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DOCUMENTS PURGED
The following file has bsan purged o£ all laboratory documents notsubmitted with results per Exhibit B, Section H - Document Controland Chain-of-Custody package.
CASE REGION
CHEMTECH JOB rf G7.- Co\\
DOCUMENTS SENT TO:
TECHLAW, INC.Attn: Keith Wegner12600 West Cclfax AvenueSuite C-310Lakewood, CO 80215
PURGE PERFORMED BY:
DATE:
L'nless noted otherwise , documents purged include: logbook pages ,document inventory shee t , cha in-of-custody sheets .ind sar.ple tags
This documents becomes a oart of the file.
X<C*CvCCo<*^,O
CCOOOOG9
001974
001975
G- 20092 h
0 fi£ H§ •<3 —
Preservative:Yes "S'No f
ANALYSES1 A.l i lfHr
i . . , , i r , . , , .COO, IDC, Nuliipiithenotics
Me»cuiy
Oil and UifdSHOnvn iM" . (ij^MSf'fionty f'cVr'atile OrganirsPesticidesMutagenicity
No
6-20453
f<»
(ot
001976
r ^ ' lN
6- 2 0 4 5 7 1
001977
F*I £>-(TUJCOV
~^< *~r/n£W
vflOCDCDOJX)
001978
YPS G No 1 ]
ANALYSES
Men myMctol
MS
1 ",\\<i t v
OO
lAJG-^6£ (OS
o
V)
X
r IANALYSES
Mrlr
V( t l l l )fV.t iu t l r
O
001979
U.S. ENVIRONMENTAL PROTECTION AGENCY H\V: S;;
INORGANICS TRAFFIC REPOKI(?) Cane Numher: s /
Samp!*. Site Name/Code:0 SAMPLE CONCENTHATK I
(Check One)• — *• —— Low Concentration———— Medium Concentration0 SAMPLE MATRIX
(Check One)—— — Water———— Soil/Sediment
(R) Samplirur Office: / . VI.'Sampling Personnel.
fMamftl , , ,(Phonal . - , • -' ,"Sampling Date(Beam) t fEnd)
(e) Shipping Information:Name Of Carrier'
ii -• '.
DflfftShtpped . . . •**" -V
A,rhilf^»mh«r' / / ; ? /( ' ^ x'/
© Sample Description:(Check One)
——— , Surface Water———— Ground Water——— Leachite
MinxA M^ta———— Solids •-
Oth^r 1 /' / L.-i . -, /r( specify)
MATTHFSORnfiNFrSAMPT PNO - ,.«Li .-:...
0 Mark Volume LevelOn Sample BottleCheck Analysis required
i/,TotaI Matais\f. Cyanide
0 Shiptb:c 'lt::i*?f:f **
. . - - • ' 1 1 n,• V
_ Attn: J A/ • ' • > # • ' • • /IratEMferSlc^ jfer
0 ANALYSIS UIB:£ } .- . , , .nr«^ ky- f fr Vrf / /<./ .^•-^- •• -• * '},.,''!
n»**R-^|- , , MJ.^f-i^f-T i
Sample Cerad&t&mOn Receipt:
(eg broken, tw^tage, dbdin of cwrtody, e*c.)
C--X- :sm\-o^-o2
IJ\BF11XCOPY
001980
(7) CASK* MhmhAT! , /Sairapl© Site Name/Code:
Q Samp&ina Office: "v5-Sampling Personnel:
i f 'fNamet -< l . r ' ' f . f .• ,r(phonal . V" •- -"-"/" .- -V*'/SflrnplirwjOftte' . /
(Beqinl f - • fBndt
/r\ Sample Description:^ {Check One)——— Surface Water——— Ground Water——— Laachate—— _- Mixed Medicsn — ---TI- Solids
Ortww(specify^
MATCHES ORGANIC SAMPIJ? NO ' X ilA
@ SAMPLE CONCENTRATION—— : —— Low Concentration_, ——— Medium Concentration0 SAMPLE MATRIX
((~ihf>f^!r rWuni———— Water—— .ifT, Soil/Sediment
(e) Shipping Information:Name Of Carrier:(-...,/*rtot *Sh*pparf: _/- •» V f" ?•
flirMHMnmhAr- / /f. <N" ¥~ ?/
(g) Mark Volume LevelOn Sample BottleCheck Analysis required
* Total Metale^erQyamde
' -^pf '"Jell'1' T
® $&a&$j&: '&.[:->' • :* ''nr£% :'/i.-' /- . • • ;
Atfea: : . ; : • : /• ' , „TVaspsSsar --Sh% :
® ANA&fSiaj&BsVtofrifoy t^AtAM UAJ&&M.'?*i--
. "•/ /
r>ateRAF¥*-: ^wS/Si^T"- ' 'x-v® ;
(eg. broken, te«faagef «? ofcu^ody, ete.). ;/: : > *r: . " . -- 1 ; --: r |
3421-Dlife 11 " '.".:: ""J^!.'rJ... .: I•™ r?:.~;-. -• 1
I
001981
i E.
