)

---- ---- ---- ----mg/kg0.000272629-94-8

0.249Perfluorotetradecanoic acid

(PFTeDA)

---- ---- ---- ----mg/kg0.0005376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.527Perfluorooctane sulfonamide

(FOSA)

---- ---- ---- ----mg/kg0.0002754-91-6

<0.0250N-Methyl perfluorooctane

sulfonamide (MeFOSA)

---- ---- ---- ----mg/kg0.000531506-32-8

<0.0250N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

---- ---- ---- ----mg/kg0.00054151-50-2

<0.0250N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

---- ---- ---- ----mg/kg0.00052448-09-7

<0.0250N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

---- ---- ---- ----mg/kg0.00051691-99-2

<0.0100N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

---- ---- ---- ----mg/kg0.00022355-31-9

<0.0100N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

---- ---- ---- ----mg/kg0.00022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.01004:2 Fluorotelomer sulfonic acid

(4:2 FTS)

---- ---- ---- ----mg/kg0.0005757124-72-4

11.06:2 Fluorotelomer sulfonic acid

(6:2 FTS)

---- ---- ---- ----mg/kg0.000527619-97-2

57.78:2 Fluorotelomer sulfonic acid

(8:2 FTS)

---- ---- ---- ----mg/kg0.000539108-34-4

0.49710:2 Fluorotelomer sulfonic acid

(10:2 FTS)

---- ---- ---- ----mg/kg0.0005120226-60-0

EP231P: PFAS Sums

151 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS

39.6Sum of PFHxS and PFOS ---- ---- ---- ----mg/kg0.0002355-46-4/1763-23-

1

110 ---- ---- ---- ----mg/kg0.0002----Sum of PFAS (WA DER List)

EP068S: Organochlorine Pesticide Surrogate

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Analytical Results

----------------0902_QC108_030717Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

----------------03-Jul-2017 00:00Client sampling date / time

--------------------------------ES1716547-045UnitLORCAS NumberCompound

Result ---- ---- ---- ----

EP068S: Organochlorine Pesticide Surrogate - Continued

104Dibromo-DDE ---- ---- ---- ----%0.0521655-73-2

EP068T: Organophosphorus Pesticide Surrogate

94.2DEF ---- ---- ---- ----%0.0578-48-8

EP074S: VOC Surrogates

74.61.2-Dichloroethane-D4 ---- ---- ---- ----%0.517060-07-0

83.9Toluene-D8 ---- ---- ---- ----%0.52037-26-5

82.04-Bromofluorobenzene ---- ---- ---- ----%0.5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

91.8Phenol-d6 ---- ---- ---- ----%0.513127-88-3

91.62-Chlorophenol-D4 ---- ---- ---- ----%0.593951-73-6

80.02.4.6-Tribromophenol ---- ---- ---- ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

81.62-Fluorobiphenyl ---- ---- ---- ----%0.5321-60-8

85.4Anthracene-d10 ---- ---- ---- ----%0.51719-06-8

86.54-Terphenyl-d14 ---- ---- ---- ----%0.51718-51-0

EP075S: Acid Extractable Surrogates

85.62-Fluorophenol ---- ---- ---- ----%0.5367-12-4

82.9Phenol-d6 ---- ---- ---- ----%0.513127-88-3

80.32-Chlorophenol-D4 ---- ---- ---- ----%0.593951-73-6

90.52.4.6-Tribromophenol ---- ---- ---- ----%0.5118-79-6

EP075T: Base/Neutral Extractable Surrogates

84.9Nitrobenzene-D5 ---- ---- ---- ----%0.54165-60-0

70.71.2-Dichlorobenzene-D4 ---- ---- ---- ----%0.52199-69-1

1022-Fluorobiphenyl ---- ---- ---- ----%0.5321-60-8

89.3Anthracene-d10 ---- ---- ---- ----%0.51719-06-8

89.14-Terphenyl-d14 ---- ---- ---- ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

76.31.2-Dichloroethane-D4 ---- ---- ---- ----%0.217060-07-0

87.1Toluene-D8 ---- ---- ---- ----%0.22037-26-5

85.24-Bromofluorobenzene ---- ---- ---- ----%0.2460-00-4

EP116S: 1.4-Dioxane Surrogate

97.9ø1.4-Dioxane-d8 ---- ---- ---- ----%0.0117647-74-4

EP231S: PFAS Surrogate

121 ---- ---- ---- ----%0.0002----13C4-PFOS

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

184 ---- ---- ---- ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 ---- ---- ---- ----mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 ---- ---- ---- ----mg/L13812-32-6

28Bicarbonate Alkalinity as CaCO3 ---- ---- ---- ----mg/L171-52-3

28 ---- ---- ---- ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

21Sulfate as SO4 - Turbidimetric ---- ---- ---- ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

43Chloride ---- ---- ---- ----mg/L116887-00-6

ED093F: Dissolved Major Cations

9Calcium ---- ---- ---- ----mg/L17440-70-2

6Magnesium ---- ---- ---- ----mg/L17439-95-4

38Sodium ---- ---- ---- ----mg/L17440-23-5

2Potassium ---- ---- ---- ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.04Aluminium ---- ---- ---- ----mg/L0.017429-90-5

<0.001Arsenic ---- ---- ---- ----mg/L0.0017440-38-2

0.0003Cadmium ---- ---- ---- ----mg/L0.00017440-43-9

<0.001Chromium ---- ---- ---- ----mg/L0.0017440-47-3

0.003Copper ---- ---- ---- ----mg/L0.0017440-50-8

<0.001Lead ---- ---- ---- ----mg/L0.0017439-92-1

0.008Manganese ---- ---- ---- ----mg/L0.0017439-96-5

<0.001Nickel ---- ---- ---- ----mg/L0.0017440-02-0

0.046Zinc ---- ---- ---- ----mg/L0.0057440-66-6

<0.05Iron ---- ---- ---- ----mg/L0.057439-89-6

<0.1Bromine ---- ---- ---- ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury ---- ---- ---- ----mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.9Fluoride ---- ---- ---- ----mg/L0.116984-48-8

EN055: Ionic Balance

2.21 ---- ---- ---- ----meq/L0.01----Total Anions

2.65 ---- ---- ---- ----meq/L0.01----Total Cations

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

9.00 ---- ---- ---- ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene ---- ---- ---- ----µg/L5100-42-5

<5Isopropylbenzene ---- ---- ---- ----µg/L598-82-8

<5n-Propylbenzene ---- ---- ---- ----µg/L5103-65-1

<51.3.5-Trimethylbenzene ---- ---- ---- ----µg/L5108-67-8

<5sec-Butylbenzene ---- ---- ---- ----µg/L5135-98-8

<51.2.4-Trimethylbenzene ---- ---- ---- ----µg/L595-63-6

<5tert-Butylbenzene ---- ---- ---- ----µg/L598-06-6

<5p-Isopropyltoluene ---- ---- ---- ----µg/L599-87-6

<5n-Butylbenzene ---- ---- ---- ----µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate ---- ---- ---- ----µg/L50108-05-4

<502-Butanone (MEK) ---- ---- ---- ----µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) ---- ---- ---- ----µg/L50108-10-1

<502-Hexanone (MBK) ---- ---- ---- ----µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide ---- ---- ---- ----µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane ---- ---- ---- ----µg/L5594-20-7

<51.2-Dichloropropane ---- ---- ---- ----µg/L578-87-5

<5cis-1.3-Dichloropropylene ---- ---- ---- ----µg/L510061-01-5

<5trans-1.3-Dichloropropylene ---- ---- ---- ----µg/L510061-02-6

<51.2-Dibromoethane (EDB) ---- ---- ---- ----µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane ---- ---- ---- ----µg/L5075-71-8

<50Chloromethane ---- ---- ---- ----µg/L5074-87-3

<50Vinyl chloride ---- ---- ---- ----µg/L5075-01-4

<50Bromomethane ---- ---- ---- ----µg/L5074-83-9

<50Chloroethane ---- ---- ---- ----µg/L5075-00-3

<50Trichlorofluoromethane ---- ---- ---- ----µg/L5075-69-4

<51.1-Dichloroethene ---- ---- ---- ----µg/L575-35-4

<5Iodomethane ---- ---- ---- ----µg/L574-88-4

<5trans-1.2-Dichloroethene ---- ---- ---- ----µg/L5156-60-5

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1-Dichloroethane ---- ---- ---- ----µg/L575-34-3

<5cis-1.2-Dichloroethene ---- ---- ---- ----µg/L5156-59-2

<51.1.1-Trichloroethane ---- ---- ---- ----µg/L571-55-6

<51.1-Dichloropropylene ---- ---- ---- ----µg/L5563-58-6

<5Carbon Tetrachloride ---- ---- ---- ----µg/L556-23-5

<51.2-Dichloroethane ---- ---- ---- ----µg/L5107-06-2

<5Trichloroethene ---- ---- ---- ----µg/L579-01-6

<5Dibromomethane ---- ---- ---- ----µg/L574-95-3

<51.1.2-Trichloroethane ---- ---- ---- ----µg/L579-00-5

<51.3-Dichloropropane ---- ---- ---- ----µg/L5142-28-9

<5Tetrachloroethene ---- ---- ---- ----µg/L5127-18-4

<51.1.1.2-Tetrachloroethane ---- ---- ---- ----µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene ---- ---- ---- ----µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene ---- ---- ---- ----µg/L51476-11-5

<51.1.2.2-Tetrachloroethane ---- ---- ---- ----µg/L579-34-5

<51.2.3-Trichloropropane ---- ---- ---- ----µg/L596-18-4

<5Pentachloroethane ---- ---- ---- ----µg/L576-01-7

<51.2-Dibromo-3-chloropropane ---- ---- ---- ----µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene ---- ---- ---- ----µg/L5108-90-7

<5Bromobenzene ---- ---- ---- ----µg/L5108-86-1

<52-Chlorotoluene ---- ---- ---- ----µg/L595-49-8

<54-Chlorotoluene ---- ---- ---- ----µg/L5106-43-4

<51.2.3-Trichlorobenzene ---- ---- ---- ----µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform ---- ---- ---- ----µg/L567-66-3

<5Bromodichloromethane ---- ---- ---- ----µg/L575-27-4

<5Dibromochloromethane ---- ---- ---- ----µg/L5124-48-1

<5Bromoform ---- ---- ---- ----µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene ---- ---- ---- ----µg/L191-20-3

<1.0Acenaphthylene ---- ---- ---- ----µg/L1208-96-8

<1.0Acenaphthene ---- ---- ---- ----µg/L183-32-9

<1.0Fluorene ---- ---- ---- ----µg/L186-73-7

Page 75: Appendix - Department of Defence

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Phenanthrene ---- ---- ---- ----µg/L185-01-8

<1.0Anthracene ---- ---- ---- ----µg/L1120-12-7

<1.0Fluoranthene ---- ---- ---- ----µg/L1206-44-0

<1.0Pyrene ---- ---- ---- ----µg/L1129-00-0

<1.0Benz(a)anthracene ---- ---- ---- ----µg/L156-55-3

<1.0Chrysene ---- ---- ---- ----µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene ---- ---- ---- ----µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene ---- ---- ---- ----µg/L1207-08-9

<0.5Benzo(a)pyrene ---- ---- ---- ----µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene ---- ---- ---- ----µg/L1193-39-5

<1.0Dibenz(a.h)anthracene ---- ---- ---- ----µg/L153-70-3

<1.0Benzo(g.h.i)perylene ---- ---- ---- ----µg/L1191-24-2

<0.5^ ---- ---- ---- ----µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ ---- ---- ---- ----µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol ---- ---- ---- ----µg/L2108-95-2

<22-Chlorophenol ---- ---- ---- ----µg/L295-57-8

<22-Methylphenol ---- ---- ---- ----µg/L295-48-7

<43- & 4-Methylphenol ---- ---- ---- ----µg/L41319-77-3

<22-Nitrophenol ---- ---- ---- ----µg/L288-75-5

<22.4-Dimethylphenol ---- ---- ---- ----µg/L2105-67-9

<22.4-Dichlorophenol ---- ---- ---- ----µg/L2120-83-2

<22.6-Dichlorophenol ---- ---- ---- ----µg/L287-65-0

<24-Chloro-3-methylphenol ---- ---- ---- ----µg/L259-50-7

<22.4.6-Trichlorophenol ---- ---- ---- ----µg/L288-06-2

<22.4.5-Trichlorophenol ---- ---- ---- ----µg/L295-95-4

<4Pentachlorophenol ---- ---- ---- ----µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene ---- ---- ---- ----µg/L291-57-6

<22-Chloronaphthalene ---- ---- ---- ----µg/L291-58-7

<2N-2-Fluorenyl Acetamide ---- ---- ---- ----µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene ---- ---- ---- ----µg/L257-97-6

<23-Methylcholanthrene ---- ---- ---- ----µg/L256-49-5

EP075C: Phthalate Esters

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<2Dimethyl phthalate ---- ---- ---- ----µg/L2131-11-3

<2Diethyl phthalate ---- ---- ---- ----µg/L284-66-2

<2Di-n-butyl phthalate ---- ---- ---- ----µg/L284-74-2

<2Butyl benzyl phthalate ---- ---- ---- ----µg/L285-68-7

<10bis(2-ethylhexyl) phthalate ---- ---- ---- ----µg/L10117-81-7

<2Di-n-octylphthalate ---- ---- ---- ----µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine ---- ---- ---- ----µg/L210595-95-6

<2N-Nitrosodiethylamine ---- ---- ---- ----µg/L255-18-5

<4N-Nitrosopyrrolidine ---- ---- ---- ----µg/L4930-55-2

<2N-Nitrosomorpholine ---- ---- ---- ----µg/L259-89-2

<2N-Nitrosodi-n-propylamine ---- ---- ---- ----µg/L2621-64-7

<2N-Nitrosopiperidine ---- ---- ---- ----µg/L2100-75-4

<2N-Nitrosodibutylamine ---- ---- ---- ----µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

---- ---- ---- ----µg/L486-30-6 122-39-4

<2Methapyrilene ---- ---- ---- ----µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline ---- ---- ---- ----µg/L2109-06-8

<2Acetophenone ---- ---- ---- ----µg/L298-86-2

<2Nitrobenzene ---- ---- ---- ----µg/L298-95-3

<2Isophorone ---- ---- ---- ----µg/L278-59-1

<42.6-Dinitrotoluene ---- ---- ---- ----µg/L4606-20-2

<42.4-Dinitrotoluene ---- ---- ---- ----µg/L4121-14-2

<21-Naphthylamine ---- ---- ---- ----µg/L2134-32-7

<24-Nitroquinoline-N-oxide ---- ---- ---- ----µg/L256-57-5

<25-Nitro-o-toluidine ---- ---- ---- ----µg/L299-55-8

<2Azobenzene ---- ---- ---- ----µg/L2103-33-3

<21.3.5-Trinitrobenzene ---- ---- ---- ----µg/L299-35-4

<2Phenacetin ---- ---- ---- ----µg/L262-44-2

<24-Aminobiphenyl ---- ---- ---- ----µg/L292-67-1

<2Pentachloronitrobenzene ---- ---- ---- ----µg/L282-68-8

<2Pronamide ---- ---- ---- ----µg/L223950-58-5

<2Dimethylaminoazobenzene ---- ---- ---- ----µg/L260-11-7

<2Chlorobenzilate ---- ---- ---- ----µg/L2510-15-6

Page 77: Appendix - Department of Defence

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

<2Bis(2-chloroethyl) ether ---- ---- ---- ----µg/L2111-44-4

<2Bis(2-chloroethoxy) methane ---- ---- ---- ----µg/L2111-91-1

<24-Chlorophenyl phenyl ether ---- ---- ---- ----µg/L27005-72-3

<24-Bromophenyl phenyl ether ---- ---- ---- ----µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene ---- ---- ---- ----µg/L2541-73-1

<21.4-Dichlorobenzene ---- ---- ---- ----µg/L2106-46-7

<21.2-Dichlorobenzene ---- ---- ---- ----µg/L295-50-1

<2Hexachloroethane ---- ---- ---- ----µg/L267-72-1

<21.2.4-Trichlorobenzene ---- ---- ---- ----µg/L2120-82-1

<2Hexachloropropylene ---- ---- ---- ----µg/L21888-71-7

<2Hexachlorobutadiene ---- ---- ---- ----µg/L287-68-3

<10Hexachlorocyclopentadiene ---- ---- ---- ----µg/L1077-47-4

<2Pentachlorobenzene ---- ---- ---- ----µg/L2608-93-5

<4Hexachlorobenzene (HCB) ---- ---- ---- ----µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline ---- ---- ---- ----µg/L262-53-3

<24-Chloroaniline ---- ---- ---- ----µg/L2106-47-8

<42-Nitroaniline ---- ---- ---- ----µg/L488-74-4

<43-Nitroaniline ---- ---- ---- ----µg/L499-09-2

<2Dibenzofuran ---- ---- ---- ----µg/L2132-64-9

<24-Nitroaniline ---- ---- ---- ----µg/L2100-01-6

<2Carbazole ---- ---- ---- ----µg/L286-74-8

<23.3`-Dichlorobenzidine ---- ---- ---- ----µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC ---- ---- ---- ----µg/L2319-84-6

<2beta-BHC ---- ---- ---- ----µg/L2319-85-7

<2gamma-BHC ---- ---- ---- ----µg/L258-89-9

<2delta-BHC ---- ---- ---- ----µg/L2319-86-8

<2Heptachlor ---- ---- ---- ----µg/L276-44-8

<2Aldrin ---- ---- ---- ----µg/L2309-00-2

<2Heptachlor epoxide ---- ---- ---- ----µg/L21024-57-3

<2alpha-Endosulfan ---- ---- ---- ----µg/L2959-98-8

Page 78: Appendix - Department of Defence

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<24.4`-DDE ---- ---- ---- ----µg/L272-55-9

<2Dieldrin ---- ---- ---- ----µg/L260-57-1

<2Endrin ---- ---- ---- ----µg/L272-20-8

<2beta-Endosulfan ---- ---- ---- ----µg/L233213-65-9

<24.4`-DDD ---- ---- ---- ----µg/L272-54-8

<2Endosulfan sulfate ---- ---- ---- ----µg/L21031-07-8

<44.4`-DDT ---- ---- ---- ----µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin ---- ---- ---- ----µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT ---- ---- ---- ----µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos ---- ---- ---- ----µg/L262-73-7

<2Dimethoate ---- ---- ---- ----µg/L260-51-5

<2Diazinon ---- ---- ---- ----µg/L2333-41-5

<2Chlorpyrifos-methyl ---- ---- ---- ----µg/L25598-13-0

<2Malathion ---- ---- ---- ----µg/L2121-75-5

<2Fenthion ---- ---- ---- ----µg/L255-38-9

<2Chlorpyrifos ---- ---- ---- ----µg/L22921-88-2

<2Pirimphos-ethyl ---- ---- ---- ----µg/L223505-41-1

<2Chlorfenvinphos ---- ---- ---- ----µg/L2470-90-6

<2Prothiofos ---- ---- ---- ----µg/L234643-46-4

<2Ethion ---- ---- ---- ----µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 ---- ---- ---- ----µg/L20----C6 - C9 Fraction

23100 ---- ---- ---- ----µg/L50----C10 - C14 Fraction

220 ---- ---- ---- ----µg/L100----C15 - C28 Fraction

<50 ---- ---- ---- ----µg/L50----C29 - C36 Fraction

23300^ ---- ---- ---- ----µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction ---- ---- ---- ----µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

---- ---- ---- ----µg/L20C6_C10-BTEX

23300 ---- ---- ---- ----µg/L100---->C10 - C16 Fraction

150 ---- ---- ---- ----µg/L100---->C16 - C34 Fraction

<100 ---- ---- ---- ----µg/L100---->C34 - C40 Fraction

Page 79: Appendix - Department of Defence

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

23400^ ---- ---- ---- ----µg/L100---->C10 - C40 Fraction (sum)

23300^ ---- ---- ---- ----µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene ---- ---- ---- ----µg/L171-43-2

<2Toluene ---- ---- ---- ----µg/L2108-88-3

<2Ethylbenzene ---- ---- ---- ----µg/L2100-41-4

<2meta- & para-Xylene ---- ---- ---- ----µg/L2108-38-3 106-42-3

<2ortho-Xylene ---- ---- ---- ----µg/L295-47-6

<2^ Total Xylenes ---- ---- ---- ----µg/L21330-20-7

<1^ ---- ---- ---- ----µg/L1----Sum of BTEX

<5Naphthalene ---- ---- ---- ----µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane ---- ---- ---- ----µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.52Perfluorobutane sulfonic acid

(PFBS)

4.08 3.95 0.02 <0.02µg/L0.02375-73-5

0.43Perfluoropentane sulfonic acid

(PFPeS)

3.62 3.44 <0.02 <0.02µg/L0.022706-91-4

0.78Perfluorohexane sulfonic acid

(PFHxS)

30.4 23.4 0.14 0.04µg/L0.02355-46-4

0.18Perfluoroheptane sulfonic acid

(PFHpS)

2.55 1.70 <0.02 <0.02µg/L0.02375-92-8

10.3Perfluorooctane sulfonic acid

(PFOS)

53.5 52.7 0.12 0.08µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

4.8Perfluorobutanoic acid (PFBA) 3.0 2.4 <0.1 <0.1µg/L0.1375-22-4

7.62Perfluoropentanoic acid (PFPeA) 3.70 2.63 <0.02 <0.02µg/L0.022706-90-3

50.6Perfluorohexanoic acid (PFHxA) 24.7 15.1 0.04 <0.02µg/L0.02307-24-4

3.93Perfluoroheptanoic acid (PFHpA) 2.54 2.27 <0.02 <0.02µg/L0.02375-85-9

9.02Perfluorooctanoic acid (PFOA) 5.28 3.34 0.01 <0.01µg/L0.01335-67-1

9.00Perfluorononanoic acid (PFNA) 3.56 0.98 <0.02 <0.02µg/L0.02375-95-1

9.37Perfluorodecanoic acid (PFDA) 1.84 0.57 <0.02 <0.02µg/L0.02335-76-2

Page 80: Appendix - Department of Defence

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

1.19Perfluoroundecanoic acid

(PFUnDA)

0.16 0.04 <0.02 <0.02µg/L0.022058-94-8

1.22Perfluorododecanoic acid

(PFDoDA)

0.09 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.07Perfluorooctane sulfonamide

(FOSA)

0.05 0.05 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

0.134:2 Fluorotelomer sulfonic acid

(4:2 FTS)

0.06 <0.05 <0.05 <0.05µg/L0.05757124-72-4

7126:2 Fluorotelomer sulfonic acid

(6:2 FTS)

123 43.4 <0.05 <0.05µg/L0.0527619-97-2

25.68:2 Fluorotelomer sulfonic acid

(8:2 FTS)

4.85 1.08 <0.05 <0.05µg/L0.0539108-34-4

0.2010:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

847 267 157 0.33 0.12µg/L0.01----Sum of PFAS

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Analytical Results

0902_SW005_0407170902_SW004_0407170902_SW003_0407170902_SW002_0407170902_SW001_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-005ES1716547-004ES1716547-003ES1716547-002ES1716547-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

11.1Sum of PFHxS and PFOS 83.9 76.1 0.26 0.12µg/L0.01355-46-4/1763-23-

1

825 255 150 0.33 0.12µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

95.91.2-Dichloroethane-D4 ---- ---- ---- ----%517060-07-0

109Toluene-D8 ---- ---- ---- ----%52037-26-5

1024-Bromofluorobenzene ---- ---- ---- ----%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

22.8Phenol-d6 ---- ---- ---- ----%113127-88-3

46.62-Chlorophenol-D4 ---- ---- ---- ----%193951-73-6

47.22.4.6-Tribromophenol ---- ---- ---- ----%1118-79-6

EP075(SIM)T: PAH Surrogates

56.22-Fluorobiphenyl ---- ---- ---- ----%1321-60-8

69.1Anthracene-d10 ---- ---- ---- ----%11719-06-8

49.64-Terphenyl-d14 ---- ---- ---- ----%11718-51-0

EP075S: Acid Extractable Surrogates

25.32-Fluorophenol ---- ---- ---- ----%2367-12-4

20.5Phenol-d6 ---- ---- ---- ----%213127-88-3

39.22-Chlorophenol-D4 ---- ---- ---- ----%293951-73-6

54.32.4.6-Tribromophenol ---- ---- ---- ----%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

49.0Nitrobenzene-D5 ---- ---- ---- ----%24165-60-0

39.21.2-Dichlorobenzene-D4 ---- ---- ---- ----%22199-69-1

23.32-Fluorobiphenyl ---- ---- ---- ----%2321-60-8

54.2Anthracene-d10 ---- ---- ---- ----%21719-06-8

55.94-Terphenyl-d14 ---- ---- ---- ----%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1031.2-Dichloroethane-D4 ---- ---- ---- ----%217060-07-0

112Toluene-D8 ---- ---- ---- ----%22037-26-5

1064-Bromofluorobenzene ---- ---- ---- ----%2460-00-4

EP116S: 1.4-Dioxane Surrogate

96.21.4-Dioxane-d8 ---- ---- ---- ----%0.517647-74-4

EP231S: PFAS Surrogate

84.6 96.3 91.4 92.6 92.1%0.02----13C4-PFOS

Page 82: Appendix - Department of Defence

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

---- ---- ---- 586 ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

----Hydroxide Alkalinity as CaCO3 ---- ---- <1 ----mg/L1DMO-210-001

----Carbonate Alkalinity as CaCO3 ---- ---- <1 ----mg/L13812-32-6

----Bicarbonate Alkalinity as CaCO3 ---- ---- 62 ----mg/L171-52-3

---- ---- ---- 62 ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

----Sulfate as SO4 - Turbidimetric ---- ---- 40 ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

----Chloride ---- ---- 306 ----mg/L116887-00-6

ED093F: Dissolved Major Cations

----Calcium ---- ---- 19 ----mg/L17440-70-2

----Magnesium ---- ---- 28 ----mg/L17439-95-4

----Sodium ---- ---- 150 ----mg/L17440-23-5

----Potassium ---- ---- 9 ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

----Aluminium ---- ---- 0.10 ----mg/L0.017429-90-5

----Arsenic ---- ---- <0.001 ----mg/L0.0017440-38-2

----Cadmium ---- ---- <0.0001 ----mg/L0.00017440-43-9

----Chromium ---- ---- <0.001 ----mg/L0.0017440-47-3

----Copper ---- ---- <0.001 ----mg/L0.0017440-50-8

----Lead ---- ---- <0.001 ----mg/L0.0017439-92-1

----Manganese ---- ---- 0.309 ----mg/L0.0017439-96-5

----Nickel ---- ---- 0.002 ----mg/L0.0017440-02-0

----Zinc ---- ---- <0.005 ----mg/L0.0057440-66-6

----Iron ---- ---- 0.31 ----mg/L0.057439-89-6

----Bromine ---- ---- 0.6 ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

----Mercury ---- ---- <0.0001 ----mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

----Fluoride ---- ---- 0.4 ----mg/L0.116984-48-8

EN055: Ionic Balance

---- ---- ---- 10.7 ----meq/L0.01----Total Anions

---- ---- ---- 10.0 ----meq/L0.01----Total Cations

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

---- ---- ---- 3.36 ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

----Styrene ---- ---- <5 ----µg/L5100-42-5

----Isopropylbenzene ---- ---- <5 ----µg/L598-82-8

----n-Propylbenzene ---- ---- <5 ----µg/L5103-65-1

----1.3.5-Trimethylbenzene ---- ---- <5 ----µg/L5108-67-8

----sec-Butylbenzene ---- ---- <5 ----µg/L5135-98-8

----1.2.4-Trimethylbenzene ---- ---- <5 ----µg/L595-63-6

----tert-Butylbenzene ---- ---- <5 ----µg/L598-06-6

----p-Isopropyltoluene ---- ---- <5 ----µg/L599-87-6

----n-Butylbenzene ---- ---- <5 ----µg/L5104-51-8

EP074B: Oxygenated Compounds

----Vinyl Acetate ---- ---- <50 ----µg/L50108-05-4

----2-Butanone (MEK) ---- ---- <50 ----µg/L5078-93-3

----4-Methyl-2-pentanone (MIBK) ---- ---- <50 ----µg/L50108-10-1

----2-Hexanone (MBK) ---- ---- <50 ----µg/L50591-78-6

EP074C: Sulfonated Compounds

----Carbon disulfide ---- ---- <5 ----µg/L575-15-0

EP074D: Fumigants

----2.2-Dichloropropane ---- ---- <5 ----µg/L5594-20-7

----1.2-Dichloropropane ---- ---- <5 ----µg/L578-87-5

----cis-1.3-Dichloropropylene ---- ---- <5 ----µg/L510061-01-5

----trans-1.3-Dichloropropylene ---- ---- <5 ----µg/L510061-02-6

----1.2-Dibromoethane (EDB) ---- ---- <5 ----µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

----Dichlorodifluoromethane ---- ---- <50 ----µg/L5075-71-8

----Chloromethane ---- ---- <50 ----µg/L5074-87-3

----Vinyl chloride ---- ---- <50 ----µg/L5075-01-4

----Bromomethane ---- ---- <50 ----µg/L5074-83-9

----Chloroethane ---- ---- <50 ----µg/L5075-00-3

----Trichlorofluoromethane ---- ---- <50 ----µg/L5075-69-4

----1.1-Dichloroethene ---- ---- <5 ----µg/L575-35-4

----Iodomethane ---- ---- <5 ----µg/L574-88-4

----trans-1.2-Dichloroethene ---- ---- <5 ----µg/L5156-60-5

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

----1.1-Dichloroethane ---- ---- <5 ----µg/L575-34-3

----cis-1.2-Dichloroethene ---- ---- <5 ----µg/L5156-59-2

----1.1.1-Trichloroethane ---- ---- <5 ----µg/L571-55-6

----1.1-Dichloropropylene ---- ---- <5 ----µg/L5563-58-6

----Carbon Tetrachloride ---- ---- <5 ----µg/L556-23-5

----1.2-Dichloroethane ---- ---- <5 ----µg/L5107-06-2

----Trichloroethene ---- ---- <5 ----µg/L579-01-6

----Dibromomethane ---- ---- <5 ----µg/L574-95-3

----1.1.2-Trichloroethane ---- ---- <5 ----µg/L579-00-5

----1.3-Dichloropropane ---- ---- <5 ----µg/L5142-28-9

----Tetrachloroethene ---- ---- <5 ----µg/L5127-18-4

----1.1.1.2-Tetrachloroethane ---- ---- <5 ----µg/L5630-20-6

----trans-1.4-Dichloro-2-butene ---- ---- <5 ----µg/L5110-57-6

----cis-1.4-Dichloro-2-butene ---- ---- <5 ----µg/L51476-11-5

----1.1.2.2-Tetrachloroethane ---- ---- <5 ----µg/L579-34-5

----1.2.3-Trichloropropane ---- ---- <5 ----µg/L596-18-4

----Pentachloroethane ---- ---- <5 ----µg/L576-01-7

----1.2-Dibromo-3-chloropropane ---- ---- <5 ----µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

----Chlorobenzene ---- ---- <5 ----µg/L5108-90-7

----Bromobenzene ---- ---- <5 ----µg/L5108-86-1

----2-Chlorotoluene ---- ---- <5 ----µg/L595-49-8

----4-Chlorotoluene ---- ---- <5 ----µg/L5106-43-4

----1.2.3-Trichlorobenzene ---- ---- <5 ----µg/L587-61-6

EP074G: Trihalomethanes

----Chloroform ---- ---- <5 ----µg/L567-66-3

----Bromodichloromethane ---- ---- <5 ----µg/L575-27-4

----Dibromochloromethane ---- ---- <5 ----µg/L5124-48-1

----Bromoform ---- ---- <5 ----µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

----Naphthalene ---- ---- <1.0 ----µg/L191-20-3

----Acenaphthylene ---- ---- <1.0 ----µg/L1208-96-8

----Acenaphthene ---- ---- <1.0 ----µg/L183-32-9

----Fluorene ---- ---- <1.0 ----µg/L186-73-7

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

----Phenanthrene ---- ---- <1.0 ----µg/L185-01-8

----Anthracene ---- ---- <1.0 ----µg/L1120-12-7

----Fluoranthene ---- ---- <1.0 ----µg/L1206-44-0

----Pyrene ---- ---- <1.0 ----µg/L1129-00-0

----Benz(a)anthracene ---- ---- <1.0 ----µg/L156-55-3

----Chrysene ---- ---- <1.0 ----µg/L1218-01-9

----Benzo(b+j)fluoranthene ---- ---- <1.0 ----µg/L1205-99-2 205-82-3

----Benzo(k)fluoranthene ---- ---- <1.0 ----µg/L1207-08-9

----Benzo(a)pyrene ---- ---- <0.5 ----µg/L0.550-32-8

----Indeno(1.2.3.cd)pyrene ---- ---- <1.0 ----µg/L1193-39-5

----Dibenz(a.h)anthracene ---- ---- <1.0 ----µg/L153-70-3

----Benzo(g.h.i)perylene ---- ---- <1.0 ----µg/L1191-24-2

----^ ---- ---- <0.5 ----µg/L0.5----Sum of polycyclic aromatic hydrocarbons

----^ ---- ---- <0.5 ----µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

----Phenol ---- ---- <2 ----µg/L2108-95-2

----2-Chlorophenol ---- ---- <2 ----µg/L295-57-8

----2-Methylphenol ---- ---- <2 ----µg/L295-48-7

----3- & 4-Methylphenol ---- ---- <4 ----µg/L41319-77-3

----2-Nitrophenol ---- ---- <2 ----µg/L288-75-5

----2.4-Dimethylphenol ---- ---- <2 ----µg/L2105-67-9

----2.4-Dichlorophenol ---- ---- <2 ----µg/L2120-83-2

----2.6-Dichlorophenol ---- ---- <2 ----µg/L287-65-0

----4-Chloro-3-methylphenol ---- ---- <2 ----µg/L259-50-7

----2.4.6-Trichlorophenol ---- ---- <2 ----µg/L288-06-2

----2.4.5-Trichlorophenol ---- ---- <2 ----µg/L295-95-4

----Pentachlorophenol ---- ---- <4 ----µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

----2-Methylnaphthalene ---- ---- <2 ----µg/L291-57-6

----2-Chloronaphthalene ---- ---- <2 ----µg/L291-58-7

----N-2-Fluorenyl Acetamide ---- ---- <2 ----µg/L253-96-3

----7.12-Dimethylbenz(a)anthracene ---- ---- <2 ----µg/L257-97-6

----3-Methylcholanthrene ---- ---- <2 ----µg/L256-49-5

EP075C: Phthalate Esters

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

----Dimethyl phthalate ---- ---- <2 ----µg/L2131-11-3

----Diethyl phthalate ---- ---- <2 ----µg/L284-66-2

----Di-n-butyl phthalate ---- ---- <2 ----µg/L284-74-2

----Butyl benzyl phthalate ---- ---- <2 ----µg/L285-68-7

----bis(2-ethylhexyl) phthalate ---- ---- <10 ----µg/L10117-81-7

----Di-n-octylphthalate ---- ---- <2 ----µg/L2117-84-0

EP075D: Nitrosamines

----N-Nitrosomethylethylamine ---- ---- <2 ----µg/L210595-95-6

----N-Nitrosodiethylamine ---- ---- <2 ----µg/L255-18-5

----N-Nitrosopyrrolidine ---- ---- <4 ----µg/L4930-55-2

----N-Nitrosomorpholine ---- ---- <2 ----µg/L259-89-2

----N-Nitrosodi-n-propylamine ---- ---- <2 ----µg/L2621-64-7

----N-Nitrosopiperidine ---- ---- <2 ----µg/L2100-75-4

----N-Nitrosodibutylamine ---- ---- <2 ----µg/L2924-16-3

----N-Nitrosodiphenyl &

Diphenylamine

---- ---- <4 ----µg/L486-30-6 122-39-4

----Methapyrilene ---- ---- <2 ----µg/L291-80-5

EP075E: Nitroaromatics and Ketones

----2-Picoline ---- ---- <2 ----µg/L2109-06-8

----Acetophenone ---- ---- <2 ----µg/L298-86-2

----Nitrobenzene ---- ---- <2 ----µg/L298-95-3

----Isophorone ---- ---- <2 ----µg/L278-59-1

----2.6-Dinitrotoluene ---- ---- <4 ----µg/L4606-20-2

----2.4-Dinitrotoluene ---- ---- <4 ----µg/L4121-14-2

----1-Naphthylamine ---- ---- <2 ----µg/L2134-32-7

----4-Nitroquinoline-N-oxide ---- ---- <2 ----µg/L256-57-5

----5-Nitro-o-toluidine ---- ---- <2 ----µg/L299-55-8

----Azobenzene ---- ---- <2 ----µg/L2103-33-3

----1.3.5-Trinitrobenzene ---- ---- <2 ----µg/L299-35-4

----Phenacetin ---- ---- <2 ----µg/L262-44-2

----4-Aminobiphenyl ---- ---- <2 ----µg/L292-67-1

----Pentachloronitrobenzene ---- ---- <2 ----µg/L282-68-8

----Pronamide ---- ---- <2 ----µg/L223950-58-5

----Dimethylaminoazobenzene ---- ---- <2 ----µg/L260-11-7

----Chlorobenzilate ---- ---- <2 ----µg/L2510-15-6

Page 87: Appendix - Department of Defence

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

----Bis(2-chloroethyl) ether ---- ---- <2 ----µg/L2111-44-4

----Bis(2-chloroethoxy) methane ---- ---- <2 ----µg/L2111-91-1

----4-Chlorophenyl phenyl ether ---- ---- <2 ----µg/L27005-72-3

----4-Bromophenyl phenyl ether ---- ---- <2 ----µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

----1.3-Dichlorobenzene ---- ---- <2 ----µg/L2541-73-1

----1.4-Dichlorobenzene ---- ---- <2 ----µg/L2106-46-7

----1.2-Dichlorobenzene ---- ---- <2 ----µg/L295-50-1

----Hexachloroethane ---- ---- <2 ----µg/L267-72-1

----1.2.4-Trichlorobenzene ---- ---- <2 ----µg/L2120-82-1

----Hexachloropropylene ---- ---- <2 ----µg/L21888-71-7

----Hexachlorobutadiene ---- ---- <2 ----µg/L287-68-3

----Hexachlorocyclopentadiene ---- ---- <10 ----µg/L1077-47-4

----Pentachlorobenzene ---- ---- <2 ----µg/L2608-93-5

----Hexachlorobenzene (HCB) ---- ---- <4 ----µg/L4118-74-1

EP075H: Anilines and Benzidines

----Aniline ---- ---- <2 ----µg/L262-53-3

----4-Chloroaniline ---- ---- <2 ----µg/L2106-47-8

----2-Nitroaniline ---- ---- <4 ----µg/L488-74-4

----3-Nitroaniline ---- ---- <4 ----µg/L499-09-2

----Dibenzofuran ---- ---- <2 ----µg/L2132-64-9

----4-Nitroaniline ---- ---- <2 ----µg/L2100-01-6

----Carbazole ---- ---- <2 ----µg/L286-74-8

----3.3`-Dichlorobenzidine ---- ---- <2 ----µg/L291-94-1

EP075I: Organochlorine Pesticides

----alpha-BHC ---- ---- <2 ----µg/L2319-84-6

----beta-BHC ---- ---- <2 ----µg/L2319-85-7

----gamma-BHC ---- ---- <2 ----µg/L258-89-9

----delta-BHC ---- ---- <2 ----µg/L2319-86-8

----Heptachlor ---- ---- <2 ----µg/L276-44-8

----Aldrin ---- ---- <2 ----µg/L2309-00-2

----Heptachlor epoxide ---- ---- <2 ----µg/L21024-57-3

----alpha-Endosulfan ---- ---- <2 ----µg/L2959-98-8

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

----4.4`-DDE ---- ---- <2 ----µg/L272-55-9

----Dieldrin ---- ---- <2 ----µg/L260-57-1

----Endrin ---- ---- <2 ----µg/L272-20-8

----beta-Endosulfan ---- ---- <2 ----µg/L233213-65-9

----4.4`-DDD ---- ---- <2 ----µg/L272-54-8

----Endosulfan sulfate ---- ---- <2 ----µg/L21031-07-8

----4.4`-DDT ---- ---- <4 ----µg/L450-29-3

----^ Sum of Aldrin + Dieldrin ---- ---- <4 ----µg/L4309-00-2/60-57-1

----^ Sum of DDD + DDE + DDT ---- ---- <4 ----µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

----Dichlorvos ---- ---- <2 ----µg/L262-73-7

----Dimethoate ---- ---- <2 ----µg/L260-51-5

----Diazinon ---- ---- <2 ----µg/L2333-41-5

----Chlorpyrifos-methyl ---- ---- <2 ----µg/L25598-13-0

----Malathion ---- ---- <2 ----µg/L2121-75-5

----Fenthion ---- ---- <2 ----µg/L255-38-9

----Chlorpyrifos ---- ---- <2 ----µg/L22921-88-2

----Pirimphos-ethyl ---- ---- <2 ----µg/L223505-41-1

----Chlorfenvinphos ---- ---- <2 ----µg/L2470-90-6

----Prothiofos ---- ---- <2 ----µg/L234643-46-4

----Ethion ---- ---- <2 ----µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

---- ---- ---- <20 ----µg/L20----C6 - C9 Fraction

---- ---- ---- <50 ----µg/L50----C10 - C14 Fraction

---- ---- ---- <100 ----µg/L100----C15 - C28 Fraction

---- ---- ---- <50 ----µg/L50----C29 - C36 Fraction

----^ ---- ---- <50 ----µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

----C6 - C10 Fraction ---- ---- <20 ----µg/L20C6_C10

----^ C6 - C10 Fraction minus BTEX

(F1)

---- ---- <20 ----µg/L20C6_C10-BTEX

---- ---- ---- <100 ----µg/L100---->C10 - C16 Fraction

---- ---- ---- <100 ----µg/L100---->C16 - C34 Fraction

---- ---- ---- <100 ----µg/L100---->C34 - C40 Fraction

Page 89: Appendix - Department of Defence

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

----^ ---- ---- <100 ----µg/L100---->C10 - C40 Fraction (sum)

----^ ---- ---- <100 ----µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

----Benzene ---- ---- <1 ----µg/L171-43-2

----Toluene ---- ---- <2 ----µg/L2108-88-3

----Ethylbenzene ---- ---- <2 ----µg/L2100-41-4

----meta- & para-Xylene ---- ---- <2 ----µg/L2108-38-3 106-42-3

----ortho-Xylene ---- ---- <2 ----µg/L295-47-6

----^ Total Xylenes ---- ---- <2 ----µg/L21330-20-7

----^ ---- ---- <1 ----µg/L1----Sum of BTEX

----Naphthalene ---- ---- <5 ----µg/L591-20-3

EP116: 1.4-Dioxane

----1.4-Dioxane ---- ---- <0.5 ----µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.03Perfluorobutane sulfonic acid

(PFBS)

<0.02 0.02 0.76 2.50µg/L0.02375-73-5

0.03Perfluoropentane sulfonic acid

(PFPeS)

0.02 <0.02 0.76 2.33µg/L0.022706-91-4

0.18Perfluorohexane sulfonic acid

(PFHxS)

0.11 0.13 4.98 15.1µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 0.42 0.49µg/L0.02375-92-8

0.12Perfluorooctane sulfonic acid

(PFOS)

0.12 0.24 16.3 13.0µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 0.3µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 <0.02 0.22 0.57µg/L0.022706-90-3

0.04Perfluorohexanoic acid (PFHxA) 0.03 0.03 0.97 2.49µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 0.23 0.60µg/L0.02375-85-9

0.02Perfluorooctanoic acid (PFOA) 0.01 0.02 0.54 0.98µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 0.03 0.04µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

Page 90: Appendix - Department of Defence

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Analytical Results

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(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 0.28 0.16µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 0.06 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

0.42 0.29 0.44 25.6 38.6µg/L0.01----Sum of PFAS

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Analytical Results

0902_SW010_0307170902_SW009_0307170902_SW008_0307170902_SW007_0407170902_SW006_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-010ES1716547-009ES1716547-008ES1716547-007ES1716547-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

0.30Sum of PFHxS and PFOS 0.23 0.37 21.3 28.1µg/L0.01355-46-4/1763-23-

1

0.39 0.27 0.44 24.3 35.7µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

----1.2-Dichloroethane-D4 ---- ---- 111 ----%517060-07-0

----Toluene-D8 ---- ---- 115 ----%52037-26-5

----4-Bromofluorobenzene ---- ---- 114 ----%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

----Phenol-d6 ---- ---- 26.3 ----%113127-88-3

----2-Chlorophenol-D4 ---- ---- 46.4 ----%193951-73-6

----2.4.6-Tribromophenol ---- ---- 58.1 ----%1118-79-6

EP075(SIM)T: PAH Surrogates

----2-Fluorobiphenyl ---- ---- 57.3 ----%1321-60-8

----Anthracene-d10 ---- ---- 92.3 ----%11719-06-8

----4-Terphenyl-d14 ---- ---- 61.7 ----%11718-51-0

EP075S: Acid Extractable Surrogates

----2-Fluorophenol ---- ---- 35.1 ----%2367-12-4

----Phenol-d6 ---- ---- 27.5 ----%213127-88-3

----2-Chlorophenol-D4 ---- ---- 43.7 ----%293951-73-6

----2.4.6-Tribromophenol ---- ---- 57.7 ----%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

----Nitrobenzene-D5 ---- ---- 51.0 ----%24165-60-0

----1.2-Dichlorobenzene-D4 ---- ---- 45.2 ----%22199-69-1

----2-Fluorobiphenyl ---- ---- 54.8 ----%2321-60-8

----Anthracene-d10 ---- ---- 66.5 ----%21719-06-8

----4-Terphenyl-d14 ---- ---- 70.7 ----%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

----1.2-Dichloroethane-D4 ---- ---- 119 ----%217060-07-0

----Toluene-D8 ---- ---- 118 ----%22037-26-5

----4-Bromofluorobenzene ---- ---- 120 ----%2460-00-4

EP116S: 1.4-Dioxane Surrogate

----1.4-Dioxane-d8 ---- ---- 111 ----%0.517647-74-4

EP231S: PFAS Surrogate

91.9 90.4 93.2 92.5 91.2%0.02----13C4-PFOS

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0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

82 102 ---- 64 ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 ---- <1 ----mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 ---- <1 ----mg/L13812-32-6

47Bicarbonate Alkalinity as CaCO3 48 ---- 32 ----mg/L171-52-3

47 48 ---- 32 ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

9Sulfate as SO4 - Turbidimetric 7 ---- <1 ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

9Chloride 18 ---- 8 ----mg/L116887-00-6

ED093F: Dissolved Major Cations

8Calcium 13 ---- 6 ----mg/L17440-70-2

3Magnesium 3 ---- 2 ----mg/L17439-95-4

13Sodium 13 ---- 7 ----mg/L17440-23-5

3Potassium 2 ---- 2 ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.02Aluminium 0.06 ---- 0.03 ----mg/L0.017429-90-5

0.001Arsenic <0.001 ---- <0.001 ----mg/L0.0017440-38-2

0.0001Cadmium 0.0002 ---- <0.0001 ----mg/L0.00017440-43-9

<0.001Chromium <0.001 ---- <0.001 ----mg/L0.0017440-47-3

<0.001Copper 0.012 ---- <0.001 ----mg/L0.0017440-50-8

<0.001Lead <0.001 ---- <0.001 ----mg/L0.0017439-92-1

0.006Manganese 0.177 ---- 0.178 ----mg/L0.0017439-96-5

<0.001Nickel <0.001 ---- <0.001 ----mg/L0.0017440-02-0

0.017Zinc 0.089 ---- <0.005 ----mg/L0.0057440-66-6

<0.05Iron 0.56 ---- 2.70 ----mg/L0.057439-89-6

<0.1Bromine <0.1 ---- <0.1 ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 ---- <0.0001 ----mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

<0.1Fluoride 0.3 ---- <0.1 ----mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.02Ammonia as N ---- ---- ---- ----mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

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0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N ---- ---- ---- ----mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

0.81Nitrate as N ---- ---- ---- ----mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

0.81 ---- ---- ---- ----mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

0.07Reactive Phosphorus as P ---- ---- ---- ----mg/L0.0114265-44-2

EN055: Ionic Balance

1.38 1.61 ---- 0.86 ----meq/L0.01----Total Anions

1.29 1.51 ---- 0.82 ----meq/L0.01----Total Cations

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 ---- <5 ----µg/L5100-42-5

<5Isopropylbenzene <5 ---- <5 ----µg/L598-82-8

<5n-Propylbenzene <5 ---- <5 ----µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 ---- <5 ----µg/L5108-67-8

<5sec-Butylbenzene <5 ---- <5 ----µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 ---- <5 ----µg/L595-63-6

<5tert-Butylbenzene <5 ---- <5 ----µg/L598-06-6

<5p-Isopropyltoluene <5 ---- <5 ----µg/L599-87-6

<5n-Butylbenzene <5 ---- <5 ----µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 ---- <50 ----µg/L50108-05-4

<502-Butanone (MEK) <50 ---- <50 ----µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 ---- <50 ----µg/L50108-10-1

<502-Hexanone (MBK) <50 ---- <50 ----µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 ---- <5 ----µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 ---- <5 ----µg/L5594-20-7

<51.2-Dichloropropane <5 ---- <5 ----µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 ---- <5 ----µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 ---- <5 ----µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 ---- <5 ----µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

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(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<50Dichlorodifluoromethane <50 ---- <50 ----µg/L5075-71-8

<50Chloromethane <50 ---- <50 ----µg/L5074-87-3

<50Vinyl chloride <50 ---- <50 ----µg/L5075-01-4

<50Bromomethane <50 ---- <50 ----µg/L5074-83-9

<50Chloroethane <50 ---- <50 ----µg/L5075-00-3

<50Trichlorofluoromethane <50 ---- <50 ----µg/L5075-69-4

<51.1-Dichloroethene <5 ---- <5 ----µg/L575-35-4

<5Iodomethane <5 ---- <5 ----µg/L574-88-4

<5trans-1.2-Dichloroethene <5 ---- <5 ----µg/L5156-60-5

<51.1-Dichloroethane <5 ---- <5 ----µg/L575-34-3

<5cis-1.2-Dichloroethene <5 ---- <5 ----µg/L5156-59-2

<51.1.1-Trichloroethane <5 ---- <5 ----µg/L571-55-6

<51.1-Dichloropropylene <5 ---- <5 ----µg/L5563-58-6

<5Carbon Tetrachloride <5 ---- <5 ----µg/L556-23-5

<51.2-Dichloroethane <5 ---- <5 ----µg/L5107-06-2

<5Trichloroethene <5 ---- <5 ----µg/L579-01-6

<5Dibromomethane <5 ---- <5 ----µg/L574-95-3

<51.1.2-Trichloroethane <5 ---- <5 ----µg/L579-00-5

<51.3-Dichloropropane <5 ---- <5 ----µg/L5142-28-9

<5Tetrachloroethene <5 ---- <5 ----µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 ---- <5 ----µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 ---- <5 ----µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 ---- <5 ----µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 ---- <5 ----µg/L579-34-5

<51.2.3-Trichloropropane <5 ---- <5 ----µg/L596-18-4

<5Pentachloroethane <5 ---- <5 ----µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 ---- <5 ----µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 ---- <5 ----µg/L5108-90-7

<5Bromobenzene <5 ---- <5 ----µg/L5108-86-1

<52-Chlorotoluene <5 ---- <5 ----µg/L595-49-8

<54-Chlorotoluene <5 ---- <5 ----µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 ---- <5 ----µg/L587-61-6

EP074G: Trihalomethanes

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(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 ---- <5 ----µg/L567-66-3

<5Bromodichloromethane <5 ---- <5 ----µg/L575-27-4

<5Dibromochloromethane <5 ---- <5 ----µg/L5124-48-1

<5Bromoform <5 ---- <5 ----µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 ---- <1.0 ----µg/L191-20-3

<1.0Acenaphthylene <1.0 ---- <1.0 ----µg/L1208-96-8

<1.0Acenaphthene <1.0 ---- <1.0 ----µg/L183-32-9

<1.0Fluorene <1.0 ---- <1.0 ----µg/L186-73-7

<1.0Phenanthrene <1.0 ---- <1.0 ----µg/L185-01-8

<1.0Anthracene <1.0 ---- <1.0 ----µg/L1120-12-7

<1.0Fluoranthene <1.0 ---- <1.0 ----µg/L1206-44-0

<1.0Pyrene <1.0 ---- <1.0 ----µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 ---- <1.0 ----µg/L156-55-3

<1.0Chrysene <1.0 ---- <1.0 ----µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 ---- <1.0 ----µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 ---- <1.0 ----µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 ---- <0.5 ----µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 ---- <1.0 ----µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 ---- <1.0 ----µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 ---- <1.0 ----µg/L1191-24-2

<0.5^ <0.5 ---- <0.5 ----µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 ---- <0.5 ----µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 ---- <2 ----µg/L2108-95-2

<22-Chlorophenol <2 ---- <2 ----µg/L295-57-8

<22-Methylphenol <2 ---- <2 ----µg/L295-48-7

<43- & 4-Methylphenol <4 ---- <4 ----µg/L41319-77-3

<22-Nitrophenol <2 ---- <2 ----µg/L288-75-5

<22.4-Dimethylphenol <2 ---- <2 ----µg/L2105-67-9

<22.4-Dichlorophenol <2 ---- <2 ----µg/L2120-83-2

<22.6-Dichlorophenol <2 ---- <2 ----µg/L287-65-0

<24-Chloro-3-methylphenol <2 ---- <2 ----µg/L259-50-7

<22.4.6-Trichlorophenol <2 ---- <2 ----µg/L288-06-2

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Analytical Results

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(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 ---- <2 ----µg/L295-95-4

<4Pentachlorophenol <4 ---- <4 ----µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 ---- <2 ----µg/L291-57-6

<22-Chloronaphthalene <2 ---- <2 ----µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 ---- <2 ----µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 ---- <2 ----µg/L257-97-6

<23-Methylcholanthrene <2 ---- <2 ----µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 ---- <2 ----µg/L2131-11-3

<2Diethyl phthalate <2 ---- <2 ----µg/L284-66-2

<2Di-n-butyl phthalate <2 ---- <2 ----µg/L284-74-2

<2Butyl benzyl phthalate <2 ---- <2 ----µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 ---- <10 ----µg/L10117-81-7

<2Di-n-octylphthalate <2 ---- <2 ----µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 ---- <2 ----µg/L210595-95-6

<2N-Nitrosodiethylamine <2 ---- <2 ----µg/L255-18-5

<4N-Nitrosopyrrolidine <4 ---- <4 ----µg/L4930-55-2

<2N-Nitrosomorpholine <2 ---- <2 ----µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 ---- <2 ----µg/L2621-64-7

<2N-Nitrosopiperidine <2 ---- <2 ----µg/L2100-75-4

<2N-Nitrosodibutylamine <2 ---- <2 ----µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 ---- <4 ----µg/L486-30-6 122-39-4

<2Methapyrilene <2 ---- <2 ----µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 ---- <2 ----µg/L2109-06-8

<2Acetophenone <2 ---- <2 ----µg/L298-86-2

<2Nitrobenzene <2 ---- <2 ----µg/L298-95-3

<2Isophorone <2 ---- <2 ----µg/L278-59-1

<42.6-Dinitrotoluene <4 ---- <4 ----µg/L4606-20-2

<42.4-Dinitrotoluene <4 ---- <4 ----µg/L4121-14-2

<21-Naphthylamine <2 ---- <2 ----µg/L2134-32-7

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Analytical Results

0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 ---- <2 ----µg/L256-57-5

<25-Nitro-o-toluidine <2 ---- <2 ----µg/L299-55-8

<2Azobenzene <2 ---- <2 ----µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 ---- <2 ----µg/L299-35-4

<2Phenacetin <2 ---- <2 ----µg/L262-44-2

<24-Aminobiphenyl <2 ---- <2 ----µg/L292-67-1

<2Pentachloronitrobenzene <2 ---- <2 ----µg/L282-68-8

<2Pronamide <2 ---- <2 ----µg/L223950-58-5

<2Dimethylaminoazobenzene <2 ---- <2 ----µg/L260-11-7

<2Chlorobenzilate <2 ---- <2 ----µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 ---- <2 ----µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 ---- <2 ----µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 ---- <2 ----µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 ---- <2 ----µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 ---- <2 ----µg/L2541-73-1

<21.4-Dichlorobenzene <2 ---- <2 ----µg/L2106-46-7

<21.2-Dichlorobenzene <2 ---- <2 ----µg/L295-50-1

<2Hexachloroethane <2 ---- <2 ----µg/L267-72-1

<21.2.4-Trichlorobenzene <2 ---- <2 ----µg/L2120-82-1

<2Hexachloropropylene <2 ---- <2 ----µg/L21888-71-7

<2Hexachlorobutadiene <2 ---- <2 ----µg/L287-68-3

<10Hexachlorocyclopentadiene <10 ---- <10 ----µg/L1077-47-4

<2Pentachlorobenzene <2 ---- <2 ----µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 ---- <4 ----µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 ---- <2 ----µg/L262-53-3

<24-Chloroaniline <2 ---- <2 ----µg/L2106-47-8

<42-Nitroaniline <4 ---- <4 ----µg/L488-74-4

<43-Nitroaniline <4 ---- <4 ----µg/L499-09-2

<2Dibenzofuran <2 ---- <2 ----µg/L2132-64-9

<24-Nitroaniline <2 ---- <2 ----µg/L2100-01-6

<2Carbazole <2 ---- <2 ----µg/L286-74-8

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(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 ---- <2 ----µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 ---- <2 ----µg/L2319-84-6

<2beta-BHC <2 ---- <2 ----µg/L2319-85-7

<2gamma-BHC <2 ---- <2 ----µg/L258-89-9

<2delta-BHC <2 ---- <2 ----µg/L2319-86-8

<2Heptachlor <2 ---- <2 ----µg/L276-44-8

<2Aldrin <2 ---- <2 ----µg/L2309-00-2

<2Heptachlor epoxide <2 ---- <2 ----µg/L21024-57-3

<2alpha-Endosulfan <2 ---- <2 ----µg/L2959-98-8

<24.4`-DDE <2 ---- <2 ----µg/L272-55-9

<2Dieldrin <2 ---- <2 ----µg/L260-57-1

<2Endrin <2 ---- <2 ----µg/L272-20-8

<2beta-Endosulfan <2 ---- <2 ----µg/L233213-65-9

<24.4`-DDD <2 ---- <2 ----µg/L272-54-8

<2Endosulfan sulfate <2 ---- <2 ----µg/L21031-07-8

<44.4`-DDT <4 ---- <4 ----µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 ---- <4 ----µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 ---- <4 ----µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 ---- <2 ----µg/L262-73-7

<2Dimethoate <2 ---- <2 ----µg/L260-51-5

<2Diazinon <2 ---- <2 ----µg/L2333-41-5

<2Chlorpyrifos-methyl <2 ---- <2 ----µg/L25598-13-0

<2Malathion <2 ---- <2 ----µg/L2121-75-5

<2Fenthion <2 ---- <2 ----µg/L255-38-9

<2Chlorpyrifos <2 ---- <2 ----µg/L22921-88-2

<2Pirimphos-ethyl <2 ---- <2 ----µg/L223505-41-1

<2Chlorfenvinphos <2 ---- <2 ----µg/L2470-90-6

<2Prothiofos <2 ---- <2 ----µg/L234643-46-4

<2Ethion <2 ---- <2 ----µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 ---- <20 ----µg/L20----C6 - C9 Fraction

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Analytical Results

0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 ---- <50 ----µg/L50----C10 - C14 Fraction

<100 <100 ---- <100 ----µg/L100----C15 - C28 Fraction

<50 <50 ---- <50 ----µg/L50----C29 - C36 Fraction

<50^ <50 ---- <50 ----µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 ---- <20 ----µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 ---- <20 ----µg/L20C6_C10-BTEX

<100 <100 ---- <100 ----µg/L100---->C10 - C16 Fraction

<100 <100 ---- <100 ----µg/L100---->C16 - C34 Fraction

<100 <100 ---- <100 ----µg/L100---->C34 - C40 Fraction

<100^ <100 ---- <100 ----µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 ---- <100 ----µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 ---- <1 ----µg/L171-43-2

<2Toluene <2 ---- <2 ----µg/L2108-88-3

<2Ethylbenzene <2 ---- <2 ----µg/L2100-41-4

<2meta- & para-Xylene <2 ---- <2 ----µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 ---- <2 ----µg/L295-47-6

<2^ Total Xylenes <2 ---- <2 ----µg/L21330-20-7

<1^ <1 ---- <1 ----µg/L1----Sum of BTEX

<5Naphthalene <5 ---- <5 ----µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 ---- <0.5 ----µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.77Perfluorobutane sulfonic acid

(PFBS)

0.07 0.36 0.05 0.06µg/L0.02375-73-5

0.74Perfluoropentane sulfonic acid

(PFPeS)

0.06 0.34 0.04 0.06µg/L0.022706-91-4

6.28Perfluorohexane sulfonic acid

(PFHxS)

0.65 2.23 0.33 0.49µg/L0.02355-46-4

0.46Perfluoroheptane sulfonic acid

(PFHpS)

0.02 0.05 <0.02 <0.02µg/L0.02375-92-8

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Analytical Results

0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

16.0Perfluorooctane sulfonic acid

(PFOS)

0.54 0.76 0.44 0.39µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 0.2 <0.1 <0.1µg/L0.1375-22-4

0.27Perfluoropentanoic acid (PFPeA) 0.03 0.10 <0.02 <0.02µg/L0.022706-90-3

1.17Perfluorohexanoic acid (PFHxA) 0.11 0.32 0.07 0.04µg/L0.02307-24-4

0.24Perfluoroheptanoic acid (PFHpA) 0.03 0.09 <0.02 <0.02µg/L0.02375-85-9

0.53Perfluorooctanoic acid (PFOA) 0.04 0.10 0.03 0.02µg/L0.01335-67-1

0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.03Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

