AR 1001*55 - semspub.epa.gov

AVTEX FIBERS FRONT ROYAL INC.AVTEX FIBERS SITE

RESPONSE MEASURES WORK PUN

ADMINISTRATIVE ORDERDocket Ho. III-90-01-DC

Prepared for U.S. Environmental Protection AgencyHazardous Waste Management Division

Region III

November 7, 1989

AVTEX FIBERS FRONT ROYAL INC.Kendrick LoneP.O. Box 1169

Front Royal, Virginia 22630

AR 1001*55

Avtex personnel have identified certain areas within the Avtex facilityshowing contamination by polychlorinated biphenyls (PCBs) resulting primarilyfrom sudden and unplanned failure of an electrical transformer. PCBs werepopular from the 1930's through the 1960'• for insulating use in electriccapacitors and transformances. They are both chemically and biologicallystable and are very poor conductors of electricity. In high concentrations,PCBs form an oily liquid heavier than water and are not readily dissolved inwater. They also have an affinity for organic matter that helps explain theirbehavior in the environment, particularly in water. According to the VirginiaDepartment of Health, PCBs are everywhere in the environment. Surveys ofambient air, soil, food, surface water and sediments, as well as human fat,blood, and milk have demonstrated measurable levels of PCBs.

Presence of PCBs on the Avtex site has been confirmed by the Virginia StateWater Control Board (SWCB) by its analysis of samples collected onAugust 28, 1989 and September 1, 1989. On September 20, 1989 the VirginiaDepartment of Waste Management (VDWM) requested an evaluation of the Avtexsite and possible assistance from USEPA to address the possible contaminationat the site. In response to this request, USEPA determined that thecompressor room roof and the polyester plant area at the site may pose athreat to public health, welfare or the environment.

In addition to acknowledgement of the presence of measurable levels of PCBs atthe Avtex facility, the USEPA has stated that a number of solvent-containingdrums may pose a potential threat for fire or explosion. The USEPA alsoidentified several process areas where certain hazardous substances may bepresent and could pose a potential threat of release.

Therefore, based on (1) a potential threat to worker health from exposure toPCBs on the site; (2) the potential for offsite migration of PCBs; (3) a fireor explosion potential from solvent"containing drums; and (4) potentialunidentified hazards from other facility process operation, the USEPA has

determined that a removal action is appropriate to abate, minimise, stabilize,mitigate, or eliminate the releases or threat of releases.

ARIOOI457

SECTION 1STATEMENT L OF UNDERSTANDING

The Regional Administrator, Region III, United States Environmental ProtectionAgency (USEPA) executed an Administrative Order concerning sampling and cleanup actions at the Avtex Fibers Front Royal, Inc site located at 1169 KendrickLane, Front Royal, Virginia. This order was issued on October 31, 1989 andbecame effective on November 1, 1989. The order was issued pursuant to theauthority vested in the President of the United States by Sections 106(a) and104(e) of the Comprehensive Environmental Response, Compensation, andLiability Act of 1980 (42 U.S.C. §§9606(a) and 9604(e)> as amended by theSuperfund Amendments and Reauthorization Act of 1986, Pub. L. No. 99-499, 100Stat. 1613 (1986). Regional Administrators of EPA have been delegated thisauthority. This order was issued to Avtex Fibers, Inc., and Avtex FibersFront Royal Inc. Notice of issuance -of this Order has been given to theCommonwealth of Virginia, pursuant to Section 106(a) of CERCLA, 42 U.S.C.§9606(a). ;

,!.-

Avtex has owned and operated a rayon producing facility in Front Royal,Virginia from August 1976 until the present. The Avtex plant occupiesapproximately 440 acres of which 60 are under roof and includes 23 basinswhere process and other wastes are disposed. Manufacturing operations beganat the plant in 1940 under ownership \6f the American Viscose Corporation; thegeneral operation has remained consistent. The facility is located on theeast bank of the South Fork of the Shenandoah River. A site map is includedas Figure 1-1*

flRIOOl*58

LJQ£Oc

OI&1*59

AVTEX FIBERS FRONT ROYAL INC,AVTEI FIBERS SITE

SECTION 1STATEMENT OF UNDERSTANDING

ADMINISTRATIVE ORDERDocket No. III-90-01-DC

Prepared for U.S. Environmental Protection AgencyHarardous Waste Management Division

Region III

November 7, 1989

AVTEX FIBERS FRONT ROYAL INC.Cendrick LaneP.O. Box 1169


ARIOOU60

AVTEXHBERSFRONTROYALINaAVTEX FIBERS SITE

WORK PLAN

CERTIFICATION

I certlQr that the ii/ormatlon contained in or aceonpanyingthto WORK PLANb true, accurate and complete*

Signature:.NanWprintV.C. KENNETH WAG1

TttteEXECimVE VICE PRESIDENT. AVTEX FIBERS FROOT ROYAL INC

ADMMST11A1IVB ORECR

U. Si BufsuDDcnUl FtotoctioD Afency

NoremtwIW

AVTEX FIBERS FRONT ROYAL INC. «D I nnr c iKm±ktL« ARIU046IP. a Ba 1169

ini* 22630

RR 1001)62

AVTEXHBERSFRONTROYALINCAVTEX FIBERS SITE

WORK STANDARDS

In compliance with Section V1H, 8.2, all work performed under thisADMINISTRATIVE ORDER, (Docket DI-90-01-DC) will be in compliance with thetcrmsandconditionsoftheOrdcr. All supervisory personnel and vendors will meettheOSHArequireroentsasdeftaedinC.F.R. $1910.120. The WORK PLAN will beconsistent with NCP, 40 C F. R. Par 1300. The cleanup levels will at least be as strictasthosein40C P. R. f Part 761, SubpartG. "PCBSfcill Cleanup Policy". All workwill use quality assurance/quality control, and chain of custody procedures inaccordance with the "EPA NAIC Policies and Procedures Manual" dated May 1978,revisedNovember 1984, EPA Document 330 / 9-78-001-R and "Interim Guidelinesand specifications for preparing Quality Assurance Project Plans", December 1980,QAMS-005 / 80. All laboratories will have a documented Quality Assurance Programthat complies with the EPA guidance document: QAMS-005 / 80.

CREER

U. S. fiirirdmattl Protection Agency

Refloain

Noremberl989

AVIEX FIBERS FRONT ROYAL INC. •niKndkiUm ARI

FrwtRoyil,Vir|hii« 22630

• PCS Clean up, compressor room roof

• PCB Clean up, stored transformer area . • . -

Sediments removed from storm sewer system

Storm sewer system inspected completely by remote video

• Build up and caulking of manholes in storm sewer system

• Removal of transformer 1A

Clean up of Manhole "I"

Polyester chip area isolated from sewer systemiRepair of final clarifiers

Removal of all stored transformers

Repair of final clarifiers

* Repair of sludge thickener raking mechanism

* Draining and cleaning of aerobic digester

; • Repair of sludge thickener pump

Draining and cleaning of sludge thickener

* Modification of wastewater treatment plan operations to reducesuspended solids

In addition to these efforts which have been completed, Avtexcontractors, engaged in PCB removal activities are in the process ofimplementing all activities required by this order. The schedule for finalcompletion is presented in Section 3 of this Work Plan.

5 Site Security Plan (VZII)(8.3)(b),• Site Access (XI)Ul.l)

6 Fire Protection Plan (VIII)(8.3)(c)

7 Identification, Segregation, andDisposal of Hazardous Substances

•PCB Contaminated Material (VIII)(8.3)(d)(2)

• Other Hazardous Waste Materials (VIII)(8.3)(d)(l)

8 Site Sampling Plan (VIII)(8.3)(e)

9 Subsequent Studies (VIII)(8.3)(f)

10 Quality Control/Quality Assurance (X)UO.l)

Appendices

A Personnel Resumes (VIII)(8.2)

B Scope and History NA

C Manifest and Material NASafety Data Sheets

D Grid Pattern Data NA

E Drawings and Sampling Data NA

F Contractor Qualification (VIII)(8.2)Statements

G Contractor Health and Safety NAPlans

2.2 CURKEHT WORK STATUS

In accordance with Avtex plans for PCB clean up at the Avtex FibersFront Royal site agreed upon with the USEPA, Region III, Eastern ResponieSection, On Scene Coordinator, prior to execution of this Order, the followingactivities have been completed!

Sewer system lined from manholes A21 to A16 (refer to sewersystem drawing - Appendix E)

ARIOOI»65

SECTION 2SUMMARY OF WORK

2.1 WORK PLAN CONTENTS

The purpose of this work plan document is to describe immediate responsemeasures to be implemented at the Avtex site necessary to eliminate the threatto public health, welfare, or the environment that may exist due to potentialworker exposure to PCBs, the potential for offsite migration of PCBs into theShenandoah River, and the potential for fire, explosion, or spillage of wastesfrom leaking drums. This work plan is^consistent with the provisions andrequirements of the National Oil and Hazardous Substances Contingency Plan,40 CFR 300 and CERCLA.

W • - ; - , ' , : •

This work plan includes the following sections:

Work Plan Description Administrative OrderSection Number Reference

1 Statement of Understanding NA

2 Summary of Work NA

* Work Plan Contents (VIII)

• Current Work Status NA

3 Management Plant

• Organization and Contractor (VII)(8.2)Responsibilities

• Reporting Requirements (VII)(8.2-8.12),CIX)(9.UD . nn| - -flR 1001*66

• Project Schedule (VIII)(8.3(g)

4 Site Health and Safety Plan (VIII)(8.3)(a)


SECTION 2SUMMARY OF WORK

ADMINISTRATIVE ORDER BY CONSENTDocket No. III-90-01-DC


Region III

The Commonwealth of Virginia

Virginia Division of Waste Management

November 7, 1989

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneP.O. Box 1169


flBIOOi»67

AVTEX FIBERS FRONT ROYAL INC.Box 1169. Kendrick Lane, Front Royal. VA 22630-1169 (703) 635-2141

November 3, 1989

Mr. Harry T. DawEnforcement Project ManagerU. S* Environmental Protection AgencyEnforcement and Title III Section (3HW33)841 Chestnut BuildingPhiladelphia, PA 19107Subject: Avtex Fibers Site, Front Royal PCB Cleanup

Dear Mr. Daw:In accordance with our plans for PCB cleanup at Avtex Fibers Front Royal asagreed upon with your Agency, and reflected In The Administrative Order Issuedunder the Comprehensive Environmental Res .iise, Compensation, and Liability

• Act of 1980, we have undertaken the following work.1) The polyester chip area was Isolated from our sewer system early 1n

September, 1989.2) All roofing and accompanying debris was removed from our Compressor room

roof by mid October and clean up of all concrete 1s well underway.3) The present piping from the roof drains of the Compressor room Is being

removed and replaced with new piping and will be complete by next week.4) The complete storm sewer system has been cleaned and all sediment removed.

Most manhole bottoms have been encapsulated.5) The process sewer on the north side of the plant Is presently being cleaned

and tested. This Is the process sewer to which the polyester dock areawas connected*

6) The stored transformer area and the 2A substation area has been clearedand all transformers removed. This area has been cleaned and we arepresently awaiting results of sampling.

7) Maintenance work has been accomplished at our Waste Treatment plant asfollows: AR I 001*68

Page 2Mr. Harry T. DawNovember 3, 1989

a) the south final clarlfler center section was replaced andthe remainder of the mechanism repaired and the basin completelycleaned and returned to service.

b) The north final clarlfler was repaired and returned to servicefollowing the work on the south unit.

c) The sludge thickener was drained and the mechanical partsrepaired. The unit was thoroughly cleaned.

d) The Aerobic digester 1s being drained and cleaned.e) The thickener sludge pump has been overhauled.

Implementation of these cleanup efforts, and especially the cleaning of theprocess sewer on the north side of the plant, could result 1n the dislodgingof PCB-contamlnated sediments to the Waste Treatment plant Influent. We aretaking all precautions possible to minimize the danger of any substantialreleases.ThU notice Is being provided as requested In The Administrative Order DocketNo. 111-90-01-DC, paragraph 8.6.

Sincerel

C. Kenneth Wagner"Executive Vice President - Engineering

CKW/ms

Ordered and Approved

EPA Project Coordinator

I certify that the Information contained 1n or accompanying this letter ofnotice Is true, accurate, and complete.

SI gnature: ____Name: £&/* UHoy

Title: ^V- t//<-«s

AVTEX FIBERS FRONT ROYAL INC.AVTEX HBERS SHE

DUTIES OF AVTEX PROJECT COORDINATOR

"Die Project Coordinator will be responsible for ovasedng the implementation of thisOrder. To the maximum extent possible, communications between Avtex and the EPA, and all documents, including reports, approvals, end other correspondenceconcerning the activities performed pursuant to the terms and conditions of thisOrder, will be directed to the EPA Project Coordinator by certified mail

AEMDCSTOATTVE ORDER

S. EuvoQMDCGtii nutation Agency

v Region ID

November WW

AVIEX FIBERS HUKTROTALINC.K0H)CfcUneP. a Box 1169

Ram RoyiLVirginU 22630

I ' "•' I ' '

7 AR|OOI»70

AVTEX FIBERS FRONT ROYAL INCAVTEX FIBERS SITE

OUTLINE OF PROGRESS REPORT

To comply with Section Vm( 8.7, beginning on the first monday following the receiptof EPA appr oval of the WORK PLAN, and continuing until EPA advises Avtex thatthe work is complete, Avta win provide EPA with a Progress Report for eachpreceding 7 day period (Sunday through Saturday). The Progress Report will includeat least:

1. adesaiption of theactionsthathavebeoitakenhacWevfag compliantthe Order.

2. AdescripdonofaUdataantidpatedandacdvitiesscheduledforthenext7day&3. A description of any problems encountered or anticipated.4. Any actions taken to prevent or mitigate such problems.5. A schedule for when such actions will be completed6. Copies if all analytical data received during the reporting period.7. AUmodifi(^cmstotheWORKPLANmadebaccordancewithsectionXVm

of this Order.8. A rtport of identifying the amount of discharge, if any, of PCB'sintothe

Shenandoah River during the prior 7 days.

ATMMSTRATTVE CHEER

Flcpnd tor

U. S> Birkonnaul Protection Aftncy

Region HI

Noremborl989

AVIEX FIBERS FRCNT ROYAL INC.

A R I O O U 7 1inu 22630 H II I U U 4 / I


METHOD OF TRANSMITTAL

To comply with Section Yin, 8.8, and in accordance with discussions with the EPAProject Coordinator, all documents including work plans, reports, sampling results,and other correspondence to be submitted pursuant to this Order will be sent bycertified mail, express mail, Federal Express, UPS Express, of other carrierproviding documented express service, with a return receipt.

ADMINISTRATIVE CREER

BocfatHWOlMX:

U. S. EnrironmoUl Protection Afency

Region ID

Notonte 1989

AVtEX FIBERS HtONT ROYAL WC.

P. a Box 1169font Roy* VittiniA 22630

AR 100472

AVTEXHBERS FROOTROYALINCAVTEX FIBERS SITE

WORKPLAN

LIST OF INFORMATION TOBE HELD BY AVTEXPENDING EPA REQUEST OR INSPECTION

Secdoitll

Any and an information resulting from and/ orpcitainmg to actions taken by AvtcxpircDanl to thisOrderincludinglmtnotliinitcdlojesolting

1. AnalyticatiaU2. Site safety dat*3. Sitemoratoringdat*4. Opexation&flogs5. CopiesofaUhazardoinwastemanifestsCncludingcopiesofaUhazaido

sifted upon receipt of hazardous waste by a licensed treatment, storage, and/or disposalfacility)

6. Identities of transporters naed7. Identitiesofcontractonandsnbcontractoisiiaed

AEMMSTRATTVE CRTER

Ptcpvod for

U* S* EnrffonDCDw FtotBction Afncy

RcflonHI

flRIOOl*73AVIEC FIBERS FRCNT ROYAL INC.

KenftickLm

ProO Royrf, Vininu 22630


WORK PLAN

STATEMENT OF AVAILABILITY OF DATA TO EPASection 1U,1U,IL4

AVTEX FIBERS FRONT ROYAL INC does make a daim to Business Confidentiality for (he yamprocess areas, Reaeardi Projects in the yarn products areas, and the polypropylene ginning area.No information has been re<pested about these areas. No records or documents about these areashave been withheld,

NodainiofconrIdenriaHtyshaUbema&rcviewiiifoniiation,orforinfoimalionrcqmiedthcrempursuanttothisr

AEMimSTRATTVE CRTER

U. S. fiorvocmaxil Protectioo

Region IE

AV1EX FIBERS FRONT ROYAL WC.KadkkLneP.O.Box 1169

22630 A R I 0 0 7 U

AVTEX FIBERS FRONT ROYALINCAVTEX FIBERS SITE

WORK PLAN

NOTOICATION OF DELAY

Sectional

The Avtex ftoject Coordinator wittnotify the EPAof any delay or ann'cipateddeky in achievingcompliance with this Order. SuchnotificationwUlbejEadeveTbaUyassoonaspossible butnotlater than2bnainessdaysafterAvtex becomes aware of the delay; and in writing no later than 7 daysafter Avtex becomesaware of the delay.