(T) Case Number: . _. .. "*_ ^ ISample Site Name/Code:
Qi SarnoHncr Office: ru£Sampling Personnel:
A J f. f, / -. i
(Phonal . » , - - • / C •-? - ^ !Sampling Date: j/^. ^ /> (._
j ' • - • / •SBeqin) (Endl ,
0 SAMPLE CONCENTRATIOM(Check On*)
————— Low Concentration————— Medium Concentration© SAMPLE MATRIX
(Check One)———— Water•• —^- —— Soil/Sediment
(&) Shipping Information:Name Of Carrier;/ , . , / - v
' ' / i / ' V •"•'/
xj\ Sample Description:^ (Check One)——— Surface Water——— Ground Water
• i Soiids(specify)
MATCHES ORGANIC SAMPLE NO, " :'
) Mark Volume LevelOn Sample BottleCheck Analysis required
* ntAl TVffttAls
0 3JJjj|[tb|P-*, , _ t J/ j j: t .' .-(- •-) i^ *
® AitakTSbt^R_, i /j^n «4 - i ' / /f H i - - 1
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^*^ - L. ^ i" ;
i r.i>-(eg . brokati, teake^ft. ds
,._ _r . 'h-iyirr- :*~ -l . jrf ^-. - -5^.|fe^L^J | [JIJ ' " rMpv"-7 *
^[ "££""!.LABFILECOPY
|..(J.p.j Mi.i^...n.-...- i , i i. i i|i ,| .1 i
' ' 1 ' / V*' 1 ••' * •t'• •
!&*
//^^Jl ,f' ' /
i
^Bof custody, etc.)
-OZ"
001982
U.S. -ENVIRONMENTAL PROTECTION AGENCY. "HWI-Sample Monfegemei
INORGANICS
LABHLECOPY
Q £!*«» Niimhar: v' 7 A/Sample Site Name/'Code:
0 SampHna Office: |£iSampling Personnel:
1 i f ' '(NMBlAf , ; J , , ' / * " £ , ' / / • •
Phonal -'/ J" <" ' / '/ •T,.! v" 'Sampling Date: ), /r *.
I £-Jf(Beoin) (Sndl
© Sample Description:f Chack One)
——— Surface Water——— Ground Water——— Leacfaate
JUTt-ro^ Mffirfia•> SoUds
OK«r(specify)
MATCHES ORGANIC SAMPLR MO • •'-
@ SAMPLE CONCENTRATION.^^ (Check One)
——— ' —— Low Concentration————— Medium Concentration0 SAMPLE MATRIX
——— •— Soil/Sediment
(5) Shipping Information:Name Oi Carrier:
ft '* <
1 -'V "." /n»tAShipp«H: ' - -* ^ f L-A»rf>iHNt»mhflr- V <**<" H '? ,? f
(£\ Mark Volume LetvelOn Sample BottleCheck Analysis required
-*CToEal Matals^^Qjfanicte
@ fl|SbBl [; ' ";- . f >/r- r\$\$ i *4. • ' |y/- '. : , - ',- f | : ;; : . • / /^"**7! ' .*J>= i-*_.'.. ....._ J^l _i_S_
Sb^Paif|i|f | - ; - ;0 AEfALY^LAE- •
- / :]^'"' ' / /,/ f)f?n« ^ y- :/ fcittu/ i vO^n^*.... -Hfr! | - - : :
L-" | ;L ; / /n*fARto«!. llryA^SV??^
• , J: f : y
^^ T> "'IL'!;'!"\L« k«w
: " "*™V.» DlruJuiiSLO i r't- itJn Jnoca io^c: •.!---
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-: -i3|in-i--.---••-i-ff^; i • • • • • - - •
001983
(T) O*aa Nwrnbetr' .__..,. - .7 ' /Sample Site Name/Code:
@ SAMPLE CONCENTRATION(Check One)
——— '• — Low Concentration————— Medium Concentration® SAMPLE MATRIX
(Check One)———— Water—— — Soil/Sediment
g) SampHnef Office: JJZJ-Sampling Personnel:
(NuiMt //? •' '' ' , / • '"fPkooaJ -. • /•/ "" '- ' - ' • ' • 'Sampling Date: / . > /, ;,.
' <*(Baoin) fEnd!
(e) Shipping Information,:Name Of Carrier:, - .. /.A'n»^«Shipp*rf: ,• ~ y -" ••AfrhrtlNumbftF- ' / L ^ 1 <. ¥~ ?(
© Sample Descariptian:(Check One)
——— Surface Water——— . Ground Water——— Leachate_•* Sofids
Dtkftr(specify)
MATCHES ORGANIC SAMPLE NO. ' ' " f
(3\ Mark Volume E-evelOn Sample BottleCheck Analysis required
^ Total Metals. QTanJiete
, .-. _ _ . , .-.„ ———^.J,, p.-r. ... .--. • - - - • - . - -
/• - . " ' • • • i -tn^-»' i f* • i fe * ' *-:•*: '_ , f - ; ,/: • |/i,
> l- ; • r ;! /*' •. ' "tore .^.. 47 ,-.//A- :IVassto ;!SltBpl 1
^^^ • . 1 1 . . , - . - - , - , ^ . , .® ANALYSIS L^B:p ,4 y- p^m kA U 4^-*K\
/*££"' /&/*n*,^ R»™I- //d*o /fit*
® - !Sample CowiitacijQ.On Receipt; :J
.: i(eg bt-okon, leakfige, d jte al ciisH xiy. »tc )/^ ^>SL^, Ail ." "^.:"*' - '
. . -^WiT. . T-5^|?f-_ . _ -- -
~ ' ^ 'V 7=3TT.' f- '" * : ': "f . ' !