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Analytical Results

0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

0.726:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

0.078:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

27.3 1.55 4.55 0.96 1.06µg/L0.01----Sum of PFAS

22.3Sum of PFHxS and PFOS 1.19 2.99 0.77 0.88µg/L0.01355-46-4/1763-23-

1

26.0 1.47 4.16 0.92 1.00µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1131.2-Dichloroethane-D4 111 ---- 111 ----%517060-07-0

114Toluene-D8 114 ---- 115 ----%52037-26-5

1124-Bromofluorobenzene 111 ---- 111 ----%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

21.7Phenol-d6 29.1 ---- 25.0 ----%113127-88-3

42.62-Chlorophenol-D4 58.2 ---- 47.1 ----%193951-73-6

43.92.4.6-Tribromophenol 68.2 ---- 54.9 ----%1118-79-6

EP075(SIM)T: PAH Surrogates

51.92-Fluorobiphenyl 65.8 ---- 55.1 ----%1321-60-8

93.3Anthracene-d10 105 ---- 88.5 ----%11719-06-8

58.84-Terphenyl-d14 73.3 ---- 55.2 ----%11718-51-0

EP075S: Acid Extractable Surrogates

28.42-Fluorophenol 38.3 ---- 34.3 ----%2367-12-4

23.0Phenol-d6 28.8 ---- 22.8 ----%213127-88-3

38.42-Chlorophenol-D4 48.9 ---- 41.6 ----%293951-73-6

41.52.4.6-Tribromophenol 66.4 ---- 48.9 ----%2118-79-6

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Analytical Results

0902_SW015_0307170902_SW014_0307170902_SW013_0307170902_SW012_0307170902_SW011_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716547-015ES1716547-014ES1716547-013ES1716547-012ES1716547-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

47.9Nitrobenzene-D5 57.6 ---- 51.3 ----%24165-60-0

40.31.2-Dichlorobenzene-D4 50.4 ---- 45.2 ----%22199-69-1

48.62-Fluorobiphenyl 62.8 ---- 52.9 ----%2321-60-8

59.2Anthracene-d10 73.7 ---- 59.1 ----%21719-06-8

65.94-Terphenyl-d14 81.4 ---- 61.6 ----%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1221.2-Dichloroethane-D4 119 ---- 119 ----%217060-07-0

116Toluene-D8 117 ---- 118 ----%22037-26-5

1184-Bromofluorobenzene 116 ---- 116 ----%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1121.4-Dioxane-d8 116 ---- 114 ----%0.517647-74-4

EP231S: PFAS Surrogate

94.1 94.9 92.9 95.4 88.9%0.02----13C4-PFOS

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Analytical Results

0902_QC105_0307170902_SW019_0407170902_SW018_0407170902_SW017_0307170902_SW016_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-020ES1716547-019ES1716547-018ES1716547-017ES1716547-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids

<0.02Perfluorobutane sulfonic acid

(PFBS)

<0.02 <0.02 <0.02 2.70µg/L0.02375-73-5

<0.02Perfluoropentane sulfonic acid

(PFPeS)

<0.02 <0.02 <0.02 2.42µg/L0.022706-91-4

<0.02Perfluorohexane sulfonic acid

(PFHxS)

<0.02 0.03 0.04 14.8µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 <0.02 0.59µg/L0.02375-92-8

<0.01Perfluorooctane sulfonic acid

(PFOS)

<0.01 0.05 0.07 10.4µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 0.4µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 0.62µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) <0.02 <0.02 0.02 2.76µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 <0.02 0.64µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) <0.01 <0.01 0.02 1.14µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 0.04µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 0.03µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

Page 104: Appendix - Department of Defence

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Analytical Results

0902_QC105_0307170902_SW019_0407170902_SW018_0407170902_SW017_0307170902_SW016_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716547-020ES1716547-019ES1716547-018ES1716547-017ES1716547-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 0.17µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

<0.01 <0.01 0.08 0.15 36.7µg/L0.01----Sum of PFAS

<0.01Sum of PFHxS and PFOS <0.01 0.08 0.11 25.2µg/L0.01355-46-4/1763-23-

1

<0.01 <0.01 0.08 0.15 33.6µg/L0.01----Sum of PFAS (WA DER List)

EP231S: PFAS Surrogate

94.1 96.8 96.1 92.1 96.8%0.02----13C4-PFOS

Page 105: Appendix - Department of Defence

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EA015: Total Dissolved Solids dried at 180 ± 5 °C

262 ---- ---- ---- ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 ---- ---- ---- ----mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 ---- ---- ---- ----mg/L13812-32-6

32Bicarbonate Alkalinity as CaCO3 ---- ---- ---- ----mg/L171-52-3

32 ---- ---- ---- ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

44Sulfate as SO4 - Turbidimetric ---- ---- ---- ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

42Chloride ---- ---- ---- ----mg/L116887-00-6

ED093F: Dissolved Major Cations

14Calcium ---- ---- ---- ----mg/L17440-70-2

8Magnesium ---- ---- ---- ----mg/L17439-95-4

42Sodium ---- ---- ---- ----mg/L17440-23-5

4Potassium ---- ---- ---- ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.13Aluminium ---- ---- ---- ----mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 ---- ----mg/L0.0017440-38-2

0.0011Cadmium <0.0001 <0.0001 ---- ----mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 ---- ----mg/L0.0017440-47-3

0.004Copper <0.001 <0.001 ---- ----mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 ---- ----mg/L0.0017439-92-1

0.059Manganese ---- ---- ---- ----mg/L0.0017439-96-5

0.002Nickel <0.001 <0.001 ---- ----mg/L0.0017440-02-0

0.079Zinc <0.005 <0.005 ---- ----mg/L0.0057440-66-6

0.19Iron ---- ---- ---- ----mg/L0.057439-89-6

<0.1Bromine ---- ---- ---- ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 ---- ----mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.6Fluoride ---- ---- ---- ----mg/L0.116984-48-8

EN055: Ionic Balance

2.74 ---- ---- ---- ----meq/L0.01----Total Anions

3.29 ---- ---- ---- ----meq/L0.01----Total Cations

Page 106: Appendix - Department of Defence

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 ---- ----µg/L5100-42-5

<5Isopropylbenzene <5 <5 ---- ----µg/L598-82-8

<5n-Propylbenzene <5 <5 ---- ----µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 ---- ----µg/L5108-67-8

<5sec-Butylbenzene <5 <5 ---- ----µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 ---- ----µg/L595-63-6

<5tert-Butylbenzene <5 <5 ---- ----µg/L598-06-6

<5p-Isopropyltoluene <5 <5 ---- ----µg/L599-87-6

<5n-Butylbenzene <5 <5 ---- ----µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 ---- ----µg/L50108-05-4

<502-Butanone (MEK) <50 <50 ---- ----µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 ---- ----µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 ---- ----µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 ---- ----µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 ---- ----µg/L5594-20-7

<51.2-Dichloropropane <5 <5 ---- ----µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 ---- ----µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 ---- ----µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 ---- ----µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 ---- ----µg/L5075-71-8

<50Chloromethane <50 <50 ---- ----µg/L5074-87-3

<50Vinyl chloride <50 <50 ---- ----µg/L5075-01-4

<50Bromomethane <50 <50 ---- ----µg/L5074-83-9

<50Chloroethane <50 <50 ---- ----µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 ---- ----µg/L5075-69-4

<51.1-Dichloroethene <5 <5 ---- ----µg/L575-35-4

<5Iodomethane <5 <5 ---- ----µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 ---- ----µg/L5156-60-5

<51.1-Dichloroethane <5 <5 ---- ----µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 ---- ----µg/L5156-59-2

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1.1-Trichloroethane <5 <5 ---- ----µg/L571-55-6

<51.1-Dichloropropylene <5 <5 ---- ----µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 ---- ----µg/L556-23-5

<51.2-Dichloroethane <5 <5 ---- ----µg/L5107-06-2

<5Trichloroethene <5 <5 ---- ----µg/L579-01-6

<5Dibromomethane <5 <5 ---- ----µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 ---- ----µg/L579-00-5

<51.3-Dichloropropane <5 <5 ---- ----µg/L5142-28-9

<5Tetrachloroethene <5 <5 ---- ----µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 ---- ----µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 ---- ----µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 ---- ----µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 ---- ----µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 ---- ----µg/L596-18-4

<5Pentachloroethane <5 <5 ---- ----µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 ---- ----µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 ---- ----µg/L5108-90-7

<5Bromobenzene <5 <5 ---- ----µg/L5108-86-1

<52-Chlorotoluene <5 <5 ---- ----µg/L595-49-8

<54-Chlorotoluene <5 <5 ---- ----µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 ---- ----µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform <5 <5 ---- ----µg/L567-66-3

<5Bromodichloromethane <5 <5 ---- ----µg/L575-27-4

<5Dibromochloromethane <5 <5 ---- ----µg/L5124-48-1

<5Bromoform <5 <5 ---- ----µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 ---- ----µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 ---- ----µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 ---- ----µg/L183-32-9

<1.0Fluorene <1.0 <1.0 ---- ----µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 ---- ----µg/L185-01-8

<1.0Anthracene <1.0 <1.0 ---- ----µg/L1120-12-7

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Fluoranthene <1.0 <1.0 ---- ----µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 ---- ----µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 ---- ----µg/L156-55-3

<1.0Chrysene <1.0 <1.0 ---- ----µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 ---- ----µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 ---- ----µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 ---- ----µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 ---- ----µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 ---- ----µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 ---- ----µg/L1191-24-2

<0.5^ <0.5 <0.5 ---- ----µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 ---- ----µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 ---- ----µg/L2108-95-2

<22-Chlorophenol <2 <2 ---- ----µg/L295-57-8

<22-Methylphenol <2 <2 ---- ----µg/L295-48-7

<43- & 4-Methylphenol <4 <4 ---- ----µg/L41319-77-3

<22-Nitrophenol <2 <2 ---- ----µg/L288-75-5

<22.4-Dimethylphenol <2 <2 ---- ----µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 ---- ----µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 ---- ----µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 ---- ----µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 ---- ----µg/L288-06-2

<22.4.5-Trichlorophenol <2 <2 ---- ----µg/L295-95-4

<4Pentachlorophenol <4 <4 ---- ----µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 ---- ----µg/L291-57-6

<22-Chloronaphthalene <2 <2 ---- ----µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 ---- ----µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 ---- ----µg/L257-97-6

<23-Methylcholanthrene <2 <2 ---- ----µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 ---- ----µg/L2131-11-3

<2Diethyl phthalate <2 <2 ---- ----µg/L284-66-2

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075C: Phthalate Esters - Continued

<2Di-n-butyl phthalate <2 <2 ---- ----µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 ---- ----µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 ---- ----µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 ---- ----µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 ---- ----µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 ---- ----µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 ---- ----µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 ---- ----µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 ---- ----µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 ---- ----µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 ---- ----µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 ---- ----µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 ---- ----µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 ---- ----µg/L2109-06-8

<2Acetophenone <2 <2 ---- ----µg/L298-86-2

<2Nitrobenzene <2 <2 ---- ----µg/L298-95-3

<2Isophorone <2 <2 ---- ----µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 ---- ----µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 ---- ----µg/L4121-14-2

<21-Naphthylamine <2 <2 ---- ----µg/L2134-32-7

<24-Nitroquinoline-N-oxide <2 <2 ---- ----µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 ---- ----µg/L299-55-8

<2Azobenzene <2 <2 ---- ----µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 ---- ----µg/L299-35-4

<2Phenacetin <2 <2 ---- ----µg/L262-44-2

<24-Aminobiphenyl <2 <2 ---- ----µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 ---- ----µg/L282-68-8

<2Pronamide <2 <2 ---- ----µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 ---- ----µg/L260-11-7

<2Chlorobenzilate <2 <2 ---- ----µg/L2510-15-6

EP075F: Haloethers

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075F: Haloethers - Continued

<2Bis(2-chloroethyl) ether <2 <2 ---- ----µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 ---- ----µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 ---- ----µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 ---- ----µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 ---- ----µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 ---- ----µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 ---- ----µg/L295-50-1

<2Hexachloroethane <2 <2 ---- ----µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 ---- ----µg/L2120-82-1

<2Hexachloropropylene <2 <2 ---- ----µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 ---- ----µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 ---- ----µg/L1077-47-4

<2Pentachlorobenzene <2 <2 ---- ----µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 ---- ----µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 ---- ----µg/L262-53-3

<24-Chloroaniline <2 <2 ---- ----µg/L2106-47-8

<42-Nitroaniline <4 <4 ---- ----µg/L488-74-4

<43-Nitroaniline <4 <4 ---- ----µg/L499-09-2

<2Dibenzofuran <2 <2 ---- ----µg/L2132-64-9

<24-Nitroaniline <2 <2 ---- ----µg/L2100-01-6

<2Carbazole <2 <2 ---- ----µg/L286-74-8

<23.3`-Dichlorobenzidine <2 <2 ---- ----µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 ---- ----µg/L2319-84-6

<2beta-BHC <2 <2 ---- ----µg/L2319-85-7

<2gamma-BHC <2 <2 ---- ----µg/L258-89-9

<2delta-BHC <2 <2 ---- ----µg/L2319-86-8

<2Heptachlor <2 <2 ---- ----µg/L276-44-8

<2Aldrin <2 <2 ---- ----µg/L2309-00-2

<2Heptachlor epoxide <2 <2 ---- ----µg/L21024-57-3

<2alpha-Endosulfan <2 <2 ---- ----µg/L2959-98-8

<24.4`-DDE <2 <2 ---- ----µg/L272-55-9

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075I: Organochlorine Pesticides - Continued

<2Dieldrin <2 <2 ---- ----µg/L260-57-1

<2Endrin <2 <2 ---- ----µg/L272-20-8

<2beta-Endosulfan <2 <2 ---- ----µg/L233213-65-9

<24.4`-DDD <2 <2 ---- ----µg/L272-54-8

<2Endosulfan sulfate <2 <2 ---- ----µg/L21031-07-8

<44.4`-DDT <4 <4 ---- ----µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 ---- ----µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 ---- ----µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 ---- ----µg/L262-73-7

<2Dimethoate <2 <2 ---- ----µg/L260-51-5

<2Diazinon <2 <2 ---- ----µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 ---- ----µg/L25598-13-0

<2Malathion <2 <2 ---- ----µg/L2121-75-5

<2Fenthion <2 <2 ---- ----µg/L255-38-9

<2Chlorpyrifos <2 <2 ---- ----µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 ---- ----µg/L223505-41-1

<2Chlorfenvinphos <2 <2 ---- ----µg/L2470-90-6

<2Prothiofos <2 <2 ---- ----µg/L234643-46-4

<2Ethion <2 <2 ---- ----µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 ----µg/L20----C6 - C9 Fraction

95600 <50 <50 ---- ----µg/L50----C10 - C14 Fraction

1050 <100 <100 ---- ----µg/L100----C15 - C28 Fraction

180 <50 <50 ---- ----µg/L50----C29 - C36 Fraction

96800^ <50 <50 ---- ----µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 ----µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 ----µg/L20C6_C10-BTEX

96600 <100 <100 ---- ----µg/L100---->C10 - C16 Fraction

840 <100 <100 ---- ----µg/L100---->C16 - C34 Fraction

<100 <100 <100 ---- ----µg/L100---->C34 - C40 Fraction

97400^ <100 <100 ---- ----µg/L100---->C10 - C40 Fraction (sum)

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

96600^ <100 <100 ---- ----µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 ----µg/L171-43-2

<2Toluene <2 <2 <2 ----µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 ----µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 ----µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 ----µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 ----µg/L21330-20-7

<1^ <1 <1 <1 ----µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 ----µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <0.5 ---- ----µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.87Perfluorobutane sulfonic acid

(PFBS)

<0.02 <0.02 ---- ----µg/L0.02375-73-5

0.71Perfluoropentane sulfonic acid

(PFPeS)

<0.02 <0.02 ---- ----µg/L0.022706-91-4

1.17Perfluorohexane sulfonic acid

(PFHxS)

<0.02 <0.02 ---- ----µg/L0.02355-46-4

0.21Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 ---- ----µg/L0.02375-92-8

10.6Perfluorooctane sulfonic acid

(PFOS)

<0.01 <0.01 ---- ----µg/L0.011763-23-1

0.23Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 ---- ----µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

3.2Perfluorobutanoic acid (PFBA) <0.1 <0.1 ---- ----µg/L0.1375-22-4

8.90Perfluoropentanoic acid (PFPeA) <0.02 <0.02 ---- ----µg/L0.022706-90-3

53.5Perfluorohexanoic acid (PFHxA) <0.02 <0.02 ---- ----µg/L0.02307-24-4

2.31Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 ---- ----µg/L0.02375-85-9

10.1Perfluorooctanoic acid (PFOA) <0.01 <0.01 ---- ----µg/L0.01335-67-1

7.49Perfluorononanoic acid (PFNA) <0.02 <0.02 ---- ----µg/L0.02375-95-1

7.79Perfluorodecanoic acid (PFDA) <0.02 <0.02 ---- ----µg/L0.02335-76-2

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

1.14Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 ---- ----µg/L0.022058-94-8

1.50Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 ---- ----µg/L0.02307-55-1

0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 ---- ----µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 ---- ----µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

0.53Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 ---- ----µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 ---- ----µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 ---- ----µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 ---- ----µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 ---- ----µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 ---- ----µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 ---- ----µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

0.614:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 ---- ----µg/L0.05757124-72-4

4776:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 ---- ----µg/L0.0527619-97-2

16.48:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 ---- ----µg/L0.0539108-34-4

0.1410:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 ---- ----µg/L0.05120226-60-0

EP231P: PFAS Sums

604 <0.01 <0.01 ---- ----µg/L0.01----Sum of PFAS

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Analytical Results

----0902_QC506_0407170902_QC505_0407170902_QC504_0307170902_QC107_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----04-Jul-2017 00:0004-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716547-024ES1716547-023ES1716547-022ES1716547-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP231P: PFAS Sums - Continued

11.8Sum of PFHxS and PFOS <0.01 <0.01 ---- ----µg/L0.01355-46-4/1763-23-

1

584 <0.01 <0.01 ---- ----µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1111.2-Dichloroethane-D4 107 109 ---- ----%517060-07-0

115Toluene-D8 108 112 ---- ----%52037-26-5

1134-Bromofluorobenzene 107 109 ---- ----%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

14.5Phenol-d6 28.2 24.7 ---- ----%113127-88-3

25.72-Chlorophenol-D4 54.3 52.3 ---- ----%193951-73-6

67.82.4.6-Tribromophenol 41.4 54.7 ---- ----%1118-79-6

EP075(SIM)T: PAH Surrogates

47.52-Fluorobiphenyl 47.7 54.3 ---- ----%1321-60-8

70.9Anthracene-d10 84.7 88.3 ---- ----%11719-06-8

55.84-Terphenyl-d14 54.2 56.0 ---- ----%11718-51-0

EP075S: Acid Extractable Surrogates

19.72-Fluorophenol 25.9 32.7 ---- ----%2367-12-4

20.4Phenol-d6 22.1 23.2 ---- ----%213127-88-3

16.42-Chlorophenol-D4 37.3 44.3 ---- ----%293951-73-6

64.52.4.6-Tribromophenol 25.5 43.6 ---- ----%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

26.9Nitrobenzene-D5 48.2 50.5 ---- ----%24165-60-0

44.21.2-Dichlorobenzene-D4 42.3 43.9 ---- ----%22199-69-1

83.62-Fluorobiphenyl 42.4 48.9 ---- ----%2321-60-8

49.6Anthracene-d10 54.1 59.5 ---- ----%21719-06-8

63.04-Terphenyl-d14 58.7 62.3 ---- ----%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1201.2-Dichloroethane-D4 114 117 112 ----%217060-07-0

118Toluene-D8 111 115 99.4 ----%22037-26-5

1194-Bromofluorobenzene 112 115 77.4 ----%2460-00-4

EP116S: 1.4-Dioxane Surrogate

93.51.4-Dioxane-d8 110 116 ---- ----%0.517647-74-4

EP231S: PFAS Surrogate

91.2 90.2 98.4 ---- ----%0.02----13C4-PFOS

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Surrogate Control Limits

Recovery Limits (%)Sub-Matrix: SOIL

Compound CAS Number Low High

EP068S: Organochlorine Pesticide Surrogate

Dibromo-DDE 21655-73-2 49 147

EP068T: Organophosphorus Pesticide Surrogate

DEF 78-48-8 35 143

EP074S: VOC Surrogates

1.2-Dichloroethane-D4 17060-07-0 64 130

Toluene-D8 2037-26-5 66 136

4-Bromofluorobenzene 460-00-4 60 122

EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 13127-88-3 63 123

2-Chlorophenol-D4 93951-73-6 66 122

2.4.6-Tribromophenol 118-79-6 40 138

EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl 321-60-8 70 122

Anthracene-d10 1719-06-8 66 128

4-Terphenyl-d14 1718-51-0 65 129

EP075S: Acid Extractable Surrogates

2-Fluorophenol 367-12-4 29 149

Phenol-d6 13127-88-3 32 128

2-Chlorophenol-D4 93951-73-6 32 128

2.4.6-Tribromophenol 118-79-6 13 121

EP075T: Base/Neutral Extractable Surrogates

Nitrobenzene-D5 4165-60-0 33 125

1.2-Dichlorobenzene-D4 2199-69-1 34 108

2-Fluorobiphenyl 321-60-8 35 121

Anthracene-d10 1719-06-8 35 123

4-Terphenyl-d14 1718-51-0 33 125

EP080S: TPH(V)/BTEX Surrogates

1.2-Dichloroethane-D4 17060-07-0 73 133

Toluene-D8 2037-26-5 74 132

4-Bromofluorobenzene 460-00-4 72 130

EP116S: 1.4-Dioxane Surrogate

1.4-Dioxane-d8 17647-74-4 70 130

EP231S: PFAS Surrogate

13C4-PFOS ---- 70 130

Recovery Limits (%)Sub-Matrix: WATER

Compound CAS Number Low High

EP074S: VOC Surrogates

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Recovery Limits (%)Sub-Matrix: WATER

Compound CAS Number Low High

EP074S: VOC Surrogates - Continued

1.2-Dichloroethane-D4 17060-07-0 78 133

Toluene-D8 2037-26-5 79 129

4-Bromofluorobenzene 460-00-4 81 124

EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 13127-88-3 10 44

2-Chlorophenol-D4 93951-73-6 14 94

2.4.6-Tribromophenol 118-79-6 17 125

EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl 321-60-8 20 104

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 32 112

EP075S: Acid Extractable Surrogates

2-Fluorophenol 367-12-4 10 117

Phenol-d6 13127-88-3 10 69

2-Chlorophenol-D4 93951-73-6 21 130

2.4.6-Tribromophenol 118-79-6 10 151

EP075T: Base/Neutral Extractable Surrogates

Nitrobenzene-D5 4165-60-0 29 142

1.2-Dichlorobenzene-D4 2199-69-1 24 121

2-Fluorobiphenyl 321-60-8 27 135

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 21 123

EP080S: TPH(V)/BTEX Surrogates

1.2-Dichloroethane-D4 17060-07-0 71 137

Toluene-D8 2037-26-5 79 131

4-Bromofluorobenzene 460-00-4 70 128

EP116S: 1.4-Dioxane Surrogate

1.4-Dioxane-d8 17647-74-4 69 127

EP231S: PFAS Surrogate

13C4-PFOS ---- 60 130

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7 7.00False

Environmental

QUALITY CONTROL REPORTWork Order : ES1716547 Page : 1 of 47

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER :Contact Loren Schiavon

:Address LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

Address : 277-289 Woodpark Road Smithfield NSW Australia 2164

::Telephone +61 02 8934 0000 +61 2 8784 8503:Telephone

:Project 60547028, TASK 3.1 Date Samples Received : 05-Jul-2017

:Order number 60547028, TASK 3.1 Date Analysis Commenced : 06-Jul-2017

:C-O-C number ---- Issue Date : 17-Jul-2017

Sampler : DIRK SANDERSON

Site : RAAF RICHMOND

Quote number : SY/308/17

No. of samples received 45:

No. of samples analysed 45:

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Dian Dao Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Sanjeshni Jyoti Senior Chemist Volatiles Sydney Organics, Smithfield, NSW

Satishkumar Trivedi Acid Sulfate Soils Supervisor Brisbane Acid Sulphate Soils, Stafford, QLD

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.

Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA055: Moisture Content (Dried @ 105-110°C) (QC Lot: 984406)

EA055: Moisture Content ---- 1 % 15.9 15.7 1.43 0% - 50%Anonymous EP1707075-031

EA055: Moisture Content ---- 1 % 23.2 23.7 2.30 0% - 20%Anonymous EP1707076-031

EA055: Moisture Content (Dried @ 105-110°C) (QC Lot: 984407)

EA055: Moisture Content ---- 1 % 51.7 49.9 3.44 0% - 20%0902_SD008_030717 ES1716547-032

EA055: Moisture Content ---- 1 % 46.6 47.5 2.05 0% - 20%0902_SD019_040717 ES1716547-043

ED007: Exchangeable Cations (QC Lot: 991755)

ED007: Exchangeable Calcium ---- 0.1 meq/100g 2.9 2.8 0.00 0% - 20%0902_SD001_030717 ES1716547-025

ED007: Exchangeable Magnesium ---- 0.1 meq/100g 3.0 3.0 0.00 0% - 20%

ED007: Exchangeable Potassium ---- 0.1 meq/100g 0.3 0.3 0.00 No Limit

ED007: Exchangeable Sodium ---- 0.1 meq/100g 0.2 0.2 0.00 No Limit

ED007: Cation Exchange Capacity ---- 0.1 meq/100g 6.4 6.3 2.43 0% - 20%

EG005T: Total Metals by ICP-AES (QC Lot: 987748)

EG005T: Cadmium 7440-43-9 1 mg/kg <1 <1 0.00 No LimitAnonymous ES1716473-006

EG005T: Chromium 7440-47-3 2 mg/kg 8 8 0.00 No Limit

EG005T: Nickel 7440-02-0 2 mg/kg 17 18 9.47 No Limit

EG005T: Arsenic 7440-38-2 5 mg/kg 6 6 0.00 No Limit

EG005T: Copper 7440-50-8 5 mg/kg 38 38 0.00 No Limit

EG005T: Lead 7439-92-1 5 mg/kg 22 21 6.48 No Limit

EG005T: Zinc 7440-66-6 5 mg/kg 69 71 2.75 0% - 50%

EG005T: Iron 7439-89-6 50 mg/kg 34400 38700 11.7 0% - 20%

EG005T: Cadmium 7440-43-9 1 mg/kg <1 <1 0.00 No LimitAnonymous ES1716635-002

EG005T: Chromium 7440-47-3 2 mg/kg 13 13 0.00 No Limit

EG005T: Nickel 7440-02-0 2 mg/kg 22 19 12.1 0% - 50%

EG005T: Arsenic 7440-38-2 5 mg/kg 6 <5 0.00 No Limit

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EG005T: Total Metals by ICP-AES (QC Lot: 987748) - continued

EG005T: Copper 7440-50-8 5 mg/kg 56 56 0.00 0% - 50%Anonymous ES1716635-002

EG005T: Lead 7439-92-1 5 mg/kg 24 23 0.00 No Limit

EG005T: Zinc 7440-66-6 5 mg/kg 99 88 11.7 0% - 50%

EG005T: Iron 7439-89-6 50 mg/kg 38000 36800 3.27 0% - 20%

EG035T: Total Recoverable Mercury by FIMS (QC Lot: 987747)

EG035T: Mercury 7439-97-6 0.1 mg/kg <0.1 <0.1 0.00 No LimitAnonymous ES1716473-006

EG035T: Mercury 7439-97-6 0.1 mg/kg <0.1 <0.1 0.00 No LimitAnonymous ES1716635-002

EP003: Total Organic Carbon (TOC) in Soil (QC Lot: 989620)

EP003: Total Organic Carbon ---- 0.02 % 0.22 0.21 0.00 0% - 50%0902_SD001_030717 ES1716547-025

EP068A: Organochlorine Pesticides (OC) (QC Lot: 982037)

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit0902_SD001_030717 ES1716547-025

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068B: Organophosphorus Pesticides (OP) (QC Lot: 982037)

EP068: Dichlorvos 62-73-7 0.05 mg/kg <0.05 <0.05 0.00 No Limit0902_SD001_030717 ES1716547-025

EP068: Demeton-S-methyl 919-86-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Dimethoate 60-51-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Diazinon 333-41-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Chlorpyrifos-methyl 5598-13-0 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Malathion 121-75-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Fenthion 55-38-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP068B: Organophosphorus Pesticides (OP) (QC Lot: 982037) - continued

EP068: Chlorpyrifos 2921-88-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit0902_SD001_030717 ES1716547-025

EP068: Pirimphos-ethyl 23505-41-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Chlorfenvinphos 470-90-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Bromophos-ethyl 4824-78-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Fenamiphos 22224-92-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Prothiofos 34643-46-4 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Ethion 563-12-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Carbophenothion 786-19-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Azinphos Methyl 86-50-0 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Monocrotophos 6923-22-4 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Parathion-methyl 298-00-0 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Parathion 56-38-2 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 982474)

EP074: Styrene 100-42-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: Isopropylbenzene 98-82-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 982474)

EP074: Vinyl Acetate 108-05-4 5 mg/kg <5 <5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: 2-Butanone (MEK) 78-93-3 5 mg/kg <5 <5 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 5 mg/kg <5 <5 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 5 mg/kg <5 <5 0.00 No Limit

EP074C: Sulfonated Compounds (QC Lot: 982474)

EP074: Carbon disulfide 75-15-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074D: Fumigants (QC Lot: 982474)

EP074: 2.2-Dichloropropane 594-20-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: 1.2-Dichloropropane 78-87-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 982474)

EP074: 1.1-Dichloroethene 75-35-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: Iodomethane 74-88-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 982474) - continued

EP074: 1.1-Dichloroethane 75-34-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: cis-1.2-Dichloroethene 156-59-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Trichloroethene 79-01-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Dibromomethane 74-95-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 5 mg/kg <5 <5 0.00 No Limit

EP074: Chloromethane 74-87-3 5 mg/kg <5 <5 0.00 No Limit

EP074: Vinyl chloride 75-01-4 5 mg/kg <5 <5 0.00 No Limit

EP074: Bromomethane 74-83-9 5 mg/kg <5 <5 0.00 No Limit

EP074: Chloroethane 75-00-3 5 mg/kg <5 <5 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 5 mg/kg <5 <5 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 982474)

EP074: Chlorobenzene 108-90-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: Bromobenzene 108-86-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 982474)

EP074: Chloroform 67-66-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP074: Bromodichloromethane 75-27-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP074: Bromoform 75-25-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 982035)

EP075(SIM): Naphthalene 91-20-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075(SIM): Acenaphthylene 208-96-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Acenaphthene 83-32-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Fluorene 86-73-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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60547028, TASK 3.1:Project

Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 982035) - continued

EP075(SIM): Phenanthrene 85-01-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075(SIM): Anthracene 120-12-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Fluoranthene 206-44-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Pyrene 129-00-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benz(a)anthracene 56-55-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Chrysene 218-01-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(k)fluoranthene 207-08-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Sum of polycyclic aromatic

hydrocarbons

---- 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(a)pyrene TEQ (zero) ---- 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075A: Phenolic Compounds (QC Lot: 982036)

EP075: Phenol 108-95-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: 2-Chlorophenol 95-57-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2-Methylphenol 95-48-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 3- & 4-Methylphenol 1319-77-3 0.5 mg/kg <0.6 <0.6 0.00 No Limit

EP075: 2-Nitrophenol 88-75-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.4-Dimethylphenol 105-67-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.4-Dichlorophenol 120-83-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.6-Dichlorophenol 87-65-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Chloro-3-methylphenol 59-50-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.4.6-Trichlorophenol 88-06-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.4.5-Trichlorophenol 95-95-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Pentachlorophenol 87-86-5 1 mg/kg <1 <1 0.00 No Limit

EP075B: Polynuclear Aromatic Hydrocarbons (QC Lot: 982036)

EP075: 2-Methylnaphthalene 91-57-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: 2-Chloronaphthalene 91-58-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-2-Fluorenyl Acetamide 53-96-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 3-Methylcholanthrene 56-49-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075C: Phthalate Esters (QC Lot: 982036)

EP075: Dimethyl phthalate 131-11-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: Diethyl phthalate 84-66-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Di-n-butyl phthalate 84-74-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Butyl benzyl phthalate 85-68-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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AECOM Australia Pty Ltd

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP075C: Phthalate Esters (QC Lot: 982036) - continued

EP075: Di-n-octylphthalate 117-84-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075D: Nitrosamines (QC Lot: 982036)

EP075: N-Nitrosomethylethylamine 10595-95-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: N-Nitrosodiethylamine 55-18-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-Nitrosopyrrolidine 930-55-2 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: N-Nitrosomorpholine 59-89-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-Nitrosodi-n-propylamine 621-64-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-Nitrosopiperidine 100-75-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-Nitrosodibutylamine 924-16-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: Methapyrilene 91-80-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075E: Nitroaromatics and Ketones (QC Lot: 982036)

EP075: 2-Picoline 109-06-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: Acetophenone 98-86-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Nitrobenzene 98-95-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Isophorone 78-59-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2.6-Dinitrotoluene 606-20-2 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: 2.4-Dinitrotoluene 121-14-2 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: 1-Naphthylamine 134-32-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Nitroquinoline-N-oxide 56-57-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 5-Nitro-o-toluidine 99-55-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 1.3.5-Trinitrobenzene 99-35-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Phenacetin 62-44-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Aminobiphenyl 92-67-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Pentachloronitrobenzene 82-68-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Pronamide 23950-58-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Dimethylaminoazobenzene 60-11-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Chlorobenzilate 510-15-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Azobenzene 103-33-3 1 mg/kg <1 <1 0.00 No Limit

EP075F: Haloethers (QC Lot: 982036)

EP075: Bis(2-chloroethyl) ether 111-44-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: Bis(2-chloroethoxy) methane 111-91-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Bromophenyl phenyl ether 101-55-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075G: Chlorinated Hydrocarbons (QC Lot: 982036)

EP075: 1.3-Dichlorobenzene 541-73-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: 1.4-Dichlorobenzene 106-46-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 1.2-Dichlorobenzene 95-50-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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AECOM Australia Pty Ltd

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP075G: Chlorinated Hydrocarbons (QC Lot: 982036) - continued

EP075: Hexachloroethane 67-72-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: 1.2.4-Trichlorobenzene 120-82-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Hexachloropropylene 1888-71-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Hexachlorobutadiene 87-68-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Hexachlorocyclopentadiene 77-47-4 0.5 mg/kg <2.5 <2.5 0.00 No Limit

EP075: Pentachlorobenzene 608-93-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Hexachlorobenzene (HCB) 118-74-1 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075H: Anilines and Benzidines (QC Lot: 982036)

EP075: Aniline 62-53-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: 4-Chloroaniline 106-47-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 2-Nitroaniline 88-74-4 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: 3-Nitroaniline 99-09-2 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075: Dibenzofuran 132-64-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4-Nitroaniline 100-01-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Carbazole 86-74-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 3.3`-Dichlorobenzidine 91-94-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075I: Organochlorine Pesticides (QC Lot: 982036)

EP075: alpha-BHC 319-84-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: beta-BHC 319-85-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: gamma-BHC 58-89-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: delta-BHC 319-86-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Heptachlor 76-44-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Aldrin 309-00-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Heptachlor epoxide 1024-57-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: alpha-Endosulfan 959-98-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4.4`-DDE 72-55-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Dieldrin 60-57-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Endrin 72-20-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: beta-Endosulfan 33213-65-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4.4`-DDD 72-54-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Endosulfan sulfate 1031-07-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: 4.4`-DDT 50-29-3 0.5 mg/kg <1.0 <1.0 0.00 No Limit

EP075J: Organophosphorus Pesticides (QC Lot: 982036)

EP075: Dichlorvos 62-73-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: Dimethoate 60-51-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Diazinon 333-41-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Chlorpyrifos-methyl 5598-13-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Malathion 121-75-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Fenthion 55-38-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Chlorpyrifos 2921-88-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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AECOM Australia Pty Ltd

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP075J: Organophosphorus Pesticides (QC Lot: 982036) - continued

EP075: Pirimphos-ethyl 23505-41-1 0.5 mg/kg <0.5 <0.5 0.00 No Limit0902_SD001_030717 ES1716547-025

EP075: Chlorfenvinphos 470-90-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Prothiofos 34643-46-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075: Ethion 563-12-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 982034)

EP071: C15 - C28 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit0902_SD001_030717 ES1716547-025

EP071: C29 - C36 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit

EP071: C10 - C14 Fraction ---- 50 mg/kg <50 <50 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 982473)

EP080: C6 - C9 Fraction ---- 10 mg/kg <10 <10 0.00 No Limit0902_SD001_030717 ES1716547-025

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 982034)

EP071: >C16 - C34 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit0902_SD001_030717 ES1716547-025

EP071: >C34 - C40 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit

EP071: >C10 - C16 Fraction ---- 50 mg/kg <50 <50 0.00 No Limit

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 982473)

EP080: C6 - C10 Fraction C6_C10 10 mg/kg <10 <10 0.00 No Limit0902_SD001_030717 ES1716547-025

EP080: BTEXN (QC Lot: 982473)

EP080: Benzene 71-43-2 0.2 mg/kg <0.2 <0.2 0.00 No Limit0902_SD001_030717 ES1716547-025

EP080: Toluene 108-88-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: Ethylbenzene 100-41-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: ortho-Xylene 95-47-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: Naphthalene 91-20-3 1 mg/kg <1 <1 0.00 No Limit

EP116: 1.4-Dioxane (QC Lot: 994104)

EP116: 1.4-Dioxane 123-91-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit0902_SD001_030717 ES1716547-025

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 982302)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0003 0.0003 0.00 No Limit0902_SD001_030717 ES1716547-025

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0005 0.0004 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0175 0.0153 13.6 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0052 0.0050 3.50 0% - 20%

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 2.05 2.41 16.0 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0329 0.0333 1.13 0% - 20%

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg 0.0003 <0.0002 0.00 No Limit0902_SD011_040717 ES1716547-035

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0005 0.0007 44.0 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.0479 0.0502 4.59 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.0068 0.0081 17.6 0% - 20%

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 0.722 0.819 12.6 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.0060 0.0063 4.03 0% - 20%

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AECOM Australia Pty Ltd

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 982303)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0100 <0.0100 0.00 No Limit0902_QC108_030717 ES1716547-045

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg 0.0135 0.0135 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg 0.671 0.785 15.7 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg 0.183 0.204 10.8 0% - 20%

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg 38.9 42.6 9.11 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg 0.318 0.306 3.85 0% - 20%

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982302)

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0032 0.0031 6.05 0% - 50%0902_SD001_030717 ES1716547-025

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0139 0.0122 13.2 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0071 0.0061 14.3 0% - 20%

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0348 0.0322 7.86 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.228 0.194 16.3 0% - 20%

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 1.12 1.08 2.76 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg 1.03 1.03 0.118 0% - 20%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg 0.150 0.179 17.7 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg 0.0121 0.0144 17.3 0% - 20%

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg 0.0031 0.0033 6.42 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg 0.002 0.002 0.00 No Limit

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit0902_SD011_040717 ES1716547-035

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.0057 0.0069 18.9 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.0014 0.0017 19.2 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.0066 0.0076 14.0 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 0.0042 0.0050 16.5 0% - 20%

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 0.0041 0.0040 3.82 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg 0.0085 0.0098 14.2 0% - 20%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg 0.0152 0.0162 6.50 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg 0.0078 0.0094 17.9 0% - 20%

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg 0.0063 0.0077 19.3 0% - 50%

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 <0.001 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982303)

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg 0.0135 0.0105 25.0 No Limit0902_QC108_030717 ES1716547-045

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg 0.508 0.432 16.0 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg 0.105 0.0991 5.88 0% - 50%

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg 0.634 0.623 1.67 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg 3.25 3.64 11.2 0% - 20%

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg 22.9 26.9 16.1 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg 8.38 10.2 19.4 0% - 20%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg 4.46 4.36 2.08 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg 0.631 0.751 17.4 0% - 20%

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg 0.249 0.291 15.6 0% - 50%

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982303) - continued

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.010 <0.010 0.00 No Limit0902_QC108_030717 ES1716547-045

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982302)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0104 0.0098 6.27 0% - 20%0902_SD001_030717 ES1716547-025

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.0106 0.0106 0.00 0% - 20%0902_SD011_040717 ES1716547-035

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 <0.0002 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982303)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg 0.527 0.556 5.27 0% - 20%0902_QC108_030717 ES1716547-045

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0100 <0.0100 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0100 <0.0100 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.0005 mg/kg <0.0250 <0.0250 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.0005 mg/kg <0.0250 <0.0250 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.0005 mg/kg <0.0250 <0.0250 0.00 No Limit

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Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982303) - continued

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.0005 mg/kg <0.0250 <0.0250 0.00 No Limit0902_QC108_030717 ES1716547-045

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 982302)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0902_SD001_030717 ES1716547-025

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.0005 mg/kg 0.508 0.464 9.04 0% - 20%

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.0005 mg/kg 4.73 4.80 1.61 0% - 20%

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.0005 mg/kg 0.0390 0.0452 14.7 0% - 20%

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.0005 mg/kg <0.0005 <0.0005 0.00 No Limit0902_SD011_040717 ES1716547-035

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.0005 mg/kg 0.0040 0.0043 7.19 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.0005 mg/kg 0.0463 0.0413 11.3 0% - 20%

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.0005 mg/kg 0.0065 0.0076 14.8 0% - 50%

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 982303)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.0005 mg/kg <0.0100 <0.0100 0.00 No Limit0902_QC108_030717 ES1716547-045

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.0005 mg/kg 11.0 10.7 2.69 0% - 20%

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.0005 mg/kg 57.7 70.1 19.3 0% - 20%

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.0005 mg/kg 0.497 0.571 13.8 0% - 20%

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 986859)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 184 178 3.59 0% - 50%0902_SW001_030717 ES1716547-001

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 512 538 5.04 0% - 20%Anonymous ES1716548-006

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 989653)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 3970 4170 5.01 0% - 20%Anonymous ES1716513-001

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 410 369 10.4 0% - 20%Anonymous ES1716621-003

ED037P: Alkalinity by PC Titrator (QC Lot: 983666)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_SW009_030717 ES1716547-009

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 62 61 2.30 0% - 20%

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Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

ED037P: Alkalinity by PC Titrator (QC Lot: 983666) - continued

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 62 61 2.30 0% - 20%0902_SW009_030717 ES1716547-009

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716462-026

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 6 5 0.00 No Limit

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 6 5 0.00 No Limit

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 983201)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 120 120 0.00 0% - 20%Anonymous ES1716411-001

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716411-010

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 983211)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 169 168 0.00 0% - 20%Anonymous ES1716366-001

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 21 21 0.00 0% - 20%0902_SW001_030717 ES1716547-001

ED045G: Chloride by Discrete Analyser (QC Lot: 983203)

ED045G: Chloride 16887-00-6 1 mg/L 950 947 0.326 0% - 20%Anonymous ES1716411-001

ED045G: Chloride 16887-00-6 1 mg/L 4 4 0.00 No LimitAnonymous ES1716411-010

ED045G: Chloride by Discrete Analyser (QC Lot: 983212)

ED045G: Chloride 16887-00-6 1 mg/L 1460 1460 0.361 0% - 20%Anonymous ES1716366-001

ED045G: Chloride 16887-00-6 1 mg/L 43 42 0.00 0% - 20%0902_SW001_030717 ES1716547-001

ED093F: Dissolved Major Cations (QC Lot: 985858)

ED093F: Calcium 7440-70-2 1 mg/L 20 20 0.00 0% - 50%Anonymous ES1716548-005

ED093F: Magnesium 7439-95-4 1 mg/L 12 14 11.6 0% - 50%

ED093F: Sodium 7440-23-5 1 mg/L 208 209 0.00 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L <1 <1 0.00 No Limit

ED093F: Calcium 7440-70-2 1 mg/L 9 9 0.00 No Limit0902_SW001_030717 ES1716547-001

ED093F: Magnesium 7439-95-4 1 mg/L 6 6 0.00 No Limit

ED093F: Sodium 7440-23-5 1 mg/L 38 36 6.23 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 2 2 0.00 No Limit

EG020F: Dissolved Metals by ICP-MS (QC Lot: 985856)

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No LimitAnonymous ES1716548-003

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L 0.001 0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.895 0.892 0.340 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.005 0.005 0.00 No Limit

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 <0.005 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.06 0.08 22.6 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L 0.07 0.07 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L 3.6 3.6 0.00 0% - 20%

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L 0.0003 0.0004 0.00 No Limit0902_SW001_030717 ES1716547-001

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Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EG020F: Dissolved Metals by ICP-MS (QC Lot: 985856) - continued

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit0902_SW001_030717 ES1716547-001

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L 0.003 0.003 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.008 0.007 0.00 No Limit

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.046 0.046 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.04 0.04 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 <0.05 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 <0.1 0.00 No Limit

EG035F: Dissolved Mercury by FIMS (QC Lot: 985857)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_SW009_030717 ES1716547-009

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No LimitAnonymous ES1716548-002

EK040P: Fluoride by PC Titrator (QC Lot: 983665)

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.4 0.4 0.00 No Limit0902_SW009_030717 ES1716547-009

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 <0.1 0.00 No LimitAnonymous ES1716462-026

EK055G: Ammonia as N by Discrete Analyser (QC Lot: 983425)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L 0.12 0.11 0.00 0% - 50%Anonymous ES1716518-001

EK057G: Nitrite as N by Discrete Analyser (QC Lot: 983204)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 <0.01 0.00 No LimitAnonymous ES1716552-001

EK057G: Nitrite as N 14797-65-0 0.01 mg/L 0.01 0.01 0.00 No LimitAnonymous ES1716552-011

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QC Lot: 983424)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L 5.08 5.10 0.406 0% - 20%Anonymous ES1716525-003

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L 0.81 0.79 2.27 0% - 20%Anonymous ES1716518-001

EK071G: Reactive Phosphorus as P by discrete analyser (QC Lot: 983200)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L 0.04 0.04 0.00 No LimitAnonymous ES1716411-001

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 <0.01 0.00 No LimitAnonymous ES1716411-010

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 983654)

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

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Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 983654) - continued

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 983654)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No LimitAnonymous ES1716548-024

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074C: Sulfonated Compounds (QC Lot: 983654)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074D: Fumigants (QC Lot: 983654)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654)

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

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Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654) - continued

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654) - continued

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No LimitAnonymous ES1716548-024

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 983654)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 983654)

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716548-024

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 983653)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_SW001_030717 ES1716547-001

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716548-024

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 990274)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous EP1707181-009

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716411-010

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 983653)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_SW001_030717 ES1716547-001

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716548-024

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 990274)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous EP1707181-009

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716411-010

EP080: BTEXN (QC Lot: 983653)

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP080: BTEXN (QC Lot: 983653) - continued

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_SW001_030717 ES1716547-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716548-024

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: BTEXN (QC Lot: 990274)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous EP1707181-009

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716411-010

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP116: 1.4-Dioxane (QC Lot: 984491)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_SW001_030717 ES1716547-001

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <1.0 <1.0 0.00 No LimitAnonymous ES1716548-023

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 982334)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 10.3 9.27 10.8 0% - 20%0902_SW001_030717 ES1716547-001

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.52 0.55 6.36 0% - 20%

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.43 0.43 0.00 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.78 0.90 13.4 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.18 0.24 26.7 0% - 50%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 16.0 15.9 0.251 0% - 20%0902_SW011_040717 ES1716547-011

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 982334) - continued

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.77 0.93 19.3 0% - 20%0902_SW011_040717 ES1716547-011

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.74 0.77 4.52 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 6.28 6.43 2.36 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.46 0.45 2.20 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 982335)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 10.6 12.0 12.4 0% - 20%0902_QC107_030717 ES1716547-021

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.87 0.86 1.38 0% - 20%

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.71 0.72 0.00 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 1.17 1.19 1.86 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.21 0.28 28.6 0% - 50%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L 0.23 0.19 15.8 0% - 50%

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982334)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 9.02 10.0 10.7 0% - 20%0902_SW001_030717 ES1716547-001

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 7.62 8.26 8.13 0% - 20%

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 50.6 48.9 3.52 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 3.93 4.36 10.2 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L 9.00 9.07 0.741 0% - 20%

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L 9.37 8.62 8.30 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L 1.19 1.05 12.3 0% - 20%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L 1.22 1.33 8.63 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L 4.8 5.6 15.6 0% - 20%

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.53 0.62 17.0 0% - 20%0902_SW011_040717 ES1716547-011

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.27 0.34 21.8 0% - 50%

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 1.17 1.40 17.5 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.24 0.27 13.3 0% - 50%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L 0.02 0.03 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982335)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 10.1 11.7 14.8 0% - 20%0902_QC107_030717 ES1716547-021

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 8.90 10.4 15.8 0% - 20%

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 53.5 62.1 14.9 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 2.31 2.24 2.98 0% - 20%

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 982335) - continued

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L 7.49 8.91 17.3 0% - 20%0902_QC107_030717 ES1716547-021

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L 7.79 8.70 11.0 0% - 20%

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L 1.14 1.18 3.45 0% - 20%

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L 1.50 1.50 0.00 0% - 20%

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L 0.02 0.03 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L 3.2 3.4 6.39 0% - 20%

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982334)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L 0.07 0.14 68.0 No Limit0902_SW001_030717 ES1716547-001

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L 0.03 0.03 0.00 No Limit0902_SW011_040717 ES1716547-011

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982335)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L 0.53 0.47 11.0 0% - 20%0902_QC107_030717 ES1716547-021

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 982335) - continued

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_QC107_030717 ES1716547-021

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 982334)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L 0.13 0.14 13.3 No Limit0902_SW001_030717 ES1716547-001

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L 712 720 1.16 0% - 20%

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L 25.6 23.5 8.88 0% - 20%

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L 0.20 0.29 36.6 No Limit

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_SW011_040717 ES1716547-011

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L 0.72 0.94 25.9 0% - 50%

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L 0.07 0.09 15.0 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 982335)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L 0.61 0.60 1.65 0% - 50%0902_QC107_030717 ES1716547-021

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L 477 569 17.6 0% - 20%

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L 16.4 18.2 10.2 0% - 20%

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L 0.14 0.10 30.7 No Limit

EP231P: PFAS Sums (QC Lot: 982334)

EP231X: Sum of PFAS ---- 0.01 µg/L 847 853 0.670 0% - 20%0902_SW001_030717 ES1716547-001

EP231X: Sum of PFAS ---- 0.01 µg/L 27.3 28.2 3.24 0% - 20%0902_SW011_040717 ES1716547-011

EP231P: PFAS Sums (QC Lot: 982335)

EP231X: Sum of PFAS ---- 0.01 µg/L 604 714 16.6 0% - 20%0902_QC107_030717 ES1716547-021

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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: SOIL Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

ED007: Exchangeable Cations (QCLot: 991755)

ED007: Exchangeable Calcium ---- 0.1 meq/100g <0.1 95.31 meq/100g 12276

ED007: Exchangeable Magnesium ---- 0.1 meq/100g <0.1 94.41.67 meq/100g 11876

ED007: Exchangeable Potassium ---- 0.1 meq/100g <0.1 1070.51 meq/100g 12080

ED007: Exchangeable Sodium ---- 0.1 meq/100g <0.1 1070.87 meq/100g 12080

ED007: Cation Exchange Capacity ---- 0.1 meq/100g <0.1 -------- --------

EG005T: Total Metals by ICP-AES (QCLot: 987748)

EG005T: Arsenic 7440-38-2 5 mg/kg <5 92.521.7 mg/kg 12686

EG005T: Cadmium 7440-43-9 1 mg/kg <1 89.24.64 mg/kg 11383

EG005T: Chromium 7440-47-3 2 mg/kg <2 86.743.9 mg/kg 12876

EG005T: Copper 7440-50-8 5 mg/kg <5 98.932 mg/kg 12086

EG005T: Iron 7439-89-6 50 mg/kg <50 74.28400 mg/kg 13070

EG005T: Lead 7439-92-1 5 mg/kg <5 86.540 mg/kg 11480

EG005T: Nickel 7440-02-0 2 mg/kg <2 91.655 mg/kg 12387

EG005T: Zinc 7440-66-6 5 mg/kg <5 91.360.8 mg/kg 12280

EG035T: Total Recoverable Mercury by FIMS (QCLot: 987747)

EG035T: Mercury 7439-97-6 0.1 mg/kg <0.1 81.42.57 mg/kg 10570

EP003: Total Organic Carbon (TOC) in Soil (QCLot: 989620)

EP003: Total Organic Carbon ---- 0.02 % <0.02 109100 % 13070

EP068A: Organochlorine Pesticides (OC) (QCLot: 982037)

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 78.80.5 mg/kg 11369

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 76.40.5 mg/kg 11765

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 83.40.5 mg/kg 11967

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 81.30.5 mg/kg 11668

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 81.40.5 mg/kg 11765

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 84.80.5 mg/kg 11567

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 83.70.5 mg/kg 11569

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 82.30.5 mg/kg 11862

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 83.90.5 mg/kg 11763

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 82.80.5 mg/kg 11666

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 82.60.5 mg/kg 11664

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 80.20.5 mg/kg 11666

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 75.60.5 mg/kg 11567

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 80.60.5 mg/kg 12367

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 82.50.5 mg/kg 11569

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP068A: Organochlorine Pesticides (OC) (QCLot: 982037) - continued

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 81.70.5 mg/kg 12169

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 99.60.5 mg/kg 12056

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 87.20.5 mg/kg 12462

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 88.00.5 mg/kg 12066

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 84.40.5 mg/kg 12264

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 87.40.5 mg/kg 13054

EP068B: Organophosphorus Pesticides (OP) (QCLot: 982037)

EP068: Dichlorvos 62-73-7 0.05 mg/kg <0.05 97.70.5 mg/kg 11959

EP068: Demeton-S-methyl 919-86-8 0.05 mg/kg <0.05 86.50.5 mg/kg 12862

EP068: Monocrotophos 6923-22-4 0.2 mg/kg <0.2 1020.5 mg/kg 12654

EP068: Dimethoate 60-51-5 0.05 mg/kg <0.05 83.00.5 mg/kg 11967

EP068: Diazinon 333-41-5 0.05 mg/kg <0.05 82.80.5 mg/kg 12070

EP068: Chlorpyrifos-methyl 5598-13-0 0.05 mg/kg <0.05 78.10.5 mg/kg 12072

EP068: Parathion-methyl 298-00-0 0.2 mg/kg <0.2 87.70.5 mg/kg 12068

EP068: Malathion 121-75-5 0.05 mg/kg <0.05 87.40.5 mg/kg 12268

EP068: Fenthion 55-38-9 0.05 mg/kg <0.05 89.20.5 mg/kg 11769

EP068: Chlorpyrifos 2921-88-2 0.05 mg/kg <0.05 83.80.5 mg/kg 11876

EP068: Parathion 56-38-2 0.2 mg/kg <0.2 85.20.5 mg/kg 12264

EP068: Pirimphos-ethyl 23505-41-1 0.05 mg/kg <0.05 87.10.5 mg/kg 11670

EP068: Chlorfenvinphos 470-90-6 0.05 mg/kg <0.05 83.00.5 mg/kg 12169

EP068: Bromophos-ethyl 4824-78-6 0.05 mg/kg <0.05 88.30.5 mg/kg 11866

EP068: Fenamiphos 22224-92-6 0.05 mg/kg <0.05 1030.5 mg/kg 12468

EP068: Prothiofos 34643-46-4 0.05 mg/kg <0.05 80.20.5 mg/kg 11262

EP068: Ethion 563-12-2 0.05 mg/kg <0.05 83.60.5 mg/kg 12068

EP068: Carbophenothion 786-19-6 0.05 mg/kg <0.05 85.30.5 mg/kg 12765

EP068: Azinphos Methyl 86-50-0 0.05 mg/kg <0.05 1080.5 mg/kg 12341

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 982474)

EP074: Styrene 100-42-5 0.5 mg/kg <0.5 93.81 mg/kg 11367

EP074: Isopropylbenzene 98-82-8 0.5 mg/kg <0.5 89.81 mg/kg 11765

EP074: n-Propylbenzene 103-65-1 0.5 mg/kg <0.5 86.61 mg/kg 12266

EP074: 1.3.5-Trimethylbenzene 108-67-8 0.5 mg/kg <0.5 89.71 mg/kg 11868

EP074: sec-Butylbenzene 135-98-8 0.5 mg/kg <0.5 87.81 mg/kg 11969

EP074: 1.2.4-Trimethylbenzene 95-63-6 0.5 mg/kg <0.5 91.01 mg/kg 11769

EP074: tert-Butylbenzene 98-06-6 0.5 mg/kg <0.5 91.21 mg/kg 11569

EP074: p-Isopropyltoluene 99-87-6 0.5 mg/kg <0.5 86.91 mg/kg 11866

EP074: n-Butylbenzene 104-51-8 0.5 mg/kg <0.5 85.11 mg/kg 12559

EP074B: Oxygenated Compounds (QCLot: 982474)

EP074: Vinyl Acetate 108-05-4 5 mg/kg <5 63.910 mg/kg 15630

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074B: Oxygenated Compounds (QCLot: 982474) - continued

EP074: 2-Butanone (MEK) 78-93-3 5 mg/kg <5 93.910 mg/kg 13658

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 5 mg/kg <5 10010 mg/kg 13262

EP074: 2-Hexanone (MBK) 591-78-6 5 mg/kg <5 97.510 mg/kg 13654

EP074C: Sulfonated Compounds (QCLot: 982474)

EP074: Carbon disulfide 75-15-0 0.5 mg/kg <0.5 74.51 mg/kg 12654

EP074D: Fumigants (QCLot: 982474)

EP074: 2.2-Dichloropropane 594-20-7 0.5 mg/kg <0.5 80.11 mg/kg 12660

EP074: 1.2-Dichloropropane 78-87-5 0.5 mg/kg <0.5 95.01 mg/kg 12468

EP074: cis-1.3-Dichloropropylene 10061-01-5 0.5 mg/kg <0.5 95.91 mg/kg 11951

EP074: trans-1.3-Dichloropropylene 10061-02-6 0.5 mg/kg <0.5 95.41 mg/kg 11452

EP074: 1.2-Dibromoethane (EDB) 106-93-4 0.5 mg/kg <0.5 97.31 mg/kg 11563

EP074E: Halogenated Aliphatic Compounds (QCLot: 982474)

EP074: Dichlorodifluoromethane 75-71-8 5 mg/kg <5 50.610 mg/kg 14830

EP074: Chloromethane 74-87-3 5 mg/kg <5 67.310 mg/kg 14141

EP074: Vinyl chloride 75-01-4 5 mg/kg <5 71.810 mg/kg 14743

EP074: Bromomethane 74-83-9 5 mg/kg <5 76.310 mg/kg 14147

EP074: Chloroethane 75-00-3 5 mg/kg <5 80.210 mg/kg 14349

EP074: Trichlorofluoromethane 75-69-4 5 mg/kg <5 74.710 mg/kg 13549

EP074: 1.1-Dichloroethene 75-35-4 0.5 mg/kg <0.5 80.31 mg/kg 12654

EP074: Iodomethane 74-88-4 0.5 mg/kg <0.5 72.21 mg/kg 12943

EP074: trans-1.2-Dichloroethene 156-60-5 0.5 mg/kg <0.5 84.71 mg/kg 12064

EP074: 1.1-Dichloroethane 75-34-3 0.5 mg/kg <0.5 90.71 mg/kg 12567

EP074: cis-1.2-Dichloroethene 156-59-2 0.5 mg/kg <0.5 92.31 mg/kg 12169

EP074: 1.1.1-Trichloroethane 71-55-6 0.5 mg/kg <0.5 89.41 mg/kg 11765

EP074: 1.1-Dichloropropylene 563-58-6 0.5 mg/kg <0.5 86.41 mg/kg 12365

EP074: Carbon Tetrachloride 56-23-5 0.5 mg/kg <0.5 86.11 mg/kg 12559

EP074: 1.2-Dichloroethane 107-06-2 0.5 mg/kg <0.5 97.51 mg/kg 12565

EP074: Trichloroethene 79-01-6 0.5 mg/kg <0.5 87.81 mg/kg 11870

EP074: Dibromomethane 74-95-3 0.5 mg/kg <0.5 95.91 mg/kg 11868

EP074: 1.1.2-Trichloroethane 79-00-5 0.5 mg/kg <0.5 97.41 mg/kg 12664

EP074: 1.3-Dichloropropane 142-28-9 0.5 mg/kg <0.5 96.91 mg/kg 12268

EP074: Tetrachloroethene 127-18-4 0.5 mg/kg <0.5 96.51 mg/kg 14367

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 0.5 mg/kg <0.5 93.41 mg/kg 12262

EP074: trans-1.4-Dichloro-2-butene 110-57-6 0.5 mg/kg <0.5 78.51 mg/kg 12854

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 0.5 mg/kg <0.5 85.51 mg/kg 12955

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 0.5 mg/kg <0.5 97.61 mg/kg 12165

EP074: 1.2.3-Trichloropropane 96-18-4 0.5 mg/kg <0.5 97.21 mg/kg 12561

EP074: Pentachloroethane 76-01-7 0.5 mg/kg <0.5 89.51 mg/kg 13420

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074E: Halogenated Aliphatic Compounds (QCLot: 982474) - continued

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 0.5 mg/kg <0.5 90.21 mg/kg 12953

EP074F: Halogenated Aromatic Compounds (QCLot: 982474)

EP074: Chlorobenzene 108-90-7 0.5 mg/kg <0.5 95.21 mg/kg 11668

EP074: Bromobenzene 108-86-1 0.5 mg/kg <0.5 92.51 mg/kg 11470

EP074: 2-Chlorotoluene 95-49-8 0.5 mg/kg <0.5 94.51 mg/kg 12268

EP074: 4-Chlorotoluene 106-43-4 0.5 mg/kg <0.5 93.21 mg/kg 12367

EP074: 1.2.3-Trichlorobenzene 87-61-6 0.5 mg/kg <0.5 95.71 mg/kg 12252

EP074G: Trihalomethanes (QCLot: 982474)

