prpremexemexreactor ag

hpm

twister

twis

ter

premex reactor agindustriestrasse 11p.o.box 4442543 lengnau/switzerland+41 (0)32 653 01 52+41 (0)32 652 11 80www.premex-reactorag.choffice@premex-reactorag.ch

delivery addresscorrespondence address

phonefax

internete-mail

Equipment for research, developmentand production in chemical, pharma-ceutical and related industries.

autoclavet w i s t e r

We are proud to present another of our success stories – the hpm-twister, an innovative and amazingly versatileproduct that can be used in a range of applications.

Premex Reactor AG - one step aheadof technology!

hpm-t

t h e

innovativePressure station on standThe pressure gauge and measuringtransducer are vital instruments,which are combined in the stand-mounted pressure station. Coiled spiralpipework is used to pass pressurereadings from the interior of the auto-clave to the instruments.

Rest for autoclave coverThe rest for the autoclave cover isanother practical idea. The magneticstirrer head and all the other fittingscan be removed from the vessel togetherwith the autoclave cover, then carefullyplaced on the rest. The flexible pipeworkis easy to manoeuvre. The submergedtubes and the stirrer are left untouch-ed, suspended from the rest. At thispoint the vessel can be removed.

Socket panel on standConnecting our “twister” couldn’t beeasier. A panel on the stand includesall the sockets you need for connect-ing to the “c-m2” control unit.

Swivel attachment for stirrer motorThe precision swivel attachment meansthat the stirrer motor can be disen-gaged from its flexible engagementcoupling and swung out to one side.The speed of the stirrer motor is deter-mined by the “c-m2” control unit.

Heating or cooling units and removing the vesselPremex Reactor AG offers two alterna-tive heating and cooling systems forthe “twister”. You can choose eitherelectric heating or a double-shell designusing thermal oil. The standard equip-ment for electric heating includes analuminium shell incorporating theheating elements and the cooling spiralfor cold water. Heat is transferredquickly and evenly from the aluminiumshell to the autoclave vessel, via a copper shell. The end result is an eventransfer of heat, with no sudden tem-perature increases. The cooling spiral is extremely effective and is sufficient,under normal circumstances even forexothermal reactions. The double-shellthermal oil heating/cooling is alsodesigned in two parts. The outer seg-ment is the double shell, equipped withfins to guide the oil. Copper, the optimumconductor of heat, is used here too,transferring the heat inwards to theautoclave vessel. Something else thatmakes Premex Reactor AG heatingsystems so special is the ability toremove the autoclave as a completelyseparate unit.

Flexible pipeworkThe pipework used by Premex ReactorAG is as flexible as we are. Coiled pipesrun from the autoclave cover to thefixed connections, providing maximumfreedom of movement. The autoclavecover can be lifted, complete with itsfittings, and placed in its rest withoutthe need to disconnect any of the valves or connections. That means it is never difficult to remove the vesselfor emptying or cleaning.Coolant supply and return

We keep the “twister” cool so you canconcentrate on other things. The cool-ing system is a complete package – withthe electric cooling valve in the base,the supply and return pipes on thestand, and the power supply on thesocket panel.

well designedflexible

Jaw lockThe jaw lock is easy to open and closewith no force required. Our secret? Thelock is in two halves that close aroundthe autoclave and are sealed effort-lessly using a hand wheel.

AC motor controlled by a frequencyconverter. A flexible coupling is usedto connect it to the magnetic stirrerhead.

Swivel attachment for stirrer drive.The stirrer motor can be swung in andout until it reaches the precision stop.

Stand-mounted pressure station,including pressure gauge and measu-ring transducer, connected to the auto-clave cover by means of coiled pipes.

Stand with socket panel on sidefor electrical connections.

Frame mount for fixed connec-tions. Flexible coiled pipes run fromthe autoclave cover to the fixed connections.

Flexible coiled pipes work likesprings to provide maximum freedomof movement.