LABFILECX^Y ; . . ; /
001984
U..S. tit AL PROTECTION AGENCY 1 JWI Sample Manaement Gift -'
TkTrf^^T^fcJ *'1 H "^"^T^^ff* '^ff'D Mi • M'Hi|'jP*iINORGANICS TRAFFICi) Case Number;
Sample Site Name/Code:g> SAMPLE CONCENTRATION
(Check OneJ—"—— Low Concentration———— Medium Concentration© SAMPLE MATRIX
{Check One)———— Water—w.— Soil/Sediment
($\ Sampling Office:.Sampling Personnel:
(Name)(Phone)
i .
e:_ (End)
(§) Shipping Iniormation:Name Of Carrier:
ov SarctpLs Description:^ (Check One)——— Surface Water——— Ground Water——— Leachate
SOQCIS
(specify)MATCHES ORGANIC SAMPLE NO. ~L
g\ Mark Volume LevelOn Sample BottleCheck Analysis required
X Total Metals
LABHLEODPY
001985
® f J
Sample Site Name/Code:
(5\ SarapHnq Office: 32*Samphrtg Personnel
t- J(Msmel /'< ' / t. .-• !~
Saaaplmg Date: \ / ? ? / £<fBeoinl < * iKndl ; • ' O
/£\ Sample Description:^ (Check One). —— „ Surface Water_ —— . Ground Wat*t, ——— Laachate——— Mixed Madia
(specify)MATCHES ORGANIC SAMPLE NO. ' ir- '' ^
0 SAMPLE CONCENTRATION, t • (Chc-ck One)'
—— *" — - Low Concentration———— - Medium Concentration@ SAMPLE MATRIX
ff^h.jaf If On£*i
———— Water. — t^-. — Soil/Sadiment
(B) Shipping Snfontiation:Mame OS Carrier:
• " / V< . . / -x
nAtftc,h Afl. ,' ^f/ . . _ , ,-
Airh'O! N"rnN»T" ^'' ' ( ' • '^
g) Mark Volume LevelOn Sample Bottl©Check Analysis required
- •"* Total Mstals^2; Cyanide
0sh^w ipRr^...r^ivif/ . - ' < • / i •'// I J . . / / . Y - / *
Attn: - '•• ! {/ . • / . .i :;!'.. - •-. l_h • . l > '..
Trar «r ^-;-^et'^ '\^'.\.'.
t— ';"B; Sub'm^m. _ «* "!"r Tf'"!: : ! :
'-'\-f- ' /n^t-ft Rf^citf; .,„„„„ 4JL^ / <i 0>
\r iJh 1: :/ -^^^ - T1 7!rf>": " " "
1 ® ;- H- :
C •> tjiL rf jsiMiL/IS-ffifliriiiftnn if tLrt^B'^ * " " '
(eg. broken, tee^ jig®, q j . ol custody, etc.)
LABFILEOC^Y
>*-; J^;it?!i :flH
001986
' U.S.' E^VIKONMENT.AL PKCTECTION AGENCY HV?/I 'Sample Management Ofcce
INORGANICS TRAFFIC" V ••* 1t f jS C-ww fJnEnfcfd"* "•* "*
Sample Site Name/Code:
^5> Sampling Office: i.TISampliiig Personnel:
- I 1 ' ' - ' 'f Phonal • /. - ' / ' / '•'• • • '- *Sampling Date: • . /- •(Bemn) ' (Snctl
© Sample Description:(Check Oite)
——— Ground Water. ——— Lsacfaate
, Mixed Media_ 'i T SoJids
(specify)MATCHES OaOANIC SAMPLE NO. -L'/J.-i..
@ SAMPLE CONCENTRATION—— — — Low Concentration———— Medium Concentration(a) SAMPLE MATRIX
(Check One)————— Water— -C — Soil/Sediment
(j6) Shipping Information:Name Of Carrier:
r •- • I
D*i-ft Shipped r : ' • v • •
Air^ff? N"mN=fr' i • , ' ' f /
(a") Mark Volume LevelOn Sample BottleCheck Analysis required
.-^TotaJ Metals_v-;C5ranide
-- ^_ M.ilj'feE " 3?*W"~"Jf^B) ^a*t|te fi | .if£|fj.|.g.rJ3~J ji." ,'
/] ^ifci;: •' ' ^^"^ , &• 1:^ ''i .^. -• M* jH^^^ :h! I!
• " '" '•" -! »" • *- B
f. J l-;ii^ E;"
:&~Jf ' £*~ f:fT\ j
-^ - ' •'-';!:, ' °
(eg. broken, leafc*go, (iiftw^f custody, «iic >
C^fel !; :;;: TUlij!"-' '-.
5Mll l)J:|ffi :•' -™!r ""Ifgfni' " :^"~ "'1 •' """i""! i :
LfiBHLECOPY
n!
001987
m-
., - mtoi-;U;S- E^ ^ONMSNtAL PROTECTlOH AGENCY HVVI
TRJffiFSCCase NSaoaapJe Site Name/Code:
SAMPLE CONCENTRATION. , (Check One*
—*— Low Concentration—— Medium ConcentrationSAMPLE MATRIX
(Check One)—— Water'-— Soil/Sediment
tee: "CTSampling Personnel:
(Nera«) . ; * > • / J - " ' -.J^^-i/ ._ r-
Sampiiag Date:(End)
(e) Shipping Information:Name Of Carrier:
Date Shipped: _i.AirbiO Number: I I CO / f 'V
_, Saxnple Description:(Check One)
Surface WaterGround WaterLe&ch&teMixed MediaSolidsOther _________(specify)
MATCHES ORGANIC SAMPLE NO. >*>*>
Mark Volume LevelOn Sample BottleChack A; .atysis t»quir«d
LABFILP.COFy
4-
!-g broken, l»«i:ac*1..iiitin oi custody
TSPipT'"Ml !
