•i r - Superfund Records Collections | US Environmental ... · IV CONCLUSION fi RECOMMENDATIONS 8 TABLES ... the top of the underlying silt-clay stratum. Test pits, performed in

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.0

TYBOUTS CORNER LANDFILLRD/RA STATEMENT OF WORK PLAN

TASK ITEM ILC

Subsurface Evaluation'Ward Clay"

Borrow Source Prequalification

Prepared for:

Tybouts Corner Landfill Trust FundManagement Steering Committee

Prepared by:

DPL Consultants

W.0.0323.HH.08 2 August 1990

AR000780

SUBSURFACE EVALUATION

"WARD CLAV"BORROW SOURCE PREQUALIFICATION

Prepared for:Tybouts Corner Landfill TrustManagement steering Committee

Prepared by:DPL Consultants

A*.Glenn K. Elliott, P.G.

W.O. 0323-HH-08 02 August 1990

AR00078

ABSTRACT

A subsurface exploration, based on 23 backhoe excavated test pits,was performed to evaluate the soil borrow potential of the "Pit 3"parcel, pit 3 is a mined out sand and gravel borrow site, locatedapproximately 2,000 feet southwesterly of the Tybouts CornerLandfill. The purpose of the exploration is an evaluation of thefeasibility of using these soils in constructing a "low permeability"cap for the landfill.The data indicate that the soils of the Pit 3 area can becharacterized into two (2) textural horizons: a sandy overburdenstratum of variable thickness overlying massive, variegated silt-claydeposits of the Potomac Formation. These silt-clays generallyconsist of low plasticity clay with interlayered high plasticitysilt-clays. Laboratory tests indicated that permeability values inthe range of l x 10'a cm/sec can be achieved at a compaction ofapproximately 90* standard Proctor density; well below the specifiedmaximum allowable permeability of 1 x lQ'f cm/sec. Environmentalanalyses do not indicate, based on current guidelines, apparentenvironmental constraints, which would preclude the use of thesesoils in construction of the proposed landfill cap.The data indicate that these Potomac Formation silt-clays arepotentially suitable for use in construction of the proposed lowpermeability cap for the Tybouts Landfill. An approximately 17 acre"proposed borrow area" has been delimited on the basis of theexploration data.

'UR000782

TABLE OF CONTENTS

Section ________liilS________ Page

I INTRODUCTION 1

II SUBSURFACE EXPLORATION 1Field Exploration 1Soils Laboratory Data 2Soil Quality Analysis 3

III EVALUATION 4Site conditions 4silt-Clay soil Borrow 5Borrow Area 7

IV CONCLUSION fi RECOMMENDATIONS 8

TABLES

TABLE 1 Soils Laboratory - Index TestsTABLE 2 Soil Engineering Property TestsTABLE 3 Target Compound List (TCL) OrganicsTABLE 4 Target Analyte List (TAL) Inorganic AnalysesTABLE 5 Comparison Total Sample & EP Toxicity

Leachate Analyses

FIGURES

FIGURE 1 Area SketchFIGURE 2 Test Pit Location SketchFIGURE 3 Proposed Silt-Clay Borrow Area

APPENDICES

APPENDIX A Test Pit Descriptive LogsAPPENDIX B Standard Proctor Test Moisture-Density CurvesAPPENDIX C Laboratory Analysis ReportsAPPENDIX D Laboratory Data Validation Reports

flf?OQ0783

_ I. INTRODUCTION

This report summarizes a subsurface exploration of soil borrowpotential on the land parcel, designated "Pit 3", which is a"mined out" sand and gravel borrow site, owned by W. c. Ward.

'*• The Pit 3 site is located west of U.S. Route 13 and south of RedLion Creek, approximately 2,000 feet southwesterly of theTybouts Corner Landfill, as indicated on Figure 1, Area Sketch.The proposed Tybouts Corner Landfill remediation requires anestimated 160,000 - 240,000 cubic yards of "low permeability"(1 x 10'6 cm/sec or less) silt-clay for capping of the landfill.Previous mining of sand and gravel borrow has exposed thevariegated silt-clays of the Potomac Formation across a portionof the Pit 3 site. The purpose of this exploration is anevaluation of the texture, engineering properties andenvironmental quality of these Potomac silt-clays as a potentialborrow source for cap construction.This exploration has been performed in general accordance withthe following:

o Tybouts Corner Landfill RD/RA, Statement of Work Plan;o Tybouts Corner Landfill Remedial Design/Remedial Action:

Field Sampling Plan (February 1990); ando Mini-Work Plan, Tybouts Corner Landfill, Borrow Source

Pre-Qualification, Ward Clay (March 1990).

II. SUBSURFACE EXPLORATION

Field Exploration.

