SpectrAA Report.

Analyst Yusryanto, S.Pd

Date Started 9:18 PM 18/10/2015 Worksheet Nickel Yusryanto Comment Nickel Methods Ni Computer name DF9J5Q1S

Method: Ni (Flame)

Element - Matrix: Instrument Type:

Conc. Units:

Instrum ent Mode:

Sampling Mode: Calibration Mode:

Measurem ent Mode: Replicates Standard: Replicates Sample:

Expansion Factor: Minim um Reading:

Sm oothing:

Conc. Dec. Places:

Wavelength: Slit Width:

Gain:

Lamp Current:

Lamp Position:

Background Correction:

STANDARD 1: STANDARD 2: STANDARD 3:

STANDARD 4:

STANDARD 5:

STANDARD 6

Reslope Rate:

Reslope Standard No.:

Reslope Lower Limit:

Reslope Upper Limit: Recalibration Rate: Calibration Algorithm :

Cal. Lower Limit:

Cal. Upper Limit:

SIPS:

Measurement Time: Pre-Read Delay: Flame Type: Air Flow :

Acetylene Flow :

Burner Height:

RSD Limit: RSD Test Min. Abs:

9:47 PM 18/10/2015

Ni - Flame

mg/L

Absorbance

Manual

Concentration

Integrate 3

3

1.0 Disabled

6 point

6

232.0 nm 0.2 nm

69 %

4.0 mA

4

BC Off

10.000 mg/L 25.000 mg/L

30.000 mg/L

45.000 mg/L

50.000 mg/L

60.000 mg/L

50

2

75.0 %

125.0 % 100

New Rational

20.0 %

150.0 %

Off

5.0 s 10 s Air/Acetylene

10.00 L/min

2.00 L/min

0.0 mm

5.0 % 0.1000 Abs

Page 1 of 2

SpectrAA Report.

Sample ID

CAL ZERO

Conc mg/L

0.000m

0.2544

STANDARD 1 10.000m

Readings

0.3046

STANDARD 2 25.000m

Readings

0.7638

STANDARD 3 30.000m

Readings

0.9001

STANDARD 4 45.000m

Readings

1.3053

STANDARD 5 50.000m

Readings

1.4849

STANDARD 6 60.000

Readings

1.6073

Abs 0.64 0.40

0.20

0.00

New Rational - Cal. Set 3

Curve Fit

Characteristic Conc

r

Calculated Conc

Residuals Abs = 0.00000 x C

= New Rational

= ******

= ******

= 0.000 0.000 0.000 0.000 0.000 0.000

= 0.000 2.000 3.000 7.000 13.000 12.000

Sample A1 53.7125

Readings

1.5176

Sample A2 52.8848

Readings

1.5003

Sample B1 45.8711

Readings

1.3091

Sample B2 47.6902

Readings

1.3589

00.5

11.5

2

0 10 20 30 40 50 60

Ni mg/L

9:47 PM 18/10/2015

Conc mg/L

0.000m

%RSD

0.1

SD

0.0002

Mean Abs

0.2543

0.2544 0.2540

0.2543

18/10/2015

.000m 0.3 0.0033 0.3009

Readings

0.3046 0.2997 0.2984 18/10/2015

.000m 2.3 0.0010 0.7678

Readings

0.7638 0.7706 0.7691 18/10/2015

30.000m 2.5 0.0010 0.9002

Readings

0.9001 0.9002 0.9004 18/10/2015

.000m 1.1 0.0033 1.3071

Readings

1.3053 1.3040 1.3120 18/10/2015

.000m 0.2 0.0109 1.4842

Readings

1.4849 1.4852 1.4824 18/10/2015

.000m 0.1 0.0010 1.6087

Readings

1.6073 1.6104 1.6085 18/10/2015

= New Rational

= 0.000 0.000 0.000 0.000 0.000 0.000

= 0.000 2.000 3.000 7.000 13.000 12.000

53.7125m 0.1 0.0010 1.5211

Readings

1.5176 1.5219 1.5237 18/10/2015

52.8848m 0.1 0.0010 1.4874

Readings

1.5003 1.4901 1.4719 18/10/2015

45.8711m 0.2 0.0023 1.3101

Readings

1.3091 1.3102 1.3111 18/10/2015

47.6902m 0.2 0.0023 1.3591

Readings

1.3589 1.3598 1.3585 18/10/2015

70

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