EP074: Chloroform 67-66-3 0.5 mg/kg <0.5 92.11 mg/kg 12466

EP074: Bromodichloromethane 75-27-4 0.5 mg/kg <0.5 95.51 mg/kg 12161

EP074: Dibromochloromethane 124-48-1 0.5 mg/kg <0.5 94.01 mg/kg 12163

EP074: Bromoform 75-25-2 0.5 mg/kg <0.5 90.81 mg/kg 12660

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 982035)

EP075(SIM): Naphthalene 91-20-3 0.5 mg/kg <0.5 91.96 mg/kg 12577

EP075(SIM): Acenaphthylene 208-96-8 0.5 mg/kg <0.5 96.86 mg/kg 12472

EP075(SIM): Acenaphthene 83-32-9 0.5 mg/kg <0.5 91.76 mg/kg 12773

EP075(SIM): Fluorene 86-73-7 0.5 mg/kg <0.5 97.86 mg/kg 12672

EP075(SIM): Phenanthrene 85-01-8 0.5 mg/kg <0.5 96.36 mg/kg 12775

EP075(SIM): Anthracene 120-12-7 0.5 mg/kg <0.5 91.86 mg/kg 12777

EP075(SIM): Fluoranthene 206-44-0 0.5 mg/kg <0.5 93.96 mg/kg 12773

EP075(SIM): Pyrene 129-00-0 0.5 mg/kg <0.5 90.26 mg/kg 12874

EP075(SIM): Benz(a)anthracene 56-55-3 0.5 mg/kg <0.5 99.46 mg/kg 12369

EP075(SIM): Chrysene 218-01-9 0.5 mg/kg <0.5 94.86 mg/kg 12775

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

0.5 mg/kg <0.5 94.06 mg/kg 11668

EP075(SIM): Benzo(k)fluoranthene 207-08-9 0.5 mg/kg <0.5 97.56 mg/kg 12674

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 mg/kg <0.5 95.76 mg/kg 12670

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 0.5 mg/kg <0.5 92.76 mg/kg 12161

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 0.5 mg/kg <0.5 93.06 mg/kg 11862

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 0.5 mg/kg <0.5 92.36 mg/kg 12163

EP075A: Phenolic Compounds (QCLot: 982036)

EP075: Phenol 108-95-2 0.5 mg/kg <0.5 90.71.5 mg/kg 11464

EP075: 2-Chlorophenol 95-57-8 0.5 mg/kg <0.5 91.91.5 mg/kg 11557

EP075: 2-Methylphenol 95-48-7 0.5 mg/kg <0.5 99.31.5 mg/kg 11755

EP075: 3- & 4-Methylphenol 1319-77-3 0.5 mg/kg <0.6 94.13 mg/kg 12246

EP075: 2-Nitrophenol 88-75-5 0.5 mg/kg <0.5 83.91.5 mg/kg 11747

EP075: 2.4-Dimethylphenol 105-67-9 0.5 mg/kg <0.5 94.81.5 mg/kg 10814

EP075: 2.4-Dichlorophenol 120-83-2 0.5 mg/kg <0.5 85.31.5 mg/kg 10547

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075A: Phenolic Compounds (QCLot: 982036) - continued

EP075: 2.6-Dichlorophenol 87-65-0 0.5 mg/kg <0.5 87.31.5 mg/kg 11048

EP075: 4-Chloro-3-methylphenol 59-50-7 0.5 mg/kg <0.5 97.91.5 mg/kg 11357

EP075: 2.4.6-Trichlorophenol 88-06-2 0.5 mg/kg <0.5 77.01.5 mg/kg 10949

EP075: 2.4.5-Trichlorophenol 95-95-4 0.5 mg/kg <0.5 76.91.5 mg/kg 10749

EP075: Pentachlorophenol 87-86-5 1 mg/kg <1 26.43 mg/kg 7612

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 982036)

EP075: 2-Methylnaphthalene 91-57-6 0.5 mg/kg <0.5 90.81.5 mg/kg 11658

EP075: 2-Chloronaphthalene 91-58-7 0.5 mg/kg <0.5 92.61.5 mg/kg 11254

EP075: N-2-Fluorenyl Acetamide 53-96-3 0.5 mg/kg <0.5 1021.5 mg/kg 11458

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 0.5 mg/kg <0.5 93.81.5 mg/kg 10648

EP075: 3-Methylcholanthrene 56-49-5 0.5 mg/kg <0.5 85.21.5 mg/kg 11650

EP075C: Phthalate Esters (QCLot: 982036)

EP075: Dimethyl phthalate 131-11-3 0.5 mg/kg <0.5 92.51.5 mg/kg 11860

EP075: Diethyl phthalate 84-66-2 0.5 mg/kg <0.5 88.51.5 mg/kg 11565

EP075: Di-n-butyl phthalate 84-74-2 0.5 mg/kg <0.5 93.61.5 mg/kg 12165

EP075: Butyl benzyl phthalate 85-68-7 0.5 mg/kg <0.5 91.71.5 mg/kg 11662

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- mg/kg ---- 88.21.5 mg/kg 13369

EP075: Di-n-octylphthalate 117-84-0 0.5 mg/kg <0.5 91.91.5 mg/kg 12462

EP075D: Nitrosamines (QCLot: 982036)

EP075: N-Nitrosomethylethylamine 10595-95-6 0.5 mg/kg <0.5 52.01.5 mg/kg 12439

EP075: N-Nitrosodiethylamine 55-18-5 0.5 mg/kg <0.5 69.21.5 mg/kg 11759

EP075: N-Nitrosopyrrolidine 930-55-2 0.5 mg/kg <0.5 96.11.5 mg/kg 12553

EP075: N-Nitrosomorpholine 59-89-2 0.5 mg/kg <0.5 93.01.5 mg/kg 12165

EP075: N-Nitrosodi-n-propylamine 621-64-7 0.5 mg/kg <0.5 87.01.5 mg/kg 12359

EP075: N-Nitrosopiperidine 100-75-4 0.5 mg/kg <0.5 92.61.5 mg/kg 11557

EP075: N-Nitrosodibutylamine 924-16-3 0.5 mg/kg <0.5 91.21.5 mg/kg 11957

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

0.5 mg/kg <0.6 88.03 mg/kg 11242

EP075: Methapyrilene 91-80-5 0.5 mg/kg <0.5 72.61.5 mg/kg 12316

EP075E: Nitroaromatics and Ketones (QCLot: 982036)

EP075: 2-Picoline 109-06-8 0.5 mg/kg <0.5 63.01.5 mg/kg 12927

EP075: Acetophenone 98-86-2 0.5 mg/kg <0.5 89.41.5 mg/kg 11660

EP075: Nitrobenzene 98-95-3 0.5 mg/kg <0.5 96.81.5 mg/kg 11965

EP075: Isophorone 78-59-1 0.5 mg/kg <0.5 90.81.5 mg/kg 11662

EP075: 2.6-Dinitrotoluene 606-20-2 0.5 mg/kg <0.5 93.51.5 mg/kg 11858

EP075: 2.4-Dinitrotoluene 121-14-2 0.5 mg/kg <0.5 90.11.5 mg/kg 11559

EP075: 1-Naphthylamine 134-32-7 0.5 mg/kg <0.5 57.01.5 mg/kg 11218

EP075: 4-Nitroquinoline-N-oxide 56-57-5 0.5 mg/kg <0.5 # 94.01.5 mg/kg 8710

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075E: Nitroaromatics and Ketones (QCLot: 982036) - continued

EP075: 5-Nitro-o-toluidine 99-55-8 0.5 mg/kg <0.5 84.11.5 mg/kg 9948

EP075: Azobenzene 103-33-3 1 mg/kg <1 87.71.5 mg/kg 11862

EP075: 1.3.5-Trinitrobenzene 99-35-4 0.5 mg/kg <0.5 85.81.5 mg/kg 11436

EP075: Phenacetin 62-44-2 0.5 mg/kg <0.5 1061.5 mg/kg 11462

EP075: 4-Aminobiphenyl 92-67-1 0.5 mg/kg <0.5 71.41.5 mg/kg 10236

EP075: Pentachloronitrobenzene 82-68-8 0.5 mg/kg <0.5 81.01.5 mg/kg 11056

EP075: Pronamide 23950-58-5 0.5 mg/kg <0.5 90.81.5 mg/kg 11054

EP075: Dimethylaminoazobenzene 60-11-7 0.5 mg/kg <0.5 95.01.5 mg/kg 10848

EP075: Chlorobenzilate 510-15-6 0.5 mg/kg <0.5 95.21.5 mg/kg 11257

EP075F: Haloethers (QCLot: 982036)

EP075: Bis(2-chloroethyl) ether 111-44-4 0.5 mg/kg <0.5 88.01.5 mg/kg 12163

EP075: Bis(2-chloroethoxy) methane 111-91-1 0.5 mg/kg <0.5 88.31.5 mg/kg 11559

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 0.5 mg/kg <0.5 86.01.5 mg/kg 11258

EP075: 4-Bromophenyl phenyl ether 101-55-3 0.5 mg/kg <0.5 91.31.5 mg/kg 11058

EP075G: Chlorinated Hydrocarbons (QCLot: 982036)

EP075: 1.3-Dichlorobenzene 541-73-1 0.5 mg/kg <0.5 86.51.5 mg/kg 11258

EP075: 1.4-Dichlorobenzene 106-46-7 0.5 mg/kg <0.5 88.41.5 mg/kg 11658

EP075: 1.2-Dichlorobenzene 95-50-1 0.5 mg/kg <0.5 88.91.5 mg/kg 11557

EP075: Hexachloroethane 67-72-1 0.5 mg/kg <0.5 90.61.5 mg/kg 11654

EP075: 1.2.4-Trichlorobenzene 120-82-1 0.5 mg/kg <0.5 89.21.5 mg/kg 10863

EP075: Hexachloropropylene 1888-71-7 0.5 mg/kg <0.5 81.21.5 mg/kg 11039

EP075: Hexachlorobutadiene 87-68-3 0.5 mg/kg <0.5 88.31.5 mg/kg 11759

EP075: Hexachlorocyclopentadiene 77-47-4 0.5 mg/kg <0.5 75.81.5 mg/kg 10824

EP075: Pentachlorobenzene 608-93-5 0.5 mg/kg <0.5 89.91.5 mg/kg 10957

EP075: Hexachlorobenzene (HCB) 118-74-1 0.5 mg/kg <0.5 89.31.5 mg/kg 11159

EP075H: Anilines and Benzidines (QCLot: 982036)

EP075: Aniline 62-53-3 0.5 mg/kg <0.5 87.01.5 mg/kg 10813

EP075: 4-Chloroaniline 106-47-8 0.5 mg/kg <0.5 72.31.5 mg/kg 9921

EP075: 2-Nitroaniline 88-74-4 0.5 mg/kg <0.5 95.41.5 mg/kg 11252

EP075: 3-Nitroaniline 99-09-2 0.5 mg/kg <0.5 77.71.5 mg/kg 9432

EP075: Dibenzofuran 132-64-9 0.5 mg/kg <0.5 91.11.5 mg/kg 11060

EP075: 4-Nitroaniline 100-01-6 0.5 mg/kg <0.5 1021.5 mg/kg 11242

EP075: Carbazole 86-74-8 0.5 mg/kg <0.5 98.41.5 mg/kg 11159

EP075: 3.3`-Dichlorobenzidine 91-94-1 0.5 mg/kg <0.5 # 1351.5 mg/kg 11323

EP075I: Organochlorine Pesticides (QCLot: 982036)

EP075: alpha-BHC 319-84-6 0.5 mg/kg <0.5 86.01.5 mg/kg 11363

EP075: beta-BHC 319-85-7 0.5 mg/kg <0.5 87.21.5 mg/kg 11357

EP075: gamma-BHC 58-89-9 0.5 mg/kg <0.5 88.51.5 mg/kg 11761

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075I: Organochlorine Pesticides (QCLot: 982036) - continued

EP075: delta-BHC 319-86-8 0.5 mg/kg <0.5 91.61.5 mg/kg 11864

EP075: Heptachlor 76-44-8 0.5 mg/kg <0.5 90.31.5 mg/kg 11555

EP075: Aldrin 309-00-2 0.5 mg/kg <0.5 95.11.5 mg/kg 11561

EP075: Heptachlor epoxide 1024-57-3 0.5 mg/kg <0.5 87.51.5 mg/kg 11856

EP075: alpha-Endosulfan 959-98-8 0.5 mg/kg <0.5 85.21.5 mg/kg 12565

EP075: 4.4`-DDE 72-55-9 0.5 mg/kg <0.5 82.31.5 mg/kg 11660

EP075: Dieldrin 60-57-1 0.5 mg/kg <0.5 89.51.5 mg/kg 11864

EP075: Endrin 72-20-8 0.5 mg/kg <0.5 93.21.5 mg/kg 11753

EP075: beta-Endosulfan 33213-65-9 0.5 mg/kg <0.5 86.21.5 mg/kg 11565

EP075: 4.4`-DDD 72-54-8 0.5 mg/kg <0.5 89.41.5 mg/kg 11862

EP075: Endosulfan sulfate 1031-07-8 0.5 mg/kg <0.5 91.41.5 mg/kg 12963

EP075: 4.4`-DDT 50-29-3 0.5 mg/kg <0.5 88.21.5 mg/kg 12246

EP075J: Organophosphorus Pesticides (QCLot: 982036)

EP075: Dichlorvos 62-73-7 0.5 mg/kg <0.5 78.51.5 mg/kg 11246

EP075: Dimethoate 60-51-5 0.5 mg/kg <0.5 97.61.5 mg/kg 11963

EP075: Diazinon 333-41-5 0.5 mg/kg <0.5 87.41.5 mg/kg 13468

EP075: Chlorpyrifos-methyl 5598-13-0 0.5 mg/kg <0.5 89.01.5 mg/kg 13060

EP075: Malathion 121-75-5 0.5 mg/kg <0.5 1031.5 mg/kg 12765

EP075: Fenthion 55-38-9 0.5 mg/kg <0.5 94.71.5 mg/kg 11660

EP075: Chlorpyrifos 2921-88-2 0.5 mg/kg <0.5 87.21.5 mg/kg 11363

EP075: Pirimphos-ethyl 23505-41-1 0.5 mg/kg <0.5 89.31.5 mg/kg 11565

EP075: Chlorfenvinphos 470-90-6 0.5 mg/kg <0.5 90.11.5 mg/kg 10359

EP075: Prothiofos 34643-46-4 0.5 mg/kg <0.5 90.01.5 mg/kg 11959

EP075: Ethion 563-12-2 0.5 mg/kg <0.5 93.81.5 mg/kg 11862

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982034)

EP071: C10 - C14 Fraction ---- 50 mg/kg <50 106200 mg/kg 12975

EP071: C15 - C28 Fraction ---- 100 mg/kg <100 100300 mg/kg 13177

EP071: C29 - C36 Fraction ---- 100 mg/kg <100 98.0200 mg/kg 12971

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982473)

EP080: C6 - C9 Fraction ---- 10 mg/kg <10 99.226 mg/kg 12868

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982034)

EP071: >C10 - C16 Fraction ---- 50 mg/kg <50 100250 mg/kg 12577

EP071: >C16 - C34 Fraction ---- 100 mg/kg <100 104350 mg/kg 13874

EP071: >C34 - C40 Fraction ---- 100 mg/kg <100 97.8150 mg/kg 13163

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982473)

EP080: C6 - C10 Fraction C6_C10 10 mg/kg <10 99.631 mg/kg 12868

EP080: BTEXN (QCLot: 982473)

EP080: Benzene 71-43-2 0.2 mg/kg <0.2 1001 mg/kg 11662

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP080: BTEXN (QCLot: 982473) - continued

EP080: Toluene 108-88-3 0.5 mg/kg <0.5 98.31 mg/kg 12167

EP080: Ethylbenzene 100-41-4 0.5 mg/kg <0.5 96.91 mg/kg 11765

EP080: meta- & para-Xylene 108-38-3

106-42-3

0.5 mg/kg <0.5 96.52 mg/kg 11866

EP080: ortho-Xylene 95-47-6 0.5 mg/kg <0.5 94.31 mg/kg 12068

EP080: Naphthalene 91-20-3 1 mg/kg <1 90.91 mg/kg 11963

EP116: 1.4-Dioxane (QCLot: 994104)

EP116: 1.4-Dioxane 123-91-1 0.05 mg/kg <0.05 86.90.096 mg/kg 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982302)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 66.20.00125 mg/kg 12157

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 93.30.00125 mg/kg 12555

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 1190.00125 mg/kg 12652

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 1040.00125 mg/kg 12354

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 1180.00125 mg/kg 12755

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 1220.00125 mg/kg 12554

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982303)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.0002 mg/kg <0.0002 66.00.00125 mg/kg 12157

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.0002 mg/kg <0.0002 65.80.00125 mg/kg 12555

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.0002 mg/kg <0.0002 1140.00125 mg/kg 12652

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.0002 mg/kg <0.0002 67.00.00125 mg/kg 12354

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.0002 mg/kg <0.0002 1160.00125 mg/kg 12755

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.0002 mg/kg <0.0002 1100.00125 mg/kg 12554

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982302)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 1110.00625 mg/kg 12852

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 86.60.00125 mg/kg 12954

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 93.40.00125 mg/kg 12758

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 1020.00125 mg/kg 12857

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1180.00125 mg/kg 13460

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1150.00125 mg/kg 13063

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1220.00125 mg/kg 13055

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 1100.00125 mg/kg 13062

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 73.80.00125 mg/kg 13453

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 68.30.00125 mg/kg 12949

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 86.70.00312 mg/kg 12959

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982303)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.001 mg/kg <0.001 88.20.00625 mg/kg 12852

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.0002 mg/kg <0.0002 73.40.00125 mg/kg 12954

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.0002 mg/kg <0.0002 73.80.00125 mg/kg 12758

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982303) - continued

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.0002 mg/kg <0.0002 83.10.00125 mg/kg 12857

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.0002 mg/kg <0.0002 1090.00125 mg/kg 13460

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.0002 mg/kg <0.0002 1170.00125 mg/kg 13063

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.0002 mg/kg <0.0002 1220.00125 mg/kg 13055

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.0002 mg/kg <0.0002 79.10.00125 mg/kg 13062

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.0002 mg/kg <0.0002 68.20.00125 mg/kg 13453

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.0002 mg/kg <0.0002 1250.00125 mg/kg 12949

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.0005 mg/kg <0.0005 1180.00312 mg/kg 12959

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982302)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 1110.00125 mg/kg 13252

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1240.00312 mg/kg 12665

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 76.90.00312 mg/kg 12664

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 88.50.00312 mg/kg 12463

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 79.60.00312 mg/kg 12558

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1180.00125 mg/kg 13061

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 1130.00125 mg/kg 13055

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982303)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.0002 mg/kg <0.0002 1130.00125 mg/kg 13252

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.0005 mg/kg <0.0005 1200.00312 mg/kg 12665

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.0005 mg/kg <0.0005 90.90.00312 mg/kg 12664

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.0005 mg/kg <0.0005 94.10.00312 mg/kg 12463

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.0005 mg/kg <0.0005 83.50.00312 mg/kg 12558

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.0002 mg/kg <0.0002 1210.00125 mg/kg 13061

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.0002 mg/kg <0.0002 1070.00125 mg/kg 13055

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982302)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 93.00.00125 mg/kg 13054

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 1140.00125 mg/kg 13061

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1250.00125 mg/kg 13062

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 1150.00125 mg/kg 13060

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982303)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.0005 mg/kg <0.0005 83.10.00125 mg/kg 13054

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982303) - continued

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.0005 mg/kg <0.0005 1210.00125 mg/kg 13061

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.0005 mg/kg <0.0005 1180.00125 mg/kg 13062

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.0005 mg/kg <0.0005 1130.00125 mg/kg 13060

Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 986859)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1002000 mg/L 10987

<10 92.3293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 989653)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 93.52000 mg/L 10987

<10 91.3293 mg/L 12666

ED037P: Alkalinity by PC Titrator (QCLot: 983666)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 97.7200 mg/L 11181

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983201)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 91.825 mg/L 12282

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983211)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 90.025 mg/L 12282

ED045G: Chloride by Discrete Analyser (QCLot: 983203)

ED045G: Chloride 16887-00-6 1 mg/L <1 90.910 mg/L 12781

<1 99.61000 mg/L 12781

ED045G: Chloride by Discrete Analyser (QCLot: 983212)

ED045G: Chloride 16887-00-6 1 mg/L <1 90.710 mg/L 12781

<1 94.41000 mg/L 12781

ED093F: Dissolved Major Cations (QCLot: 985858)

ED093F: Calcium 7440-70-2 1 mg/L <1 90.850 mg/L 11480

ED093F: Magnesium 7439-95-4 1 mg/L <1 91.750 mg/L 11690

ED093F: Sodium 7440-23-5 1 mg/L <1 10250 mg/L 12082

ED093F: Potassium 7440-09-7 1 mg/L <1 10450 mg/L 11385

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856)

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 91.90.5 mg/L 11680

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 94.40.1 mg/L 11485

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 92.40.1 mg/L 11084

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 91.60.1 mg/L 11185

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 89.80.1 mg/L 11181

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 90.40.1 mg/L 11183

EG020A-F: Manganese 7439-96-5 0.001 mg/L <0.001 91.00.1 mg/L 11082

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856) - continued

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 90.60.1 mg/L 11282

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 90.60.1 mg/L 11781

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 91.80.5 mg/L 11282

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 -------- --------

EG035F: Dissolved Mercury by FIMS (QCLot: 985857)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 98.70.01 mg/L 10583

EK040P: Fluoride by PC Titrator (QCLot: 983665)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1065 mg/L 11682

EK055G: Ammonia as N by Discrete Analyser (QCLot: 983425)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L <0.01 1011 mg/L 11490

EK057G: Nitrite as N by Discrete Analyser (QCLot: 983204)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 1110.5 mg/L 11482

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 983424)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L <0.01 1020.5 mg/L 11391

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 983200)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 98.30.5 mg/L 11785

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 983654)

EP074: Styrene 100-42-5 5 µg/L <5 93.810 µg/L 11973

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 90.910 µg/L 11876

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 76.310 µg/L 11969

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 81.610 µg/L 11674

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 79.810 µg/L 11973

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 82.210 µg/L 11674

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 82.110 µg/L 11672

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 80.010 µg/L 11971

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 71.310 µg/L 12365

EP074B: Oxygenated Compounds (QCLot: 983654)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 81.4100 µg/L 13461

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 80.6100 µg/L 13074

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 97.9100 µg/L 13266

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 91.1100 µg/L 13765

EP074C: Sulfonated Compounds (QCLot: 983654)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 75.010 µg/L 12773

EP074D: Fumigants (QCLot: 983654)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 90.210 µg/L 12268

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 90.810 µg/L 11876

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 80.210 µg/L 12062

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074D: Fumigants (QCLot: 983654) - continued

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 84.310 µg/L 11460

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 98.410 µg/L 11769

EP074E: Halogenated Aliphatic Compounds (QCLot: 983654)

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 63.6100 µg/L 13861

EP074: Chloromethane 74-87-3 50 µg/L <50 80.6100 µg/L 13067

EP074: Vinyl chloride 75-01-4 50 µg/L <50 98.6100 µg/L 12969

EP074: Bromomethane 74-83-9 50 µg/L <50 109100 µg/L 14056

EP074: Chloroethane 75-00-3 50 µg/L <50 85.5100 µg/L 13961

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 88.4100 µg/L 13169

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 83.010 µg/L 12470

EP074: Iodomethane 74-88-4 5 µg/L <5 12410 µg/L 12870

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 91.210 µg/L 11874

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 93.810 µg/L 12074

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 97.010 µg/L 11977

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 93.510 µg/L 11967

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 88.910 µg/L 11973

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 83.410 µg/L 12062

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 10610 µg/L 12373

EP074: Trichloroethene 79-01-6 5 µg/L <5 95.710 µg/L 11876

EP074: Dibromomethane 74-95-3 5 µg/L <5 98.710 µg/L 11973

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 94.110 µg/L 12672

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 95.010 µg/L 12971

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 91.810 µg/L 12472

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 88.810 µg/L 11466

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 81.810 µg/L 12060

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 77.410 µg/L 12871

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 10610 µg/L 12470

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 11210 µg/L 12674

EP074: Pentachloroethane 76-01-7 5 µg/L <5 76.310 µg/L 12672

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 87.410 µg/L 13666

EP074F: Halogenated Aromatic Compounds (QCLot: 983654)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 96.710 µg/L 11779

EP074: Bromobenzene 108-86-1 5 µg/L <5 87.310 µg/L 11676

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 83.110 µg/L 11973

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 82.810 µg/L 11973

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 91.610 µg/L 12367

EP074G: Trihalomethanes (QCLot: 983654)

EP074: Chloroform 67-66-3 5 µg/L <5 10310 µg/L 12072

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074G: Trihalomethanes (QCLot: 983654) - continued

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 86.910 µg/L 11864

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 85.710 µg/L 11565

EP074: Bromoform 75-25-2 5 µg/L <5 99.210 µg/L 12674

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 982669)

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 77.05 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 78.05 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 78.15 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 79.05 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 96.05 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 1045 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 1105 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 1105 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 90.95 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 86.75 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 81.75 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 92.65 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 86.35 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 88.85 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 88.85 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 89.15 µg/L 11859

EP075A: Phenolic Compounds (QCLot: 982668)

EP075: Phenol 108-95-2 2 µg/L <2 38.65 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 62.65 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 50.55 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 48.210 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 65.05 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 57.25 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 # 61.85 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 64.35 µg/L 10862

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 67.05 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 64.05 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 62.45 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 55.610 µg/L 9513

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 982668)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 64.95 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 64.15 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 66.25 µg/L 11060

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 982668) - continued

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 75.85 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 69.15 µg/L 11060

EP075C: Phthalate Esters (QCLot: 982668)

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 73.35 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 73.15 µg/L 11167

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 74.35 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 73.15 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 82.35 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 75.15 µg/L 11562

EP075D: Nitrosamines (QCLot: 982668)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 63.85 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 # 60.65 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 50.35 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 51.25 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 70.15 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 66.95 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 82.05 µg/L 10863

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 71.310 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 61.95 µg/L 12523

EP075E: Nitroaromatics and Ketones (QCLot: 982668)

EP075: 2-Picoline 109-06-8 2 µg/L <2 # 28.75 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 # 66.05 µg/L 11268

EP075: Nitrobenzene 98-95-3 2 µg/L <2 # 63.55 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 71.85 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 69.25 µg/L 11364

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 69.65 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 74.65 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 65.95 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 71.55 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 83.35 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 82.15 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 71.05 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 75.95 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 72.85 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 76.45 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 69.55 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 70.95 µg/L 11058

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075F: Haloethers (QCLot: 982668)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 70.85 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 67.05 µg/L 11166

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 70.55 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 68.95 µg/L 10862

EP075G: Chlorinated Hydrocarbons (QCLot: 982668)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 59.85 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 59.75 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 55.35 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 59.95 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 57.85 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 64.55 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 61.25 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 58.85 µg/L 10724

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 66.85 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 69.35 µg/L 11066

EP075H: Anilines and Benzidines (QCLot: 982668)

EP075: Aniline 62-53-3 2 µg/L <2 62.35 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 65.85 µg/L 10642

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 70.75 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 67.25 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 70.85 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 67.55 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 76.55 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 87.65 µg/L 11960

EP075I: Organochlorine Pesticides (QCLot: 982668)

EP075: alpha-BHC 319-84-6 2 µg/L <2 73.25 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 81.05 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 76.65 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 78.25 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 71.35 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 73.85 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 73.25 µg/L 11850

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 74.35 µg/L 11159

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 68.25 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 78.85 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 79.05 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 76.35 µg/L 11654

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 73.15 µg/L 11555

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Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075I: Organochlorine Pesticides (QCLot: 982668) - continued

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 74.15 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 74.95 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075J: Organophosphorus Pesticides (QCLot: 982668)

EP075: Dichlorvos 62-73-7 2 µg/L <2 79.15 µg/L 11351

EP075: Dimethoate 60-51-5 2 µg/L <2 68.05 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 78.75 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 72.75 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 81.65 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 72.25 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 70.35 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 74.45 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 67.25 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 75.25 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 69.55 µg/L 11751

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982670)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 95.22000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 90.33000 µg/L 10983

EP071: C29 - C36 Fraction ---- 50 µg/L <50 89.92000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983653)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 94.4260 µg/L 12775

EP080/071: Total Petroleum Hydrocarbons (QCLot: 990274)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 97.8260 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982670)

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 91.32500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 1053500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 90.91500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983653)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 94.3310 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 990274)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 99.4310 µg/L 12775

EP080: BTEXN (QCLot: 983653)

EP080: Benzene 71-43-2 1 µg/L <1 98.010 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 92.210 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 90.210 µg/L 12070

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Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP080: BTEXN (QCLot: 983653) - continued

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 92.010 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 97.610 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 97.910 µg/L 12070

EP080: BTEXN (QCLot: 990274)

EP080: Benzene 71-43-2 1 µg/L <1 93.610 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 86.710 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 83.210 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 84.210 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 86.810 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 10610 µg/L 12070

EP116: 1.4-Dioxane (QCLot: 984491)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 10110 µg/L 11979

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982334)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 1300.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1290.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1270.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 1250.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1190.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 94.60.5 µg/L 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982335)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 1170.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1260.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1150.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 1210.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1030.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 1170.5 µg/L 13070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982334)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 87.12.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 1290.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1250.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1180.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1200.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 1160.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 1160.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 93.20.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1030.5 µg/L 13070

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982334) - continued

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 1140.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 89.61.25 µg/L 15070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982335)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 90.82.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 1110.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1150.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1180.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1090.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 1130.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 1140.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1090.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 93.40.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 93.00.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 75.91.25 µg/L 15070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982334)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1280.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 1071.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 1251.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 79.91.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 1241.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1130.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 87.40.5 µg/L 13070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982335)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1130.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 1081.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 1031.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 90.81.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 89.21.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 84.40.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 81.40.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982334)

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982334) - continued

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 1220.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 94.20.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1030.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 84.00.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982335)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 1200.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 83.80.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 94.00.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 74.00.5 µg/L 13070

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EG005T: Total Metals by ICP-AES (QCLot: 987748)

Anonymous ES1716473-006 7440-38-2EG005T: Arsenic 10150 mg/kg 13070

7440-43-9EG005T: Cadmium 90.650 mg/kg 13070

7440-47-3EG005T: Chromium 91.450 mg/kg 13070

7440-50-8EG005T: Copper 98.7250 mg/kg 13070

7439-92-1EG005T: Lead 86.8250 mg/kg 13070

7440-02-0EG005T: Nickel 87.450 mg/kg 13070

7440-66-6EG005T: Zinc 85.1250 mg/kg 13070

EG035T: Total Recoverable Mercury by FIMS (QCLot: 987747)

Anonymous ES1716473-006 7439-97-6EG035T: Mercury 99.25 mg/kg 13070

EP068A: Organochlorine Pesticides (OC) (QCLot: 982037)

0902_SD001_030717 ES1716547-025 58-89-9EP068: gamma-BHC 1000.5 mg/kg 13070

76-44-8EP068: Heptachlor 99.60.5 mg/kg 13070

309-00-2EP068: Aldrin 88.20.5 mg/kg 13070

60-57-1EP068: Dieldrin 87.40.5 mg/kg 13070

72-20-8EP068: Endrin 87.62 mg/kg 13070

50-29-3EP068: 4.4`-DDT 93.32 mg/kg 13070

EP068B: Organophosphorus Pesticides (OP) (QCLot: 982037)

0902_SD001_030717 ES1716547-025 333-41-5EP068: Diazinon 91.80.5 mg/kg 13070

5598-13-0EP068: Chlorpyrifos-methyl 1020.5 mg/kg 13070

23505-41-1EP068: Pirimphos-ethyl 94.80.5 mg/kg 13070

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Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP068B: Organophosphorus Pesticides (OP) (QCLot: 982037) - continued

0902_SD001_030717 ES1716547-025 4824-78-6EP068: Bromophos-ethyl 95.70.5 mg/kg 13070

34643-46-4EP068: Prothiofos 83.30.5 mg/kg 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 982474)

0902_SD001_030717 ES1716547-025 75-35-4EP074: 1.1-Dichloroethene 73.02.5 mg/kg 13070

79-01-6EP074: Trichloroethene 75.92.5 mg/kg 13070

EP074F: Halogenated Aromatic Compounds (QCLot: 982474)

0902_SD001_030717 ES1716547-025 108-90-7EP074: Chlorobenzene 85.12.5 mg/kg 13070

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 982035)

0902_SD001_030717 ES1716547-025 83-32-9EP075(SIM): Acenaphthene 96.510 mg/kg 13070

129-00-0EP075(SIM): Pyrene 99.010 mg/kg 13070

EP075A: Phenolic Compounds (QCLot: 982036)

0902_SD001_030717 ES1716547-025 108-95-2EP075: Phenol 89.810 mg/kg 13060

95-57-8EP075: 2-Chlorophenol 93.810 mg/kg 13060

88-75-5EP075: 2-Nitrophenol 91.110 mg/kg 13050

59-50-7EP075: 4-Chloro-3-methylphenol 95.410 mg/kg 13050

87-86-5EP075: Pentachlorophenol 48.820 mg/kg 13010

EP075D: Nitrosamines (QCLot: 982036)

0902_SD001_030717 ES1716547-025 621-64-7EP075: N-Nitrosodi-n-propylamine 85.710 mg/kg 13050

EP075E: Nitroaromatics and Ketones (QCLot: 982036)

0902_SD001_030717 ES1716547-025 121-14-2EP075: 2.4-Dinitrotoluene 94.510 mg/kg 13040

EP075G: Chlorinated Hydrocarbons (QCLot: 982036)

0902_SD001_030717 ES1716547-025 106-46-7EP075: 1.4-Dichlorobenzene 95.010 mg/kg 13060

120-82-1EP075: 1.2.4-Trichlorobenzene 98.010 mg/kg 13050

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982034)

0902_SD001_030717 ES1716547-025 ----EP071: C10 - C14 Fraction 85.9523 mg/kg 13773

----EP071: C15 - C28 Fraction 1042319 mg/kg 13153

----EP071: C29 - C36 Fraction 1171714 mg/kg 13252

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982473)

0902_SD001_030717 ES1716547-025 ----EP080: C6 - C9 Fraction 12232.5 mg/kg 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982034)

0902_SD001_030717 ES1716547-025 ----EP071: >C10 - C16 Fraction 96.6860 mg/kg 13773

----EP071: >C16 - C34 Fraction 1113223 mg/kg 13153

----EP071: >C34 - C40 Fraction 1081058 mg/kg 13252

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982473)

0902_SD001_030717 ES1716547-025 C6_C10EP080: C6 - C10 Fraction 11737.5 mg/kg 13070

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Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP080: BTEXN (QCLot: 982473)

0902_SD001_030717 ES1716547-025 71-43-2EP080: Benzene 1182.5 mg/kg 13070

108-88-3EP080: Toluene 1092.5 mg/kg 13070

100-41-4EP080: Ethylbenzene 1102.5 mg/kg 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 1082.5 mg/kg 13070

95-47-6EP080: ortho-Xylene 1062.5 mg/kg 13070

91-20-3EP080: Naphthalene 95.42.5 mg/kg 13070

EP116: 1.4-Dioxane (QCLot: 994104)

0902_SD009_030717 ES1716547-033 123-91-1EP116: 1.4-Dioxane 73.30.096 mg/kg 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982302)

0902_SD001_030717 ES1716547-025 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 69.50.00125 mg/kg 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 96.10.00125 mg/kg 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) # Not

Determined

0.00125 mg/kg 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 91.10.00125 mg/kg 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.00125 mg/kg 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) # Not

Determined

0.00125 mg/kg 13050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982302)

0902_SD001_030717 ES1716547-025 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1090.00625 mg/kg 13030

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 1090.00125 mg/kg 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.00125 mg/kg 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) # Not

Determined

0.00125 mg/kg 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) # Not

Determined

0.00125 mg/kg 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) # Not

Determined

0.00125 mg/kg 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) # Not

Determined

0.00125 mg/kg 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) # Not

Determined

0.00125 mg/kg 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) # Not

Determined

0.00125 mg/kg 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) # Not

Determined

0.00125 mg/kg 13030

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 31.90.00312 mg/kg 13030

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Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982302)

0902_SD001_030717 ES1716547-025 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) # Not

Determined

0.00125 mg/kg 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

90.70.00312 mg/kg 13030

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 54.50.00312 mg/kg 13030

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

63.70.00312 mg/kg 13030

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

55.70.00312 mg/kg 13030

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

80.00.00125 mg/kg 13030

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

95.60.00125 mg/kg 13030

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982302)

0902_SD001_030717 ES1716547-025 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 92.60.00125 mg/kg 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) # Not

Determined

0.00125 mg/kg 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) # Not

Determined

0.00125 mg/kg 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) # Not

Determined

0.00125 mg/kg 13050

Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983201)

Anonymous ES1716411-001 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric # Not

Determined

10 mg/L 13070

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983211)

Anonymous ES1716366-001 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric # Not

Determined

10 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 983203)

Anonymous ES1716411-001 16887-00-6ED045G: Chloride 74.7250 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 983212)

Anonymous ES1716366-001 16887-00-6ED045G: Chloride # Not

Determined

250 mg/L 13070

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856)

0902_SW009_030717 ES1716547-009 7440-38-2EG020A-F: Arsenic 1211 mg/L 13070

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856) - continued

0902_SW009_030717 ES1716547-009 7440-43-9EG020A-F: Cadmium 1180.25 mg/L 13070

7440-47-3EG020A-F: Chromium 1111 mg/L 13070

7440-50-8EG020A-F: Copper 1111 mg/L 13070

7439-92-1EG020A-F: Lead 1141 mg/L 13070

7439-96-5EG020A-F: Manganese 1121 mg/L 13070

7440-02-0EG020A-F: Nickel 1101 mg/L 13070

7440-66-6EG020A-F: Zinc 1221 mg/L 13070

EG035F: Dissolved Mercury by FIMS (QCLot: 985857)

0902_SW001_030717 ES1716547-001 7439-97-6EG035F: Mercury 76.50.01 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 983665)

Anonymous ES1716462-026 16984-48-8EK040P: Fluoride 89.45 mg/L 13070

EK055G: Ammonia as N by Discrete Analyser (QCLot: 983425)

Anonymous ES1716518-001 7664-41-7EK055G: Ammonia as N 96.61 mg/L 13070

EK057G: Nitrite as N by Discrete Analyser (QCLot: 983204)

Anonymous ES1716552-001 14797-65-0EK057G: Nitrite as N 1130.5 mg/L 13070

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 983424)

Anonymous ES1716518-001 ----EK059G: Nitrite + Nitrate as N 94.60.5 mg/L 13070

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 983200)

Anonymous ES1716411-001 14265-44-2EK071G: Reactive Phosphorus as P 1070.5 mg/L 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 983654)

0902_SW001_030717 ES1716547-001 75-35-4EP074: 1.1-Dichloroethene 72.225 µg/L 13070

79-01-6EP074: Trichloroethene 89.025 µg/L 13070

EP074F: Halogenated Aromatic Compounds (QCLot: 983654)

0902_SW001_030717 ES1716547-001 108-90-7EP074: Chlorobenzene 99.125 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983653)

0902_SW001_030717 ES1716547-001 ----EP080: C6 - C9 Fraction 125325 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 990274)

Anonymous EP1707181-009 ----EP080: C6 - C9 Fraction 127325 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983653)

0902_SW001_030717 ES1716547-001 C6_C10EP080: C6 - C10 Fraction 125375 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 990274)

Anonymous EP1707181-009 C6_C10EP080: C6 - C10 Fraction 124375 µg/L 13070

EP080: BTEXN (QCLot: 983653)

0902_SW001_030717 ES1716547-001 71-43-2EP080: Benzene 99.925 µg/L 13070

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP080: BTEXN (QCLot: 983653) - continued

0902_SW001_030717 ES1716547-001 108-88-3EP080: Toluene 10625 µg/L 13070

100-41-4EP080: Ethylbenzene 11725 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 11825 µg/L 13070

95-47-6EP080: ortho-Xylene 12125 µg/L 13070

91-20-3EP080: Naphthalene 10625 µg/L 13070

EP080: BTEXN (QCLot: 990274)

Anonymous EP1707181-009 71-43-2EP080: Benzene 11525 µg/L 13070

108-88-3EP080: Toluene 10225 µg/L 13070

100-41-4EP080: Ethylbenzene 10725 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 10825 µg/L 13070

95-47-6EP080: ortho-Xylene 11425 µg/L 13070

91-20-3EP080: Naphthalene 12325 µg/L 13070

EP116: 1.4-Dioxane (QCLot: 984491)

0902_SW009_030717 ES1716547-009 123-91-1EP116: 1.4-Dioxane 11010 µg/L 12080

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982334)

0902_SW001_030717 ES1716547-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1230.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1290.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 74.40.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1120.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 68.20.5 µg/L 13050

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 982335)

0902_QC107_030717 ES1716547-021 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1150.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1180.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 67.40.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 75.00.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) # 6.400.5 µg/L 13050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982334)

0902_SW001_030717 ES1716547-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1272.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) # Not

Determined

0.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.5 µg/L 13050

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982334) - continued

0902_SW001_030717 ES1716547-001 375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) # Not

Determined

0.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) # Not

Determined

0.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) # Not

Determined

0.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) # Not

Determined

0.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 67.00.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1250.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1300.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 73.41.25 µg/L 15050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 982335)

0902_QC107_030717 ES1716547-021 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 96.02.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) # Not

Determined

0.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) # Not

Determined

0.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) # Not

Determined

0.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) # Not

Determined

0.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) # Not

Determined

0.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 90.20.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) # Not

Determined

0.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 59.80.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) # 14.41.25 µg/L 15050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982334)

0902_SW001_030717 ES1716547-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1010.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

1011.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1281.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

83.81.25 µg/L 15050

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982334) - continued

0902_SW001_030717 ES1716547-001 1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1181.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

88.00.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

88.00.5 µg/L 13050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 982335)

0902_QC107_030717 ES1716547-021 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 51.20.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

1131.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 94.01.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

91.41.25 µg/L 15050

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1091.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

77.80.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

1070.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982334)

0902_SW001_030717 ES1716547-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1170.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) # Not

Determined

0.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) # Not

Determined

0.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 57.80.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 982335)

0902_QC107_030717 ES1716547-021 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1080.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) # Not

Determined

0.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) # Not

Determined

0.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 86.40.5 µg/L 13050

Page 164: Appendix - Department of Defence

True

Environmental

QA/QC Compliance Assessment to assist with Quality ReviewWork Order : ES1716547 Page : 1 of 30

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER Telephone : +61 2 8784 8503

:Project 60547028, TASK 3.1 Date Samples Received : 05-Jul-2017

Site : RAAF RICHMOND Issue Date : 17-Jul-2017

DIRK SANDERSON:Sampler No. of samples received : 45

:Order number 60547028, TASK 3.1 No. of samples analysed : 45

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l Laboratory Control outliers exist - please see following pages for full details.

l Matrix Spike outliers exist - please see following pages for full details.

l Surrogate recovery outliers exist for all regular sample matrices - please see following pages for full details.

Outliers : Analysis Holding Time Compliance

l Analysis Holding Time Outliers exist - please see following pages for full details.

Outliers : Frequency of Quality Control Samples

l Quality Control Sample Frequency Outliers exist - please see following pages for full details.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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Outliers : Quality Control Samples

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

Matrix: SOIL

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Laboratory Control Spike (LCS) Recoveries

QC-982036-002 56-57-54-Nitroquinoline-N-oxid

e

---- Recovery greater than upper control

limit

10-87%94.0 %EP075E: Nitroaromatics and Ketones

QC-982036-002 91-94-13.3`-Dichlorobenzidine---- Recovery greater than upper control

limit

23-113%135 %EP075H: Anilines and Benzidines

Matrix Spike (MS) Recoveries

ES1716547--025 355-46-4Perfluorohexane

sulfonic acid

(PFHxS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--025 1763-23-1Perfluorooctane

sulfonic acid (PFOS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--025 335-77-3Perfluorodecane

sulfonic acid (PFDS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--025 307-24-4Perfluorohexanoic acid

(PFHxA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 375-85-9Perfluoroheptanoic

acid (PFHpA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 335-67-1Perfluorooctanoic acid

(PFOA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 375-95-1Perfluorononanoic acid

(PFNA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 335-76-2Perfluorodecanoic acid

(PFDA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 2058-94-8Perfluoroundecanoic

acid (PFUnDA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 307-55-1Perfluorododecanoic

acid (PFDoDA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--025 72629-94-8Perfluorotridecanoic

acid (PFTrDA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

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Matrix: SOIL

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries - Continued

ES1716547--025 754-91-6Perfluorooctane

sulfonamide (FOSA)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231C: Perfluoroalkyl Sulfonamides

ES1716547--025 27619-97-26:2 Fluorotelomer

sulfonic acid (6:2

FTS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

ES1716547--025 39108-34-48:2 Fluorotelomer

sulfonic acid (8:2

FTS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

ES1716547--025 120226-60-010:2 Fluorotelomer

sulfonic acid (10:2

FTS)

0902_SD001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Laboratory Control Spike (LCS) Recoveries

QC-982668-002 120-83-22.4-Dichlorophenol---- Recovery less than lower control limit62-109%61.8 %EP075A: Phenolic Compounds

QC-982668-002 55-18-5N-Nitrosodiethylamine---- Recovery less than lower control limit61-113%60.6 %EP075D: Nitrosamines

QC-982668-002 109-06-82-Picoline---- Recovery less than lower control limit41-109%28.7 %EP075E: Nitroaromatics and Ketones

QC-982668-002 98-86-2Acetophenone---- Recovery less than lower control limit68-112%66.0 %EP075E: Nitroaromatics and Ketones

QC-982668-002 98-95-3Nitrobenzene---- Recovery less than lower control limit68-112%63.5 %EP075E: Nitroaromatics and Ketones

Matrix Spike (MS) Recoveries

ES1716366--001 14808-79-8Sulfate as SO4 -

Turbidimetric

Anonymous MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

ES1716411--001 14808-79-8Sulfate as SO4 -

Turbidimetric

Anonymous MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

ES1716366--001 16887-00-6ChlorideAnonymous MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED045G: Chloride by Discrete Analyser

ES1716547--001 1763-23-1Perfluorooctane

sulfonic acid (PFOS)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--021 1763-23-1Perfluorooctane

sulfonic acid (PFOS)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--021 335-77-3Perfluorodecane

sulfonic acid (PFDS)

0902_QC107_030717 Recovery less than lower data quality

objective

50-130%6.40 %EP231A: Perfluoroalkyl Sulfonic Acids

ES1716547--001 2706-90-3Perfluoropentanoic

acid (PFPeA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

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Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries - Continued

ES1716547--021 2706-90-3Perfluoropentanoic

acid (PFPeA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 307-24-4Perfluorohexanoic acid

(PFHxA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 307-24-4Perfluorohexanoic acid

(PFHxA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 375-85-9Perfluoroheptanoic

acid (PFHpA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 375-85-9Perfluoroheptanoic

acid (PFHpA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 335-67-1Perfluorooctanoic acid

(PFOA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 335-67-1Perfluorooctanoic acid

(PFOA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 375-95-1Perfluorononanoic acid

(PFNA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 375-95-1Perfluorononanoic acid

(PFNA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 335-76-2Perfluorodecanoic acid

(PFDA)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 335-76-2Perfluorodecanoic acid

(PFDA)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--021 376-06-7Perfluorotetradecanoic

acid (PFTeDA)

0902_QC107_030717 Recovery less than lower data quality

objective

50-150%14.4 %EP231B: Perfluoroalkyl Carboxylic Acids

ES1716547--001 27619-97-26:2 Fluorotelomer

sulfonic acid (6:2

FTS)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

ES1716547--021 27619-97-26:2 Fluorotelomer

sulfonic acid (6:2

FTS)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

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Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries - Continued

ES1716547--001 39108-34-48:2 Fluorotelomer

sulfonic acid (8:2

FTS)

0902_SW001_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

ES1716547--021 39108-34-48:2 Fluorotelomer

sulfonic acid (8:2

FTS)

0902_QC107_030717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231D: (n:2) Fluorotelomer Sulfonic Acids

Regular Sample Surrogates

Sub-Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Samples Submitted

ES1716547-021 93951-73-62-Chlorophenol-D40902_QC107_030717 Recovery less than lower data quality

objective

21-130 %EP075S: Acid Extractable Surrogates 16.4 %

ES1716547-021 4165-60-0Nitrobenzene-D50902_QC107_030717 Recovery less than lower data quality

objective

29-142 %EP075T: Base/Neutral Extractable Surrogates 26.9 %

ES1716547-001 321-60-82-Fluorobiphenyl0902_SW001_030717 Recovery less than lower data quality

objective

27-135 %EP075T: Base/Neutral Extractable Surrogates 23.3 %

Outliers : Analysis Holding Time Compliance

Matrix: WATER

AnalysisExtraction / Preparation

Date analysedDate extractedContainer / Client Sample ID(s) Days

overdue

Days

overdue

Due for extraction Due for analysis

Method

EK055G: Ammonia as N by Discrete Analyser

Clear Plastic Bottle - Natural

05-Jul-2017----0902_SW011_040717 06-Jul-2017---- ---- 1

Outliers : Frequency of Quality Control Samples

Matrix: SOIL

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC StandardPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS 4.76 5.001 21

Matrix: WATER

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 10.000 8

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 10.000 8

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 10.000 8

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 5.000 8

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Matrix: WATER

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Matrix Spikes (MS) - Continued

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 5.000 8

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 5.000 8

Analysis Holding Time Compliance

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.

This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA055: Moisture Content (Dried @ 105-110°C)

HDPE Soil Jar (EA055)

0902_SD008_030717, 0902_SD013_030717,

0902_SD015_030717, 0902_SD016_030717,

0902_SD017_030717, 0902_QC106_030717

17-Jul-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE Soil Jar (EA055)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD018_040717, 0902_SD019_040717

18-Jul-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

Soil Glass Jar - Unpreserved (EA055)

0902_SD001_030717, 0902_SD009_030717,

0902_SD010_030717, 0902_SD012_030717,

0902_SD014_030717, 0902_QC108_030717

17-Jul-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

Soil Glass Jar - Unpreserved (EA055)

0902_SD011_040717 18-Jul-2017---- 07-Jul-2017----04-Jul-2017 ---- üED007: Exchangeable Cations

Soil Glass Jar - Unpreserved (ED007)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

31-Jul-201731-Jul-2017 12-Jul-201712-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (ED007)

0902_SD011_040717 01-Aug-201701-Aug-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EG005T: Total Metals by ICP-AES

Soil Glass Jar - Unpreserved (EG005T)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

30-Dec-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EG005T)

0902_SD011_040717 31-Dec-201731-Dec-2017 10-Jul-201710-Jul-201704-Jul-2017 ü üEG035T: Total Recoverable Mercury by FIMS

Soil Glass Jar - Unpreserved (EG035T)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

31-Jul-201731-Jul-2017 10-Jul-201710-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EG035T)

0902_SD011_040717 01-Aug-201701-Aug-2017 10-Jul-201710-Jul-201704-Jul-2017 ü üEP003: Total Organic Carbon (TOC) in Soil

Pulp Bag (EP003)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

31-Jul-201731-Jul-2017 11-Jul-201711-Jul-201703-Jul-2017 ü ü

Pulp Bag (EP003)

0902_SD011_040717 01-Aug-201701-Aug-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üEP068A: Organochlorine Pesticides (OC)

Soil Glass Jar - Unpreserved (EP068)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP068)

0902_SD011_040717 15-Aug-201718-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP068B: Organophosphorus Pesticides (OP)

Soil Glass Jar - Unpreserved (EP068)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP068)

0902_SD011_040717 15-Aug-201718-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP074A: Monocyclic Aromatic Hydrocarbons

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü ü

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074B: Oxygenated Compounds

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP074C: Sulfonated Compounds

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP074D: Fumigants

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP074E: Halogenated Aliphatic Compounds

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP074F: Halogenated Aromatic Compounds

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP074G: Trihalomethanes

Soil Glass Jar - Unpreserved (EP074)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

10-Jul-201710-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP074)

0902_SD011_040717 11-Jul-201711-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü ü

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AECOM Australia Pty Ltd

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

Soil Glass Jar - Unpreserved (EP075(SIM))

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075(SIM))

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075A: Phenolic Compounds

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075B: Polynuclear Aromatic Hydrocarbons

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075C: Phthalate Esters

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075D: Nitrosamines

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075E: Nitroaromatics and Ketones

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü ü

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075F: Haloethers

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075G: Chlorinated Hydrocarbons

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075H: Anilines and Benzidines

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075I: Organochlorine Pesticides

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP075J: Organophosphorus Pesticides

Soil Glass Jar - Unpreserved (EP075)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP075)

0902_SD011_040717 15-Aug-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü ü

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AECOM Australia Pty Ltd

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Petroleum Hydrocarbons

Soil Glass Jar - Unpreserved (EP080)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

17-Jul-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP071)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP080)

0902_SD011_040717 18-Jul-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üSoil Glass Jar - Unpreserved (EP071)

0902_SD011_040717 15-Aug-201718-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

Soil Glass Jar - Unpreserved (EP080)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

17-Jul-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP071)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

15-Aug-201717-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP080)

0902_SD011_040717 18-Jul-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üSoil Glass Jar - Unpreserved (EP071)

0902_SD011_040717 15-Aug-201718-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP080: BTEXN

Soil Glass Jar - Unpreserved (EP080)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

17-Jul-201717-Jul-2017 06-Jul-201706-Jul-201703-Jul-2017 ü ü

Soil Glass Jar - Unpreserved (EP080)

0902_SD011_040717 18-Jul-201718-Jul-2017 06-Jul-201706-Jul-201704-Jul-2017 ü üEP116: 1.4-Dioxane

Soil Glass Jar - Unpreserved (EP116)

0902_SD001_030717, 0902_SD009_030717,

0902_SD012_030717, 0902_SD014_030717,

0902_QC108_030717

17-Jul-2017---- 13-Jul-2017----03-Jul-2017 ---- ü

Soil Glass Jar - Unpreserved (EP116)

0902_SD011_040717 18-Jul-2017---- 13-Jul-2017----04-Jul-2017 ---- ü

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AECOM Australia Pty Ltd

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231A: Perfluoroalkyl Sulfonic Acids

HDPE Soil Jar (EP231X)

0902_SD001_030717, 0902_SD008_030717,

0902_SD009_030717, 0902_SD010_030717,

0902_SD012_030717, 0902_SD013_030717,

0902_SD014_030717, 0902_SD015_030717,

0902_SD016_030717, 0902_SD017_030717,

0902_QC106_030717

16-Aug-201730-Dec-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

HDPE Soil Jar (EP231X)

0902_QC108_030717 19-Aug-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü üHDPE Soil Jar (EP231X)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD011_040717, 0902_SD018_040717,

0902_SD019_040717

16-Aug-201731-Dec-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

EP231B: Perfluoroalkyl Carboxylic Acids

HDPE Soil Jar (EP231X)

0902_SD001_030717, 0902_SD008_030717,

0902_SD009_030717, 0902_SD010_030717,

0902_SD012_030717, 0902_SD013_030717,

0902_SD014_030717, 0902_SD015_030717,

0902_SD016_030717, 0902_SD017_030717,

0902_QC106_030717

16-Aug-201730-Dec-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

HDPE Soil Jar (EP231X)

0902_QC108_030717 19-Aug-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü üHDPE Soil Jar (EP231X)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD011_040717, 0902_SD018_040717,

0902_SD019_040717

16-Aug-201731-Dec-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

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ES1716547

AECOM Australia Pty Ltd

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231C: Perfluoroalkyl Sulfonamides

HDPE Soil Jar (EP231X)

0902_SD001_030717, 0902_SD008_030717,

0902_SD009_030717, 0902_SD010_030717,

0902_SD012_030717, 0902_SD013_030717,

0902_SD014_030717, 0902_SD015_030717,

0902_SD016_030717, 0902_SD017_030717,

0902_QC106_030717

16-Aug-201730-Dec-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

HDPE Soil Jar (EP231X)

0902_QC108_030717 19-Aug-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü üHDPE Soil Jar (EP231X)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD011_040717, 0902_SD018_040717,

0902_SD019_040717

16-Aug-201731-Dec-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

EP231D: (n:2) Fluorotelomer Sulfonic Acids

HDPE Soil Jar (EP231X)

0902_SD001_030717, 0902_SD008_030717,

0902_SD009_030717, 0902_SD010_030717,

0902_SD012_030717, 0902_SD013_030717,

0902_SD014_030717, 0902_SD015_030717,

0902_SD016_030717, 0902_SD017_030717,

0902_QC106_030717

16-Aug-201730-Dec-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

HDPE Soil Jar (EP231X)

0902_QC108_030717 19-Aug-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü üHDPE Soil Jar (EP231X)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD011_040717, 0902_SD018_040717,

0902_SD019_040717

16-Aug-201731-Dec-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

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AECOM Australia Pty Ltd

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231P: PFAS Sums

HDPE Soil Jar (EP231X)

0902_SD001_030717, 0902_SD008_030717,

0902_SD009_030717, 0902_SD010_030717,

0902_SD012_030717, 0902_SD013_030717,

0902_SD014_030717, 0902_SD015_030717,

0902_SD016_030717, 0902_SD017_030717,

0902_QC106_030717

16-Aug-201730-Dec-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

HDPE Soil Jar (EP231X)

0902_QC108_030717 19-Aug-201730-Dec-2017 10-Jul-201710-Jul-201703-Jul-2017 ü üHDPE Soil Jar (EP231X)

0902_SD002_040717, 0902_SD003_040717,

0902_SD004_040717, 0902_SD005_040717,

0902_SD006_040717, 0902_SD007_040717,

0902_SD011_040717, 0902_SD018_040717,

0902_SD019_040717

16-Aug-201731-Dec-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA015: Total Dissolved Solids dried at 180 ± 5 °C

Clear Plastic Bottle - Natural (EA015H)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

10-Jul-2017---- 10-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EA015H)

0902_SW011_040717 11-Jul-2017---- 11-Jul-2017----04-Jul-2017 ---- üED037P: Alkalinity by PC Titrator

Clear Plastic Bottle - Natural (ED037-P)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

17-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED037-P)

0902_SW011_040717 18-Jul-2017---- 06-Jul-2017----04-Jul-2017 ---- üED041G: Sulfate (Turbidimetric) as SO4 2- by DA

Clear Plastic Bottle - Natural (ED041G)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED041G)

0902_SW011_040717 01-Aug-2017---- 06-Jul-2017----04-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

ED045G: Chloride by Discrete Analyser

Clear Plastic Bottle - Natural (ED045G)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED045G)

0902_SW011_040717 01-Aug-2017---- 06-Jul-2017----04-Jul-2017 ---- üED093F: Dissolved Major Cations

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

31-Jul-2017---- 08-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_SW011_040717 01-Aug-2017---- 08-Jul-2017----04-Jul-2017 ---- üEG020F: Dissolved Metals by ICP-MS

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

30-Dec-2017---- 08-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_SW011_040717, 0902_QC505_040717 31-Dec-2017---- 08-Jul-2017----04-Jul-2017 ---- üEG035F: Dissolved Mercury by FIMS

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

31-Jul-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_SW011_040717, 0902_QC505_040717 01-Aug-2017---- 11-Jul-2017----04-Jul-2017 ---- üEK040P: Fluoride by PC Titrator

Clear Plastic Bottle - Natural (EK040P)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK040P)

0902_SW011_040717 01-Aug-2017---- 06-Jul-2017----04-Jul-2017 ---- üEK055G: Ammonia as N by Discrete Analyser

Clear Plastic Bottle - Natural (EK055G)

0902_SW011_040717 05-Jul-2017---- 06-Jul-2017----04-Jul-2017 ---- ûEK057G: Nitrite as N by Discrete Analyser

Clear Plastic Bottle - Natural (EK057G)

0902_SW011_040717 06-Jul-2017---- 06-Jul-2017----04-Jul-2017 ---- ü

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AECOM Australia Pty Ltd

60547028, TASK 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

Clear Plastic Bottle - Natural (EK059G)

0902_SW011_040717 06-Jul-2017---- 06-Jul-2017----04-Jul-2017 ---- üEK071G: Reactive Phosphorus as P by discrete analyser

Clear Plastic Bottle - Natural (EK071G)

0902_SW011_040717 06-Jul-2017---- 06-Jul-2017----04-Jul-2017 ---- üEP074A: Monocyclic Aromatic Hydrocarbons

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP074B: Oxygenated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP074C: Sulfonated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP074D: Fumigants

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP074E: Halogenated Aliphatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074F: Halogenated Aromatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP074G: Trihalomethanes

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üEP075(SIM)B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075A: Phenolic Compounds

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075C: Phthalate Esters

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075D: Nitrosamines

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075E: Nitroaromatics and Ketones

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075F: Haloethers

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075G: Chlorinated Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075H: Anilines and Benzidines

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP075I: Organochlorine Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075J: Organophosphorus Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üEP080/071: Total Petroleum Hydrocarbons

Amber Glass Bottle - Unpreserved (EP071)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC506_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üEP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

Amber Glass Bottle - Unpreserved (EP071)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_SW011_040717, 0902_QC505_040717 15-Aug-201711-Jul-2017 07-Jul-201706-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC506_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080: BTEXN

Amber VOC Vial - Sulfuric Acid (EP080)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_SW011_040717, 0902_QC505_040717 18-Jul-201718-Jul-2017 07-Jul-201707-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC506_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üEP116: 1.4-Dioxane

Amber VOC Vial - Sulfuric Acid (EP116)

0902_SW001_030717, 0902_SW009_030717,

0902_SW012_030717, 0902_SW014_030717,

0902_QC107_030717, 0902_QC504_030717

17-Jul-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_SW011_040717, 0902_QC505_040717 18-Jul-2017---- 07-Jul-2017----04-Jul-2017 ---- üEP231A: Perfluoroalkyl Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_SW001_030717, 0902_SW008_030717,

0902_SW009_030717, 0902_SW010_030717,

0902_SW012_030717, 0902_SW013_030717,

0902_SW014_030717, 0902_SW015_030717,

0902_SW016_030717, 0902_SW017_030717,

0902_QC105_030717, 0902_QC107_030717,

0902_QC504_030717

30-Dec-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_SW002_040717, 0902_SW003_040717,

0902_SW004_040717, 0902_SW005_040717,

0902_SW006_040717, 0902_SW007_040717,

0902_SW011_040717, 0902_SW018_040717,

0902_SW019_040717, 0902_QC505_040717

31-Dec-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231B: Perfluoroalkyl Carboxylic Acids

HDPE (no PTFE) (EP231X)

0902_SW001_030717, 0902_SW008_030717,

0902_SW009_030717, 0902_SW010_030717,

0902_SW012_030717, 0902_SW013_030717,

0902_SW014_030717, 0902_SW015_030717,

0902_SW016_030717, 0902_SW017_030717,

0902_QC105_030717, 0902_QC107_030717,

0902_QC504_030717

30-Dec-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_SW002_040717, 0902_SW003_040717,

0902_SW004_040717, 0902_SW005_040717,

0902_SW006_040717, 0902_SW007_040717,

0902_SW011_040717, 0902_SW018_040717,

0902_SW019_040717, 0902_QC505_040717

31-Dec-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

EP231C: Perfluoroalkyl Sulfonamides

HDPE (no PTFE) (EP231X)

0902_SW001_030717, 0902_SW008_030717,

0902_SW009_030717, 0902_SW010_030717,

0902_SW012_030717, 0902_SW013_030717,

0902_SW014_030717, 0902_SW015_030717,

0902_SW016_030717, 0902_SW017_030717,

0902_QC105_030717, 0902_QC107_030717,

0902_QC504_030717

30-Dec-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_SW002_040717, 0902_SW003_040717,

0902_SW004_040717, 0902_SW005_040717,

0902_SW006_040717, 0902_SW007_040717,

0902_SW011_040717, 0902_SW018_040717,

0902_SW019_040717, 0902_QC505_040717

31-Dec-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231D: (n:2) Fluorotelomer Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_SW001_030717, 0902_SW008_030717,

0902_SW009_030717, 0902_SW010_030717,

0902_SW012_030717, 0902_SW013_030717,

0902_SW014_030717, 0902_SW015_030717,

0902_SW016_030717, 0902_SW017_030717,

0902_QC105_030717, 0902_QC107_030717,

0902_QC504_030717

30-Dec-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_SW002_040717, 0902_SW003_040717,

0902_SW004_040717, 0902_SW005_040717,

0902_SW006_040717, 0902_SW007_040717,

0902_SW011_040717, 0902_SW018_040717,

0902_SW019_040717, 0902_QC505_040717

31-Dec-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

EP231P: PFAS Sums

HDPE (no PTFE) (EP231X)

0902_SW001_030717, 0902_SW008_030717,

0902_SW009_030717, 0902_SW010_030717,

0902_SW012_030717, 0902_SW013_030717,

0902_SW014_030717, 0902_SW015_030717,

0902_SW016_030717, 0902_SW017_030717,

0902_QC105_030717, 0902_QC107_030717,

0902_QC504_030717

30-Dec-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_SW002_040717, 0902_SW003_040717,

0902_SW004_040717, 0902_SW005_040717,

0902_SW006_040717, 0902_SW007_040717,

0902_SW011_040717, 0902_SW018_040717,

0902_SW019_040717, 0902_QC505_040717

31-Dec-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 ü1,4-Dioxane in Soils EP116

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üExchangeable Cations ED007

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üMoisture Content EA055

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üPAH/Phenols (SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 14.29 10.003 21 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üPesticides by GCMS EP068

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üTotal Mercury by FIMS EG035T

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üTotal Metals by ICP-AES EG005T

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üTotal Organic Carbon EP003

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 11.11 10.001 9 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üVolatile Organic Compounds EP074

Laboratory Control Samples (LCS)

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 ü1,4-Dioxane in Soils EP116

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üExchangeable Cations ED007

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPAH/Phenols (SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 9.52 5.002 21 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPesticides by GCMS EP068

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Mercury by FIMS EG035T

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Metals by ICP-AES EG005T

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üTotal Organic Carbon EP003

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 11.11 5.001 9 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üVolatile Organic Compounds EP074

Method Blanks (MB)

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 ü1,4-Dioxane in Soils EP116

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üExchangeable Cations ED007

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPAH/Phenols (SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 9.52 5.002 21 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPesticides by GCMS EP068

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Mercury by FIMS EG035T

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Metals by ICP-AES EG005T

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üTotal Organic Carbon EP003

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Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Method Blanks (MB) - Continued

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 11.11 5.001 9 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üVolatile Organic Compounds EP074

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 ü1,4-Dioxane in Soils EP116

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPAH/Phenols (SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 4.76 5.001 21 ûPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üPesticides by GCMS EP068

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Mercury by FIMS EG035T

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üTotal Metals by ICP-AES EG005T

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 11.11 5.001 9 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üVolatile Organic Compounds EP074

Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC Standard 16.67 10.002 12 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 16.67 10.001 6 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 20.00 10.002 10 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 11.76 10.002 17 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 8 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 13.04 10.003 23 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 10.00 10.002 20 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 8 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 8 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 14.29 10.004 28 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 18.18 10.002 11 üVolatile Organic Compounds EP074

Laboratory Control Samples (LCS)

NEPM 2013 B3 & ALS QC Standard 8.33 5.001 12 ü1.4-Dioxane by HS-GCMS EP116

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Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Control Samples (LCS) - Continued

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 10.00 5.001 10 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.88 5.001 17 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 7.14 5.002 28 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 9.09 5.001 11 üVolatile Organic Compounds EP074

Method Blanks (MB)

NEPM 2013 B3 & ALS QC Standard 8.33 5.001 12 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 10.00 5.001 10 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.88 5.001 17 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 12.50 5.001 8 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 7.14 5.002 28 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 9.09 5.001 11 üVolatile Organic Compounds EP074

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC Standard 8.33 5.001 12 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 16.67 5.001 6 üAmmonia as N by Discrete analyser EK055G

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Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Matrix Spikes (MS) - Continued

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 10.00 5.001 10 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.88 5.001 17 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 8 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 5.00 5.001 20 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 8 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 8 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 7.14 5.002 28 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 9.09 5.001 11 üVolatile Organic Compounds EP074

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Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

In house: A gravimetric procedure based on weight loss over a 12 hour drying period at 105-110 degrees C.