ADMINISTRATIVE ORDER

Ftcpnd fcf

U. S. Enrirocoeatil Protecti

Region ID

November 1989

AVTEX FIBERS FRCNTROTAL INCEmtkiLaiP.aBoill69

FrottRoyil, Vnpni* 22630

AVTEXEIBERSFRONTROYALINCAVTEX HBERSSTTE

WORK FLAN

FORM OF CERTIFICATION

faction

Alinotices, reports cetifications, data presentations or other documents snbmittedby Avtex whichdiscusses, describes, demonstrates, or supports Avtex'scompliance ornon-compliance with thisOrderwillbccertifaedinthefollowingform:

I certify that the information contained in OT accompanying this(spe dry type of sobmission)istroe»accurateandcomplete.

Signature:

Name(print):.

TiUe:___

ADMuNBTRATTVE CRECR

U. S. Enrkwmentil Protecdoc

Region III

Nowmbff 1989

AVTBCHBERS FRONT ROYAL INC. ^ R I 0 0 k 7 6

P.O.Box 1169Front Royii,VirjinU 22630


SECTION 3MANAGEMENT PLAN



Region III

The Commonwealth of Virginia

Virginia Division of Waste Management

November 7y 1989


Front Royalv Virginia 22630

flRIOOi»77

SECTION 3MANAGEMENT PLAN

Avtex has assigned a project coordinator to be responsible for overseeing theimplementation of this Order. All communication of Avtex to and from USEPA,including all documents, reports, approvals, and any other correspondenceconcerning the activities performed pursuant to the terms and conditions ofthis Order will be conducted by the Avtex Project 'Coordinator. The AvtexProject Coordinator shall implement the management plan described in thissection to ensure efficient, effective, and timely completion of the elementsof this work plan.

The initial management plan includes the following:

General Organization

Reporting Procedures

Project Schedule

During the course of work plan implementation, additions or modifications tothis work plan may become necessary. These will be presented to USEPA inaccordance with the provisions of this Order.

flRIOOl*78

3.1 PROJECT OBCAHIZATIOH CHART

AVTBXP1»BK0 FRONT ROY AL1MC. (AVTBX 0ITB1ADMINISTRATIVE ORDBRB Y CONSENT, DOCKETI1I4M1M>C

ORGANIZATIONAL CHART

EPAPROJECT COORDINATOR

HARRYT.DAWAVTEX

PROJECT COORDINATORC KENNETH WAGNER

EPASENIOROSC

ROBERT E.CARONAVTEX

PROJECT MANAGERPAULJ.MALINA

PCD CLEAN-UP GROUP

ALLIANCE TECHNOLOGIESmEUROPA DRIVECHAPEL HILL, NC

PRINaPAL ENGINEERALAN RIMER

S.D.MYERSTRANSFORMER CONSULTANTS

18* SOUTH AVENUETALLMADGC, OHIO

MGR. FIELD SERVICEXYNN FRITZFIELD SUPVSR.4>AVID BISHEL

1

STEAMKATHAZMATofVAP.a BOX 24242RICHMOND, VA

FIELD SUPVSR.410N ALD BARNESBRYANTBARNESGEORGE CWALTON

NON-PCB DRUM DISPOSAL GROUP

CHEMICAL WASTE MAN AGEMENTINCITECHNICAL SERVICES DIVISIONp.a BOX H

SE ALSTON, AAPROJECT MGE-JOBN BAKER

FIELD ANALYSTII-PHILIPLAWHON

AVTEXPIPESHOPFOREMANl

JOEL IL AUGER

W.B.OOQDEINC28HCOFERROADRICHMOND, VAFIELS SERVICEJAMES GOOD WIN

JETBLASTofVAMtE. RANDOLPH ROAD

HOPE WELL, VAOHL MGR.-GENE F. WADE

ARIOOU80ROBINSON PIPE CLEANINGCa

HELD SUPVSR. PIPE VIDEO SERVICECLARANCE JONES

3.2 REPORTING REQUIREMENTS FOR AVTEX FIBERS

Within five (5) business days of effective date of this Order, Avtex willperform the following activities.

Avtex will retain all appropriate contractors.

Avtex will notify the USEPA in writing regarding the identity andqualifications of persons primarily responsible for carrying out the terms ofthis Order. This will be accomplished by this work plan.

All supervisory personnel employed by hazardous waste contractors will meetOSUA 29 CFR 1910.120 and applicable state law.

If contractor personnel are disapproved, Avtex will select replacements withinfive (S) days.

Avtex will submit work plan and schedule to USEPA*

The work plan will be consistent with 40 CFR 300.

The work plan will consist of the following components:

Health and Safety Plan.

Site Security Plan*

Fire Protection Plan for drum storage and disposal areas.

Plan to identify, segregate, and dispose of—

a* substances in drums

b. PCBs in the following areas

1* polyester building

2* compressor room roof

3* transformer storage area

4* rain water sewer system

S. other areas designated by EPA designated prior to submission ofWP

Plan to sample entire site.

ARIOOi*8l

( - Study that evaluates operations, processes, chemical storage areas,^^ ancillary equipment or plant systems, and any preventative or

mitigative clean up options to address a major release.

The work plan will include a schedule for completion of the Work Plan.

If deficiencies in the submitted work plan are noted by the USEPA, Avtex willcorrect those deficiencies within 5;business days of disapproval*

Within 5 business days of approval of the work plan, Avtex will implement thework plan. It should be noted that implementation of all major provisionsother than formal reporting has commenced.

Within 24 hours, Avtex will give notice to EPA if Avtex believes at any timePCBs have the potential to reach the influent of the waste treatment plant.

Seven days after approval of the work plan and until USEPA notifies Avtex thatwork is completed, Avtex will provide a progress report for each 7 day period.This progress report will include the following information:

1. description of actions taken to complete order.

2. description of all data anticipated and activities scheduled for thenext 7 days.

, 3. description of problems encountered or anticipated.

4. Actions taken to prevent or mitigate problems.

S. A schedule for when such actions will be completed.

6. Copies of all analytical data received during reporting period (7days).

7. All modifications to the work plan.

8. Report of any discharge of PCBs into the Shenandoah River.

All correspondence regarding activities pursuant to this Order will be sentvia certified or express mail to USEPA.

All reports, plans, specifications when approved, become part of this Order.If disapproved, corrections shall amend and submit revised submission thatresponds to specified deficiencies*' .

Upon request of USEPA, Avtex will provide any and all information resultingfrom this actions including the following information:

1. Analytical data. '

AR 1

2. Site Safety data.

3. Site monitoring data.

4. Operational logs and copies of hazardous waste manifests includingsigned receipts from disposal facilities.

5* Identifies of treatment/storage/disposal facilities used.

6* Identities of transportation facilities used*

7. Identities of contractors and subcontractors used*

Within 30 days of completion Avtex will submit a written report to USEPAdetailing actions taken and notifying USEPA of completion.

If USEPA notifies Avtex of deficiencies (no deadline). Avtex will correctdeficiencies.

If it becomes necessary to change project coordinators during the course ofwork required under this. Order, Avtex will notify USEPA three (3) days priorto the change.

Avtex will consult with USEPA prior to all sampling and analysis. Avtex willuse a laboratory which complies with EPA QAMS-005/80.

Fines for failure to comply are payable in 5 days of demand. A copy of thesubmittal letter will be sent to USEPA coordinator; letter and check will besent to EPA Region III Hearing Clerk (3RCOO), 841 Chestnut Street,Philadelphia, PA 19107.

Avtex Project Coordinator will notify EPA of any delay or anticipated delaybecause of FORCE MAJEURE, in achieving this order. Notification will beverbally as soon as possible, at least within 2 days, and in writing within 7days. The notification will include the following information:

1. Fully describe nature of delay.

2. Fully describe reasons delay is beyond control of Avtex.

3. Actions taken to mitigate/prevent/minimize delay*

4. Failure to provide timely notice will constitute a waiver of Avtex'sright to a delay.

Avtex understands that minor modifications to this work plan and schedule maybe made by the mutual consent of Project Coordinators. Such modificationsmust be memorialized in writing by Project Coordinators.

Any notice, report, certification, data presentation or other documentsubmitted shall be certified by an Avtex corporate officer.

"I certify that the information contained in or accompanying this (specifytype of submission) is true, accurate and complete."

Signature __________________

Name (print)

Title:

AR I00l*8l»

3.3 PROJECT SCHEDULE

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j I 1 ' t 1 t ' 1 ' ' 1 ' 'I 1 I ! . I | 1 ! 1 1 f i l l1 j 1 1 . 1 ! j 1 1 1 1 1 t 1j i i i i i i i J i i i i i it i < < i > • { f i ! i ' 'i 1 j i j i i | 1 i t ;i I 1 ! ! i j ! ! ! ! ! ' 'i i i i i i j i j ! ! !i i i l i i i i i 1 i i i i1 ! i i ! t t 1 ! f '1 ! ! ! ! 1 ! ! ! ! ! ' : 'l i i i 1 j i j i * i ii l ! | i ! ! ) ! ! ' : .'| ) i 1 > 1 i ) i i i ii t i i i i i j i i Ii i i i f i • i i i i ! pi i i i i i i i i i i i! ! ! ! ! ! i j i i ! i ii i l i i ! ) j | . i i i1 i j i 1 i 1 1 1 1 1 ! 1 !

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i i i i ' l ! | A R 1 QQ'lj 8 8i i ! i j i ! 1 i 1 • •( t 1 | j 1 1 j f 1 I I I !i i i j i i i l i t > i i

3.4 Additional Information

AVTEXHBERSFROKTROyALINaAVTEX FIBERS SITE

NOTIFICATION TO CONTRACTORS

In compliance with Section VI, 6.3, a copy of ADMINISTRATIVE ORDER Docket

ffi-90-01 -DC was provided to cadi contractor, sab-contractor, laboratory, and

consultant effective November 3, 1989, by amending the purchase agreement with

each vendor to include the Or der t require that all work paf armed be in compliance

with toe terms and conditions of the Order, and that all vendorsmeettheOSHA

requirements as defined in CF.R. (1910.120.

ORDER

for

U. S. nmnoncflUi Protection Agency

November 1989

AVTDC FIBERS FRCKT RCHTAL INC.

P. a Box U69inU 22630 flfi 100^90

AVTEX FIBERS FRONT ROYAL INC.Box 1169. Kendrick Lane, Front Royal. VA 22630-1169 (703) 635-2141

Hovember 1,1939

C.Kennetn WagnerExecutive Vice PresidentAvtex Fibers Front Royal Inc.P.O.BoxU69KendrfcxLaneFront Royal Virginia 22630

Mr. Harry T.DavEnforcement ManagerU. S. EnvliDninental Protection AgencyEnforcement and Title m Section (3HW33)841 Chestnut BufldingPhiladelphia, PA 19107

Re: Avtex Fibers Site, Front Royal, tfrgnla; Unilateral Administrative Order; Docket m-90-Ol-DC

Deer Mr. Dav.

The Project Coordinator for Avtex Fibea Front Royal toe. fa:Mr. C. Kenneth WagnerExecutive Vice PresidentAvtex Fibers Front Royal Inc.P.O. Box 1169Kendrick LaneFront Royal Virginia 22630

THs letter constitutes "notice' as required t>y Avtex Fibers Site, Front Royal, 'Virginia; UnilateralAdministrative Orte; Docket Xn-90-Ol-DC section 9.L

Sincerely,

C. Kenneth WagnerExecutive Vice PresidentAvtex Fibers Front Royal Inc.

this tetter of notice Is true and completes?*ff a ttl-Signature:

Name:_£


SECTION 4SITE HEALTH AND SAFETY PLAN

ADMINISTRATIVE ORDERDocket Ho. III-90HU-DC

Prepared for U.S. Environment*! Protection AgencyHazardous Waste Management Division

Region III

November 7, 1989



SECTION 4

SITE HEALTH AND SAFETY PLAN

4.1 PURPOSE

The purpose of this plan is to describe the measures to be implemented at theAvtex site necessary to eliminate the threat to public health, welfare, or theenvironment due to potential exposure to hazardous substances, the potentialfor off site migration of hazardous substances, and the potential for fire,explosion, or spillage of waste from drums.

Any entry onto a site potentially containing hazardous materials must be madewith caution. A safety plan for work performed in response to this Order(Docket No. 111-90-01-DC) has been developed to ensure that all the hazards ofthe site are evaluated prior to entry. The Occupational Safety and HealthAdministration requires that a written safety plan be present on site and thatall personnel working on the site have read and understood the plan.

Because of the fact that the Avtex site includes an operating manufacturingfacility and because of the significant number of individual projectscontractors involved in removal activities, the focus of this safetymanagement plan is to define clearly those areas of the Avtex propertyinvolved in removal or assessment activities and to ensure that procedures arein place for segregating those areas and defining where possible, anypotential hazards in those areas. Individual contractors have been,maderesponsible for their own safety plans, and these are included in Appendix Gof this work plan.

4.2 GENERAL INFORMATION

4.2.1 Site Name and Address

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneFront Royal, Virginia 22630(703) 635-2141

4.2.2 Project Dates

Start Date: November 7, 1989

Finish Date: to be determined

4.2.3 Site Location ' ' '

The Avtex Site is located on the south side of Kendrick lane in Front Royal, 'Virginia. The site is bordered by Kendrick Lane on the north, a wooded areaon the east, West Main Street and Luray Avenue on the south, and the southfork of the Shenandoah river on the vest. The site contains approximately 400acres.

4.2.4 Directions to Site

Front Royal is serviced by interstate route 66, and by state route 55, and340. Interstate route 66 has exits onto routes 55 east of Front Royal andonto route 340 north of the town. Route 55 west combines with route 340 tobecome Royal Avenue, the major north/south road in Front Royal. Turning westonto 6th Street will lead directly into Kendrick Lane and to the Avtex Site.A map is included in Appendix E of this work plan.

4*2*5 Emergency Phone Numbers

Emergency medical servicesl 'Gate Guard (703) 635-2141 extension 141Plant Dispensary 8 AH-4 FM extension 119Warren Memorial Hospital (703) 636-0333Ambulance service 911Police 911Poison Control Center (Charlottesville) (800) 451-1428

4.2*6 Directions to Hospital

Warren Memorial Hospital emergency room is located on Shenandoah Avenue. Turnright at the plant gate, proceed to the top of the grade, and nake a left turnonto Shenandoah Avenue (2nd left), 'the hospital is on the right in the thirdblock. The emergency room entrance is clearly narked, and is the firstbuilding seen* A map to Warren Memorial Hospital is included in Appendix E ofthis work plan. - v ;f

4.3 CHEMICAL HAZARDS

PCB's are defined as a series of technical mixtures consisting of many isomenand compounds that vary from mobile oily liquids to white crystalline solidsand hard non-crystalline resins. "They are...components of dielectric fluidsin transformers and capacitors." (from Monsanto MSDS, appended)

Any additional materials discovered as a result of sampling activities will bereported to the USEPA and their hazards documented. MSDS's will be included.

4.4 PROJECT SUMMARIES

4.4.1 Objectives

Avtex's objectives for this project are to manage, control, and ensurecompletion of all required assessments and removal activities, provide allreasonable precautions to protect the public, workers, contractors,subcontractors, and the environment from exposure to hazardous substances, todefine clearly those areas of the Avtex property involved in removal orassessment activities, and ensure that procedures are in place for segregatingthose areas and defining where possible, any potential hazards in those areas.

4.4.2 Contractors

Alliance Technologies Corporation100 Europe Drive, Suite ISO, Chapel Hill, NC 27515

Chemical Waste ManagementTechnical Services Division, P.O. Box 96, Sealston, VA 22547

Conoco

Jet Blast of Virginia920 E. Randolph Road, Hopewell, VA 23860

Robinson Pipe Cleaning CompanyP.O. Box 396, Eighty Four, PA 15330

Steam Kat Haz Mat of VirginiaP.O. Box 24242, Richmond, VA 23224-0242

Transformers Consultants/S.D. Myers180 South Avenue, Tallmadge, OH 44278

4.4*3 Key Personnel

Project CoordinatorsFor EPA

Mr. Harry T. DawU. S. EPAEnforcement and Title III Section (3HW33)841 Chestnut BuildingPhiladelphia, PA 19107(215) 597-6687

ARiOQlf95

For Avtex Fibers >:; ;!'

Mr. C. Kenneth WagnerExecutive Vice PresidentAvtex Fibers Front Royal Inc.Kendrick LaneP. 0. Box 1169Front Royal, VA 22630

Avtex Fibers Front Royal Inc.Utilities Engineer, PCB's Project Engineer: Paul Malina,extension 400

Alliance Technologies CorporationProgram Manager: Alan Rimer, P.E.

Chemical Waste Management vProject Manager: John BakerField Analyst II: Philip Lawhon

Conoco

Jet Blast of VirginiaOperations Manager: Gene F. Wade

Robinson Pipe Cleaning CompanyField Supervisor; Clarence Jones

Steam Kat Haz Mat of VirginiaField Supervisors: Donald BarnesField Supervisors! Bryant BarnesField Supervisors! George Walton

Transformers ConsultantS/S.D. MyersManager Field Service! Lynn FritzField Supervisor: David S. Bishel

4*4.4 Site Work, Zones

4.4.4.1 Compressor room roof: The area outside the powerhouselocated on top of .the compressor room. This area includesthe concrete transformer pad as well as the roof itself.

4.4.4.2 Sub 1A: The substation of the corporate offices.

4.4.4.3 Transformer storage area: An area located on the eastside of fl pulp storage. This area contains approximately10 tr.n.fo™er..

4.4.4.4 Polyester dock: An area on the north and east side of thepolyester building dock area. This area includes the dockand rail road track areas.