3-
001988
f(T) CTase fiSwinlier: „„...., .V , ,.— /
Sample Site Name/Code:
<7^ SainpIiTKT Office: tZSTSampling Personnel:
. i .-- .'fN^m^ / ; ' " ft" / > ! • : , . ' -fPhoeal .- V "• </• ft^ y._*+S~Samptimg Date:(Beoin) (Sndl
© Sample E>escription:(Cfaacfc One)
——— . Surface Water——— Ground Water——— Leachate
1lrfj^**-jJl \JVdu^jiA
.^" Solida„ , , r>hftr
(specify)1 MATCHES ORGANIC SAMPLE NO. f,< -'. •',
@ SAMPLE CONCENTRATIONi/ (Check One)
————— Low Concentration————— Medium Concentration0 SAMPLE MATRIX——— T~ Water— i^I — Soil/Sediment
® Shipping Information:Name Of Carrier;
; ' \n«t«Shipp«H- f - '^V "_- C-
a*rhi»M»mhAr- // f f *- If 'V //
f£y Mark Volume LevelOn Sample BottleCheck Analysis required
^ Total Metals..xrQyanide
'--•——' 'f*r-"-« pf-tl r ; - ;- '!! " -® atljBfeJfeB;- " :
. / ,;f: ''$*''. fr-.i>' r k-. ;1:1: - . - ' " > ^-1- IX- - y : ,,*M*IM7f! j Mitfjiif; *',-f/f f ftISwiJllBa? *J . ; -. ;
(*) AM .Y i i -jEjjBi; I •c / -;^ r '"" • / ..-js*
R^-^»>yj tuJJitfrf ^/rf (/(4*"- :--* ' -; ' • T •
i i /r-. -. '•, "'-•'<• //nr^/o^Hate P^s^f* -IJ*/W St /XA; - ITl ! * i i
." _,. ";i£ : - - - : - ' - : :
@ f I;JT;; - ;Sample CoEtdS tccwOn Reo^teffe: : i'' •Xl^*~ * "VTPW*"1" », ! :.
• i : l(eg. brokan, l*skag(i dw*n leustody, « c.)CJ{L..!A'. .
.L. .JH 1 -^^ ... , . , . .
———————————— - ———— LOJrij- T^ ——— ^ ——————— ™»-
;;.j. . , 3 r . r : , .- . • ; • - • -• ! ' JTl" , • ' • ; " j
LABFUEOQPY
001989
ffiTi1""1
——— ••—— ————— " - "— — —— ' "—- —— "— —— -"'———'.—— — ..-— ——— . -
Sample Site Name/Code:
©RampJJnq; Office: J^L
Sampling Personnel:(fMsmA) • • • • '• V i
• f . _
AtmnHng DfttA"
{Becnnl (End}
© Sample Description:(Check Onel
—— — Ground Water
-r-.-_!rnT SolidS
(specify^MATCHES OBGANICSAMPLS MO. ' V '
i
0 SAMPLE CONCENTRATION(Check One}
————— Low Concentration————— Medium Concentration® SAMPLE MATRIX
(Check One)———— Water—— 'j~— Soil/Sediment
(e) Shipping Information:Name Of Carrier:-;.. / x
i - .'." V -^{ -"• / • t — iAirMIM»mh«r- ' V L f( t'J
(j£\ Mark Volume LevelOn Sample BottleCheck Analysis required
J^-Totai MetalsjfS. Cyanide
L&BFILEOOPY
©sfcSi&lp-; !', : f '|fe 1t(/ y 11, rf f , ' . . > / bi / fl-f :~. ' ,
^^r ; .'^ f // K 4* t;^^ -: ^ r!il ' ;" * '^^A^LM^MJ^^^^
. '. : n* "' " '" !
: l i . i . ; * ! : , /
^^ . ™ "T'T-"" •-
C? a vOiJJU. IcSrufl /IBtll&Mai-S^n^^EL^^tf"-'
(eg, broken, Saakag ihftin; o£ custody. s?cjIfc^iii":"TT n3:T! ••:
5^^f5|b2. . : -.Tl- •|^p»-|-r. - . . . .
. :i- i :
f"
001990
ONG h.r 1201 Elm St. I
\, it i LV i * » t i < _ i v I /A._ C ' C t U 1 UL, 6
Office of Enforcement CHAIN OF CUSTODY RECORD f
OaEe /Time ReceivedReiinquished by: Refinquisned by:
Relinquished by- Relinquished by:
Received for Laboratory by:
Original Accompanies ; Copy to Coordinator Field Files
001991
5 M 2 1 - Ob- 05SAMPLE. jVNALYSIS TRACKING CHART
BATCH tCHEMBQB. JOB.f EFA CASE WATER SOIL, SEt) TOTAL DATE DATE DAT
SAMPLE EXTRACTED/DIGESTEDPERCENT SOLIDS
TASK I ANALYSISTASK II ANALYSIS:
As
DATE
y c a -
INITIALS
DH
ee.
ADDITIIONAL ANAX.YSIS (SAS)JOB ft:
SnTl
KCtf
:
1 SC'- PARAMETERS: C*T
•»v,. «•* • • t.-». rar»M
001992
Form 1U.S. EFA Contract Laboratory ProgramSampla Management OfficeP.O. Box 818 - Alexandria, VA 22313703/557-2490 FTS: 8-557-2490
|£PA Sample No.