This method is compliant with NEPM (2013) Schedule B(3) Section 7.1 and Table 1 (14 day holding time).

Moisture Content EA055 SOIL

In house: Referenced to Rayment & Lyons (2011) Method 15A1. Cations are exchanged from the sample by

contact with Ammonium Chloride. They are then quantitated in the final solution by ICPAES and reported as

meq/100g of original soil. This method is compliant with NEPM (2013) Schedule B(3) (Method 301)

Exchangeable Cations ED007 SOIL

In house: Referenced to APHA 3120; USEPA SW 846 - 6010. Metals are determined following an appropriate

acid digestion of the soil. The ICPAES technique ionises samples in a plasma, emitting a characteristic

spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix

matched standards. This method is compliant with NEPM (2013) Schedule B(3)

Total Metals by ICP-AES EG005T SOIL

In house: Referenced to AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2) (Cold Vapour generation) AAS)

FIM-AAS is an automated flameless atomic absorption technique. Mercury in solids are determined following an

appropriate acid digestion. Ionic mercury is reduced online to atomic mercury vapour by SnCl2 which is then

purged into a heated quartz cell. Quantification is by comparing absorbance against a calibration curve. This

method is compliant with NEPM (2013) Schedule B(3)

Total Mercury by FIMS EG035T SOIL

In house C-IR17. Dried and pulverised sample is reacted with acid to remove inorganic Carbonates, then

combusted in a LECO furnace in the presence of strong oxidants / catalysts. The evolved (Organic) Carbon (as

CO2) is automaticaly measured by infra-red detector.

Total Organic Carbon EP003 SOIL

In house: Referenced to USEPA SW 846 - 8270D Extracts are analysed by Capillary GC/MS and quantification is

by comparison against an established 5 point calibration curve. This technique is compliant with NEPM (2013)

Schedule B(3) (Method 504,505)

Pesticides by GCMS EP068 SOIL

In house: Referenced to USEPA SW 846 - 8015A Sample extracts are analysed by Capillary GC/FID and

quantified against alkane standards over the range C10 - C40. Compliant with NEPM amended 2013.

TRH - Semivolatile Fraction EP071 SOIL

In house: Referenced to USEPA SW 846 - 8260B Extracts are analysed by Purge and Trap, Capillary GC/MS.

Quantification is by comparison against an established 5 point calibration curve. This method is compliant with

NEPM (2013) Schedule B(3) (Method 501)

Volatile Organic Compounds EP074 SOIL

In house: Referenced to USEPA SW 846 - 8270D Extracts are analysed by Capillary GC/MS and quantification is

by comparison against an established 5 point calibration curve. This technique is compliant with NEPM (2013)

Schedule B(3) (Method 502)

Semivolatile Organic Compounds EP075 SOIL

In house: Referenced to USEPA SW 846 - 8270D. Extracts are analysed by Capillary GC/MS in Selective Ion

Mode (SIM) and quantification is by comparison against an established 5 point calibration curve. This method is

compliant with NEPM (2013) Schedule B(3) (Method 502 and 507)

PAH/Phenols (SIM) EP075(SIM) SOIL

In house: Referenced to USEPA SW 846 - 8260B. Extracts are analysed by Purge and Trap, Capillary GC/MS.

Quantification is by comparison against an established 5 point calibration curve. Compliant with NEPM

amended 2013.

TRH Volatiles/BTEX EP080 SOIL

In-house; A 12 mL aliquot of a 1:5 soil:water extract is mixed with 4.5 g of sodium chloride, equilibrated at 80

degrees C for 30 minutes and the headspace analysed by GCMS in the selected ion monitoring mode.

1,4-Dioxane in Soils * EP116 SOIL

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Analytical Methods Method DescriptionsMatrixMethod

In-House. A portion of soil is extracted with MTBE. The extract is taken to dryness, made up in mobile phase.

Analysis is by LC/MSMS, ESI Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.

Per- and Polyfluoroalkyl Substances

(PFAS) by LCMSMS

EP231X SOIL

In house: Referenced to APHA 2540C. A gravimetric procedure that determines the amount of `filterable` residue

in an aqueous sample. A well-mixed sample is filtered through a glass fibre filter (1.2um). The filtrate is

evaporated to dryness and dried to constant weight at 180+/-5C. This method is compliant with NEPM (2013)

Schedule B(3)

Total Dissolved Solids (High Level) EA015H WATER

In house: Referenced to APHA 2320 B This procedure determines alkalinity by automated measurement (e.g. PC

Titrate) using pH 4.5 for indicating the total alkalinity end-point. This method is compliant with NEPM (2013)

Schedule B(3)

Alkalinity by PC Titrator ED037-P WATER

In house: Referenced to APHA 4500-SO4. Dissolved sulfate is determined in a 0.45um filtered sample. Sulfate

ions are converted to a barium sulfate suspension in an acetic acid medium with barium chloride. Light

absorbance of the BaSO4 suspension is measured by a photometer and the SO4-2 concentration is determined

by comparison of the reading with a standard curve. This method is compliant with NEPM (2013) Schedule B(3)

Sulfate (Turbidimetric) as SO4 2- by

Discrete Analyser

ED041G WATER

In house: Referenced to APHA 4500 Cl - G.The thiocyanate ion is liberated from mercuric thiocyanate through

sequestration of mercury by the chloride ion to form non-ionised mercuric chloride.in the presence of ferric ions

the librated thiocynate forms highly-coloured ferric thiocynate which is measured at 480 nm APHA 21st edition

seal method 2 017-1-L april 2003

Chloride by Discrete Analyser ED045G WATER

In house: Referenced to APHA 3120 and 3125; USEPA SW 846 - 6010 and 6020; Cations are determined by

either ICP-AES or ICP-MS techniques. This method is compliant with NEPM (2013) Schedule B(3)

Sodium Adsorption Ratio is calculated from Ca, Mg and Na which determined by ALS in house method

QWI-EN/ED093F. This method is compliant with NEPM (2013) Schedule B(3)

Hardness parameters are calculated based on APHA 2340 B. This method is compliant with NEPM (2013)

Schedule B(3)

Major Cations - Dissolved ED093F WATER

In house: Referenced to APHA 3125; USEPA SW846 - 6020, ALS QWI-EN/EG020. Samples are 0.45µm filtered

prior to analysis. The ICPMS technique utilizes a highly efficient argon plasma to ionize selected elements. Ions

are then passed into a high vacuum mass spectrometer, which separates the analytes based on their distinct

mass to charge ratios prior to their measurement by a discrete dynode ion detector.

Dissolved Metals by ICP-MS - Suite A EG020A-F WATER

In house: Referenced to AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS)

Samples are 0.45µm filtered prior to analysis. FIM-AAS is an automated flameless atomic absorption technique.

A bromate/bromide reagent is used to oxidise any organic mercury compounds in the filtered sample. The ionic

mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell.

Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM

(2013) Schedule B(3)

Dissolved Mercury by FIMS EG035F WATER

In house: Referenced to APHA 4500-F C: CDTA is added to the sample to provide a uniform ionic strength

background, adjust pH, and break up complexes. Fluoride concentration is determined by either manual or

automatic ISE measurement. This method is compliant with NEPM (2013) Schedule B(3)

Fluoride by PC Titrator EK040P WATER

In house: Referenced to APHA 4500-NH3 G Ammonia is determined by direct colorimetry by Discrete Analyser.

This method is compliant with NEPM (2013) Schedule B(3)

Ammonia as N by Discrete analyser EK055G WATER

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Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 4500-NO2- B. Nitrite is determined by direct colourimetry by Discrete Analyser.

This method is compliant with NEPM (2013) Schedule B(3)

Nitrite as N by Discrete Analyser EK057G WATER

In house: Referenced to APHA 4500-NO3- F. Nitrate is reduced to nitrite by way of a chemical reduction followed

by quantification by Discrete Analyser. Nitrite is determined seperately by direct colourimetry and result for Nitrate

calculated as the difference between the two results. This method is compliant with NEPM (2013) Schedule B(3)

Nitrate as N by Discrete Analyser EK058G WATER

In house: Referenced to APHA 4500-NO3- F. Combined oxidised Nitrogen (NO2+NO3) is determined by

Chemical Reduction and direct colourimetry by Discrete Analyser. This method is compliant with NEPM (2013)

Schedule B(3)

Nitrite and Nitrate as N (NOx) by Discrete

Analyser

EK059G WATER

In house: Referenced to APHA 4500-P F Ammonium molybdate and potassium antimonyl tartrate reacts in acid

medium with othophosphate to form a heteropoly acid -phosphomolybdic acid - which is reduced to intensely

coloured molybdenum blue by ascorbic acid. Quantification is by Discrete Analyser. This method is compliant

with NEPM (2013) Schedule B(3)

Reactive Phosphorus as P-By Discrete

Analyser

EK071G WATER

In house: Referenced to APHA 1030F. This method is compliant with NEPM (2013) Schedule B(3)Ionic Balance by PCT DA and Turbi SO4

DA

EN055 - PG WATER

In house: Referenced to USEPA SW 846 - 8015A The sample extract is analysed by Capillary GC/FID and

quantification is by comparison against an established 5 point calibration curve of n-Alkane standards. This

method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH - Semivolatile Fraction EP071 WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. This

method is compliant with NEPM (2013) Schedule B(3)

Volatile Organic Compounds EP074 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS and

quantification is by comparison against an established 5 point calibration curve. This method is compliant with

NEPM (2013) Schedule B(3)

Semivolatile Organic Compounds EP075 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS in SIM Mode

and quantification is by comparison against an established 5 point calibration curve. This method is compliant

with NEPM (2013) Schedule B(3)

PAH/Phenols (GC/MS - SIM) EP075(SIM) WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve.

Alternatively, a sample is equilibrated in a headspace vial and a portion of the headspace determined by GCMS

analysis. This method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH Volatiles/BTEX EP080 WATER

In house: A 12 mL aliquot of sample is mixed with 4.5 g of sodium chloride, equilibrated at 80 degrees C for 30

minutes and the headspace analysed by GCMS in the selected ion monitoring mode.

1.4-Dioxane by HS-GCMS EP116 WATER

In house: Direct injection analysis of fresh waters after dilution (1:1) with methanol. Analysis by

LC-Electrospray-MS-MS, Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.

Per- and Polyfluoroalkyl Substances

(PFAS) by LCMSMS

EP231X WATER

Preparation Methods Method DescriptionsMatrixMethod

In house: Referenced to Rayment & Higginson (1992) method 15A1. A 1M NH4Cl extraction by end over end

tumbling at a ratio of 1:20. There is no pretreatment for soluble salts. Extracts can be run by ICP for cations.

Exchangeable Cations Preparation

Method

ED007PR SOIL

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Preparation Methods Method DescriptionsMatrixMethod

In house: Referenced to USEPA 200.2. Hot Block Acid Digestion 1.0g of sample is heated with Nitric and

Hydrochloric acids, then cooled. Peroxide is added and samples heated and cooled again before being filtered

and bulked to volume for analysis. Digest is appropriate for determination of selected metals in sludge,

sediments, and soils. This method is compliant with NEPM (2013) Schedule B(3) (Method 202)

Hot Block Digest for metals in soils

sediments and sludges

EN69 SOIL

In houseSample Extraction for PFAS EP231-PR SOIL

#Dry and Pulverise (up to 100g) GEO30 SOIL

In house: Referenced to USEPA SW 846 - 5030A. 5g of solid is shaken with surrogate and 10mL methanol prior

to analysis by Purge and Trap - GC/MS.

Methanolic Extraction of Soils for Purge

and Trap

* ORG16 SOIL

In house: Mechanical agitation (tumbler). 10g of sample, Na2SO4 and surrogate are extracted with 30mL 1:1

DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the

desired volume for analysis.

Tumbler Extraction of Solids ORG17 SOIL

In house: Referenced to USEPA SW 846 - 3510B 100 mL to 1L of sample is transferred to a separatory funnel

and serially extracted three times using 60mL DCM for each extract. The resultant extracts are combined,

dehydrated and concentrated for analysis. This method is compliant with NEPM (2013) Schedule B(3) . ALS

default excludes sediment which may be resident in the container.

Separatory Funnel Extraction of Liquids ORG14 WATER

A 5 mL aliquot or 5 mL of a diluted sample is added to a 40 mL VOC vial for sparging.Volatiles Water Preparation ORG16-W WATER

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Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1716548

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8503

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60547028, task 3.1 Page 1 of 4

:Order number 60547028 :Quote number ES2017AECOMAU0002 (SY/308/17)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : RAAF Richmond

Sampler : BEN HUNTER

DatesDate Samples Received : Issue Date : 06-Jul-201705-Jul-2017 13:15

Scheduled Reporting Date: 12-Jul-2017:Client Requested Due

Date

12-Jul-2017

Delivery DetailsMode of Delivery : :Undefined Not AvailableSecurity Seal

No. of coolers/boxes : :2 Temperature 0.1'C - Ice present

: : 24 / 24Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l 6/7/17: This is an updated SRA which indicates the updated analysis.

l Sample (902_QC201_030717) forwarded to Envirolab as per COCl No green plastic unpreserved bottle was received for sample 0902_QC101_030717 hence the Anions can't be done on this

sample.

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 200: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716548 Amendment 02 of 4:Page

06-Jul-2017:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

WA

TE

R -

EA

015H

Tota

l Dis

solv

ed S

olid

s -

Hig

h L

eve

l

WA

TE

R -

EP

116

1.4

-Dio

xan

e

WA

TE

R -

EP

231X

PF

AS

- F

ull

Su

ite (

28 a

na

lyte

s)

WA

TE

R -

NT

-01 &

02A

Ca, M

g, N

a, K

, C

l, S

O4

, A

lka

linity

& F

luo

rid

e

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

WA

TE

R -

W-2

3

SV

OC

/VO

C

WA

TE

R -

W-2

6

TR

H/B

TE

XN

/PA

H/8

Me

tals

ES1716548-001 03-Jul-2017 00:00 0902_MW01_030717 ü ü ü ü ü ü

ES1716548-002 03-Jul-2017 00:00 0902_MW02_030717 ü ü ü ü ü ü

ES1716548-003 03-Jul-2017 00:00 0902_MW03_030717 ü ü ü ü ü ü

ES1716548-004 03-Jul-2017 00:00 0902_MW12_030717 ü ü ü ü ü ü

ES1716548-005 03-Jul-2017 00:00 0902_MW13_030717 ü ü ü ü ü ü

ES1716548-006 03-Jul-2017 00:00 0902_MW14_030717 ü ü ü ü ü ü

ES1716548-007 03-Jul-2017 00:00 0902_MW15_030717 ü ü ü ü ü ü

ES1716548-008 03-Jul-2017 00:00 0902_MW17_030717 ü ü ü ü ü ü

ES1716548-009 03-Jul-2017 00:00 0902_QC103_030717 ü ü ü ü ü ü

ES1716548-010 03-Jul-2017 00:00 0902_QC503_030717 ü ü ü ü ü ü

ES1716548-011 04-Jul-2017 00:00 0902_QC507_040717 ü

ES1716548-012 30-Jun-2017 00:00 0902_QC501_300617 ü ü ü ü ü ü

ES1716548-013 03-Jul-2017 00:00 0902_QC502_030717 ü ü ü ü ü ü

ES1716548-014 30-Jun-2017 00:00 0902_MW08_300617 ü ü ü ü ü ü

ES1716548-015 30-Jun-2017 00:00 0902_MW09_300617 ü ü ü ü ü ü

ES1716548-016 03-Jul-2017 00:00 0902_MW56_030717 ü ü ü ü ü ü

ES1716548-017 30-Jun-2017 00:00 0902_MW54_300617 ü ü ü ü ü ü

ES1716548-018 30-Jun-2017 00:00 0902_MW58_300617 ü ü ü ü ü ü

ES1716548-019 03-Jul-2017 00:00 0902_MW59_030717 ü ü ü ü ü ü

ES1716548-020 03-Jul-2017 00:00 0902_QC101_030717 ü ü ü ü

ES1716548-021 03-Jul-2017 00:00 0902_MW57_030717 ü ü ü ü ü ü

ES1716548-022 30-Jun-2017 00:00 0902_MW10_300617 ü ü ü ü ü ü

ES1716548-023 03-Jul-2017 00:00 0902_MW30_030717 ü ü ü ü ü ü

ES1716548-024 03-Jul-2017 00:00 0902_MW53_030717 ü ü ü ü ü ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 201: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716548 Amendment 03 of 4:Page

06-Jul-2017:Issue Date

WA

TE

R -

NT

-01

Ma

jor

Ca

tion

s (C

a,

Mg

, N

a,

K)

ES1716548-020 03-Jul-2017 00:00 0902_QC101_030717 ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Page 202: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716548 Amendment 04 of 4:Page

06-Jul-2017:Issue Date

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

BEN HUNTER2

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 URS (EQUIS_V5_URS) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

CATHERINE HANSEN

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 URS (EQUIS_V5_URS) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

CLAYTON COWPER

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 URS (EQUIS_V5_URS) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

DIRK SANDERSON

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - EQUIS V5 URS (EQUIS_V5_URS) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

- EDI Format - XTab (XTAB) Email [email protected]

- Electronic SRN for EQuIS (ESRN_EQUIS) Email [email protected]

Page 203: Appendix - Department of Defence

0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 53ES1716548

:: LaboratoryClient AECOM Australia Pty Ltd Environmental Division Sydney

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield NSW Australia 2164

:Telephone +61 02 8934 0000 :Telephone +61 2 8784 8503

:Project 60547028, task 3.1 Date Samples Received : 05-Jul-2017 13:15

:Order number 60547028 Date Analysis Commenced : 06-Jul-2017

:C-O-C number ---- Issue Date : 13-Jul-2017 12:44

Sampler : BEN HUNTER

Site : RAAF Richmond

Quote number : SY/308/17

24:No. of samples received

24:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Wisam Marassa Inorganics Coordinator Sydney Inorganics, Smithfield, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When no sampling time is provided, the sampling time will default 00:00 on the date of sampling. If no sampling date is provided, the sampling date will be assumed by the laboratory and displayed in brackets without a

time component.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

No green plastic unpreserved bottle was received for sample 0902_QC101_030717 hence the Anions can't be done on this sample.l

EG020: Bromine quantification may be unreliable due to its low solubility in acid, leading to variable volatility during measurement by ICPMS.l

Positive Hg results have been confirmed by reanalysisl

TDS by method EA-015 may bias high for various samples due to the presence of fine particulate matter, which may pass through the prescribed GF/C paper.l

TDS by method EA-015 may bias high due to the presence of fine particulate matter, which may pass through the prescribed GF/C paper.l

EP231X: Particular samples required dilution prior to extraction due to matrix interferences. LOR values have been adjusted accordingly.l

EP116: Particular samples required dilution due to sample matrix . LOR values have been adjusted accordingly.l

EP075: 'Sum of PAH' is the sum of the USEPA 16 priority PAHsl

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero.

l

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

652 3080 2320 2200 617mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

119Bicarbonate Alkalinity as CaCO3 482 336 141 148mg/L171-52-3

119 482 336 141 148mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

32Sulfate as SO4 - Turbidimetric 64 84 68 25mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

314Chloride 900 1030 1080 272mg/L116887-00-6

ED093F: Dissolved Major Cations

44Calcium 94 132 100 20mg/L17440-70-2

38Magnesium 100 130 72 12mg/L17439-95-4

124Sodium 498 511 613 208mg/L17440-23-5

<1Potassium 1 <1 2 <1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

<0.01Aluminium <0.01 0.06 <0.01 <0.01mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 0.001 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 0.001 <0.001 <0.001mg/L0.0017439-92-1

0.098Manganese 0.822 0.895 4.01 0.069mg/L0.0017439-96-5

0.002Nickel 0.027 0.005 0.014 0.010mg/L0.0017440-02-0

<0.005Zinc 0.006 <0.005 0.008 0.018mg/L0.0057440-66-6

0.18Iron 0.12 0.07 2.95 <0.05mg/L0.057439-89-6

0.8Bromine 2.6 3.6 3.1 1.5mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 0.0002mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.4Fluoride 0.8 0.3 <0.1 0.2mg/L0.116984-48-8

EN055: Ionic Balance

11.9 36.4 37.5 34.7 11.2meq/L0.01----Total Anions

10.7 34.6 39.5 37.6 11.0meq/L0.01----Total Cations

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

5.24 2.46 2.59 4.05 0.53%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

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0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

Page 211: Appendix - Department of Defence

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

<50 <50 <50 <50 <50µg/L50----C29 - C36 Fraction

<50^ <50 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 <100 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

Page 212: Appendix - Department of Defence

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

<100^ <100 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <0.5 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.04Perfluorobutane sulfonic acid

(PFBS)

<0.02 <0.02 2.14 0.38µg/L0.02375-73-5

0.02Perfluoropentane sulfonic acid

(PFPeS)

<0.02 <0.02 1.21 0.22µg/L0.022706-91-4

0.11Perfluorohexane sulfonic acid

(PFHxS)

<0.02 <0.02 5.91 1.23µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 0.10 <0.02µg/L0.02375-92-8

<0.01Perfluorooctane sulfonic acid

(PFOS)

<0.01 <0.01 0.73 0.08µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 <0.02 0.42 <0.02µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) <0.02 <0.02 1.34 0.06µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 0.15 <0.02µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) <0.01 <0.01 0.22 <0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

Page 213: Appendix - Department of Defence

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

0.17 <0.01 <0.01 12.2 1.97µg/L0.01----Sum of PFAS

Page 214: Appendix - Department of Defence

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Analytical Results

0902_MW13_0307170902_MW12_0307170902_MW03_0307170902_MW02_0307170902_MW01_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-005ES1716548-004ES1716548-003ES1716548-002ES1716548-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

0.11Sum of PFHxS and PFOS <0.01 <0.01 6.64 1.31µg/L0.01355-46-4/1763-23-

1

0.15 <0.01 <0.01 10.9 1.75µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1081.2-Dichloroethane-D4 108 102 108 102%517060-07-0

115Toluene-D8 116 104 114 109%52037-26-5

1074-Bromofluorobenzene 106 101 108 102%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

24.0Phenol-d6 31.2 21.3 29.8 30.0%113127-88-3

50.92-Chlorophenol-D4 50.0 52.3 63.5 63.3%193951-73-6

50.12.4.6-Tribromophenol 59.4 41.4 65.8 70.9%1118-79-6

EP075(SIM)T: PAH Surrogates

49.72-Fluorobiphenyl 63.7 64.1 66.0 69.1%1321-60-8

80.6Anthracene-d10 102 94.8 92.0 92.4%11719-06-8

64.44-Terphenyl-d14 68.6 65.8 76.8 86.0%11718-51-0

EP075S: Acid Extractable Surrogates

33.52-Fluorophenol 36.9 34.4 40.3 34.8%2367-12-4

24.8Phenol-d6 27.8 25.5 29.1 28.0%213127-88-3

46.72-Chlorophenol-D4 48.8 47.2 53.1 51.7%293951-73-6

47.42.4.6-Tribromophenol 50.5 53.9 63.1 67.9%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

57.2Nitrobenzene-D5 58.4 57.9 64.6 63.3%24165-60-0

41.51.2-Dichlorobenzene-D4 43.4 44.8 48.9 47.0%22199-69-1

53.22-Fluorobiphenyl 53.6 57.1 61.5 60.0%2321-60-8

65.2Anthracene-d10 70.2 68.9 79.0 79.0%21719-06-8

69.24-Terphenyl-d14 74.7 71.8 84.7 84.3%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1101.2-Dichloroethane-D4 109 104 110 104%217060-07-0

119Toluene-D8 120 108 118 113%22037-26-5

1094-Bromofluorobenzene 109 101 110 105%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1031.4-Dioxane-d8 122 122 108 108%0.517647-74-4

EP231S: PFAS Surrogate

70.6 69.0 75.2 61.0 62.5%0.02----13C4-PFOS

Page 215: Appendix - Department of Defence

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

512 1010 3300 2350 <10mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

288Bicarbonate Alkalinity as CaCO3 212 563 143 <1mg/L171-52-3

288 212 563 143 <1mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

10Sulfate as SO4 - Turbidimetric 8 156 69 <1mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

159Chloride 102 1250 1080 <1mg/L116887-00-6

ED093F: Dissolved Major Cations

21Calcium 10 52 100 <1mg/L17440-70-2

22Magnesium 12 73 66 <1mg/L17439-95-4

160Sodium 124 1160 577 <1mg/L17440-23-5

<1Potassium <1 <1 2 <1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.14Aluminium 0.03 <0.01 <0.01 <0.01mg/L0.017429-90-5

0.002Arsenic <0.001 0.001 0.002 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

0.011Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.207Manganese 0.095 0.017 4.07 <0.001mg/L0.0017439-96-5

<0.001Nickel 0.001 0.002 0.013 <0.001mg/L0.0017440-02-0

0.006Zinc 0.009 <0.005 0.008 <0.005mg/L0.0057440-66-6

1.82Iron <0.05 <0.05 2.84 <0.05mg/L0.057439-89-6

0.4Bromine 0.4 2.4 3.2 <0.1mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.8Fluoride 0.4 1.0 <0.1 <0.1mg/L0.116984-48-8

EN055: Ionic Balance

10.4 7.28 49.8 34.8 <0.01meq/L0.01----Total Anions

9.82 6.88 59.0 35.6 <0.01meq/L0.01----Total Cations

Page 216: Appendix - Department of Defence

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

3.11 2.82 8.55 1.15 ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

Page 217: Appendix - Department of Defence

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

<50 <50 <50 <50 <50µg/L50----C29 - C36 Fraction

<50^ <50 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 <100 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

Page 222: Appendix - Department of Defence

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

<100^ <100 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <0.5 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.44Perfluorobutane sulfonic acid

(PFBS)

0.95 0.68 2.14 <0.02µg/L0.02375-73-5

0.26Perfluoropentane sulfonic acid

(PFPeS)

0.73 0.56 1.25 <0.02µg/L0.022706-91-4

0.90Perfluorohexane sulfonic acid

(PFHxS)

5.07 5.06 5.99 <0.02µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

0.24 0.06 0.11 <0.02µg/L0.02375-92-8

0.04Perfluorooctane sulfonic acid

(PFOS)

3.92 1.03 0.73 <0.01µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

0.04Perfluoropentanoic acid (PFPeA) 0.20 <0.02 0.42 <0.02µg/L0.022706-90-3

0.16Perfluorohexanoic acid (PFHxA) 0.64 0.03 1.36 <0.02µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) 0.07 <0.02 0.15 <0.02µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) 0.20 <0.01 0.22 <0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

Page 223: Appendix - Department of Defence

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

1.84 12.0 7.42 12.4 <0.01µg/L0.01----Sum of PFAS

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Analytical Results

0902_QC503_0307170902_QC103_0307170902_MW17_0307170902_MW15_0307170902_MW14_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-010ES1716548-009ES1716548-008ES1716548-007ES1716548-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

0.94Sum of PFHxS and PFOS 8.99 6.09 6.72 <0.01µg/L0.01355-46-4/1763-23-

1

1.58 11.0 6.80 11.0 <0.01µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1061.2-Dichloroethane-D4 108 101 105 105%517060-07-0

107Toluene-D8 113 106 104 111%52037-26-5

1024-Bromofluorobenzene 108 99.5 99.9 103%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

25.3Phenol-d6 38.2 11.4 32.6 29.2%113127-88-3

53.02-Chlorophenol-D4 68.0 13.9 50.6 57.9%193951-73-6

58.02.4.6-Tribromophenol 87.0 31.2 65.8 61.9%1118-79-6

EP075(SIM)T: PAH Surrogates

87.42-Fluorobiphenyl 59.8 20.4 57.1 62.1%1321-60-8

106Anthracene-d10 110 60.9 82.4 104%11719-06-8

74.94-Terphenyl-d14 101 58.8 73.0 70.1%11718-51-0

EP075S: Acid Extractable Surrogates

40.62-Fluorophenol 48.2 36.2 34.3 36.1%2367-12-4

31.7Phenol-d6 38.3 33.7 24.4 27.6%213127-88-3

54.92-Chlorophenol-D4 60.4 57.1 46.2 50.6%293951-73-6

54.82.4.6-Tribromophenol 85.2 66.3 62.5 55.9%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

66.1Nitrobenzene-D5 73.2 57.3 55.9 60.1%24165-60-0

49.91.2-Dichlorobenzene-D4 50.7 51.2 40.5 45.1%22199-69-1

65.82-Fluorobiphenyl 68.6 63.6 55.4 59.5%2321-60-8

80.6Anthracene-d10 88.7 74.2 75.3 76.4%21719-06-8

83.64-Terphenyl-d14 92.4 74.4 79.6 79.0%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1081.2-Dichloroethane-D4 110 102 107 106%217060-07-0

111Toluene-D8 117 110 107 115%22037-26-5

1034-Bromofluorobenzene 110 99.5 99.1 104%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1061.4-Dioxane-d8 122 113 110 111%0.517647-74-4

EP231S: PFAS Surrogate

63.8 69.0 70.4 66.9 60.4%0.02----13C4-PFOS

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

---- <10 ---- ---- ----mg/L10----Total Dissolved Solids @180°C

---- ---- <10 2720 6180mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

----Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

----Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

----Bicarbonate Alkalinity as CaCO3 <1 <1 150 125mg/L171-52-3

---- <1 <1 150 125mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

----Sulfate as SO4 - Turbidimetric <1 <1 6 23mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

----Chloride <1 <1 951 3760mg/L116887-00-6

ED093F: Dissolved Major Cations

----Calcium <1 <1 57 160mg/L17440-70-2

----Magnesium <1 <1 79 327mg/L17439-95-4

----Sodium <1 <1 502 1390mg/L17440-23-5

----Potassium <1 <1 1 2mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

----Aluminium <0.01 <0.01 0.01 0.03mg/L0.017429-90-5

----Arsenic <0.001 <0.001 0.001 <0.001mg/L0.0017440-38-2

----Cadmium <0.0001 <0.0001 <0.0001 0.0002mg/L0.00017440-43-9

----Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

----Copper <0.001 <0.001 <0.001 0.007mg/L0.0017440-50-8

----Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

----Manganese <0.001 <0.001 0.982 0.093mg/L0.0017439-96-5

----Nickel <0.001 <0.001 0.016 0.045mg/L0.0017440-02-0

----Zinc <0.005 <0.005 0.020 0.223mg/L0.0057440-66-6

----Iron <0.05 <0.05 1.53 0.10mg/L0.057439-89-6

----Bromine <0.1 <0.1 2.4 8.8mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

----Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

----Fluoride <0.1 <0.1 0.5 0.3mg/L0.116984-48-8

EN055: Ionic Balance

---- <0.01 <0.01 29.9 109meq/L0.01----Total Anions

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

---- <0.01 <0.01 31.2 95.4meq/L0.01----Total Cations

---- ---- ---- 2.06 6.67%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

----Styrene <5 <5 <5 <5µg/L5100-42-5

----Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

----n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

----1.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

----sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

----1.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

----tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

----p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

----n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

----Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

----2-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

----4-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

----2-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

----Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

----2.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

----1.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

----cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

----trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

----1.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

----Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

----Chloromethane <50 <50 <50 <50µg/L5074-87-3

----Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

----Bromomethane <50 <50 <50 <50µg/L5074-83-9

----Chloroethane <50 <50 <50 <50µg/L5075-00-3

----Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

----1.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

----Iodomethane <5 <5 <5 <5µg/L574-88-4

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

----trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

----1.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

----cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

----1.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

----1.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

----Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

----1.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

----Trichloroethene <5 <5 <5 <5µg/L579-01-6

----Dibromomethane <5 <5 <5 <5µg/L574-95-3

----1.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

----1.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

----Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

----1.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

----trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

----cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

----1.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

----1.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

----Pentachloroethane <5 <5 <5 <5µg/L576-01-7

----1.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

----Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

----Bromobenzene <5 <5 <5 <5µg/L5108-86-1

----2-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

----4-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

----1.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

----Chloroform <5 <5 <5 <5µg/L567-66-3

----Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

----Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

----Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

----Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

----Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

----Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

----Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

----Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

----Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

----Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

----Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

----Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

----Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

----Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

----Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

----Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

----Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

----Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

----Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

----^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

----^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

----Phenol <2 <2 <2 <2µg/L2108-95-2

----2-Chlorophenol <2 <2 <2 <2µg/L295-57-8

----2-Methylphenol <2 <2 <2 <2µg/L295-48-7

----3- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

----2-Nitrophenol <2 <2 <2 <2µg/L288-75-5

----2.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

----2.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

----2.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

----4-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

----2.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

----2.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

----Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

----2-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

----2-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

----N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

----7.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

----3-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters

----Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

----Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

----Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

----Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

----bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

----Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

----N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

----N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

----N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

----N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

----N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

----N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

----N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

----N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

----Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

----2-Picoline <2 <2 <2 <2µg/L2109-06-8

----Acetophenone <2 <2 <2 <2µg/L298-86-2

----Nitrobenzene <2 <2 <2 <2µg/L298-95-3

----Isophorone <2 <2 <2 <2µg/L278-59-1

----2.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

----2.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

----1-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

----4-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

----5-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

----Azobenzene <2 <2 <2 <2µg/L2103-33-3

----1.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

----Phenacetin <2 <2 <2 <2µg/L262-44-2

----4-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

----Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

----Pronamide <2 <2 <2 <2µg/L223950-58-5

----Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

----Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

----Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

----Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

----4-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

----4-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

----1.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

----1.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

----1.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

----Hexachloroethane <2 <2 <2 <2µg/L267-72-1

----1.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

----Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

----Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

----Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

----Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

----Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

----Aniline <2 <2 <2 <2µg/L262-53-3

----4-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

----2-Nitroaniline <4 <4 <4 <4µg/L488-74-4

----3-Nitroaniline <4 <4 <4 <4µg/L499-09-2

----Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

----4-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

----Carbazole <2 <2 <2 <2µg/L286-74-8

----3.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

----alpha-BHC <2 <2 <2 <2µg/L2319-84-6

----beta-BHC <2 <2 <2 <2µg/L2319-85-7

----gamma-BHC <2 <2 <2 <2µg/L258-89-9

----delta-BHC <2 <2 <2 <2µg/L2319-86-8

----Heptachlor <2 <2 <2 <2µg/L276-44-8

----Aldrin <2 <2 <2 <2µg/L2309-00-2

----Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

----alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

----4.4`-DDE <2 <2 <2 <2µg/L272-55-9

----Dieldrin <2 <2 <2 <2µg/L260-57-1

----Endrin <2 <2 <2 <2µg/L272-20-8

----beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

----4.4`-DDD <2 <2 <2 <2µg/L272-54-8

----Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

----4.4`-DDT <4 <4 <4 <4µg/L450-29-3

----^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

----^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

----Dichlorvos <2 <2 <2 <2µg/L262-73-7

----Dimethoate <2 <2 <2 <2µg/L260-51-5

----Diazinon <2 <2 <2 <2µg/L2333-41-5

----Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

----Malathion <2 <2 <2 <2µg/L2121-75-5

----Fenthion <2 <2 <2 <2µg/L255-38-9

----Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

----Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

----Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

----Prothiofos <2 <2 <2 <2µg/L234643-46-4

----Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

---- <50 <50 <50 <50µg/L50----C10 - C14 Fraction

---- <100 <100 <100 <100µg/L100----C15 - C28 Fraction

---- <50 <50 <50 <50µg/L50----C29 - C36 Fraction

----^ <50 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

---- <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

---- <100 <100 <100 <100µg/L100---->C16 - C34 Fraction

---- <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

----^ <100 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

----^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

----1.4-Dioxane <0.5 <0.5 <0.5 <1.0µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

----Perfluorobutane sulfonic acid

(PFBS)

<0.02 <0.02 0.05 <0.02µg/L0.02375-73-5

----Perfluoropentane sulfonic acid

(PFPeS)

<0.02 <0.02 0.04 <0.02µg/L0.022706-91-4

----Perfluorohexane sulfonic acid

(PFHxS)

<0.02 <0.02 0.18 0.10µg/L0.02355-46-4

----Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 <0.02 <0.02µg/L0.02375-92-8

----Perfluorooctane sulfonic acid

(PFOS)

<0.01 <0.01 <0.01 0.06µg/L0.011763-23-1

----Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

----Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

----Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 <0.02µg/L0.022706-90-3

----Perfluorohexanoic acid (PFHxA) <0.02 <0.02 <0.02 <0.02µg/L0.02307-24-4

----Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-85-9

----Perfluorooctanoic acid (PFOA) <0.01 <0.01 <0.01 <0.01µg/L0.01335-67-1

----Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

----Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

Page 233: Appendix - Department of Defence

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

----Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

----Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

----Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

----Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

----Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

----N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

----N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

----N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

----N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

----N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

----N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

----4:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

----6:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

----8:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

----10:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

---- <0.01 <0.01 0.27 0.16µg/L0.01----Sum of PFAS

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Analytical Results

0902_MW09_3006170902_MW08_3006170902_QC502_0307170902_QC501_3006170902_QC507_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

30-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716548-015ES1716548-014ES1716548-013ES1716548-012ES1716548-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

----Sum of PFHxS and PFOS <0.01 <0.01 0.18 0.16µg/L0.01355-46-4/1763-23-

1

---- <0.01 <0.01 0.23 0.16µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

----1.2-Dichloroethane-D4 106 108 111 110%517060-07-0

----Toluene-D8 109 98.6 112 110%52037-26-5

----4-Bromofluorobenzene 102 99.4 108 102%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

----Phenol-d6 29.7 27.0 23.0 21.2%113127-88-3

----2-Chlorophenol-D4 51.4 36.2 44.3 39.8%193951-73-6

----2.4.6-Tribromophenol 38.0 40.3 59.0 67.4%1118-79-6

EP075(SIM)T: PAH Surrogates

----2-Fluorobiphenyl 59.7 51.7 49.2 39.0%1321-60-8

----Anthracene-d10 77.4 73.7 105 74.3%11719-06-8

----4-Terphenyl-d14 73.1 61.0 51.1 80.9%11718-51-0

EP075S: Acid Extractable Surrogates

----2-Fluorophenol 29.2 25.6 28.5 27.7%2367-12-4

----Phenol-d6 28.0 24.6 21.8 22.6%213127-88-3

----2-Chlorophenol-D4 44.8 38.0 38.0 38.2%293951-73-6

----2.4.6-Tribromophenol 38.1 33.6 51.4 57.3%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

----Nitrobenzene-D5 59.8 49.6 47.0 46.3%24165-60-0

----1.2-Dichlorobenzene-D4 43.6 34.0 33.2 32.3%22199-69-1

----2-Fluorobiphenyl 56.2 45.8 45.9 45.4%2321-60-8

----Anthracene-d10 75.2 61.4 65.8 68.9%21719-06-8

----4-Terphenyl-d14 80.8 64.5 72.8 83.3%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1011.2-Dichloroethane-D4 108 110 113 112%217060-07-0

103Toluene-D8 113 102 117 114%22037-26-5

97.44-Bromofluorobenzene 104 97.9 109 106%2460-00-4

EP116S: 1.4-Dioxane Surrogate

----1.4-Dioxane-d8 119 114 126 122%0.517647-74-4

EP231S: PFAS Surrogate

---- 67.7 65.9 62.8 71.3%0.02----13C4-PFOS

Page 235: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

2330 1930 4360 3960 ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 ----mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 ----mg/L13812-32-6

78Bicarbonate Alkalinity as CaCO3 410 287 147 ----mg/L171-52-3

78 410 287 147 ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

9Sulfate as SO4 - Turbidimetric 53 27 13 ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

1110Chloride 591 1070 1670 ----mg/L116887-00-6

ED093F: Dissolved Major Cations

72Calcium 22 64 88 89mg/L17440-70-2

127Magnesium 33 86 194 194mg/L17439-95-4

447Sodium 478 613 873 859mg/L17440-23-5

2Potassium 1 <1 <1 <1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

<0.01Aluminium 0.03 0.01 0.01 ----mg/L0.017429-90-5

0.001Arsenic <0.001 <0.001 <0.001 <0.001mg/L0.0017440-38-2

0.0002Cadmium <0.0001 0.0001 0.0001 0.0002mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.046Manganese 0.336 0.084 0.038 ----mg/L0.0017439-96-5

0.027Nickel 0.034 0.017 0.028 0.030mg/L0.0017440-02-0

0.052Zinc 0.050 0.067 0.057 0.058mg/L0.0057440-66-6

<0.05Iron 0.61 <0.05 <0.05 ----mg/L0.057439-89-6

2.8Bromine 2.0 3.3 4.2 ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.1Fluoride 1.2 0.3 0.2 ----mg/L0.116984-48-8

EN055: Ionic Balance

33.0 26.0 36.5 50.3 ----meq/L0.01----Total Anions

33.5 24.6 36.9 58.3 ----meq/L0.01----Total Cations

Page 236: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EN055: Ionic Balance - Continued

0.72 2.64 0.62 7.38 ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

Page 237: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

Page 238: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

Page 239: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075C: Phthalate Esters - Continued

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075I: Organochlorine Pesticides - Continued

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

<50 <50 <50 <50 <50µg/L50----C29 - C36 Fraction

<50^ <50 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 <100 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

<100^ <100 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<1.01.4-Dioxane <1.0 <1.0 <1.0 <1.0µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

<0.02Perfluorobutane sulfonic acid

(PFBS)

0.06 1.66 2.20 2.22µg/L0.02375-73-5

<0.02Perfluoropentane sulfonic acid

(PFPeS)

0.03 0.92 1.21 1.20µg/L0.022706-91-4

<0.02Perfluorohexane sulfonic acid

(PFHxS)

0.09 1.86 1.96 1.96µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 <0.02 <0.02µg/L0.02375-92-8

0.02Perfluorooctane sulfonic acid

(PFOS)

<0.01 <0.01 0.01 0.01µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 0.37 0.34 0.33µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) <0.02 1.30 1.17 1.18µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 0.21 0.09 0.09µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) <0.01 0.02 <0.01 <0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

Page 243: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

0.02 0.18 6.34 6.98 6.99µg/L0.01----Sum of PFAS

Page 244: Appendix - Department of Defence

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Analytical Results

0902_QC101_0307170902_MW59_0307170902_MW58_3006170902_MW54_3006170902_MW56_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

ES1716548-020ES1716548-019ES1716548-018ES1716548-017ES1716548-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231P: PFAS Sums - Continued

0.02Sum of PFHxS and PFOS 0.09 1.86 1.97 1.97µg/L0.01355-46-4/1763-23-

1

0.02 0.15 5.42 5.77 5.79µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1061.2-Dichloroethane-D4 114 113 107 110%517060-07-0

107Toluene-D8 118 115 107 109%52037-26-5

98.84-Bromofluorobenzene 112 106 103 102%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

30.5Phenol-d6 32.3 35.0 28.3 28.2%113127-88-3

59.22-Chlorophenol-D4 56.9 65.0 60.6 55.0%193951-73-6

68.02.4.6-Tribromophenol 47.8 72.2 62.2 60.0%1118-79-6

EP075(SIM)T: PAH Surrogates

72.42-Fluorobiphenyl 66.1 70.9 58.9 62.8%1321-60-8

98.0Anthracene-d10 86.7 91.3 112 109%11719-06-8

94.74-Terphenyl-d14 63.4 86.7 72.1 71.5%11718-51-0

EP075S: Acid Extractable Surrogates

37.12-Fluorophenol 36.4 36.3 36.9 35.1%2367-12-4

28.4Phenol-d6 30.0 29.4 27.4 28.2%213127-88-3

51.42-Chlorophenol-D4 52.7 52.6 50.8 49.4%293951-73-6

77.72.4.6-Tribromophenol 69.8 66.8 54.4 53.0%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

61.6Nitrobenzene-D5 62.3 64.0 60.7 59.6%24165-60-0

44.31.2-Dichlorobenzene-D4 48.1 47.9 46.6 44.2%22199-69-1

59.32-Fluorobiphenyl 64.1 59.5 58.2 56.0%2321-60-8

89.3Anthracene-d10 80.0 79.2 76.0 72.8%21719-06-8

1044-Terphenyl-d14 83.5 80.1 79.2 71.6%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1071.2-Dichloroethane-D4 115 114 110 111%217060-07-0

111Toluene-D8 122 119 112 113%22037-26-5

1014-Bromofluorobenzene 113 107 105 102%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1261.4-Dioxane-d8 104 124 111 124%0.517647-74-4

EP231S: PFAS Surrogate

71.6 64.1 76.0 62.4 63.8%0.02----13C4-PFOS

Page 245: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EA015: Total Dissolved Solids dried at 180 ± 5 °C

858 4660 1040 4710 ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 ----mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 ----mg/L13812-32-6

387Bicarbonate Alkalinity as CaCO3 138 203 156 ----mg/L171-52-3

387 138 203 156 ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

52Sulfate as SO4 - Turbidimetric 15 15 90 ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

28Chloride 365 360 2820 ----mg/L116887-00-6

ED093F: Dissolved Major Cations

8Calcium 33 15 128 ----mg/L17440-70-2

14Magnesium 27 21 186 ----mg/L17439-95-4

198Sodium 177 242 1200 ----mg/L17440-23-5

<1Potassium 2 1 6 ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.02Aluminium 0.03 0.02 0.02 ----mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 0.002 ----mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 0.0001 ----mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 ----mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 ----mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 ----mg/L0.0017439-92-1

<0.001Manganese 0.983 1.24 2.87 ----mg/L0.0017439-96-5

0.025Nickel 0.020 0.007 0.028 ----mg/L0.0017440-02-0

0.016Zinc 0.052 0.678 0.033 ----mg/L0.0057440-66-6

<0.05Iron 0.32 0.45 2.41 ----mg/L0.057439-89-6

0.3Bromine 0.8 1.0 6.8 ----mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 ----mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.4Fluoride 0.3 0.3 0.4 ----mg/L0.116984-48-8

EN055: Ionic Balance

9.60 13.4 14.5 84.5 ----meq/L0.01----Total Anions

10.2 11.6 13.0 74.0 ----meq/L0.01----Total Cations

Page 246: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EN055: Ionic Balance - Continued

2.83 6.99 5.42 6.62 ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 ----µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 ----µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 ----µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 ----µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 ----µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 ----µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 ----µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 ----µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 ----µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 ----µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 ----µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 ----µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 ----µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 ----µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 ----µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 ----µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 ----µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 ----µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 ----µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 ----µg/L5075-71-8

<50Chloromethane <50 <50 <50 ----µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 ----µg/L5075-01-4

<50Bromomethane <50 <50 <50 ----µg/L5074-83-9

<50Chloroethane <50 <50 <50 ----µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 ----µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 ----µg/L575-35-4

<5Iodomethane <5 <5 <5 ----µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 ----µg/L5156-60-5

Page 247: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP074E: Halogenated Aliphatic Compounds - Continued

<51.1-Dichloroethane <5 <5 <5 ----µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 ----µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 ----µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 ----µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 ----µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 ----µg/L5107-06-2

<5Trichloroethene <5 <5 <5 ----µg/L579-01-6

<5Dibromomethane <5 <5 <5 ----µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 ----µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 ----µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 ----µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 ----µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 ----µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 ----µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 ----µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 ----µg/L596-18-4

<5Pentachloroethane <5 <5 <5 ----µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 ----µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 ----µg/L5108-90-7

<5Bromobenzene <5 <5 <5 ----µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 ----µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 ----µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 ----µg/L587-61-6

EP074G: Trihalomethanes

<5Chloroform <5 <5 <5 ----µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 ----µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 ----µg/L5124-48-1

<5Bromoform <5 <5 <5 ----µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 ----µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 ----µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 ----µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 ----µg/L186-73-7

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<1.0Phenanthrene <1.0 <1.0 <1.0 ----µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 ----µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 ----µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 ----µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 ----µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 ----µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 ----µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 ----µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 ----µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 ----µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 ----µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 ----µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 ----µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 ----µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 ----µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 ----µg/L295-57-8

<22-Methylphenol <2 <2 <2 ----µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 ----µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 ----µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 ----µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 ----µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 ----µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 ----µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 ----µg/L288-06-2

<22.4.5-Trichlorophenol <2 <2 <2 ----µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 ----µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 ----µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 ----µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 ----µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 ----µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 ----µg/L256-49-5

EP075C: Phthalate Esters

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075C: Phthalate Esters - Continued

<2Dimethyl phthalate <2 <2 <2 ----µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 ----µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 ----µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 ----µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 ----µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 ----µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 ----µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 ----µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 ----µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 ----µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 ----µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 ----µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 ----µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 ----µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 ----µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 ----µg/L2109-06-8

<2Acetophenone <2 <2 <2 ----µg/L298-86-2

<2Nitrobenzene <2 <2 <2 ----µg/L298-95-3

<2Isophorone <2 <2 <2 ----µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 ----µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 ----µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 ----µg/L2134-32-7

<24-Nitroquinoline-N-oxide <2 <2 <2 ----µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 ----µg/L299-55-8

<2Azobenzene <2 <2 <2 ----µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 ----µg/L299-35-4

<2Phenacetin <2 <2 <2 ----µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 ----µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 ----µg/L282-68-8

<2Pronamide <2 <2 <2 ----µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 ----µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 ----µg/L2510-15-6

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075E: Nitroaromatics and Ketones - Continued

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 ----µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 ----µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 ----µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 ----µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 ----µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 ----µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 ----µg/L295-50-1

<2Hexachloroethane <2 <2 <2 ----µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 ----µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 ----µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 ----µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 ----µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 ----µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 ----µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 ----µg/L262-53-3

<24-Chloroaniline <2 <2 <2 ----µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 ----µg/L488-74-4

<43-Nitroaniline <4 <4 <4 ----µg/L499-09-2

<2Dibenzofuran <2 <2 <2 ----µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 ----µg/L2100-01-6

<2Carbazole <2 <2 <2 ----µg/L286-74-8

<23.3`-Dichlorobenzidine <2 <2 <2 ----µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 ----µg/L2319-84-6

<2beta-BHC <2 <2 <2 ----µg/L2319-85-7

<2gamma-BHC <2 <2 <2 ----µg/L258-89-9

<2delta-BHC <2 <2 <2 ----µg/L2319-86-8

<2Heptachlor <2 <2 <2 ----µg/L276-44-8

<2Aldrin <2 <2 <2 ----µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 ----µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 ----µg/L2959-98-8

Page 251: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP075I: Organochlorine Pesticides - Continued

<24.4`-DDE <2 <2 <2 ----µg/L272-55-9

<2Dieldrin <2 <2 <2 ----µg/L260-57-1

<2Endrin <2 <2 <2 ----µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 ----µg/L233213-65-9

<24.4`-DDD <2 <2 <2 ----µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 ----µg/L21031-07-8

<44.4`-DDT <4 <4 <4 ----µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 ----µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 ----µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 ----µg/L262-73-7

<2Dimethoate <2 <2 <2 ----µg/L260-51-5

<2Diazinon <2 <2 <2 ----µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 ----µg/L25598-13-0

<2Malathion <2 <2 <2 ----µg/L2121-75-5

<2Fenthion <2 <2 <2 ----µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 ----µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 ----µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 ----µg/L2470-90-6

<2Prothiofos <2 <2 <2 ----µg/L234643-46-4

<2Ethion <2 <2 <2 ----µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 ----µg/L20----C6 - C9 Fraction

<50 <50 <50 <50 ----µg/L50----C10 - C14 Fraction

<100 <100 <100 <100 ----µg/L100----C15 - C28 Fraction

<50 <50 <50 <50 ----µg/L50----C29 - C36 Fraction

<50^ <50 <50 <50 ----µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 ----µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 ----µg/L20C6_C10-BTEX

<100 <100 <100 <100 ----µg/L100---->C10 - C16 Fraction

<100 <100 <100 <100 ----µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 ----µg/L100---->C34 - C40 Fraction

Page 252: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

<100^ <100 <100 <100 ----µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 ----µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 ----µg/L171-43-2

<2Toluene <2 <2 <2 ----µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 ----µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 ----µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 ----µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 ----µg/L21330-20-7

<1^ <1 <1 <1 ----µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 ----µg/L591-20-3

EP116: 1.4-Dioxane

<1.01.4-Dioxane <1.0 <1.0 <1.0 ----µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.12Perfluorobutane sulfonic acid

(PFBS)

0.07 0.52 0.16 ----µg/L0.02375-73-5

0.10Perfluoropentane sulfonic acid

(PFPeS)

0.05 0.36 0.11 ----µg/L0.022706-91-4

0.90Perfluorohexane sulfonic acid

(PFHxS)

0.56 3.82 0.35 ----µg/L0.02355-46-4

<0.05Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 0.10 <0.02 ----µg/L0.02375-92-8

0.13Perfluorooctane sulfonic acid

(PFOS)

0.16 1.21 <0.01 ----µg/L0.011763-23-1

<0.05Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 ----µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.2Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 ----µg/L0.1375-22-4

<0.05Perfluoropentanoic acid (PFPeA) <0.02 0.06 0.04 ----µg/L0.022706-90-3

0.08Perfluorohexanoic acid (PFHxA) 0.10 0.34 0.08 ----µg/L0.02307-24-4

<0.05Perfluoroheptanoic acid (PFHpA) <0.02 0.07 <0.02 ----µg/L0.02375-85-9

<0.05Perfluorooctanoic acid (PFOA) 0.02 0.18 <0.01 ----µg/L0.01335-67-1

<0.05Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 ----µg/L0.02375-95-1

<0.05Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 ----µg/L0.02335-76-2

Page 253: Appendix - Department of Defence

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Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP231B: Perfluoroalkyl Carboxylic Acids - Continued

<0.05Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 ----µg/L0.022058-94-8

<0.05Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 ----µg/L0.02307-55-1

<0.05Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 ----µg/L0.0272629-94-8

<0.12Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 ----µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.05Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 ----µg/L0.02754-91-6

<0.12N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 ----µg/L0.0531506-32-8

<0.12N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 ----µg/L0.054151-50-2

<0.12N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 ----µg/L0.052448-09-7

<0.12N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 ----µg/L0.051691-99-2

<0.05N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 ----µg/L0.022355-31-9

<0.05N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 ----µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 ----µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 ----µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 ----µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 ----µg/L0.05120226-60-0

EP231P: PFAS Sums

1.33 0.96 6.66 0.74 ----µg/L0.01----Sum of PFAS

Page 254: Appendix - Department of Defence

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60547028, task 3.1:Project

AECOM Australia Pty Ltd

Analytical Results

----0902_MW53_0307170902_MW30_0307170902_MW10_3006170902_MW57_030717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

----03-Jul-2017 00:0003-Jul-2017 00:0030-Jun-2017 00:0003-Jul-2017 00:00Client sampling date / time

--------ES1716548-024ES1716548-023ES1716548-022ES1716548-021UnitLORCAS NumberCompound

Result Result Result Result ----

EP231P: PFAS Sums - Continued

1.03Sum of PFHxS and PFOS 0.72 5.03 0.35 ----µg/L0.01355-46-4/1763-23-

1

1.23 0.91 6.20 0.63 ----µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1171.2-Dichloroethane-D4 109 110 110 ----%517060-07-0

119Toluene-D8 109 107 107 ----%52037-26-5

1134-Bromofluorobenzene 108 109 107 ----%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

