15
ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003 Tel:(304)231-1176, Fax:(304)231-0920 SDMSDoc.0 Date: September 05, 2003 Ms. Betty Jeffery RPOC USEPA Region III , Environmental Science Center 701 MapesRoad Fort Meade, MD 20755-5250 Re: Chain of Custody Records for Big John Salvage Hoult Road-Tar Seep Site, Case No 32129 Dear Ms. Jeffery, Enclosed, please find the Region Copy of the chain of custody records for the above referenced site for shipment dated 9/5/03. If you have any questions, please contact me at (304) 769-0085 Thanks'! > V Younus Burhan START Project Manager CC: Site File Deliverable File recycled paper AR115282

ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

  • Upload
    others

  • View
    0

  • Download
    0

Embed Size (px)

Citation preview

Page 1: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

ecology and environment, inc.International Specialists in the Environment

131 Peninsula Street, Suite BWheeling, West Virginia 26003Tel:(304)231-1176, Fax:(304)231-0920

SDMSDoc.0

Date: September 05, 2003

Ms. Betty JefferyRPOCUSEPA Region III ,Environmental Science Center701 MapesRoadFort Meade, MD 20755-5250

Re: Chain of Custody Records for Big John Salvage Hoult Road-Tar Seep Site, Case No32129

Dear Ms. Jeffery,

Enclosed, please find the Region Copy of the chain of custody records for the above referencedsite for shipment dated 9/5/03. If you have any questions, please contact me at (304) 769-0085

Thanks'!>

V

Younus BurhanSTART Project Manager

CC: Site FileDeliverable File

recycled paper

AR115282

Page 2: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

Region 3 Laboratory Assignment NotificationShipweek 09/01/03

case# 32129 RASCASE No. CT1915Site: BIG JOHN'S HOULT RD

Sampler: Suddha Graves, Ecology & Environment, Inc.

Program Lab Address

ILM05.2 Bonner Analytical Testing Co. (BONNER)ICP-AES 2703 Oak Grove Road

Hattiesburg, MS 39402(601)264-2854

Contact: Chris Bonner

Samples Scheduled:6 Water ICP Metals/HG

Turnaround Time14

OLM04.3 Ceimic Corporation (CEIMIC)10 Dean Knauss Dr.Narragansett, Rl 02882(401)782-8900

Contact: Ryan Montalbano

Samples Scheduled:1 Water VOA6 Water VOA/BNA/PEST

Turnaround Time1414

Key

Ag - Silver SNA - Semivoaltiles Cu - CopperAl - Aluminum Ca - Calcium Fe - IronSb - Antimony Cd - Cadmium Hg - MercuryAs - Arsenic CN - Cyanide K - PotassiumBa - Barium Co - Cobalt Mg - MagnesiumBe - Beryllium Cr- Chromium Mn - Manganese

ICP Metals - TAL Metals without Mercury (Hg)Filtered - Samples have been filtered in the field

Na - SodiumNi - NickelPb - LeadPEST - PesticidesPR - Preliminary Results

Se - SeleniumTl- ThalliumV - VanadiumVOA - VolatilesZn - Zinc

ILM04.1 AnalysesTM - Total Metals CN - CyanideDM - Dissolved Metals

cJL

C

AR115283

Page 3: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

** CDA USEPA Contract Laboratory Program^St—* r^ Organic Traffic Report & Chain of Custody Record

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 828048990079

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By (Date / Time)

1 ;Q,Vl6 1 /<-)** / / G O

2

3

4

Sampler

Received By (Date / Time)

Case No: 32129DAS No: 1SDG No: L.