Field exploration consisted of backhoe excavated test pits,performed at the approximate locations indicated on Figure 2,Test Pit Location Sketch. Twenty-three (23) exploration testpits, designated TP-A through W, were performed on 22 and 26March 1990 to expose the subsurface soil/sediment profile forvisual review and to obtain samples for textural evaluation andclassification. In the field review and logging of the test pitexcavations and field sampling were performed by a DPLConsultants geologist. Descriptive Logs for the explorationtest pits are attached as Appendix A.

Five (5) supplemental test pits were performed on 29 March 1990to obtain bulk samples for engineering property testing andenvironmental quality analysis. Approximate test pit locationsare indicated on Figure 2. These test pits were performedimmediately adjacent to previously excavated exploration testpit locations, selected on the basis of indicated subsurface

flR00078l*

conditions. The supplemental test pit locations were selectedto provide areal and depth coverage, throughout the area ofexploration, along with samples encompassing the range in soilclassifications, encountered by the exploration test pits.Supplemental test pits and sample depth intervals are asfollows:

Sample Depth IntervalTest Pit No. (Below Existing Grade)

G-l 5-7 feet

1-1 5-7 feet

L-l 7-9 feet

N-l 4-6 feet

S-l 1-2 feet

Soils Laboratory Data

Index TestingLaboratory textural evaluation of selected soil samples fromboth the exploration and supplemental test pits wasperformed to aid in classification and characterization ofthe soils encountered by the test pits. Soil sampleevaluation included:

o Soil moisture content (as sampled) — ASTM:D 2216,o silt-clay content (t finer than No. 200 Sieve) ~

ASTM:D 1140, and

o Soil plasticity (Atterberg Limits) — ASTM:D 4318.These data, including soil classification based on theUnified Soil Classification System (ASTM:D 2487), aresummarized on Table l, Soils Laboratory-Index Tests.Engineering Property TestingOn the basis of the textural data and indicated soilclassification, bulk samples from four (4) of thesupplemental test pits (I-l, L-l, N-l and S-l) were selected

/1ROQ0785

for soil engineering property evaluation. These four (4)samples generally encompass the range in soilclassifications as encountered by the exploration test pits.Laboratory testing included:

o standard Proctor tests (ASTM:D 698) performed toevaluate soil moisture-density relationship; and

o Laboratory permeability (i.e. hydraulicconductivity) tests on compacted samples, based onthe U.S. Army Corps of Engineers procedure forPermeability Tests With Consolidometer (EM1110-2-1906, Appendix VII).

These data are summarized Table 2, Soil Engineering PropertyTests. The standard Proctor moisture-density curves areattached as Appendix B.

Soil Quality Analysis

The five (5) soil samples, obtained from the supplemental testpits, were submitted under chain-of-custody to LancasterLaboratories, Inc. for environmental quality analysis asfollows:

o Target compound List (TCL) volatile organics (withlibrary search of "tentatively identified compounds");

o Target Compound List (TCL) pesticides/PCBs; ando Target Analyte List (TAL) metals.

In addition, two (2) samples: L-l (7 to 9 ft.) and N-l (4 to6 ft.), were evaluated as follows:

o Target Compound List semi-volatlles (with library searchof "tentatively identified compounds"); and

o "Leachable" Target Analyte List (TAL) metals, based onthe EP Toxicity leachate.

These laboratory data are summarized on Table 3, Target CompoundList (TCL) Organics; Table 4, Target Analyte List (TAL)Inorganic Analyses; and, Table 5, Comparison Total Sample & EPToxicity Leachate Analyses. The Lancaster Laboratories AnalysisReports are attached as Appendix c.The Contract Laboratory Program (CLP) deliverables data packagefor the laboratory analyses were submitted to ECHEM, Inc. forreview and validation. The laboratory data validation report isattached as Appendix D.

AROQ0786

III. EVALUATION s-\

Site Conditions ••-

StratigraphyIn general the test pits, performed at the site indicatethat subsurface conditions, to a depth of approximately ten(10) feet below existing ground surface grade within thearea of exploration, can be characterized into two (2)generalized textural horizons: a layer of generally sandysoil/ sediments overlying silt-clay sediments of the PotomacFormation.

o Texturally, the overlying sandy soils are highlyvariable, ranging from very fine sands to coarsesands and gravels. In addition, the thickness ofthese soils is also highly variable,, ranging fromless than 0.1 feet at TP-L and S to greater than10.5 feet at TP-W. In some areas the thicknessvariation is indicated as being relatively extreme;for example, TP-W is located within 100 feet of TP-S. The observed textural and thickness variation,along with the apparent loose relative density (asindicated by slumping and caving of the test pitexcavations), suggests that these sandy soils have /*t>v.been disturbed and reworked, and may even represent [_,)fill, placed during regrading of the former sand andgravel borrow operation.

o The underlying Potomac silt-clay sediments cangenerally be characterized as massive, variegated(red, white, gray, purple), low plasticity clay andinterlayered high plasticity silt-clay. Thethickness of the silt-clay deposits is undetermined;generally extending to depths greater than theapproximately ten (10) foot excavation depth for thetest pits.