26.6Phenol-d6 25.0 23.9 25.4 ----%113127-88-3

48.32-Chlorophenol-D4 52.5 44.9 51.1 ----%193951-73-6

57.72.4.6-Tribromophenol 58.9 58.2 55.2 ----%1118-79-6

EP075(SIM)T: PAH Surrogates

54.62-Fluorobiphenyl 57.1 52.8 58.2 ----%1321-60-8

100Anthracene-d10 75.6 84.7 73.6 ----%11719-06-8

71.54-Terphenyl-d14 59.5 64.6 59.1 ----%11718-51-0

EP075S: Acid Extractable Surrogates

33.32-Fluorophenol 34.6 26.6 31.1 ----%2367-12-4

24.9Phenol-d6 27.9 21.1 23.5 ----%213127-88-3

44.12-Chlorophenol-D4 47.3 37.6 41.2 ----%293951-73-6

51.62.4.6-Tribromophenol 47.6 48.1 52.6 ----%2118-79-6

EP075T: Base/Neutral Extractable Surrogates

53.9Nitrobenzene-D5 56.3 46.2 49.7 ----%24165-60-0

39.81.2-Dichlorobenzene-D4 43.9 37.2 43.6 ----%22199-69-1

49.72-Fluorobiphenyl 52.2 46.8 52.4 ----%2321-60-8

65.7Anthracene-d10 63.0 60.3 58.4 ----%21719-06-8

67.54-Terphenyl-d14 67.5 66.9 61.3 ----%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1191.2-Dichloroethane-D4 118 118 118 ----%217060-07-0

124Toluene-D8 112 109 110 ----%22037-26-5

1144-Bromofluorobenzene 113 113 114 ----%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1151.4-Dioxane-d8 99.2 105 126 ----%0.517647-74-4

EP231S: PFAS Surrogate

68.0 116 104 107 ----%0.02----13C4-PFOS

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Surrogate Control Limits

Recovery Limits (%)Sub-Matrix: WATER

Compound CAS Number Low High

EP074S: VOC Surrogates

1.2-Dichloroethane-D4 17060-07-0 78 133

Toluene-D8 2037-26-5 79 129

4-Bromofluorobenzene 460-00-4 81 124

EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 13127-88-3 10 44

2-Chlorophenol-D4 93951-73-6 14 94

2.4.6-Tribromophenol 118-79-6 17 125

EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl 321-60-8 20 104

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 32 112

EP075S: Acid Extractable Surrogates

2-Fluorophenol 367-12-4 10 117

Phenol-d6 13127-88-3 10 69

2-Chlorophenol-D4 93951-73-6 21 130

2.4.6-Tribromophenol 118-79-6 10 151

EP075T: Base/Neutral Extractable Surrogates

Nitrobenzene-D5 4165-60-0 29 142

1.2-Dichlorobenzene-D4 2199-69-1 24 121

2-Fluorobiphenyl 321-60-8 27 135

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 21 123

EP080S: TPH(V)/BTEX Surrogates

1.2-Dichloroethane-D4 17060-07-0 71 137

Toluene-D8 2037-26-5 79 131

4-Bromofluorobenzene 460-00-4 70 128

EP116S: 1.4-Dioxane Surrogate

1.4-Dioxane-d8 17647-74-4 69 127

EP231S: PFAS Surrogate

13C4-PFOS ---- 60 130

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5 5.00True

Environmental

QUALITY CONTROL REPORTWork Order : ES1716548 Page : 1 of 36

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER :Contact Loren Schiavon

:Address LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

Address : 277-289 Woodpark Road Smithfield NSW Australia 2164

::Telephone +61 02 8934 0000 +61 2 8784 8503:Telephone

:Project 60547028, task 3.1 Date Samples Received : 05-Jul-2017

:Order number 60547028 Date Analysis Commenced : 06-Jul-2017

:C-O-C number ---- Issue Date : 13-Jul-2017

Sampler : BEN HUNTER

Site : RAAF Richmond

Quote number : SY/308/17

No. of samples received 24:

No. of samples analysed 24:

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Wisam Marassa Inorganics Coordinator Sydney Inorganics, Smithfield, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 985195)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 2720 2520 7.79 0% - 20%0902_MW08_300617 ES1716548-014

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 986859)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 184 178 3.59 0% - 50%Anonymous ES1716547-001

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 512 538 5.04 0% - 20%0902_MW14_030717 ES1716548-006

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 986860)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 4710 4810 2.27 0% - 20%0902_MW53_030717 ES1716548-024

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 970 953 1.77 0% - 20%Anonymous ME1700927-002

ED037P: Alkalinity by PC Titrator (QC Lot: 983666)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716547-009

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 62 61 2.30 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 62 61 2.30 0% - 20%

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716462-026

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 6 5 0.00 No Limit

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 6 5 0.00 No Limit

ED037P: Alkalinity by PC Titrator (QC Lot: 983668)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_MW15_030717 ES1716548-007

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 212 210 0.955 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 212 210 0.955 0% - 20%

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716577-001

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 24 23 0.00 0% - 20%

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

ED037P: Alkalinity by PC Titrator (QC Lot: 983668) - continued

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 24 23 0.00 0% - 20%Anonymous ES1716577-001

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 983211)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 169 168 0.00 0% - 20%Anonymous ES1716366-001

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 21 21 0.00 0% - 20%Anonymous ES1716547-001

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 983215)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 8 8 0.00 No Limit0902_MW15_030717 ES1716548-007

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 53 54 0.00 0% - 20%0902_MW54_300617 ES1716548-017

ED045G: Chloride by Discrete Analyser (QC Lot: 983212)

ED045G: Chloride 16887-00-6 1 mg/L 1460 1460 0.361 0% - 20%Anonymous ES1716366-001

ED045G: Chloride 16887-00-6 1 mg/L 43 42 0.00 0% - 20%Anonymous ES1716547-001

ED045G: Chloride by Discrete Analyser (QC Lot: 983213)

ED045G: Chloride 16887-00-6 1 mg/L 102 101 1.50 0% - 20%0902_MW15_030717 ES1716548-007

ED045G: Chloride 16887-00-6 1 mg/L 591 590 0.318 0% - 20%0902_MW54_300617 ES1716548-017

ED093F: Dissolved Major Cations (QC Lot: 985858)

ED093F: Calcium 7440-70-2 1 mg/L 20 20 0.00 0% - 50%0902_MW13_030717 ES1716548-005

ED093F: Magnesium 7439-95-4 1 mg/L 12 14 11.6 0% - 50%

ED093F: Sodium 7440-23-5 1 mg/L 208 209 0.00 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L <1 <1 0.00 No Limit

ED093F: Calcium 7440-70-2 1 mg/L 9 9 0.00 No LimitAnonymous ES1716547-001

ED093F: Magnesium 7439-95-4 1 mg/L 6 6 0.00 No Limit

ED093F: Sodium 7440-23-5 1 mg/L 38 36 6.23 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 2 2 0.00 No Limit

ED093F: Dissolved Major Cations (QC Lot: 985861)

ED093F: Calcium 7440-70-2 1 mg/L 72 71 1.62 0% - 20%0902_MW56_030717 ES1716548-016

ED093F: Magnesium 7439-95-4 1 mg/L 127 128 1.48 0% - 20%

ED093F: Sodium 7440-23-5 1 mg/L 447 483 7.75 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 2 2 0.00 No Limit

ED093F: Calcium 7440-70-2 1 mg/L 42 42 0.00 0% - 20%Anonymous ES1716568-002

ED093F: Magnesium 7439-95-4 1 mg/L 96 96 0.00 0% - 20%

ED093F: Sodium 7440-23-5 1 mg/L 1010 1010 0.00 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 18 18 0.00 0% - 50%

EG020F: Dissolved Metals by ICP-MS (QC Lot: 985856)

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW03_030717 ES1716548-003

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L 0.001 0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.895 0.892 0.340 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.005 0.005 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EG020F: Dissolved Metals by ICP-MS (QC Lot: 985856) - continued

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 <0.005 0.00 No Limit0902_MW03_030717 ES1716548-003

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.06 0.08 22.6 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L 0.07 0.07 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L 3.6 3.6 0.00 0% - 20%

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L 0.0003 0.0004 0.00 No LimitAnonymous ES1716547-001

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L 0.003 0.003 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.008 0.007 0.00 No Limit

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.046 0.046 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.04 0.04 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 <0.05 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 <0.1 0.00 No Limit

EG020F: Dissolved Metals by ICP-MS (QC Lot: 985860)

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW08_300617 ES1716548-014

EG020A-F: Arsenic 7440-38-2 0.001 mg/L 0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.982 0.997 1.47 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.016 0.016 0.00 0% - 50%

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.020 0.020 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.01 <0.01 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L 1.53 1.55 0.969 0% - 20%

EG020A-F: Bromine 7726-95-6 0.1 mg/L 2.4 2.4 0.00 0% - 20%

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L 0.0001 0.0001 0.00 No Limit0902_MW53_030717 ES1716548-024

EG020A-F: Arsenic 7440-38-2 0.001 mg/L 0.002 0.002 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 2.87 2.84 0.870 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.028 0.028 0.00 0% - 20%

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.033 0.031 5.70 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.02 0.02 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L 2.41 2.44 1.45 0% - 20%

EG020A-F: Bromine 7726-95-6 0.1 mg/L 6.8 6.6 2.34 0% - 20%

EG035F: Dissolved Mercury by FIMS (QC Lot: 985857)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No LimitAnonymous ES1716547-009

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EG035F: Dissolved Mercury by FIMS (QC Lot: 985857) - continued

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW02_030717 ES1716548-002

EG035F: Dissolved Mercury by FIMS (QC Lot: 985859)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW09_300617 ES1716548-015

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW30_030717 ES1716548-023

EK040P: Fluoride by PC Titrator (QC Lot: 983665)

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.4 0.4 0.00 No LimitAnonymous ES1716547-009

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 <0.1 0.00 No LimitAnonymous ES1716462-026

EK040P: Fluoride by PC Titrator (QC Lot: 983669)

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.4 0.4 0.00 No Limit0902_MW15_030717 ES1716548-007

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 <0.1 0.00 No LimitAnonymous ES1716577-001

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 983652)

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 983654)

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 983654) - continued

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 983652)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 983654)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No LimitAnonymous ES1716547-001

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074C: Sulfonated Compounds (QC Lot: 983652)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074C: Sulfonated Compounds (QC Lot: 983654)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074D: Fumigants (QC Lot: 983652)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

Page 262: Appendix - Department of Defence

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Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074D: Fumigants (QC Lot: 983652) - continued

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074D: Fumigants (QC Lot: 983654)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983652)

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

Page 263: Appendix - Department of Defence

8 of 36:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983652) - continued

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654)

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

Page 264: Appendix - Department of Defence

9 of 36:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654) - continued

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

Page 265: Appendix - Department of Defence

10 of 36:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 983654) - continued

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 983652)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 983654)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 983652)

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 983654)

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

Page 266: Appendix - Department of Defence

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Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074G: Trihalomethanes (QC Lot: 983654) - continued

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No LimitAnonymous ES1716547-001

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_MW53_030717 ES1716548-024

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 983651)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_MW01_030717 ES1716548-001

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_QC501_300617 ES1716548-012

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 983653)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716547-001

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_MW53_030717 ES1716548-024

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 987359)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716694-002

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716694-001

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 983651)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_MW01_030717 ES1716548-001

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_QC501_300617 ES1716548-012

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 983653)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716547-001

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_MW53_030717 ES1716548-024

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 987359)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716694-002

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716694-001

EP080: BTEXN (QC Lot: 983651)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_MW01_030717 ES1716548-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_QC501_300617 ES1716548-012

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

Page 267: Appendix - Department of Defence

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Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP080: BTEXN (QC Lot: 983651) - continued

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP080: BTEXN (QC Lot: 983653)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716547-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_MW53_030717 ES1716548-024

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: BTEXN (QC Lot: 987359)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716694-002

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716694-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP116: 1.4-Dioxane (QC Lot: 984488)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_MW01_030717 ES1716548-001

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_QC501_300617 ES1716548-012

EP116: 1.4-Dioxane (QC Lot: 984491)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No LimitAnonymous ES1716547-001

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <1.0 <1.0 0.00 No Limit0902_MW30_030717 ES1716548-023

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 984234)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_MW01_030717 ES1716548-001

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 984234) - continued

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.04 0.04 0.00 No Limit0902_MW01_030717 ES1716548-001

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.02 0.02 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.11 0.11 0.00 No Limit

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 984235)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 0.16 0.16 0.00 0% - 50%0902_MW10_300617 ES1716548-022

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.07 0.07 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.05 0.05 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.56 0.55 1.97 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984234)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_MW01_030717 ES1716548-001

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984234) - continued

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984235)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.02 0.02 0.00 No Limit0902_MW10_300617 ES1716548-022

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.10 0.09 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 984234)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW01_030717 ES1716548-001

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 984235)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW10_300617 ES1716548-022

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 984234)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW01_030717 ES1716548-001

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 984235)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW10_300617 ES1716548-022

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231P: PFAS Sums (QC Lot: 984234)

EP231X: Sum of PFAS ---- 0.01 µg/L 0.17 0.17 0.00 0% - 50%0902_MW01_030717 ES1716548-001

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231P: PFAS Sums (QC Lot: 984234) - continued

EP231X: Sum of PFAS ---- 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_QC501_300617 ES1716548-012

EP231P: PFAS Sums (QC Lot: 984235)

EP231X: Sum of PFAS ---- 0.01 µg/L 0.96 0.94 2.10 0% - 20%0902_MW10_300617 ES1716548-022

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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 985195)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1012000 mg/L 10987

<10 102293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 986859)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1002000 mg/L 10987

<10 92.3293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 986860)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1052000 mg/L 10987

<10 82.1293 mg/L 12666

ED037P: Alkalinity by PC Titrator (QCLot: 983666)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 97.7200 mg/L 11181

ED037P: Alkalinity by PC Titrator (QCLot: 983668)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 97.6200 mg/L 11181

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983211)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 90.025 mg/L 12282

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983215)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 87.625 mg/L 12282

ED045G: Chloride by Discrete Analyser (QCLot: 983212)

ED045G: Chloride 16887-00-6 1 mg/L <1 90.710 mg/L 12781

<1 94.41000 mg/L 12781

ED045G: Chloride by Discrete Analyser (QCLot: 983213)

ED045G: Chloride 16887-00-6 1 mg/L <1 85.010 mg/L 12781

<1 93.51000 mg/L 12781

ED093F: Dissolved Major Cations (QCLot: 985858)

ED093F: Calcium 7440-70-2 1 mg/L <1 90.850 mg/L 11480

ED093F: Magnesium 7439-95-4 1 mg/L <1 91.750 mg/L 11690

ED093F: Sodium 7440-23-5 1 mg/L <1 10250 mg/L 12082

ED093F: Potassium 7440-09-7 1 mg/L <1 10450 mg/L 11385

ED093F: Dissolved Major Cations (QCLot: 985861)

ED093F: Calcium 7440-70-2 1 mg/L <1 91.250 mg/L 11480

ED093F: Magnesium 7439-95-4 1 mg/L <1 100.050 mg/L 11690

ED093F: Sodium 7440-23-5 1 mg/L <1 95.850 mg/L 12082

ED093F: Potassium 7440-09-7 1 mg/L <1 98.050 mg/L 11385

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856)

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Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856) - continued

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 91.90.5 mg/L 11680

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 94.40.1 mg/L 11485

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 92.40.1 mg/L 11084

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 91.60.1 mg/L 11185

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 89.80.1 mg/L 11181

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 90.40.1 mg/L 11183

EG020A-F: Manganese 7439-96-5 0.001 mg/L <0.001 91.00.1 mg/L 11082

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 90.60.1 mg/L 11282

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 90.60.1 mg/L 11781

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 91.80.5 mg/L 11282

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 -------- --------

EG020F: Dissolved Metals by ICP-MS (QCLot: 985860)

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 90.10.5 mg/L 11680

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 94.50.1 mg/L 11485

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 90.20.1 mg/L 11084

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 91.80.1 mg/L 11185

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 89.30.1 mg/L 11181

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 90.20.1 mg/L 11183

EG020A-F: Manganese 7439-96-5 0.001 mg/L <0.001 88.10.1 mg/L 11082

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 89.80.1 mg/L 11282

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 88.30.1 mg/L 11781

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 92.90.5 mg/L 11282

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 -------- --------

EG035F: Dissolved Mercury by FIMS (QCLot: 985857)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 98.70.01 mg/L 10583

EG035F: Dissolved Mercury by FIMS (QCLot: 985859)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 1020.01 mg/L 10583

EK040P: Fluoride by PC Titrator (QCLot: 983665)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1065 mg/L 11682

EK040P: Fluoride by PC Titrator (QCLot: 983669)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1085 mg/L 11682

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 983652)

EP074: Styrene 100-42-5 5 µg/L <5 90.010 µg/L 11973

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 90.410 µg/L 11876

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 86.610 µg/L 11969

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 86.410 µg/L 11674

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 86.210 µg/L 11973

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 85.410 µg/L 11674

Page 274: Appendix - Department of Defence

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 983652) - continued

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 93.010 µg/L 11672

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 82.610 µg/L 11971

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 80.610 µg/L 12365

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 983654)

EP074: Styrene 100-42-5 5 µg/L <5 93.810 µg/L 11973

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 90.910 µg/L 11876

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 76.310 µg/L 11969

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 81.610 µg/L 11674

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 79.810 µg/L 11973

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 82.210 µg/L 11674

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 82.110 µg/L 11672

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 80.010 µg/L 11971

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 71.310 µg/L 12365

EP074B: Oxygenated Compounds (QCLot: 983652)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 62.2100 µg/L 13461

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 89.6100 µg/L 13074

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 87.2100 µg/L 13266

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 86.5100 µg/L 13765

EP074B: Oxygenated Compounds (QCLot: 983654)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 81.4100 µg/L 13461

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 80.6100 µg/L 13074

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 97.9100 µg/L 13266

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 91.1100 µg/L 13765

EP074C: Sulfonated Compounds (QCLot: 983652)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 87.710 µg/L 12773

EP074C: Sulfonated Compounds (QCLot: 983654)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 75.010 µg/L 12773

EP074D: Fumigants (QCLot: 983652)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 81.510 µg/L 12268

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 93.210 µg/L 11876

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 88.710 µg/L 12062

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 89.210 µg/L 11460

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 91.410 µg/L 11769

EP074D: Fumigants (QCLot: 983654)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 90.210 µg/L 12268

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 90.810 µg/L 11876

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 80.210 µg/L 12062

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 84.310 µg/L 11460

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074D: Fumigants (QCLot: 983654) - continued

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 98.410 µg/L 11769

EP074E: Halogenated Aliphatic Compounds (QCLot: 983652)

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 64.3100 µg/L 13861

EP074: Chloromethane 74-87-3 50 µg/L <50 84.1100 µg/L 13067

EP074: Vinyl chloride 75-01-4 50 µg/L <50 85.2100 µg/L 12969

EP074: Bromomethane 74-83-9 50 µg/L <50 90.3100 µg/L 14056

EP074: Chloroethane 75-00-3 50 µg/L <50 93.1100 µg/L 13961

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 86.1100 µg/L 13169

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 88.310 µg/L 12470

EP074: Iodomethane 74-88-4 5 µg/L <5 82.810 µg/L 12870

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 89.510 µg/L 11874

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 92.010 µg/L 12074

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 91.810 µg/L 11977

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 91.510 µg/L 11967

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 86.910 µg/L 11973

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 87.510 µg/L 12062

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 93.910 µg/L 12373

EP074: Trichloroethene 79-01-6 5 µg/L <5 87.110 µg/L 11876

EP074: Dibromomethane 74-95-3 5 µg/L <5 94.310 µg/L 11973

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 92.510 µg/L 12672

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 94.810 µg/L 12971

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 88.610 µg/L 12472

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 92.110 µg/L 11466

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 75.710 µg/L 12060

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 74.810 µg/L 12871

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 89.810 µg/L 12470

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 89.010 µg/L 12674

EP074: Pentachloroethane 76-01-7 5 µg/L <5 95.710 µg/L 12672

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 81.010 µg/L 13666

EP074E: Halogenated Aliphatic Compounds (QCLot: 983654)

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 63.6100 µg/L 13861

EP074: Chloromethane 74-87-3 50 µg/L <50 80.6100 µg/L 13067

EP074: Vinyl chloride 75-01-4 50 µg/L <50 98.6100 µg/L 12969

EP074: Bromomethane 74-83-9 50 µg/L <50 109100 µg/L 14056

EP074: Chloroethane 75-00-3 50 µg/L <50 85.5100 µg/L 13961

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 88.4100 µg/L 13169

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 83.010 µg/L 12470

EP074: Iodomethane 74-88-4 5 µg/L <5 12410 µg/L 12870

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 91.210 µg/L 11874

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074E: Halogenated Aliphatic Compounds (QCLot: 983654) - continued

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 93.810 µg/L 12074

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 97.010 µg/L 11977

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 93.510 µg/L 11967

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 88.910 µg/L 11973

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 83.410 µg/L 12062

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 10610 µg/L 12373

EP074: Trichloroethene 79-01-6 5 µg/L <5 95.710 µg/L 11876

EP074: Dibromomethane 74-95-3 5 µg/L <5 98.710 µg/L 11973

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 94.110 µg/L 12672

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 95.010 µg/L 12971

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 91.810 µg/L 12472

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 88.810 µg/L 11466

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 81.810 µg/L 12060

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 77.410 µg/L 12871

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 10610 µg/L 12470

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 11210 µg/L 12674

EP074: Pentachloroethane 76-01-7 5 µg/L <5 76.310 µg/L 12672

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 87.410 µg/L 13666

EP074F: Halogenated Aromatic Compounds (QCLot: 983652)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 94.510 µg/L 11779

EP074: Bromobenzene 108-86-1 5 µg/L <5 94.510 µg/L 11676

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 91.310 µg/L 11973

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 90.910 µg/L 11973

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 94.810 µg/L 12367

EP074F: Halogenated Aromatic Compounds (QCLot: 983654)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 96.710 µg/L 11779

EP074: Bromobenzene 108-86-1 5 µg/L <5 87.310 µg/L 11676

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 83.110 µg/L 11973

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 82.810 µg/L 11973

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 91.610 µg/L 12367

EP074G: Trihalomethanes (QCLot: 983652)

EP074: Chloroform 67-66-3 5 µg/L <5 92.210 µg/L 12072

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 93.310 µg/L 11864

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 94.310 µg/L 11565

EP074: Bromoform 75-25-2 5 µg/L <5 93.210 µg/L 12674

EP074G: Trihalomethanes (QCLot: 983654)

EP074: Chloroform 67-66-3 5 µg/L <5 10310 µg/L 12072

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 86.910 µg/L 11864

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Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074G: Trihalomethanes (QCLot: 983654) - continued

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 85.710 µg/L 11565

EP074: Bromoform 75-25-2 5 µg/L <5 99.210 µg/L 12674

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 982918)

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 64.05 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 65.25 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 63.55 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 64.85 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 84.25 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 76.55 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 72.15 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 72.05 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 72.95 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 67.05 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 70.25 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 65.25 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 72.45 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 71.15 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 70.85 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 70.55 µg/L 11859

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 982930)

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 75.25 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 65.15 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 63.75 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 71.45 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 70.75 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 75.35 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 71.75 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 71.15 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 72.65 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 67.55 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 68.65 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 68.65 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 72.35 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 71.25 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 70.75 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 70.55 µg/L 11859

EP075A: Phenolic Compounds (QCLot: 982917)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075A: Phenolic Compounds (QCLot: 982917) - continued

EP075: Phenol 108-95-2 2 µg/L <2 44.25 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 66.45 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 57.25 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 56.210 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 78.05 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 # 45.45 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 75.45 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 75.25 µg/L 10862

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 75.15 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 78.55 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 79.75 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 80.810 µg/L 9513

EP075A: Phenolic Compounds (QCLot: 982928)

EP075: Phenol 108-95-2 2 µg/L <2 38.25 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 61.95 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 52.65 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 53.010 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 66.05 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 56.65 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 69.95 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 69.65 µg/L 10862

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 72.75 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 73.85 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 76.45 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 71.710 µg/L 9513

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 982917)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 78.25 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 74.45 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 84.65 µg/L 11060

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 85.45 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 81.55 µg/L 11060

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 982928)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 68.45 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 73.05 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 89.95 µg/L 11060

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 85.95 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 84.15 µg/L 11060

EP075C: Phthalate Esters (QCLot: 982917)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075C: Phthalate Esters (QCLot: 982917) - continued

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 84.15 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 84.05 µg/L 11167

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 87.05 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 81.75 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 92.45 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 85.65 µg/L 11562

EP075C: Phthalate Esters (QCLot: 982928)

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 80.45 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 77.75 µg/L 11167

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 90.75 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 86.25 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 96.35 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 85.85 µg/L 11562

EP075D: Nitrosamines (QCLot: 982917)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 59.45 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 68.15 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 61.65 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 61.25 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 73.45 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 74.65 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 82.05 µg/L 10863

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 83.610 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 31.55 µg/L 12523

EP075D: Nitrosamines (QCLot: 982928)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 69.45 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 64.25 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 58.05 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 60.25 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 71.65 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 71.35 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 84.45 µg/L 10863

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 73.310 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 38.25 µg/L 12523

EP075E: Nitroaromatics and Ketones (QCLot: 982917)

EP075: 2-Picoline 109-06-8 2 µg/L <2 45.25 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 73.35 µg/L 11268

Page 280: Appendix - Department of Defence

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075E: Nitroaromatics and Ketones (QCLot: 982917) - continued

EP075: Nitrobenzene 98-95-3 2 µg/L <2 70.45 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 73.35 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 83.75 µg/L 11364

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 82.95 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 81.25 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 # 98.25 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 86.35 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 82.75 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 86.85 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 88.15 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 95.85 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 83.45 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 85.65 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 79.75 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 86.85 µg/L 11058

EP075E: Nitroaromatics and Ketones (QCLot: 982928)

EP075: 2-Picoline 109-06-8 2 µg/L <2 52.85 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 70.85 µg/L 11268

EP075: Nitrobenzene 98-95-3 2 µg/L <2 69.85 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 75.65 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 84.75 µg/L 11364

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 77.45 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 79.45 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 87.65 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 80.65 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 78.65 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 83.15 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 85.95 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 93.65 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 79.95 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 84.95 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 83.25 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 85.85 µg/L 11058

EP075F: Haloethers (QCLot: 982917)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 72.65 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 71.55 µg/L 11166

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 82.95 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 84.45 µg/L 10862

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075F: Haloethers (QCLot: 982928)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 # 68.05 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 67.45 µg/L 11166

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 73.65 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 76.95 µg/L 10862

EP075G: Chlorinated Hydrocarbons (QCLot: 982917)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 68.25 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 67.45 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 64.25 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 67.15 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 72.65 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 72.45 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 72.25 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 68.65 µg/L 10724

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 79.15 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 79.45 µg/L 11066

EP075G: Chlorinated Hydrocarbons (QCLot: 982928)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 62.25 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 60.35 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 59.15 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 60.55 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 61.25 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 63.45 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 63.65 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 59.45 µg/L 10724

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 68.75 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 74.05 µg/L 11066

EP075H: Anilines and Benzidines (QCLot: 982917)

EP075: Aniline 62-53-3 2 µg/L <2 70.65 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 73.85 µg/L 10642

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 80.45 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 83.85 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 80.65 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 85.05 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 87.15 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 1015 µg/L 11960

EP075H: Anilines and Benzidines (QCLot: 982928)

EP075: Aniline 62-53-3 2 µg/L <2 66.05 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 67.55 µg/L 10642

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075H: Anilines and Benzidines (QCLot: 982928) - continued

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 76.95 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 76.05 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 71.75 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 81.55 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 89.95 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 1125 µg/L 11960

EP075I: Organochlorine Pesticides (QCLot: 982917)

EP075: alpha-BHC 319-84-6 2 µg/L <2 80.85 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 85.15 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 86.45 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 80.95 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 78.45 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 81.15 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 80.95 µg/L 11850

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 83.45 µg/L 11159

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 76.25 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 82.45 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 89.05 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 83.95 µg/L 11654

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 84.35 µg/L 11555

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 89.15 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 83.35 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075I: Organochlorine Pesticides (QCLot: 982928)

EP075: alpha-BHC 319-84-6 2 µg/L <2 77.15 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 84.75 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 81.15 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 83.05 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 82.05 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 87.25 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 83.25 µg/L 11850

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 90.05 µg/L 11159

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 85.05 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 88.45 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 92.35 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 85.65 µg/L 11654

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075I: Organochlorine Pesticides (QCLot: 982928) - continued

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 85.55 µg/L 11555

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 88.65 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 89.85 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075J: Organophosphorus Pesticides (QCLot: 982917)

EP075: Dichlorvos 62-73-7 2 µg/L <2 87.55 µg/L 11351

EP075: Dimethoate 60-51-5 2 µg/L <2 90.65 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 86.75 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 82.35 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 99.95 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 86.25 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 84.85 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 85.85 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 87.05 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 82.35 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 81.55 µg/L 11751

EP075J: Organophosphorus Pesticides (QCLot: 982928)

EP075: Dichlorvos 62-73-7 2 µg/L <2 84.65 µg/L 11351

EP075: Dimethoate 60-51-5 2 µg/L <2 83.65 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 90.55 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 84.25 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 1025 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 87.15 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 84.95 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 86.95 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 88.75 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 88.45 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 84.85 µg/L 11751

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982919)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 90.32000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 86.73000 µg/L 10983

EP071: C29 - C36 Fraction ---- 50 µg/L <50 85.92000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982929)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 94.92000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 94.83000 µg/L 10983

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP080/071: Total Petroleum Hydrocarbons (QCLot: 982929) - continued

EP071: C29 - C36 Fraction ---- 50 µg/L <50 98.62000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983651)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 91.9260 µg/L 12775

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983653)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 94.4260 µg/L 12775

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987359)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 78.5260 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982919)

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 84.42500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 86.33500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 1101500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 982929)

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 99.72500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 86.33500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 1111500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983651)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 91.9310 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983653)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 94.3310 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987359)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 80.3310 µg/L 12775

EP080: BTEXN (QCLot: 983651)

EP080: Benzene 71-43-2 1 µg/L <1 10110 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 95.410 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 95.110 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 91.110 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 91.410 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 88.510 µg/L 12070

EP080: BTEXN (QCLot: 983653)

EP080: Benzene 71-43-2 1 µg/L <1 98.010 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 92.210 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 90.210 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 92.010 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 97.610 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 97.910 µg/L 12070

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP080: BTEXN (QCLot: 987359)

EP080: Benzene 71-43-2 1 µg/L <1 84.710 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 86.410 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 85.010 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 82.810 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 86.610 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 97.010 µg/L 12070

EP116: 1.4-Dioxane (QCLot: 984488)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 10610 µg/L 11979

EP116: 1.4-Dioxane (QCLot: 984491)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 10110 µg/L 11979

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984234)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 1250.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 89.40.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 94.00.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 95.00.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 92.80.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 98.80.5 µg/L 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984235)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 1010.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 96.20.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1140.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 1120.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1010.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 1140.5 µg/L 13070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984234)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 89.42.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 90.20.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 97.40.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 97.00.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1010.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 95.20.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 97.00.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1090.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1070.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 1030.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 99.01.25 µg/L 15070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984235)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984235) - continued

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 87.22.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 98.40.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1040.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1020.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1150.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 1040.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 99.60.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1060.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1250.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 1070.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 99.81.25 µg/L 15070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984234)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1180.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 96.01.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 87.31.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 98.01.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 88.31.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1150.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 1160.5 µg/L 13070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984235)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1110.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 1021.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 86.51.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 1111.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 86.21.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 90.00.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 1010.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984234)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 98.40.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1080.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1000.5 µg/L 13070

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Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984234) - continued

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 1110.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984235)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 1000.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1040.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1080.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 1230.5 µg/L 13070

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983211)

Anonymous ES1716366-001 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric # Not

Determined

10 mg/L 13070

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 983215)

0902_MW15_030717 ES1716548-007 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric 91.310 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 983212)

Anonymous ES1716366-001 16887-00-6ED045G: Chloride # Not

Determined

250 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 983213)

0902_MW15_030717 ES1716548-007 16887-00-6ED045G: Chloride 119250 mg/L 13070

EG020F: Dissolved Metals by ICP-MS (QCLot: 985856)

Anonymous ES1716547-009 7440-38-2EG020A-F: Arsenic 1211 mg/L 13070

7440-43-9EG020A-F: Cadmium 1180.25 mg/L 13070

7440-47-3EG020A-F: Chromium 1111 mg/L 13070

7440-50-8EG020A-F: Copper 1111 mg/L 13070

7439-92-1EG020A-F: Lead 1141 mg/L 13070

7439-96-5EG020A-F: Manganese 1121 mg/L 13070

7440-02-0EG020A-F: Nickel 1101 mg/L 13070

7440-66-6EG020A-F: Zinc 1221 mg/L 13070

EG020F: Dissolved Metals by ICP-MS (QCLot: 985860)

0902_MW09_300617 ES1716548-015 7440-38-2EG020A-F: Arsenic 1121 mg/L 13070

7440-43-9EG020A-F: Cadmium 98.50.25 mg/L 13070

7440-47-3EG020A-F: Chromium 1201 mg/L 13070

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EG020F: Dissolved Metals by ICP-MS (QCLot: 985860) - continued

0902_MW09_300617 ES1716548-015 7440-50-8EG020A-F: Copper 1061 mg/L 13070

7439-92-1EG020A-F: Lead 1031 mg/L 13070

7439-96-5EG020A-F: Manganese 1051 mg/L 13070

7440-02-0EG020A-F: Nickel 1081 mg/L 13070

7440-66-6EG020A-F: Zinc 92.01 mg/L 13070

EG035F: Dissolved Mercury by FIMS (QCLot: 985857)

Anonymous ES1716547-001 7439-97-6EG035F: Mercury 76.50.01 mg/L 13070

EG035F: Dissolved Mercury by FIMS (QCLot: 985859)

0902_MW08_300617 ES1716548-014 7439-97-6EG035F: Mercury 91.00.01 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 983665)

Anonymous ES1716462-026 16984-48-8EK040P: Fluoride 89.45 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 983669)

0902_MW15_030717 ES1716548-007 16984-48-8EK040P: Fluoride 84.45 mg/L 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 983652)

0902_MW01_030717 ES1716548-001 75-35-4EP074: 1.1-Dichloroethene 83.925 µg/L 13070

79-01-6EP074: Trichloroethene 98.325 µg/L 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 983654)

Anonymous ES1716547-001 75-35-4EP074: 1.1-Dichloroethene 72.225 µg/L 13070

79-01-6EP074: Trichloroethene 89.025 µg/L 13070

EP074F: Halogenated Aromatic Compounds (QCLot: 983652)

0902_MW01_030717 ES1716548-001 108-90-7EP074: Chlorobenzene 10225 µg/L 13070

EP074F: Halogenated Aromatic Compounds (QCLot: 983654)

Anonymous ES1716547-001 108-90-7EP074: Chlorobenzene 99.125 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983651)

0902_MW01_030717 ES1716548-001 ----EP080: C6 - C9 Fraction 113325 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 983653)

Anonymous ES1716547-001 ----EP080: C6 - C9 Fraction 125325 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987359)

Anonymous ES1716694-002 ----EP080: C6 - C9 Fraction 93.4325 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983651)

0902_MW01_030717 ES1716548-001 C6_C10EP080: C6 - C10 Fraction 105375 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 983653)

Anonymous ES1716547-001 C6_C10EP080: C6 - C10 Fraction 125375 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987359)

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987359) - continued

Anonymous ES1716694-002 C6_C10EP080: C6 - C10 Fraction 91.0375 µg/L 13070

EP080: BTEXN (QCLot: 983651)

0902_MW01_030717 ES1716548-001 71-43-2EP080: Benzene 11125 µg/L 13070

108-88-3EP080: Toluene 10125 µg/L 13070

100-41-4EP080: Ethylbenzene 10125 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 98.525 µg/L 13070

95-47-6EP080: ortho-Xylene 10025 µg/L 13070

91-20-3EP080: Naphthalene 95.725 µg/L 13070

EP080: BTEXN (QCLot: 983653)

Anonymous ES1716547-001 71-43-2EP080: Benzene 99.925 µg/L 13070

108-88-3EP080: Toluene 10625 µg/L 13070

100-41-4EP080: Ethylbenzene 11725 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 11825 µg/L 13070

95-47-6EP080: ortho-Xylene 12125 µg/L 13070

91-20-3EP080: Naphthalene 10625 µg/L 13070

EP080: BTEXN (QCLot: 987359)

Anonymous ES1716694-002 71-43-2EP080: Benzene 84.125 µg/L 13070

108-88-3EP080: Toluene 84.925 µg/L 13070

100-41-4EP080: Ethylbenzene 84.625 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 82.825 µg/L 13070

95-47-6EP080: ortho-Xylene 87.225 µg/L 13070

91-20-3EP080: Naphthalene 96.625 µg/L 13070

EP116: 1.4-Dioxane (QCLot: 984488)

0902_MW02_030717 ES1716548-002 123-91-1EP116: 1.4-Dioxane 91.810 µg/L 12080

EP116: 1.4-Dioxane (QCLot: 984491)

Anonymous ES1716547-009 123-91-1EP116: 1.4-Dioxane 11010 µg/L 12080

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984234)

0902_MW01_030717 ES1716548-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 91.60.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 72.20.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 78.00.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 79.60.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 77.20.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 87.00.5 µg/L 13050

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984235)

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984235) - continued

0902_MW10_300617 ES1716548-022 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1100.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 99.20.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 1030.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1190.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 1230.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1230.5 µg/L 13050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984234)

0902_MW01_030717 ES1716548-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 73.62.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 97.80.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 65.60.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 57.80.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 79.80.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 73.80.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 67.80.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 71.60.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 70.60.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 59.20.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 63.51.25 µg/L 15050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984235)

0902_MW10_300617 ES1716548-022 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 95.92.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 90.80.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 1030.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1030.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 1170.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 1010.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 1020.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 59.40.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 56.80.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1240.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 1171.25 µg/L 15050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984234)

0902_MW01_030717 ES1716548-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 75.00.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

81.31.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 81.11.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

78.31.25 µg/L 15050

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984234) - continued

0902_MW01_030717 ES1716548-001 1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

68.31.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

67.60.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

73.60.5 µg/L 13050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984235)

0902_MW10_300617 ES1716548-022 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1190.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

83.61.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1021.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

71.91.25 µg/L 15050

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

96.41.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

55.60.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

62.20.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984234)

0902_MW01_030717 ES1716548-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1020.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 95.00.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 85.20.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 66.20.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984235)

0902_MW10_300617 ES1716548-022 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 1190.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 97.00.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 1120.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 1140.5 µg/L 13050

Page 292: Appendix - Department of Defence

True

Environmental

QA/QC Compliance Assessment to assist with Quality ReviewWork Order : ES1716548 Page : 1 of 25

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER Telephone : +61 2 8784 8503

:Project 60547028, task 3.1 Date Samples Received : 05-Jul-2017

Site : RAAF Richmond Issue Date : 13-Jul-2017

BEN HUNTER:Sampler No. of samples received : 24

:Order number 60547028 No. of samples analysed : 24

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l Laboratory Control outliers exist - please see following pages for full details.

l Matrix Spike outliers exist - please see following pages for full details.

l Surrogate recovery outliers exist for all regular sample matrices - please see following pages for full details.

Outliers : Analysis Holding Time Compliance

l NO Analysis Holding Time Outliers exist.

Outliers : Frequency of Quality Control Samples

l Quality Control Sample Frequency Outliers exist - please see following pages for full details.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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Outliers : Quality Control Samples

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Laboratory Control Spike (LCS) Recoveries

QC-982917-002 105-67-92.4-Dimethylphenol---- Recovery less than lower control limit50-94%45.4 %EP075A: Phenolic Compounds

QC-982917-002 56-57-54-Nitroquinoline-N-oxid

e

---- Recovery greater than upper control

limit

40-96%98.2 %EP075E: Nitroaromatics and Ketones

QC-982928-002 111-44-4Bis(2-chloroethyl) ether---- Recovery less than lower control limit69-112%68.0 %EP075F: Haloethers

Matrix Spike (MS) Recoveries

ES1716366--001 14808-79-8Sulfate as SO4 -

Turbidimetric

Anonymous MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

ES1716366--001 16887-00-6ChlorideAnonymous MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED045G: Chloride by Discrete Analyser

Regular Sample Surrogates

Sub-Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Samples Submitted

ES1716548-008 93951-73-62-Chlorophenol-D40902_MW17_030717 Recovery less than lower data quality

objective

14-94 %EP075(SIM)S: Phenolic Compound Surrogates 13.9 %

Outliers : Frequency of Quality Control Samples

Matrix: WATER

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 10.000 23

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 10.000 25

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 10.000 23

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 5.000 23

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 5.000 25

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 5.000 23

Analysis Holding Time Compliance

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.

This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA015: Total Dissolved Solids dried at 180 ± 5 °C

Clear Plastic Bottle - Natural (EA015H)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_MW57_030717,

0902_MW30_030717, 0902_MW53_030717

10-Jul-2017---- 10-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EA015H)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

07-Jul-2017---- 07-Jul-2017----30-Jun-2017 ---- ü

ED037P: Alkalinity by PC Titrator

Clear Plastic Bottle - Natural (ED037-P)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_MW57_030717,

0902_MW30_030717, 0902_MW53_030717

17-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED037-P)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-2017---- 06-Jul-2017----30-Jun-2017 ---- ü

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

Clear Plastic Bottle - Natural (ED041G)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_MW57_030717,

0902_MW30_030717, 0902_MW53_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED041G)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

28-Jul-2017---- 06-Jul-2017----30-Jun-2017 ---- ü

Page 295: Appendix - Department of Defence

4 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

ED045G: Chloride by Discrete Analyser

Clear Plastic Bottle - Natural (ED045G)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_MW57_030717,

0902_MW30_030717, 0902_MW53_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED045G)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

28-Jul-2017---- 06-Jul-2017----30-Jun-2017 ---- ü

ED093F: Dissolved Major Cations

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

31-Jul-2017---- 08-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

28-Jul-2017---- 08-Jul-2017----30-Jun-2017 ---- ü

Page 296: Appendix - Department of Defence

5 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EG020F: Dissolved Metals by ICP-MS

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

30-Dec-2017---- 08-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

27-Dec-2017---- 08-Jul-2017----30-Jun-2017 ---- ü

EG035F: Dissolved Mercury by FIMS

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

31-Jul-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

28-Jul-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

Page 297: Appendix - Department of Defence

6 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK040P: Fluoride by PC Titrator

Clear Plastic Bottle - Natural (EK040P)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_MW57_030717,

0902_MW30_030717, 0902_MW53_030717

31-Jul-2017---- 06-Jul-2017----03-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK040P)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

28-Jul-2017---- 06-Jul-2017----30-Jun-2017 ---- ü

EP074A: Monocyclic Aromatic Hydrocarbons

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

Page 298: Appendix - Department of Defence

7 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074B: Oxygenated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

EP074C: Sulfonated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

Page 299: Appendix - Department of Defence

8 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074D: Fumigants

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

EP074E: Halogenated Aliphatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

Page 300: Appendix - Department of Defence

9 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074F: Halogenated Aromatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

EP074G: Trihalomethanes

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

Page 301: Appendix - Department of Defence

10 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

EP075A: Phenolic Compounds

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

Page 302: Appendix - Department of Defence

11 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

EP075C: Phthalate Esters

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

Page 303: Appendix - Department of Defence

12 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075D: Nitrosamines

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

EP075E: Nitroaromatics and Ketones

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

Page 304: Appendix - Department of Defence

13 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075F: Haloethers

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

EP075G: Chlorinated Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075H: Anilines and Benzidines

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

EP075I: Organochlorine Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075J: Organophosphorus Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Petroleum Hydrocarbons

Amber Glass Bottle - Unpreserved (EP071)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_QC507_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

Amber Glass Bottle - Unpreserved (EP071)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

15-Aug-201710-Jul-2017 07-Jul-201706-Jul-201703-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

15-Aug-201707-Jul-2017 07-Jul-201706-Jul-201730-Jun-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_QC507_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080: BTEXN

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-201717-Jul-2017 07-Jul-201707-Jul-201703-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_QC507_040717 18-Jul-201718-Jul-2017 11-Jul-201711-Jul-201704-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-201714-Jul-2017 07-Jul-201707-Jul-201730-Jun-2017 ü ü

EP116: 1.4-Dioxane

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717, 0902_MW30_030717,

0902_MW53_030717

17-Jul-2017---- 07-Jul-2017----03-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617, 0902_MW10_300617

14-Jul-2017---- 07-Jul-2017----30-Jun-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231A: Perfluoroalkyl Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_MW30_030717, 0902_MW53_030717 30-Dec-2017---- 09-Jul-2017----03-Jul-2017 ---- üHDPE (no PTFE) (EP231X)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717

30-Dec-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW10_300617 27-Dec-2017---- 09-Jul-2017----30-Jun-2017 ---- üHDPE (no PTFE) (EP231X)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617

27-Dec-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

EP231B: Perfluoroalkyl Carboxylic Acids

HDPE (no PTFE) (EP231X)

0902_MW30_030717, 0902_MW53_030717 30-Dec-2017---- 09-Jul-2017----03-Jul-2017 ---- üHDPE (no PTFE) (EP231X)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717

30-Dec-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW10_300617 27-Dec-2017---- 09-Jul-2017----30-Jun-2017 ---- üHDPE (no PTFE) (EP231X)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617

27-Dec-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231C: Perfluoroalkyl Sulfonamides

HDPE (no PTFE) (EP231X)

0902_MW30_030717, 0902_MW53_030717 30-Dec-2017---- 09-Jul-2017----03-Jul-2017 ---- üHDPE (no PTFE) (EP231X)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717

30-Dec-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW10_300617 27-Dec-2017---- 09-Jul-2017----30-Jun-2017 ---- üHDPE (no PTFE) (EP231X)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617

27-Dec-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

EP231D: (n:2) Fluorotelomer Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_MW30_030717, 0902_MW53_030717 30-Dec-2017---- 09-Jul-2017----03-Jul-2017 ---- üHDPE (no PTFE) (EP231X)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717

30-Dec-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW10_300617 27-Dec-2017---- 09-Jul-2017----30-Jun-2017 ---- üHDPE (no PTFE) (EP231X)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617

27-Dec-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231P: PFAS Sums

HDPE (no PTFE) (EP231X)

0902_MW30_030717, 0902_MW53_030717 30-Dec-2017---- 09-Jul-2017----03-Jul-2017 ---- üHDPE (no PTFE) (EP231X)

0902_MW01_030717, 0902_MW02_030717,

0902_MW03_030717, 0902_MW12_030717,

0902_MW13_030717, 0902_MW14_030717,

0902_MW15_030717, 0902_MW17_030717,

0902_QC103_030717, 0902_QC503_030717,

0902_QC502_030717, 0902_MW56_030717,

0902_MW59_030717, 0902_QC101_030717,

0902_MW57_030717

30-Dec-2017---- 11-Jul-2017----03-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW10_300617 27-Dec-2017---- 09-Jul-2017----30-Jun-2017 ---- üHDPE (no PTFE) (EP231X)

0902_QC501_300617, 0902_MW08_300617,

0902_MW09_300617, 0902_MW54_300617,

0902_MW58_300617

27-Dec-2017---- 11-Jul-2017----30-Jun-2017 ---- ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC Standard 12.90 10.004 31 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 11.76 10.004 34 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 10.81 10.004 37 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 10.81 10.004 37 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 11.43 10.004 35 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 23 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 12.50 10.003 24 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 25 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 11.63 10.005 43 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 23 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 11.76 10.006 51 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 12.90 10.004 31 üVolatile Organic Compounds EP074

Laboratory Control Samples (LCS)

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 10.00 10.004 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.88 5.002 34 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 5.71 5.002 35 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.33 5.002 24 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 8.00 5.002 25 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 13.95 10.006 43 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.88 5.003 51 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üVolatile Organic Compounds EP074

Method Blanks (MB)

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.88 5.002 34 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üDissolved Metals by ICP-MS - Suite A EG020A-F

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Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Method Blanks (MB) - Continued

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 5.71 5.002 35 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.33 5.002 24 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 8.00 5.002 25 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 6.98 5.003 43 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 8.70 5.002 23 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.88 5.003 51 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üVolatile Organic Compounds EP074

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.88 5.002 34 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 23 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 8.33 5.002 24 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 25 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.00 5.002 40 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 23 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.88 5.003 51 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üVolatile Organic Compounds EP074

Page 315: Appendix - Department of Defence

24 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 2540C. A gravimetric procedure that determines the amount of `filterable` residue

in an aqueous sample. A well-mixed sample is filtered through a glass fibre filter (1.2um). The filtrate is

evaporated to dryness and dried to constant weight at 180+/-5C. This method is compliant with NEPM (2013)

Schedule B(3)

Total Dissolved Solids (High Level) EA015H WATER

In house: Referenced to APHA 2320 B This procedure determines alkalinity by automated measurement (e.g. PC

Titrate) using pH 4.5 for indicating the total alkalinity end-point. This method is compliant with NEPM (2013)

Schedule B(3)

Alkalinity by PC Titrator ED037-P WATER

In house: Referenced to APHA 4500-SO4. Dissolved sulfate is determined in a 0.45um filtered sample. Sulfate

ions are converted to a barium sulfate suspension in an acetic acid medium with barium chloride. Light

absorbance of the BaSO4 suspension is measured by a photometer and the SO4-2 concentration is determined

by comparison of the reading with a standard curve. This method is compliant with NEPM (2013) Schedule B(3)

Sulfate (Turbidimetric) as SO4 2- by

Discrete Analyser

ED041G WATER

In house: Referenced to APHA 4500 Cl - G.The thiocyanate ion is liberated from mercuric thiocyanate through

sequestration of mercury by the chloride ion to form non-ionised mercuric chloride.in the presence of ferric ions

the librated thiocynate forms highly-coloured ferric thiocynate which is measured at 480 nm APHA 21st edition

seal method 2 017-1-L april 2003

Chloride by Discrete Analyser ED045G WATER

In house: Referenced to APHA 3120 and 3125; USEPA SW 846 - 6010 and 6020; Cations are determined by

either ICP-AES or ICP-MS techniques. This method is compliant with NEPM (2013) Schedule B(3)

Sodium Adsorption Ratio is calculated from Ca, Mg and Na which determined by ALS in house method

QWI-EN/ED093F. This method is compliant with NEPM (2013) Schedule B(3)

Hardness parameters are calculated based on APHA 2340 B. This method is compliant with NEPM (2013)

Schedule B(3)

Major Cations - Dissolved ED093F WATER

In house: Referenced to APHA 3125; USEPA SW846 - 6020, ALS QWI-EN/EG020. Samples are 0.45µm filtered

prior to analysis. The ICPMS technique utilizes a highly efficient argon plasma to ionize selected elements. Ions

are then passed into a high vacuum mass spectrometer, which separates the analytes based on their distinct

mass to charge ratios prior to their measurement by a discrete dynode ion detector.

Dissolved Metals by ICP-MS - Suite A EG020A-F WATER

In house: Referenced to AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS)

Samples are 0.45µm filtered prior to analysis. FIM-AAS is an automated flameless atomic absorption technique.

A bromate/bromide reagent is used to oxidise any organic mercury compounds in the filtered sample. The ionic

mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell.

Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM

(2013) Schedule B(3)

Dissolved Mercury by FIMS EG035F WATER

In house: Referenced to APHA 4500-F C: CDTA is added to the sample to provide a uniform ionic strength

background, adjust pH, and break up complexes. Fluoride concentration is determined by either manual or

automatic ISE measurement. This method is compliant with NEPM (2013) Schedule B(3)

Fluoride by PC Titrator EK040P WATER

Page 316: Appendix - Department of Defence

25 of 25:Page

Work Order :

:Client

ES1716548

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 1030F. This method is compliant with NEPM (2013) Schedule B(3)Ionic Balance by PCT DA and Turbi SO4

DA

EN055 - PG WATER

In house: Referenced to USEPA SW 846 - 8015A The sample extract is analysed by Capillary GC/FID and

quantification is by comparison against an established 5 point calibration curve of n-Alkane standards. This

method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH - Semivolatile Fraction EP071 WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. This

method is compliant with NEPM (2013) Schedule B(3)

Volatile Organic Compounds EP074 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS and

quantification is by comparison against an established 5 point calibration curve. This method is compliant with

NEPM (2013) Schedule B(3)

Semivolatile Organic Compounds EP075 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS in SIM Mode

and quantification is by comparison against an established 5 point calibration curve. This method is compliant

with NEPM (2013) Schedule B(3)

PAH/Phenols (GC/MS - SIM) EP075(SIM) WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve.

Alternatively, a sample is equilibrated in a headspace vial and a portion of the headspace determined by GCMS

analysis. This method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH Volatiles/BTEX EP080 WATER

In house: A 12 mL aliquot of sample is mixed with 4.5 g of sodium chloride, equilibrated at 80 degrees C for 30

minutes and the headspace analysed by GCMS in the selected ion monitoring mode.

1.4-Dioxane by HS-GCMS EP116 WATER

In house: Direct injection analysis of fresh waters after dilution (1:1) with methanol. Analysis by

LC-Electrospray-MS-MS, Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.

Per- and Polyfluoroalkyl Substances

(PFAS) by LCMSMS

EP231X WATER

Preparation Methods Method DescriptionsMatrixMethod

In house: Referenced to USEPA SW 846 - 3510B 100 mL to 1L of sample is transferred to a separatory funnel

and serially extracted three times using 60mL DCM for each extract. The resultant extracts are combined,

dehydrated and concentrated for analysis. This method is compliant with NEPM (2013) Schedule B(3) . ALS

default excludes sediment which may be resident in the container.