4.4.4.5 Storm Sewer: The manholes and connecting lines for thefollowing manholes: A10, All, A16, A17, A21, A22, A24,A26, A27, A28, A31, A33, A3S, A40, A41, A42, NA13, NAll,NA10, A43, and A44. The actual numbers may change astesting indicates either a need for more testing ordecontamination.

4.4.4.6 Any other sites found during the required site survey.

4.4.5 Access Route*. Evacuation Routes, Problem Areas

Access to the compressor room roof is through the turbine room downthe stairs located in the northwest and southeast corners of theroom to the ground level and to the exterior of the building.

The Substation 1A, and polyester dock areas are already outside ofthe plant buildings.

Access to each manhole is through the manhole access cover opening.In these cases, climb the ladder to ground level.

The two drum storage areas are immediately adjacent to large openloading docks, and to normal marked exits. Leave these sitesthrough the opening furthest away from the hazard. All exits leadto the exterior of the plant.

In all cases, once outside of all plant buildings, proceed to themain gate via the perimeter road in the direction furthest from thehazard •

Egress from storm sewer manholes is limited, therefore everyprecaution must be taken to strictly limit the number of workers ineach manhole.

Safety plans for individual contractors are included as Appendix Gof this work plan.

ARIOQl»97

5.9.2 The gate guard will assure that only fire-personnel and police withproper identification are allowed on plant property. If necessary,request the assistance of the Front Royal Police to assure that thepublic is protected from possible exposure to hazardous materials.

5.9.3 Community Relations and Communications

A copy of this procedure will be mailed to:

• Chairman of the local Hazardous Chemical Response Team

Avtex Fibers will meet with local officials to communicatethe nature and the extent of the chemical clean-upproject, and to communicate the possible hazard due tofire.

AFU00498

5.8.3 PCBs can be absorbed through the skin which may lead to drying andcracking of the skin.

5.8.4 PCB liquid and vapors may be mildly irritating to eye tissues.

5.8. 5 Prolonged exposure to PCBs may cause chloracne.

5.8.6 All solids and liquids handled during the clean-up may contain PCBs.

5*8.7 All enclosed spaces may contain C$2 or H2S gas or may be deficientin oxygen. Plant "Tank entry and entry of enclosed spaces"procedures should be followed at all times.

5.8.8 MSDS for PCBs is attached.

5.8.9 PCBs are fire resistant. They may decompose to CO, C02, HC1,phenolics, aldehydes and other potentially toxic products if exposedto heat or flame.

5.8.10 PCBs in electrical fires may form chlorinated dioxins (PCDDs) andfurans (PCDFs).

5.8.11 Standard self contained breathing equipment should be worn whenfighting fires.

5.8.12 PCBs are listed in the International Agency for Research on Cancer(IARC) monographs (1982)-Group 2B and in the National ToxicologyProgram (NTP) Annual Report on Carcinogens (third).

5.9 FIRE REPORTING

5.9.1 Reporting Fires

All plant phones are equipped with a label that gives the number tocall (300) to report a fire as well as the fire assembly station foreach area.

To report a fire, dial 300 give the guard the following information:

Your nameThe telephone extension number you are usingThe fire assembly station printed on the telephone labelThe location of the fireAny additional important information such as know personalinjury or size of the fire

Stay at the extension so that the guard can obtain furtherinformation.

ARIOOJ*99

5.7.2 Storage Site Security : .1*' ' '•'-. '.• <*-'

The site security plan will be followed.

* The drum storage and the drum disposal areas are contained inconcrete floor steel frame masonry buildings and are barricaded andposted with yellow caution tape.

In the event that outside fire fighting help is requested, securethe gate and permit only fire, emergency, police, and fullyidentified volunteers onto plant property.

5.7.3 Site Fire Protection

Sites are equipped with sprinklers.

* Three hose houses with hydrants are adjacent to each area (a totalo f seven). . : • > • •

The two areas are separated by approximately 1/2 mile of plantbuilding so it is highly unlikely that a fire at one site.wouldspread to the other.

Both storage areas are in one story buildings which are used for noother purpose, and are not normal passage ways.

* No smoking is allowed in either storage area or outside of the areasor adjacent to the areas* '••

Both buildings are of steel frame-masonry construction.

Easy access is possible both by road and by walkway, into bothareas.

Both areas are at the 1st floor level.

5.8 HAZARDOBS* COMMUNICATIONS ^

5*8*1 Fire in the drum storage area or in the drum disposal area mayinvolve used lubricating oil and therefore may be very hot andvolatile.

5.8*2 Drums in these areas have been sampled but are awaiting analysisbefore disposal. All fires therefore may involve the combustion ofunknown and potentially hazardous materials.

ARI00500

of these areas are on fire, call the Front Royal Fire Department at 911immediately, then call the normal plant call list.

5.5 PROJECT SUMMARY

To eliminate the threat to public health, welfare, or the environment, due topotential exposure to hazardous substances, the potential for off sitemigration of hazardous substances, and the potential for fire, explosion, orspillage of waste from drums, the material and containers must be assembled,identified and properly removed from the site. Methods and procedures aregiven in individual project work plans.

5.6 SAFETY MANAGEMENT

5.6.1 The Site Safety and Health Plan vill be followed.

5.6*2 Fire fighting by Avtex personnel will be limited to flamesuppression and preservation of adjacent structures. Actual firefighting at these sites will be by trained members of the FrontRoyal Volunteer Fire Department.

5.7 SITE SECURITY

5.7.1 Responsibilities of Avtex Employee*

Stay away from all drum storage and drum disposal sites. It shallbe cause for immediate discipline (up to and including discharge)for any AVTEX employee to enter a drum storage or drum disposal areaexcept to place a drum or drums in the area, monitor the conditionof the drums, transfer the contents of one drum to another toprevent a leak, place a drum in a drum contained to contain a leak,or count drums for an inspection or inventory.

Report all fires in a drum storage or drum disposal area by dialing300 and report the problem to the guard giving the fire assemblystation number posted on each phone, the help needed, and your name.

Report all real or potential fire hazards to your supervisor.

Report all deficiencies in fire fighting equipment to yoursupervisor*

Read and understand Material Safety Data Sheet (MSDS) for PCB's(attached).

Know and observe all plant rules, safety requirements, warningsignals, and eplant property.signals, and emergency, police, and fully identified volunteer* -pnta _

A ill U U J U I

5.2.7 Emergency Phone Numbers.',.'• ' t, 'f':-'-

Emergency medical services: Gate Guard (703) 635-2141 extension 141Plant Dispensary 8 AM-4 PM extension 119Warren Memorial Hospital (703) 636-0333Ambulance service 911Police 911Poison Control Center (Charlottesville) (800) 451-1428

5.2.8 Directions to Hospital

Warren Memorial Hospital emergency room is located on Shenandoah Avenue. Turnright at the plant gate, proceed to the top of the grade, and make a left turnonto Shenandoah Avenue (2nd left). The hospital is on the right in the thirdblock. The emergency room entrance is clearly marked, and is the firstbuilding seen.

5.2.9 PCB Project Coordinator *

C. Kenneth Wagner11 Portsmouth RoadFront Royal, Virginia 22630

Home: (703) 636-2109Plant: (703) 635-2141 extension 110

T Plant Page: 72-358

5.2.10 Site Contact:

C* Kenneth Wagner, Vice President, Engineering: extension 110 (page72-358)Paul Malina, Utilities Engineer, PCB's Project Engineer: extension400 (page 72-409)

1 ,i5.3 SITE WORK ZONES

The temporary drum storage area is located in the northwest corner of theplant in an area previously used as a bale storage and shipping dock. It isadjacent to the rail road spur used for staple rail shipments.

The permanent drum disposal area is located on a curbed, grounded, sealedconcrete floor in the southwest corner of fl pulp storage.

5*4 AUTHORIZATION TO CALL FOR OUTSIDE FIRE FIGHTING HELP- i '. '. 4 ''!

If fire is reported at fire assembly station 542 (temporary drum storage),fire assembly station 514 (#1 pulp storage) or fire assembly station 511determine if drum storage areas are actually on fire. If the drums in either

i

ARI00502

5.2.2 Project Date* , \

Start Datet November 7, 1989

Finish Date: to be determined

5.2.3 Site Location

The Avtex Site i* located on the south side of Kendrick lane in Front Royal,Virginia. The site is bordered by Kendrick Lane on the north, a wooded areaon the east, West Main Street and Luray Avenue on the south, and the southfork of the Shenandoah river on the west. The site contains approximately 400acres.

5.2.4 Direction* to Site

Front Royal is serviced by interstate route 66, and by state routes 55, and340. Interstate route 66 has exits onto routes 55 east of Front Royal andonto route 340 north of the town. Route 55 west combines with rout 340 tobecome Royal Avenue; the major north/south road in Front Royal. Turning westonto 6th Street will lead directly into Kendrick Lane and to the Avtex Site.

5.2.5 Site History

Manufacturing of rayon fiber began at the Front Royal site in 1940 under theAmerican Viscose Corporation. Ownership was transferred to the FMCCorporation in 1963 (as the American Viscose Division of FMC Corporation andsubsequently the Fibers Division of FMC Corp.) In August 1976 Avtex Fiberswas formed from the fibers plants in that division. Approximately 300 workersare employed at the site. The principal product is rayon yarn for thecarbonizing industry*

5.2.6 Site Description

The Avtex Site consists of an approximately 400 acre fenced plant facilitysouth of Kendrick lane in Front Royal, Virginia. The Site is located on thesouth side of Kendrick lane in Front Royal, Virginia. The site is bordered byKendrick Lane on the north, a wooded area on the east, West Main Street andLuray Avenue on the south, and the south fork of the Shenandoah river on thewest.

The plant itself i* a steel framed, red brick building covering approximately62 acres of the site. Warehouse space and space for the polyester plant areprovided by green metal clad steel frame structures adjacent to and north ofthe original plant.

All drum storage areas are inside of plant buildings within the plantperimeter fence.

ARI00503

SECTION 5

, FIRE PROTECTION PLAN FOR DRUM .• STORAGE AND DISPOSAL AREA

5.1 PURPOSE

Because the Avtex Site contains a manufacturing operation which has beenreduced in scope by approximately 85%, many areas of the plant are nowabandoned. Lubrication supplies, cleaning supplies, and manufacturingsupplies in these areas are now waste. To eliminate the threat to publichealth, welfare, or the environment, due to potential exposure to hazardoussubstances, the potential for off site migration of hazardous substances, andthe potential for fire, explosion, or spillage of waste from drums, thematerial and containers must be assembled, identified and properly removedfrom the site.

Any entry onto a site potentially containing hazardous materials must be madewith caution. A safety plan for work performed in response to this order(Docket No. 111-90-01-DC) has been developed to ensure that all the hazards ofthe site are evaluated prior to entry. The Occupational Safety and HealthAdministration requires that a written safety plan be present on site and thatall personnel working on the site have read and understood the plan.

Because of the fact that the Avtex site includes an operating manufacturingfacility and because of the significant number of individual contractorsinvolved in removal activities, the focus of this safety management plan is todefine clearly those areas of the Avtex property involved in removal orassessment activities and to ensure that procedures are in place forsegregating those areas and defining where possible, any potential hazards inthose areas* Individual contractors have been made responsible for their ownsafety plans, and these are included in Appendix G to this plan.

Because the majority of the materials found are fuels, it is imperative thatevery reasonable precaution be taken to avoid the possibility of fire. If afire does occur, to avoid possible'threat to the general public, employees,and contractors of exposure to potentially hazardous materials, the provisionsof this plan must be followed. "-•''••'


5.2.1 Site Name and Address

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneFront Royal, Virginia 22630

(703)635-21A1 A R I D 050U


SECTION 5FIRE PROTECTION PLAN

FORDRUM STORAGE AND DISPOSAL AREAS

ADMINISTRATIVE ORDER BY CONSENTDocket III-90-01-DC

Prepared for U. S* Environmental Protection AgencyHazardous Waste Management Division

Region III

November 7, 1989

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneP.O* Box 1169


ARI00505


WORK PLAN

STATEMENT OF ACCESS TO PLANT

BYEPASection It I

EPAtnd/or their tmhorizedrcprcacntativcshavc (he authority tocnlcrtnd freely move about (be siteat ill reasonable foes. ThcymayinspectrccOTreview (be progress of Avtex in carrying out the terms of (he Order; conduct iodi tests ts EPA deemsnecessary; using camera, soundrecording or other documentary equipment; verify data submitted toEPA ty Avtex; tnd canying out any leqnfcejnents of (his order wliicn Avtex failstopropeily or inatanery manner complete. EPAmay copy all iccords, files, photographs, documents and otherwritings, includingall tamplingandmom'toringdata,

AVTEXHBERSFRC ritOYALINCdoesmalcetdaimtoBpsmessComldenlproass areas, ReKarch Projects in the yarn products areas, md the polypropykne nnmng area. Noinfonnationhasbeenrcquestediboutthesetreas. NorccordsordocumentstbouttbeKtreashavebeenwithheld.

AEMMSTOATIVE CREER

U. S. BaTTOnaul Protection A|mcy

Region in

AVTCXFffiERSFRONTROVALINC. ff D I n n r n rXoxftfcLsne A n l U U O U OP. a Box 1169

Ra*Rayit,VaginU 226X

AVTEX FIBERS FRONT ROYAL INC.AVTEX FIBERS SITS

SECTION 6SITE SECURITY PLAN



Region III

November 7f 1989

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneP.O. Bos 1169


ARI00507

SECTION 6

SITE SECURITY PLAN

6.1 PURPOSE

Avtex will prevent unknowing entry and minimize the possibility forunauthorized entry onto the portions of the Avtex facility site subjectto the conditions of this Order. In addition, to achieve maximumprotection, security will be extended to all areas within the facilityboundary .

According to the Administrative Order, EPA and/or their authorizedrepresentative shall have the authority to enter and freely move aboutthe site at all reasonable times for the purpose of, inter alia:inspecting records, operating logs, and contracts related to the site;reviewing the progress of the Respondents in carrying out the terms ofthis Order; conducting such tests as EPA deems necessary; using a camera,sound recording or other documentary type equipment; and verifying thedata submitted to EPA by the Respondents. The Respondents shall permitsuch persons to inspect and copy alt records, files, photographs,documents, and other writings, including all sampling and monitoringdata, in any way pertaining to work undertaken pursuant to this Order.Nothing herein shall be interpreted as limiting the inspection authorityof EPA under federal law, or Virginia under state law.

Although these provisions of the Order allow for unrestricted access tothe Site by USEPA personnel, Avtex cannot sacrifice worker safety.Therefore, Avtex will require that all visitors to the site underauthority of this Order, as well as Other personnel conducting removaloperations, adhere strictly to the regulations described in this generalSecurity plan.

flRI00508

A security plan specific for each project has been prepared by therespective contractor and is included as addenda to this plan.


6.2.1 PCB Project Coordinator

C. Kenneth Wagner11 Portsmouth RoadFront Royal, Virginia 22630

Home: (703) 636-2109Plant: (703) 635*2141 extension 110Plant Page: 72-358

6.2.2 Site Address:

AVTEX FIBERS FRONT ROYAL INC.Kendrick LaneFront Royal, Virginia 22630

6.2.3 Site Contact:

C. Kenneth Wagner, Vice President, Engineering: extension 110 (page72-358)Paul Malina, Utilities Engineer, PCB's Project Engineer: extension400 (page 72-409)

ARI00509

6.2.4 Location of Clean-up cites:

1. Compressor room roof: The area outside the powerhouse locatedon top of the compressor room. This area includes the concretetransformer pad as well as the roof itself.

2. Sub lA! The substation north of the corporate offices.3. Transformer storage area! An area located on the east side of

I 1 pulp storage* This area contains approximately 10transformers.

4. Polyster dock: An area on the north and east side of thepolyster building dock area. This area includes the dock andrail road track areas.

5. Storm Sewer: The manholes and connecting lines for thefollowing manholes: A10, All, A16, A17, A21, A22, A24, A26,A27, A28, A31, A33, A 35, A40, A41, A42, NA13, NA11, NA10, A43,and A44. The actual numbers may change as testing indicateseither a need for more testing or decontamination•

6. Any other sites found during the required site survey.

6.3 FACILITY DESCRIPTION .

The Avtex Site consists of an approximately 400 acre fenced plant facilitysouth of Kendrick Lane in Front Royal Virginia. The Site is located on thesouth side of Kendrick Lane in Front Royal, Virginia. The site is bordered byKendrick Lane on the north, a wooded area on the east, West Main Street andLuray Avenue on the south, and the south fork of the Shenandoah river on thewest.

The plant itself is a steel framed, red brick building covering approximately62 acres of the site. Warehouse space,.and space for the polyester plant isprovided by green metal clad steel frame structures adjacent to and north ofthe original plant. \ '

Front Royal is serviced by interstate route 66, and by state routes 55, and340. Interstate route 66 has exits onto routes 55 east of Front Royal andonto route 340 north of the town. Rout* 55 west combines with route 340 tobecome Royal Avenue; the major north/south road in Front Royal. Turning westonto 6th Street will lead directly into Kendrick Lane and to the AvtfJxDsftfff) C I n

All drum storage areas are inside of plant buildings. All drum storage areasand all PCB sites except the storm sewer'line and manholes between the fenceand the river, are within the plant perimeter fence.

6.3*1 Access to Avtex Site

Access to the site is controlled by a 24 hour guard post at the plant's onlygate and is restricted to employees of Avtex Fibers, contractors,subcontractors, railroad and trucking delivery and shipping workers, andfederal and state regulatory officers* Access to PCB sites and Drum StorageAreas is limited to workers and agency personnel required to be in thoseareas.