Test Pits, TP-B, J and M, performed in the northeasterlyarea of the site, were terminated in the sandy overburdenstratum, due to excessive caving of the excavation. As aresult, the presence of the Potomac silt-clays, beneath thisarea of the site, is undetermined.GroundwaterGroundwater seepage from the overlying sandy stratum wasobserved in several of the test pits. With the possibleexception of the northeasterly area of the site, where theencountered thickness of the sand stratum is in excess of . , , ;seven (7) feet, this seepage appeared to be water perched on I J

4

AR000787

the top of the underlying silt-clay stratum. Test pits,performed in the northeasterly area of the site, may haveencountered the actual groundwater-table.No seepage from the underlying silt-clay stratum wasobserved in any of the test pit excavations, This isfurther indication of the textural uniformity and massivecharacter of the Potomac silt-clay deposits.

Silt-Clay Soil Borrow

Engineering Properties

Laboratory textural evaluation to classify the Potomac silt-clay deposits, encountered by the test pit excavations,indicates that these soils generally consist of lowplasticity clay (CL) with interlayered high plasticity silt-clay (MH and CH), as defined by the Unified SoilClassification System (ASTM:D 2487). The Atterberg Limitstests (ASTM:D 4318) indicate Liquid Limit values, rangingfrom 36% to 56.5%, and Plasticity Index values, ranging from13.5% to 27.5% (see Table 1). Silt-clay soils with thesecharacteristics are typically considered "suitable" forconstruction of "low permeability" barriers to impedeinfiltration/percolation.Laboratory testing of selected soil samples indicatespermeability (i.e. hydraulic conductivity) values in therange of l x 10'8 centimeters per second (cm/sec). The testdata indicate that these permeability values were achievedover a range of compaction (from 90.5% to 96% standardProctor density) and for the range of soil classifications,including both low plasticity clay and high plasticity silt-clay (see Table 2). For comparison, the Delaware SolidWaste Disposal Regulation defines "impermeable" to mean "apermeability of no greater than l x 10'7 cm/sec." Theproposed cap design for the Tybouts Landfill is based on atwo (2) foot thick layer of "low permeability" soil with apermeability value of 1 x 10'6 cm/sec or less.

The laboratory data indicate compaction in the range of 90%of the maximum dry density, as determined by the standardProctor test (ASTM:D 698), is adequate to achieve theproposed design permeability of l x 10'6 cm/sec. Comparisonof the soil sample moisture data (Table 1) with the StandardProctor moisture-density curves (Appendix B) indicates thatin-situ soil moisture at the time of sampling was generallywet of the optimum moisture content value but in a rangecapable of achieving 90% compaction.In general, the indicated plasticity and hydrauliccharacteristics of the Potomac silt-clay sediments,

flROOQ788

encountered by the test pits performed in Pit 3, indicate /—Nthat these soils are potentially suitable for use in ' . }construction of the proposed low permeability cap for the '••••Tybouts Landfill. Although soil moisture is weatherdependent and, therefore, subject to change, the dataindicate potentially favorable soil moisture for workabilityand compaction to 90% Standard Proctor density.Environmental QualityFive (5) soil samples were submitted to LancasterLaboratories, Inc. for environmental quality analyses, whichare summarized on Tables 3, 4 and 5. In general these dataindicate the following:

o Target Analyte List (TAL) metals concentrations inthe samples do not exceed the uses reportedconcentration ranges for soils in the eastern UnitedStates [Shacklette, H.T. and Boerngen, J.G. (1984),Element Concentration In Soils And other SurficialMaterials Of The Coterminous United states: U.S.Geologic Survey, Prof. Paper 1270.].

o Based on the EP Toxicity leachate analyses,"leachable" metals are indicated as being limited toa trace presence of what can generally be /•«*«characterized as the more common, naturally , .' )occurring, soil and rock forming elements (e.g., s**rcalcium, magnesium and sodium).

o Target Compound List (TCL) pesticides/PCBs were notdetected in the samples submitted for analyses.

o Of the Target compound List (TCL) volatile organics,acetone was detected in four (4) of the five (5)samples submitted for analysis (at 13 to 28 ug/kg)and methylene chloride was detected in one (1)sample (at 7 ug/kg), The relatively ubiquitous andfairly uniform reported presence of acetone, atthese varied locations and sample depths, is bothconspicuous and suspicious because acetone isextremely volatile and water soluble. The reportedpresence of acetone in one (1) of the laboratorymethod blanks (at 9 ug/kg) suggests that theindicated presence of acetone, which is a commonlaboratory solvent, may represent "crosscontamination" associated with the analyticalprocess. While there is no similar reported

AROOQ789

presence of methylene chloride in any of the methodblanks, it also appears possible that this commonlaboratory chemical could have been similarlyintroduced in trace amount into the one (1) sample.

o Target Compound List (TCL) semi-volatile organicsare not reported as having been detected in thesamples submitted for analysis. However, severalnon-listed, "tentatively identified compounds" arereported as having been detected. However, many ofthese compounds have also been reported as beingpresent in the laboratory method blank, suggestingthat their reported presence may represent "crosscontamination" associated with the analyticalprocess.