Magnetic stirrer head, completewith engagement coupling (for con-necting to motor). The speed can bemeasured directly at the drive shaft ofthe magnetic stirrer head, with thereadings processed digitally.

The standard unit is supplied withthe following fittings: sample-takingvalve with submerged tube to the bottom of the autoclave, gas inputvalve, pressure release valve, springpressure safety valve, submerged temperature sensor and connection to stand-mounted pressure station.

Practical rest for the autoclavecover.

There is a choice of gas injectionstirrer, disk blade stirrer, propellerstirrer or anchor stirrer. One of thesestirrer options is supplied with theautoclave.

Premex Reactor AG offers two different lock systems: the tried-and-tested jaw lock, or high-tensile boltsand nuts for pressures exceeding 200 bar.

1

2

3

4

5

6

7

8

9

10

11

The autoclave vessel can be remo-ved from the heating/cooling unit as aseparate unit. In the locking systemusing the two half jaws, the sealingring rests loose in the autoclave vessel.In the high-tensile bolt system, the flatseal is fixed to the autoclave cover.

In the jaw lock system, the O ringseal between autoclave cover and vessel is made of Kalrez, EPDM or Viton.The standard model can be used fortemperatures up to 250°C with a Kalrezseal. The high-tensile bolt system usesflat seals made of pure silver, PTFE car-bon or Graphoil. The standard model,when used for temperatures up to350°C, is supplied with a silver seal.

We offer two different heating/cooling systems – one using electricheating, and the other using a doubleshell for thermal oil. The electric systemincorporates the heating elements anda cooling spiral for cold water withinan aluminium block. Heat as well ascold are transferred via the aluminiumblock to the inner copper shell, and onto the autoclave vessel. The thermal oilsystem uses a double-shell design. This double-shell is equipped with finsto guide the oil, and an inner coppershell transfers the heat, as well as cold,on to the autoclave vessel.

The rear of the autoclave baseincludes two plug-type connectionsfor coolant supply and return. The cooling valve is built into the base. Theplug-type connections and the coolingvalve are only fitted on models usingthe electric heating system.

12

13

14

15

in every particular

1

2

3

4

5

7

8

9

10

11

14

15

6

13

12

perfectly

Perfectly formed technology, tested inevery particular. We renew this philo-sophy every day. We are proud of theperformance of our high-pressureautoclaves.

form

ed

data

technicalt w i s t e rhpm

High-pressure autoclaveType: hpm-twisterModel: Jaw lock

Electric heating

hpm-t-0070eb hpm-t-0125eb hpm-t-0380eb hpm-t-0600eb hpm-t-1200ebRated volume, l 0,07 0,125 0,38 0,6 1,2Working volume, l 0,05 0,1 0,3 0,5 1,0Working temperature, °C 250 250 250 250 250Working pressure, bar 200 200 200 150 80Autoclave material AISI 316 Ti 316 Ti 316 Ti 316 Ti 316 TiFittings material AISI 316 316 316 316 316Torque of magnetic coupling, Ncm 20 20 40 60 90Rated output of AC motor, W 40 40 120 120 120Drive shaft speed, rpm * 200–1500 200-1500 200-1500 200-1500 200-1500Heating output, W 1000 1200 1500 2000 2500Cooling output, W 2000 2400 3000 4000 5000Cover connections 1 / 8’’G 1 / 8’’G 1 / 4’’G 1 / 4’’G 1 / 4’’GUnit width A, mm 200 200 200 200 280Overall width B, mm 430 430 450 480 600Unit depth C, mm 380 380 380 380 450Height D, mm 650 650 720 750 800