6.3.2 Barrier* to access

The unfenced portion of the plant property is bordered on the north byadjacent fenced industrial property, on the east by the plant fence, on thesouth by large industrial waste lagoons and a wooded field, and on the west bythe Shenandoah river.

6.3.3 Posted Sign*

There are no road ways into the unfenced portion of the plant property otherthan those which originate on Avtex property. The land along West Hain Streetand Luray Avenue have been posted with "No Trespassing" signs.

6.3.4 Telephone System

The plant working spaces are equipped with a standard telephone system whichallows point to point contact anywhere within the plant and through theswitchboard to an outside line. Many units are "9" enabled so that directoutside dialing is possible. The guard can be reached at extension 141, andin the event of fire or emergency at extension 300 which will be givenpriority.

6.3.5 Fire Signal

All plant spaces are equipped with a fire signal. This consists of a siren inworking spaces and a loud bell in office spaces* Workers are then directed bya light code system to go to a fire assembly station for fire duty. Everyphone is marked with the fire assembly station of that location.

6.4 PLANT ACCESS CONTROL

Access to the site is controlled by a 24 hour guard post at the plant'sonly gate and is restricted to employees of Avtex Fibers, contract/ ,] 005 I I

. ;••(;* , .fc*;Vsubcontractors, railroad and trucking .delivery and shipping workers, andfederal and state regulatory officers (and their contractors). Access to PCBsites and Drum Storage Areas is limited to workers and agency personnelrequired to be in those areas.

6.4.1 Procedure* for Visitors, Contractors, Employees

Entry will be allowed only to authorized persons who present properidentification:

active employees on the shift they are scheduled to work.active employees on overtime when cleared through the gate by asupervisor.all supervisory personnel.all authorized contractor employees.governmental employees only with an escort, unless authorized by avice president Mr. David Tousignant.emergency cervices personnel only when specifically called.retired Avtex employees and their families to visit the doctor orthe pharmacy.

6.4*2 Plant Security Procedures

6*4.2.1 Main Gate at Kendrick Lane: A guard will remain on duty at alltimes, 7 days a week, 24 hours a day.

6.4.2*2 Rear Gate on West Main Street: Shall remain locked.6*4*2.3 A roving guard will patrol all plant areas, the plant perimeter

fence, and PCB sites not under constant work. All problems andtrespass will be reported immediately to Mr* Kenneth Wagner.

6*4.2.4 Persons other than Avtex Employees and Contractor Employeeswhen in contractor supplied buses, are stopped at the gate andasked for identification. Each visitor is issued a plantvisitor's gate pass. Each visitor is asked for the name of theperson he is visiting and that person is call to escort thevisitor. Governmental agency personnel are held at the gateuntil an authorized person is available to provide escort.

6.4.2.5 Governmental agency personnel and government contact personnelon full time assignment at the plant, and who are aware of

. plant safety and health rules and restrictions may be grantedunescorted access to the facility.

6.4.2.6 It is the responsibilities of Avtex employees to stay out ofand away from all PCB sites. It shall be cause for immediatediscipline (up to and including discharge) for any Avtexemployee to cross marked PCB clean-up boundary withoutspecific authorization from the Avtex PCB Project Coordinator:C. Kenneth Wagner.

ARI005I2

6.4.4 PCB Site Security

6.4.4*1 Contractors will barricade off the entire work area at each PCBsite.

6.4.4.2 The perimeter of each site will clearly be posted with signsdirecting all non-authorized persons to stay out.

6.4*4*3 Contractors will promptly report all unauthorized persons tothe PCB Project Coordinator, or to Mr. Paul Malina.

6.4.4.4 Contractors will challenge unauthorized percons at the job siteand will direct them to leave their work area.

6*4*4*5 Contractors will prevent intruders with clear malicious intentfrom entering the work areas and will immediately notify theguard that trespassers are on plant property*

6.4.5- Authorization to Request Police Assistance

If, in the judgment of the gate guard or roving security guard on duty, it isnecessary to call for police assistance, to provide all reasonable precautionsto protect the public, workers, contractors, subcontractors and theenvironment from exposure to hazardous substances, he will dial 911-and askfor assistance, then call the plant duty person, and the Employee RelationsManager.

ARI005I3

"" "~ " " ' ' ' ' ' " ' " " ' " r

f

ALLIANCE0051


SECTION 7IDENTIFICATION, SEGREGATION, AND DISPOSAL OF HAZARDOUS WASTES

ADMINISTRATIVE ORDERDocket Ho. III-90-01-DC

Prepared for U.S* Environmental Protection AgencyHazardous Haste Management Division

Region III

November 7, 1989


Front Royal. Virginia 22630

RRI005I5

SECTION 7

IDENTIFICATION, SEGREGATION, AND DISPOSAL OF HAZARDOUS WASTES

This section consists of detailed plans of contractors and subcontractorshaving been assigned responsibilities for PCB removal and solvent-containingwaste drums. Work plans from Chemical Waste Management, INC., S.D. Myers,Inc. and subcontractors, and Alliance Technologies Corporation are included.

ARI005I6

AVTEX FIBERS FRONT ROYAL INC.AYTEX FIBERS SITE

WORK PUN

PLANTOIDENnFYÊOREGATE, AND DISPOSE

OF CERTAIN HAZARDOUS SUB STANCES

ADMMBTRAT1VE ORDER

0. Cartoutittl fioUetiox A eiqr

ATOX FIBERS F80HT ROYAL KG.

iiiii 22630

ARI005I7

AVTEX FIBERS FRONTROYAL INC. v JAVTEX FIBERS SITE ^

WORK PLAN

PLAN TO IDENTIFY, SECT EOATE, AND DISPOSE

OF HAZARDOUS SUBSTANCES IN DRUMSScctfoaSJAl

ADMHBTEAHVE ORDER

0. 0. Eivtoiautal Protwboi A«cv7

AVTEX FIBER! FROHT ROYAL INC.

P.O.Box 1169FroM Rojil, Wjiiii 22(30

/JRI005I8

Chemical Waste Management, Inc.Technical Servict. DivisionP.O. Box 96Sealston. Virginia 2254?703/775-9000

17 October 1989

Avtex FibersKendrick Lane, P.O. Box 1169Front Royal, VA 22630

Attn: Paul Ma line

Subj: Work Plan Schedule

Dear Mr. Kaline: i- • . ,Chemical Waste Management, Inc. (CWM), presents the followingwork schedule for your review.

I. Work Scope ScheduleA. Segregate/Stage waste drum for subsequent sampling/CWM

analysis for disposal approval.1. Commence 9/25/892. 90% Completion by 9/28/893. continue staging as drums are generated.

B. Soil Sampling for drum storage area (dirt base)1. Commence 10/2/892. Completion 10/25/893. Straggler drums will be sampled as received.

C. Liquid Sampling1. Commence 10/2/892. Completion 10/25/893. Straggler drums will be sampled as received.

D. Sample Analytical Turnaround1* Soil Sample (3)

a. Sent on 10/2/89b. Expect results/disposal decision by 10/23/89

ARI005I9

2. Liquid Samples

a. Sent on 10/10/89, 10/16/89, and 10/23/89 ,b. Expect all results/disposal decision by 11/9/89

E. Liquid Disposal

1. Commence 11/13/892. Completion 12/1/89

F. Drum Disposal1. Commence 11/20/892. Completion 12/8/89

G. Soil Disposal

1* commence 11/22/892. Completion 12/15/89

Should you have any questions or require additional information,please do not hesitate to contact me. Thank you for yourassistance in this matter.

Sincerely,CHEMICAL WASTE MANAGEMENT, INC.

iir leyGeneral Manager

encl (1)

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LegendStaoe nmim^ for Sampling

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13 Liquid Sampling

14 Soil Sample Sent

*4' Expect Soil Results

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JB1 Expect all liquid analytical results

/6 Liquid Disposal

£2. Drum Disposal

IB. Soil Removal ;

AVTEX FIBERS

FRONT ROYAL, VIRGINA

SAMPLING AND ANALYSIS PLAN

FOR DRUMMED WASTE MATERIALS

October 12, 1989(revised October 18, 1989)

ARI00522

TABLE OF CONTENTS

1.0 INTRODUCTION 1

2.0 SAMPLING PLAN 1V'

2.1 ORGANIZATION , 1

2.2 SAMPLE COLLECTION 1

2.3 SAMPLE CONTAINERS, PRESERVATION ANDHOLDING TIMES 7

2.4 SAMPLING EQUIPMENT DECONTAMINATION 7

2.5 QUALITY CONTROL PROGRAM 9

2.6 HEALTH AND SAFETY 9

3.0 SAMPLE CUSTODY AND DECUMENTATION 10

3.1 SAMPLE LABELS - 10

3.2 SAMPLE LOG BOOK 10

3.3 CHAIN OF CUSTODY RECORD 10

3.4 SAMPLE PACKAGING AND SHIPPING 11

3.5 SAMPLING PERSONNEL AND TRAINING 13

4.0 SAMPLE ANALYSIS 17

4.1 DRUMMED WASTE ANALYSIS 17

4.2 OFF-SITE LABORATORY ! 17

ATTACHMENT AATTACHMENT BATTACHMENT CATTACHMENT D

AR 100523

SAMPLINfl AND ANALYSIS PLAN

AVTEX FIBERSFRONT ROYAL. VIRGINIA

1.0 INTRODUCTION

The Avtex Fibers Site, located in Front Royal, Virginia, containsapproximately one thousand drums containing various chemicalsubstances including waste lubricating oil, acids and unknowns.This sampling and analysis plan details the methods chemical WasteManagement will use for collection and analysis of the drummedsubstances. These substances will ba characterized forcompatibility, consolidated and classified for off-site disposal.2.0 SMtPLINO PLAN

2.1 ORGANIZATION

Sample collection will be performed by CWM and/or itssubcontractors. One drum sampling team will be required for thisproject. This team will consist of a sampling supervisor and twosampling technicians. The sampling personnel will report throughthe sampling supervisor to the CWM Project Manager. Technicalguidance and support will be provided via a dotted line report tothe ENRAC Technical Manager. Tha sampling team will be responsiblefor tha collection, fingerprint characterization and documentationof all drummed waste samples. Their responsibilities will alsoinclude the shipment of samples for off-site analysis.2.2 SAMPLE COLLECTION

CWM will sample each drum at the Avtex Fibers site for the purposesof characterizing and consolidating the drummed substances for off-site treatment/disposal. This section describes the protocols CWMintends to use for sampling at the Avtex Fibers site. Specific CWMprotocols for tha sampling of drummed materials can be found inAttachment A.

A discrete sample of each staged drum will ba collected andcharacterized via fingerprint analysis (Sea section 4.0). Basedon tha results of this analysis and previous knowledge of the drumcontents, compatible drums will be composited for furthertreatment/disposal analysis. For those drums which are clearlymarked and for which the contents are previously known, onecomposite sampla par group of 20 drums will ba prepared. Forunmarked drums* one composite sample per group of 10 drums will bemade.

Site specific sampling protocols for unanticipated environmentalor wasta sampling will be submitted as the need arises.

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2.3 SAMPLE CONTAINERS. PRESERVATION AND HOLDINO TIMES

Figure 2-1 is a listing of required sample containers, preservationtechniques and holding times for all analytical parameters whichmay be associated with the Avtex Fibers site. Also included in thetable are the required volumes and number of containers for eachparameter and matrix. Sample containers, preservatives, volumes,and holding times will vary with organic drum samples due toobvious incompatabilities. Typically organic drum samples will becollected in 1/2 pint or pint wide mouth glass jars with teflonlined lids. These samples may or may not be cooled until aftereach composite is made. All sampling containers will be obtainedfrom a commercially available source of EPA-approved samplecontainers.

2.4 8AMPLINQ EQUIPMENT DECONTAMINATION

Due to the nature of tha drummed substances expected at the AvtexFibers site (i.e. high concentrations of organic material) it isanticipated that disposable sampling equipment will be used.However, in the event that sampling equipment is to be reused, thedecontamination methods described in this section will be utilizedto minimize cross-contamination between sampling events.BULK LOADS/DRUMS OP 8QLID3 OR WASTE PILES REQUIRING METALS.CYANIDE. 5ULPIDB AND/OR GENERAL SCREENING ANALYZES.

PROCEDURE

a) Wipe any excess sample from the sample equipment with eitherdisposable paper toweling or a wire brush.

b) Scrub the sample equipment with a warm detergent solution(Liquinox, Aloconx or Phosphate free detergent) and rinse withtap water.

c) Rinse the sample equipment twice with either distilled ordeionized water.

d) Wipe the sample equipment dry with paper toweling or allowthe sample equipment to air dry.

e) Proceed to next sampling location or protect sample equipmentfrom contamination during storage.

flRI00530

PnnMMl AH iMytf0v Mpf

_ .BULK LIQUIDS/DRUMS ••' OF SOLIDS OR WASTE PILES REQUIRINGPCBa/PESTICIDES. VOLATILE ORGANIC AND/OR SEMI-VOLATILE ORGANICANALYSES.

PROCEDURE

a) Wipe any excess sample from the sample equipment with eitherdisposable paper toweling or wire brush.

b) Scrub the sample equipment with a warm detergent solution(Liquinox, Aloconx or Phosphate free detergent) and rinse witheither distilled or deionized water.

c) Wipe the sample equipment dry with paper toweling.

d) Rinse first with nanograde hexane followed by a rinse withreagent methanol. Double rinse with either distilled ordeionized water.

e) Wipe the sample equipment dry with paper toweling or allowthe sample equipment to air dry.

f) Proceed to next sampling location or protect sample equipmentfrom contamination during storage.

BULK LOADS/DRUMS OF AQUEOUS WASTE REQUIRING METALS. CYANIDE•SULFIDE AND/OR GENERAL SCREENING ANALYSIS

PROCEDURE :• < ! •

a) Drain any excess sample into the original container (i.e.,tanker, drum, railcar, etc.).

b) Triple rinse the Bample equipment with a warm detergentsolution (Liquinox, Alconox or Phosphate free detergent).When using a colliwasa, withdraw the detergent solution anddischarge it into a container (drum) labeled "Waste Rinsate."

c) Rinse the sample equipment with nanograde hexane until thesampler is visible free of sample (minimum triple rinse).

" -f.

d) Rinse the sample equipment with tap water.

e) Triple rinse the sampling equipment with distilled ordeionized water. .

f) Proceed to next sampling location or protect the sampleequipment from contamination during storage.

ARI005318 "_________________ ...___________J_J__^^_^

BULK LOADS/DRUMS OF ORGANIC WASTE REQUIRING PCBS/PESTICIDES ANPCAL6RIMBTRIG ANALYSIS

PROCEDURE

a) Drain any excess sample into the original container (i.e.,tanker railcar, drum, etc.)

b) Triple rinse the sample equipment with a warm detergentsolution (i.e., Liquinox, Alconox or Phosphate freedetergent).

c) Rinse the sample equipment with nanograde hexane until thesampler is visibly free of sample (minimum triple rinse).

d) Rinse tha sample equipment with tap water.

e) Triple rinse the sampling equipment with distilled ordeionized water.

f) Proceed to next sampling location or protect tha sampleequipment from contamination during storage.

2.5 QUALITY CONTROL PROGRAM

Chemical Waste Management will collect and analyze Quality Control(QC) samples as part of the overall field sampling program at theAvtex Fibers sita. These QC samples will be analyzed by CWM and/orits subcontractors as an internal quality control check. Thefollowing will be considered individual matrices for determiningthe proper number of QC samples:

ODrum Samples

Tha following types of samples will be collected as part of thefield QC program:

O Duplicates - Duplicate samples at a frequency of ona duplicatefor avary 20 samples will ba collected at tha same time andsampling location, using tha same sampling methodologyemployed to collect tha original sample.

In addition to tha field QC program the CWM Technical CanterLaboratory will analyze QC samples as per their StandardOperating Procedures.

2.6 HEALTH ANP SAFETY

Specific requirements for personnel protective equipment/airmonitoring during sampling at the Avtex Fibers Site, are outlinedin tha Sita Specific Health and Safety Plan, Attachi&RtJ Q.Q 5 3 2

3.0 SAMPLE CUSTODY AND DOCUMENTATION

CWM will institute sample custody procedures at the Avtex FibersSite to ensure the integrity of the sample from time of collectionto analysis. The components of the sample c4. Custody procedurewill be sample labels, field logbooks and chain of custody records.The procedures for their use, is described as follows.3 • 1 SAMPLE LABELS : ,,

Sample labels will be affixed to sample containers prior to thetime of sampling. Sample labels will include the followinginformation:

OS ample Identification NumberOName of Sampler '. . ..'.•,"ODate and Time of SamplingOSampling Location©Preservative .OSample Type (i.e. - Grab or Composite)

All sample labels will be completed in black indelible ink.

3.2 CAMPLE LOG BOOKS

All information pertinent to field sampling will be recorded inlogbooks . Separate log books will be kept for each of thefollowing sample types:

ODrum Samples "

Each of these notebooks will be bound and contain consecutivelynumbered 8 1/2" x 11" pages. Entries in each notebook will be madein black indelible ink and will include the following:

OSample Identification NumberOSample Location -tOField ObservationsONumber and Volumes of Samples TakenOSample Type t •©Preservatives Used©Analysis RequestedODate /Time of Sampling©Sampler Name(s) >

3.3 CHAIN OF CUSTODY RECORD

To establish the documentation necessary to trace sample possessionfrom the time of collection, a chain of custody record (Figure 3-2) will be completed and will accompany every sample. Whentransferring the possession of samples, the transferee will signand record the date of transfer on the chain of custody, tacord.