In general, the environmental quality analyses do notappear, based on current guidelines and regulations, toindicate environmental constraints, which would preclude theuse of the Potomac silt-clay soils in construction of theproposed low permeability cap for the Tybouts Landfill.

Borrow Area

The test pit data indicate an approximately 17 acre area of Pit3 as being underlain by Potomac silt-clay soils, which arepotentially suitable for use in the proposed cap constructionfor the Tybouts Landfill. This area is approximately delimitedon Figure 3, Proposed Silt-Clay Borrow Area. Review of the testpit logs indicates that the silt-clay soils are buried beneath asandy overburden stratum. The indicated thickness of the sandyoverburden ranges from approximately 0.1 feet to in excess of10,5 feet; with an indicated mean average thickness of 3.8 feet.This overburden will have to be removed to allow access to theunderlying silt-clay deposits.The depth of excavation will be a function of the size of thelandfill cap and the volume of soil required for construction.Preliminary estimates indicate that between 160,000 cubic yardsand 240,000 cubic yards of low permeability silt-clay may berequired for cap construction. Assuming a 17 acre borrow areaand removal of an average 3.8 foot thickness of sandyoverburden, the indicated average excavation depth rangesbetween approximately 9.5 feet and 12.5 feet. At 12.5 feetdepth, the bottom of the excavation will approach and may evenextend below the level of nearby Red Lion creek, which flowsalong the northerly side of Pit 3 (see Figure l). Depending onactual excavation depth, contingency for groundwater controlshould be anticipated during design of the borrow operation.

flR00079Q

IV. CONCLUSION & RECOMMENDATIONS

The variegated, Potomac Formation silt-clay, encountered withinthe approximately 17 acre proposed borrow area; delimited onFigure 3, is indicated by the test pit and laboratory data aspotentially suitable for use in construction of the proposed lowpermeability cap for the Tybouts Landfill remediation. Thelaboratory data indicate that these soils, compacted toapproximately 90% of the maximum dry density, as determined bythe standard Proctor test (ASTMiD 698), will achieve thespecified permeability (i.e., hydraulic conductivity) value of1 x 10'6 cm/sec or less.

The exploration data indicate that the practicable borrow areamay be limited to the central area of Pit 3; the thickness ofthe sandy overburden apparently increases in the northeasterlyarea and, possibly, the southeasterly area of the site (seeFigure 3). Because of the potentially limited availability ofthese silt-clay soils, cap design should be configured tooptimize the use of these soils.The manner in which these soils are excavated from the borrowarea will effect workability and constructability of the cap.Based on the above evaluation, the following conceptrecommendations should be considered during design of the borrowoperation to obtain these soils:

\1. Perform a topographic survey of the borrow area, including

comparison of relative elevation to the nearby Red LionCreek.

2. Develop borrow operations specifications that includeprovision for the following:

o Stripping and grubbing of vegetation and otherdeleterious surficial materials from the borrowarea;

o Removal of the irregularly configured sandyoverburden from the borrow area to expose (withminimal disturbance) the underlying silt-clay;

o Excavation of the silt-clay soils in a manner thatallows the contractor to control the size of thesoil clumps and soil moisture; and

o Control of rainwater, surficial runoff, seepage ofperched groundwater from the sandy overburden and,depending on depth of excavation, possiblygroundwater flow into the borrow excavation.

AR00079

The above evaluation and concept recommendations, which have\ been prepared in accordance with our understanding of generally

accepted geologic and engineering principles and practice, arebased on conditions encountered by the exploration test pitsperformed at the project site. It should be noted that although

"*• site and area conditions have been inferred throughinterpolation/extrapolation of these data, subsurface conditionsbetween individual test pits is, in fact, unknown. As a result,these recommendations may require modifications, based onconditions encountered during construction. Should subsurfaceconditions be encountered or observed, which differ from thosedescribed in this report, this office should be notified inorder to review and, if required, modify these recommendations.

,OAROOQ792

•UAU CUT' EVALUATIONTTWUTS LANDFILL

TAKE 1 "it

90ILI tAMXATWr • IKDEX TEJTI

Ttlt Smpll Dlpth Soil Sllt-Cliy Att«rb«ra Llnlt; U) SoilPit Inttrvil Holituri Friction Liquid Pliitlclty dm. ••no. - "i«ti <ii mm na <i> Limit m indtx mi uses (5)

A 0 - 6 . 3 14.3 44.26.5 -8 21.5 90.9

C 0-2 13.5 11.32.3 • 4.3 20.1 97.8 36 13.5 CL4.5- 6.5 21.2 98.46.5 • 8 27.4 95.5 46.5 21 Cl8 • 10 27.3 97.0