For Lab Use Only

Lab Contract No:

Unit Price:

Transfer To:

Lab Contract No:

Unit Price:

ORGANIC MATRIX/ CONG/ ANALYSIS' TAGNoJ STATION SAMPLE COILECT INORGANIC FOR LAB USE ONLYSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Boltes LOCATION DATE/TWE SAMPLE No. Sample Condii on On Receipt

C0047

C0048

Surface Water/Gene Nance

Surface Water/Gene Nance

UG BNA/PEST (14)

L/G BNA/PEST (14)

3216 (Ice Only), 3217 (Ice W05 8:9/3/2003 20:00 MC0047Only), 3218 (Ice Only), 3219(Ice Only) (4)3223 (Ice Only), 3224 (Ice W06 5:9/3/2003 20:15 MC0048Only), 3225 (Ice Only), 3226(Ice Only) (4)

Shipment for Case

Corrptefe?Y

Analysis Key:

BNA/PEST = CLP TCL £

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s): Cooler TemperatureUpon Receipt:

Concentration: L = Low. M = Low/Medium. H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Custody Seal Intact? I Shipment Iced?

emivolatiles and Pesticides/PC

TR Number: 3^84523714-090503-0001PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office. 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Ragel of 1

AR115284

Page 4: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

^XppA USEPA Contract Laboratory Program Case NO: 32129 Q^^ Organic Traffic Report & Chain of Custody Record DAS No t\.

Region: 3

Project Code:

AccountCode: 03T03N50102D0371RVOO

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage/WV

Project Leader: Gene Nance

Action: Removal Action

Sampling Co: Ecology & Environment, Inc.

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 828048990079

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By (Date / Time)

1 -&Y\G ^ ?A/« !>**

2

3

4

SamplerSignature: ^ f**~~-~-> "-

Received By (Date / Time)

ORGANIC MATRDO CONO ANALYSIS/ TAGNoJ STATION SAMPLE COLLECT INORGANIC QCSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Bottles LOCATION DATE/HME SAMPLE No. Type

C0047

C0048

Surface Water/Gene Nance

Surface Water/Gene Nance

L/G

L/G

BNA/PEST (14)

BNA/PEST(14)

3216 (Ice Only), 3217 (IceOnly), 3218 (Ice Only), 3219(Ice Only) (4)3223 (Ice Only), 3224 (IceOnly), 3225 (Ice Only), 3226(Ice Only) (4)

W05

W06

S: 9/3/2003 20:00 MC0047

S: 9/3/2003 20:15 MC0048

Shipment for Case

Complete? Y

Analysis Key:

BNA/PEST = CLP TCL

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: L = Low. M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

Semivoiatiles and Pesticides/HC

TR Number: 3-484523714-090503-0001PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYF2V5.1.043 Pagel of 1

AR115285

Page 5: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

^^CIpA USEPA Contract Laboratory Program Case NO: 32129 f}Organic Traffic Report & Chain of Custody Record DAS No IX

Region:

Project Code:

Account Code:

CERCLIS ID:

Spill ID:

Site Name/State

Project Leader:

Action:

Sampling Co:

ORGANICSAMPLE No.

C0042

C0046

C0049

3

03T03N50102D0371RVOO

WVD054827944

: Big John Salvage/WV

Gene NanceRemoval Action

Ecology & Environment, Inc.

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 828048990068

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By (Date / Time)

1 Jb^o-^-*- f /CA> / / O Q

2

3

4

SamplerSignature: -^-5 T\ a_~<_>-

Received By (Date / Time)

MATRIX/ CONC/ ANAYSe/ TAG No./ STATION SAMPLE COLLECT INORGANIC QCSAMPLER TYPE TUFWAROUND PRESERVATIVB Bodies LOCATION DATE/TWE SAMPLE No. Type

Surface Water/ L/G BNA/PEST (14) 3173 (Ice Only), 3174 (Ice W01 8:9/3/2003 17:45 MC0042 Lab QC : MS/MSDJoe Carter Only), 31 75 (Ice Only), 31 76

(Ice Only), 3177 (Ice Only),31 78 (Ice Only), 3179 (IceOnly), 31 80 (Ice Only), 3181(Ice Only), 3182 (Ice Only),31 83 (Ice Only), 3184 (IceOnly) (12)

Surface Water/ L/G BNA/PEST (14) 3209 (Ice Only), 3210 (Ice W04 8:9/3/2003 19:35 MC0046Gene Nance Only), 3211 (Ice Only), 3212

(Ice Only) (4)Surface Water/ L/G BNA/PEST (14) 3230 (Ice Only), 3231 (Ice W07 S: 9/3/2003 20:25 MC0049Gene Nance Only), 3232 (Ice Only), 3233

(Ice Only) (4)

Shipment for CaseComptefe?Y

Analysis Key:

BNA/PEST = CLP TCL

Sample(s) to be used for laboratory QC:

C0042

Additional Sampler Signature(s):

Concentration: i_ = Low, M = Low/Medium, H = High Type/Designate: Composite = C. Grab = G

Chain of Custody Seal Number:

Shipment Iced?