Bate Q VHfORGAHlC ANALYSIS DATA SHEET
CAS£ HO,
NO
Elementa tdencified and MeasuredConcentration: tow JMatrix: Water / Soil
MediumSludge Other 6uf\viW
(ug/L)or ag/kg dry weight (Circle One)1. Aluminum |l*f<? p 13. Magnesium L^dSj P,2. Antimony ^0 V?- 14.3. Arsenic 5? U^.4. Barium 6f 5* Beryllium 3<^6. Cadmium i/(/47. Calcium 5^<?8. Chroalum I9>5~9. Cobalt o?^)10. Copper ?Q_11, Iroa /^^12. Lead /"#/"Cyanide /^ cFootnoted: For reporting
IS.P. 16.>. - 17.°. 18.P 19.
/? 20.^ 21.y/*. 22.0 /? 23.? F. 24.
Manganese $/ PMercury 0, 1^ (J.Hickel ^0 vf>.Potassium ) fOfOA f.Selenium H uF.Silver f vf.Sodium £b?5^2 P.Thallium 6 f/fTin o?? u^Vanadium 3d vf.Zinc SI P.
) . , Percent Solids (X)results to EPA. standard result qualifiers are us
is defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of auch flags must be explicitand cQtKained on Gav&r Page, however.
Consents; Oto- 01
Lab Manager
001993
Fora IU.S. EPA Contract Laboratory ProgramSample Management OCficaP.Q* »ox 818 - Alexandria, VA 22313703/557-2490 PfS: 8-557-2490
|EPA Sample Ho.
IMORCANIC AKAtYSIS DATA SHEETCASE
H0.
Elements Identified and MeasuredConcentration: LcMatrix: Water
1. Aluminum iff 302* Aatitaony ^3. Arsenic 5"./4. Barium t/35, Beryllium /, ?6. Cadmium J.(t7. Calcium _^/^BC8. Chromium $,)9. Cobalt /310. Copper /O11. Iron y$bt12. Lead f/. 1?Cyanide 0, 3
w / MediumSoil / Sludge Other
/F*"' ~*~*~*\ug/L or fe/kg dry weighe) (Circle One)*U " "' ' J • «M
/; 13. Magnesium Z//«*^J )L3p, 14. Manganese ,5"V uf^. 15. Mercury 0*/*2v£ 16. Nickel IB V?.\jp.. 17. Potassium L5*^fA 18. Selenium *?. 6 L
Q P. 19. Silver V- 5* t/e/A 20. Sodium f?£0 IOf. 21. thallium 3. %\fP- 22. Tin 7?05 /? 23. Vanadium /? fi^TS.^ 24. Zinc C/%3
o?u. , Percent Solida (%) "!*&»?
ct4S
->•
«>f.
lt>-OF.
£!>
Footnotes; For reporting results to EPA, standard result qualifiers are usedM defined on Cover Page. Additional flags or footnotes explainingresults are encouraged* Definition of such flags must be explicitand contained on Grvar Page, however.
Commenta:
±£-n- i '(\ HeMtab Manager
001994
Form IU.S . EPA Contract Laboratory ProgramSdfflple Management, OfficeP.0. Box 318 - Alexandria, VA 22313703/357-2490 FTS: 8-557-2490
|E?A Sample Ho,
Date
US HAHSINQRCAKtC ANALYSIS DATA SHEET„___ CASE HO.
• > • > . - i i^i
Eft.. NO.
Elements Identified and MeasuredConcentration;Matrix: Water
1» Aluminum2. Antimony3. ArsenicA. Bariua5. Serylliua6 . Cadmi ura7. Calcium8. Chroaiura9* Cobalt10. Copper11, Iron12. LeadCyanideFootnotes: For n
Low / MediumSoil / Sludge Other
ug/L or mg/fcg dry weight) (Circle One)365*0 P. 13. Magnesium If </#J P,
30 <"*P- *** Hanganese V5^ /? ^^/•B Of^ 15 . Mercury 0 - / / UV6? uft 16. Nickel /^ f/>1$ u& 17. Potassium LJU&^l T>o?.^ J *, 18. Selenium «?• V ur.
//S503 /? 19- Silver Vn? ^.j2 /! 20. Sodium /^/^ f£/5 ^. 21. Thallium 3,fc Uf:f,$vP. 22. Tin /6 uP.*/^?<? /J 23* Vanadium IB uftV.7 T5,^ 24, Zinc D/JtfO . B u . . Percent Solids (t) %3.%
sporting results to EPA, standard result qualifiers are us&• defined on Cover Page. Additional flags or footnotes explainingreauUa are encouraged* Definition of such flag* muse be axpHeieand contained on Cover Page, however*
Lab Manager.-Stf
001995
Form tU.S , EPA Contract Laboratory ProgramSaapla Manageaiant Of flea?»0* Box 818 - Alexandria, VA 22313703/557-2490 FTS: 8-557-2490
|EPA Sample No.
/o3INORGANIC ANALYSIS DATA SHEET
CASK HO.
QC-AiraK-
Elements Identified and MeasuredConcentration:Matrix: Water
1 . Aluminum2. Antimony3* Arsenic4. B&rlum5. Beryllium6* Cadmium7. Calcium8. Chromium9. Cobalt;10. Copper11. Iron12. LeadCyanide
Low J MediumSoil / Sludge Other
ug/L or og/ttg dry weighy (Clrela One)/ 0$0@ t- 13. Magnesium t$&z5O r-^1 Up- 14. Manganese oiB^ r, %^•7 UK 15. Mercury 0. /«3 (J.