10

Tha parson taking custody of the sample will raconcila theinformation on tha chain of custody record with that on tha samplelabel before signing and dating tha chain of custody. Tha originalchain of custody records will accompany tha sample and a copy willbe placed in the project file.

In addition, any samples sent to off-site laboratories by CWM willbe accompanied by a Sample Analysis Request Form (Figure 3-3).The usa of this form ensures that tha receiving laboratory has beennotified of pending sample shipment and provides additionalinformation as to the source of tha samples.3.4 SAMPLE PACKAGING AND SHIPPING

All samples requiring shipment to off-sita laboratories, will beshipped in accordance with appropriate DOT regulations.

Samples collected at tha Avtex Fibers Sita will, for the purposesof packaging and shipping, be considered hazardous substancesamples and will be transported according to the followingrequirements:a If tha hazardous substance in the sample is known or can ba

identified, tha sample will be packaged, labeled and shippedaccording to the specific instructions for tha material (ifit is listed) in the DOT Hazardous Materials Table (49 CFR172.101).

O If tha hazardous substance in the sample is unknown, 49 CFR172.402 (h) allows for the designation of hazard class basedon the shippers knowledge of the material and the selectionof the appropriate hazard class from 49 CFR 173.2 (as listedin Figure 3-4). CWM will, generally, ship hazardous samplesof unknown content as "Flammable Liquid" or "Flammable Solid"if tha hazard classification listed above these on Figure 3-4 (i.e. radioactive material, Poison A, flammable/non-flammable gas) can be eliminated. Sample categories listedbalow flammable liquid/solid on Figure 3-4 will generally notbe considered sinca classifying substances into thesecategories requires flashpoint testing (which is not requiredof most samples from this sita)*

Thus, unless tha sample is known to consist of material listedbalow flammable liquid/solid on Figure 3-4, it is considereda flammable liquid/solid and shipped as such.

SAMPLE PACKING AND SHIPPING PROCEDURESt

Sample Classified as Flam-nab la Liquid for Solid)

This procedure is designed to meet tha requirements for the"limited quantity1* exclusion for the shipment of flanaable liouids

11 " " -

and solids, as described in 49 CFR 173.118 and 173.153. Limitedquantities of flammable solids are defined as one pound net weightper inner container and not greater the 25 pounds net weight in the ,outer container. The procedure is as follows:

a) Secure sample jar lids with strapping tape or evidence tape.

b) Place sample jar in Ziploc polyethylene bag (one sample perbag) . Seal bag,

c) Place sealed bag inside metal can and cushion it with enoughnon-combustible , absorbent material (i.e. -vermiculite) toprevent breakage and absorb leakage .

d) Pressure close the can and secure the lid with tape.e) Place the following information, either handprinted or in

label form, on the metal can:

O Laboratory name and address.

O "Flammable Liquid, N.O.S., UN1993" or"Flammable Solid, N.O.S., UN1325".Not Otherwise Specified (N.O.S.) is not used if theflammable liquid (or solid) is identified. In that casathe name of the specific material is listed before thecategory (for example, Acetone, Flammable Liquid)followed by its appropriate UN number found in the DOTHazardous Materials ..Table .

f) Place the following applicable DOT labels on the outside ofthe can:

O "Flammable Liquid" or "Flammable Solid"

Also place "This Side Up" label on top of can.

G) Place approximately one inch of non-combustible, absorbent,cushioning material in bottom of a metal or equivalentstrength cooler.

h) Place one or more metal cans in cooler and place bags of icearound, among and on top of cans when applicable.

i) Fill the remainder of the cooler with packing material.

j) Place paper work in plastic bag and tape bag to inside lid ofcooler. T

k) Tape cooler drain shut, If applicable.

AR10053512

PntvM ail <ev)£iati papa*

1) Placa tha following information on tha outside of tha shippingcontainer:O Proper shipping nameo UN or NA numberO Proper DOT labelsO Addressee and addrassor

m) Print "Laboratory Sample" and "This End Up" clearly on tip ofthe shipping container. Place upward pointing arrows on allfour sides of the container.

n) Complete carrier provided bill of lading and hazardousmaterial certification form (if carrier does not provide this,use industry standard form). Include on this form:

O "Flammable Liquid, N.O.S., UN1993" orO "Flammable Solid, N.O.S., UN1325".O "Limited Quantity" (Or "Ltd. Qty.")O Net weight or net volume just after "Flammable Liquid,

N.O.S., UN1993" or Flammable Solid, N.O.S., UN1325."O Further descriptions. Such as "Laboratory Samples" or

"Cargo Aircraft Only" (if applicable).

o) After acceptance by shipper, tapa cooler with strapping tapeat two locations. Secure lid by taping, do not cover anylabels.

p) Affix numbered custody seals on from right and back left ofcooler.

q) Cover seals with wide, clear tape.

Samples Classified As Other Than Flammable Liquid (or Solid!

Any sample which can be classified as other than flammableliquid/solid (as according to Figure 3-4) will ba shipped accordingto the appropriate DOT regulations as sat forth in 49CFR.

3.5 SAMPLING PERSONNEL AND TRAINING

Chemical Waste Management will provide personnel for all samplingactivities required at the Avtex Fibers Sita.

In order to ansura tha compatency of the personnel who performsampling at tha Avtex Fibers site, Chemical Waste Management willinstitute a Sampler Training Program, whereby any and allindividuals involved in sampling at tha sita will be required tocomplete training in tha site specific sampling procedures asdescribed elsewhere in this plan. flR | 00536

13

FIGURE 3-2

CHAIN OF CUSTODY FORM

ARI00537

0Xha-s

2P8•mO£^

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^?lg5u0)5Q.wW

PM<H 00 B•H

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538

FIGURE 3-3

SAMPLE ANALYSIS REQUEST FORM

DATE:_________________ PRIORITY "1" _________ STD..

SITE: _________________

FROM:________________ PHONE: •________________

SUBJECT: SAMPLE .SHIPMENT

Please find ______________________ sample (s) sent for thefollowing analysis:

A telephone call to _______________ on

was made to confirm notification.

ADDITIONAL COMMENTS:

ARI0053915

FIGURE 3-4

DOT HAZARDOUS MATERIAL CLASSIFICATION (49 CFR 173.2)

1. Radioactive material

2. Poison A

3. Flammable gas

4. Nonflammable gas

5. Flammable liquid

6. Oxidizer

7. Flammable solid

8. Corrosive material (liquid)

9. Poison B

10. Corrosive material (solid)

11. Corrosive material (solid)

12. Combustible liquid (in containers having capacitiesexceeding 100 gallons)

13. ORM-B

14. ORM-A

15. Combustible liquid (in containers having capacities of100 gallons or less)

16. ORM-E

ARIOQ5i*016

4.0 SAMPLE ANALYSIS

4.1 DRUMMED WASTE ANALYSIS

Fingerprint characterization will be performed on or off site bythe sampling team. At a minimum, waste samples will becharacterized for the following properties. See attachment D forMethodologies.

pH RadioactivitySolubility in Water Physical AppearanceReactivity with Water Percent SolidsCyanide Screen IgnitabilityThe results of the fingerprint analysis and knowledge of thedrummed material will be used to consolidate compatible materialsfor disposal. Additional analysis will be performed onconsolidated material to further classify the material fortreatment/disposal. This analysis will be performed by CWM'sTechnical Center Analytical Laboratory, Riverdale, II. AttachmentB is a copy of waste profile form that will be completed foracceptance to the disposal facility. This form demonstrates thetest parameters that may be required for analysis.

4«2 OFF-BITE LABORATORY

Samples will be transferred to the CWM Technical Center Laboratoryon a daily basis,. A copy of their Standard Operating Proceduresand Quality Control Protocol are available for review upon request.

ARJOOSM17

ATTACHMENT A

CHEMICAL WASTE MANAGEMENT SAMPUNG PROTOCOLS

f*mt wi raeyciM PMW

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL KO. S DATE

SUPERSEDES NE «tf PACE 1 ef 7

,/ '///> DATE //I ?

SAMPLING OF SOLIDS AND

SEMI-SOLIDS IN DRUMS AND PAILS

ARI005l*3

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. g _____ DATB

SUPERSEDES N£ »/ PACE 2 of 7

APPROVAL riaLOL<b> DATE

X. 0 PurposaTo ansura that a representative saapla of solid or saai-solidwasta contained in drums or pails is taken.

2.0 ScopaThis protocol describes tha sampling of solid or semi-solidwastes contained in drums or pails. Tha objective is to collecta portion of wasta material small enough in volume to batransported and handled conveniently in tha laboratory whilestill accurately representing tha material that was sampled.

3.0 Responsibilities

3.1 Sampling Personnel

3*1.1 Shall ba diractly responsible for any equipment andtools usad during tha course of sampling

3.1.2 Shall ba responsible for notifying their immediatesupervisor of tha naad to replace equipment

3.1.3 Shall notify management of any discrepanciesancountarad

3.2 Sampling SupervisorShall ba responsible for purchasing sampling equipment

3.3 Laboratory Manager/Technical ManagerShall ba rasponsibla for davaloping a sita Specific Practicewhan th.is protocol is insufficient to covar all aspects oftha sampling avant.

4.0 Definitions4.1 Open-head drums - Drums from which tha antira lid can ba

removed by removing tha ring (also known as a ring-liddrum).

4.2 Bung-top drums - Drums that hava only a 3-inDhi flPpqiPfl intha top and a plug (bung) that screws into thVb£&xn%7

4.3 Combination drums - Drums froa which tha antira lid can bareaovad and which also hava a bung top opening.

AH I 00514it

CHEMICAL WASTE MANAGEMENT, INC* .PROTOCOL NO. g_____DATE

l) SUPERSEDES NEW PAGE 3 of 7

APPROVAL v /fli/C- DATE

4.4 Scoop - A davica that is of a size suitable for the quantityand siza of the particles to ba sampled. It is used fortaking small, equal portions at random spots near thasurface of tha waste material.

4.5 Concentric Tuba Thief (Grain Thiaf) - This device is similarto a split tuba thief. The grain thief has an inner movabletube. Both tha inner and outer tubes hava several openingsto allow free flowing solids to pass into tha inner tube.Tha thief is removed from the material and tha inner tubeemptied into a sample container (cee Figure A, Appendix I).

4.6 Soil Saapla Auger - This device is similar to a large drillbit with a handle. It is screwed or turned into thamaterial then pulled straight out. Tha saapla incraaant istakan from this extracted portion (sae Figure B,Appendix I).

4.7 corar (Split Tube Thiaf) - This device is a natal orplastic tuba (about 3/4-inch in diameter) from which about1/3 to 1/2 of the side of tha tube has been removed to forma slot along its antira length. Tha thiaf can be up to 4faet long and should have a sharp/ angled point at its lowerand (sea Figure C, Appendix I). A saapla will normally beraaovad fr.-m tha thiaf with a spatula or similar instrument(reamer) and placed in the cample container.

4.8 Drum - For this document, drum will mean any drum, pail orether non-bulk container.

4.9 Paperwork * tha site documentation which may include themanifest, Wasta Profile Sheet, MSDS and sita forms.

ARIOOSliS

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. S _____ DATE 6/24/P

SUPERSEDES NEW PAGE 4 of

APPROVAL y / r - DATE

5.0 Etc* pmant5.1 Choica of Equipment

Scissors,Tongs, Hammer Gloved

& Chisel Scoop Thiaf Auger Corar HandSolIda;

Powdery X X

Homogeneous X XHeterogeneous X X X

Compacted X XLarge chunks XMonolithic X

Semi-Solida:

Sticky X

5.2 Materials of ConstructionEach of tha sampling devices listed abova should baconstructed of materials which ara inert to any wastas whichmay ba encountered at a specific sita. These devices willusually be made of steal, aluminum, or plastic.

5.3 SCOOp

5.4 Concentric tuba thiaf (grain thiaf)5.5 Soil augar5.6 Corar (Split-tuba thiaf) and reamer

5.7 Hammer and chisel 4/7/00546

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 6 DATE g/24/flfi

... l SUPERSEDES^ && VV PACE S of 7

APPROVAL //-/flt'.'.My DATE (•'+

5.6 Sampling Tools and Accessories

Equipment needed to open drums and pails should, wheneverpossible, ba non-sparking (brass) and include, but not belimited, to the following:

(1) 2 Bung wrenches (one straight and one bent)(2) Medium and large screwdriver cat(3) 1/2" breaker bar(4) 1/2" ratchet(5) 1/2" spaed handle(6) 10" and 12" crescent wrenches(7) Vice grip pliers(8) Tool box : 5(9) Scissors or tongs

5.9 Rags or paper towels

5.10 Sample container with .cap and liner as specified by tha SPP' - - • • • ;-.•'-..• , :5.11 Indalibla black marker

5.12 Sample labels

6.0 Facilities t

6.1 Shelter should ba provided for sampling activities.6.2 Reference: Sampling Protocol No. 5

7.0 Sampling Procedure V?7.1 Review tha paperwork.

, - . '' ' - - •*= L="-= '9 ' "^ & " '

7.2 Collect tha sampling equipment and transport to tha camplingarea. ^

7.3 Visually inspect drums for integrity and proper labeling(note problems cuch as bulges or laakc) . Document containertypes and piece count and any diccrapanciac. Notify thesupervisor of any discrepancies,

7.4 Number all drums with unique identification. nnci7.5 Open each drum.

7.6 Inspect each drum for vie ibla liquid and any other obviousdiccrepancias . Document the findings.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO.

NEWSUPERSEDES PACE 6 of

APPROVAL ///?#,WX4,*- DATE

7.7 Sample each drum using appropriate device (Reference Section5.1).7.7.1 Scissors, Tongs, Brass Hammer, and Chisel - use as

needed.

7.7.2 Scoop - Scrapa asida tha surface layer of theaatarial to tha approximate depth of ona scoop. Takea scoopful and placa it with tha other scraped asidamaterial. Taka a second scoopful and placa it in thasample container.

7.7.3 Concentric Tuba Thiaf - Insert tha thiaf as far aspossible into tha drum. Rotate tha outer tuba toallow tha inner tuba to fill. Closa tha outer tubaand raaova tha thiaf. Pour tha saapla into thasaapla container.

7.7.4 Auger * Screw or turn tha auger into tha aatarial;than pull straight out. Transfer tha saapla to tha \ Jsample container with a spatula or other suitabledavica.

7.7.5 Corar (Split Tuba Thiaf) - Insert tha corar as far aspossible into tha drum, remove tha corar and transfersaapla to saapla container by pushing tha reamerthrough tuba.

7.7.6 Gloved Hand - Uca only whan no other means ofsampling is possible (a.g. filtar caka) and only withtha approval of tha sita safety officer for a givenwasta straaa. Sample as specified by tha SSP.

7.8 Cap tha saapla container. Clean tha outar surface and labeltha container appropriately.

7.9 Replace tha drum lid or bung and tighten.7.10 Usa sampling equipment repeatedly without dacontaaination

only within tha saaa wasta straaa.7.11 Placa disposables in appropriate wasta container.7.12 Dacontaainata reusable equipment accordjjrft J QQ gijpbocol

HO. 5. - - . . . . . . ^,

7.13 Transport tha samples to laboratory and log them in.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL K0._ g_____DATE 6/24/aa

SUPERSEDES NEW PACE 7 of 7Ay j ——————

APPROVAL //lfffi**<tM>

8.0 Compositing

Samples from a maximum of ten drums or pails of identical wastefrom one waste straaa may ba coapositad into one camplecontainer.

9.0 Corrective Action

Racampling may ba necessary.

APPENDIX Z

SAMPLZN3 BQBZWtZST

ARI00550

FIGURE AGRAIN PROBE

CONCENTRIC TUBE THIEF

Reference: ASTM E 300-86flRIO.0551

FIGURE BAUGER SAMPLER

Reference: ASTM E 300-86ARI00552

FIGURE CSPLIT TUBE THIEF

ORCORER

Reference: ASTM E 300-86flR'00553

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. f_____DATE 6/24/9P

SUPERSEDES NEW PAGE 3 of &

APPROVAL W/Wfl'fl** PACT

4.4 Combination drums - Drums froa which tha antira lid can beremoved and which also hava a bung top opening.

4.5 Empty drums - A container froa which all residua has beenreaovad is RCRA empty by practical aaans (contains lass than1" of rasidua in tha bottoa).

4.6 Glass tuba - A tuba which has a saall dlaaatar, normallyona-half inch or lass. Tha tuba yields a verticalraprasantation of a drum.

4.7 Coliwasa - A glass, plastic or aatal tuba with an endclosure that can ba opened and closed while tha tuba issubmerged in tha wasta to ba sampled.

4.8 Long-handled sludga sampler - This is a curved, hoe-liketool.

4.9 Paperwork - Tha sita documentation which may include themanifest, Wasta Sheet Profile, MSDS, and sita forms.

4.10 Drum * For this document, drum will mean any drum, pail, orother non-bulk container.

5.0 Equipment

5.1 Saapla containers, lids and liners5.2 Labels

5.3 Class tuba

5.4 Coliwasa5.5 Measuring stick

ARI00551*

i j

CHEMICAL WASTE MANAGEMENT, IKC. PROTOCOL NO. 7_____DATE S/2*/aa

SUPERSEDES N£ VV PAGE 4 ef 6

5.?. Saapling Tools and Accessories

Equipment needed to open drums and pails should, wheneverpossible, ba non-sparking (brass) and include, but not belimited, to tha following:

, ,(1) 2 Bung wrencr.es (one straight and one bent)(2) Medium and large screwdriver set(3) 1/2" breaker bar(4) 1/2" ratchet(5) 1/2" speed handle(6) 10" and 12" crescent wrenches(7) Vice grip pliers(8) Tool box(9) Scissors or tongs.