Semivolatnes and Peslicides/PC

TR Number: 3-484523714-090503-0002PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr.. Reston, VA 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYFZV5.1.043 Page 1 of 1

AR115286

Page 6: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

«P CDA USEPA Contract Laboratory Program^KyCrr^ organic Traffic Report & Chain of Custody Record

Date Shipped:

Carrier Name:

Airbill:

Shipped to:

ORGANICSAMPLE No.

9/5/2003

FedEx

828048990068

Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By

1^/A^^_

2

(Date / Time)

?/c/,, „**' /

3

4

MATRIX/ CONC/ ANALYSIS/

SAMPLER TYPE TURNAROUND

SamplerolyjMluns: r ** *- c—*^

Received By (Date / Time)

Case No: 32129DAS No: 1SDG No: L_

For Lab Use Only

Lab Contract No:

Unit Price:

Transfer To:

Lab Contract No:

Unit Price:

TAG No./ STATION SAMPLE COLLECT INORGANICPRESERVATIVE/ Bottes LOCATION DATE/TME SAMPLE No.

FOR LAB USE ONLYSample CondM on On Receipt

C0042 Surface Water/ UG BNA/PEST(14) 3173 (Ice Only), 3174 (Ice W01 8:9/3/2003 17:45 MC0042Joe Carter Only), 3175 (Ice Only), 3176

(Ice Only), 3177 (Ice Only),3178 (Ice Only), 3179 (IceOnly), 3180 (Ice Only), 3181(Ice Only), 3182 (Ice Only),3183 (Ice Only), 3184 (IceOnly) (12)

C0046 Surface Water/ L/G BNA/PEST(14) 3209 (Ice Only), 3210 (Ice W04 5:9/3/2003 19:35 MC0046Gene Nance Only), 3211 (Ice Only), 3212

(Ice Only) (4)C0049 Surface Water/ L/G BNA/PEST(14) 3230 (Ice Only), 3231 (Ice W07 8:9/3/2003 20:25 MC0049

Gene Nance Only). 3232 (Ice Only), 3233(Ice Only) (4)

Shipment (or CaseComptele?Y

Analysis Key:

BNA/PEST = CLP TCL S

Sample(s) to be used for laboratory QC:

C0042

Additional Sampler Slgnature(s): Cooler TemperatureUpon Receipt:

Concentration: L = Low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab - G

Chain of Custody Seal Number:

Custody Seal Intact? Shipment Iced?

>emivolatiles and Pesticides/PC

TR Number: 3-484523714-090503-0002PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office. 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Pagel of 1

AR115287

Page 7: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

J^PPA USEPA Contract Laboratory Program^^ Inorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code:

Account Code: 03T03N50102D0371RVOO

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage/WV

Project Leader: Gene Nance

Action: Removal Action

Sampling Co: Ecology & Environment, Inc.

INORGANIC MATRIX; CONC/ AN/M.YSB/SAMPLE No. SAMPLER TYPE TURNAROUND

MC0042 Surface Water/ UG TM (14)Joe Carter

MC0043 Surface Water/ UG TM (14)Gene Nance

MC0045 Surface Water/ UG TM (14)Gene Nance

MC0046 Surface Water/ UG TM (14)Gene Nance

MC0047 Surface Water/ UG TM (14)Gene Nance

MC0048 Surface Water/ UG TM (14)Gene Nance

MC0049 Surface Water/ UG TM (14)Gene Nance

MC0050 Surface Water/ UG TM (14)Gene Nance

MC0051 Field QC/ UG TM (14)Gene Nance

Date Shipped: 9/5/2003 Chair

Carrier Nam«r FedEx

Airbill: 837541203464 Re"nq

Shipped to: Bonner Analytical Testing ^ j~)