£~55] £ *6« Nickel }£ vP.l,$ vf. 17. Potassium / H^Oj f.3t*{ UP. 18. Selenium ^ V U F-$<olOQ P. 19. Silver Y-3 f/^
/e? t^' P. 20. Sodium /(*50 U/^/^t/P. 21. Thallium 3.?- u^^.? UP. 22, tia /? f/^?&30_ £ 23. Vanadium Z"o?/J £7^2 T5.* 24a Zinc 5^ />0,31 O. . Percent Solids (%) o\."1
Footnotes: Pot reporting results to EPA, standard result qualifiers are usedAJ» defined on Cover Page. Additional flags or footnotes explainingresult a are encouraged. Definition o£ ftuch flags osuat be explicitand contained on Cover Page t however.
Coaoeata:
Lab Manager
001996
Sample Management OfficeP.O. Bo* 81S * Alexandria, VA 223137G3/557-2490 FTSt 8-557-2490
EPA Sample Ho,
Date S- $0 - OWAHAtTOS OAtA
&A& BMItit £&&?&j. " «'«"'" . fiiji ' • ' " " ' ; ' ' '• fOT 'SS'* ' :~ :" " : ' :"r ;3NS
UUI-MUU 10*- NO,
Concentration:M j* F1 f^f v * Wa t* is i*1 1. t 1# 1* •a 'JW * « O w Cfr *>
1 . Alutalnun2. Antimony3. Arsenic4« Barium5. Berylllua6 . CadmiuB7. Calcium8. Chromium9. Cobalt10* Copper11. Iron12. LeadCyanideFootnotes: For r
T<a/*u• , {v;-. . . • • ; : . ' . : - . . : . r . ' . ; . . . : .^j.,...,, , , , . , . , , „ , . : , . „ . , . , -
ElementsLow /
Soil
ug/L or (3320 f>.
30 oP.^/.^ uf?^0 uP-;.^up.«?,*/ ^.
}b50Q P.tf.g- vt/o? Vfi7.5 of.
WJO £t Xi ^** f* \1//t) A-S TT:/ y ^ ^^/ i\
0.3u.eporting results
. ail 'si-s y^jH. . : . , . . . : . . . . • . , : ; ! . . . , , . ; , . : . „ ^ , . - , : . , . . - . , , . • . . , „ • - . • , , ,; . • - . . : ; - 1 ! . -.-/•'•-- '•••<.« ; • ! • ' . - : - . . - -^ ;-;;,-:;;:|,;-/-', . • : . ; s - , . • ; . . • ; • . , ! . , . . !
QfilttCffBf HO. &f!
Identified and MeasuredMedlua
/ Sludge Other
5g/kg dry weigh?) (Circle One)13. Magnesium i/36o] P.14. Manganese 65" r, ^IS* Mercury 0.//U.16. Nickel A? ^17. Potassium }202>®\ P.18. Seleniun «?' V 6»F.19. Silver Y. o? W^20. Sodium /^(3 f£21. Thallium 3,6 u/s;22. Tin Ib uf.23, Vanadium /» uP.24. Zinc }0 wP.Percent Solids (Z) *c.M."2_
to EPA, standard result qualifiers are usedaa defined on Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flags must be explicitand contained oa Covar Page, however.
Lab Manager
001997
Fora IU.S. 8?& Contract Laboratory ProgramSaoipla Managesent OfficeF.O* 9m 818 - Alexandria, VA 22313703/1537-2490
No.
INORGANIC ANALYSIS DATA SHEETCASK HO, 5Vnhf
•IWBSii^^iSKBIW'l*''1"'"'*11!"*''"-"1-^'**^^!-'/1' """ - ". i l" 1 '"- 1- i' ;™~ ; . - , • • • " • • ! • ! • •T^Sr-HJPk " " " • : • • - --•Tt-igfl^i ; - . . . . - - . . . . . • - . - - . . , . . . . - , . . . . . ; - . . . .
ElementsConcentration : Low /Matrix: Water Soil
ug/L or (1. Alufflinum /3&0O p.
3 t **I or.8 (7 £"_ , — - - - •or.
4* Barium L rVj r.5. Beryllium /. 7 W^-6 . CadmiutB ^ 5 UP.7. Calcium $1000 ?.8. Chrotaium /o A,9. Cobalt /3 c/A10. Copper /O iff.11. Iroo 15 $00 P.12. Lead /«? f • ^ _.Cyanide 0 * 3 / U. _Footnotes: For reporting results
. , . . , ; . , . . , . , , . , . : . . , , , . . - „ . . . . ; , „ . , . , , . , . . . , . . . , . ' . , . , , , . . . 1i , ,.T. .... . .
QC. REPORT
Identified and MeasuredMedium
/ Sludge
^/kg dry weight) (Circle C13. Ha goes turn1 4. Manganese15. Mercury16. Nickel17. Potassium18, Selenium19. Silver20. Sodium21. thallium22. Tin23* Vanadium24. ZincPercent Solids (%}
to EPA, standard result
, ; :„- , , i i ;5,,. .7,. . : ; : , . ' . . ' . . . 'HO. fatf
Other
tae)sno />3Ht> /*.*a 13 u.Oil?.r%t>ip*-?.5*u/=:V*V^/^^ y/>
J7, O Uf^j ^r | 'M- • — .
l¥oF.3V /?34 Pt*>* / * •
%G£>qualifiers are us<
defiaed on Cover Page. Additional flags or footnotes explainingresults «r* encouraged. Definition* of such flags tauat be explicitand contained on Cover Page* however*
Coa&ents:
L*h Manager
001998
Form IU.S. EPA CoocrP.O. Box 818 -703/SS7-2490
t3i)K iwwE Oj^.^..jHWira*!.^^
LAB SAMPLE 18.