D 0 - 4 . 2 17.9 28.0E 1-3 26.9 96.3

L : 7.5 S$ SB8 • 10 21.3 96.7

F 4.5 • 6.5 25.5 87.97 • 9 17.4 87.4 32.5 15

0 1-3 26.5 97.53 • 5 26.0 97.9 56.5 27.55 • 7 22.8 92.87 • 9.5 16.9 85.6

0-1 (6) 5-7 25.6 99.1 53 24.5

H 3 - 5 . 5 26.6 99.95.5 • 7.5 21.0 96.9 42.5 19 CL8 • 10 16.4 96.4

I 5,5 • 7.5 32.1 97.18 • 10 20.6 99.5

1-1 (6) 9-7 30.8 98.1 56 27.5 CH

I 1-3 25.0 99,2 50 23.5 CL/CH4 • 6 18.3 96,07-9 23.6 99.2

L-1 (6) 7-9 20.4 98,1 44 22 CL

N-1 (6) ' 4 - 6 14.2 88.1 42 21 CL

0 2-4 27.7 98,24 • 6 26.7 97.06 • 8 23.0 91.68 • 10 21.2 90.0

P 2-4 26.8 99.J4 • 6 21.4 99.1 44 21.5 CL6 • 8 16.8 97.38 • 11 22.6 91.5

« 8 • 10 29.8 97.0

U.O. 323-HH-08DPL Coniultmtl

AROOQ793 P"t1°"

-UMO OAT* EVAIIMTIONHIOUTI LAWFUL

TAILS 1

SOILI LAMMTMT • IWEX TESTI

Tilt S*H!li Dipth Soil Sllt-Cliy Aturlxrg Llmlti (t) SoilPit Intirwl Nolitun Friction Liquid Ptiitlclty Clin. ••HO. tfnti »> m (2) IM (3) _ |,tn)it tin ind«» n;^ USM «i

I 0-2 23.2 97.72-4 23.3 97.34 • 6 27.0 99.46 • 8 27.5 99.2 55.5 26.5 CH/HH8 • 10 26.7 98.9

M (6) 1-3 25.2 99.7 51 22.5 KH/CH

T 6-8 19.1 97.28 • 10 19.8 94.0

V 5-7 25.5 96.7 47 21 CL7 • 9 21.1 95.29 • 11 20.7 98.0

HOTEl!

1..) Dtpth btlM ulitlng ground lurfKi gridi it tint md locitlon of iMpllng.2.) AITNl 0 22163.) drcmt flmr thin Ho. 200 ilivt •• ASTN: 0 11404.) AITNl 0 43185.) USCI • Unlfltd toll Cliiilflcitlon lyitm •• ASTNi 0 2487

CL > Ion pliitlclty cityCH • high pliitlclty cliyNH • high pliitlclty illt

6.) Suppltmntal tut pit to obtiln bulk impli for englntirlng proptrty ind/or loll quillty iviluitlon.

OM.O. 323-HH-09DPI Coniultmti

AR00079lt

•MAW CUT* EVALUATIONTTNUTS LAWFUL

TAUEZ

SOIL ENGIWailM PHOPEMT TESTS

stindird Proctor (4)Tilt Smplt Soil Hol«tur«-P«fliltv RtliHoq Lab. Oeterailntd PirmtiblUty (51Pit Oipth Ctui. • KIN. Dry Optlmui Smpli std. Proctor IndlcittdHo. . Inttrvil (11 U5C5 (2)(31 p«nflt> Hotiturt Ho. Caimctlon PimmbUltv (61

1-1 5 -7ft. CH 101.6 PCF 23.5X 1-1 (A) 90.6X1-1 (B) 94.5X

L-1 7- 9ft. CL 111.3 PCF 16.5X L-l (A) 96.2X1-1 (B) 96.0X

"•I * • 6 ft. Cl 112.2 PCf 17.9H K-1 (A) 96.3XN-1 (B) 93.2X

.5 X 10*

.5 II 10* OH/IK

.5 K 10* an/lieK 10* en/lie

x 10*X 10*

S-1 1-3 ft. MH/CH 105.5 PFC 21. IX S-1 (A) 92.1X 1.5 x 10* M/IKS-1 (B) 91.5X 1.5 x 10* M/MC

NOTES)1.) Oipth IxloN Mlitlng ground lurfici grid* it tlra ind locitlon of2.) USCS • Unlflid Soil Cluilflcitlon SyitM •• ASTHl 0 2487

CL • ION pliitlclty cliyCH • high ptiitlclty cliyMil • high pliitlclty illt

3.) Sn Tiblt 1 for toll Indtx Ttit diti.4.) ASTNi D 698 •• m ittichtd Proctor Curvu.5.) "Filling ht*d" tut, biitd on U.S. Army Corpi of Englnnn procidun for Pirmiblllty Tut Ulth Curaolldomtir

(EN 1110-2-1906).6.) Iffpoifd.virtlnl itrm • 250 pif.