U0' -32703 Oak Grove Road lL

Hattiesburg MS 39402(601)264-2854 3

4

TAG No./ STATIONPRESERVATIVE/ Bottles LOCATION

3170 (HNO3), 3171 (HNO3), W013172(HNO3)(3)

3191 (HNO3)(1) W02

3201 (HNO3)(1) W03

3208(HNO3)(1) W04

3215(HNO3)(1) W05

3222(HNO3)(1) W06

3229(HN03)(1) W07

3236(HNO3)(1) W08

3243 (HNO3)(1) W09

Case No: 32129 [^DAS No: IX

i of Custody Record SamplerSigiature: .£> /Tff-v-c-^~-

ulshed By (Date / Time) Received By (Date / Time)

r\*w~->^_ tf/5/^ "a-i

SAMPLE COLLECT ORGANIC QCDATE/HME SAMPLE No. Type

8:9/3/2003 17:45 C0042 Lab QC : MS/MSD

S: 9/3/2003 18:50 C0043

8:9/3/2003 19:00 C0045 Field Duplicate of W02

S: 9/3/2003 19:35 C0046

S: 9/3/2003 20:00 C0047

S. 9/3/2003 20:15 C0048

S: 9/3/2003 20:25 C0049

S: 9/3/2003 20:35 C0050

S: 9/3/2003 20:50 C0051 Field Blank

Shipment for Case

Complete ?Y

Analysis Key:

TM = CLP TAL Total Me

Sample(s) to be used for laboratory QC:

MC0042

Additional Sampler Signatures):

Concentration: L = Low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G

Chain of Custody Seal Number:

Shipment Iced?

tals

TR Number: 3-484523714-090503-0003PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston. VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYF2V5.1.043 Page 1 of 1

AR115288

Page 8: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

*J F-PA USEPA Contract Laboratory ProgramSjf Cr.r\ inorganic Traffic Report & Chain of Custody Record

Date Shipper 9/5/2003

Carrier Name: FedEx

Airbill. 837541203464

Shipped to: Bonner Analytical TestingCo.2703 Oak Grove RoadHattiesburg MS 39402(601)264-2854

Chain of Custody Record

Relinquished By (Date / Time)

1 -^AV>-x^_^ f/£/o^ / y o o2

3

4

8*"i*f *> y^ri ^Siyuture ' "*~Received By (Date / Time)

Case No: 32129DAS No: 1

SDG No: 1

For Lab Use Only

Lab Contract No:

UnK Price:

Transfer To:

Lab Contract No.

UnK Price:

INORGANIC MATRIX/ CONG/ ANALYSIS/ TAGNoJ STATION SAMPLE OOILECT ORGANIC FOR LAB USE ONLYSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE Botles LOCATION DATE/nME SAMPLE No. Sample Core* on On Receipt

MC0042

MC0043

MC0045

MC0046

MC0047

MC0048

MC0049

MC0050

MC0051

Surface Water/Joe Carter

Surface Water/Gene Nance

Surface Water/Gene Nance

Surface Water/Gene Nance

Surface Water/Gene Nance

Surface Water/Gene Nance

Surface Water/Gene Nance

Surface Water/Gene Nance

Field QC/Gene Nance

L/G

L/G

UG

L/G

L/G

L/G

L/G

L/G

L/G

TM

TM

TM

TM

TM

TM

TM

TM

TM

(14)

(U)

(14)

(14)

(14)

(14)

(14)

(14)

(14)

3170(HNO3), 3171 (HNO3),3172 (HNO3) (3)

3191 (HNO3)(1)

3201 (HNO3)(1)

3208(HNO3)(1)

3215(HNO3)(1)

3222(HNO3)(1)

3229(HNO3)(1)

3236(HNO3)(1)

3243(HNO3)(1)

W01

W02

W03

W04

W05

W06

W07

W08

W09

S:

S:

S:

S:

S:

S:

S:

S:

S:

9/3/2003

9/3/2003

9/3/2003

9/3/2003

9/3/2003

9/3/2003

9/3/2003

9/3/2003

9/3/2003

17:45

18:50

19:00

19:35

20:00

20:15

20:25

20:35

20:50

C0042

C0043

C0045

C0046

C0047

C0048

C0049

C0050

C0051

Shipment (or CaseComplete ?Y

Analysis Key:

TM = CLP TAL Total Me

Sample<s) to be used for laboratory QC:

MC0042

Additional Sampler Signatures): Cooler TemperatureUpon Rec dpi:

Concentration: L = Low. M = LovWMedium. H = High Type/Designate: Composite - C. Grab = G

Chain of Custody Seal Number:

Custody Seal Intact? Shipment Iced?

tals

TR Number: 3-484523714-090503-0003PR provides preliminary results. Requests for preliminary result* will Increase analytical costs.Send Copy to: Sample Management Office. 2000 Edmund Halley Dr.. Reston, VA. 20191-3400 Phone 703/254-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Pagel of 1

AR115289

Page 9: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

^FR/X USEPA Contract Laboratory Program^^ Organic Traffic Report & Chain of Custody Record

Region: 3

Project Code:

Account Code: 63T03N50102O0371 RVOO

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage/WV

Project Leader: Gene Nance

Action: Removal Action

Sampling Co: Ecology & Environment, Inc.

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 828048990127

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Case No: 32129 O

DAS No: IX

Chain of Custody Record

Relinquished By (Date / Time)

1 ^n— _ V^/oi >'°°2

3

4

SamplerSignature ?^> f\ o-r~ c-*

Received By (Date / Time)

ORGANIC MATRIX/ CONO ANALYSIS/ TAG No./ STATION SAMPLE 00 LLECT INORGANIC QCSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. Type

C0043

COCK 5

Surface Water/Gene Nance

Surface Water/Gene Nance

L/G

UG

BNA/PEST (14)

BNA/PEST (14)

3192 (Ice Only), 3193 (IceOnly), 3194 (Ice Only), 3195(Ice Only) (4)3202 (Ice Only), 3203 (IceOnly), 3204 (Ice Only), 3205(Ice Only) (4)

W02

W03

S: 9/3/2003

S: 9/3/2003

18:50

19:00

MC0043

MC0045 Field Duplicate of W02

Shipment for Case

Comptete?/'Jfr«^

Analysis Key:

BNA/PEST = CLP TCL

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: |_ = Low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G

Chain of Custody Seal Number:

Shipment Iced?

iemivolatiles and Pesticides/HC

TR Number: 3-484523714-090403-0004PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYF2VS1.043 Page 1 of 1

AR115290

Page 10: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

*J PDA USEPA Contract Laboratory Program^Cr Ci /A organic Traffic Report & Chain of Custody Record

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 828048990127

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Rriinquterwd By (Oat* / Time)

1 X*KL_._ ?/^M nco2

3

4

SamplerSignature -£> Y\jtt-r~ <— 4—Received By (Date / Time)

Case No: 32129

DAS No: 1

SDG No: |_

For Lab Use Only

Lab Contract No:

Unit Price:

Transfer To:

Lab Contract No:

Unit Price:

ORGANIC MATRDO CONG ANALYSIS/ TAGNoJ STATION SAMPLE COLLECT INORGANIC FOR LAB USE ONLYSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Botles LOCATION DATE/TME SAMPLE No. Sample Condition On Receipt

C0043

C0045

Surface Water/Gene Nance

Surface Water/Gene Nance

UG BNA/PEST (14)

L/G BNA/PEST (14)

3192 (Ice Only), 3193 (Ice W02 8:9/3/2003 18:50 MC0043Only), 3194 (Ice Only), 3195(Ice Only) (4)3202 (Ice Only), 3203 (Ice W03 3:9/3/2003 19:00 MC0045Only), 3204 (Ice Only), 3205(Ice Only) (4)

Shipment (or CaseComplete?^ Uei

Analysis Key:

BNA7PEST = CLP TCL 5

Sample(s) to be used for laboratory QC: Additional Sampler Slgnature(s): Cooler TemperatureUpon Receipt:

Concentration: L = Low. M = Low/Medium, H = High Type/Designate: Composite - C, Grab = G

Chain of Custody Seal Number:

Custody Seal Intact? Shipment Iced?

emivolatiles and Pesticides/PC

TR Number: 3-484523714-090403-0004PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr.. Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Page 1 Of 1

AR115291

Page 11: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

^XpDA USEPA Contract Laboratory Program^^ Organic Traffic Report & Chain of Custody Record

Region: 3

Project Code:

Account Code: 03T03N50102D0371RVOO

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage/WV

Project Leader: Qene Nance

Action: Removal Action

Sampling Co: Ecology & Environment, Inc.