Double-shell thermal oil heating

hpm-t-0070ob hpm-t-0125ob hpm-t-0380ob hpm-t-0600ob hpm-t-1200obRated volume, l 0,07 0,125 0,38 0,6 1,2Working volume, l 0,05 0,1 0,3 0,5 1,0Working temperature, °C 250 250 250 250 250Working pressure, bar 200 200 200 150 80Autoclave material AISI 316 Ti 316 Ti 316 Ti 316 Ti 316 TiFittings material AISI 316 316 316 316 316Torque of magnetic coupling, Ncm 20 20 40 60 90Rated output of AC motor, W 40 40 120 120 120Drive shaft speed, rpm * 200–1500 200-1500 200-1500 200-1500 200-1500Heating output, W 1000 1200 1500 2000 2500Cooling output, W 2000 2400 3000 4000 5000Cover connections 1 / 8’’G 1 / 8’’G 1 / 4’’G 1 / 4’’G 1 / 4’’GUnit width A, mm 200 200 200 200 280Overall width B, mm 430 430 450 480 600Unit depth C, mm 380 380 380 380 450Height D, mm 650 650 720 750 800* adjustable for other speeds

e = electric heatingo = double-shell heatingb = jaw lockd = high-tensile bolt lock

High-pressure autoclaveType: hpm-twisterModel: High-tensile bolt lock

Electric heating

hpm-t-0125ed hpm-t-0380ed hpm-t-0600ed hpm-t-1200edRated volume, l 0,125 0,38 0,6 1,2Working volume, l 0,1 0,3 0,5 1,0Working temperature, °C 350 350 350 350Working pressure, bar 325 325 325 325Autoclave material AISI 316 Ti 316 Ti 316 Ti 316 TiFittings material AISI 316 316 316 316Torque of magnetic coupling, Ncm 20 40 60 90Rated output of AC motor, W 40 120 120 120Drive shaft speed, rpm * 200-1500 200-1500 200-1500 200-1500Heating output, W 1200 1500 2000 2500Cooling output, W 2400 3000 4000 5000Cover connections 1 / 4’’G 1 / 4’’G 1 / 4’’G 1 / 4’’GUnit width A, mm 200 200 200 280Overall width B, mm 450 470 500 630Unit depth C, mm 380 380 380 450Height D, mm 650 720 750 800

Double-shell thermal oil heating

hpm-t-0125od hpm-t-0380od hpm-t-0600od hpm-t-1200odRated volume, l 0,125 0,38 0,6 1,2Working volume, l 0,1 0,3 0,5 1,0Working temperature, °C 350 350 350 350Working pressure, bar 325 325 325 325Autoclave material AISI 316 Ti 316 Ti 316 Ti 316 TiFittings material AISI 316 316 316 316Torque of magnetic coupling, Ncm 20 40 60 90Rated output of AC motor, W 40 120 120 120Drive shaft speed, rpm * 200-1500 200-1500 200-1500 200-1500Heating output, W 1200 1500 2000 2500Cooling output, W 2400 3000 4000 5000Cover connections 1 / 4’’G 1 / 4’’G 1 / 4’’G 1 / 4’’GUnit width A, mm 200 200 200 280Overall width B, mm 450 470 500 630Unit depth C, mm 380 380 380 450Height D, mm 650 720 750 800* adjustable for other speeds

e = electric heatingo = double-shell heatingb = jaw lockd = high-tensile bolt lock

auto

klav

en

Control unit case. A modern,light-grey aluminium case, with anintegral three-position support thatdoubles as a carrying handle. Thenatural silver coloured front and rearpanels have abrasion-resistant mar-kings, anodised under the final coating.The “c-m2” control unit is 320 mmwide (including support), 350 mmdeep and 210 mm high.

The AC758 controller is a cascadecontroller and programmable control-ler combined. A cascade controller isable to regulate the internal temper-ature and shell temperature simultan-eously, thereby preventing the internaltemperature rising above the set value.The software-based “programmablecontroller” can be used to implementsmall and large scale temperatureprograms, with gradual temperaturechanges, holding times and sequentialoperations. And there is more – theAC758 controller includes a digitalmotor speed indicator at the bottomright of the display.