Separatory Funnel Extraction of Liquids ORG14 WATER

A 5 mL aliquot or 5 mL of a diluted sample is added to a 40 mL VOC vial for sparging.Volatiles Water Preparation ORG16-W WATER

Page 317: Appendix - Department of Defence
Page 318: Appendix - Department of Defence
Page 319: Appendix - Department of Defence
Page 320: Appendix - Department of Defence

Environmental

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1716700

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield

NSW Australia 2164

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 02 8934 0000 +61 2 8784 8503

:: FacsimileFacsimile +61 02 8934 0001 +61-2-8784 8500

::Project 60547028, task 3.1 Page 1 of 5

:Order number 60547028 :Quote number ES2017AECOMAU0002 (SY/308/17)

:C-O-C number ---- :QC Level NEPM 2013 B3 & ALS QC Standard

Site : RAAF Richmond

Sampler : James Tomilson and Sebastian

McDlay

DatesDate Samples Received : Issue Date : 07-Jul-201706-Jul-2017 18:00

Scheduled Reporting Date: 14-Jul-2017:Client Requested Due

Date

14-Jul-2017

Delivery DetailsMode of Delivery : :Undefined Not intact.Security Seal

No. of coolers/boxes : :4 Temperature 1.7'C - Ice present

: : 40 / 40Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l 7/7/17: This is an updated SRA which indicates the updated bottles and analysis.

l 7/7/17b: This is an updated SRA.

l No green bottle received for samples 31,37,39, unable to do TDS, NO2, NO3, PO4.l Samples 0902_QC204_050717, 0902_QC203_050717, 0902_QC202_060717 to be forwarded to

Envirolab.l Sample #40 received extra, placed on hold.l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 321: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716700 Amendment 02 of 5:Page

07-Jul-2017:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exists.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

If no sampling time is provided, the sampling time will

default 00:00 on the date of sampling. If no sampling date

is provided, the sampling date will be assumed by the

laboratory and displayed in brackets without a time

component

WA

TE

R -

EG

020F

Dis

solv

ed

Meta

ls b

y IC

PM

S

WA

TE

R -

EK

055G

Am

mon

ia a

s N

By

Dis

cre

te A

na

lyse

r

WA

TE

R -

EP

116

1.4

-Dio

xan

e

WA

TE

R -

EP

231X

PF

AS

- F

ull

Su

ite (

28 a

na

lyte

s)

WA

TE

R -

NT

-01 &

02A

Ca, M

g, N

a, K

, C

l, S

O4

, A

lka

linity

& F

luo

rid

e

WA

TE

R -

NT

-04

Nitr

ite a

nd N

itra

te

WA

TE

R -

W-2

6

TR

H/B

TE

XN

/PA

H/8

Me

tals

ES1716700-001 05-Jul-2017 00:00 0902_MW61_050717 ü ü ü ü ü ü ü

ES1716700-002 05-Jul-2017 00:00 0902_MW60_050717 ü ü ü ü ü ü ü

ES1716700-003 05-Jul-2017 00:00 0902_MW25_050717 ü ü ü ü ü ü ü

ES1716700-004 05-Jul-2017 00:00 0902_MW48_050717 ü ü ü ü ü ü ü

ES1716700-005 05-Jul-2017 00:00 0902_MW26_050717 ü ü ü ü ü ü ü

ES1716700-006 05-Jul-2017 00:00 0902_MW68_050717 ü ü ü ü ü ü ü

ES1716700-007 06-Jul-2017 00:00 0902_MW20_060717 ü ü ü ü ü ü ü

ES1716700-008 06-Jul-2017 00:00 0902_MW22_060717 ü ü ü ü ü ü ü

ES1716700-009 06-Jul-2017 00:00 0902_MW36_060717 ü ü ü ü ü ü ü

ES1716700-010 06-Jul-2017 00:00 0902_MW45_060717 ü ü ü ü ü ü ü

ES1716700-011 06-Jul-2017 00:00 0902_MW21_060717 ü ü ü ü ü ü ü

ES1716700-012 06-Jul-2017 00:00 0902_MW23_060717 ü ü ü ü ü ü ü

ES1716700-013 06-Jul-2017 00:00 0902_MW44_060717 ü ü ü ü ü ü ü

ES1716700-014 06-Jul-2017 00:00 0902_MW46_060717 ü ü ü ü ü ü ü

ES1716700-015 06-Jul-2017 00:00 0902_MW51_060717 ü ü ü ü ü ü ü

ES1716700-016 04-Jul-2017 00:00 0902_MW34_040717 ü ü ü ü ü

ES1716700-017 04-Jul-2017 00:00 0902_MW32_040717 ü ü ü ü ü

ES1716700-018 04-Jul-2017 00:00 0902_MW33_040717 ü ü ü ü ü ü ü

ES1716700-019 04-Jul-2017 00:00 0902_MW73_040717 ü ü ü ü ü ü ü

ES1716700-020 04-Jul-2017 00:00 0902_MW74_040717 ü ü ü ü ü ü ü

ES1716700-021 04-Jul-2017 00:00 0902_MW72_040717 ü ü ü ü ü ü ü

ES1716700-022 04-Jul-2017 00:00 0902_MW65_040717 ü ü ü ü ü ü ü

ES1716700-023 04-Jul-2017 00:00 0902_MW66_040717 ü ü ü ü ü ü ü

ES1716700-024 04-Jul-2017 00:00 0902_MW64_040717 ü ü ü ü ü ü ü

ES1716700-025 04-Jul-2017 00:00 0902_MW71_040717 ü ü ü ü ü ü ü

ES1716700-026 05-Jul-2017 00:00 0902_MW70_050717 ü ü ü ü ü ü ü

ES1716700-027 05-Jul-2017 00:00 0902_MW67_050717 ü ü ü ü ü ü ü

ES1716700-028 05-Jul-2017 00:00 0902_MW69_050717 ü ü ü ü ü ü ü

ES1716700-029 05-Jul-2017 00:00 0902_MW63_050717 ü ü ü ü ü ü ü

ES1716700-030 05-Jul-2017 00:00 0902_MW62_050717 ü ü ü ü ü ü ü

ES1716700-031 06-Jul-2017 00:00 0902_QC102_060717 ü ü ü ü ü

ES1716700-032 06-Jul-2017 00:00 0902_MW47_060717 ü ü ü ü ü ü ü

ES1716700-033 06-Jul-2017 00:00 0902_MW52_060717 ü ü ü ü ü ü ü

ES1716700-034 06-Jul-2017 00:00 0902_QC104_060717 ü ü ü ü ü

ES1716700-035 04-Jul-2017 00:00 0902_QC508_040717 ü ü ü ü ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 322: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716700 Amendment 03 of 5:Page

07-Jul-2017:Issue Date

WA

TE

R -

EG

020F

Dis

solv

ed

Me

tals

by

ICP

MS

WA

TE

R -

EK

05

5G

Am

mo

nia

as

N B

y D

iscr

ete

An

aly

ser

WA

TE

R -

EP

11

6

1.4

-Dio

xan

e

WA

TE

R -

EP

23

1X

PF

AS

- F

ull

Suite

(28 a

naly

tes)

WA

TE

R -

NT

-01 &

02

A

Ca,

Mg,

Na,

K, C

l, S

O4,

Alk

alin

ity &

Flu

orid

e

WA

TE

R -

NT

-04

Nitr

ite a

nd N

itrate

WA

TE

R -

W-2

6

TR

H/B

TE

XN

/PA

H/8

Meta

ls

ES1716700-036 05-Jul-2017 00:00 0902_QC509_050717 ü ü ü ü ü

ES1716700-037 06-Jul-2017 00:00 0902_QC510_050717 ü ü ü ü ü

ES1716700-039 06-Jul-2017 00:00 0902_QC511_060717 ü ü ü ü ü

ES1716700-040 06-Jul-2017 00:00 0902_MW50_060717 ü ü ü ü ü ü üW

AT

ER

- E

A0

15

H

To

tal D

isso

lve

d S

olid

s -

Hig

h L

eve

l

WA

TE

R -

EK

07

1G

Re

act

ive

Ph

osp

ho

rus

by

Dis

cre

te a

na

lyse

r

WA

TE

R -

W-1

8

TR

H(C

6 -

C9

)/B

TE

XN

WA

TE

R -

W-2

3

SV

OC

/VO

C

ES1716700-001 05-Jul-2017 00:00 0902_MW61_050717 ü ü ü

ES1716700-002 05-Jul-2017 00:00 0902_MW60_050717 ü ü ü

ES1716700-003 05-Jul-2017 00:00 0902_MW25_050717 ü ü ü

ES1716700-004 05-Jul-2017 00:00 0902_MW48_050717 ü ü ü

ES1716700-005 05-Jul-2017 00:00 0902_MW26_050717 ü ü ü

ES1716700-006 05-Jul-2017 00:00 0902_MW68_050717 ü ü ü

ES1716700-007 06-Jul-2017 00:00 0902_MW20_060717 ü ü ü

ES1716700-008 06-Jul-2017 00:00 0902_MW22_060717 ü ü ü

ES1716700-009 06-Jul-2017 00:00 0902_MW36_060717 ü ü ü

ES1716700-010 06-Jul-2017 00:00 0902_MW45_060717 ü ü ü

ES1716700-011 06-Jul-2017 00:00 0902_MW21_060717 ü ü ü

ES1716700-012 06-Jul-2017 00:00 0902_MW23_060717 ü ü ü

ES1716700-013 06-Jul-2017 00:00 0902_MW44_060717 ü ü ü

ES1716700-014 06-Jul-2017 00:00 0902_MW46_060717 ü ü ü

ES1716700-015 06-Jul-2017 00:00 0902_MW51_060717 ü ü ü

ES1716700-016 04-Jul-2017 00:00 0902_MW34_040717 ü ü

ES1716700-017 04-Jul-2017 00:00 0902_MW32_040717 ü ü

ES1716700-018 04-Jul-2017 00:00 0902_MW33_040717 ü ü ü

ES1716700-019 04-Jul-2017 00:00 0902_MW73_040717 ü ü ü

ES1716700-020 04-Jul-2017 00:00 0902_MW74_040717 ü ü ü

ES1716700-021 04-Jul-2017 00:00 0902_MW72_040717 ü ü ü

ES1716700-022 04-Jul-2017 00:00 0902_MW65_040717 ü ü ü

ES1716700-023 04-Jul-2017 00:00 0902_MW66_040717 ü ü ü

ES1716700-024 04-Jul-2017 00:00 0902_MW64_040717 ü ü ü

ES1716700-025 04-Jul-2017 00:00 0902_MW71_040717 ü ü ü

ES1716700-026 05-Jul-2017 00:00 0902_MW70_050717 ü ü ü

Matrix: WATER

Client sample IDLaboratory sample

ID

Client sampling

date / time

Page 323: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716700 Amendment 04 of 5:Page

07-Jul-2017:Issue Date

WA

TE

R -

EA

01

5H

Tota

l Dis

solv

ed

Solid

s

- H

igh

Le

vel

WA

TE

R -

EK

07

1G

Rea

ctiv

e P

hosp

ho

rus

by

Dis

cre

te a

naly

ser

WA

TE

R -

W-1

8

TR

H(C

6 -

C9)/

BT

EX

N

WA

TE

R -

W-2

3

SV

OC

/VO

C

ES1716700-027 05-Jul-2017 00:00 0902_MW67_050717 ü ü ü

ES1716700-028 05-Jul-2017 00:00 0902_MW69_050717 ü ü ü

ES1716700-029 05-Jul-2017 00:00 0902_MW63_050717 ü ü ü

ES1716700-030 05-Jul-2017 00:00 0902_MW62_050717 ü ü ü

ES1716700-031 06-Jul-2017 00:00 0902_QC102_060717 ü

ES1716700-032 06-Jul-2017 00:00 0902_MW47_060717 ü ü ü

ES1716700-033 06-Jul-2017 00:00 0902_MW52_060717 ü ü ü

ES1716700-034 06-Jul-2017 00:00 0902_QC104_060717 ü

ES1716700-035 04-Jul-2017 00:00 0902_QC508_040717 ü

ES1716700-036 05-Jul-2017 00:00 0902_QC509_050717 ü

ES1716700-037 06-Jul-2017 00:00 0902_QC510_050717 ü

ES1716700-038 06-Jul-2017 00:00 0902_QC601_060717 ü

ES1716700-039 06-Jul-2017 00:00 0902_QC511_060717 ü

ES1716700-040 06-Jul-2017 00:00 0902_MW50_060717 ü ü ü

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Page 324: Appendix - Department of Defence

:Client AECOM Australia Pty Ltd

Work Order : ES1716700 Amendment 05 of 5:Page

07-Jul-2017:Issue Date

Requested Deliverables

ACCOUNTS PAYABLE

- A4 - AU Tax Invoice (INV) Email AP_CustomerService.ANZ@aecom.

com

BEN HUNTER2

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CATHERINE HANSEN

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

CLAYTON COWPER

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

DIRK SANDERSON

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

Page 325: Appendix - Department of Defence

0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 91ES1716700

:: LaboratoryClient AECOM Australia Pty Ltd Environmental Division Sydney

: :ContactContact MR CLAYTON COWPER Loren Schiavon

:: AddressAddress LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

277-289 Woodpark Road Smithfield NSW Australia 2164

:Telephone +61 02 8934 0000 :Telephone +61 2 8784 8503

:Project 60547028, task 3.1 Date Samples Received : 06-Jul-2017 18:00

:Order number 60547028 Date Analysis Commenced : 07-Jul-2017

:C-O-C number ---- Issue Date : 17-Jul-2017 17:31

Sampler : James Tomilson and Sebastian McDlay

Site : RAAF Richmond

Quote number : SY/308/17

40:No. of samples received

40:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Sanjeshni Jyoti Senior Chemist Volatiles Sydney Organics, Smithfield, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

Page 326: Appendix - Department of Defence

2 of 91:Page

Work Order :

:Client

ES1716700

60547028, task 3.1:Project

AECOM Australia Pty Ltd

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When no sampling time is provided, the sampling time will default 00:00 on the date of sampling. If no sampling date is provided, the sampling date will be assumed by the laboratory and displayed in brackets without a

time component.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

EG020: Bromine quantification may be unreliable due to its low solubility in acid, leading to variable volatility during measurement by ICPMS.l

ED041G: LOR raised for Sulfate on sample nos: 7 and 18 due to sample matrix.l

TDS by method EA-015 may bias high for various samples due to the presence of fine particulate matter, which may pass through the prescribed GF/C paper.l

TDS by method EA-015 may bias high for various samples due to the presence of fine particulate matter, which may pass through the prescribed GF/C paper.l

It has been noted that Nitrite is greater than NOx for sample 19, however this difference is within the limits of experimental variation.l

EN055 : Ionic Balance out of acceptable limits for sample 7, 19 and 21 due to analytes not quantified in this report.l

EP116: Particular samples required dilution due to sample matrix . LOR values have been adjusted accordingly.l

EP075: 'Sum of PAH' is the sum of the USEPA 16 priority PAHsl

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero.

l

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

545 2130 1950 2660 606mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

437Bicarbonate Alkalinity as CaCO3 179 237 222 332mg/L171-52-3

437 179 237 222 332mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

4Sulfate as SO4 - Turbidimetric 20 12 31 22mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

39Chloride 776 768 357 59mg/L116887-00-6

ED093F: Dissolved Major Cations

37Calcium 74 108 5 8mg/L17440-70-2

41Magnesium 74 79 8 12mg/L17439-95-4

100Sodium 327 350 329 199mg/L17440-23-5

3Potassium 1 6 <1 1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.02Aluminium 0.01 <0.01 0.14 3.19mg/L0.017429-90-5

0.010Arsenic <0.001 <0.001 <0.001 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 0.003mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 0.002mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 0.004mg/L0.0017439-92-1

4.22Manganese 0.120 0.202 0.026 0.027mg/L0.0017439-96-5

0.016Nickel 0.018 0.048 0.004 0.011mg/L0.0017440-02-0

0.024Zinc 0.010 0.012 0.008 0.008mg/L0.0057440-66-6

19.3Iron <0.05 <0.05 0.14 1.64mg/L0.057439-89-6

0.2Bromine 1.9 1.5 1.0 0.5mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.4Fluoride 0.2 0.3 1.4 1.0mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.10Ammonia as N 0.01 <0.01 0.02 0.01mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N <0.01 <0.01 <0.01 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

<0.01Nitrate as N 0.31 0.33 3.26 6.42mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

<0.01 0.31 0.33 3.26 6.42mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

<0.01Reactive Phosphorus as P 0.01 0.01 0.07 0.04mg/L0.0114265-44-2

EN055: Ionic Balance

9.91 25.9 26.6 15.2 8.76meq/L0.01----Total Anions

9.65 24.0 27.3 15.2 10.1meq/L0.01----Total Cations

1.37 3.71 1.15 0.22 6.97%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene 7 6 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene 17 61 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

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0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 50 <20 <20µg/L20----C6 - C9 Fraction

Page 334: Appendix - Department of Defence

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

760 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

60 <50 <50 <50 <50µg/L50----C29 - C36 Fraction

820^ <50 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 50 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 50 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

780 <100 <100 100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

780^ <100 <100 100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<2.01.4-Dioxane <0.5 <1.0 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.12Perfluorobutane sulfonic acid

(PFBS)

0.24 0.02 0.07 1.02µg/L0.02375-73-5

0.12Perfluoropentane sulfonic acid

(PFPeS)

0.36 0.02 0.08 1.31µg/L0.022706-91-4

1.43Perfluorohexane sulfonic acid

(PFHxS)

2.98 0.07 0.20 12.7µg/L0.02355-46-4

0.04Perfluoroheptane sulfonic acid

(PFHpS)

0.09 <0.02 <0.02 0.38µg/L0.02375-92-8

Page 335: Appendix - Department of Defence

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

1.02Perfluorooctane sulfonic acid

(PFOS)

0.73 <0.01 <0.01 1.23µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 0.14µg/L0.022706-90-3

0.13Perfluorohexanoic acid (PFHxA) 0.25 <0.02 0.07 0.84µg/L0.02307-24-4

0.09Perfluoroheptanoic acid (PFHpA) 0.06 <0.02 <0.02 0.23µg/L0.02375-85-9

0.10Perfluorooctanoic acid (PFOA) 0.10 <0.01 <0.01 0.39µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 336: Appendix - Department of Defence

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

3.05 4.81 0.11 0.42 18.2µg/L0.01----Sum of PFAS

2.45Sum of PFHxS and PFOS 3.71 0.07 0.20 13.9µg/L0.01355-46-4/1763-23-

1

2.89 4.36 0.09 0.34 16.6µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1261.2-Dichloroethane-D4 111 116 111 97.2%517060-07-0

117Toluene-D8 119 119 107 92.1%52037-26-5

1114-Bromofluorobenzene 110 110 102 87.9%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

24.3Phenol-d6 32.3 30.8 30.5 28.9%113127-88-3

49.02-Chlorophenol-D4 55.4 61.5 55.2 55.1%193951-73-6

60.62.4.6-Tribromophenol 84.8 74.6 68.0 55.6%1118-79-6

EP075(SIM)T: PAH Surrogates

54.72-Fluorobiphenyl 51.0 49.5 57.4 53.5%1321-60-8

63.3Anthracene-d10 72.4 91.3 96.5 66.0%11719-06-8

66.64-Terphenyl-d14 86.7 73.8 62.5 67.6%11718-51-0

EP075S: Acid Extractable Surrogates

30.42-Fluorophenol 37.2 34.2 33.1 32.4%2367-12-4

21.4Phenol-d6 28.5 25.6 27.4 24.4%213127-88-3

40.52-Chlorophenol-D4 50.6 49.8 47.6 44.1%293951-73-6

66.72.4.6-Tribromophenol 64.3 63.7 63.5 54.8%2118-79-6

Page 337: Appendix - Department of Defence

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Analytical Results

0902_MW26_0507170902_MW48_0507170902_MW25_0507170902_MW60_0507170902_MW61_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-005ES1716700-004ES1716700-003ES1716700-002ES1716700-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

49.8Nitrobenzene-D5 61.4 58.8 58.9 55.1%24165-60-0

34.01.2-Dichlorobenzene-D4 36.0 36.7 37.2 34.4%22199-69-1

50.32-Fluorobiphenyl 49.3 50.8 52.2 48.8%2321-60-8

67.4Anthracene-d10 73.7 74.3 73.9 65.7%21719-06-8

71.84-Terphenyl-d14 83.0 80.4 79.5 72.5%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1351.2-Dichloroethane-D4 113 118 112 99.5%217060-07-0

121Toluene-D8 124 124 112 95.7%22037-26-5

1204-Bromofluorobenzene 108 108 99.7 86.3%2460-00-4

EP116S: 1.4-Dioxane Surrogate

95.31.4-Dioxane-d8 125 103 110 117%0.517647-74-4

EP231S: PFAS Surrogate

95.6 92.1 93.6 94.1 95.5%0.02----13C4-PFOS

Page 338: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

910 612 2280 2390 2920mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

72Bicarbonate Alkalinity as CaCO3 52 470 300 274mg/L171-52-3

72 52 470 300 274mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

1Sulfate as SO4 - Turbidimetric <10 50 35 8mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

309Chloride 73 922 374 424mg/L116887-00-6

ED093F: Dissolved Major Cations

12Calcium 13 120 32 46mg/L17440-70-2

20Magnesium 7 105 35 38mg/L17439-95-4

171Sodium 96 556 288 291mg/L17440-23-5

<1Potassium 1 2 <1 6mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

<0.01Aluminium 0.06 <0.01 0.01 0.02mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 <0.001 0.006mg/L0.0017440-38-2

<0.0001Cadmium 0.0004 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper 0.003 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.258Manganese 0.068 0.771 0.047 2.20mg/L0.0017439-96-5

0.017Nickel 0.013 <0.001 0.007 0.018mg/L0.0017440-02-0

0.009Zinc 0.028 0.015 0.006 0.007mg/L0.0057440-66-6

0.80Iron <0.05 1.46 <0.05 3.84mg/L0.057439-89-6

0.8Bromine 0.3 2.6 1.3 0.9mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.3Fluoride <0.1 0.7 0.5 0.6mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.02Ammonia as N 0.02 0.16 <0.01 0.06mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

Page 339: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N <0.01 <0.01 <0.01 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

<0.01Nitrate as N 2.22 0.07 5.07 <0.01mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

<0.01 2.22 0.07 5.07 <0.01mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

<0.01Reactive Phosphorus as P 0.10 <0.01 0.03 <0.01mg/L0.0114265-44-2

EN055: Ionic Balance

10.2 3.10 36.4 17.3 17.6meq/L0.01----Total Anions

9.68 5.43 38.9 17.0 18.2meq/L0.01----Total Cations

2.48 27.3 3.22 0.78 1.76%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

Page 340: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

Page 342: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 343: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

Page 344: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

Page 345: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 <100 410 1620µg/L100----C15 - C28 Fraction

60 <50 <50 270 810µg/L50----C29 - C36 Fraction

60^ <50 <50 680 2430µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

140 <100 <100 640 2520µg/L100---->C16 - C34 Fraction

<100 <100 <100 110 150µg/L100---->C34 - C40 Fraction

140^ <100 <100 750 2670µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <0.5 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.12Perfluorobutane sulfonic acid

(PFBS)

0.71 0.35 0.25 <0.02µg/L0.02375-73-5

0.22Perfluoropentane sulfonic acid

(PFPeS)

1.00 0.44 0.23 <0.02µg/L0.022706-91-4

2.00Perfluorohexane sulfonic acid

(PFHxS)

13.3 3.05 0.86 0.05µg/L0.02355-46-4

0.05Perfluoroheptane sulfonic acid

(PFHpS)

0.22 0.12 <0.02 <0.02µg/L0.02375-92-8

Page 346: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

0.32Perfluorooctane sulfonic acid

(PFOS)

0.89 4.00 0.06 <0.01µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 <0.02µg/L0.022706-90-3

0.13Perfluorohexanoic acid (PFHxA) 0.30 0.24 0.08 <0.02µg/L0.02307-24-4

0.03Perfluoroheptanoic acid (PFHpA) 0.06 0.06 <0.02 <0.02µg/L0.02375-85-9

0.06Perfluorooctanoic acid (PFOA) 0.22 0.10 <0.01 <0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 347: Appendix - Department of Defence

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Work Order :

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

2.93 16.7 8.41 1.48 0.05µg/L0.01----Sum of PFAS

2.32Sum of PFHxS and PFOS 14.2 7.05 0.92 0.05µg/L0.01355-46-4/1763-23-

1

2.66 15.5 7.85 1.25 0.05µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1101.2-Dichloroethane-D4 108 106 105 107%517060-07-0

105Toluene-D8 104 104 95.2 99.8%52037-26-5

99.24-Bromofluorobenzene 99.7 98.8 92.2 95.9%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

33.0Phenol-d6 22.3 26.6 29.6 25.2%113127-88-3

61.02-Chlorophenol-D4 47.8 52.6 55.3 44.2%193951-73-6

86.32.4.6-Tribromophenol 61.1 63.3 73.9 62.6%1118-79-6

EP075(SIM)T: PAH Surrogates

62.62-Fluorobiphenyl 44.3 50.5 57.9 44.0%1321-60-8

77.8Anthracene-d10 57.3 62.2 67.4 79.5%11719-06-8

78.04-Terphenyl-d14 61.5 67.4 67.0 62.8%11718-51-0

EP075S: Acid Extractable Surrogates

36.92-Fluorophenol 28.6 32.0 35.9 36.0%2367-12-4

27.7Phenol-d6 21.5 24.0 27.6 30.6%213127-88-3

50.72-Chlorophenol-D4 39.4 45.8 45.4 45.9%293951-73-6

71.22.4.6-Tribromophenol 55.3 54.6 62.5 53.7%2118-79-6

Page 348: Appendix - Department of Defence

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Analytical Results

0902_MW45_0607170902_MW36_0607170902_MW22_0607170902_MW20_0607170902_MW68_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-010ES1716700-009ES1716700-008ES1716700-007ES1716700-006UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

62.2Nitrobenzene-D5 48.3 56.2 53.4 52.8%24165-60-0

40.21.2-Dichlorobenzene-D4 31.3 36.1 49.6 50.8%22199-69-1

56.22-Fluorobiphenyl 43.2 47.4 63.4 60.1%2321-60-8

78.2Anthracene-d10 59.9 65.8 68.6 65.1%21719-06-8

85.84-Terphenyl-d14 68.0 73.0 69.3 64.6%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1121.2-Dichloroethane-D4 109 107 106 108%217060-07-0

108Toluene-D8 108 108 98.8 104%22037-26-5

98.14-Bromofluorobenzene 97.3 98.0 92.4 95.1%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1031.4-Dioxane-d8 106 106 110 98.1%0.517647-74-4

EP231S: PFAS Surrogate

92.6 94.4 92.1 92.9 93.1%0.02----13C4-PFOS

Page 349: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

474 1840 1890 2310 454mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

282Bicarbonate Alkalinity as CaCO3 302 302 239 379mg/L171-52-3

282 302 302 239 379mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

41Sulfate as SO4 - Turbidimetric 14 9 8 15mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

25Chloride 210 357 501 16mg/L116887-00-6

ED093F: Dissolved Major Cations

6Calcium 16 36 61 92mg/L17440-70-2

5Magnesium 15 33 51 15mg/L17439-95-4

161Sodium 246 276 279 46mg/L17440-23-5

<1Potassium <1 5 10 6mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.01Aluminium 0.01 <0.01 <0.01 <0.01mg/L0.017429-90-5

<0.001Arsenic <0.001 0.001 0.001 0.002mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

0.004Copper <0.001 <0.001 <0.001 0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.006Manganese 0.048 0.239 0.772 0.239mg/L0.0017439-96-5

<0.001Nickel 0.003 0.013 0.014 <0.001mg/L0.0017440-02-0

<0.005Zinc <0.005 <0.005 0.006 0.006mg/L0.0057440-66-6

<0.05Iron <0.05 <0.05 <0.05 3.57mg/L0.057439-89-6

0.7Bromine 0.6 0.7 1.0 0.4mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

0.5Fluoride 1.0 0.5 0.4 0.2mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

<0.01Ammonia as N 0.06 0.04 0.05 0.90mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N <0.01 <0.01 <0.01 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

4.83Nitrate as N 0.02 0.02 0.01 0.09mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

4.83 0.02 0.02 0.01 0.09mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

0.01Reactive Phosphorus as P 0.03 <0.01 <0.01 <0.01mg/L0.0114265-44-2

EN055: Ionic Balance

7.19 12.2 16.3 19.1 8.34meq/L0.01----Total Anions

7.71 12.7 16.6 19.6 7.98meq/L0.01----Total Cations

3.49 1.94 1.07 1.44 2.18%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

Page 353: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 354: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

Page 355: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

Page 356: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 260 290 <100µg/L100----C15 - C28 Fraction

<50 <50 130 160 <50µg/L50----C29 - C36 Fraction

<50^ <50 390 450 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 370 470 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

<100^ <100 370 470 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <0.5 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.34Perfluorobutane sulfonic acid

(PFBS)

0.02 0.02 <0.02 33.6µg/L0.02375-73-5

0.53Perfluoropentane sulfonic acid

(PFPeS)

<0.02 0.02 <0.02 33.9µg/L0.022706-91-4

8.01Perfluorohexane sulfonic acid

(PFHxS)

0.05 0.08 0.04 267µg/L0.02355-46-4

0.28Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 <0.02 14.4µg/L0.02375-92-8

Page 357: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

7.16Perfluorooctane sulfonic acid

(PFOS)

<0.01 <0.01 <0.01 167µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

0.15Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 7.88µg/L0.022706-90-3

0.63Perfluorohexanoic acid (PFHxA) <0.02 0.02 <0.02 38.7µg/L0.02307-24-4

0.21Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 <0.02 5.31µg/L0.02375-85-9

0.49Perfluorooctanoic acid (PFOA) <0.01 <0.01 <0.01 9.69µg/L0.01335-67-1

0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 0.09µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 0.10µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 358: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 0.08µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

17.8 0.07 0.14 0.04 578µg/L0.01----Sum of PFAS

15.2Sum of PFHxS and PFOS 0.05 0.08 0.04 434µg/L0.01355-46-4/1763-23-

1

17.0 0.07 0.12 0.04 529µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1051.2-Dichloroethane-D4 108 110 102 113%517060-07-0

102Toluene-D8 101 104 88.2 104%52037-26-5

98.64-Bromofluorobenzene 97.0 98.9 88.6 102%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

33.0Phenol-d6 30.2 33.3 30.3 29.0%113127-88-3

65.32-Chlorophenol-D4 52.2 54.7 52.4 51.2%193951-73-6

73.92.4.6-Tribromophenol 63.0 65.3 72.8 67.6%1118-79-6

EP075(SIM)T: PAH Surrogates

57.72-Fluorobiphenyl 52.6 52.9 55.5 55.5%1321-60-8

97.5Anthracene-d10 61.2 80.3 72.2 66.2%11719-06-8

93.34-Terphenyl-d14 64.3 64.9 75.0 69.7%11718-51-0

EP075S: Acid Extractable Surrogates

38.42-Fluorophenol 30.5 33.9 29.7 31.8%2367-12-4

30.0Phenol-d6 24.2 25.5 24.1 25.1%213127-88-3

52.62-Chlorophenol-D4 43.8 45.7 42.0 46.4%293951-73-6

64.62.4.6-Tribromophenol 53.7 55.7 61.3 58.4%2118-79-6

Page 359: Appendix - Department of Defence

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Analytical Results

0902_MW51_0607170902_MW46_0607170902_MW44_0607170902_MW23_0607170902_MW21_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-015ES1716700-014ES1716700-013ES1716700-012ES1716700-011UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

64.7Nitrobenzene-D5 52.8 56.2 53.2 58.0%24165-60-0

41.11.2-Dichlorobenzene-D4 32.5 31.8 32.8 38.1%22199-69-1

51.22-Fluorobiphenyl 45.3 46.7 48.6 49.8%2321-60-8

79.7Anthracene-d10 61.8 65.0 72.5 68.2%21719-06-8

89.04-Terphenyl-d14 68.8 73.9 83.4 76.4%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1071.2-Dichloroethane-D4 110 112 105 115%217060-07-0

106Toluene-D8 104 108 91.4 107%22037-26-5

96.04-Bromofluorobenzene 95.1 97.2 86.6 99.5%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1111.4-Dioxane-d8 103 114 115 112%0.517647-74-4

EP231S: PFAS Surrogate

97.7 94.3 95.1 94.7 93.9%0.02----13C4-PFOS

Page 360: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

1090 1470 3710 272 557mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

254Bicarbonate Alkalinity as CaCO3 319 1000 171 431mg/L171-52-3

254 319 1000 171 431mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

19Sulfate as SO4 - Turbidimetric 44 <10 3 5mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

330Chloride 300 1070 20 46mg/L116887-00-6

ED093F: Dissolved Major Cations

8Calcium 14 70 16 9mg/L17440-70-2

7Magnesium 19 82 11 16mg/L17439-95-4

330Sodium 338 1050 64 203mg/L17440-23-5

1Potassium <1 <1 3 <1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

3.62Aluminium <0.01 <0.01 0.05 <0.01mg/L0.017429-90-5

0.002Arsenic <0.001 <0.001 0.001 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

0.004Chromium <0.001 0.002 <0.001 <0.001mg/L0.0017440-47-3

0.008Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

0.007Lead <0.001 <0.001 0.001 <0.001mg/L0.0017439-92-1

0.169Manganese 0.004 0.010 0.640 0.223mg/L0.0017439-96-5

0.006Nickel 0.008 0.010 0.017 0.011mg/L0.0017440-02-0

0.021Zinc <0.005 <0.005 <0.005 0.006mg/L0.0057440-66-6

2.01Iron <0.05 <0.05 3.29 0.15mg/L0.057439-89-6

1.1Bromine 0.9 3.8 0.5 0.9mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

2.2Fluoride 1.0 1.5 0.4 0.7mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

----Ammonia as N ---- 0.02 0.28 0.06mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

----Nitrite as N ---- <0.01 0.03 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

----Nitrate as N ---- 3.25 <0.01 0.02mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

---- ---- 3.25 <0.01 0.02mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

----Reactive Phosphorus as P ---- 0.02 0.46 0.05mg/L0.0114265-44-2

EN055: Ionic Balance

14.8 15.8 50.2 4.04 10.0meq/L0.01----Total Anions

15.4 17.0 55.9 4.56 10.6meq/L0.01----Total Cations

1.91 3.70 5.42 6.05 2.83%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

Page 362: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

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0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 365: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

Page 366: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

Page 367: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

180 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

100 <50 80 <50 <50µg/L50----C29 - C36 Fraction

280^ <50 80 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

300 <100 140 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

300^ <100 140 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <1.0 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

1.47Perfluorobutane sulfonic acid

(PFBS)

4.09 0.55 3.21 4.85µg/L0.02375-73-5

1.57Perfluoropentane sulfonic acid

(PFPeS)

4.67 0.65 4.20 6.41µg/L0.022706-91-4

7.58Perfluorohexane sulfonic acid

(PFHxS)

25.4 4.77 32.0 38.9µg/L0.02355-46-4

0.22Perfluoroheptane sulfonic acid

(PFHpS)

0.64 0.02 0.85 0.72µg/L0.02375-92-8

Page 368: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

0.50Perfluorooctane sulfonic acid

(PFOS)

5.98 0.07 3.70 11.6µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

0.18Perfluoropentanoic acid (PFPeA) 0.53 0.10 0.93 0.97µg/L0.022706-90-3

1.06Perfluorohexanoic acid (PFHxA) 3.10 0.45 4.89 5.61µg/L0.02307-24-4

0.23Perfluoroheptanoic acid (PFHpA) 0.45 0.08 0.57 0.84µg/L0.02375-85-9

0.22Perfluorooctanoic acid (PFOA) 0.50 0.04 1.39 0.95µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 369: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

13.0 45.4 6.73 51.7 70.8µg/L0.01----Sum of PFAS

8.08Sum of PFHxS and PFOS 31.4 4.84 35.7 50.5µg/L0.01355-46-4/1763-23-

1

11.2 40.0 6.06 46.7 63.7µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1091.2-Dichloroethane-D4 108 107 114 107%517060-07-0

102Toluene-D8 102 100 104 98.7%52037-26-5

97.94-Bromofluorobenzene 96.9 97.0 99.0 95.5%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

31.8Phenol-d6 33.3 36.8 24.2 32.6%113127-88-3

54.72-Chlorophenol-D4 66.3 62.2 47.8 59.2%193951-73-6

66.02.4.6-Tribromophenol 71.6 71.5 63.6 63.8%1118-79-6

EP075(SIM)T: PAH Surrogates

58.22-Fluorobiphenyl 61.2 65.6 61.0 59.2%1321-60-8

72.1Anthracene-d10 85.7 68.9 61.8 63.3%11719-06-8

77.94-Terphenyl-d14 75.0 68.6 64.6 75.1%11718-51-0

EP075S: Acid Extractable Surrogates

31.42-Fluorophenol 33.4 33.7 26.2 34.7%2367-12-4

29.2Phenol-d6 25.7 27.1 21.9 27.0%213127-88-3

46.92-Chlorophenol-D4 49.6 50.5 40.6 49.7%293951-73-6

55.92.4.6-Tribromophenol 63.5 62.6 56.6 66.0%2118-79-6

Page 370: Appendix - Department of Defence

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Analytical Results

0902_MW74_0407170902_MW73_0407170902_MW33_0407170902_MW32_0407170902_MW34_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-020ES1716700-019ES1716700-018ES1716700-017ES1716700-016UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

57.0Nitrobenzene-D5 63.8 62.4 51.3 60.8%24165-60-0

33.31.2-Dichlorobenzene-D4 40.4 41.1 37.8 51.9%22199-69-1

52.02-Fluorobiphenyl 54.9 54.7 51.4 59.3%2321-60-8

73.1Anthracene-d10 77.3 74.1 61.3 74.5%21719-06-8

86.34-Terphenyl-d14 85.1 81.8 68.8 80.7%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1111.2-Dichloroethane-D4 110 109 116 108%217060-07-0

105Toluene-D8 106 104 108 102%22037-26-5

95.74-Bromofluorobenzene 94.6 93.3 96.8 93.6%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1141.4-Dioxane-d8 118 111 106 108%0.517647-74-4

EP231S: PFAS Surrogate

92.4 95.4 91.4 95.4 97.7%0.02----13C4-PFOS

Page 371: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

376 632 942 1810 112mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

138Bicarbonate Alkalinity as CaCO3 234 231 302 30mg/L171-52-3

138 234 231 302 30mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

2Sulfate as SO4 - Turbidimetric 10 10 12 10mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

20Chloride 226 330 308 13mg/L116887-00-6

ED093F: Dissolved Major Cations

15Calcium 22 24 25 4mg/L17440-70-2

13Magnesium 21 23 28 6mg/L17439-95-4

15Sodium 176 229 249 10mg/L17440-23-5

4Potassium <1 2 <1 <1mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

<0.01Aluminium <0.01 <0.01 <0.01 <0.01mg/L0.017429-90-5

<0.001Arsenic 0.002 <0.001 <0.001 <0.001mg/L0.0017440-38-2

0.0002Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

1.35Manganese 4.69 0.375 0.437 0.001mg/L0.0017439-96-5

0.015Nickel 0.015 0.010 0.012 0.002mg/L0.0017440-02-0

0.022Zinc 0.008 <0.005 <0.005 <0.005mg/L0.0057440-66-6

<0.05Iron 0.85 <0.05 0.10 <0.05mg/L0.057439-89-6

0.1Bromine 0.7 0.8 0.8 <0.1mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

<0.1Fluoride 0.6 0.4 0.6 0.1mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.03Ammonia as N 0.02 0.03 0.04 0.01mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

Page 372: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N <0.01 <0.01 <0.01 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

<0.01Nitrate as N 0.01 0.09 <0.01 1.19mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

<0.01 0.01 0.09 <0.01 1.19mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

<0.01Reactive Phosphorus as P <0.01 <0.01 <0.01 <0.01mg/L0.0114265-44-2

EN055: Ionic Balance

3.36 11.2 14.1 15.0 1.17meq/L0.01----Total Anions

2.57 10.5 13.1 14.4 1.13meq/L0.01----Total Cations

13.3 3.57 3.78 2.01 ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 376: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

Page 377: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

60 80 <20 <20 <20µg/L20----C6 - C9 Fraction

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 100 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 <100 <100 <100 <100µg/L100----C15 - C28 Fraction

<50 <50 <50 <50 <50µg/L50----C29 - C36 Fraction

<50^ 100 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

60C6 - C10 Fraction 90 <20 <20 <20µg/L20C6_C10

60^ C6 - C10 Fraction minus BTEX

(F1)

90 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 <100 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

<100^ <100 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane 0.8 <0.5 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

21.5Perfluorobutane sulfonic acid

(PFBS)

0.06 0.11 0.16 0.38µg/L0.02375-73-5

11.4Perfluoropentane sulfonic acid

(PFPeS)

0.06 0.10 0.12 0.02µg/L0.022706-91-4

80.0Perfluorohexane sulfonic acid

(PFHxS)

0.42 0.66 0.76 0.32µg/L0.02355-46-4

4.64Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 0.02 0.02 0.03µg/L0.02375-92-8

Page 379: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

14.6Perfluorooctane sulfonic acid

(PFOS)

0.05 0.18 0.22 1.72µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

1.3Perfluorobutanoic acid (PFBA) <0.1 <0.1 2.7 <0.1µg/L0.1375-22-4

3.67Perfluoropentanoic acid (PFPeA) <0.02 <0.02 <0.02 0.11µg/L0.022706-90-3

14.5Perfluorohexanoic acid (PFHxA) <0.02 0.02 <0.02 0.09µg/L0.02307-24-4

0.77Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 <0.02 0.03µg/L0.02375-85-9

3.94Perfluorooctanoic acid (PFOA) <0.01 <0.01 <0.01 0.09µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 380: Appendix - Department of Defence

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

156 0.59 1.09 3.98 2.79µg/L0.01----Sum of PFAS

94.6Sum of PFHxS and PFOS 0.47 0.84 0.98 2.04µg/L0.01355-46-4/1763-23-

1

140 0.53 0.97 3.84 2.74µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1141.2-Dichloroethane-D4 112 112 106 98.6%517060-07-0

119Toluene-D8 111 112 107 94.8%52037-26-5

1124-Bromofluorobenzene 109 107 104 92.0%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

38.2Phenol-d6 31.6 24.9 33.8 35.4%113127-88-3

79.82-Chlorophenol-D4 62.4 48.3 58.4 65.9%193951-73-6

75.32.4.6-Tribromophenol 69.0 56.3 66.3 70.2%1118-79-6

EP075(SIM)T: PAH Surrogates

62.72-Fluorobiphenyl 60.9 46.5 49.5 55.1%1321-60-8

76.0Anthracene-d10 92.3 56.7 59.4 89.9%11719-06-8

78.84-Terphenyl-d14 77.0 57.6 71.7 73.8%11718-51-0

EP075S: Acid Extractable Surrogates

36.62-Fluorophenol 33.2 29.4 35.0 34.2%2367-12-4

28.0Phenol-d6 26.3 22.6 27.4 27.1%213127-88-3

55.12-Chlorophenol-D4 51.6 42.7 52.7 50.9%293951-73-6

68.92.4.6-Tribromophenol 61.0 50.1 68.9 63.3%2118-79-6

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Analytical Results

0902_MW71_0407170902_MW64_0407170902_MW66_0407170902_MW65_0407170902_MW72_040717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:0004-Jul-2017 00:00Client sampling date / time

ES1716700-025ES1716700-024ES1716700-023ES1716700-022ES1716700-021UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

68.0Nitrobenzene-D5 63.7 51.1 64.2 62.6%24165-60-0

40.91.2-Dichlorobenzene-D4 39.1 29.0 34.8 34.0%22199-69-1

56.82-Fluorobiphenyl 52.9 41.6 48.9 50.4%2321-60-8

79.0Anthracene-d10 74.1 57.5 74.5 72.0%21719-06-8

84.94-Terphenyl-d14 80.4 61.5 78.9 78.6%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1161.2-Dichloroethane-D4 114 114 108 99.5%217060-07-0

123Toluene-D8 116 116 111 98.5%22037-26-5

1104-Bromofluorobenzene 106 107 103 91.3%2460-00-4

EP116S: 1.4-Dioxane Surrogate

93.01.4-Dioxane-d8 102 91.3 79.2 92.9%0.517647-74-4

EP231S: PFAS Surrogate

72.6 71.6 72.7 76.5 75.1%0.02----13C4-PFOS

Page 382: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

508 5000 5800 1430 9850mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

<1Hydroxide Alkalinity as CaCO3 <1 <1 <1 <1mg/L1DMO-210-001

<1Carbonate Alkalinity as CaCO3 <1 <1 <1 <1mg/L13812-32-6

31Bicarbonate Alkalinity as CaCO3 534 59 73 804mg/L171-52-3

31 534 59 73 804mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

21Sulfate as SO4 - Turbidimetric 27 19 3 256mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

38Chloride 1950 53 687 4960mg/L116887-00-6

ED093F: Dissolved Major Cations

<1Calcium 114 2 36 263mg/L17440-70-2

4Magnesium 208 3 78 441mg/L17439-95-4

43Sodium 1140 70 295 2500mg/L17440-23-5

<1Potassium 2 <1 <1 6mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.04Aluminium <0.01 0.06 <0.01 <0.01mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 <0.001 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

0.002Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.014Manganese 0.129 0.033 0.708 0.309mg/L0.0017439-96-5

0.002Nickel 0.017 0.001 0.108 0.023mg/L0.0017440-02-0

0.017Zinc 0.007 0.006 0.019 <0.005mg/L0.0057440-66-6

<0.05Iron <0.05 <0.05 0.44 0.31mg/L0.057439-89-6

0.2Bromine 4.9 0.2 1.8 11.9mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

<0.1Fluoride 0.8 0.2 0.2 0.9mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.02Ammonia as N 0.01 0.04 0.03 0.07mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

Page 383: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

<0.01Nitrite as N <0.01 0.03 <0.01 <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

4.20Nitrate as N <0.01 12.6 <0.01 0.47mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

4.20 <0.01 12.6 <0.01 0.47mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

<0.01Reactive Phosphorus as P <0.01 0.02 <0.01 0.02mg/L0.0114265-44-2

EN055: Ionic Balance

2.13 66.2 3.07 20.9 161meq/L0.01----Total Anions

2.20 72.4 3.39 21.0 158meq/L0.01----Total Cations

---- 4.48 4.98 0.35 0.94%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

Page 384: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 17 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 8 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 245 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

Page 386: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 387: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 190 <20 <20µg/L20----C6 - C9 Fraction

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 170 110 <100 2550µg/L100----C15 - C28 Fraction

<50 110 70 50 1340µg/L50----C29 - C36 Fraction

<50^ 280 180 50 3890µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 190 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 190 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 260 200 120 4000µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 300µg/L100---->C34 - C40 Fraction

<100^ 260 200 120 4300µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 2.0 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

0.54Perfluorobutane sulfonic acid

(PFBS)

<0.02 0.07 4.92 0.02µg/L0.02375-73-5

0.20Perfluoropentane sulfonic acid

(PFPeS)

<0.02 0.04 2.96 0.03µg/L0.022706-91-4

2.08Perfluorohexane sulfonic acid

(PFHxS)

0.02 0.37 20.0 0.31µg/L0.02355-46-4

0.07Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 <0.02 1.16 <0.02µg/L0.02375-92-8

Page 390: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

1.22Perfluorooctane sulfonic acid

(PFOS)

0.01 0.65 1.47 0.51µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

0.18Perfluoropentanoic acid (PFPeA) <0.02 <0.02 0.94 <0.02µg/L0.022706-90-3

0.28Perfluorohexanoic acid (PFHxA) <0.02 0.04 3.33 0.04µg/L0.02307-24-4

0.06Perfluoroheptanoic acid (PFHpA) <0.02 <0.02 0.33 <0.02µg/L0.02375-85-9

0.17Perfluorooctanoic acid (PFOA) <0.01 0.03 1.08 0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 <0.02 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 <0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 391: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

4.80 0.03 1.20 36.2 0.92µg/L0.01----Sum of PFAS

3.30Sum of PFHxS and PFOS 0.03 1.02 21.5 0.82µg/L0.01355-46-4/1763-23-

1

4.53 0.03 1.16 32.1 0.89µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1101.2-Dichloroethane-D4 109 108 107 113%517060-07-0

106Toluene-D8 104 107 108 110%52037-26-5

1044-Bromofluorobenzene 103 101 102 105%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

31.2Phenol-d6 32.2 28.0 31.2 28.4%113127-88-3

62.92-Chlorophenol-D4 60.1 58.0 68.2 59.2%193951-73-6

73.72.4.6-Tribromophenol 62.4 80.1 78.9 68.8%1118-79-6

EP075(SIM)T: PAH Surrogates

60.92-Fluorobiphenyl 48.3 63.8 62.6 50.1%1321-60-8

68.9Anthracene-d10 79.2 72.6 92.0 70.5%11719-06-8

73.34-Terphenyl-d14 62.2 73.7 73.9 62.4%11718-51-0

EP075S: Acid Extractable Surrogates

35.82-Fluorophenol 49.3 35.5 34.8 41.5%2367-12-4

27.6Phenol-d6 41.0 28.5 26.9 36.7%213127-88-3

51.32-Chlorophenol-D4 60.4 54.4 53.2 53.8%293951-73-6

70.42.4.6-Tribromophenol 75.0 76.0 69.6 76.3%2118-79-6

Page 392: Appendix - Department of Defence

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Analytical Results

0902_MW62_0507170902_MW63_0507170902_MW69_0507170902_MW67_0507170902_MW70_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

05-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-030ES1716700-029ES1716700-028ES1716700-027ES1716700-026UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

60.9Nitrobenzene-D5 68.0 64.3 64.7 63.0%24165-60-0

33.51.2-Dichlorobenzene-D4 65.4 53.0 40.9 56.1%22199-69-1

50.12-Fluorobiphenyl 85.7 60.2 54.0 74.7%2321-60-8

75.1Anthracene-d10 89.3 78.3 71.6 85.2%21719-06-8

82.84-Terphenyl-d14 92.1 83.4 77.0 87.3%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1121.2-Dichloroethane-D4 112 110 108 116%217060-07-0

110Toluene-D8 108 111 111 114%22037-26-5

1004-Bromofluorobenzene 99.9 102 100 104%2460-00-4

EP116S: 1.4-Dioxane Surrogate

89.51.4-Dioxane-d8 94.5 113 77.3 125%0.517647-74-4

EP231S: PFAS Surrogate

73.0 65.2 68.7 73.2 65.9%0.02----13C4-PFOS

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

---- 3840 3250 ---- ----mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

----Hydroxide Alkalinity as CaCO3 <1 <1 ---- ----mg/L1DMO-210-001

----Carbonate Alkalinity as CaCO3 <1 <1 ---- ----mg/L13812-32-6

----Bicarbonate Alkalinity as CaCO3 528 1150 ---- ----mg/L171-52-3

---- 528 1150 ---- ----mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

----Sulfate as SO4 - Turbidimetric 145 170 ---- ----mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

----Chloride 1060 970 ---- ----mg/L116887-00-6

ED093F: Dissolved Major Cations

----Calcium 66 48 ---- ----mg/L17440-70-2

----Magnesium 74 68 ---- ----mg/L17439-95-4

----Sodium 900 1030 ---- ----mg/L17440-23-5

----Potassium 2 <1 ---- ----mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

0.02Aluminium <0.01 <0.01 0.08 <0.01mg/L0.017429-90-5

<0.001Arsenic <0.001 <0.001 0.003 <0.001mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 <0.001 <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 <0.001 <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 <0.001 <0.001 <0.001mg/L0.0017439-92-1

0.050Manganese 0.400 0.187 1.03 <0.001mg/L0.0017439-96-5

0.004Nickel 0.006 <0.001 0.003 <0.001mg/L0.0017440-02-0

0.006Zinc 0.006 <0.005 0.005 <0.005mg/L0.0057440-66-6

<0.05Iron <0.05 <0.05 2.63 <0.05mg/L0.057439-89-6

0.6Bromine 3.2 8.4 0.1 <0.1mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 <0.0001 <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

----Fluoride 1.6 2.0 ---- ----mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.02Ammonia as N <0.01 0.01 0.87 0.01mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

----Nitrite as N 0.11 <0.01 ---- ----mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

----Nitrate as N 106 1.81 ---- ----mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

---- 106 1.81 ---- ----mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

----Reactive Phosphorus as P 0.03 0.02 ---- ----mg/L0.0114265-44-2

EN055: Ionic Balance

---- 43.5 53.9 ---- ----meq/L0.01----Total Anions

---- 48.6 52.8 ---- ----meq/L0.01----Total Cations

---- 5.55 1.02 ---- ----%0.01----Ionic Balance

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 <5 <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 <5 <5 <5µg/L598-82-8

<5n-Propylbenzene <5 <5 <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 <5 <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 <5 <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 <5 <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 <5 <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 <5 <5 <5µg/L599-87-6

<5n-Butylbenzene <5 <5 <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 <50 <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 <50 <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 <50 <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 <50 <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 <5 <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 <5 <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 <5 <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 <5 <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 <5 <5 <5µg/L5106-93-4

Page 395: Appendix - Department of Defence

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AECOM Australia Pty Ltd

Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds

<50Dichlorodifluoromethane <50 <50 <50 <50µg/L5075-71-8

<50Chloromethane <50 <50 <50 <50µg/L5074-87-3

<50Vinyl chloride <50 <50 <50 <50µg/L5075-01-4

<50Bromomethane <50 <50 <50 <50µg/L5074-83-9

<50Chloroethane <50 <50 <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 <50 <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 <5 <5 <5µg/L575-35-4

<5Iodomethane <5 <5 <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 <5 <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 <5 <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 <5 <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 <5 <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 <5 <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 <5 <5 <5µg/L5107-06-2

<5Trichloroethene <5 <5 <5 <5µg/L579-01-6

<5Dibromomethane <5 <5 <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 <5 <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 <5 <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 <5 <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 <5 <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 <5 <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 <5 <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 <5 <5 <5µg/L596-18-4

<5Pentachloroethane <5 <5 <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 <5 <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 <5 <5 <5µg/L5108-90-7

<5Bromobenzene <5 <5 <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 <5 <5 <5µg/L595-49-8

<54-Chlorotoluene <5 <5 <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 <5 <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 <5 <5 <5µg/L567-66-3

<5Bromodichloromethane <5 <5 <5 <5µg/L575-27-4

<5Dibromochloromethane <5 <5 <5 <5µg/L5124-48-1

<5Bromoform <5 <5 <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 <1.0 <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 <1.0 <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 <1.0 <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 <1.0 <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 <1.0 <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 <1.0 <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 <1.0 <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 <1.0 <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 <1.0 <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 <1.0 <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 <1.0 <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 <1.0 <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 <1.0 <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 <2 <2 <2µg/L2108-95-2

<22-Chlorophenol <2 <2 <2 <2µg/L295-57-8

<22-Methylphenol <2 <2 <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 <4 <4 <4µg/L41319-77-3

<22-Nitrophenol <2 <2 <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 <2 <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 <2 <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 <2 <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 <2 <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 <2 <2 <2µg/L288-06-2

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 <2 <2 <2µg/L295-95-4

<4Pentachlorophenol <4 <4 <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 <2 <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 <2 <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 <2 <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 <2 <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 <2 <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 <2 <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 <2 <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 <2 <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 <2 <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 <10 <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 <2 <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 <2 <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 <2 <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 <4 <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 <2 <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 <2 <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 <2 <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 <2 <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 <4 <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 <2 <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 <2 <2 <2µg/L2109-06-8

<2Acetophenone <2 <2 <2 <2µg/L298-86-2

<2Nitrobenzene <2 <2 <2 <2µg/L298-95-3

<2Isophorone <2 <2 <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 <4 <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 <4 <4 <4µg/L4121-14-2

<21-Naphthylamine <2 <2 <2 <2µg/L2134-32-7

Page 398: Appendix - Department of Defence

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 <2 <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 <2 <2 <2µg/L299-55-8

<2Azobenzene <2 <2 <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 <2 <2 <2µg/L299-35-4

<2Phenacetin <2 <2 <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 <2 <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 <2 <2 <2µg/L282-68-8

<2Pronamide <2 <2 <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 <2 <2 <2µg/L260-11-7

<2Chlorobenzilate <2 <2 <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 <2 <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 <2 <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 <2 <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 <2 <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 <2 <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 <2 <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 <2 <2 <2µg/L295-50-1

<2Hexachloroethane <2 <2 <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 <2 <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 <2 <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 <2 <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 <10 <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 <2 <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 <4 <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 <2 <2 <2µg/L262-53-3

<24-Chloroaniline <2 <2 <2 <2µg/L2106-47-8

<42-Nitroaniline <4 <4 <4 <4µg/L488-74-4

<43-Nitroaniline <4 <4 <4 <4µg/L499-09-2

<2Dibenzofuran <2 <2 <2 <2µg/L2132-64-9

<24-Nitroaniline <2 <2 <2 <2µg/L2100-01-6

<2Carbazole <2 <2 <2 <2µg/L286-74-8

Page 399: Appendix - Department of Defence

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 <2 <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 <2 <2 <2µg/L2319-84-6

<2beta-BHC <2 <2 <2 <2µg/L2319-85-7

<2gamma-BHC <2 <2 <2 <2µg/L258-89-9

<2delta-BHC <2 <2 <2 <2µg/L2319-86-8

<2Heptachlor <2 <2 <2 <2µg/L276-44-8

<2Aldrin <2 <2 <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 <2 <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 <2 <2 <2µg/L2959-98-8

<24.4`-DDE <2 <2 <2 <2µg/L272-55-9

<2Dieldrin <2 <2 <2 <2µg/L260-57-1

<2Endrin <2 <2 <2 <2µg/L272-20-8

<2beta-Endosulfan <2 <2 <2 <2µg/L233213-65-9

<24.4`-DDD <2 <2 <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 <2 <2 <2µg/L21031-07-8

<44.4`-DDT <4 <4 <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 <4 <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 <4 <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 <2 <2 <2µg/L262-73-7

<2Dimethoate <2 <2 <2 <2µg/L260-51-5

<2Diazinon <2 <2 <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 <2 <2 <2µg/L25598-13-0

<2Malathion <2 <2 <2 <2µg/L2121-75-5

<2Fenthion <2 <2 <2 <2µg/L255-38-9

<2Chlorpyrifos <2 <2 <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 <2 <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 <2 <2 <2µg/L2470-90-6

<2Prothiofos <2 <2 <2 <2µg/L234643-46-4

<2Ethion <2 <2 <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 <50 <50 <50µg/L50----C10 - C14 Fraction

<100 240 <100 <100 <100µg/L100----C15 - C28 Fraction

<50 170 <50 <50 <50µg/L50----C29 - C36 Fraction

<50^ 410 <50 <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 <100 <100 <100µg/L100---->C10 - C16 Fraction

<100 420 <100 <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 <100 <100 <100µg/L100---->C34 - C40 Fraction

<100^ 420 <100 <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 <100 <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 <1.0 <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

<0.02Perfluorobutane sulfonic acid

(PFBS)

4.00 16.9 1.74 <0.02µg/L0.02375-73-5

<0.02Perfluoropentane sulfonic acid

(PFPeS)

2.71 8.99 1.11 <0.02µg/L0.022706-91-4

0.03Perfluorohexane sulfonic acid

(PFHxS)

14.0 24.9 7.68 <0.02µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

0.59 0.06 0.48 <0.02µg/L0.02375-92-8

Page 401: Appendix - Department of Defence

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

<0.01Perfluorooctane sulfonic acid

(PFOS)

8.61 0.20 17.4 <0.01µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 <0.02 <0.02 <0.02µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 <0.1 <0.1 <0.1µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) 0.59 3.19 0.79 <0.02µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) 1.74 10.8 1.68 <0.02µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) 0.23 0.53 0.24 <0.02µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) 0.60 0.31 0.75 <0.01µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 <0.02 0.03 <0.02µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 <0.02 <0.02 <0.02µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 <0.02 <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 <0.02 <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 <0.02 <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 <0.05 <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 <0.02 0.02 <0.02µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 <0.05 <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 <0.05 <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022355-31-9

Page 402: Appendix - Department of Defence

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 <0.02 <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 <0.05 0.24 <0.05µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 <0.05 0.09 <0.05µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 <0.05 <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

0.03 33.1 65.9 32.2 <0.01µg/L0.01----Sum of PFAS

0.03Sum of PFHxS and PFOS 22.6 25.1 25.1 <0.01µg/L0.01355-46-4/1763-23-

1

0.03 29.8 56.8 30.6 <0.01µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1101.2-Dichloroethane-D4 110 108 103 107%517060-07-0

108Toluene-D8 110 103 97.8 107%52037-26-5

1054-Bromofluorobenzene 103 100.0 95.2 102%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

28.8Phenol-d6 31.3 35.0 30.9 29.7%113127-88-3

58.12-Chlorophenol-D4 55.1 65.6 58.1 59.4%193951-73-6

63.82.4.6-Tribromophenol 65.1 65.7 68.4 66.3%1118-79-6

EP075(SIM)T: PAH Surrogates

54.52-Fluorobiphenyl 50.0 59.8 64.8 59.3%1321-60-8

62.9Anthracene-d10 66.9 71.8 69.0 67.5%11719-06-8

62.94-Terphenyl-d14 65.3 71.4 70.0 67.4%11718-51-0

EP075S: Acid Extractable Surrogates

29.22-Fluorophenol 27.5 33.3 32.8 32.2%2367-12-4

23.4Phenol-d6 23.1 26.2 26.6 24.8%213127-88-3

44.52-Chlorophenol-D4 43.8 50.2 50.6 47.1%293951-73-6

58.02.4.6-Tribromophenol 59.3 59.8 64.9 60.6%2118-79-6

Page 403: Appendix - Department of Defence

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Analytical Results

0902_QC508_0407170902_QC104_0607170902_MW52_0607170902_MW47_0607170902_QC102_060717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

04-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:00Client sampling date / time

ES1716700-035ES1716700-034ES1716700-033ES1716700-032ES1716700-031UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

55.5Nitrobenzene-D5 54.1 62.3 61.2 59.3%24165-60-0

38.71.2-Dichlorobenzene-D4 32.4 40.5 53.0 48.1%22199-69-1

47.82-Fluorobiphenyl 44.2 52.9 57.2 53.8%2321-60-8

63.8Anthracene-d10 66.2 70.4 68.9 67.1%21719-06-8

65.94-Terphenyl-d14 70.4 73.4 71.7 70.7%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1121.2-Dichloroethane-D4 112 110 104 107%217060-07-0

112Toluene-D8 114 107 102 111%22037-26-5

1034-Bromofluorobenzene 103 98.9 94.7 101%2460-00-4

EP116S: 1.4-Dioxane Surrogate

1041.4-Dioxane-d8 80.7 110 106 95.3%0.517647-74-4

EP231S: PFAS Surrogate

66.0 64.2 69.3 60.8 62.4%0.02----13C4-PFOS

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EA015: Total Dissolved Solids dried at 180 ± 5 °C

---- ---- ---- ---- 276mg/L10----Total Dissolved Solids @180°C

ED037P: Alkalinity by PC Titrator

----Hydroxide Alkalinity as CaCO3 ---- ---- ---- <1mg/L1DMO-210-001

----Carbonate Alkalinity as CaCO3 ---- ---- ---- <1mg/L13812-32-6

----Bicarbonate Alkalinity as CaCO3 ---- ---- ---- 122mg/L171-52-3

---- ---- ---- ---- 122mg/L1----Total Alkalinity as CaCO3

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

----Sulfate as SO4 - Turbidimetric ---- ---- ---- 7mg/L114808-79-8

ED045G: Chloride by Discrete Analyser

----Chloride ---- ---- ---- 20mg/L116887-00-6

ED093F: Dissolved Major Cations

----Calcium ---- ---- ---- 22mg/L17440-70-2

----Magnesium ---- ---- ---- 5mg/L17439-95-4

----Sodium ---- ---- ---- 26mg/L17440-23-5

----Potassium ---- ---- ---- 3mg/L17440-09-7

EG020F: Dissolved Metals by ICP-MS

<0.01Aluminium <0.01 ---- <0.01 0.07mg/L0.017429-90-5

<0.001Arsenic <0.001 ---- <0.001 0.003mg/L0.0017440-38-2

<0.0001Cadmium <0.0001 ---- <0.0001 <0.0001mg/L0.00017440-43-9

<0.001Chromium <0.001 ---- <0.001 <0.001mg/L0.0017440-47-3

<0.001Copper <0.001 ---- <0.001 <0.001mg/L0.0017440-50-8

<0.001Lead <0.001 ---- <0.001 <0.001mg/L0.0017439-92-1

<0.001Manganese <0.001 ---- <0.001 1.05mg/L0.0017439-96-5

<0.001Nickel <0.001 ---- <0.001 0.003mg/L0.0017440-02-0

<0.005Zinc <0.005 ---- <0.005 0.005mg/L0.0057440-66-6

<0.05Iron <0.05 ---- <0.05 2.65mg/L0.057439-89-6

<0.1Bromine <0.1 ---- <0.1 0.1mg/L0.17726-95-6

EG035F: Dissolved Mercury by FIMS

<0.0001Mercury <0.0001 ---- <0.0001 <0.0001mg/L0.00017439-97-6

EK040P: Fluoride by PC Titrator

----Fluoride ---- ---- ---- 0.2mg/L0.116984-48-8

EK055G: Ammonia as N by Discrete Analyser

0.01Ammonia as N <0.01 ---- <0.01 0.84mg/L0.017664-41-7

EK057G: Nitrite as N by Discrete Analyser

Page 405: Appendix - Department of Defence

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EK057G: Nitrite as N by Discrete Analyser - Continued

----Nitrite as N ---- ---- ---- <0.01mg/L0.0114797-65-0

EK058G: Nitrate as N by Discrete Analyser

----Nitrate as N ---- ---- ---- <0.01mg/L0.0114797-55-8

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

---- ---- ---- ---- <0.01mg/L0.01----Nitrite + Nitrate as N

EK071G: Reactive Phosphorus as P by discrete analyser

----Reactive Phosphorus as P ---- ---- ---- <0.01mg/L0.0114265-44-2

EN055: Ionic Balance

---- ---- ---- ---- 3.15meq/L0.01----Total Anions

---- ---- ---- ---- 2.72meq/L0.01----Total Cations

EP074A: Monocyclic Aromatic Hydrocarbons

<5Styrene <5 ---- <5 <5µg/L5100-42-5

<5Isopropylbenzene <5 ---- <5 <5µg/L598-82-8

<5n-Propylbenzene <5 ---- <5 <5µg/L5103-65-1

<51.3.5-Trimethylbenzene <5 ---- <5 <5µg/L5108-67-8

<5sec-Butylbenzene <5 ---- <5 <5µg/L5135-98-8

<51.2.4-Trimethylbenzene <5 ---- <5 <5µg/L595-63-6

<5tert-Butylbenzene <5 ---- <5 <5µg/L598-06-6

<5p-Isopropyltoluene <5 ---- <5 <5µg/L599-87-6

<5n-Butylbenzene <5 ---- <5 <5µg/L5104-51-8

EP074B: Oxygenated Compounds

<50Vinyl Acetate <50 ---- <50 <50µg/L50108-05-4

<502-Butanone (MEK) <50 ---- <50 <50µg/L5078-93-3

<504-Methyl-2-pentanone (MIBK) <50 ---- <50 <50µg/L50108-10-1

<502-Hexanone (MBK) <50 ---- <50 <50µg/L50591-78-6

EP074C: Sulfonated Compounds

<5Carbon disulfide <5 ---- <5 <5µg/L575-15-0

EP074D: Fumigants

<52.2-Dichloropropane <5 ---- <5 <5µg/L5594-20-7

<51.2-Dichloropropane <5 ---- <5 <5µg/L578-87-5

<5cis-1.3-Dichloropropylene <5 ---- <5 <5µg/L510061-01-5

<5trans-1.3-Dichloropropylene <5 ---- <5 <5µg/L510061-02-6

<51.2-Dibromoethane (EDB) <5 ---- <5 <5µg/L5106-93-4

EP074E: Halogenated Aliphatic Compounds

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP074E: Halogenated Aliphatic Compounds - Continued

<50Dichlorodifluoromethane <50 ---- <50 <50µg/L5075-71-8

<50Chloromethane <50 ---- <50 <50µg/L5074-87-3

<50Vinyl chloride <50 ---- <50 <50µg/L5075-01-4

<50Bromomethane <50 ---- <50 <50µg/L5074-83-9

<50Chloroethane <50 ---- <50 <50µg/L5075-00-3

<50Trichlorofluoromethane <50 ---- <50 <50µg/L5075-69-4

<51.1-Dichloroethene <5 ---- <5 <5µg/L575-35-4

<5Iodomethane <5 ---- <5 <5µg/L574-88-4

<5trans-1.2-Dichloroethene <5 ---- <5 <5µg/L5156-60-5

<51.1-Dichloroethane <5 ---- <5 <5µg/L575-34-3

<5cis-1.2-Dichloroethene <5 ---- <5 <5µg/L5156-59-2

<51.1.1-Trichloroethane <5 ---- <5 <5µg/L571-55-6

<51.1-Dichloropropylene <5 ---- <5 <5µg/L5563-58-6

<5Carbon Tetrachloride <5 ---- <5 <5µg/L556-23-5

<51.2-Dichloroethane <5 ---- <5 <5µg/L5107-06-2

<5Trichloroethene <5 ---- <5 <5µg/L579-01-6

<5Dibromomethane <5 ---- <5 <5µg/L574-95-3

<51.1.2-Trichloroethane <5 ---- <5 <5µg/L579-00-5

<51.3-Dichloropropane <5 ---- <5 <5µg/L5142-28-9

<5Tetrachloroethene <5 ---- <5 <5µg/L5127-18-4

<51.1.1.2-Tetrachloroethane <5 ---- <5 <5µg/L5630-20-6

<5trans-1.4-Dichloro-2-butene <5 ---- <5 <5µg/L5110-57-6

<5cis-1.4-Dichloro-2-butene <5 ---- <5 <5µg/L51476-11-5

<51.1.2.2-Tetrachloroethane <5 ---- <5 <5µg/L579-34-5

<51.2.3-Trichloropropane <5 ---- <5 <5µg/L596-18-4

<5Pentachloroethane <5 ---- <5 <5µg/L576-01-7

<51.2-Dibromo-3-chloropropane <5 ---- <5 <5µg/L596-12-8

EP074F: Halogenated Aromatic Compounds

<5Chlorobenzene <5 ---- <5 <5µg/L5108-90-7

<5Bromobenzene <5 ---- <5 <5µg/L5108-86-1

<52-Chlorotoluene <5 ---- <5 <5µg/L595-49-8

<54-Chlorotoluene <5 ---- <5 <5µg/L5106-43-4

<51.2.3-Trichlorobenzene <5 ---- <5 <5µg/L587-61-6

EP074G: Trihalomethanes

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP074G: Trihalomethanes - Continued

<5Chloroform <5 ---- <5 <5µg/L567-66-3

<5Bromodichloromethane <5 ---- <5 <5µg/L575-27-4

<5Dibromochloromethane <5 ---- <5 <5µg/L5124-48-1

<5Bromoform <5 ---- <5 <5µg/L575-25-2

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<1.0Naphthalene <1.0 ---- <1.0 <1.0µg/L191-20-3