ORGANIC MATRDO CONG/ ANA.YS6/SAMPLE No. SAMPLER TYPE TURNAROUND

C0042 Surface Water/ UG VOA (14)Joe Carter

C0043 Surface Water/ UG VOA (14)Gene Nance

C0045 Surface Water/ UG VOA (14)Gene Nance

C0046 Surface Water/ UG VOA (14)Gene Nance

C0047 Surface Water/ UG VOA (14)Gene Nance

C0048 Surface Water/ UG VOA (14)Gene Nance

C0049 Surface Water/ UG VOA (14)Gene Nance

C0050 Surface Water/ UG VOA (14)Gene Nance

C0051 Field QC/ UG VOA (14)Gene Nance

C0052 Field QC/ UG VOA (14)Gene Nance

Date Shipped: 9/5/2003 Chail

Carrier Name* FedExRellnq

Airbill: 828048990116

Shipped to: Ceimic Corporation ' S3,iu uean Knauss LmveNarragansett Rl 02882 2

(401) /82-8900

4

TAGNOJ STATIONPRESERVATIVE/ Bottles LOCATION

3185 (HCL), 3186 (HCL), W013187 (HCL), 3188 (HCL),31 89 (HCL), 31 90 (HCL) (6)3196 (HCL), 3197 (HCL) (2) W02

3206 (HCL), 3207 (HCL) (2) W03

3213 (HCL), 3214 (HCL) (2) W04

3220 (HCL), 3221 (HCL) (2) W05

3227 (HCL), 3228 (HCL) (2) W06

3234 (HCL), 3235 (HCL) (2) W07

3241 (HCL), 3242 (HCL) (2) W08

3248 (HCL), 3249 (HCL) (2) W09

3250 (HCL), 3251 (HCL) (2) W10

Case No: 32129 O

DAS No: Iv

i of Custody Record S3"**"Signature ^^D/tA^-^-"

ulsMdBy (Date /Time) Received By (Date /Time)

f^~^^ 7/S/oi //oo

SAMPLE OOHECT INORGANIC QCDATE/TME SAMPLE No. Type

5:9/3/2003 17:45 MC0042 Lab QC : MS/MSD

S: 9/3/2003 18:50 MC0043

5:9/3/2003 19:00 MC0045 Field Duplicate of W02

S: 9/3/2003 19:35 MC0046

S: 9/3/2003 20:00 MC0047

S: 9/3/2003 20:15 MC0048

S: 9/3/2003 20:25 MC0049

S: 9/3/2003 20:35 MC0050

S: 9/3/2003 20:50 MC0051 Field Blank

S: 9/3/2003 20:55 Trip Blank

Shipment for CaseComplete? N

Analysis Key.

VOA = CLP TCL Volatile

Sample(s) to be used for laboratory QC:

C0042

Additional Sampler Slgnature(s):

Concentration: L = Low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab - G

Chain of Custody Seal Number:

Shipment Iced?

:s

TR Number: 3-484523714-090403-0005PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYF2V5.1.043 Pagel of 1

AR115292

Page 12: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

*J PDA USEPA Contract Laboratory Program^*y « ^ Organic Traffic Report & Chain of Custody Record

Date Shipped: 9/5/2003

Carrier Nam«: FedEx

Airbill: 828048990116

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By (Date / Time)

1 *>Y\o r »__ t/^/a*> HO&2

3

4

SamplerSigature ,£>/'U_^~t

Received By (Date / Time)

Case No: 32129DAS No: 1

SDG No: L_

For Lab Use Only

Lab Contract No

Unit Price:

Transfer To:

Lab Contract No:

Unit Price:

ORGANIC MATRDU CONC/ ANALYSIS/ TAGNoV STATION SAMPLECOLLECT INORGANIC FOR LAB USE OM.YSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Bottes LOCATION DATE/TWE SAMPLE No. Sample Condition On Receipt

C0042

C0043

C0045

C0046

C0047

C0048

C0049

C0050

C0051

C0052

Surface Water/ L/GJoe Carter

Surface Water/ L/GGene Nance

Surface Water/ UGGene Nance

Surface Water/ L/GGene Nance

Surface Water/ UGGene Nance

Surface Water/ L/GGene Nance

Surface Water/ L/GGene Nance

Surface Water/ UGGene Nance

Field QC/ UGGene Nance

Field QC/ UGGene Nance

VGA (14)

VOA (14)

VOA(14)

VOA (14)

VOA (14)

VOA (14)

VOA (14)

VOA (14)

VOA (14)

VOA (14)

3185 (HCL), 3186 (HCL), W013187 (HCL), 3188 (HCL),3189 (HCL), 31 90 (HCL) (6)3196 (HCL), 3197 (HCL) (2) W02

3206 (HCL), 3207 (HCL) (2) W03

3213 (HCL), 3214 (HCL) (2) W04

3220 (HCL), 3221 (HCL) (2) W05

3227 (HCL), 3228 (HCL) (2) W06

3234 (HCL), 3235 (HCL) (2) W07

3241 (HCL), 3242 (HCL) (2) W08

3248 (HCL), 3249 (HCL) (2) W09

3250 (HCL), 3251 (HCL) (2) W10

S: 9/3/2003 17:45 MC0042

S: 9/3/2003 18:50 MC0043

S: 9/3/2003 19:00 MC0045

S: 9/3/2003 19:35 MC0046

S: 9/3/2003 20:00 MC0047

S: 9/3/2003 20:15 MC0048

S: 9/3/2003 20:25 MC0049

S: 9/3/2003 20:35 MC0050

S: 9/3/2003 20:50 MC0051

S: 9/3/2003 20:55

Shipment for CaseComptete?N

Analysis Key:

VOA = CLP TCL Volatile

Sample(s) to be used for laboratory QC:

C0042

Additional Sampler Signature(s): Cooler TemperatureUpon Receipt:

Concentration: L = low, M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G

Chain of Custody Seal Number:

Custody Seal Intact? Shipment Iced?

S

TR Number: 3-484523714-090403-0005PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston, VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Page 1 of 1

AR115293

Page 13: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

£ CDA USEPA Contract Laboratory Program\XCi/n Organic Traffic Report & Chain of Custody Record

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 837541203453

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401)782-8900

Chain of Custody Record

Relinquished By (Date / Time)

S>/\C**—iJ^- ?/Oci ^ / fcO

2

3

4

Sampler „ _Signature "^ /w>— cJ» —

Received By (Date / Time)

Case No: 32129DAS No: 1SDG No: L_

For Lab Use Only

Lab Contract No:

Unit Price:

Transfer To:

Lab Contract No:

Unit Price:

ORGANIC MATRIX/ CONC/ AfWLYStS/ TAG No./ STATION SAMPLE CO LLECT INORGANIC FOR LAB USE ONLYSAMPLE No. SAMPLER TYPE TURNAROUND PRESERVATIVE/ Botles LOCATION DATE/TWE SAMPLE No. Sample Condition On Receipt

C0050 Surface Water/ L/G BNA/PEST (14) 3237 (Ice Only), 3238 (Ice W08 S: 9/3/2003 20:35 MC0050Gene Nance Only), 3239 (Ice Only), 3240

(Ice Only) (4)C0051 Field QC/ UG BNA/PEST (14) 3244 (Ice Only), 3245 (Ice W09 5:9/3/2003 20:50 MC0051

Gene Nance Only), 3246 (Ice Only), 3247(Ice Only) (4)

Shipment for CaseComplete TpToLt^

Analysis Key:

BNA/PEST = CLPTCLS

Sample(s) to be used for laboratory QC. Additional Sampler Signature(s): Cooler TemperatureUpon Receipt:

Concentration: L = Low. M = Low/Medium. H = High Type/Designate: Composite = C. Grab = G

Chain of Custody Seal Number:

Custody Seal Intact? Shipment Iced?

emivolatiles and Pesticides/PC

TR Number: 3-484523714-090403-0006PR provides preliminary results. Requests for preliminary results will Increase analytical costs.Send Copy to: Sample Management Office, 2000 Edmund Halley Dr., Reston. VA 20191-3400 Phone 703/264-9348 Fax 703/264-9222

LABORATORY COPYF2V5.1.043 Rage 1 of 1

AR115294

Page 14: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

^^CDA USEPA Contract Laboratory Program Case NO:^^ Organic Traffic Report & Chain of Custody Record DAS No

Region: 3

Project Code:

Account Code: 03T03N50102D0371RVOO

CERCLIS ID: WVD054827944

Spill ID:

Site Name/State: Big John Salvage/WV

Project Leader: Gene Nance

Action: Removal Action

Sampling Co: Ecology & Environment, Inc.

Date Shipped: 9/5/2003

Carrier Name: FedEx

Airbill: 837541203453

Shipped to: Ceimic Corporation10 Dean Knauss DriveNarragansett Rl 02882(401) 782-8900

Chain of Custody Record

Relinquished By (Date / Time)

1 /?n^-^»_ ?/c/>^ //o°/

3

4

32129 O

Sampler

Signature -^/f^^^j^

Received By (Date / Time)

ORGANIC MATRIX/ CONC/ ANALYSIS/ TAGNoJ STATION SAMPLE COLLECT INORGANIC QCSAMPLE No. SAMPLE* TYPE TURNAROUND PRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. Type

C0050

C0051

Surface Water/Gene Nance

Field QC/Gene Nance

UG

L/G

BNA/PEST(14)

BNA/PEST(14)

3237 (Ice Only), 3238 (IceOnly), 3239 (Ice Only), 3240(Ice Only) (4)3244 (Ice Only), 3245 (IceOnly), 3246 (Ice Only), 3247(Ice Only) (4)

W08

W09

S: 9/3/2003

S: 9/3/2003

20:35

20:50

MC0050

MC0051 Field Blank

Shipment fprCase

CompteteTjPft «•>

Analysis Key:

BNA/PEST = CLP TCL

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: |_ = Low. M = Low/Medium. H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

iemivolatiles and Pesticides/PC

TR Number: 3-484523714-090403-0006PR provides preliminary results. Requests for preliminary results will Increase analytical costs.

Send Copy to: Sample Management Office. 2000 Edmund Halley Dr., Reston. VA. 20191-3400 Phone 703/264-9348 Fax 703/264-9222

REGION COPYF2V5L1.043 Page 1 of 1

AR115295

Page 15: ecology and environment, inc. · 2019-12-16 · ecology and environment, inc. International Specialists in the Environment 131 Peninsula Street, Suite B Wheeling, West Virginia 26003

UPS Next Day Air Saver"

S h i p p i n g D o c u m e n t

See instructions on back. Call 1-8OOPICK-UPS (8OO-742-5877)for additional information.

TRACKING NUMBER

1 SHIPMENT FROMSHIPPER'S I

UPSACCOUNT

1Z5A450V 23 1000063 7

Y •

TFI FPMONE

; T Ai'

2 EXTREMELY URGENT DELIVERY TO

as

NEXT DAY

AIR SAVER

CHARGE

n S-MURHAv P;CKUP

s.. „«,„,.•.»»

OPTIONALSERVICES

INSUHR) VALUE ,Contents are attorrMically Jprotected ip lo $100 For injuredvalue ow $100. see inwuctiorm AMOUNT

D CO.DIt C O.D . erter *reur« KJ be

1JPSCOD i j to package AMOUNT6 ADDITIONAL

I HANDLINGCHARGE

TOTALCHARGES

n An Additional Handling Charge applies tor certainitems See instructions

SHIPPER'SCOPY

METHOD

OFPAYMENT D D D

1P1P

*zK

-it

till-

x

AR115296