U.O. 323-HH-OBOPL Comultmti

,_ "MMO CUT* EVALUATIOI' \ TTMMII LAWFUL

TAILS 3

TARGET rafON) LIST (TCl) ORGANIC!.'L SOU SAMPLE AULT5H

Tilt Pit Ho.

(SMpIt Dlpth)(3>

SMpIt No.

Amlyili [ug/kg) (1)(2)(4)(5)Volitl In

Tirgit Compound LIitmthylmt Chlorldt NO 7. NO HD HOAcitOM 24. B 13. B 13. B 29. B HO

Tmtltlvily Idmtlfltd HO HD NO ND HO

Swl-Volitlln

Tirgit Co*pound Lilt NT NT NT HO NO

Tmtltlvily Idmtlfltd NT • NT NT

Funn,2,5-dlMthyl- 260. t,i 700. B.J2-Pmt«M,3,4-dlMthyl- HD 160. B.JHtpttnt,2,5-dlMthyl- 150. B J HOUnknoMi 1,900. B J NDUnknown HD 2,100. B,JHtMnt,2,3-dlMthyl- 190. B J ND

< Unknown illphitlc hydrocir. 190, I J HDUnknown iromtlc 860, B J HD3-Hlxm-2,5-dlont HO 290. B,JUnknown cirbotyllc Mid 230. J HOUnknown phthilitt titir 530. J HDUnknown cirbonyllc Kid ntir 190. J HOUnknown tllcycllc hydrocirbon HD 330. B,J

Ptitlcldii/PCBiTirgit Compound Lilt NO ' ND m HD ND

NOTES! 1.) soil iwpln obtilntd 29 Nirch 1990 by DPI comultmti. Liboritory imlym ptrformd by LmciitirLiboritorln, Inc.

2.) Abbnvlitlomi ug/kg • Mlcrogrm ptr kllogrm; l.t., pirti far billion (ppb)NO • Not dittcttd (it concmtritlon ncttdlng libontory minimum Limit Of Quintlflcitlon)HT • Not Ttlttd

3.) Depth btloH Mlitlng ground turfm grtdt it tint ind locitlon of impllng,4.) IdmitHled iri only thoit orgmlci dtttctid In om (1) or mori of thi imlym pirformd. Qthir TCL orgmlci

irt rtportid n not dttcctid it conctntritloni Mcitdlng thi libontory minimum Limit Of Dumtlflcitlon,5.) Diti Qwllflir codtn g • Not d«tictid tubitintlilly ibovt livil riportid In lib or flild blmki

J • Anilytt priimt. Rtporttd vilui my not b* iccuritt or priclit.

«.0, 0323-HH-OBOPL Coniultmti

flR000796

•HARD CUT" EVALUATIONTYBOUTS LAWFUL

TABLE * """'

TARGET ANALITE LIST (TAL) INORGANIC AMLTSEI•'*,rut Pit Ho. G-1 1-1 L-1 H-t S-1 Rtporttd Elmtnti conctntntlont In Soil

Smplti from Entim Unlttd Ititn(SmpliDipthl(4) 15-7 ft.) 15-7 ft.) [7-9 ft.] (4-6 ft.] (1-3 ft.) [Pirti Pir Nllllon (ppi)] (2)(3)

( Ntm )iMpltHo. IP-02-05 IP-05-05 TP-04-07 TP-03-04 IP-01-01 (Giomtrlc) (Kwgt)

Arulyili Ing/kg) (1)(2)(5)Cymldi (Totil) <0.1 <0.1 <0.1 <0.1 <0.1 HI 'NRHltlll

Alumlmn 3,300. J 3,340. J 2,950. J 2,070. J 3,660. I 33,000. 7,000->tOO,000Antimony ND NO ND HD ND UJ NR NRAntnlc ND NO ND HD ND 4.9 0.1-73BlHu* 30. J 30. J ND ND 70. J 290. 10-1,500Birylllu* 2.0 J 2.0 J HD 1.0 J 1.3 J 0.55 <1-7

CKhlm ND NO ND ND HD ND NRCllclin 1,130. 1,020. 650. 670. 950. 3,400. 1,000-280,000Chromlun 30. J 30. J 11. J 11. J 30. J 33. 1-1,000Cobllt ND ND ND HD ND 5.9 O.3-70Coppir 21. J 31. J 9. J 15. J 17. J 13. <t-700

Iron 36,500. J 63,800. J 5,090. J 16,600. J 39,700. J 14,000. 100->10lLlld 5.3 J 13.3 J 4.4 J 5.0 J 3.4 J 14. <10-300'Hignnlum 360. 330. 190. 390. 400. 2,100. 50-50,W.Mtngmni 6. J 2. J 1. J ND 181. J 260. <2-7,000Ntrcury HD ND ND ND ND 0.081 0.01-3.4