5.7 Indelible black markers5.8 Rags or paper towels ^

6.0 Facilities - Sea Protocol No. 5.

7.0 Sampling Procedure7.1 Review tha paperwork.

- - t- -' -7.2 Prapara and inspect tha necessary sampling equipment. The

sampling equipment must be clean, dry and free of anyvisible contamination. •

7 . 3 Visually inspect the Wasta containers for integrity andproper labeling (note problems such as bulges or leaks).Document container types and piace count and anydiscrepancies. Notify the supervisor of any discrepancies.

•

7.4 Number all drums with unique identification.7.5 Open each drum.7.6 Insert tha stick into each drum to determine its volume and

to determine tha presence and amount of solids at thabottom. Inspect tha stick as it is removed to characterizecontents. Document tha findings.

' AR 1 00555


SUPERSEDES NEW .PAGE 5 of_6

DATE

7.7 Saapla each drum7.7.1 Glass Tuba

7.7.1.1 Insert tha tuba vertically until it reachestha bottoa of tha liquid.

7.7.1.2 Cover tha top of tha tuba with tha thumb tofora a vacuua and carefully withdraw thetuba.

7.7.1.3 Allow tha contents of tha tuba to drain backinto tha drum. Repeat two times.

7.7.1.4 Taka tha sample and drain antira contentsinto tha saapla container.. Cap tha saaplacontainer, clean tha outer surface, andlabal tha container appropriately.

7.7.2 Coliwasa7.7.2.1 Open tha and valve.

7.7.2.2 Rinsa tha coliwasa three times by slowlyiaaarsing tha coliwasa (to tha bottoa of thacontainer) and fully withdrawing. Do notallow coliwasa to hit tha bottom of thecontainer vigorously.

7.7.2.3 To saapla, immerse tha coliwasa, with andvalva opan, to tha bottoa of tha container.

7.7.2.4 Close and valva of tha coliwasa."7.7.2.5 Withdraw tha coliwasa and drain entire

contents into tha saapla container.7.7.3 If solids ara present in tha drum, extend tha sludge

sampler into tha drum and scoop up tha solid likeaatarial. Remove tha saapla froa tha drum andtransfer tha saapla to a saapla container.

7.8 Claan tha outar surface of tha container. flR | 005567.9 Labal tha sample container and nota tha proportions of any

layers and/or solids.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 7_____DATE 6/24/88

SUPERSEDES NEW PAGE g of 6

_...._ APPROVAL

. 7.30 The cama tuba or coliwasa may ba used repeatedly withoutcleaning and decontamination or dicpocal only for the camewacta stream.

7.11 Decontaminate - reusable equipment according to Protocol No.5.

*7.12 Dicpoca of used rags and tubes in appropriate wacta

containers. NOTE: Tubes or colivacac chould not be dicpocedof in tha sampled drums.

7.13 Transport tha camples to tha laboratory and log in.6.0 Compositing

8.1 Samplac from a maximum of ten drums or pailc froa ona vactactraaa may ba composited into one cample container.

8.2 Drums with solids may not ba composited.

9.0 Corrective Action9.1 Racaapling may be necessary.

4RI00557


SUPERSEDES NEW

SAMPLING OF LIQUIDS AND

SLUDGES IN DRUMS AND PAILS

ARI00558

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 7_____DATE 6/24/88

t / SUPERSEDES NEW PAGE 2 of 6^——^ •'Vl . .A * /

APPROVAL '/tlf/l&uM* DATE_6/

1.0 Purpose

To ensure that a representative sample of sludge or liquid wastecontained in drums or pailc ic takan.

2.0 Scope

Thic protocol daccribes tha procedure for obtaining arcpracantativa cample of a liquid or cludga from a drum or pail.

3.0 Recponsibiliticc3.1 Sampling Perconnel

3.1.1 Shall ba directly responsible for any equipment andtools used during campling

3.1.2 Shall be responsible for notifying their immediatesupervisor of the need to replace equipment

3.1.3 Shall notify management of any discrepancies3.2 Sampling Supervisor

Shall ba responsible for purchasing caapling equipment

3.3 Laboratory Manager/Technical Manager3.3.1 Shall ba responsible for developing a Site Specific

Practice whan this protocol is insufficient to coverall aspects of tha campling avent

3.3.2 Shall ba rasponsibla for determining and approvingany compositing of camples

4.0 Definitions4.1 Individual Sample - A discrete sample that ic not mixed with

any cample takan froa another drum.4.2 Open-head drums - Drums from which the antira lid can ba

removed by removing tha ring (also known as a ring-liddrum).

4.3 Bung-top drums - Drums that hava only a 3-ittih/ fcpftsDLoiJ ini ; tha top and a plug (bung) that ccrawc into tha opening.

A'RI00559

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL HO. 7_____DATE 6/2A/aa

SUPERSEDES NE^V PAGE 1 of 6

SAMPLING OF LIQUIDS AND

SLUDGES IN DRUMS AND PAILS

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL KQ. j 7_____DATE g/24/BB

SUPERSEDES NEW PAGE 2 ef g' '

DATE &*

1.0 PurposeTo ensure that a representative sampla of sludge or liquid wastecontained in drums or pails is taken.

2.0 ScopeThis protocol describes the procedure for obtaining arepresentative sampla of a liquid or sludge from a drum or pail.

3.0 Responsibilities3.1 Sampling Personnel

3.1.1 Shall ba directly responsible for any equipment andtools used during sampling

3.1.2 Shall be responsible for notifying their immediatesupervisor of the need to replace equipment

i , 3.1.3 Shall notify management of any discrepancies3.2 Sampling Supervisor

Shall ba responsible for purchasing campling equipment

3.3 Laboratory Manager/Technical Manager3.3.1 Shall ba responsible for developing a Site Specific

Practice when this protocol is insufficient to coverall aspects of tha sampling avant

3.3.2 Shall ba responsible for determining and approvingany compositing of samples

4 . o Definitions4.1 Individual Sampla * A discrete sampla that is not mixed with

any saapla takan froa another drum.4.2 open-head drums * Drums from which tha antira lid can be

raaoved by raaoving tha ring (also known as a ring-liddrum) .

4.3 Bung-top drums * Drums that hava only a 3-tha top and a plug (bung) that screws into tha opening.

ARI 0056 I

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL KQ- 7_____DATE^6/24/aa

SUPERSEDES NEW PACE 3 of 6

APPROVAL /#rXr( i* DATE

4.4 Combination drums - Drums froa which tha antira lid can beremoved and which also hava a bung top opening.

4.5 Empty drums - A container froa which all residua has beenraaovad is RCRA empty by practical means (contains lass than1" of rasidua in tha bottoa).

4.6 Glass tuba - A tuba which has a small diameter, normallyone-half inch or lass. Tha tuba yields a verticalraprasantation of a drum.

4.7 Coliwasa - A glass, plastic or aatal tuba with an endclosure that can ba opened and closed while tha tuba issubmerged in tha wasta to ba sampled.

4.8 Long-handled sludge saaplar - This is a curved, hoe-liketool.

4.9 Paperwork * Tha sita documentation which may include thaaanifast, Wasta Sheet Profile, MSDS, and sita forms.

4.10 Drum - For this document, drum will mean any drum, pail, orother non-bulk container.

5.0 Equipment

5.1 Sampla containers, lids and linars

5.2 Labals5.3 Glass tuba

5.4 Coliwasa5.5 Measuring stick

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 7_____DATE 6/24/B8

i j SUPERSEDES N2 VV PAGE 4 of fi

, DATE

5.5. Sampling Tools and AccessoriesEquipment needed to open drums and pailc should, wheneverpoccibla, be non-sparking (braes) and include, but not balimited, to tha following:(1) 2 Bung wrenches (one straight and one bent)(2) Medium and large screwdriver set(3) 1/2" breaker bar(4) 1/2" ratchet(5) 1/2" speed handle(6) 10" and 12" crescent wrenches(7) vica grip pliers(8) Tool box(9) Sciccorc or tongs.

5.7 Indelible black markers5.8 Rags or paper towels

6.0 Facilities - Sea Protocol No. 5.7.0 Sampling Procedure

7.1 Review tha paperwork.

7.2 Prepare and inspect tha necessary sampling equipment. Thecampling equipment must be clean, dry and free of anyvisible contamination.

7.3 Visually inspect the vaste containers for integrity andproper labeling (note problems such as bulges or leaks).Document container •, types and piece count and anydiscrepancies. Notify the supervisor of any discrepancies.

•

7.4 Number all drums with unique identification.7.5 Open each drum. . ,;._ , - .7.6 Insert tha stick into each drum to determine its volume and

to determine tha presence and amount of colidc at thebottom. Inspect tha stick ac it ic removed tocontents. Document the findingc. fi n i

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL N0.___2_____DATE 6/24a

SUPERSEDE3 NEW PAGE 5 ef

* DATE

7.? Sampla each drum7.7.1 Glass Tuba

7*7.1.1 Insert tha tuba vertically until it reachestha bottoa of tha liquid.

7.7.1.2 Covar tha top of tha tuba with tha thumb tofora a vacuum and carefully withdraw thatuba.

7.7.1,3 Allow tha contents of tha tuba to drain backinto tha drum. Repeat two tiaas.

7.7.1.4 Taka tha saapla and drain antira contentsinto tha saapla container.* Cap tha saaplacontainer, clean tha outar surface, andlabal tha container appropriately.

7.7.2 Coliwasa7.7.2.1 Open the and valva.

7.7.2.2 Rinsa tha coliwasa three times by slowlyimmersing tha coliwasa (to tha bottoa of thacontainer) and fully withdrawing. Do notallow coliwasa to hit tha bottoa of thecontainer vigorously.

7.7.2.3 To saapla, iaaarsa tha colivasa, with andvalva opan, to tha bottoa of tha container.

7.7*2.4 Closa and valva of tha colivasa."7.7.2.5 Withdraw tha coliwasa and drain entire

contents into tha saapla container.7.7.3 If solids ara prasant in tha drum, extend tha sludge

sampler into tha drua and scoop up tha sol id 1 ikeaatarial. Remove tha saapla from tha drua andtransfer tha saapla to a saapla container.

7.8 Claan tha outar surface of tha container. ARI005647.9 Labal tha saapla container and nota tha proportions of any

layers and/or solids.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO.__Z_____DATE g/2*/fl8

: SUPERSEDES NEW PAGE 6 of fi

7.30 The came tuba or coliwaca may ba ucad repeatedly withoutcleaning and decontamination or disposal only for tha camewaste stream.

7.11 Decontaainata - reusable equipment according to Protocol No.5.

*7.12 Dispose of used rags and tubes in appropriate waste

containers* NOTE: Tubes or coliwacac should not ba disposedof in tha campled drums.

7.13 Transport tha camplas to tha laboratory and log in.8.0 Compositing

8.1 Samples froa a maximum of ten drums or pails froa ona wastectraaa may be composited into ona cample container.

8.2 Drums with solidc may not ba coapocited.9.0 Corrective Action

9.1 Resampling may ba necessary.

ARI00565

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO.____a___0ATz___fim/-

SUPERSEDES NEW PACE

SAMPLING OF BULK LIQUIDS

AND SLUDGES

CHEMICAL WASTE MANAGEMENT, INC.% PROTOCOL NO. 9 _____ DATE fi/24/aa

SUPERSEDES \\L\J PAGE 2 ef S

DATE

1.0To ensure that rcprecantativa samples are taken from bulk liquidsand cludges.

2.0 Scope

To outline tha procedure for obtaining a representative samplefroa a tanker truck containing bulk liquid and/or cludga.

3 . 0 Responsibilities

3.1 General Manager3.1.1 Shall be responsible for providing proper campling

equipment.

3*1.2 Shall ba responsible for providing caf a, convenientfacilities for the campling of bulk liquids/sludges.

3.2 Sampling Parconnel3.2.1 Shall be directly responsible for all equipment used

during the course of campling.3.2.2 Shall ba responsible to notify management of all

diccrapancias encountered.3.2.3 Shall ba responsible for notifying their immediate

supervisor of the need to replace equipment.3.3 Sampling Supervicor

Shall be rasponcibla for purchacing campling equipment.3.4 Laboratory Manager/Technical Manager

3.4.1 Shall be responsible for developing a Sita specificPractice whan this protocol is insufficient to coverall aspectc of the campling avant.

3.4.2 Shall be responsible for determining the maximumd.gr« or costing. ftRl00567

CHEMICAL WASTE MANAGEMENT, INC, PROTOCOL NO. 9_____DATE 6/2A/P*

SUPERSEDES NEW PACE 3 of

APPROVAL J7ffM IC QATE _6/~!?/?

4.0 Definitions

4.1 A coliwasa consists of a glass, plastic or aatal tuba withan and closure that can ba opened and closed while tha tubeis submerged in tha wasta to ba sampled. Tha coliwasa takesa proportional cross-sactional sampla of tha layers.

4.2 Paperwork - Tha sita documentation which may includemanifest, Wasta Profile Sheet, MSDS, and sita forms.

5.0 Equipment

5.1 Coliwasa(s)5.2 Two (2) aapty containers (i.e., 5 gallon buckets)

5.3 S-Hook5.4 Rags or papar towals5.5 Saapla containers5.6 Sample labels

5.7 Black indelible aarkar

6.0 Facilities * Saa Protocol No. 57.0 Saapling Procadura

7.1 Prepara and inspect tha necessary saapling equipment. Thesampling equipment oust ba claan, dry and fraa of anyvisible contaaination.

7.2 Carry tha saapling equipment to tha top of tha truck standor catwalk.

7.3 Usa special cara if a truck stand or catwalk is unavailable.7.3.1 Placa ona empty container (bucket) at tha base of the

tankar and placa tha coliwasa into tha bucket so thecoliwasa leans against the tankar.

7.3.2 Placa tha saapla container into tha other bucket.Carry it to top of tha tankar and placa it securelyon top of tha tankar.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 9_____DATE 6/2A/aa

. SUPERSEDES NEW PAGE 4 of 5r*

APPROVAL f/ V/ DATE h*'-?!

7.4 Slowly open the bleeder on hatch valves to release pressurein the tankar, if the hatch is not already opened.

7.5 Open tha trailer hatch slowly, so that any axcesc pressurewill be released.

7.6 Open tha cample container and place it in the bucket.7.7 Draw the sample .

: 'i' ' " i '

7.7.1 Take coliwasa and open the and valve.7.7.2 Rinca tha coliwaca three times by c lowly immersing

tha coliwasa to tha bottom of tha tankar and fullywithdrawing it. Do not allow coliwasa to hit thebottom of tha tanker vigorously.

7.7.3 Draw a cample by immersing tha coliwaca, with endvalva open, to the bottom of tha tankar and closing

, , the end valve of tha coliwasa.

7.7.4 Slowly withdraw tha coliwaca out of the tanker andralaace tha < antire contentc into tha camplecontainer.

7.8 Drain any residual material from tha coliwaca back into thatanker and wipe off any excess material with a rag or papertoval .

7.9 Replace the coliwaca in the bucket at the bace of tha tankarfor support.

7.10 Cap tha sampla container and wipe it claan. Place allsaapla materials, a.g., containers, rags, etc into thabuckat".

7.11 Close .and secure the tanker hatch.

7.12 Label tha sample container.7.13 Claan campling equipment using appropriate colvcnt (e.g.,

Mineral Spirits, 1,1,1 Tricloroethane, water).-' \ ~~- ii fc

7.14 Properly dispose of any contaminated rage/paper towalc intha designated waste container.

7.15 Deliver sampla containers to tha laboratory.7.16 Return saapling equipment to designated storage area.

CHEMICAL WASTE MANAGEMENT, INC, PROTOCOL NO. 9 _____ DATE

SUPERSEDES c n PACE S of

APPROVAL ?% /V*.. DATE L /1_I

8.08.1 Multi-Compartment Tankers - Draw a sampla froa each

compartment of tha tankar truck. Each saapla containerlabal oust indicate tha compartment number and tha volume ofaatarial tha compartment contains* Tha laboratory willcomposite samples if compositing is allowed.

8.2 Multi-Layered Load - Draw a saapla froa tha liquid and thasludga layar of a multilayered bulk load. Tha saaplaobtained should follow tha procedure as explained inProtocol No. 7 for saapling liquids and sludges in drums andpails.

9.0 corrective Action

Rasaapling, as directed by tha laboratory, aay ba needed.10.0 Precautions: .

Tha following precautions aust ba observed whan saapling:

10. 1 Apparent discrepancies in aanifasting, placarding, orhauler's permitting oust ba resolved bafora saapling.

10.2 Never leave any sampling equipment outside tha designatedarea whan it is not in usa.

10.3 Never laava hatches open unnecessarily (i.e., opan hatchesonly for tha tiaa required for saapling) .

10.4 Never reuse any protective equipment unless it has beaninspected and functions properly and tha rausa is sanctionedby the sita safety officer.

10.5 Navar reusa any saapling equipment unices it has beenproparly dacontaainatad and inspected for cleanliness.

10.6 Do not usa saapling equipment aada of polyvinyl chloride forsaapling katonas, tatrahydrofuran or dime thy Iformamide.