<1.0Acenaphthylene <1.0 ---- <1.0 <1.0µg/L1208-96-8

<1.0Acenaphthene <1.0 ---- <1.0 <1.0µg/L183-32-9

<1.0Fluorene <1.0 ---- <1.0 <1.0µg/L186-73-7

<1.0Phenanthrene <1.0 ---- <1.0 <1.0µg/L185-01-8

<1.0Anthracene <1.0 ---- <1.0 <1.0µg/L1120-12-7

<1.0Fluoranthene <1.0 ---- <1.0 <1.0µg/L1206-44-0

<1.0Pyrene <1.0 ---- <1.0 <1.0µg/L1129-00-0

<1.0Benz(a)anthracene <1.0 ---- <1.0 <1.0µg/L156-55-3

<1.0Chrysene <1.0 ---- <1.0 <1.0µg/L1218-01-9

<1.0Benzo(b+j)fluoranthene <1.0 ---- <1.0 <1.0µg/L1205-99-2 205-82-3

<1.0Benzo(k)fluoranthene <1.0 ---- <1.0 <1.0µg/L1207-08-9

<0.5Benzo(a)pyrene <0.5 ---- <0.5 <0.5µg/L0.550-32-8

<1.0Indeno(1.2.3.cd)pyrene <1.0 ---- <1.0 <1.0µg/L1193-39-5

<1.0Dibenz(a.h)anthracene <1.0 ---- <1.0 <1.0µg/L153-70-3

<1.0Benzo(g.h.i)perylene <1.0 ---- <1.0 <1.0µg/L1191-24-2

<0.5^ <0.5 ---- <0.5 <0.5µg/L0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 ---- <0.5 <0.5µg/L0.5----Benzo(a)pyrene TEQ (zero)

EP075A: Phenolic Compounds

<2Phenol <2 ---- <2 <2µg/L2108-95-2

<22-Chlorophenol <2 ---- <2 <2µg/L295-57-8

<22-Methylphenol <2 ---- <2 <2µg/L295-48-7

<43- & 4-Methylphenol <4 ---- <4 <4µg/L41319-77-3

<22-Nitrophenol <2 ---- <2 <2µg/L288-75-5

<22.4-Dimethylphenol <2 ---- <2 <2µg/L2105-67-9

<22.4-Dichlorophenol <2 ---- <2 <2µg/L2120-83-2

<22.6-Dichlorophenol <2 ---- <2 <2µg/L287-65-0

<24-Chloro-3-methylphenol <2 ---- <2 <2µg/L259-50-7

<22.4.6-Trichlorophenol <2 ---- <2 <2µg/L288-06-2

Page 408: Appendix - Department of Defence

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP075A: Phenolic Compounds - Continued

<22.4.5-Trichlorophenol <2 ---- <2 <2µg/L295-95-4

<4Pentachlorophenol <4 ---- <4 <4µg/L487-86-5

EP075B: Polynuclear Aromatic Hydrocarbons

<22-Methylnaphthalene <2 ---- <2 <2µg/L291-57-6

<22-Chloronaphthalene <2 ---- <2 <2µg/L291-58-7

<2N-2-Fluorenyl Acetamide <2 ---- <2 <2µg/L253-96-3

<27.12-Dimethylbenz(a)anthracene <2 ---- <2 <2µg/L257-97-6

<23-Methylcholanthrene <2 ---- <2 <2µg/L256-49-5

EP075C: Phthalate Esters

<2Dimethyl phthalate <2 ---- <2 <2µg/L2131-11-3

<2Diethyl phthalate <2 ---- <2 <2µg/L284-66-2

<2Di-n-butyl phthalate <2 ---- <2 <2µg/L284-74-2

<2Butyl benzyl phthalate <2 ---- <2 <2µg/L285-68-7

<10bis(2-ethylhexyl) phthalate <10 ---- <10 <10µg/L10117-81-7

<2Di-n-octylphthalate <2 ---- <2 <2µg/L2117-84-0

EP075D: Nitrosamines

<2N-Nitrosomethylethylamine <2 ---- <2 <2µg/L210595-95-6

<2N-Nitrosodiethylamine <2 ---- <2 <2µg/L255-18-5

<4N-Nitrosopyrrolidine <4 ---- <4 <4µg/L4930-55-2

<2N-Nitrosomorpholine <2 ---- <2 <2µg/L259-89-2

<2N-Nitrosodi-n-propylamine <2 ---- <2 <2µg/L2621-64-7

<2N-Nitrosopiperidine <2 ---- <2 <2µg/L2100-75-4

<2N-Nitrosodibutylamine <2 ---- <2 <2µg/L2924-16-3

<4N-Nitrosodiphenyl &

Diphenylamine

<4 ---- <4 <4µg/L486-30-6 122-39-4

<2Methapyrilene <2 ---- <2 <2µg/L291-80-5

EP075E: Nitroaromatics and Ketones

<22-Picoline <2 ---- <2 <2µg/L2109-06-8

<2Acetophenone <2 ---- <2 <2µg/L298-86-2

<2Nitrobenzene <2 ---- <2 <2µg/L298-95-3

<2Isophorone <2 ---- <2 <2µg/L278-59-1

<42.6-Dinitrotoluene <4 ---- <4 <4µg/L4606-20-2

<42.4-Dinitrotoluene <4 ---- <4 <4µg/L4121-14-2

<21-Naphthylamine <2 ---- <2 <2µg/L2134-32-7

Page 409: Appendix - Department of Defence

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP075E: Nitroaromatics and Ketones - Continued

<24-Nitroquinoline-N-oxide <2 ---- <2 <2µg/L256-57-5

<25-Nitro-o-toluidine <2 ---- <2 <2µg/L299-55-8

<2Azobenzene <2 ---- <2 <2µg/L2103-33-3

<21.3.5-Trinitrobenzene <2 ---- <2 <2µg/L299-35-4

<2Phenacetin <2 ---- <2 <2µg/L262-44-2

<24-Aminobiphenyl <2 ---- <2 <2µg/L292-67-1

<2Pentachloronitrobenzene <2 ---- <2 <2µg/L282-68-8

<2Pronamide <2 ---- <2 <2µg/L223950-58-5

<2Dimethylaminoazobenzene <2 ---- <2 <2µg/L260-11-7

<2Chlorobenzilate <2 ---- <2 <2µg/L2510-15-6

EP075F: Haloethers

<2Bis(2-chloroethyl) ether <2 ---- <2 <2µg/L2111-44-4

<2Bis(2-chloroethoxy) methane <2 ---- <2 <2µg/L2111-91-1

<24-Chlorophenyl phenyl ether <2 ---- <2 <2µg/L27005-72-3

<24-Bromophenyl phenyl ether <2 ---- <2 <2µg/L2101-55-3

EP075G: Chlorinated Hydrocarbons

<21.3-Dichlorobenzene <2 ---- <2 <2µg/L2541-73-1

<21.4-Dichlorobenzene <2 ---- <2 <2µg/L2106-46-7

<21.2-Dichlorobenzene <2 ---- <2 <2µg/L295-50-1

<2Hexachloroethane <2 ---- <2 <2µg/L267-72-1

<21.2.4-Trichlorobenzene <2 ---- <2 <2µg/L2120-82-1

<2Hexachloropropylene <2 ---- <2 <2µg/L21888-71-7

<2Hexachlorobutadiene <2 ---- <2 <2µg/L287-68-3

<10Hexachlorocyclopentadiene <10 ---- <10 <10µg/L1077-47-4

<2Pentachlorobenzene <2 ---- <2 <2µg/L2608-93-5

<4Hexachlorobenzene (HCB) <4 ---- <4 <4µg/L4118-74-1

EP075H: Anilines and Benzidines

<2Aniline <2 ---- <2 <2µg/L262-53-3

<24-Chloroaniline <2 ---- <2 <2µg/L2106-47-8

<42-Nitroaniline <4 ---- <4 <4µg/L488-74-4

<43-Nitroaniline <4 ---- <4 <4µg/L499-09-2

<2Dibenzofuran <2 ---- <2 <2µg/L2132-64-9

<24-Nitroaniline <2 ---- <2 <2µg/L2100-01-6

<2Carbazole <2 ---- <2 <2µg/L286-74-8

Page 410: Appendix - Department of Defence

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP075H: Anilines and Benzidines - Continued

<23.3`-Dichlorobenzidine <2 ---- <2 <2µg/L291-94-1

EP075I: Organochlorine Pesticides

<2alpha-BHC <2 ---- <2 <2µg/L2319-84-6

<2beta-BHC <2 ---- <2 <2µg/L2319-85-7

<2gamma-BHC <2 ---- <2 <2µg/L258-89-9

<2delta-BHC <2 ---- <2 <2µg/L2319-86-8

<2Heptachlor <2 ---- <2 <2µg/L276-44-8

<2Aldrin <2 ---- <2 <2µg/L2309-00-2

<2Heptachlor epoxide <2 ---- <2 <2µg/L21024-57-3

<2alpha-Endosulfan <2 ---- <2 <2µg/L2959-98-8

<24.4`-DDE <2 ---- <2 <2µg/L272-55-9

<2Dieldrin <2 ---- <2 <2µg/L260-57-1

<2Endrin <2 ---- <2 <2µg/L272-20-8

<2beta-Endosulfan <2 ---- <2 <2µg/L233213-65-9

<24.4`-DDD <2 ---- <2 <2µg/L272-54-8

<2Endosulfan sulfate <2 ---- <2 <2µg/L21031-07-8

<44.4`-DDT <4 ---- <4 <4µg/L450-29-3

<4^ Sum of Aldrin + Dieldrin <4 ---- <4 <4µg/L4309-00-2/60-57-1

<4^ Sum of DDD + DDE + DDT <4 ---- <4 <4µg/L472-54-8/72-55-9/5

0-2

EP075J: Organophosphorus Pesticides

<2Dichlorvos <2 ---- <2 <2µg/L262-73-7

<2Dimethoate <2 ---- <2 <2µg/L260-51-5

<2Diazinon <2 ---- <2 <2µg/L2333-41-5

<2Chlorpyrifos-methyl <2 ---- <2 <2µg/L25598-13-0

<2Malathion <2 ---- <2 <2µg/L2121-75-5

<2Fenthion <2 ---- <2 <2µg/L255-38-9

<2Chlorpyrifos <2 ---- <2 <2µg/L22921-88-2

<2Pirimphos-ethyl <2 ---- <2 <2µg/L223505-41-1

<2Chlorfenvinphos <2 ---- <2 <2µg/L2470-90-6

<2Prothiofos <2 ---- <2 <2µg/L234643-46-4

<2Ethion <2 ---- <2 <2µg/L2563-12-2

EP080/071: Total Petroleum Hydrocarbons

<20 <20 <20 <20 <20µg/L20----C6 - C9 Fraction

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP080/071: Total Petroleum Hydrocarbons - Continued

<50 <50 ---- <50 <50µg/L50----C10 - C14 Fraction

<100 <100 ---- <100 <100µg/L100----C15 - C28 Fraction

<50 <50 ---- <50 <50µg/L50----C29 - C36 Fraction

<50^ <50 ---- <50 <50µg/L50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<20C6 - C10 Fraction <20 <20 <20 <20µg/L20C6_C10

<20^ C6 - C10 Fraction minus BTEX

(F1)

<20 <20 <20 <20µg/L20C6_C10-BTEX

<100 <100 ---- <100 <100µg/L100---->C10 - C16 Fraction

<100 <100 ---- <100 <100µg/L100---->C16 - C34 Fraction

<100 <100 ---- <100 <100µg/L100---->C34 - C40 Fraction

<100^ <100 ---- <100 <100µg/L100---->C10 - C40 Fraction (sum)

<100^ <100 ---- <100 <100µg/L100---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<1Benzene <1 <1 <1 <1µg/L171-43-2

<2Toluene <2 <2 <2 <2µg/L2108-88-3

<2Ethylbenzene <2 <2 <2 <2µg/L2100-41-4

<2meta- & para-Xylene <2 <2 <2 <2µg/L2108-38-3 106-42-3

<2ortho-Xylene <2 <2 <2 <2µg/L295-47-6

<2^ Total Xylenes <2 <2 <2 <2µg/L21330-20-7

<1^ <1 <1 <1 <1µg/L1----Sum of BTEX

<5Naphthalene <5 <5 <5 <5µg/L591-20-3

EP116: 1.4-Dioxane

<0.51.4-Dioxane <0.5 ---- <0.5 <0.5µg/L0.5123-91-1

EP231A: Perfluoroalkyl Sulfonic Acids

<0.02Perfluorobutane sulfonic acid

(PFBS)

<0.02 ---- <0.02 1.56µg/L0.02375-73-5

<0.02Perfluoropentane sulfonic acid

(PFPeS)

<0.02 ---- <0.02 1.25µg/L0.022706-91-4

<0.02Perfluorohexane sulfonic acid

(PFHxS)

<0.02 ---- <0.02 8.86µg/L0.02355-46-4

<0.02Perfluoroheptane sulfonic acid

(PFHpS)

<0.02 ---- <0.02 0.62µg/L0.02375-92-8

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP231A: Perfluoroalkyl Sulfonic Acids - Continued

<0.01Perfluorooctane sulfonic acid

(PFOS)

<0.01 ---- <0.01 22.1µg/L0.011763-23-1

<0.02Perfluorodecane sulfonic acid

(PFDS)

<0.02 ---- <0.02 0.04µg/L0.02335-77-3

EP231B: Perfluoroalkyl Carboxylic Acids

<0.1Perfluorobutanoic acid (PFBA) <0.1 ---- <0.1 0.6µg/L0.1375-22-4

<0.02Perfluoropentanoic acid (PFPeA) <0.02 ---- <0.02 0.69µg/L0.022706-90-3

<0.02Perfluorohexanoic acid (PFHxA) <0.02 ---- <0.02 2.32µg/L0.02307-24-4

<0.02Perfluoroheptanoic acid (PFHpA) <0.02 ---- <0.02 0.43µg/L0.02375-85-9

<0.01Perfluorooctanoic acid (PFOA) <0.01 ---- <0.01 0.90µg/L0.01335-67-1

<0.02Perfluorononanoic acid (PFNA) <0.02 ---- <0.02 0.04µg/L0.02375-95-1

<0.02Perfluorodecanoic acid (PFDA) <0.02 ---- <0.02 0.03µg/L0.02335-76-2

<0.02Perfluoroundecanoic acid

(PFUnDA)

<0.02 ---- <0.02 <0.02µg/L0.022058-94-8

<0.02Perfluorododecanoic acid

(PFDoDA)

<0.02 ---- <0.02 <0.02µg/L0.02307-55-1

<0.02Perfluorotridecanoic acid

(PFTrDA)

<0.02 ---- <0.02 <0.02µg/L0.0272629-94-8

<0.05Perfluorotetradecanoic acid

(PFTeDA)

<0.05 ---- <0.05 <0.05µg/L0.05376-06-7

EP231C: Perfluoroalkyl Sulfonamides

<0.02Perfluorooctane sulfonamide

(FOSA)

<0.02 ---- <0.02 0.08µg/L0.02754-91-6

<0.05N-Methyl perfluorooctane

sulfonamide (MeFOSA)

<0.05 ---- <0.05 <0.05µg/L0.0531506-32-8

<0.05N-Ethyl perfluorooctane

sulfonamide (EtFOSA)

<0.05 ---- <0.05 <0.05µg/L0.054151-50-2

<0.05N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

<0.05 ---- <0.05 <0.05µg/L0.052448-09-7

<0.05N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

<0.05 ---- <0.05 <0.05µg/L0.051691-99-2

<0.02N-Methyl perfluorooctane

sulfonamidoacetic acid

(MeFOSAA)

<0.02 ---- <0.02 <0.02µg/L0.022355-31-9

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP231C: Perfluoroalkyl Sulfonamides - Continued

<0.02N-Ethyl perfluorooctane

sulfonamidoacetic acid

(EtFOSAA)

<0.02 ---- <0.02 <0.02µg/L0.022991-50-6

EP231D: (n:2) Fluorotelomer Sulfonic Acids

<0.054:2 Fluorotelomer sulfonic acid

(4:2 FTS)

<0.05 ---- <0.05 <0.05µg/L0.05757124-72-4

<0.056:2 Fluorotelomer sulfonic acid

(6:2 FTS)

<0.05 ---- <0.05 0.29µg/L0.0527619-97-2

<0.058:2 Fluorotelomer sulfonic acid

(8:2 FTS)

<0.05 ---- <0.05 0.16µg/L0.0539108-34-4

<0.0510:2 Fluorotelomer sulfonic acid

(10:2 FTS)

<0.05 ---- <0.05 <0.05µg/L0.05120226-60-0

EP231P: PFAS Sums

<0.01 <0.01 ---- <0.01 40.0µg/L0.01----Sum of PFAS

<0.01Sum of PFHxS and PFOS <0.01 ---- <0.01 31.0µg/L0.01355-46-4/1763-23-

1

<0.01 <0.01 ---- <0.01 37.9µg/L0.01----Sum of PFAS (WA DER List)

EP074S: VOC Surrogates

1101.2-Dichloroethane-D4 109 ---- 107 108%517060-07-0

106Toluene-D8 108 ---- 104 103%52037-26-5

1024-Bromofluorobenzene 102 ---- 100 99.8%5460-00-4

EP075(SIM)S: Phenolic Compound Surrogates

36.4Phenol-d6 39.3 ---- 32.3 22.9%113127-88-3

58.22-Chlorophenol-D4 69.2 ---- 60.7 61.5%193951-73-6

66.22.4.6-Tribromophenol 84.4 ---- 67.7 51.6%1118-79-6

EP075(SIM)T: PAH Surrogates

63.22-Fluorobiphenyl 77.3 ---- 63.1 76.5%1321-60-8

67.1Anthracene-d10 85.9 ---- 84.7 98.5%11719-06-8

69.14-Terphenyl-d14 86.4 ---- 70.3 72.4%11718-51-0

EP075S: Acid Extractable Surrogates

30.72-Fluorophenol 39.7 ---- 34.6 26.7%2367-12-4

25.6Phenol-d6 30.5 ---- 25.7 27.0%213127-88-3

48.22-Chlorophenol-D4 59.9 ---- 51.0 54.1%293951-73-6

57.72.4.6-Tribromophenol 77.2 ---- 62.5 61.7%2118-79-6

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Analytical Results

0902_MW50_0607170902_QC511_0607170902_QC601_0607170902_QC510_0507170902_QC509_050717Client sample IDSub-Matrix: WATER

(Matrix: WATER)

06-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0006-Jul-2017 00:0005-Jul-2017 00:00Client sampling date / time

ES1716700-040ES1716700-039ES1716700-038ES1716700-037ES1716700-036UnitLORCAS NumberCompound

Result Result Result Result Result

EP075T: Base/Neutral Extractable Surrogates

58.1Nitrobenzene-D5 72.8 ---- 62.3 58.6%24165-60-0

48.01.2-Dichlorobenzene-D4 61.3 ---- 54.6 42.6%22199-69-1

56.52-Fluorobiphenyl 69.5 ---- 57.7 59.0%2321-60-8

66.2Anthracene-d10 86.2 ---- 67.4 71.0%21719-06-8

71.14-Terphenyl-d14 90.9 ---- 73.8 73.0%21718-51-0

EP080S: TPH(V)/BTEX Surrogates

1121.2-Dichloroethane-D4 111 99.5 109 110%217060-07-0

110Toluene-D8 112 113 108 107%22037-26-5

1004-Bromofluorobenzene 99.7 88.9 97.6 96.9%2460-00-4

EP116S: 1.4-Dioxane Surrogate

92.51.4-Dioxane-d8 108 ---- 103 113%0.517647-74-4

EP231S: PFAS Surrogate

83.1 89.7 ---- 87.8 105%0.02----13C4-PFOS

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Surrogate Control Limits

Recovery Limits (%)Sub-Matrix: WATER

Compound CAS Number Low High

EP074S: VOC Surrogates

1.2-Dichloroethane-D4 17060-07-0 78 133

Toluene-D8 2037-26-5 79 129

4-Bromofluorobenzene 460-00-4 81 124

EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 13127-88-3 10 44

2-Chlorophenol-D4 93951-73-6 14 94

2.4.6-Tribromophenol 118-79-6 17 125

EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl 321-60-8 20 104

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 32 112

EP075S: Acid Extractable Surrogates

2-Fluorophenol 367-12-4 10 117

Phenol-d6 13127-88-3 10 69

2-Chlorophenol-D4 93951-73-6 21 130

2.4.6-Tribromophenol 118-79-6 10 151

EP075T: Base/Neutral Extractable Surrogates

Nitrobenzene-D5 4165-60-0 29 142

1.2-Dichlorobenzene-D4 2199-69-1 24 121

2-Fluorobiphenyl 321-60-8 27 135

Anthracene-d10 1719-06-8 27 113

4-Terphenyl-d14 1718-51-0 21 123

EP080S: TPH(V)/BTEX Surrogates

1.2-Dichloroethane-D4 17060-07-0 71 137

Toluene-D8 2037-26-5 79 131

4-Bromofluorobenzene 460-00-4 70 128

EP116S: 1.4-Dioxane Surrogate

1.4-Dioxane-d8 17647-74-4 69 127

EP231S: PFAS Surrogate

13C4-PFOS ---- 60 130

Page 416: Appendix - Department of Defence

False

5 5.00True

Environmental

QUALITY CONTROL REPORTWork Order : ES1716700 Page : 1 of 47

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER :Contact Loren Schiavon

:Address LEVEL 21, 420 GEORGE STREET

SYDNEY NSW, AUSTRALIA 2000

Address : 277-289 Woodpark Road Smithfield NSW Australia 2164

::Telephone +61 02 8934 0000 +61 2 8784 8503:Telephone

:Project 60547028, task 3.1 Date Samples Received : 06-Jul-2017

:Order number 60547028 Date Analysis Commenced : 07-Jul-2017

:C-O-C number ---- Issue Date : 17-Jul-2017

Sampler : James Tomilson and Sebastian McDlay

Site : RAAF Richmond

Quote number : SY/308/17

No. of samples received 40:

No. of samples analysed 40:

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Alex Rossi Organic Chemist Sydney Organics, Smithfield, NSW

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Celine Conceicao Senior Spectroscopist Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Sanjeshni Jyoti Senior Chemist Volatiles Sydney Organics, Smithfield, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR: 0% - 50%; Result > 20 times LOR: 0% - 20%.

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 989654)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 428 404 5.77 0% - 20%Anonymous ES1716632-006

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 1810 1780 1.90 0% - 20%0902_MW64_040717 ES1716700-024

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 991957)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 <10 0.00 No LimitAnonymous ES1716552-001

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 545 544 0.184 0% - 20%0902_MW61_050717 ES1716700-001

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 991958)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 9850 11400 14.7 0% - 20%0902_MW62_050717 ES1716700-030

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 74 81 8.58 No LimitAnonymous EW1702973-004

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QC Lot: 994357)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 612 601 1.81 0% - 20%0902_MW20_060717 ES1716700-007

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L 3250 3140 3.38 0% - 20%0902_MW52_060717 ES1716700-033

ED037P: Alkalinity by PC Titrator (QC Lot: 987911)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_MW61_050717 ES1716700-001

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 437 472 7.58 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 437 472 7.58 0% - 20%

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_MW45_060717 ES1716700-010

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 274 285 3.91 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 274 285 3.91 0% - 20%

ED037P: Alkalinity by PC Titrator (QC Lot: 987913)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_MW72_040717 ES1716700-021

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 138 142 3.28 0% - 20%

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

ED037P: Alkalinity by PC Titrator (QC Lot: 987913) - continued

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 138 142 3.28 0% - 20%0902_MW72_040717 ES1716700-021

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716763-001

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 1150 1180 3.18 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 1150 1180 3.18 0% - 20%

ED037P: Alkalinity by PC Titrator (QC Lot: 988505)

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No Limit0902_MW62_050717 ES1716700-030

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 804 778 3.30 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 804 778 3.30 0% - 20%

ED037-P: Hydroxide Alkalinity as CaCO3 DMO-210-001 1 mg/L <1 <1 0.00 No LimitAnonymous ES1716765-006

ED037-P: Carbonate Alkalinity as CaCO3 3812-32-6 1 mg/L <1 <1 0.00 No Limit

ED037-P: Bicarbonate Alkalinity as CaCO3 71-52-3 1 mg/L 272 283 3.76 0% - 20%

ED037-P: Total Alkalinity as CaCO3 ---- 1 mg/L 272 283 3.76 0% - 20%

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 985225)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 1 1 0.00 No LimitAnonymous ES1716586-001

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 22 22 0.00 0% - 20%Anonymous ES1716649-008

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 985228)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 35 35 0.00 0% - 20%0902_MW36_060717 ES1716700-009

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 10 10 0.00 No Limit0902_MW66_040717 ES1716700-023

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 985232)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 170 168 0.842 0% - 20%0902_MW52_060717 ES1716700-033

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QC Lot: 985453)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 34 30 10.7 0% - 20%Anonymous ES1716557-001

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L 147 162 9.49 0% - 20%Anonymous ES1716656-001

ED045G: Chloride by Discrete Analyser (QC Lot: 985224)

ED045G: Chloride 16887-00-6 1 mg/L 268 266 0.735 0% - 20%Anonymous ES1716586-001

ED045G: Chloride 16887-00-6 1 mg/L 47 47 0.00 0% - 20%Anonymous ES1716649-008

ED045G: Chloride by Discrete Analyser (QC Lot: 985227)

ED045G: Chloride 16887-00-6 1 mg/L 374 375 0.00 0% - 20%0902_MW36_060717 ES1716700-009

ED045G: Chloride 16887-00-6 1 mg/L 330 316 4.22 0% - 20%0902_MW66_040717 ES1716700-023

ED045G: Chloride by Discrete Analyser (QC Lot: 985231)

ED045G: Chloride 16887-00-6 1 mg/L 970 962 0.827 0% - 20%0902_MW52_060717 ES1716700-033

ED045G: Chloride by Discrete Analyser (QC Lot: 985452)

ED045G: Chloride 16887-00-6 1 mg/L 35 35 0.00 0% - 20%Anonymous ES1716557-001

ED045G: Chloride 16887-00-6 1 mg/L 178 178 0.00 0% - 20%Anonymous ES1716656-001

ED093F: Dissolved Major Cations (QC Lot: 991315)

ED093F: Calcium 7440-70-2 1 mg/L 37 37 0.00 0% - 20%0902_MW61_050717 ES1716700-001

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AECOM Australia Pty Ltd

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

ED093F: Dissolved Major Cations (QC Lot: 991315) - continued

ED093F: Magnesium 7439-95-4 1 mg/L 41 42 0.00 0% - 20%0902_MW61_050717 ES1716700-001

ED093F: Sodium 7440-23-5 1 mg/L 100 98 2.23 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 3 3 0.00 No Limit

ED093F: Calcium 7440-70-2 1 mg/L 6 6 0.00 No Limit0902_MW21_060717 ES1716700-011

ED093F: Magnesium 7439-95-4 1 mg/L 5 6 0.00 No Limit

ED093F: Sodium 7440-23-5 1 mg/L 161 172 6.28 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L <1 <1 0.00 No Limit

ED093F: Dissolved Major Cations (QC Lot: 991318)

ED093F: Calcium 7440-70-2 1 mg/L 15 14 0.00 0% - 50%0902_MW72_040717 ES1716700-021

ED093F: Magnesium 7439-95-4 1 mg/L 13 12 0.00 0% - 50%

ED093F: Sodium 7440-23-5 1 mg/L 15 14 7.04 0% - 50%

ED093F: Potassium 7440-09-7 1 mg/L 4 4 0.00 No Limit

ED093F: Calcium 7440-70-2 1 mg/L 66 63 4.08 0% - 20%0902_MW47_060717 ES1716700-032

ED093F: Magnesium 7439-95-4 1 mg/L 74 76 2.74 0% - 20%

ED093F: Sodium 7440-23-5 1 mg/L 900 954 5.78 0% - 20%

ED093F: Potassium 7440-09-7 1 mg/L 2 2 0.00 No Limit

EG020F: Dissolved Metals by ICP-MS (QC Lot: 991313)

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW61_050717 ES1716700-001

EG020A-F: Arsenic 7440-38-2 0.001 mg/L 0.010 0.007 25.8 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 4.22 4.98 16.4 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.016 0.014 13.2 0% - 50%

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.024 0.021 11.7 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.02 0.01 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L 19.3 16.8 13.8 0% - 20%

EG020A-F: Bromine 7726-95-6 0.1 mg/L 0.2 0.3 0.00 No Limit

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW21_060717 ES1716700-011

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L 0.004 0.004 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.006 0.008 34.9 No Limit

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 <0.005 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L 0.01 0.02 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 <0.05 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L 0.7 0.6 0.00 No Limit

EG020F: Dissolved Metals by ICP-MS (QC Lot: 991316)

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EG020F: Dissolved Metals by ICP-MS (QC Lot: 991316) - continued

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L 0.0002 0.0003 0.00 No Limit0902_MW72_040717 ES1716700-021

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 1.35 1.36 1.09 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.015 0.014 9.06 0% - 50%

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.022 0.021 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 <0.01 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 <0.05 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L 0.1 0.1 0.00 No Limit

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW47_060717 ES1716700-032

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 <0.001 0.00 No Limit

EG020A-F: Manganese 7439-96-5 0.001 mg/L 0.400 0.387 3.23 0% - 20%

EG020A-F: Nickel 7440-02-0 0.001 mg/L 0.006 0.006 0.00 No Limit

EG020A-F: Zinc 7440-66-6 0.005 mg/L 0.006 <0.005 0.00 No Limit

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 <0.01 0.00 No Limit

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 <0.05 0.00 No Limit

EG020A-F: Bromine 7726-95-6 0.1 mg/L 3.2 3.2 0.00 0% - 20%

EG035F: Dissolved Mercury by FIMS (QC Lot: 991314)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW48_050717 ES1716700-004

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW45_060717 ES1716700-010

EG035F: Dissolved Mercury by FIMS (QC Lot: 991317)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW64_040717 ES1716700-024

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 <0.0001 0.00 No Limit0902_MW62_050717 ES1716700-030

EK040P: Fluoride by PC Titrator (QC Lot: 987910)

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.4 0.4 0.00 No Limit0902_MW61_050717 ES1716700-001

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.6 0.6 0.00 No Limit0902_MW45_060717 ES1716700-010

EK040P: Fluoride by PC Titrator (QC Lot: 987912)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 <0.1 0.00 No Limit0902_MW72_040717 ES1716700-021

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.6 0.6 0.00 No LimitAnonymous ES1716763-001

EK040P: Fluoride by PC Titrator (QC Lot: 988504)

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.9 0.9 0.00 No Limit0902_MW62_050717 ES1716700-030

EK040P: Fluoride 16984-48-8 0.1 mg/L 0.1 0.1 0.00 No LimitAnonymous ES1716765-006

EK055G: Ammonia as N by Discrete Analyser (QC Lot: 985831)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L 0.10 0.09 0.00 No Limit0902_MW61_050717 ES1716700-001

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AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EK055G: Ammonia as N by Discrete Analyser (QC Lot: 985831) - continued

EK055G: Ammonia as N 7664-41-7 0.01 mg/L 0.06 0.06 0.00 No Limit0902_MW45_060717 ES1716700-010

EK055G: Ammonia as N by Discrete Analyser (QC Lot: 985833)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L 0.03 0.05 47.7 No Limit0902_MW66_040717 ES1716700-023

EK055G: Ammonia as N 7664-41-7 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW47_060717 ES1716700-032

EK057G: Nitrite as N by Discrete Analyser (QC Lot: 985226)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW45_060717 ES1716700-010

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW36_060717 ES1716700-009

EK057G: Nitrite as N by Discrete Analyser (QC Lot: 985230)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW66_040717 ES1716700-023

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW52_060717 ES1716700-033

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QC Lot: 985830)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW61_050717 ES1716700-001

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW45_060717 ES1716700-010

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QC Lot: 985832)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L 0.09 0.09 0.00 No Limit0902_MW66_040717 ES1716700-023

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L 106 107 1.46 0% - 20%0902_MW47_060717 ES1716700-032

EK071G: Reactive Phosphorus as P by discrete analyser (QC Lot: 985223)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 <0.01 0.00 No LimitAnonymous ES1716586-001

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L 0.84 1.01 18.8 0% - 20%Anonymous ES1716649-008

EK071G: Reactive Phosphorus as P by discrete analyser (QC Lot: 985229)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW45_060717 ES1716700-010

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 <0.01 0.00 No Limit0902_MW66_040717 ES1716700-023

EK071G: Reactive Phosphorus as P by discrete analyser (QC Lot: 985233)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L 6.28 6.61 5.24 0% - 20%Anonymous EW1702979-001

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L 0.02 0.02 0.00 No Limit0902_MW52_060717 ES1716700-033

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 987304)

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

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AECOM Australia Pty Ltd

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 987304) - continued

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074A: Monocyclic Aromatic Hydrocarbons (QC Lot: 987321)

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074: Styrene 100-42-5 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 <5 0.00 No Limit

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 <5 0.00 No Limit

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 <5 0.00 No Limit

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 <5 0.00 No Limit

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 <5 0.00 No Limit

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 <5 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 987304)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074B: Oxygenated Compounds (QC Lot: 987321)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 <50 0.00 No Limit0902_QC102_060717 ES1716700-031

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074B: Oxygenated Compounds (QC Lot: 987321) - continued

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 <50 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 <50 0.00 No Limit

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 <50 0.00 No Limit

EP074C: Sulfonated Compounds (QC Lot: 987304)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074C: Sulfonated Compounds (QC Lot: 987321)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: Carbon disulfide 75-15-0 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074D: Fumigants (QC Lot: 987304)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074D: Fumigants (QC Lot: 987321)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 <5 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 987304)

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 987304) - continued

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

Page 425: Appendix - Department of Defence

10 of 47:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 987304) - continued

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074E: Halogenated Aliphatic Compounds (QC Lot: 987321)

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: Iodomethane 74-88-4 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 <5 0.00 No Limit

Page 426: Appendix - Department of Defence

11 of 47:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074E: Halogenated Aliphatic Compounds (QC Lot: 987321) - continued

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 <5 0.00 No Limit

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 <5 0.00 No Limit

EP074: Trichloroethene 79-01-6 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromomethane 74-95-3 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 <5 0.00 No Limit

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 <5 0.00 No Limit

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 <5 0.00 No Limit

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 <5 0.00 No Limit

EP074: Pentachloroethane 76-01-7 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 <5 0.00 No Limit

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 <50 0.00 No Limit

EP074: Chloromethane 74-87-3 50 µg/L <50 <50 0.00 No Limit

EP074: Vinyl chloride 75-01-4 50 µg/L <50 <50 0.00 No Limit

EP074: Bromomethane 74-83-9 50 µg/L <50 <50 0.00 No Limit

EP074: Chloroethane 75-00-3 50 µg/L <50 <50 0.00 No Limit

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 <50 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 987304)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074F: Halogenated Aromatic Compounds (QC Lot: 987321)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074: Chlorobenzene 108-90-7 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

Page 427: Appendix - Department of Defence

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Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP074F: Halogenated Aromatic Compounds (QC Lot: 987321) - continued

EP074: Bromobenzene 108-86-1 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 <5 0.00 No Limit

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 <5 0.00 No Limit

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 <5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 987304)

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_MW61_050717 ES1716700-001

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074G: Trihalomethanes (QC Lot: 987321)

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP074: Chloroform 67-66-3 5 µg/L <5 <5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 <5 0.00 No Limit

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 <5 0.00 No Limit

EP074: Bromoform 75-25-2 5 µg/L <5 <5 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 987303)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_MW61_050717 ES1716700-001

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_MW21_060717 ES1716700-011

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 987322)

EP080: C6 - C9 Fraction ---- 20 µg/L 60 60 0.00 No Limit0902_MW72_040717 ES1716700-021

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No Limit0902_QC102_060717 ES1716700-031

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 990407)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716485-001

EP080: C6 - C9 Fraction ---- 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716917-001

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 987303)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_MW61_050717 ES1716700-001

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_MW21_060717 ES1716700-011

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 987322)

EP080: C6 - C10 Fraction C6_C10 20 µg/L 60 60 0.00 No Limit0902_MW72_040717 ES1716700-021

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No Limit0902_QC102_060717 ES1716700-031

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 990407)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716485-001

Page 428: Appendix - Department of Defence

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Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 990407) - continued

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 <20 0.00 No LimitAnonymous ES1716917-001

EP080: BTEXN (QC Lot: 987303)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_MW61_050717 ES1716700-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_MW21_060717 ES1716700-011

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: BTEXN (QC Lot: 987322)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_MW72_040717 ES1716700-021

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No Limit0902_QC102_060717 ES1716700-031

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: BTEXN (QC Lot: 990407)

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716485-001

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No Limit

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP080: Benzene 71-43-2 1 µg/L <1 <1 0.00 No LimitAnonymous ES1716917-001

Page 429: Appendix - Department of Defence

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Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP080: BTEXN (QC Lot: 990407) - continued

EP080: Toluene 108-88-3 2 µg/L <2 <2 0.00 No LimitAnonymous ES1716917-001

EP080: Ethylbenzene 100-41-4 2 µg/L <2 <2 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 <2 0.00 No Limit

EP080: ortho-Xylene 95-47-6 2 µg/L <2 <2 0.00 No Limit

EP080: Naphthalene 91-20-3 5 µg/L <5 <5 0.00 No Limit

EP116: 1.4-Dioxane (QC Lot: 987038)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <2.0 <2.0 0.00 No Limit0902_MW61_050717 ES1716700-001

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_MW21_060717 ES1716700-011

EP116: 1.4-Dioxane (QC Lot: 989615)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_MW72_040717 ES1716700-021

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 <0.5 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 984238)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 1.02 1.06 3.86 0% - 20%0902_MW61_050717 ES1716700-001

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.12 0.12 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.12 0.13 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 1.43 1.49 3.70 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.04 0.04 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 7.16 7.58 5.68 0% - 20%0902_MW21_060717 ES1716700-011

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 0.34 0.36 5.10 0% - 50%

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 0.53 0.52 0.00 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 8.01 8.21 2.54 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.28 0.30 7.18 0% - 50%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 984239)

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 14.6 14.6 0.00 0% - 20%0902_MW72_040717 ES1716700-021

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 21.5 21.2 1.37 0% - 20%

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 11.4 11.2 2.30 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 80.0 78.9 1.38 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 4.64 4.72 1.69 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 0.03 0.03 0.00 No Limit

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 986813)

Page 430: Appendix - Department of Defence

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Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231A: Perfluoroalkyl Sulfonic Acids (QC Lot: 986813) - continued

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L 22.1 19.6 12.0 0% - 20%0902_MW50_060717 ES1716700-040

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L 1.56 1.38 12.1 0% - 20%

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L 1.25 1.14 8.88 0% - 20%

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L 8.86 8.03 9.80 0% - 20%

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L 0.62 0.55 12.0 0% - 20%

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L 0.04 0.03 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984238)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.10 0.10 0.00 0% - 50%0902_MW61_050717 ES1716700-001

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.13 0.13 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.09 0.09 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.49 0.54 8.58 0% - 20%0902_MW21_060717 ES1716700-011

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.15 0.16 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 0.63 0.70 11.1 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.21 0.24 15.0 0% - 50%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L 0.02 0.03 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984239)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 3.94 3.95 0.329 0% - 20%0902_MW72_040717 ES1716700-021

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 3.67 3.62 1.32 0% - 20%

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 14.5 13.7 5.67 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.77 0.78 0.00 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 984239) - continued

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L 1.3 1.3 0.00 0% - 50%0902_MW72_040717 ES1716700-021

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 <0.01 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 <0.1 0.00 No Limit

EP231B: Perfluoroalkyl Carboxylic Acids (QC Lot: 986813)

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L 0.90 0.81 10.1 0% - 20%0902_MW50_060717 ES1716700-040

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L 0.69 0.62 11.0 0% - 20%

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L 2.32 2.06 12.0 0% - 20%

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L 0.43 0.38 12.2 0% - 20%

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L 0.04 0.05 0.00 No Limit

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L 0.03 0.02 0.00 No Limit

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L 0.6 0.5 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 984238)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW61_050717 ES1716700-001

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW21_060717 ES1716700-011

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 984238) - continued

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW21_060717 ES1716700-011

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 984239)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW72_040717 ES1716700-021

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 986813)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L 0.08 0.07 0.00 No Limit0902_MW50_060717 ES1716700-040

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231C: Perfluoroalkyl Sulfonamides (QC Lot: 986813) - continued

EP231X: N-Methyl perfluorooctane

sulfonamidoacetic acid (MeFOSAA)

2355-31-9 0.02 µg/L <0.02 <0.02 0.00 No Limit0902_MW50_060717 ES1716700-040

EP231X: N-Ethyl perfluorooctane

sulfonamidoacetic acid (EtFOSAA)

2991-50-6 0.02 µg/L <0.02 <0.02 0.00 No Limit

EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

31506-32-8 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane sulfonamide

(EtFOSA)

4151-50-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Methyl perfluorooctane

sulfonamidoethanol (MeFOSE)

2448-09-7 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: N-Ethyl perfluorooctane

sulfonamidoethanol (EtFOSE)

1691-99-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 984238)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW61_050717 ES1716700-001

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW21_060717 ES1716700-011

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 984239)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW72_040717 ES1716700-021

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_QC102_060717 ES1716700-031

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Sub-Matrix: WATER Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 984239) - continued

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QC Lot: 986813)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2

FTS)

757124-72-4 0.05 µg/L <0.05 <0.05 0.00 No Limit0902_MW50_060717 ES1716700-040

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2

FTS)

27619-97-2 0.05 µg/L 0.29 0.26 9.76 No Limit

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2

FTS)

39108-34-4 0.05 µg/L 0.16 0.13 20.5 No Limit

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2

FTS)

120226-60-0 0.05 µg/L <0.05 <0.05 0.00 No Limit

EP231P: PFAS Sums (QC Lot: 984238)

EP231X: Sum of PFAS ---- 0.01 µg/L 3.05 3.16 3.54 0% - 20%0902_MW61_050717 ES1716700-001

EP231X: Sum of PFAS ---- 0.01 µg/L 17.8 18.6 4.50 0% - 20%0902_MW21_060717 ES1716700-011

EP231P: PFAS Sums (QC Lot: 984239)

EP231X: Sum of PFAS ---- 0.01 µg/L 156 154 1.51 0% - 20%0902_MW72_040717 ES1716700-021

EP231X: Sum of PFAS ---- 0.01 µg/L 0.03 0.03 0.00 No Limit0902_QC102_060717 ES1716700-031

EP231P: PFAS Sums (QC Lot: 986813)

EP231X: Sum of PFAS ---- 0.01 µg/L 40.0 35.6 11.5 0% - 20%0902_MW50_060717 ES1716700-040

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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Spike (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 989654)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 99.22000 mg/L 10987

<10 102293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 991957)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1072000 mg/L 10987

<10 105293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 991958)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1012000 mg/L 10987

<10 85.2293 mg/L 12666

EA015: Total Dissolved Solids dried at 180 ± 5 °C (QCLot: 994357)

EA015H: Total Dissolved Solids @180°C ---- 10 mg/L <10 1012000 mg/L 10987

<10 94.0293 mg/L 12666

ED037P: Alkalinity by PC Titrator (QCLot: 987911)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 98.5200 mg/L 11181

ED037P: Alkalinity by PC Titrator (QCLot: 987913)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 97.2200 mg/L 11181

ED037P: Alkalinity by PC Titrator (QCLot: 988505)

ED037-P: Total Alkalinity as CaCO3 ---- ---- mg/L ---- 95.5200 mg/L 11181

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985225)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 10125 mg/L 12282

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985228)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 10225 mg/L 12282

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985232)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 10125 mg/L 12282

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985453)

ED041G: Sulfate as SO4 - Turbidimetric 14808-79-8 1 mg/L <1 10125 mg/L 12282

ED045G: Chloride by Discrete Analyser (QCLot: 985224)

ED045G: Chloride 16887-00-6 1 mg/L <1 10110 mg/L 12781

<1 98.61000 mg/L 12781

ED045G: Chloride by Discrete Analyser (QCLot: 985227)

ED045G: Chloride 16887-00-6 1 mg/L <1 99.810 mg/L 12781

<1 1031000 mg/L 12781

ED045G: Chloride by Discrete Analyser (QCLot: 985231)

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Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

ED045G: Chloride by Discrete Analyser (QCLot: 985231) - continued

ED045G: Chloride 16887-00-6 1 mg/L <1 10210 mg/L 12781

<1 1021000 mg/L 12781

ED045G: Chloride by Discrete Analyser (QCLot: 985452)

ED045G: Chloride 16887-00-6 1 mg/L <1 92.510 mg/L 12781

<1 90.41000 mg/L 12781

ED093F: Dissolved Major Cations (QCLot: 991315)

ED093F: Calcium 7440-70-2 1 mg/L <1 95.250 mg/L 11480

ED093F: Magnesium 7439-95-4 1 mg/L <1 93.650 mg/L 11690

ED093F: Sodium 7440-23-5 1 mg/L <1 90.350 mg/L 12082

ED093F: Potassium 7440-09-7 1 mg/L <1 93.250 mg/L 11385

ED093F: Dissolved Major Cations (QCLot: 991318)

ED093F: Calcium 7440-70-2 1 mg/L <1 90.550 mg/L 11480

ED093F: Magnesium 7439-95-4 1 mg/L <1 92.750 mg/L 11690

ED093F: Sodium 7440-23-5 1 mg/L <1 95.650 mg/L 12082

ED093F: Potassium 7440-09-7 1 mg/L <1 90.450 mg/L 11385

EG020F: Dissolved Metals by ICP-MS (QCLot: 991313)

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 83.90.5 mg/L 11680

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 92.10.1 mg/L 11485

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 86.20.1 mg/L 11084

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 89.20.1 mg/L 11185

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 86.70.1 mg/L 11181

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 84.20.1 mg/L 11183

EG020A-F: Manganese 7439-96-5 0.001 mg/L <0.001 84.80.1 mg/L 11082

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 86.80.1 mg/L 11282

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 85.50.1 mg/L 11781

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 87.00.5 mg/L 11282

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 -------- --------

EG020F: Dissolved Metals by ICP-MS (QCLot: 991316)

EG020A-F: Aluminium 7429-90-5 0.01 mg/L <0.01 88.10.5 mg/L 11680

EG020A-F: Arsenic 7440-38-2 0.001 mg/L <0.001 85.80.1 mg/L 11485

EG020A-F: Cadmium 7440-43-9 0.0001 mg/L <0.0001 84.40.1 mg/L 11084

EG020A-F: Chromium 7440-47-3 0.001 mg/L <0.001 85.20.1 mg/L 11185

EG020A-F: Copper 7440-50-8 0.001 mg/L <0.001 84.50.1 mg/L 11181

EG020A-F: Lead 7439-92-1 0.001 mg/L <0.001 86.70.1 mg/L 11183

EG020A-F: Manganese 7439-96-5 0.001 mg/L <0.001 87.40.1 mg/L 11082

EG020A-F: Nickel 7440-02-0 0.001 mg/L <0.001 84.00.1 mg/L 11282

EG020A-F: Zinc 7440-66-6 0.005 mg/L <0.005 82.40.1 mg/L 11781

EG020A-F: Iron 7439-89-6 0.05 mg/L <0.05 84.00.5 mg/L 11282

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EG020F: Dissolved Metals by ICP-MS (QCLot: 991316) - continued

EG020A-F: Bromine 7726-95-6 0.1 mg/L <0.1 -------- --------

EG035F: Dissolved Mercury by FIMS (QCLot: 991314)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 97.80.01 mg/L 10583

EG035F: Dissolved Mercury by FIMS (QCLot: 991317)

EG035F: Mercury 7439-97-6 0.0001 mg/L <0.0001 97.90.01 mg/L 10583

EK040P: Fluoride by PC Titrator (QCLot: 987910)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1105 mg/L 11682

EK040P: Fluoride by PC Titrator (QCLot: 987912)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1145 mg/L 11682

EK040P: Fluoride by PC Titrator (QCLot: 988504)

EK040P: Fluoride 16984-48-8 0.1 mg/L <0.1 1085 mg/L 11682

EK055G: Ammonia as N by Discrete Analyser (QCLot: 985831)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L <0.01 1001 mg/L 11490

EK055G: Ammonia as N by Discrete Analyser (QCLot: 985833)

EK055G: Ammonia as N 7664-41-7 0.01 mg/L <0.01 1021 mg/L 11490

EK057G: Nitrite as N by Discrete Analyser (QCLot: 985226)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 1110.5 mg/L 11482

EK057G: Nitrite as N by Discrete Analyser (QCLot: 985230)

EK057G: Nitrite as N 14797-65-0 0.01 mg/L <0.01 1130.5 mg/L 11482

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 985830)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L <0.01 1070.5 mg/L 11391

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 985832)

EK059G: Nitrite + Nitrate as N ---- 0.01 mg/L <0.01 99.50.5 mg/L 11391

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985223)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 97.30.5 mg/L 11785

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985229)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 99.60.5 mg/L 11785

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985233)

EK071G: Reactive Phosphorus as P 14265-44-2 0.01 mg/L <0.01 99.10.5 mg/L 11785

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 987304)

EP074: Styrene 100-42-5 5 µg/L <5 98.610 µg/L 11973

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 97.610 µg/L 11876

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 87.410 µg/L 11969

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 94.310 µg/L 11674

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 93.110 µg/L 11973

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 92.810 µg/L 11674

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 987304) - continued

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 93.910 µg/L 11672

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 92.610 µg/L 11971

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 84.310 µg/L 12365

EP074A: Monocyclic Aromatic Hydrocarbons (QCLot: 987321)

EP074: Styrene 100-42-5 5 µg/L <5 94.110 µg/L 11973

EP074: Isopropylbenzene 98-82-8 5 µg/L <5 97.910 µg/L 11876

EP074: n-Propylbenzene 103-65-1 5 µg/L <5 97.710 µg/L 11969

EP074: 1.3.5-Trimethylbenzene 108-67-8 5 µg/L <5 10410 µg/L 11674

EP074: sec-Butylbenzene 135-98-8 5 µg/L <5 95.910 µg/L 11973

EP074: 1.2.4-Trimethylbenzene 95-63-6 5 µg/L <5 10610 µg/L 11674

EP074: tert-Butylbenzene 98-06-6 5 µg/L <5 96.710 µg/L 11672

EP074: p-Isopropyltoluene 99-87-6 5 µg/L <5 97.910 µg/L 11971

EP074: n-Butylbenzene 104-51-8 5 µg/L <5 10510 µg/L 12365

EP074B: Oxygenated Compounds (QCLot: 987304)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 98.0100 µg/L 13461

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 81.4100 µg/L 13074

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 93.4100 µg/L 13266

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 84.4100 µg/L 13765

EP074B: Oxygenated Compounds (QCLot: 987321)

EP074: Vinyl Acetate 108-05-4 50 µg/L <50 88.1100 µg/L 13461

EP074: 2-Butanone (MEK) 78-93-3 50 µg/L <50 91.3100 µg/L 13074

EP074: 4-Methyl-2-pentanone (MIBK) 108-10-1 50 µg/L <50 95.5100 µg/L 13266

EP074: 2-Hexanone (MBK) 591-78-6 50 µg/L <50 90.9100 µg/L 13765

EP074C: Sulfonated Compounds (QCLot: 987304)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 10710 µg/L 12773

EP074C: Sulfonated Compounds (QCLot: 987321)

EP074: Carbon disulfide 75-15-0 5 µg/L <5 10510 µg/L 12773

EP074D: Fumigants (QCLot: 987304)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 10310 µg/L 12268

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 92.010 µg/L 11876

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 91.910 µg/L 12062

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 96.910 µg/L 11460

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 10310 µg/L 11769

EP074D: Fumigants (QCLot: 987321)

EP074: 2.2-Dichloropropane 594-20-7 5 µg/L <5 10110 µg/L 12268

EP074: 1.2-Dichloropropane 78-87-5 5 µg/L <5 10010 µg/L 11876

EP074: cis-1.3-Dichloropropylene 10061-01-5 5 µg/L <5 92.410 µg/L 12062

EP074: trans-1.3-Dichloropropylene 10061-02-6 5 µg/L <5 96.010 µg/L 11460

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074D: Fumigants (QCLot: 987321) - continued

EP074: 1.2-Dibromoethane (EDB) 106-93-4 5 µg/L <5 95.510 µg/L 11769

EP074E: Halogenated Aliphatic Compounds (QCLot: 987304)

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 73.6100 µg/L 13861

EP074: Chloromethane 74-87-3 50 µg/L <50 91.1100 µg/L 13067

EP074: Vinyl chloride 75-01-4 50 µg/L <50 120100 µg/L 12969

EP074: Bromomethane 74-83-9 50 µg/L <50 117100 µg/L 14056

EP074: Chloroethane 75-00-3 50 µg/L <50 103100 µg/L 13961

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 108100 µg/L 13169

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 10110 µg/L 12470

EP074: Iodomethane 74-88-4 5 µg/L <5 10010 µg/L 12870

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 99.910 µg/L 11874

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 99.610 µg/L 12074

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 10210 µg/L 11977

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 10810 µg/L 11967

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 93.810 µg/L 11973

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 10010 µg/L 12062

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 10110 µg/L 12373

EP074: Trichloroethene 79-01-6 5 µg/L <5 10110 µg/L 11876

EP074: Dibromomethane 74-95-3 5 µg/L <5 10410 µg/L 11973

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 97.610 µg/L 12672

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 10010 µg/L 12971

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 10410 µg/L 12472

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 10110 µg/L 11466

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 87.410 µg/L 12060

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 84.910 µg/L 12871

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 10210 µg/L 12470

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 10810 µg/L 12674

EP074: Pentachloroethane 76-01-7 5 µg/L <5 98.710 µg/L 12672

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 98.910 µg/L 13666

EP074E: Halogenated Aliphatic Compounds (QCLot: 987321)

EP074: Dichlorodifluoromethane 75-71-8 50 µg/L <50 124100 µg/L 13861

EP074: Chloromethane 74-87-3 50 µg/L <50 119100 µg/L 13067

EP074: Vinyl chloride 75-01-4 50 µg/L <50 121100 µg/L 12969

EP074: Bromomethane 74-83-9 50 µg/L <50 109100 µg/L 14056

EP074: Chloroethane 75-00-3 50 µg/L <50 109100 µg/L 13961

EP074: Trichlorofluoromethane 75-69-4 50 µg/L <50 108100 µg/L 13169

EP074: 1.1-Dichloroethene 75-35-4 5 µg/L <5 10810 µg/L 12470

EP074: Iodomethane 74-88-4 5 µg/L <5 94.910 µg/L 12870

EP074: trans-1.2-Dichloroethene 156-60-5 5 µg/L <5 10310 µg/L 11874

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074E: Halogenated Aliphatic Compounds (QCLot: 987321) - continued

EP074: 1.1-Dichloroethane 75-34-3 5 µg/L <5 10010 µg/L 12074

EP074: cis-1.2-Dichloroethene 156-59-2 5 µg/L <5 10210 µg/L 11977

EP074: 1.1.1-Trichloroethane 71-55-6 5 µg/L <5 98.710 µg/L 11967

EP074: 1.1-Dichloropropylene 563-58-6 5 µg/L <5 10210 µg/L 11973

EP074: Carbon Tetrachloride 56-23-5 5 µg/L <5 10210 µg/L 12062

EP074: 1.2-Dichloroethane 107-06-2 5 µg/L <5 99.410 µg/L 12373

EP074: Trichloroethene 79-01-6 5 µg/L <5 10010 µg/L 11876

EP074: Dibromomethane 74-95-3 5 µg/L <5 97.210 µg/L 11973

EP074: 1.1.2-Trichloroethane 79-00-5 5 µg/L <5 98.610 µg/L 12672

EP074: 1.3-Dichloropropane 142-28-9 5 µg/L <5 94.410 µg/L 12971

EP074: Tetrachloroethene 127-18-4 5 µg/L <5 10310 µg/L 12472

EP074: 1.1.1.2-Tetrachloroethane 630-20-6 5 µg/L <5 98.110 µg/L 11466

EP074: trans-1.4-Dichloro-2-butene 110-57-6 5 µg/L <5 87.810 µg/L 12060

EP074: cis-1.4-Dichloro-2-butene 1476-11-5 5 µg/L <5 10310 µg/L 12871

EP074: 1.1.2.2-Tetrachloroethane 79-34-5 5 µg/L <5 96.810 µg/L 12470

EP074: 1.2.3-Trichloropropane 96-18-4 5 µg/L <5 95.310 µg/L 12674

EP074: Pentachloroethane 76-01-7 5 µg/L <5 98.710 µg/L 12672

EP074: 1.2-Dibromo-3-chloropropane 96-12-8 5 µg/L <5 94.310 µg/L 13666

EP074F: Halogenated Aromatic Compounds (QCLot: 987304)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 10010 µg/L 11779

EP074: Bromobenzene 108-86-1 5 µg/L <5 96.010 µg/L 11676

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 96.910 µg/L 11973

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 92.510 µg/L 11973

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 10210 µg/L 12367

EP074F: Halogenated Aromatic Compounds (QCLot: 987321)

EP074: Chlorobenzene 108-90-7 5 µg/L <5 10110 µg/L 11779

EP074: Bromobenzene 108-86-1 5 µg/L <5 97.010 µg/L 11676

EP074: 2-Chlorotoluene 95-49-8 5 µg/L <5 99.210 µg/L 11973

EP074: 4-Chlorotoluene 106-43-4 5 µg/L <5 98.110 µg/L 11973

EP074: 1.2.3-Trichlorobenzene 87-61-6 5 µg/L <5 10110 µg/L 12367

EP074G: Trihalomethanes (QCLot: 987304)

EP074: Chloroform 67-66-3 5 µg/L <5 10510 µg/L 12072

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 96.810 µg/L 11864

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 10310 µg/L 11565

EP074: Bromoform 75-25-2 5 µg/L <5 11510 µg/L 12674

EP074G: Trihalomethanes (QCLot: 987321)

EP074: Chloroform 67-66-3 5 µg/L <5 10110 µg/L 12072

EP074: Bromodichloromethane 75-27-4 5 µg/L <5 98.210 µg/L 11864

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP074G: Trihalomethanes (QCLot: 987321) - continued

EP074: Dibromochloromethane 124-48-1 5 µg/L <5 95.310 µg/L 11565

EP074: Bromoform 75-25-2 5 µg/L <5 96.010 µg/L 12674

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 984025)

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 60.65 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 71.25 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 65.55 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 70.55 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 80.85 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 77.65 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 67.85 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 74.35 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 75.05 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 66.05 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 74.95 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 71.65 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 66.05 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 66.25 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 66.75 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 67.85 µg/L 11859

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 984028)

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 52.65 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 64.95 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 64.75 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 68.05 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 84.65 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 81.25 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 84.25 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 84.05 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 75.05 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 66.65 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 78.65 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 76.85 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 70.25 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 72.25 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 72.85 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 72.95 µg/L 11859

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 985848)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 985848) - continued

EP075(SIM): Naphthalene 91-20-3 1 µg/L <1.0 70.35 µg/L 9450

EP075(SIM): Acenaphthylene 208-96-8 1 µg/L <1.0 86.85 µg/L 11464

EP075(SIM): Acenaphthene 83-32-9 1 µg/L <1.0 80.75 µg/L 11362

EP075(SIM): Fluorene 86-73-7 1 µg/L <1.0 91.25 µg/L 11564

EP075(SIM): Phenanthrene 85-01-8 1 µg/L <1.0 70.35 µg/L 11663

EP075(SIM): Anthracene 120-12-7 1 µg/L <1.0 89.25 µg/L 11664

EP075(SIM): Fluoranthene 206-44-0 1 µg/L <1.0 84.65 µg/L 11864

EP075(SIM): Pyrene 129-00-0 1 µg/L <1.0 75.45 µg/L 11863

EP075(SIM): Benz(a)anthracene 56-55-3 1 µg/L <1.0 67.95 µg/L 11764

EP075(SIM): Chrysene 218-01-9 1 µg/L <1.0 73.45 µg/L 11663

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

1 µg/L <1.0 84.05 µg/L 11962

EP075(SIM): Benzo(k)fluoranthene 207-08-9 1 µg/L <1.0 93.25 µg/L 11563

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 µg/L <0.5 83.15 µg/L 11763

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 1 µg/L <1.0 77.85 µg/L 11860

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 1 µg/L <1.0 75.65 µg/L 11761

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 1 µg/L <1.0 70.45 µg/L 11859

EP075A: Phenolic Compounds (QCLot: 984024)

EP075: Phenol 108-95-2 2 µg/L <2 34.85 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 64.85 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 57.05 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 58.010 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 72.05 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 56.65 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 76.25 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 74.75 µg/L 10862

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 72.05 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 73.95 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 77.25 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 77.810 µg/L 9513

EP075A: Phenolic Compounds (QCLot: 984027)

EP075: Phenol 108-95-2 2 µg/L <2 41.25 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 73.85 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 53.55 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 57.910 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 68.25 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 69.25 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 72.05 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 70.15 µg/L 10862

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075A: Phenolic Compounds (QCLot: 984027) - continued

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 80.55 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 83.45 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 89.55 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 84.410 µg/L 9513

EP075A: Phenolic Compounds (QCLot: 985847)

EP075: Phenol 108-95-2 2 µg/L <2 40.25 µg/L 6426

EP075: 2-Chlorophenol 95-57-8 2 µg/L <2 69.15 µg/L 8852

EP075: 2-Methylphenol 95-48-7 2 µg/L <2 64.45 µg/L 9450

EP075: 3- & 4-Methylphenol 1319-77-3 2 µg/L <2 62.410 µg/L 9645

EP075: 2-Nitrophenol 88-75-5 2 µg/L <2 87.95 µg/L 9848

EP075: 2.4-Dimethylphenol 105-67-9 2 µg/L <2 76.15 µg/L 9450

EP075: 2.4-Dichlorophenol 120-83-2 2 µg/L <2 86.95 µg/L 10962

EP075: 2.6-Dichlorophenol 87-65-0 2 µg/L <2 87.95 µg/L 10862

EP075: 4-Chloro-3-methylphenol 59-50-7 2 µg/L <2 80.95 µg/L 10761

EP075: 2.4.6-Trichlorophenol 88-06-2 2 µg/L <2 87.65 µg/L 11258

EP075: 2.4.5-Trichlorophenol 95-95-4 2 µg/L <2 88.25 µg/L 11058

EP075: Pentachlorophenol 87-86-5 4 µg/L <4 84.810 µg/L 9513

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 984024)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 71.35 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 72.15 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 85.55 µg/L 11060