Nlckll ND NO HD ND 5. 11 <5-700PotllllM 690. J 600. J 120. J 190. J 950. J 12,000, 50-37,000Slltnlux ND ND ND ND HD UJ 0.30 <0.1-3.9Sllvir HD ND ND ND HD HR NRSodlw NO NO ND ND ND 2,500. <500-50,000

Thi! Hum ND HD HD ND NO NR NRVintdlin 55. R 53. R 40. R 26. R 49. R,J 43. 47-300Zinc 11. J 40. J 3. J NO 20. J 40. <5-2,900

•OTES: 1.) Soil iwplu outlined 29 Nirch 1990 by DPI Contultinti. Laboratory imlyiu performed by leocuter Libontorld, Inc.2.) Abbnvlitloni! ng/kg > mllllgriM ptr kilogram; I.e., pirti ptr million (ppm)

ND > Hot detected (it concentration exceeding liboritory minimum limit of quantification)NR • Not Reported< • Leu Tnm> • Qrutir Thm

3.) Source! Shickltttt, H.I. ind J.O. Botrngen (1984), Element Concentrations in Sold And Othir Surflclil Hittrlili OfTht cotirmlnoui Unlttd Ititut U.S. Geologic surviy, Prof. Piper 1270.

4.) Depth below txlitlng ground lurfict grtdt it time ind location of sampling.5.) Oiti Quillfltr Codui J » Anilytt present. Reported vilue miy not bt iccuritt or preclie.

R > Unreliable result. Anilytt my or ray not bt present In tht simple. Supporting datineeded to confirm result,

,-•*'>!

H.O. 0323-HH-09flR000797DplCwiMluntl

"WHO CUT* EVALUATIONTTIOUTI LAWFUL

TARE 5

COMPARISON TOTAL SANPLS I EP TOXICITY LEACHATE ANALYSES

Ttlt Pit NO. N-t S-1

[Simplf Dtpth]<4) 14-6 ft.] (1-3 ft.]HO. TTF-TP-03-04 ITF-IP-01-01

Total Sample EP Tox. Leechatt Totil Semplt EP Ton. Lmhitt(mg/kg • dry Ht.l N/ll (mg/kg • dry wt.l [mg/l]

(11(21(51 (11(21(31(51 (11(21(51 (11(2I(31(»

Nltlll

Aluminum 2,070. J <0.1 3,960. J <0.1Antimony <6. <0.05 <6. ' <0.05Areenlc <2. <0.01 <1. «0.01Birlm <20. 0.2 J 70. J 0.2 JgtrylllM 1.0 J <o.oos 1.3 J <o.o«Cadilue <0.6 <0.005 <0.6 <0.005Calclw 670. 1.4 950. 0.9ChroilM 11. J <0.01 30. J <0.01Cobalt <6. <0.05 <6. <O.OJCopper 15. J <0.02 17, J <0,OZIron 16,600. J <0.05 39,700. J <O.OSHid 5.0 J <0.005 3.4 J <O.OOSNigntllM 390. 0.93 400. 0.39Hangmen <1. 0.02 U 191. J <0.01Mercury <0.05 0.0002 U <0.05 <0.0002Nlcktl <5. <0.04 5. <0.04PotiHlu* 190, J <1. 950. J <1.Selenium <0.6 «0,001 <0.6UJ <0.005Silver <1. >0.01 <1. <0.01Sodlui. <60. 3.0 <60. ' 2.0ThllllM <1. <0,0t <1. <0.01Vanedlin 26. R <0,05 49. «,J <0.«Zinc <2. 0.20 J 20. J 0.11 J

NOTES! 1.) Soil iMpIn obtained 29 Nirch 1990 by OPL Consultants, laboratory enalysea performed by Lanciittr' Liboritorln, Inc.

2,) AtabrtvUtlomi mg/kg > mllllgrM/kllogrim; I.e., perti ptr million (ppm)mg/l » mllllgram/lltir,- appro*, parti ptr million (ppm)< • Ltei thin Indicated laboratory minimum limit of quantification

3.) EP Toxicity Ltichiti prepared In accordance with procedure specified In Ftdtril Register, 19 Nay 1990(p. 33127).

4.) Depth btlon exletlng ground turfict gradt it tlmt and location of iwpllng.5.) Dili owllflir Codn: J • limlytt prtitnt. Reported vilut may not bt accurate or praelii.

R • Unreliable result. Anilytt may or ray not bt present In thi iwpli.Supporting data needed to confirm mult.

U • Not Detected.

.

W.O, 0323-HH-08DPL COMUltwtl

flR000798

NOTE;THIS AREA SKETCH WAS APAPTED FBOM THE U.3.G.S. TOPOGRAPHIC MAP,7,5 MINUTE SERIES, FOB THE 9AINT GEOBGES , PEUWAPE QUADPAM6UE

F1QOHE1 _____DUFFIELD ASSOCIATES, INC

AREA SKETCH . _, m num OEOTECHNICAL"WARD CUY" EVALUATIONTYBOUTS UNDFILL

NCTC/flTU COUNTY, 06LAW« „. W,HH08., .