Concentration:Matrix: Water
1 . Aluminum2. Antimony3. Arsenic4. Barium5* Beryllium6* Cadmium7. Calcium8* Chromium9. Cobalt10, Copper11. Iron12. LeadCyanide
act Laboratory Program |EPA Sample No.Wttf Officer ' • • • • • • • • • • • • • . . . . . . . . j • * . . . . - . . - . . • . . . • . . . . . . . . . . . .Alexandria, VA 22313 | ^r?p"C /<Ot£
FTS: 8-557-2490 & p~Date ft-MO" SO?
INORGANIC ANALYSIS DATA SHEETJ irKfi* a $&&• wGT, IfWsP'l.iXftSf... , . , . , . , , , , i , , - . , . , , . , , , , . , . , . . , ; , . , . , , , . . ' . . I , . . : . . : , . . , , . , ' , . . : . , : : ; . , . . : . ; , . . . . . , . : ,
NO, ^£~£// ~ OT* QC REPORT NO. ^/f
Elements Identified arid MeasuredLow / Medium
Soil / Sludge Other
ug/L or ogAg dry weight) (Circle Ose)IH%00 ?• 13. Magnesium [ \B$Ol p.
30 vP. 14. Manganese IH P.*T- 0 Of. 15. Mercur/ Q> II O .
/T^5jP. 16. Nickel /o? ^J, % vf. • 17. Potass iuia L95Sj r«7, V L>^ i8- Selenium o?. V U^-SS'/O P. 19. Silver V-^ tf>12 P. 20. Sodium l^fO uP.1$ vP. 21. Thallium 3>(o oF.
&&! P. 22. Tin 33 FS05O P. 23. Vanadium l % u P .^.OJF. * 24. Zinc /? ^^ .3^ . Percent Solids (J) ^?).l
Footnotes; For reporting results to EPA, standard result qualifiers are usedAJ defined on Cover Page. Additional flags or footnotes explaining?«sult« are encouraged. Definition of auch flags auat be explicit*o4 contained on Cover Page, hovsver.
Cooaents:
_ . ....._... . . . . . . . . . . . - . ~...-^^,/ -A-=5Lab Manager
001999
Fons IU.S . EPA Contract Laboratory ProgramSample Management OfficeF,0* gox 818 - Alexandria, VA 22313703/557-2490 MS: 8-557-242(3
| SPA Sample Ho,(OFC.
INOftOANIC ANALYSIS DATA SHEETNO,
LAS SAMPLE NO. QC REPORT HO.
Elements Identified and MeasuredConcentration:Matrix; Water
1* Aluminum2. Antimony3. Arsenic4. Barium5, Beryllium6. Cadmium7. Calcium8. Chromium9. Cobalt10. Copper11. Iron12. LeadCyanideFootnote*: For r
Low j£Soil J
ug/L or ft/x ^y&Soo P.32 of.?.l F.ys^o ?.f/.?7 f.3. to oP.
555-QO P.3$ P.IB op.Jt P.
B0$00 P./J P.*
MediumSludge Other
ig/kg dry welg^) (Circle Oae)13 *14,15.
IJ*T1 • i 1 ,\
16 .17.18.19.20.21.22.23.24.
MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumTinVanadiumZiac
()• fe^ . Percent Solids OX)eporting results to EPA. «tandard result
jyyoo fi5BO P.%.0./3*
35 fi7ZOO P.
J,(> vT.H, 5 oP,1750 up.
3-9u£B^ f.52. f-bB P.11. t
aualifiera are useas defined on Cover Page.results are encouraged.and contained oa Cover
Additional flags or footnoted explainingDefinition o£ such flags oust be explicit
hovevar.Comment*
Lab Manager
002000
Form IU.S . EPA Contract taboratoty ProgramSample Manageaent OfficeP.O. Sex 818 - Alexandria, VA 223 13703/557-2490 FTS: 8-557-2490
IEPA Sample No. j
SAHPLE ID, NO,
DateINORGANIC ANALYSIS DATA SHEET
QC R1PORT NO
Elements Identified and MeasuredConcentration: Low /Matrix! Water Soil J
MediumSludge
ug/L or fg/kg dry weight) (Circle 0!• Aluminum o?^602. Antimony 3^3* Arsenic V-5
P. 13.( j P 14is i . i **.UK 15.
4. Barium VO P. 16.5. Beryllium /, $6. Cadmium <2. 47. Calcium uT2>4,8. Chromium ^o9. Cobalt /•=?10. Copper 9-5"11. troa /J70
\tf. • 17.uP. 18.P. 19.
(jp 9fti/r . ft \J .
i/A 21.t^. 22.
/J 23.12. Lead _j[T?.</.7^# 24.Cyanide 0. J
MagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumthalliumtinVanadiumZinc
Other
fie)bstifia P. *O - l l u .13 u£33% 0?.J.^of.y.jrf.lt> 10 up.
3. 6 1/£lt> u£1% vP.lO uP.
* O , , Percent Solids (%) ^>3-%Footnotes: For reporting results to EPA, standard result qualifiers are used
ad defined on Cover Page* Additional flagu or footnotes explainingresults are encouraged. Definition of euch flags must be explicitand scmtained on Cover Page, however.
L«b Manager
002001
JBfc
Form IU.S * EPA Contract Laboratory ProgramP,0. Sost 818 - Alexandria, VA 22313703/557-2490 FfS; 8-557-2490
IEFA
UB WAMEANALYSIS DATA SHEET
CASE m
SAMPLE ID. m<
NO*/0P
HO
Corscerteraeion:Matrix: Water
MediumSludgft ___ Other
1. Aluminum
Cyanide
ug/t or S/kg dry weight)(Circle Oaa)v~ , —"^P. Hagngaium
2.3.4.5.6.7.8.9.10,U.12 .