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 80.05 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 81.55 µg/L 11060

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 984027)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 63.45 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 65.45 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 94.25 µg/L 11060

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 95.55 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 94.85 µg/L 11060

EP075B: Polynuclear Aromatic Hydrocarbons (QCLot: 985847)

EP075: 2-Methylnaphthalene 91-57-6 2 µg/L <2 86.35 µg/L 10859

EP075: 2-Chloronaphthalene 91-58-7 2 µg/L <2 86.55 µg/L 10661

EP075: N-2-Fluorenyl Acetamide 53-96-3 2 µg/L <2 95.05 µg/L 11060

EP075: 7.12-Dimethylbenz(a)anthracene 57-97-6 2 µg/L <2 88.35 µg/L 10850

EP075: 3-Methylcholanthrene 56-49-5 2 µg/L <2 87.85 µg/L 11060

EP075C: Phthalate Esters (QCLot: 984024)

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 80.85 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 85.05 µg/L 11167

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075C: Phthalate Esters (QCLot: 984024) - continued

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 84.85 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 83.75 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 88.45 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 84.45 µg/L 11562

EP075C: Phthalate Esters (QCLot: 984027)

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 93.45 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 99.25 µg/L 11167

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 1045 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 99.85 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 1095 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 98.05 µg/L 11562

EP075C: Phthalate Esters (QCLot: 985847)

EP075: Dimethyl phthalate 131-11-3 2 µg/L <2 91.65 µg/L 11264

EP075: Diethyl phthalate 84-66-2 2 µg/L <2 86.15 µg/L 11167

EP075: Di-n-butyl phthalate 84-74-2 2 µg/L <2 94.75 µg/L 12268

EP075: Butyl benzyl phthalate 85-68-7 2 µg/L <2 90.05 µg/L 11461

EP075: bis(2-ethylhexyl) phthalate 117-81-7 ---- µg/L ---- 1015 µg/L 13260

EP075: Di-n-octylphthalate 117-84-0 2 µg/L <2 91.05 µg/L 11562

EP075D: Nitrosamines (QCLot: 984024)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 49.05 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 69.05 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 62.05 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 60.65 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 74.95 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 73.85 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 78.75 µg/L 10863

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 81.810 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 33.75 µg/L 12523

EP075D: Nitrosamines (QCLot: 984027)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 57.25 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 66.05 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 56.95 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 60.25 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 70.65 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 70.65 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 86.05 µg/L 10863

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075D: Nitrosamines (QCLot: 984027) - continued

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 93.310 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 52.65 µg/L 12523

EP075D: Nitrosamines (QCLot: 985847)

EP075: N-Nitrosomethylethylamine 10595-95-6 2 µg/L <2 57.65 µg/L 11046

EP075: N-Nitrosodiethylamine 55-18-5 2 µg/L <2 66.45 µg/L 11361

EP075: N-Nitrosopyrrolidine 930-55-2 4 µg/L <4 62.85 µg/L 9145

EP075: N-Nitrosomorpholine 59-89-2 2 µg/L <2 58.05 µg/L 10042

EP075: N-Nitrosodi-n-propylamine 621-64-7 2 µg/L <2 81.65 µg/L 10864

EP075: N-Nitrosopiperidine 100-75-4 2 µg/L <2 86.25 µg/L 10762

EP075: N-Nitrosodibutylamine 924-16-3 2 µg/L <2 91.35 µg/L 10863

EP075: N-Nitrosodiphenyl & Diphenylamine 86-30-6

122-39-4

4 µg/L <4 88.110 µg/L 11265

EP075: Methapyrilene 91-80-5 2 µg/L <2 35.75 µg/L 12523

EP075E: Nitroaromatics and Ketones (QCLot: 984024)

EP075: 2-Picoline 109-06-8 2 µg/L <2 45.95 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 71.45 µg/L 11268

EP075: Nitrobenzene 98-95-3 2 µg/L <2 73.15 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 79.75 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 80.45 µg/L 11364

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 82.75 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 82.35 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 90.55 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 80.65 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 82.55 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 80.85 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 84.55 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 93.15 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 80.15 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 84.05 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 85.05 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 88.45 µg/L 11058

EP075E: Nitroaromatics and Ketones (QCLot: 984027)

EP075: 2-Picoline 109-06-8 2 µg/L <2 # 39.95 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 70.65 µg/L 11268

EP075: Nitrobenzene 98-95-3 2 µg/L <2 71.15 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 78.85 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 92.55 µg/L 11364

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ES1716700

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075E: Nitroaromatics and Ketones (QCLot: 984027) - continued

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 94.25 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 76.15 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 75.95 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 85.85 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 87.25 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 91.25 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 85.85 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 # 57.75 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 98.05 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 99.65 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 98.55 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 1045 µg/L 11058

EP075E: Nitroaromatics and Ketones (QCLot: 985847)

EP075: 2-Picoline 109-06-8 2 µg/L <2 # 33.85 µg/L 10941

EP075: Acetophenone 98-86-2 2 µg/L <2 82.35 µg/L 11268

EP075: Nitrobenzene 98-95-3 2 µg/L <2 74.05 µg/L 11268

EP075: Isophorone 78-59-1 2 µg/L <2 81.15 µg/L 11168

EP075: 2.6-Dinitrotoluene 606-20-2 4 µg/L <4 96.15 µg/L 11364

EP075: 2.4-Dinitrotoluene 121-14-2 4 µg/L <4 89.65 µg/L 10960

EP075: 1-Naphthylamine 134-32-7 2 µg/L <2 93.15 µg/L 10247

EP075: 4-Nitroquinoline-N-oxide 56-57-5 2 µg/L <2 # 1055 µg/L 9640

EP075: 5-Nitro-o-toluidine 99-55-8 2 µg/L <2 92.25 µg/L 10658

EP075: Azobenzene 103-33-3 2 µg/L <2 84.75 µg/L 11266

EP075: 1.3.5-Trinitrobenzene 99-35-4 2 µg/L <2 84.85 µg/L 10846

EP075: Phenacetin 62-44-2 2 µg/L <2 83.75 µg/L 10158

EP075: 4-Aminobiphenyl 92-67-1 2 µg/L <2 90.25 µg/L 11260

EP075: Pentachloronitrobenzene 82-68-8 2 µg/L <2 83.15 µg/L 10959

EP075: Pronamide 23950-58-5 2 µg/L <2 90.65 µg/L 10963

EP075: Dimethylaminoazobenzene 60-11-7 2 µg/L <2 91.65 µg/L 10859

EP075: Chlorobenzilate 510-15-6 2 µg/L <2 93.25 µg/L 11058

EP075F: Haloethers (QCLot: 984024)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 70.05 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 70.95 µg/L 11166

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 77.65 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 80.75 µg/L 10862

EP075F: Haloethers (QCLot: 984027)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 69.55 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 70.85 µg/L 11166

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ES1716700

AECOM Australia Pty Ltd

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075F: Haloethers (QCLot: 984027) - continued

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 79.45 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 88.55 µg/L 10862

EP075F: Haloethers (QCLot: 985847)

EP075: Bis(2-chloroethyl) ether 111-44-4 2 µg/L <2 75.15 µg/L 11269

EP075: Bis(2-chloroethoxy) methane 111-91-1 2 µg/L <2 83.35 µg/L 11166

EP075: 4-Chlorophenyl phenyl ether 7005-72-3 2 µg/L <2 88.65 µg/L 10965

EP075: 4-Bromophenyl phenyl ether 101-55-3 2 µg/L <2 86.55 µg/L 10862

EP075G: Chlorinated Hydrocarbons (QCLot: 984024)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 67.25 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 65.35 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 66.05 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 68.55 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 73.15 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 68.05 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 69.75 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 69.15 µg/L 10724

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 78.05 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 80.85 µg/L 11066

EP075G: Chlorinated Hydrocarbons (QCLot: 984027)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 50.05 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 50.35 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 49.85 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 49.25 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 52.85 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 52.05 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 55.55 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 42.85 µg/L 10724

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 71.55 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 87.55 µg/L 11066

EP075G: Chlorinated Hydrocarbons (QCLot: 985847)

EP075: 1.4-Dichlorobenzene 106-46-7 2 µg/L <2 76.35 µg/L 9741

EP075: 1.3-Dichlorobenzene 541-73-1 2 µg/L <2 74.05 µg/L 9640

EP075: 1.2-Dichlorobenzene 95-50-1 2 µg/L <2 72.35 µg/L 9541

EP075: Hexachloroethane 67-72-1 2 µg/L <2 76.25 µg/L 8846

EP075: 1.2.4-Trichlorobenzene 120-82-1 2 µg/L <2 81.25 µg/L 9646

EP075: Hexachloropropylene 1888-71-7 2 µg/L <2 75.15 µg/L 9634

EP075: Hexachlorobutadiene 87-68-3 2 µg/L <2 74.15 µg/L 10037

EP075: Hexachlorocyclopentadiene 77-47-4 10 µg/L <10 81.75 µg/L 10724

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AECOM Australia Pty Ltd

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075G: Chlorinated Hydrocarbons (QCLot: 985847) - continued

EP075: Pentachlorobenzene 608-93-5 2 µg/L <2 83.65 µg/L 10765

EP075: Hexachlorobenzene (HCB) 118-74-1 4 µg/L <4 84.85 µg/L 11066

EP075H: Anilines and Benzidines (QCLot: 984024)

EP075: Aniline 62-53-3 2 µg/L <2 66.95 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 70.25 µg/L 10642

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 80.45 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 82.05 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 78.45 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 85.35 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 89.15 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 1075 µg/L 11960

EP075H: Anilines and Benzidines (QCLot: 984027)

EP075: Aniline 62-53-3 2 µg/L <2 62.35 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 71.35 µg/L 10642

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 87.35 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 85.45 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 75.45 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 82.75 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 94.65 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 91.15 µg/L 11960

EP075H: Anilines and Benzidines (QCLot: 985847)

EP075: Aniline 62-53-3 2 µg/L <2 72.95 µg/L 10450

EP075: 4-Chloroaniline 106-47-8 2 µg/L <2 84.65 µg/L 10642

EP075: 2-Nitroaniline 88-74-4 4 µg/L <4 90.75 µg/L 11061

EP075: 3-Nitroaniline 99-09-2 4 µg/L <4 87.65 µg/L 9752

EP075: Dibenzofuran 132-64-9 2 µg/L <2 86.45 µg/L 10865

EP075: 4-Nitroaniline 100-01-6 2 µg/L <2 88.25 µg/L 10049

EP075: Carbazole 86-74-8 2 µg/L <2 94.95 µg/L 10764

EP075: 3.3`-Dichlorobenzidine 91-94-1 2 µg/L <2 1115 µg/L 11960

EP075I: Organochlorine Pesticides (QCLot: 984024)

EP075: alpha-BHC 319-84-6 2 µg/L <2 79.15 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 84.05 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 83.05 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 81.85 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 82.45 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 84.25 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 84.35 µg/L 11850

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 84.35 µg/L 11159

Page 449: Appendix - Department of Defence

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075I: Organochlorine Pesticides (QCLot: 984024) - continued

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 80.05 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 85.85 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 89.35 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 84.25 µg/L 11654

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 85.65 µg/L 11555

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 88.15 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 86.85 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075I: Organochlorine Pesticides (QCLot: 984027)

EP075: alpha-BHC 319-84-6 2 µg/L <2 94.45 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 98.95 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 98.25 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 96.65 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 99.95 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 1005 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 1065 µg/L 11850

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 1025 µg/L 11159

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 93.95 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 1045 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 1045 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 1055 µg/L 11654

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 1045 µg/L 11555

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 1085 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 96.35 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075I: Organochlorine Pesticides (QCLot: 985847)

EP075: alpha-BHC 319-84-6 2 µg/L <2 86.05 µg/L 11064

EP075: beta-BHC 319-85-7 2 µg/L <2 85.25 µg/L 10753

EP075: gamma-BHC 58-89-9 2 µg/L <2 87.15 µg/L 11151

EP075: delta-BHC 319-86-8 2 µg/L <2 87.45 µg/L 11157

EP075: Heptachlor 76-44-8 2 µg/L <2 88.25 µg/L 10858

EP075: Aldrin 309-00-2 2 µg/L <2 88.05 µg/L 11256

EP075: Heptachlor epoxide 1024-57-3 2 µg/L <2 87.15 µg/L 11850

Page 450: Appendix - Department of Defence

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AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075I: Organochlorine Pesticides (QCLot: 985847) - continued

EP075: alpha-Endosulfan 959-98-8 2 µg/L <2 87.25 µg/L 11159

EP075: 4.4`-DDE 72-55-9 2 µg/L <2 85.65 µg/L 11553

EP075: Dieldrin 60-57-1 2 µg/L <2 88.35 µg/L 11559

EP075: Endrin 72-20-8 2 µg/L <2 88.25 µg/L 11458

EP075: beta-Endosulfan 33213-65-9 2 µg/L <2 82.95 µg/L 11654

EP075: 4.4`-DDD 72-54-8 2 µg/L <2 90.05 µg/L 11555

EP075: Endosulfan sulfate 1031-07-8 2 µg/L <2 90.95 µg/L 11453

EP075: 4.4`-DDT 50-29-3 4 µg/L <4 89.45 µg/L 11456

EP075: Sum of Aldrin + Dieldrin 309-00-2/60-

57-1

4 µg/L <4 -------- --------

EP075: Sum of DDD + DDE + DDT 72-54-8/72-5

5-9/50-2

4 µg/L <4 -------- --------

EP075J: Organophosphorus Pesticides (QCLot: 984024)

EP075: Dichlorvos 62-73-7 2 µg/L <2 80.75 µg/L 11351

EP075: Dimethoate 60-51-5 2 µg/L <2 84.85 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 89.15 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 86.85 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 1025 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 85.05 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 81.75 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 82.75 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 75.95 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 85.35 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 86.85 µg/L 11751

EP075J: Organophosphorus Pesticides (QCLot: 984027)

EP075: Dichlorvos 62-73-7 2 µg/L <2 91.45 µg/L 11351

EP075: Dimethoate 60-51-5 2 µg/L <2 89.45 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 1025 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 1045 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 1015 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 1085 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 1025 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 1025 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 91.05 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 1005 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 1075 µg/L 11751

EP075J: Organophosphorus Pesticides (QCLot: 985847)

EP075: Dichlorvos 62-73-7 2 µg/L <2 93.25 µg/L 11351

Page 451: Appendix - Department of Defence

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AECOM Australia Pty Ltd

60547028, task 3.1:Project

Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP075J: Organophosphorus Pesticides (QCLot: 985847) - continued

EP075: Dimethoate 60-51-5 2 µg/L <2 84.65 µg/L 10943

EP075: Diazinon 333-41-5 2 µg/L <2 87.65 µg/L 11349

EP075: Chlorpyrifos-methyl 5598-13-0 2 µg/L <2 91.25 µg/L 11654

EP075: Malathion 121-75-5 2 µg/L <2 1115 µg/L 12454

EP075: Fenthion 55-38-9 2 µg/L <2 92.85 µg/L 11557

EP075: Chlorpyrifos 2921-88-2 2 µg/L <2 86.75 µg/L 10953

EP075: Pirimphos-ethyl 23505-41-1 2 µg/L <2 88.65 µg/L 11155

EP075: Chlorfenvinphos 470-90-6 2 µg/L <2 87.85 µg/L 11650

EP075: Prothiofos 34643-46-4 2 µg/L <2 86.65 µg/L 11854

EP075: Ethion 563-12-2 2 µg/L <2 89.75 µg/L 11751

EP080/071: Total Petroleum Hydrocarbons (QCLot: 984026)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 86.72000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 91.43000 µg/L 10983

EP071: C29 - C36 Fraction ---- 50 µg/L <50 92.42000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 984029)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 86.32000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 90.33000 µg/L 10983

EP071: C29 - C36 Fraction ---- 50 µg/L <50 90.02000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 985849)

EP071: C10 - C14 Fraction ---- 50 µg/L <50 93.92000 µg/L 11676

EP071: C15 - C28 Fraction ---- 100 µg/L <100 89.43000 µg/L 10983

EP071: C29 - C36 Fraction ---- 50 µg/L <50 88.42000 µg/L 11375

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987303)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 100260 µg/L 12775

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987322)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 102260 µg/L 12775

EP080/071: Total Petroleum Hydrocarbons (QCLot: 990407)

EP080: C6 - C9 Fraction ---- 20 µg/L <20 86.2260 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 984026)

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 85.82500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 93.73500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 87.91500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 984029)

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 85.22500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 92.13500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 94.51500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 985849)

Page 452: Appendix - Department of Defence

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 985849) - continued

EP071: >C10 - C16 Fraction ---- 100 µg/L <100 90.02500 µg/L 11476

EP071: >C16 - C34 Fraction ---- 100 µg/L <100 89.53500 µg/L 11181

EP071: >C34 - C40 Fraction ---- 100 µg/L <100 91.61500 µg/L 11977

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987303)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 103310 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987322)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 104310 µg/L 12775

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 990407)

EP080: C6 - C10 Fraction C6_C10 20 µg/L <20 88.1310 µg/L 12775

EP080: BTEXN (QCLot: 987303)

EP080: Benzene 71-43-2 1 µg/L <1 89.910 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 96.810 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 92.010 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 92.710 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 92.510 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 98.310 µg/L 12070

EP080: BTEXN (QCLot: 987322)

EP080: Benzene 71-43-2 1 µg/L <1 10810 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 10310 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 10010 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 99.510 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 96.910 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 89.510 µg/L 12070

EP080: BTEXN (QCLot: 990407)

EP080: Benzene 71-43-2 1 µg/L <1 91.910 µg/L 12270

EP080: Toluene 108-88-3 2 µg/L <2 93.910 µg/L 12369

EP080: Ethylbenzene 100-41-4 2 µg/L <2 88.610 µg/L 12070

EP080: meta- & para-Xylene 108-38-3

106-42-3

2 µg/L <2 86.810 µg/L 12169

EP080: ortho-Xylene 95-47-6 2 µg/L <2 91.010 µg/L 12272

EP080: Naphthalene 91-20-3 5 µg/L <5 10710 µg/L 12070

EP116: 1.4-Dioxane (QCLot: 987038)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 10810 µg/L 11979

EP116: 1.4-Dioxane (QCLot: 989615)

EP116: 1.4-Dioxane 123-91-1 0.5 µg/L <0.5 99.610 µg/L 11979

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984238)

Page 453: Appendix - Department of Defence

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984238) - continued

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 1230.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1230.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1260.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 1290.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1260.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 1260.5 µg/L 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984239)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 96.20.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 1250.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 1240.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 1290.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 92.60.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 1180.5 µg/L 13070

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 986813)

EP231X: Perfluorobutane sulfonic acid (PFBS) 375-73-5 0.02 µg/L <0.02 94.60.5 µg/L 13070

EP231X: Perfluoropentane sulfonic acid (PFPeS) 2706-91-4 0.02 µg/L <0.02 89.60.5 µg/L 13070

EP231X: Perfluorohexane sulfonic acid (PFHxS) 355-46-4 0.02 µg/L <0.02 90.60.5 µg/L 13070

EP231X: Perfluoroheptane sulfonic acid (PFHpS) 375-92-8 0.02 µg/L <0.02 91.60.5 µg/L 13070

EP231X: Perfluorooctane sulfonic acid (PFOS) 1763-23-1 0.01 µg/L <0.01 1080.5 µg/L 13070

EP231X: Perfluorodecane sulfonic acid (PFDS) 335-77-3 0.02 µg/L <0.02 1080.5 µg/L 13070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984238)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 96.42.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 82.40.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1280.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1190.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1270.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 1260.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 1290.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1150.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1280.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 1190.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 1121.25 µg/L 15070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984239)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 1172.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 1100.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 1170.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 1070.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 1280.5 µg/L 13070

Page 454: Appendix - Department of Defence

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Sub-Matrix: WATER Method Blank (MB)

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Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984239) - continued

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 95.20.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 80.00.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1040.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 97.40.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 89.60.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 98.41.25 µg/L 15070

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 986813)

EP231X: Perfluorobutanoic acid (PFBA) 375-22-4 0.1 µg/L <0.1 84.62.5 µg/L 13070

EP231X: Perfluoropentanoic acid (PFPeA) 2706-90-3 0.02 µg/L <0.02 81.60.5 µg/L 13070

EP231X: Perfluorohexanoic acid (PFHxA) 307-24-4 0.02 µg/L <0.02 93.40.5 µg/L 13070

EP231X: Perfluoroheptanoic acid (PFHpA) 375-85-9 0.02 µg/L <0.02 96.20.5 µg/L 13070

EP231X: Perfluorooctanoic acid (PFOA) 335-67-1 0.01 µg/L <0.01 95.60.5 µg/L 13070

EP231X: Perfluorononanoic acid (PFNA) 375-95-1 0.02 µg/L <0.02 1090.5 µg/L 13070

EP231X: Perfluorodecanoic acid (PFDA) 335-76-2 0.02 µg/L <0.02 1180.5 µg/L 13070

EP231X: Perfluoroundecanoic acid (PFUnDA) 2058-94-8 0.02 µg/L <0.02 1150.5 µg/L 13070

EP231X: Perfluorododecanoic acid (PFDoDA) 307-55-1 0.02 µg/L <0.02 1000.5 µg/L 13070

EP231X: Perfluorotridecanoic acid (PFTrDA) 72629-94-8 0.02 µg/L <0.02 1130.5 µg/L 13070

EP231X: Perfluorotetradecanoic acid (PFTeDA) 376-06-7 0.05 µg/L <0.05 1101.25 µg/L 15070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984238)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1270.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 1111.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 1171.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 89.71.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 1261.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1090.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 1130.5 µg/L 13070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984239)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 85.00.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 1081.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 1091.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 1201.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 89.01.25 µg/L 15070

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Sub-Matrix: WATER Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984239) - continued

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1060.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 1210.5 µg/L 13070

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 986813)

EP231X: Perfluorooctane sulfonamide (FOSA) 754-91-6 0.02 µg/L <0.02 1060.5 µg/L 13070

EP231X: N-Methyl perfluorooctane sulfonamide (MeFOSA) 31506-32-8 0.05 µg/L <0.05 94.51.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 4151-50-2 0.05 µg/L <0.05 90.71.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

2448-09-7 0.05 µg/L <0.05 1061.25 µg/L 15070

EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1691-99-2 0.05 µg/L <0.05 92.31.25 µg/L 15070

EP231X: N-Methyl perfluorooctane sulfonamidoacetic acid

(MeFOSAA)

2355-31-9 0.02 µg/L <0.02 1020.5 µg/L 13070

EP231X: N-Ethyl perfluorooctane sulfonamidoacetic acid

(EtFOSAA)

2991-50-6 0.02 µg/L <0.02 97.40.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984238)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 1230.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1260.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1270.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 1170.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984239)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 92.00.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1260.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 99.40.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 99.20.5 µg/L 13070

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 986813)

EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 757124-72-4 0.05 µg/L <0.05 96.40.5 µg/L 13070

EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 27619-97-2 0.05 µg/L <0.05 1010.5 µg/L 13070

EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 39108-34-4 0.05 µg/L <0.05 1110.5 µg/L 13070

EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 120226-60-0 0.05 µg/L <0.05 1040.5 µg/L 13070

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985225)

Anonymous ES1716586-001 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric 11810 mg/L 13070

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985228)

0902_MW45_060717 ES1716700-010 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric 84.310 mg/L 13070

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985232)

0902_MW52_060717 ES1716700-033 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric # Not

Determined

10 mg/L 13070

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA (QCLot: 985453)

Anonymous ES1716557-001 14808-79-8ED041G: Sulfate as SO4 - Turbidimetric 73.610 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 985224)

Anonymous ES1716586-001 16887-00-6ED045G: Chloride 106250 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 985227)

0902_MW45_060717 ES1716700-010 16887-00-6ED045G: Chloride 112250 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 985231)

0902_MW52_060717 ES1716700-033 16887-00-6ED045G: Chloride 102250 mg/L 13070

ED045G: Chloride by Discrete Analyser (QCLot: 985452)

Anonymous ES1716557-001 16887-00-6ED045G: Chloride 119250 mg/L 13070

EG020F: Dissolved Metals by ICP-MS (QCLot: 991313)

0902_MW60_050717 ES1716700-002 7440-38-2EG020A-F: Arsenic 1001 mg/L 13070

7440-43-9EG020A-F: Cadmium 94.30.25 mg/L 13070

7440-47-3EG020A-F: Chromium 98.21 mg/L 13070

7440-50-8EG020A-F: Copper 91.31 mg/L 13070

7439-92-1EG020A-F: Lead 93.41 mg/L 13070

7439-96-5EG020A-F: Manganese 91.31 mg/L 13070

7440-02-0EG020A-F: Nickel 94.01 mg/L 13070

7440-66-6EG020A-F: Zinc 94.81 mg/L 13070

EG020F: Dissolved Metals by ICP-MS (QCLot: 991316)

0902_MW65_040717 ES1716700-022 7440-38-2EG020A-F: Arsenic 75.91 mg/L 13070

7440-43-9EG020A-F: Cadmium 75.00.25 mg/L 13070

7440-47-3EG020A-F: Chromium 73.81 mg/L 13070

7440-50-8EG020A-F: Copper 71.61 mg/L 13070

7439-92-1EG020A-F: Lead 75.41 mg/L 13070

7439-96-5EG020A-F: Manganese # Not

Determined

1 mg/L 13070

7440-02-0EG020A-F: Nickel 73.41 mg/L 13070

7440-66-6EG020A-F: Zinc 76.81 mg/L 13070

EG035F: Dissolved Mercury by FIMS (QCLot: 991314)

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EG035F: Dissolved Mercury by FIMS (QCLot: 991314) - continued

0902_MW25_050717 ES1716700-003 7439-97-6EG035F: Mercury 95.20.01 mg/L 13070

EG035F: Dissolved Mercury by FIMS (QCLot: 991317)

0902_MW66_040717 ES1716700-023 7439-97-6EG035F: Mercury 97.80.01 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 987910)

Anonymous ES1716393-001 16984-48-8EK040P: Fluoride 95.45 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 987912)

0902_MW74_040717 ES1716700-020 16984-48-8EK040P: Fluoride 1055 mg/L 13070

EK040P: Fluoride by PC Titrator (QCLot: 988504)

Anonymous EN1702861-001 16984-48-8EK040P: Fluoride 95.25 mg/L 13070

EK055G: Ammonia as N by Discrete Analyser (QCLot: 985831)

0902_MW61_050717 ES1716700-001 7664-41-7EK055G: Ammonia as N 76.61 mg/L 13070

EK055G: Ammonia as N by Discrete Analyser (QCLot: 985833)

0902_MW66_040717 ES1716700-023 7664-41-7EK055G: Ammonia as N 1071 mg/L 13070

EK057G: Nitrite as N by Discrete Analyser (QCLot: 985226)

0902_MW45_060717 ES1716700-010 14797-65-0EK057G: Nitrite as N 1160.5 mg/L 13070

EK057G: Nitrite as N by Discrete Analyser (QCLot: 985230)

0902_MW52_060717 ES1716700-033 14797-65-0EK057G: Nitrite as N 1180.5 mg/L 13070

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 985830)

0902_MW61_050717 ES1716700-001 ----EK059G: Nitrite + Nitrate as N 1080.5 mg/L 13070

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser (QCLot: 985832)

0902_MW66_040717 ES1716700-023 ----EK059G: Nitrite + Nitrate as N 97.60.5 mg/L 13070

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985223)

Anonymous ES1716586-001 14265-44-2EK071G: Reactive Phosphorus as P 1080.5 mg/L 13070

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985229)

0902_MW45_060717 ES1716700-010 14265-44-2EK071G: Reactive Phosphorus as P 97.10.5 mg/L 13070

EK071G: Reactive Phosphorus as P by discrete analyser (QCLot: 985233)

0902_MW52_060717 ES1716700-033 14265-44-2EK071G: Reactive Phosphorus as P 1120.5 mg/L 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 987304)

0902_MW61_050717 ES1716700-001 75-35-4EP074: 1.1-Dichloroethene 73.225 µg/L 13070

79-01-6EP074: Trichloroethene 86.625 µg/L 13070

EP074E: Halogenated Aliphatic Compounds (QCLot: 987321)

0902_MW72_040717 ES1716700-021 75-35-4EP074: 1.1-Dichloroethene 72.325 µg/L 13070

79-01-6EP074: Trichloroethene 90.925 µg/L 13070

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP074F: Halogenated Aromatic Compounds (QCLot: 987304)

0902_MW61_050717 ES1716700-001 108-90-7EP074: Chlorobenzene 96.325 µg/L 13070

EP074F: Halogenated Aromatic Compounds (QCLot: 987321)

0902_MW72_040717 ES1716700-021 108-90-7EP074: Chlorobenzene 94.925 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987303)

0902_MW61_050717 ES1716700-001 ----EP080: C6 - C9 Fraction 113325 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 987322)

0902_MW72_040717 ES1716700-021 ----EP080: C6 - C9 Fraction 113325 µg/L 13070

EP080/071: Total Petroleum Hydrocarbons (QCLot: 990407)

Anonymous ES1716485-001 ----EP080: C6 - C9 Fraction 122325 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987303)

0902_MW61_050717 ES1716700-001 C6_C10EP080: C6 - C10 Fraction 112375 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 987322)

0902_MW72_040717 ES1716700-021 C6_C10EP080: C6 - C10 Fraction 110375 µg/L 13070

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 990407)

Anonymous ES1716485-001 C6_C10EP080: C6 - C10 Fraction 112375 µg/L 13070

EP080: BTEXN (QCLot: 987303)

0902_MW61_050717 ES1716700-001 71-43-2EP080: Benzene 94.825 µg/L 13070

108-88-3EP080: Toluene 96.025 µg/L 13070

100-41-4EP080: Ethylbenzene 95.925 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 96.025 µg/L 13070

95-47-6EP080: ortho-Xylene 97.625 µg/L 13070

91-20-3EP080: Naphthalene 94.225 µg/L 13070

EP080: BTEXN (QCLot: 987322)

0902_MW72_040717 ES1716700-021 71-43-2EP080: Benzene 10725 µg/L 13070

108-88-3EP080: Toluene 10125 µg/L 13070

100-41-4EP080: Ethylbenzene 10225 µg/L 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 99.825 µg/L 13070

95-47-6EP080: ortho-Xylene 99.825 µg/L 13070

91-20-3EP080: Naphthalene 93.525 µg/L 13070

EP080: BTEXN (QCLot: 990407)

Anonymous ES1716485-001 71-43-2EP080: Benzene 11925 µg/L 13070

108-88-3EP080: Toluene 11425 µg/L 13070

100-41-4EP080: Ethylbenzene 11425 µg/L 13070

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP080: BTEXN (QCLot: 990407) - continued

Anonymous ES1716485-001 108-38-3

106-42-3

EP080: meta- & para-Xylene 11025 µg/L 13070

95-47-6EP080: ortho-Xylene 11625 µg/L 13070

91-20-3EP080: Naphthalene 11025 µg/L 13070

EP116: 1.4-Dioxane (QCLot: 987038)

0902_MW60_050717 ES1716700-002 123-91-1EP116: 1.4-Dioxane 10510 µg/L 12080

EP116: 1.4-Dioxane (QCLot: 989615)

0902_MW65_040717 ES1716700-022 123-91-1EP116: 1.4-Dioxane 98.710 µg/L 12080

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984238)

0902_MW61_050717 ES1716700-001 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 91.40.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 1270.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) 1160.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 1080.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) 1100.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1120.5 µg/L 13050

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 984239)

0902_MW72_040717 ES1716700-021 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) # Not

Determined

0.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) # Not

Determined

0.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) # Not

Determined

0.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) # Not

Determined

0.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 81.20.5 µg/L 13050

EP231A: Perfluoroalkyl Sulfonic Acids (QCLot: 986813)

0902_MW50_060717 ES1716700-040 375-73-5EP231X: Perfluorobutane sulfonic acid (PFBS) 1160.5 µg/L 13050

2706-91-4EP231X: Perfluoropentane sulfonic acid (PFPeS) 96.80.5 µg/L 13050

355-46-4EP231X: Perfluorohexane sulfonic acid (PFHxS) # Not

Determined

0.5 µg/L 13050

375-92-8EP231X: Perfluoroheptane sulfonic acid (PFHpS) 91.00.5 µg/L 13050

1763-23-1EP231X: Perfluorooctane sulfonic acid (PFOS) # Not

Determined

0.5 µg/L 13050

335-77-3EP231X: Perfluorodecane sulfonic acid (PFDS) 1050.5 µg/L 13050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984238)

0902_MW61_050717 ES1716700-001

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984238) - continued

0902_MW61_050717 ES1716700-001 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 61.92.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 84.00.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) 83.80.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 1260.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 1170.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 1030.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 1110.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 1040.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 1250.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1080.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 63.01.25 µg/L 15050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 984239)

0902_MW72_040717 ES1716700-021 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 97.52.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) # Not

Determined

0.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 52.20.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) # Not

Determined

0.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 71.00.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 65.80.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 77.20.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 74.40.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 57.20.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 67.91.25 µg/L 15050

EP231B: Perfluoroalkyl Carboxylic Acids (QCLot: 986813)

0902_MW50_060717 ES1716700-040 375-22-4EP231X: Perfluorobutanoic acid (PFBA) 1182.5 µg/L 13050

2706-90-3EP231X: Perfluoropentanoic acid (PFPeA) 94.20.5 µg/L 13050

307-24-4EP231X: Perfluorohexanoic acid (PFHxA) # Not

Determined

0.5 µg/L 13050

375-85-9EP231X: Perfluoroheptanoic acid (PFHpA) 86.60.5 µg/L 13050

335-67-1EP231X: Perfluorooctanoic acid (PFOA) 89.20.5 µg/L 13050

375-95-1EP231X: Perfluorononanoic acid (PFNA) 97.20.5 µg/L 13050

335-76-2EP231X: Perfluorodecanoic acid (PFDA) 1090.5 µg/L 13050

2058-94-8EP231X: Perfluoroundecanoic acid (PFUnDA) 1160.5 µg/L 13050

307-55-1EP231X: Perfluorododecanoic acid (PFDoDA) 96.80.5 µg/L 13050

72629-94-8EP231X: Perfluorotridecanoic acid (PFTrDA) 1020.5 µg/L 13050

376-06-7EP231X: Perfluorotetradecanoic acid (PFTeDA) 83.41.25 µg/L 15050

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984238)

0902_MW61_050717 ES1716700-001 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1020.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

1271.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 1141.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

1281.25 µg/L 15050

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

1241.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

67.60.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

70.00.5 µg/L 13050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 984239)

0902_MW72_040717 ES1716700-021 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 77.00.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

78.71.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 63.21.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

77.41.25 µg/L 15050

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

70.21.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

65.60.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

58.00.5 µg/L 13050

EP231C: Perfluoroalkyl Sulfonamides (QCLot: 986813)

0902_MW50_060717 ES1716700-040 754-91-6EP231X: Perfluorooctane sulfonamide (FOSA) 1170.5 µg/L 13050

31506-32-8EP231X: N-Methyl perfluorooctane sulfonamide

(MeFOSA)

1021.25 µg/L 15050

4151-50-2EP231X: N-Ethyl perfluorooctane sulfonamide (EtFOSA) 87.81.25 µg/L 15050

2448-09-7EP231X: N-Methyl perfluorooctane sulfonamidoethanol

(MeFOSE)

1141.25 µg/L 15050

1691-99-2EP231X: N-Ethyl perfluorooctane sulfonamidoethanol

(EtFOSE)

87.31.25 µg/L 15050

2355-31-9EP231X: N-Methyl perfluorooctane sulfonamidoacetic

acid (MeFOSAA)

99.00.5 µg/L 13050

2991-50-6EP231X: N-Ethyl perfluorooctane sulfonamidoacetic

acid (EtFOSAA)

95.00.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984238)

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Sub-Matrix: WATER Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984238) - continued

0902_MW61_050717 ES1716700-001 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 85.60.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 1060.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 92.40.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 75.60.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 984239)

0902_MW72_040717 ES1716700-021 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 82.20.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 85.80.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 88.40.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 80.00.5 µg/L 13050

EP231D: (n:2) Fluorotelomer Sulfonic Acids (QCLot: 986813)

0902_MW50_060717 ES1716700-040 757124-72-4EP231X: 4:2 Fluorotelomer sulfonic acid (4:2 FTS) 90.40.5 µg/L 13050

27619-97-2EP231X: 6:2 Fluorotelomer sulfonic acid (6:2 FTS) 99.80.5 µg/L 13050

39108-34-4EP231X: 8:2 Fluorotelomer sulfonic acid (8:2 FTS) 1030.5 µg/L 13050

120226-60-0EP231X: 10:2 Fluorotelomer sulfonic acid (10:2 FTS) 1210.5 µg/L 13050

Page 463: Appendix - Department of Defence

True

Environmental

QA/QC Compliance Assessment to assist with Quality ReviewWork Order : ES1716700 Page : 1 of 45

:: LaboratoryClient Environmental Division SydneyAECOM Australia Pty Ltd

:Contact MR CLAYTON COWPER Telephone : +61 2 8784 8503

:Project 60547028, task 3.1 Date Samples Received : 06-Jul-2017

Site : RAAF Richmond Issue Date : 17-Jul-2017

James Tomilson and Sebastian McDlay:Sampler No. of samples received : 40

:Order number 60547028 No. of samples analysed : 40

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l Laboratory Control outliers exist - please see following pages for full details.

l Matrix Spike outliers exist - please see following pages for full details.

l For all regular sample matrices, NO surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

l Analysis Holding Time Outliers exist - please see following pages for full details.

Outliers : Frequency of Quality Control Samples

l Quality Control Sample Frequency Outliers exist - please see following pages for full details.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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Outliers : Quality Control Samples

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Laboratory Control Spike (LCS) Recoveries

QC-984027-002 109-06-82-Picoline---- Recovery less than lower control limit41-109%39.9 %EP075E: Nitroaromatics and Ketones

QC-985847-002 109-06-82-Picoline---- Recovery less than lower control limit41-109%33.8 %EP075E: Nitroaromatics and Ketones

QC-985847-002 56-57-54-Nitroquinoline-N-oxid

e

---- Recovery greater than upper control

limit

40-96%105 %EP075E: Nitroaromatics and Ketones

QC-984027-002 92-67-14-Aminobiphenyl---- Recovery less than lower control limit60-112%57.7 %EP075E: Nitroaromatics and Ketones

Matrix Spike (MS) Recoveries

ES1716700--033 14808-79-8Sulfate as SO4 -

Turbidimetric

0902_MW52_060717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

ES1716700--022 7439-96-5Manganese0902_MW65_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EG020F: Dissolved Metals by ICP-MS

ES1716700--021 375-73-5Perfluorobutane

sulfonic acid (PFBS)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--021 2706-91-4Perfluoropentane

sulfonic acid

(PFPeS)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--021 355-46-4Perfluorohexane

sulfonic acid

(PFHxS)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--040 355-46-4Perfluorohexane

sulfonic acid

(PFHxS)

0902_MW50_060717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--021 375-92-8Perfluoroheptane

sulfonic acid

(PFHpS)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--021 1763-23-1Perfluorooctane

sulfonic acid (PFOS)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--040 1763-23-1Perfluorooctane

sulfonic acid (PFOS)

0902_MW50_060717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231A: Perfluoroalkyl Sulfonic Acids

ES1716700--021 2706-90-3Perfluoropentanoic

acid (PFPeA)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716700--021 307-24-4Perfluorohexanoic acid

(PFHxA)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

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Matrix: WATER

Compound Group Name CommentLimitsDataAnalyteClient Sample IDLaboratory Sample ID CAS Number

Matrix Spike (MS) Recoveries - Continued

ES1716700--040 307-24-4Perfluorohexanoic acid

(PFHxA)

0902_MW50_060717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

ES1716700--021 335-67-1Perfluorooctanoic acid

(PFOA)

0902_MW72_040717 MS recovery not determined,

background level greater than or

equal to 4x spike level.

----Not

Determined

EP231B: Perfluoroalkyl Carboxylic Acids

Outliers : Analysis Holding Time Compliance

Matrix: WATER

AnalysisExtraction / Preparation

Date analysedDate extractedContainer / Client Sample ID(s) Days

overdue

Days

overdue

Due for extraction Due for analysis

Method

EK055G: Ammonia as N by Discrete Analyser

Clear Plastic Bottle - Natural

06-Jul-2017----0902_MW61_050717 07-Jul-2017---- ---- 1

EK057G: Nitrite as N by Discrete Analyser

Clear Plastic Bottle - Natural

06-Jul-2017----0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

07-Jul-2017---- ---- 1

EK071G: Reactive Phosphorus as P by discrete analyser

Clear Plastic Bottle - Natural

06-Jul-2017----0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

07-Jul-2017---- ---- 1

Outliers : Frequency of Quality Control Samples

Matrix: WATER

Quality Control SpecificationQuality Control Sample Type

Method ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type Count

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 10.000 48

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 10.000 45

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 10.000 45

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC StandardPAH/Phenols (GC/MS - SIM) 0.00 5.000 48

NEPM 2013 B3 & ALS QC StandardSemivolatile Organic Compounds 0.00 5.000 45

NEPM 2013 B3 & ALS QC StandardTRH - Semivolatile Fraction 0.00 5.000 45

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Analysis Holding Time Compliance

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

If samples are identified below as having been analysed or extracted outside of recommended holding times, this should be taken into consideration when interpreting results.

This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA015: Total Dissolved Solids dried at 180 ± 5 °C

Clear Plastic Bottle - Natural (EA015H)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

11-Jul-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EA015H)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

12-Jul-2017---- 12-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EA015H)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

13-Jul-2017---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

ED037P: Alkalinity by PC Titrator

Clear Plastic Bottle - Natural (ED037-P)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

18-Jul-2017---- 10-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED037-P)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

19-Jul-2017---- 10-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED037-P)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

20-Jul-2017---- 10-Jul-2017----06-Jul-2017 ---- ü

ED041G: Sulfate (Turbidimetric) as SO4 2- by DA

Clear Plastic Bottle - Natural (ED041G)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

01-Aug-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED041G)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

02-Aug-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED041G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

03-Aug-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

ED045G: Chloride by Discrete Analyser

Clear Plastic Bottle - Natural (ED045G)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

01-Aug-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED045G)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

02-Aug-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (ED045G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

03-Aug-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

ED093F: Dissolved Major Cations

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

01-Aug-2017---- 12-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

02-Aug-2017---- 12-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (ED093F)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

03-Aug-2017---- 12-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EG020F: Dissolved Metals by ICP-MS

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 12-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 12-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG020A-F)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

02-Jan-2018---- 12-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EG035F: Dissolved Mercury by FIMS

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

01-Aug-2017---- 13-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

02-Aug-2017---- 13-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Nitric Acid; Filtered (EG035F)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

03-Aug-2017---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK040P: Fluoride by PC Titrator

Clear Plastic Bottle - Natural (EK040P)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

01-Aug-2017---- 10-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK040P)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

02-Aug-2017---- 10-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK040P)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

03-Aug-2017---- 10-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK055G: Ammonia as N by Discrete Analyser

Clear Plastic Bottle - Natural (EK055G)

0902_MW61_050717 06-Jul-2017---- 07-Jul-2017----05-Jul-2017 ---- ûClear Plastic Bottle - Sulfuric Acid (EK055G)

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

01-Aug-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Sulfuric Acid (EK055G)

0902_MW60_050717, 0902_MW25_050717,

0902_MW48_050717, 0902_MW26_050717,

0902_MW68_050717, 0902_MW70_050717,

0902_MW67_050717, 0902_MW69_050717,

0902_MW63_050717, 0902_MW62_050717,

0902_QC509_050717

02-Aug-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Sulfuric Acid (EK055G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

03-Aug-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

Page 473: Appendix - Department of Defence

11 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK057G: Nitrite as N by Discrete Analyser

Clear Plastic Bottle - Natural (EK057G)

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

06-Jul-2017---- 07-Jul-2017----04-Jul-2017 ---- û

Clear Plastic Bottle - Natural (EK057G)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

07-Jul-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK057G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

08-Jul-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

EK059G: Nitrite plus Nitrate as N (NOx) by Discrete Analyser

Clear Plastic Bottle - Natural (EK059G)

0902_MW61_050717 07-Jul-2017---- 07-Jul-2017----05-Jul-2017 ---- üClear Plastic Bottle - Sulfuric Acid (EK059G)

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

01-Aug-2017---- 07-Jul-2017----04-Jul-2017 ---- ü

Clear Plastic Bottle - Sulfuric Acid (EK059G)

0902_MW60_050717, 0902_MW25_050717,

0902_MW48_050717, 0902_MW26_050717,

0902_MW68_050717, 0902_MW70_050717,

0902_MW67_050717, 0902_MW69_050717,

0902_MW63_050717, 0902_MW62_050717

02-Aug-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Sulfuric Acid (EK059G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

03-Aug-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

Page 474: Appendix - Department of Defence

12 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EK071G: Reactive Phosphorus as P by discrete analyser

Clear Plastic Bottle - Natural (EK071G)

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717

06-Jul-2017---- 07-Jul-2017----04-Jul-2017 ---- û

Clear Plastic Bottle - Natural (EK071G)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717

07-Jul-2017---- 07-Jul-2017----05-Jul-2017 ---- ü

Clear Plastic Bottle - Natural (EK071G)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_MW50_060717

08-Jul-2017---- 07-Jul-2017----06-Jul-2017 ---- ü

Page 475: Appendix - Department of Defence

13 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074A: Monocyclic Aromatic Hydrocarbons

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 476: Appendix - Department of Defence

14 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074B: Oxygenated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 477: Appendix - Department of Defence

15 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074C: Sulfonated Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 478: Appendix - Department of Defence

16 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074D: Fumigants

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 479: Appendix - Department of Defence

17 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074E: Halogenated Aliphatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 480: Appendix - Department of Defence

18 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074F: Halogenated Aromatic Compounds

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 481: Appendix - Department of Defence

19 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP074G: Trihalomethanes

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP074)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717, 0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 482: Appendix - Department of Defence

20 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075(SIM))

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 483: Appendix - Department of Defence

21 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075A: Phenolic Compounds

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 484: Appendix - Department of Defence

22 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075B: Polynuclear Aromatic Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 485: Appendix - Department of Defence

23 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075C: Phthalate Esters

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 486: Appendix - Department of Defence

24 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075D: Nitrosamines

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 487: Appendix - Department of Defence

25 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075E: Nitroaromatics and Ketones

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 488: Appendix - Department of Defence

26 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075F: Haloethers

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 489: Appendix - Department of Defence

27 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075G: Chlorinated Hydrocarbons

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 490: Appendix - Department of Defence

28 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075H: Anilines and Benzidines

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 491: Appendix - Department of Defence

29 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075I: Organochlorine Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 492: Appendix - Department of Defence

30 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075J: Organophosphorus Pesticides

Amber Glass Bottle - Unpreserved (EP075)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 08-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 08-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 08-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP075)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü ü

Page 493: Appendix - Department of Defence

31 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Petroleum Hydrocarbons

Amber Glass Bottle - Unpreserved (EP071)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 10-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 10-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 10-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

Page 494: Appendix - Department of Defence

32 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Petroleum Hydrocarbons - Continued

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC601_060717, 0902_QC511_060717,

0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

Page 495: Appendix - Department of Defence

33 of 45:Page

Work Order :

:Client

ES1716700

AECOM Australia Pty Ltd

60547028, task 3.1:Project

Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

Amber Glass Bottle - Unpreserved (EP071)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

16-Aug-201711-Jul-2017 10-Jul-201707-Jul-201704-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

16-Aug-201712-Jul-2017 10-Jul-201707-Jul-201705-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

16-Aug-201713-Jul-2017 10-Jul-201707-Jul-201706-Jul-2017 ü ü

Amber Glass Bottle - Unpreserved (EP071)

0902_MW50_060717 19-Aug-201713-Jul-2017 10-Jul-201710-Jul-201706-Jul-2017 ü üAmber VOC Vial - Sulfuric Acid (EP080)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions - Continued

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC601_060717, 0902_QC511_060717,

0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

EP080: BTEXN

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

18-Jul-201718-Jul-2017 12-Jul-201712-Jul-201704-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-201719-Jul-2017 12-Jul-201712-Jul-201705-Jul-2017 ü ü

Amber VOC Vial - Sulfuric Acid (EP080)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC601_060717, 0902_QC511_060717,

0902_MW50_060717

20-Jul-201720-Jul-2017 12-Jul-201712-Jul-201706-Jul-2017 ü ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP116: 1.4-Dioxane

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717

18-Jul-2017---- 10-Jul-2017----04-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW72_040717, 0902_MW65_040717,

0902_MW66_040717, 0902_MW64_040717,

0902_MW71_040717, 0902_QC508_040717

18-Jul-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717

19-Jul-2017---- 10-Jul-2017----05-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

19-Jul-2017---- 11-Jul-2017----05-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717

20-Jul-2017---- 10-Jul-2017----06-Jul-2017 ---- ü

Amber VOC Vial - Sulfuric Acid (EP116)

0902_QC102_060717, 0902_MW47_060717,

0902_MW52_060717, 0902_QC104_060717,

0902_QC510_050717, 0902_QC511_060717,

0902_MW50_060717

20-Jul-2017---- 11-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231A: Perfluoroalkyl Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 11-Jul-2017----05-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

02-Jan-2018---- 11-Jul-2017----06-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW50_060717 02-Jan-2018---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231B: Perfluoroalkyl Carboxylic Acids

HDPE (no PTFE) (EP231X)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 11-Jul-2017----05-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

02-Jan-2018---- 11-Jul-2017----06-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW50_060717 02-Jan-2018---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231C: Perfluoroalkyl Sulfonamides

HDPE (no PTFE) (EP231X)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 11-Jul-2017----05-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

02-Jan-2018---- 11-Jul-2017----06-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW50_060717 02-Jan-2018---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231D: (n:2) Fluorotelomer Sulfonic Acids

HDPE (no PTFE) (EP231X)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 11-Jul-2017----05-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

02-Jan-2018---- 11-Jul-2017----06-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW50_060717 02-Jan-2018---- 13-Jul-2017----06-Jul-2017 ---- ü

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Matrix: WATER Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP231P: PFAS Sums

HDPE (no PTFE) (EP231X)

0902_MW34_040717, 0902_MW32_040717,

0902_MW33_040717, 0902_MW73_040717,

0902_MW74_040717, 0902_MW72_040717,

0902_MW65_040717, 0902_MW66_040717,

0902_MW64_040717, 0902_MW71_040717,

0902_QC508_040717

31-Dec-2017---- 11-Jul-2017----04-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW61_050717, 0902_MW60_050717,

0902_MW25_050717, 0902_MW48_050717,

0902_MW26_050717, 0902_MW68_050717,

0902_MW70_050717, 0902_MW67_050717,

0902_MW69_050717, 0902_MW63_050717,

0902_MW62_050717, 0902_QC509_050717

01-Jan-2018---- 11-Jul-2017----05-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW20_060717, 0902_MW22_060717,

0902_MW36_060717, 0902_MW45_060717,

0902_MW21_060717, 0902_MW23_060717,

0902_MW44_060717, 0902_MW46_060717,

0902_MW51_060717, 0902_QC102_060717,

0902_MW47_060717, 0902_MW52_060717,

0902_QC104_060717, 0902_QC510_050717,

0902_QC511_060717

02-Jan-2018---- 11-Jul-2017----06-Jul-2017 ---- ü

HDPE (no PTFE) (EP231X)

0902_MW50_060717 02-Jan-2018---- 13-Jul-2017----06-Jul-2017 ---- ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Duplicates (DUP)

NEPM 2013 B3 & ALS QC Standard 10.26 10.004 39 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 10.00 10.006 60 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 10.81 10.004 37 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 10.45 10.007 67 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 10.26 10.004 39 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 10.26 10.004 39 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 10.00 10.006 60 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 12.12 10.004 33 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 12.90 10.004 31 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 10.81 10.004 37 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 48 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 11.11 10.005 45 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 12.77 10.006 47 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 45 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 10.29 10.007 68 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 11.11 10.008 72 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 0.00 10.000 45 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 10.17 10.006 59 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 10.26 10.004 39 üVolatile Organic Compounds EP074

Laboratory Control Samples (LCS)

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.00 5.003 60 üAlkalinity by PC Titrator ED037-P

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 11.94 10.008 67 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.003 60 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 6.06 5.002 33 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 6.25 5.003 48 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 6.38 5.003 47 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.88 5.004 68 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 11.11 10.008 72 üTotal Dissolved Solids (High Level) EA015H

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Matrix: WATER Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Control Samples (LCS) - Continued

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.08 5.003 59 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üVolatile Organic Compounds EP074

Method Blanks (MB)

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 5.97 5.004 67 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.003 60 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 6.06 5.002 33 üMajor Cations - Dissolved ED093F

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 6.25 5.003 48 üPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 6.38 5.003 47 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.88 5.004 68 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 5.56 5.004 72 üTotal Dissolved Solids (High Level) EA015H

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.08 5.003 59 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üVolatile Organic Compounds EP074

Matrix Spikes (MS)

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 ü1.4-Dioxane by HS-GCMS EP116

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üAmmonia as N by Discrete analyser EK055G

NEPM 2013 B3 & ALS QC Standard 5.97 5.004 67 üChloride by Discrete Analyser ED045G

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Mercury by FIMS EG035F

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üDissolved Metals by ICP-MS - Suite A EG020A-F

NEPM 2013 B3 & ALS QC Standard 5.00 5.003 60 üFluoride by PC Titrator EK040P

NEPM 2013 B3 & ALS QC Standard 6.45 5.002 31 üNitrite and Nitrate as N (NOx) by Discrete Analyser EK059G

NEPM 2013 B3 & ALS QC Standard 5.41 5.002 37 üNitrite as N by Discrete Analyser EK057G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 48 ûPAH/Phenols (GC/MS - SIM) EP075(SIM)

NEPM 2013 B3 & ALS QC Standard 6.67 5.003 45 üPer- and Polyfluoroalkyl Substances (PFAS) by LCMSMS EP231X

NEPM 2013 B3 & ALS QC Standard 6.38 5.003 47 üReactive Phosphorus as P-By Discrete Analyser EK071G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 45 ûSemivolatile Organic Compounds EP075

NEPM 2013 B3 & ALS QC Standard 5.88 5.004 68 üSulfate (Turbidimetric) as SO4 2- by Discrete Analyser ED041G

NEPM 2013 B3 & ALS QC Standard 0.00 5.000 45 ûTRH - Semivolatile Fraction EP071

NEPM 2013 B3 & ALS QC Standard 5.08 5.003 59 üTRH Volatiles/BTEX EP080

NEPM 2013 B3 & ALS QC Standard 5.13 5.002 39 üVolatile Organic Compounds EP074

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Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 2540C. A gravimetric procedure that determines the amount of `filterable` residue

in an aqueous sample. A well-mixed sample is filtered through a glass fibre filter (1.2um). The filtrate is

evaporated to dryness and dried to constant weight at 180+/-5C. This method is compliant with NEPM (2013)

Schedule B(3)

Total Dissolved Solids (High Level) EA015H WATER

In house: Referenced to APHA 2320 B This procedure determines alkalinity by automated measurement (e.g. PC

Titrate) using pH 4.5 for indicating the total alkalinity end-point. This method is compliant with NEPM (2013)

Schedule B(3)

Alkalinity by PC Titrator ED037-P WATER

In house: Referenced to APHA 4500-SO4. Dissolved sulfate is determined in a 0.45um filtered sample. Sulfate

ions are converted to a barium sulfate suspension in an acetic acid medium with barium chloride. Light

absorbance of the BaSO4 suspension is measured by a photometer and the SO4-2 concentration is determined

by comparison of the reading with a standard curve. This method is compliant with NEPM (2013) Schedule B(3)

Sulfate (Turbidimetric) as SO4 2- by

Discrete Analyser

ED041G WATER

In house: Referenced to APHA 4500 Cl - G.The thiocyanate ion is liberated from mercuric thiocyanate through

sequestration of mercury by the chloride ion to form non-ionised mercuric chloride.in the presence of ferric ions

the librated thiocynate forms highly-coloured ferric thiocynate which is measured at 480 nm APHA 21st edition

seal method 2 017-1-L april 2003

Chloride by Discrete Analyser ED045G WATER

In house: Referenced to APHA 3120 and 3125; USEPA SW 846 - 6010 and 6020; Cations are determined by

either ICP-AES or ICP-MS techniques. This method is compliant with NEPM (2013) Schedule B(3)

Sodium Adsorption Ratio is calculated from Ca, Mg and Na which determined by ALS in house method

QWI-EN/ED093F. This method is compliant with NEPM (2013) Schedule B(3)

Hardness parameters are calculated based on APHA 2340 B. This method is compliant with NEPM (2013)

Schedule B(3)

Major Cations - Dissolved ED093F WATER

In house: Referenced to APHA 3125; USEPA SW846 - 6020, ALS QWI-EN/EG020. Samples are 0.45µm filtered

prior to analysis. The ICPMS technique utilizes a highly efficient argon plasma to ionize selected elements. Ions

are then passed into a high vacuum mass spectrometer, which separates the analytes based on their distinct

mass to charge ratios prior to their measurement by a discrete dynode ion detector.

Dissolved Metals by ICP-MS - Suite A EG020A-F WATER

In house: Referenced to AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS)

Samples are 0.45µm filtered prior to analysis. FIM-AAS is an automated flameless atomic absorption technique.

A bromate/bromide reagent is used to oxidise any organic mercury compounds in the filtered sample. The ionic

mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell.

Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM

(2013) Schedule B(3)

Dissolved Mercury by FIMS EG035F WATER

In house: Referenced to APHA 4500-F C: CDTA is added to the sample to provide a uniform ionic strength

background, adjust pH, and break up complexes. Fluoride concentration is determined by either manual or

automatic ISE measurement. This method is compliant with NEPM (2013) Schedule B(3)

Fluoride by PC Titrator EK040P WATER

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Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 4500-NH3 G Ammonia is determined by direct colorimetry by Discrete Analyser.

This method is compliant with NEPM (2013) Schedule B(3)

Ammonia as N by Discrete analyser EK055G WATER

In house: Referenced to APHA 4500-NO2- B. Nitrite is determined by direct colourimetry by Discrete Analyser.

This method is compliant with NEPM (2013) Schedule B(3)

Nitrite as N by Discrete Analyser EK057G WATER

In house: Referenced to APHA 4500-NO3- F. Nitrate is reduced to nitrite by way of a chemical reduction followed

by quantification by Discrete Analyser. Nitrite is determined seperately by direct colourimetry and result for Nitrate

calculated as the difference between the two results. This method is compliant with NEPM (2013) Schedule B(3)

Nitrate as N by Discrete Analyser EK058G WATER

In house: Referenced to APHA 4500-NO3- F. Combined oxidised Nitrogen (NO2+NO3) is determined by

Chemical Reduction and direct colourimetry by Discrete Analyser. This method is compliant with NEPM (2013)

Schedule B(3)

Nitrite and Nitrate as N (NOx) by Discrete

Analyser

EK059G WATER

In house: Referenced to APHA 4500-P F Ammonium molybdate and potassium antimonyl tartrate reacts in acid

medium with othophosphate to form a heteropoly acid -phosphomolybdic acid - which is reduced to intensely

coloured molybdenum blue by ascorbic acid. Quantification is by Discrete Analyser. This method is compliant

with NEPM (2013) Schedule B(3)

Reactive Phosphorus as P-By Discrete

Analyser

EK071G WATER

In house: Referenced to APHA 1030F. This method is compliant with NEPM (2013) Schedule B(3)Ionic Balance by PCT DA and Turbi SO4

DA

EN055 - PG WATER

In house: Referenced to USEPA SW 846 - 8015A The sample extract is analysed by Capillary GC/FID and

quantification is by comparison against an established 5 point calibration curve of n-Alkane standards. This

method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH - Semivolatile Fraction EP071 WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. This

method is compliant with NEPM (2013) Schedule B(3)

Volatile Organic Compounds EP074 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS and

quantification is by comparison against an established 5 point calibration curve. This method is compliant with

NEPM (2013) Schedule B(3)

Semivolatile Organic Compounds EP075 WATER

In house: Referenced to USEPA SW 846 - 8270D Sample extracts are analysed by Capillary GC/MS in SIM Mode

and quantification is by comparison against an established 5 point calibration curve. This method is compliant

with NEPM (2013) Schedule B(3)

PAH/Phenols (GC/MS - SIM) EP075(SIM) WATER

In house: Referenced to USEPA SW 846 - 8260B Water samples are directly purged prior to analysis by

Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve.

Alternatively, a sample is equilibrated in a headspace vial and a portion of the headspace determined by GCMS

analysis. This method is compliant with the QC requirements of NEPM (2013) Schedule B(3)

TRH Volatiles/BTEX EP080 WATER

In house: A 12 mL aliquot of sample is mixed with 4.5 g of sodium chloride, equilibrated at 80 degrees C for 30

minutes and the headspace analysed by GCMS in the selected ion monitoring mode.

1.4-Dioxane by HS-GCMS EP116 WATER

In house: Direct injection analysis of fresh waters after dilution (1:1) with methanol. Analysis by

LC-Electrospray-MS-MS, Negative Mode using MRM. PFOS is quantified using a certified, traceable standard

consisting of linear and branched PFOS isomers.

Per- and Polyfluoroalkyl Substances

(PFAS) by LCMSMS

EP231X WATER

Preparation Methods Method DescriptionsMatrixMethod

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Preparation Methods Method DescriptionsMatrixMethod

In house: Referenced to USEPA SW 846 - 3510B 100 mL to 1L of sample is transferred to a separatory funnel

and serially extracted three times using 60mL DCM for each extract. The resultant extracts are combined,

dehydrated and concentrated for analysis. This method is compliant with NEPM (2013) Schedule B(3) . ALS

default excludes sediment which may be resident in the container.

Separatory Funnel Extraction of Liquids ORG14 WATER

A 5 mL aliquot or 5 mL of a diluted sample is added to a 40 mL VOC vial for sparging.Volatiles Water Preparation ORG16-W WATER

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