10.7 Do not laava any sample (s) in tha laboratory unless it isproparly labeled and logged in. AH I 00570

CAUTION: Positive prassura in tha tank aay causa injury. \

CHEMICAL HASTE MANAGEMENT, INC. PROTOCO*I NO..DATE_6/24/88

SAKPtING OF LIQUIDS AND

SUSPENDED MATERIALS IN STATIONARY TANKS

ARI0057I

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 10 DATE «/2yaa

SUPERSEDES NEW PAGE 2 of fi

APPROVAL ffl ffa* <

1.0 P»rposs

To ansura that representative samples ara taken of wastescontained in stationary tanks.

2 . 0 Scope

This protocol describes tha procedure for obtaining samples ofliquid and suspended wasta contained in stationary tanks.

3 . 0 Responsibilities3.1 Saapling Personnel

3.1.1 Shall be directly responsible for any equipment andtools used during saapling

3.1.2 Shall ba responsible for notifying their immediatesupervisor of tha naad to replace equipment

3.1.3 Shall notify management of any discrepancies

3.2 Saapling SupervisorShall ba responsible for purchasing sampling equipment

3.3 Laboratory Manager/Technical Manager3.3.1 Shall ba responsible for developing a Sita Specific

Practice whan this protocol is insufficient to coverall aspects of tha saapling event

3*3*2 Shall ba responsible for determining and approvingany compositing of samples

4.0 Definitions

4.1 Weighted Bottle - This sampler consists of a glass orplastic bottle, weight, removable lid, and lina built to thaspecifications in ASTM, Methods D 270 and E 300 (SeeAppandix I), or a similar commercially available device.

4.2 Cavitation - Formation of partial vacuum in JaniklpUff 'as aresult of tha passage through it of a swiftly moving solidbody such as a propeller blada.

4.3 Eduction * Process of conducting a fluid away from acontainer (such as oil froa a tank).

fl«IOOS72

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 10 DATE 6/24/88

SUPERSEDES Ng M PAGE 3 of fi

APPROVAL //£.$*• fu** DATE 6/!

5.0 Eytpntnt5.1 Saapla containers5.2 Weighted bottle or Bacon bomb-type (Reference Appendix I)5.3 Bucket or similar container5.4 Rage or paper towels5.5 Label c and indelible black markers

6.0 Facilities - see Protocol No. 56.1 Sea Protocol No. 5

7.0 ProcedureSelection of campling method ic determined by the configurationof the tank to be sampled, Ona of tha following four methodschould be ucad.

7.1 Mechanically- mixed tank samplingTanks with mechanical mixers are used primarily for blendingand ctorage of materials of different compositions that alsohava slightly soluble dr suspended matter pracant that willracolubiliza or rasuspend upon mixing. Under normalconditions, tha mixing process can homogenize a tank so thata cingla point saaplc from a campling port on tha eide oftha tank can ba takan with a high degree of certainty thattha cample is raprasantative of the material in the tank.7.1.1 -Allow the tank to adequately mix prior to sampling.

Tha mixer on the tank should be on for a minimum ofthirty (30) minutes before a saapla is taken.

7.1.2 Placa a bucket tinder tha saapla port. Open tha valveand allow at least three times tha saapla port volumeto flow through the saapla port.

7.1.3 Place a suitable saapla container under tha sampleport.

AR 100573« , 7.1.4 Open tha valve and fill tha saapla container.7.1.5 Close tha saapla valva.7.1.6 Cover and claan cample container.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL WO. 10 DATE

SUPERSEDES "&" PAGE 4 of 6

APPROVAL

7,1.7 Labal tha container.

7.1.8 Placa excess aatarial froa tha bucket into anappropriate drua for recycling.

7.2 Multi-point saapling

Multi-point sampling involves taking samples from severalpoints of tha tank using sample ports installed verticallyalong tha height of tha tank. These samples can beanalyzed individually to certify homogeneity or can becoapositad to obtain a full tank assay (Sea Section 8.0).7.2.1 Select sample parts on tha tank that will giva you

tha bast vertical section of tha tank. Taka a sampletakan from each of tha top, aiddla and bottoa of theliquid in tha tank at a ainiaua. Ba sura samplestakan from these locations ara labeled as such.

7.2.2 To -take tha saapla, follow steps 7.1.2 through7.1.8.

7.3 Weighted bottle sampling

Tha weighted bottla is used to obtain liquid and free-flowing slurries froa tha top of large stationary tanks. Asampla must ba takan from at least four (4) points; a topsaapla no aora than six (6) inches froa tha surface, anuppar saapla, a aiddla saapla, and a lowar saapla.7.3.1 Clean tha bottla, bottla assembly, and inspect line

for wear or dafacts.7.3.2 Assemble weighted bottla sampler.7*3.3 Lowar sampler to tha correct depth (saa the SSP)7.3*4 Opan tha lid and allow bottla to fill completely as

avidancad by tha cassation of bubbles.7*3.5 Raisa tha sampler, placa cap on and wipe off with a

disposable cloth.7.3.6 Pour saapla into appropriate saapla contain&ftajiflflC7/...... labal. • '

Ml 00571*

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 10 DATE fi/24/aa

SUPERSEDES N£ vV PAGE S eg fi/ ^ . . •

APPROVAL./7r//W!iy?' DATE

7.4. Sampling tanks with recirculation loopsTanks with recirculation loops can provide accurateraprccentativc camples by obtaining aatarial from a sampleport on the recirculation lina. This method applies to bulkliquids and pumpabla clurriac only.7.4,1 Allow tha tank to mix adequately. At least half the

volume of tha tank should be circulated prior tocampling.

Note: It ic recommended that the pump suction point ba neartha bottoa of the recirculation tank. This minimizespump damage due to cavitation. Tha pump dischargeshould ba through an aduction cyctaa elevatedslightly above the bottoa. Eduction cpeedc themixing process, and a ring of aductorc gives moreavan mixing to all parts of tha tank. Tha volumecirculated ic determined by dividing tha volume inthe tank by tha pump rate. Adequacy of the mixingsystem may ba determined by taking multipleanalytical samples over a period of time. Therasultc are then plotted to chow at what time the•implec become consistent. ASTM method E 300 is a»afsrence for cample port design.

7.4.2 Protect tha campling araa to maintain sampleintegrity.

7.4.3 Follow tha ctaps in mechanically mixed tanks,Sections 7.1.2 through 7.1,8*

7.5 Decontaainate all non-disposable campling equipment.7.6 Transport tha camples to the laboratory and log in.

8.0 Compositing8.1 With tha approval of tha Laboratory Manager/Technical

Manager, tha individual sample points may ba combined into asingle cample container if tha individual camples are ofequal volume and if the antira volume of aach cample iccombined into a single cample container. nr-ic

8.2 Only samples from the same stationary tank may becomposited.

CHEMICAL WASTE MANAGEMENT, INC. pROTOCOL NO. jQ _ _ r

SUPERSEDES N£ __

APPROVAL fflerf*,.-T f i'r i r*

9.0 Corractiv. Action

, as dir.ct.d by th. laboratory, may b. n..ded.

ARI00576

I APPENDIX X

SANK LEVEL SCHEXE

flRI00577

i UTW (I OUMT)

WEIGHTED BOTTLES

^ft/00578TANK SAMPLE LEVELS

Ptgt 1 of 2

I—CHAIN

*«»

AletnuelTtt eo eh« v«ljhc«d hotel* - from AS1X E300

ARI00579

P«gt 2 of 2


SUPERSEDES

SAMPLING OF

PONDS, LAGOONS,

AND SURFACE IMPOUNDMENTS

flfiiooseo

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL KQ. 11 DATE 6/2*/aa

SUPERSEDES PAC£ 2 pf

APPROVAL VUS-SATE 4 /^

1,0To ensure that representative camples ara taken of the liquidstrata and/or bottom sediments from ponds, lagoons, and surfaceimpoundments.

2 . 0 ScopeTo provide sufficient data for tha generation of Sita specificPractices (SSP) that will ensure tha collection of representativecamplec of a curfaca iapoundaent cuitabla to meat tha physical,chemical and regulatory objactivac. Sea Section 10.0.Recponsibilitias

General Manager3.0

Designate the individual (s) responsible for generating theSita Specific Practices (SSP) and ultimately responsible forcampling. •

3.2 Laboratory Manager

3.2.1 Generate the SSP or assist the individual sodesignated by the General ..anagar in the SSPgeneration.

3.2.2 Determine tha minimum volume of cample that must becollected in order to run all the desired analyses,allowing sufficient volume for duplicates, fortifiedsamples and reanalyses.

3.2.3 Determine container preparation and sample handlingauch as sample splitting and preservation. SeeProtocol No. 4.

3.3 Safety OfficerProvides tha safety requirements for sampling the CWMSampling Protocol a.

3.4 Sampling PersonnelPerform tha eaapling as required by the ssft Ra g Qt§§ |CWMSaapling Protocols*

All 00581

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL MO* 11 DATE 6/24/aa

SUPERSEDES NEW PAGE 3 of

APPROVAL_Jflf'ffl&JL1&' DATE _

4.0 Definitions4.1 Surface lapoundaant - for tha purposes of this document any

pond, lagoon, or other opan in-ground or above-groundsurface unit used as aaans of receiving, collecting,storing, or treating liquid .

4.2 Watar/Wastawatar Pond - surface impoundment receivingtreating, and storing wastawatar or traatad or untreatedwatar. Such ponds ara generally shallow enough to provideaarobic conditions throughout and ara used forclarification.

4.3 Procacs Pond or **Fac Pond11 - surface impoundment receivingand treating wastawatar which is known to ba non-hazardousand does not exceed any criterion for EP Toxicity. "Fac" isshort for faculativa and rafars to a treatment pond d««penough that anaerobic conditions persist at tha bottom foranaerobic traataant of wastes.

5.0 Equipment

Tha following ara recommendations of sampling equipment that mayba used for sampling surface impoundments, depending on thesampling avant objectives:

5.1 Grab sampla equipment - access froa shora (bara), dock orplatform5.1.1 Saapling valva or pump discharge of material being

transferred into or recirculatad within theimpoundment

5.1.2 Dippar (a.g. bottla affixed to and of rod, chain,rope)

5.1.3 Weighted bottla or Bacon bomb5.1.4 conduit or other axtandar and duct tapa

5.2 Multiple location saapla equipment for a nonhazardouc ornon-corrosive liquid containing impoundment, as defined bytha corporate Health and Safety SOP 1325.3.1 Rowboat with oars or electric5.2.2 Dippar at specified locations (a.g. grid locations as

specified in tha SSP

AS 100582

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO- li DATE g/24/88

SUPERSEDES NEW PAGE 4 of .O

tu* DATElr

5.2.3 Weighted bottla, VanDorn sampler or other suchsampler that allows closure of tha device at aspecified liquid level

5.2.4 Hand-operated Clam shell or other cludga sampler forobtaining bottom sludge samples - exact device willdepend on consistency of cludga

5.3 Multiple location sampla equipment for campling a corrosiveor hazardous liquid contained in an impoundment or unit thatcontains sludge with no bearing strength chould utilize araaota means, such as a crane, equipped with:5.3*1 Claa shall ^5.3.2 Bucket sampler5.3.3 Corer

5.3.4 Dippar5.4 Sample Containers

5.4.1 Appropriately •sized glass or plastic bottles forgeneral camples

t '',: "'

5.4.2 VOA vials and Oil t Grease bottlec (to be filleddirectly during sampling ac appropriate)

5.4.3 Appropriately preserved glass or plastic bottles forspacific water camples

5.4*4 .Coolers and ice or blue ice packc5.5 Safety equipment and FPE raquiramentc will vary widely

depending on tha type of campling and tha physical/chemicalhazards of tha material in the surface impoundment. The

. Health and Safety Officer or equivalent should specify therequired safety equipment for a given sampling event. Inaddition to tha more routine PPE and safety equipment, lifajackets, two-way radios, safety harnesses and lifa lines mayba required.

6.0 Facilities - Refer to CWM Protocol 15 An I 0058 J

7.0 Sampling Procadura ,

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 11 DATE 6/24/8?

SUPERSEDES_NEW PAGE_5 of lo""*

APPROVAL

7.1 Preparation for saapling7.1.1 Maka arrangamants for any large sampling equipment

(crana, boat, ate.) to ba assembled at sampling sita.7.1.2 Collect tha containers that ara to ba usad in the

fiald for saapling including tha bottles for anyparameter that must ba filled directly during thesaapling avant (and not split off froa tha mainsaapla afterwards) such as oil and graasa and VGA.If a fiald blank is necessary it should ba preparedat this tima.

7.1.3 Load sampla containers (in carrier), samplingequipment, and safety equipment into transportvehicle. Ba sura to include fiald -blanks (if used)with sampla containers and a fiald nota book.Transport equipment to tha saapling sita.

7.1.4 Notify any necessary aanageaant of saapling activity(e.g., Shift Supervisor) as par SSP.

7.2 Tha Sampling Evant7.2.1 Prepare all appropriate PPE and safety equipment.7.2.2 Arrange saapling equipment and containers for usa.7.2.3 Procaad with tha specific saapling avant dictated by

tha SSP.7.2.4 Nota any pertinent observations during sampling in

fiald notebook (a.g. presence of an oil sheen on tha•pond, odor, variations in color).

7.2*5 Placa VOA samples and any other specified samples intha coolar with ica or blua ica packs.

7.2.6 Transfer tha samples to tha laboratory for analysisand/or preparation for shipment*

7.2.7 Return all cafaty equipment (a.g. safety harnesses,lifa jackats) to propar storaga plac ft 100584

7.2.8 Properly dispose of any contaminated PPE anddisposable saapling equipment according to tha SSP.

7.3 Specific saapling equipment

CHEMICAL WASTE MANAGEMENT, INC* PROTOCOL NO. 11 DATE

SUPERSEDES NEW PAGE 6 ef 10

i DATE

7.3.1 Dipper7.3.1.1 Assemble dipper by bolting the adjustable

clamp to the pole. Place beaker in clampand fasten chut (cee Figure C, Appendix I) .

7.3.1.2 Turn dipper co tha mouth of tha beaker facesdown and insert into wasta material. Turnbeaker right side up when dipper ic atdesired depth. Allow beaker to fillcompletely ac shown by tha cacsation of airbubbles .

7.3.1*3 Raise dipper and aapty the contents backinto the pond.

7,3.1.4 Rinse the dipper 2 more times.7, 3.1. 5 Collect the cample ac in 7.3.1.2, raise tha

dipper, and transfer tha cample to the(j sampla container.

7.3.1.6 Close the bottla and claan the outside oftha container.

7.3.1.7 Attach the labal and complete tha requiredinformation.

7.3.1.8 Wipe the sampling 'equipment dry with rags,paper towels, ate.

7.3.2 "Transfer" grab sample'.;- ' ' 1 1 '• t , - * - '-

.If transfer from tha surface impoundment is inprogress, a grab sampla may be taken from tha pumpdischarge. Then follow steps 7.3.1.2 through7*3.1.8. K ,

7.3.3 Van Dorn Sampler7.3.3.1 To activate tha Van Dorn sampler, pull out

i tha and seals and maintain them in the openposition by attaching the retaining viree totha pins on tha top of tha sampler(saa Figure B, Appendix fltjfj. I 00585

7.3.?.2 Lowar the sampler to about oTieufoot belowthe surfaca to obtain tha top cample.

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 11 DATE g/24/aa

SUPERSEDES NEW PAGE 7 of lf

DATE ''"

7.3.3.3 Sand tha messenger waight down tha samplerropa. Whan tha weight hits tha top of thasampler, tha retaining wiras will releaseand tha ands of sampler will snap shut.

7.3.3.4 Raisa tha full sampler and return it to theboat, deck, or platform.

7.3.3.5 Position tha sampler ovar tha composite jar.Pull out ona and of tha sampler and allowsome of sampla to flow into tha jar.

7.3.3.6 Rinsa tha jar with tha sampla and dump itoverboard . Rapaat rinsing of j ar andsampler two aora times.

7.3.3.7 Refill tha saaplar as needed and fill thesampla container using tha total volume oftha sampla each time.

7.3.3.8 Proceed with staps 7.3.1.6 through 7.3,1.8.7.3.4 Weighted Bottla or Bacon Bomb

7.3.4.1 Assemble the weighted bottla sampler (SeeFigure A, Appendix I) .

7.3.4.2 Lowar tha sampler to tha required depth andpull out tha bottla stopper by jarking thelina.

7.3.4.3 Allow bottla to fill completely as evidencedby cassation of air bubbles.

-7.3.4.4 Withdraw tha saaplar.7.3.4.5 Empty contents into pond.7.3.4.6 In tha same fashion, rinse tha weighted

bottla sampler twica more.7.3.4.7 Collect a saapla following steps 7.3.4.2 *

7.3.4.4 and transfer tha contenta ftt»r £ csaapla container. «« 1 UTTDffb

7.3.4.8 Proceed with staps 7.3.1.6 through 7.3.1.8.

7.3.5 Claa Shall

JUHOQ586

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL KO.^ 11 DATE g/24/88

i j ;.•* SUPERSEDES NEW PAGE 8 ef 10

APPROVAL yjfrW.tCPATE & «*V £$.

7.3.5.1 Assemble the claa shell.

7.3.5.2 Lower the claa shall all tha way to thebottom.

7.3.5.3 Activate tha closure mechanism.7.3.5.4 Raise the claa shall.7*3.5.5 Transfer the sampla to the sample container.7.3.5.6 Proceed with steps 7.3.1.6 through 7*3.1.8.