SA3 security switch. This safetycut-out monitors the internal temper-ature and/or shell temperature, check-ing it against an adjustable maximumsetting. If the temperature exceeds themaximum setting, the heating is cutoff with no override possible. The cooling remains unaffected. The upperdisplay of the security switch alsoshows the pressure inside the reactor.

Main switch. The green illumin-ated pushbutton is used to switch onthe power to all components in thecontrol system.

Heating switch. The red illumin-ated pushbutton can be used to switchthe heating on and off independentlyof the controller.

Cooling switch. Pressing the blue illuminated pushbutton activates cooling immediately, independently of the controller. To activate “controllercooling”, this function must be switched off.

Stirrer switch. The yellow illumin-ated pushbutton switches the stirreron and off.

Stirrer motor speed control.The central component in controllingthe stirrer motor is the potentiometer(rotary knob). The speed is shown inrpm at the bottom right of the AC758controller display. The fuses are at therear of the control unit, with electricalplug-type connections for attachingthe autoclave.

Connection to stirrer motor.A seven-pin plug is used to connect tothe stirrer motor. The stirrer motor iscontrolled by the built-in frequencyconverter, which has a maximum loadof 370 W.

Connection to heating.A four-pin, two-phase plug is used asthe main heating connection. Maxi-mum heating output: 3000 W.

Connection to cooling valve.A three-pin plug is used as the connec-tion to the cooling valve integrated intothe autoclave frame. It is controlledautomatically via the programmablecontroller, or manually by pressing theilluminated pushbutton.

Connection to temperature sen-sor 1. This connection is used to attachthe 2 x Pt100 temperature sensor (threeleads) of type K or type N, and allowsthe temperature inside the medium tobe measured (product temperature).

Connection to temperaturesensor 2. This is the connection for the2 x Pt100 temperature sensor (threeleads) used for monitoring the heatingcontrol and security switch. If type K or type N sensors are used, it onlyperforms the function of heatingmonitoring – an additional connectionis required for the security switch.

Connection to temperaturesensor 3. A connection for a type K ortype N sensor carrying out the securityswitch function.

Connection to motor speed display. A two-pin plug is used totransmit the measured speed of thestirrer to the AC758 controller, where it is shown in the lower display.

Connection to emergency cooling valve. This connection is usedto control an emergency cooling valvewhich is regulated by an adjustablealarm signal at the temperature con-troller. This optional extra is requiredfor strongly exothermal reactions.

Analogue output to printer. Theanalogue printer output means thatdata – such as product temperaturereadings, heating readings, mediumtemperature settings or the speed ofthe stirrer motor – can be permanentlyrecorded.

Connection to pressure indi-cator. This socket is used to transmitthe pressure reading from the pressuremeasuring transducer to the SA3 –security switch, where the pressure isshown in bar at the top of the display.

RS485 interface. When used incombination with the specially develop-ed software suite, the RS485 data logging and PC connection interfaceopens up a wealth of applications. Thetwo sockets, one above the other, makeit possible to interconnect a number of control units, or connect auxiliaryequipment via the software.

Socket for mains power230 V/ A.

Fuses for heating, one for eachphase, 2 x 10 A.

Fuse for electronic system, 2.5 A.

1

2

3

4

5

7

8

9

10

11

12

13

14

Premex Reactor AG offers a fully-integrated concept, encompassing thehigh-pressure autoclave, the controlunit, and the online visualisation soft-ware. The “c-m2” control unit describedhere was designed specifically to regulate and control high-pressureautoclaves.

6

15

16

17

18

19

20

21

22

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15 16 17 1819

20

21 22

systematic

auto

clav

e

cont

rol

c-m

2

Pressure

Heater

Cooling-

valve

CH-254

3 LENGN

AU

1

ESS

Alarm

REAL

2

RPM

SP2

% P

REAL

1+2

START

STOP

P

1

2

STIRRER

MOTOR

PR

EMEX R

EACTOR

AG

CH-25

43 Leng

nau

Security

Switch

RPM

Cooling

Main Sw

itch

Heating

Tempera

ture Con

troller

Stirrer

PREMEX

REACT

OR AG

h.m.