Aatimony 3^Arsenic V-$
Up 14.\JF. 15. Mercury
Barium tfO <JP- 16. NickelBeryllium /. $Cad nil urn «?• HCalcium &SV'Chromium ty, oCobalt /<x (Copper 1*5Iron /6?70Lead /^?.Vj
rf. - 17.v?. 18*
PotassiumSelenium
II P. *0. // u./o? i/£2?^ OP.J.VvF
r. 19. Silver ^,<S \)f.vP. 20./^. 21.vP. 22./! 23.F.& 24.
SodiumthalliumTinVanadiumZinc
/btoup.3.& vF.fa Of.1% vf.lO uP.
Percent Solids (Z)Footnotes: For reporting results to EPA, standard result qualifiers ara used
a* defined oa Cover Page. Additional flags or footnotes explainingresults are encouraged. Definition of such flag* nuat be explicitfind contained oa Cover Page, however.
Lab Manager
002002
Ports IU.S. £FA Contract Laboratory Program
rtdgaeant Office818 - Alexandria, VA 22313
703/557-2490 rtS: 8-557-2490
|EPA Sample Ho.t
NO.
DateINORGAUIC ANALYSIS DAtA SKEEt
NO.
QC REPORT HO,
Elements Identified and MeasuredConcentration:Matrix: Water
1. Aluminum2* Astimony3. Arsenic4. Barium5. Beryllium6 . Cadmium7. Calcium8. Chromium9. Cobalt10. Copper11. Iron12. LeadCyanide
tow /Soil
ug/L or? 430 P,31uf>,46 vK
f?sl P>/.^ uP.^..3 I/P.
?//«? P7.3 AI2rf.f .3u/>.//w £// F.S.&A TOt/. oc/U-
Mediuay Sludge
fe/kg dry weight) (Circle13. Magnesium14. Manganese15, Mercury16. Nickel17. Potasaiuia13. Selenium19. Silver20. Soclium21. thallium22. fin23. Vanadium24. ZincPercent Solida (t)
Other
One)3800 P.353 ?.^O./lu.13. vf.
r/B5O] /?3, 3uFif. 1 y/>1570 UP,j. 5 up.Ik if.
feW! f.0*? Po* 7 * •%to.l
Footnotes: For reporting results to EPA, standard result qualifiers are uaedaa defined on Cover Page. Additional flage or footnoted explainingrasults ar« encouraged. Definition of such flaga must he explicit*nd contained on Cover Page, however.
Oomaeate: __ J
Manager
002003
Fora IU.S. EFA Contract Laboratory ProgramSample «anagemenc OfficeP,0* Base 8ia - Alexandria, VA 22313703/557-2490 FTS: 8-557-2490
|EPA Sample No.
SateINORGANIC ANALYSIS DATA SHEET
LAB
LAS SAKFtE ID. SO. NQ,
Elements Identified and MeasuredConcentration:Matrix: Water
tow /Soil /
ug/L or fg/kg dry1 * Alu&imim2* Aseisony3. Arsenic4. Barium5. Beryllium6. Cadmium7. Calciuta8* Chromium9. Cobalt10. Copper11. Iron12. LeadCyanideFootnotes: ?or
3710 f>dO op.V-? of.HI i/Af.8of..^.v^.
32300 /?Y.# /o? (//>9. 7- rf.
3?50 P.1 _/. 1 1 /" "M*/ " J '
0. 30 u.reporting results to
13.14.15 .16.
18.19.20.21.22.23.24.
MediumSludge Other
weight) (Circle One)Magnesium / /<£3QJ /?Manganese /Vo2 /^ ^Mercury t/«/o? u.Mickel /^ ^/?Potassium / V^J /?Selenium o/« u£Silver y. c? Sodium IktfQUi'thallium J?. 6 u^"Tin /6 u^Vanadium /$ c^PZloc f//j# />
Percent Solids (Z) *fe1.MEPA, standard result qualifiers are us<
defined oo Cover Page, Additional flags or footnote* explainingresults are encouraged. Definition of such flags muse be explicit
contained on Covac Page, how«var*
Lab Manager HllL^L
002004
£
QC REPORT NO:iEPA CASE NO:;£HaiS OP CUSTODY;
5
OS06
to
Sanrole No. EPft No.£ ^OQ
TVPEyatary Soil
Z
Other cocTag No. Seal Metals CM Qotae.O.K.
002005
CtEfTKECH
INDEX OF DOCUMENTS PURGED
CODECASE f - REGION * - SERIALISED *
CASE * REGION »
SERIALIZED
- 01. 02
0304
- 050607080910
ITEM f IN FILE
Carrier Airbill to Chemtech IInorganics Traffic Reports (yellow) \\Chain-of-Custody sheets \Sample tags 12.Sample tracking form IInstrument logbook pages or bench sheets ©Inorganic Data Sheets M • "Logbook Page ( s ) 1Index of Documents IOthers - Specify Phone &ecx»>ui V-CA *
M2\ oq
002006
In Reference to Case No(s):
REGIONAL/LABORATORY COMMUNICATION SYSTEMTelephone Record Log
D*te erf Call:Laboratory Name:
Contact!Call Initiated Byj __ Laboratory
In reference to data for the following sample nurnbeKs)
Summary of Questions/Issues Discussed:
Summary of Resolution:MFC- 1 00
Signature
Distribution: (1) Lab Copy, (2) Region Copy, (3) SMO CopyOate
002007