8.0 Compositing8.1 The degree of compositing will ba dictated primarily by the

site's permits as explained in tha SSP. Tha laboratorymanager will determine the maximum degree of compositingbased on analytical considerations.

. 8.2 The compositing will be specified in the SSP and may be""- vertical and/or horizontal.

9.0 Corrective Action 'Corrective Action may involve resampling using tha originalcampling techniques or different ones as directed by thaLaboratory Manager.

10.0 Sita Specific Sampling Plan (SSP)10.1 An SSP must ba generated for each saapling event.10*2 Tha SSP mist address tha goal of tha saapling event, such

Mt • " ' - ".V V-'.:1.'. •"

10.2*1 To perform a daily spot chack for a limited number ofparameters in a process lagoon

10.2.2 To qualify the pond for discharge in compliance witha discharge permit

10.2.3 To characterize the unknown contents in a lagooninvolved in a remedial cite • p t Q 0 5 8 7

. 10.3 Tha SSP must address, at a minimum, tha following issues:

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO. 11 DATE 6/24/aa

SUPERSEDES NEW PACE 9 of

APPROVAL

10.3.1 Physical stata - liquid, solid, sludga or multiplephases

10.3.2 Volume of tha impoundment

10.3.3 Hazardous properties of tha materials in theimpoundment for safety considerations

10.3.4 Composition of tha aatarial - historical informationon processes involved and any available pastanalytical data will ba helpful in identifying thecomponents and tha homogeneity/stratification of theaatarial

10.3.5 Accessibility - A satisfactory daily grab samplemight ba obtained easily froa a pump discharge orraeirculation lina. Access to a pond of non-hazardous material aight ba obtained via a row boat.Access to a hazardous wasta lagoon aight ba limitedto . shore access and the usa of an extended rodsampler or a mechanical saapling davica such as acrana and a claa shall. Refer to specific facilitySOP's for access to controlled areas.

10.3.6 Sita permits, Wasta Analysis Plan, approvals, consentDaeraes, regulatory requirements, as appropriate

10.4 Tha SSP will specify, at a minimum:10.4.1 Tha saapling avant location(s)10.4.2 Tha number of samples to ba takan, for example: One

daily grab sampla may ba sufficient for processmonitoring. This saapla is generally obtained from apump discharge whila tha operation or a transfer isin progress; or, it aay ba obtained diractly froa theimpoundment using a dippar where physical accessallows. For a aora extensive saapling plan, theoptiaua number of random samples may ba determinedstatistically basad on preliminary astiaatas, theaaan, tha variance and knowledge of thecontrol/action liait of tha contaainant.(4L n ofconcern. Rafar to SW-846 for description.! UQjOO

10.4.3 Typa(s) of samples to ba takan, taking into accounttha following:10.4.3.1 Vertical or horizontal stratification

AR100588

CHEMICAL WASTE MANAGEMENT, INC. PROTOCOL NO!

SUPERSEDES NEW PACE 10 e, 1ft

APPROVAL^ ?//**, .tr • PATg /. /• ./? i?

10*4.3.2 Preliminary data and site history10.4.3.3 Sampling objectives

10.4.3.4 Degree of compositing, in the fiald or inthe laboratory

10.4.3.5 A three-dimensional grid system for eachpond or other impoundments to be used toidentify where each sample, including eachcubsample in a composite, ic obtained.

flRI00589

APPENDIX Z

SAMPLING EQOIPMZNT

/1RJ00590

FICORE A - WEIGHTED BOTTLSS

FICTOI B - VAN DORM SAMPLER flRI0059|

ii3 /IRI00592

FIGURE C - DIPPER

ATTACHMENT B

WASTE MATERIAL PROFILE SHEET

ARI00593

PMNM M fMtdM MOM

Chemical Waste Management, Inc.GENERATOR'S WASTE MATERIAL PROFILE SHEET

PLCASI PRINT IN INK Oft TYPI (HIM. 12-pttch).

af-- I •' 73730.Waste Profile Sheet Code

CWM Location of Original;,—-_________ (SHADED AHEAS POM cwu usa ONLY) CWM Sates Rep. <h

A. GENERAL INFORMATION1 Generator Name: —————————————————————————2.3. Facility Address: —————————————————————————— 4.

S. Zip Code:7. Title: ______________ 8. Phone: (

B. MAIL CHEMICAL WASTE MANAGEMENT, INC. INVOICES TO 1. G Generating Facility (A. above), or2. Company Name: ______,——-——-—.————————-————————————— 3. Phone: { )

5. Zip Code:

3. Is this waste a Oioxin listed waste as defined in 40 CFR 261.31 {e.g.. F020, F021. F022. F023, F026. FQ27. or F026)?G Yes G Ko lfyes.DONOTCOMPLETEthfsform.ContactyourChefnicalWasteManagement.tnc.uiesrepresentativeforai*ittance.

O. PHYSICAL CHARACTERISTICS OP WASTE . .t fVtlnr 9 Oo*< '!** waste have a

stron j incidental odor?CNo D Yes If known.riM-rh*

j. Physical State 1$ 70* F;G Solid G Semi-SolidG Liquid G Powdernth«r

4. Uyers.D MultilayeredG Bi-layeredG Single Phased

5. Specific Gravity:

Range:

6. PfSttiqudvG Yes U Nn

Volume: . j

.J NAp J _. . .

8. Liquid Flash Point: Q < 73* F Q 73-39* F Q 100-139'F Q 14Q-199'F Q i 200'F Q None Q Closed Cup GOpenCup

E. CHEMICAL COMPOSITION RANGE1. MIN. • MAX.

atflt4L

H

_. ., .: .. . . „ .. . : „ , %**<t

U

Please note; The chem.ul composition total in the maximumcolumn must be greater than or equal to 1 00%. TOTAL: %2. Indicate if this waste contains any of the following:

NONE .Of LESS THAN or ACTUALPCS'* Q D < SOppm ppmCyanides G G < SOppm ppmPtienolict Q Q < 50 pp"l PPmSulfides G G < SOppm ppm

F. METALS indithe following:

1. QEPTOX/METAL

ArsenicBariumCadmiumChromiumLeadMercurySeleniumSilverChromium-HexCopperNickelThalliumZinc

cate if this waste contains any of

TCLP or 2. Q TotalLESS THAN or ACTUAL

(Parts Per Million)

Q< 100 ... ,.., .n< i n< 100n< 5n< «-n<MfiQ< 02 G< 20Q* i G< 1flOG< sG< 5 G< 500n< sO< ff Q< 12^n<Ri |rf) &94n< ^G<G<

Side 1 of 2 TURN PAGE AND COMPLETE SIDE 2Forrti CWM-eOOO* 1987 Chemical Waste Management. Inc. mn I fl fl R Q li

GENERATOR'S WASTE MATERIAL PROFILE SHEET (Continued)

J 73730Waste Profile Sheet Code

G. OTHER HAZARDOUS CHARACTERISTICS. is *n.$ v. .*.j.u a J'stefl aolvent waste as defined by 40 CFR 281 31 (F001, F002. F003. F004 or FOOSP G Yes :'I Nn2. Does tnis w«ste contain greater tn«n ,COo m toiai h*fogeii*ted org&ilic compounds? G Yes U No3. Indicate if this waste is any of the following:G RCRA Reactive G RadioactiveG Water Reactive G EtfologicalG Explosive G Pesticide Manufacturing WasteG Shock Sensitive G Other ,Q Pyrophoric G None of the above

H. COMPLETE ONLY FOR WASTES INTENDEDFOR FUELS or INCINERATION

LESS THAN or ACTUALBpryHfUm Q< MOO ppm ppmPotass'um O < 5000 ppm ppmSodium G < 5000 ppm . ———— ppmTotal Bromine O < 2 % HTotal Chlorine G< 35% %Totai Fluorine O< 1% ____ % .Total Sulfur . _ .." *•'

J. TRANSPORTATION INFORMATION1 . la this a DOT Hazardous Material? G Yes C

A Hnrft'rt C'ftirft A/Mftlftnal r>«rvHpfi«rv (

7. Method of Shipment: G Bulk Liquid G Bulk Sc»t^CC^Î A DAfiAv fi'hlA iiiontitu /fit il*

10. USEPA Hazardous Waste? 'd Yes G No 112. State Hazardous Waste? GYes G No 1

I- fPTtONAL- RECLAMATION. FUELS, OR INCINERATIONPARAMETERS Provide if information is available.

RangeI.MMt \tehi* {RTU/lh}- - 9 W.f.i..3. Viscosity (cps): «_ ® G **• G 1QQ*F

6, VtpO"1 Pf ?«Uf* @ $Tp (mm/Hgf;7. la this waste a pumpable liquid? G Yes G NoTypanfpump? __ IMI , _

SQ150«F

• 8 Can this waste be heated to improve flow? G Yes G No9, Is ihK wajtecrtiMble'" water? ' G ve» G M? '

'10. f article sizei'V/ill the solid o'ortion of thin wasv- OASS throughir ***: "..;• 1/8 inch screen? * LJ Yes LJ No

« i n *

llrt n Drum {Typ«/&]M}: ., „/ O»h«r,_. 0 BO ynitf (H»/ltg)-

3. State Hazardous Waste Numb*r(f )•

_ . i

r corriat uAunLiMftiMcnQUATimi

-

n AririltlAnil P.n t,Attached

L. GENERATOR CERTIFICATION 1 hereby certify that all Information submitted In this and all attached documents contains true andaccurate descriptions of this waste materiel end yil t levan* information 'egarding known or suspected hazards in the possession r*the generator has been mw.iosed

t 9Signature

; - ! . ' . _ • . . . . _ .Name (Type or Print)

Title

ARJ00595Date

Side2of2Form CWM-6000 «1987 Chemical Waste Management. Inc.

ATTACHMENT C

EMD APPROVAL PACKAGE

flRI00596_j

pro APPROVAL PACKAGE

DIVISION. ' • . • • ' ••/,:/''' •!,'

CUSTOMER NAME m

ADDRESS AWaVrfrV Z^til .Q.tet /Xfe-7 ?-

CUSTOMER CONTACT ftiuJ YWI'.vA PHONE NUMBER 3o3/ l»

LOCATION (IF DIFFERENT FROM ABOVE)

PROJECTED START DATE qfAiT-ffy END DATE

CONTRACT IN PLACE? < S> NO

IF NO, WHY? ________________________

NEW PROJECT? NO

REPEAT OF PREVIOUS END APPROVED PROJECT? YES NO

IF YES, COMPLETE ONLY PAGE 1,DATE OF PREVIOUS APPROVED PROJECT_________________

CWM CONTACT DATE PREPARED

^COMMENTS

EMD APPROVAL

DATE

HEALTH AND SAFETY

ENGINEERING ____________ OTHER

fiRIOOS97

I SCOPE OF WORK

(BRIEF DESCRIPTION OF PROJECT INCLUDING TYPES OF MAJORvJEQUIPMENT TO BE USED, QUANTITIES OF "MATERIAL TO BE MANAGED, CON-TAMINANTS, NUMBER OF SPECIFIC JOB LOCATIONS (IE. NUMBER OF TANKS,SUMPS, ETC.)

•Polloujcpfl ' xi

rvi 10 r

J.

» U

CATEGORIES (MORE THAN ONE MAY APPLY)

O TANK EXCAVATION o ONSITB TREATMENTO SOIL EXCAVATION O CONFINED SPACEO POND CLEAH-OT o ASBESTOSO BUILDIKO DECONTAKZNATZON O ONSITB STORAGEO IQUZPXEMT D2CONTAMZNATZOH O CONSTRUCTIONX DROX SAKPLINO AND MANAGEMENT O DEMOLITIONX LAB PACK O OTHER

EMERGENCY RESPONSE?

O YES X K0

flft/00598

II KAJOR CONTAMINANTS AND CONCENTRATIONS

CARCINOGENS? YES NO V

REGULATED MATERIALS? / YES NO

WASTE PROFILE INCLUDED? YESIF NO, WHY? M li Ixt

MSDS PROVIDED? N) N/AorH-M-r

Ill MANPOWER

CREW SIZE NUMBER

PROJECT MANAGER /CHEMIST tTECHNICIANSITE SAFETY OFFICERHEALTH AND SAFETY MANAGEROTHER

SCOPE rr/>0iri^ i^vxôxOaJr4p 4L*g«r- U\' OF ^CLvv^litv!, A.jkA fj »wsA.A I-~ --.. ..

< i

SUBCONTRACTOR(S)

'10 ft £rf>*Ae__________, PREQUALIFIED Y3E NO

PREQUALIFIED YES NO

*' WORK

_________\ • ";v:.::-- -• * PREQUAL1FIEO YES NO

SCOPE \___________________________wog- \ ARTD0599

IV MATERIAL HANDLING EQUIPMENT (DESCRIBE TYPE OF EQUIPMENT)

o DRUM DOLLY \X PUMPS l4i «f*rt

\/ O FORK TRUCK ____ MANUF.______LIFT

O EARTHKOVING ____ CRANEEQUIPMENT

\AOTHER

DISPOSAL AND TRANSPORTATION ( Q

ULTIMATE FACILITY S £f\^ GU'iCd o

INTERMEDIATE FACILITIES

V DISPOJ5AL SITB APPROVAL feûVa'o STATE JO LOCALO FEDERALO ENVIRONMENTALO HEALTH AND SAFETYO OTHER

VII TRAZKIKQ

TRANSPORTATION COMPANY Oj? fl ffcf C > H-V ;

VI PERMITS

CWH CRW RKIXVBD INITIAL TRAINING? (Y*3 ) NO, WT?___________________

SPZCZA& TRAIKINa REQUIRED

rv&jg r / rl ivr p

CREW RSCEIV2D SPECIAL TRAINING? (YES NIFKO. WHY?

SUBCONTRACTOR RECEIVED REQUIRED TRAINING? (MS ) NOIF NO, WHY? _______________________

ADDITIONAL INFORMATION

VIII MEDICAL REQUIREMENTS

ENTIRE CREW RECEKgD REQUIRED BASELINE PHYSICALEXAMINATIONS? QfET) HO

IF HO, WHY? _______;____________________

SPECIAL TESTS REQUIRED

COMPLETE? YES HO IF HO, WHY? ___ ______

IX DECONTAMINATION

DESCRIBE EQUIPMENT AND PERSONNEL DECONTAMINATION

otss 4-or Liuiproforl m»g s for L.A.UJ.J C. upi II k» nftferitt^fi.

*r£tirfAi«s -Dor re_i3SecbU. Sa/f*\ /iAJ J?4jiT /*Vlflif '

HOW IS .CONTAMINATED EQUIPMENT DISPOSED?

<ffnjifx.8 y>j.t\rf i M /( iA ft.r/U' e*r* ula.r^

CONTINGENCY PIAH INCLUDED

YES __ HO X

IF HO, WHY? &/T«JC Wg ^4s omy\ vrvajJiCflil iAr^- » i i **** &«™™ii*o*— ^> i • ••! "T T ^ ~ | ni Î fcfl fP.S s£Lfv«._ j •PfvVvJLy gT^_tA3_L_LL__i3Jt__A

(MAY STATE CONTIHGENCY PLAN HILL BE PREttUOT RK)ft TOONSITE OPERATIONS).

XI WORKER PROTECTION

1) -. WORK DESCRIPTION SflL d^2) LEVEL O A O B Vc " o D

3) RESPIRATORY PROTECTION

O XT1UPURTPYINQ

O HALF MASK X KILL M*S* O OTHER

CARTRIDGE TYPE 01///1 6--/4 ____

O SUPPLIED AIR f}t

O SCBA O AIRLINEO ESCAPE BOTTLEO OTHER __ '

4) PROTECTIVE CLOTHING

HARD HAT X

EYE PROTECTIONO SAFETY GLASSESO CHEMICAL RESISTANT GOGGLESo 7ACS SHIELD.

BODYSUIT O TYVEK o HOODEDy POLYTYVEK o HOODEDO SARONEX o HOODEDO SIGALO PVCO HEOPRENSO RAIHGEAR (PVC)O BUTYLO OTHER ___________

GLOWS. X LATEX X XJEATKER^ ' ,« O SURGICAL RUBBER O COTTON' *- O VITOM o OTHER,* ' o HEOPRENX ——

O NZOPRZNB (MILLED) —————————————O SltVERSHIILD

BOOTS X LEATHER - STEEL TOED X PVC BOOTIESO PVC - STEEL TOED O TYVEK BOOTIES0 HEOPREHB - STEEL TOED O OTHER _____

—— ARIQOG02

XI WORKER PROTECTION (continued)

5) AIR MONITORIHG

COMBUSTIBLE CAS/02 METER V t^S MONITORDRAEGER TUBES 2 t S

CO MONITOROTHER

PHOTOIONIZATION (HNU) MONITOR /W.ftJ.W v £ rFIAME IONIZATION (OVA) DETECTOR f" > W1FT> r*yrAEROSOL MONITOR ————————'•~

PERSONNEL SAMPLING YES

CONTAMINANTS 0

6) SAFETY EQUIPMENT

SAFETY SHOWERS X UME HOOD-PORTABLE EYEWASH <5 GROUNDING RODSFIRE EXTINGUISHER O LIFELINE/HARNESSBARRIERS • O EXTRACTION DEVICEWARHING SICKS O LADDERSBARRIER TAPE X AIR HORNSDECON UNIT V WATER/GATORADE

O OTHER ___

'V<»•

ARI00603

Documents

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