Alarm

SP

S2

P

S3

S2

S1

SA 3

P

STOP

RESET

Master

E.SP

2Slav

eoutp

ut

SP2

RAMP

REAL

1

SP1

RPM INPU

T

C1

Sens.1

Sens.3

MAIN INPU

T

Sens.2

COOLING

VALVE 2

4V DC

HEATER

ANAL. OU

T

C3

F1=10A/F

2=10A/F3

=3.15A

C5/C6:RS

485

PRESSURE

C4

EXT. SP

C2

Stirrer m

otor

AC758

Internal

tempera

ture sen

sor

External

tempera

ture sen

sor (hea

ting)

Electrica

l connect

ions

on fram

e

Stirrer s

peed

Online and FlowchartWhile the experiment is underway, “allview” generates an x-y chart on thescreen, just like a standard plotter out-put. The real-time chart plots curves fortemperature, pressure, stirrer speed,etc. in relation to the duration of theexperiment. The standard software issupplied with “Flowchart”, whichdisplays in real time all the importantreadings in a diagram of the high-

The “allview” data capture and recording software allows the user tovisualise the progress of the experi-ment in real time on a PC screen, whilealso storing all relevant readings in an ASCII or Excel file.

pressure autoclave. This componentallows the user to track and monitorprogress in the system (outside thereaction cavity) directly on the screen.

ReadingsThe following readings can be display-ed from experiments carried out in theautoclave:– Internal temperature reading of

autoclave in °C– Internal temperature setting of

autoclave in °C– Shell temperature reading of

autoclave in °C– Shell temperature setting of

autoclave in °C– Heating and cooling output of the

heating block– Stirrer speed in rpm– Autoclave pressure in bar– Safety limit /cut-out value in °C

“allview” interface The latest release of “allview” requires a Windows interface, i.e. Windows 95,Windows 98 or Windows NT 4.0. Be-cause Windows NT 4.0 is a multitaskingenvironment, a number of applicationscan be run simultaneously, for example“allview” with Excel or MS Word.

PC hardware requirementsThe main hardware requirements are as follows:– Pentium processor, 266 MHz or higher– At least 64 Mb RAM, preferably

128 Mb– Good graphics board with at least

8Mb RAM– At least 6 Gb hard disk– At least 17” screen, with sufficiently

high resolution

Requirements for connecting control unit to PCTo get the application running, the following items are necessary in addition to the PC:– RS232/RS485 interface converter including dongle,

from Premex Reactor AG– Cable to connect converter to PC– Cable to connect converter to “c-m2” control unit

(standard length 2m)

allview

soft

war

e

Wor

king

pre

ssur

e80

bar

150

bar

200

bar

325

bar

700

bar*

Wor

king

tem

pera

ture

250

°C35

0°C

Mat

eria

lSta

ndar

dAI

SI 3

16Ti

– D

IN 1

.457

1AI

SI 6

60 –

DIN

1.4

980*

Allo

y C2

2 –

DIN

2.4

602*

Allo

y C2

76 –

DIN

2.4

819*

Tita

nium

Gra

de 2

– D

IN 3

.703

5*Sp

ecia

l mat

eria

ls on

requ

est:

Allo

y B2

/3 –

DIN

2.4

617/

2.46

00Al

loy

400

– DI

N 2

.436

0Al

loy

600

– DI

N 2

.481

6Al

loy

718

– DI

N 2

.466

8Zi

rcon

ium

Gra

de 7

02Ta

ntal

umN

imon

ic 1

05 –

DIN

2.4

634

Cove

r loc

kFa

st-a

ctin

g ja

w lo

ckHi

gh-t

ensil

e bo

lts a

nd n

uts

Auto

clav

e se

alEl

asto

mer

O ri

ngs:

EPDM

*Vi

ton*

Kalre

zFl

at se

als:

Pure

silv

erPT

FE ca

rbon

*Gr

apho

il*St

irrer

ele

men

tGa

s inj

ectio

n st

irrer

Prop

elle

r stir

rer

Disk

bla

de st

irrer

Anch

or st

irrer

Fitt

ings

Site

c val

ves (

Nov

a va

lves

)W

hite

y va

lves

Pres

sure

inst

rum

ents

Pres

sure

gau

geM

easu

ring

tran

sduc

erSe

nsin

g m

embr

ane

HC/T

i*Te

mpe

ratu

re se

nsor

sTy

pe K

*Ty

pe N

*Ty

pe P

t100

Mag

netic

stirr

er h

ead

Type

MIN

I 100

MRK

10–

17 se

ries

MRK

30–

37* s

erie

sTo

rque

of m

agne

tic20

Ncm

coup

ling

40 N

cm60

Ncm

90 N

cmDr

ive

shaf

t bea

ring

CN st

eel b

all b

earin

gsPT

FE/c

arbo

n fr

ictio

n be

arin

gs*

Carb

on/g

raph

ite C

BT fr

ictio

n be

arin

gs*

AC m

otor

Pow

er su

pply

:3

x 400

/240

V, 5

0 Hz

Rate

d ou

tput

:40

W12

0 W

Outp

ut sp

eed

200–

1500

rpm

(bal

l bea

rings

)20

0–13

00 rp

m (f

rictio

n be

arin

gs)

Heat

ing

syst

emEl

ectr

ic h

eatin

gDo

uble

-she

ll he

atin

gOp

tions

for

Insp

ectio

n w

indo

wst

anda

rd m

odel

sGa

s flo

w m

eter

pH e

lect

rode

pH p

rote

ctiv

e tu

be in

SS/

HC/T

iLe

vel p

robe

in S

S/HC

IR m

anom

etric

pro

beCa

taly

st ca

ge w

ith b

affle

Com

puta

tion

and

Com

puta

tion

as p

er TÜ

V gu

idel

ines

acce

ptan

ceIte

m su

bjec

t to

com

pulso

ry a

ccep

tanc

eN

ot su

bjec

t to

com

pulso

ry a

ccep

tanc

eCa

scad

e co

ntro

l“c

-m2”

cont

rol u

nit

LR3-

S-75

0 co

ntro

l uni

tPC

soft

war

e“a

llvie

w” V

1.0

X“a

llvie

w” V

3.0

X

Doub

le-s

hell

heat

ing

Elec

tric

hea

ting

Elec

tric

hea

ting

Doub

le-s

hell

heat

ing

Hig

h-te

nsile

bol

t lo

ckJa

w lo

ck• • •

•

•

•

•

•

•

•

•

•

•

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • • • • • • • • • • •

• • • • • • • • • • • • • • • •

•

•

•

•

• • • • • • • •

Mod

el c

odes

e =

Elec

tric

hea

ting

o =

Doub

le-s

hell

heat

ing

b =

Jaw

lock

d =

High

-ten

sile

bolt

lock

* Ava

ilabl

e

hpm-t-1200odVol. 1200 mlhpm-t-0600odVol. 600 mlhpm-t-0380odVol. 380 mlhpm-t-0125odVol. 125 mlhpm-t-1200edVol. 1200 mlhpm-t-0600edVol. 600 mlhpm-t-0380edVol. 380 mlhpm-t-0125edVol. 125 mlhpm-t-1200obVol. 1200 mlhpm-t-0600obVol. 600 mlhpm-t-0380obVol. 380 mlhpm-t-0125obVol. 125 mlhpm-t-0070obVol. 70 mlhpm-t-1200ebVol. 1200 mlhpm-t-0600ebVol. 600 mlhpm-t-0380ebVol. 380 mlhpm-t-0125ebVol. 125 mlhpm-t-0070ebVol. 70 ml

Stan

dard