Or«wre DHP Chk'd; GKE8oiH): |" : 2000'

0«lt; 17 JULY I99QW.O.: 3Z3HH-08

••*,

3 APPENDIX A

Test Pit Descriptive Logs(TP-A through W)

,J

flR000802

DPL CONSULTANTS

TEST PITDESCRIPTIVE LOG

PROJECT: Hard Clay Evaluation W.O. NO.: 323.HH.08

CLIENT: Tybouts Trust DATE: 22 March 1990REVIEWED BY! EWR _____________________________________

Test Pit DepthNo. Range fft.) Generalised Soil Description

TP-A o.o - 6.3 Brown, very fine to medium sand andclayey silt; trace gravel, cobbles andred clay blocks; trace ironstonefragments -- looks disturbed, possiblefill?

6.3 - — Red, low plasticity clay; very stiff

Notes: 1. Test pit terminated at approx. 8 ft. depth.2. Hole caving badly - terminated excavation and

backfilled.

TP-B 0.0 - 4.5 Brown, fine sand; some silt; littlegravel (rounded) ; layer of fine whitesand approx. 1.5 to 2.0 ft. depthinterval (wet)

4.5 - — • Green-gray, fine to medium sand andsilt; little gravel (wet)

Notes: 1. Test pit terminated at approx. 7.0 ft. depth.2. Sides caving at approx. 4 ft. depth; pit approx. 10 ft.

diameter. No further excavation possible; backfilled.

TP-C 0.0 - 2 ± Brown, fine sand; little small graveland small cobbles; little silt (wet) -- bottom of stratum sloped

2 ± - — Varicolored, low plasticity clay,trace very fine sand; few mediumironstone fragments

Notes: 1. Test pit terminated at 10.3 ft. depth.2. Slight caving at 9.7 ft.3. Hater level in excavation at 10 ft.± depth after 3

hours; backfilled.

SR000803

o

DPL CONSULTANTS


PROJECT: Hard Clay Evaluation H.O. NO.: 323.HH.08

CLIENT: Tybouts Trust DATE: 22 March 1990

REVIEWED By; EHR _____________________________________

Test Pit DepthNo. Ranae (ft.) Generalized Soil Description

TP-D 0.0 - 8 ± Brown, fine to medium sand; littlecoarse sand (rounded) ; some clayeysilt; few cobbles, clay blocks (wet) -- disturbed, possible fill?

@ 8 ± Varicolored silt-clay

Notes: 1. Test pit terminated at approx. 8 ft. depth.2. Sides caving badly — terminated excavation and

backfilled.

TP-E 0.0 - 0.9 • Brown, fine to medium sand) littlegravel; some silt (wet)

0.9 - 8.0 Varicolored, high plasticity clay-silt; trace very fine sand; trace fineironstone fragments

8.0 - — '. Varicolored, low plasticity clay;little very fine sand; few fineironstone fragments

Notes: 1. Test pit terminated at 10.2 ft. depth.2. Pit open and dry to 10.2 ft. after 3 hrs.; backfilled.

TP-F 0.0 - 4.3 • Brown, fine to medium sand; some silt;little gravel; blocks of red clay (wet- water seepage along top of underly-ing clay stratum) ~ possible fill

4.3 - — • Varicolored, low plasticity clay;little very fine sand, trace ironstonefragments

Notes: 1. Test pit terminated at 10. l ft. depth.2. Caved to 8.0 ft, water level at 7.5 ft. depth after 30

minutes; backfilled.

f 3

DPL CONSULTANTS


PROJECT: Ward Clay Evaluation W.O. NO.: 323.HH.08


REVIEHED BY: EWR__________________ _________________

Test Pit DepthNo. Range (ft.) Generalized s°il Description

TP-G 0.0 - 0.2 Brown and red, fine to coarse sand;gravel and cobbles

0.2 - 74 Varicolored, high plasticity clay-silt; trace very fine sand; few fineironstone fragments; few cobbles;stiff; yellow (Fe oxide?) colorationbelow 5 ft.

7 ± - — Varicolored, low plasticity clay;little very fine sand

Notes: 1. Test pit terminated at 9.9 ft. depth.2. Pit open and dry to 9.9 ft. after 1 hour; backfilled.

TP-H 0.0 - 2.4 Brown, fine to coarse sand and gravel;large cobbles; some silt (wet)

2.4 - — Varicolored, low plasticity clay,traco very fine sand; stiff

Notes: 1. Test pit terminated at ?.•> ft. depth,2. Water seepage at 2.4 ft,: iopth level (top of clay

stratum); approx. 0.05 rt. water in bottom atcompletion.

3. Pit open to 9.6 ft., water level at 9.1 ft. depth after45 minutes; backfilled.

GENERAL NOTES:

1.) Textural gradation classes (e.g., silt, sand, gravel) aredefined on the basis of the Unified Soil classificationSystem (ASTM: D 2487).

2.) Component amounts delimited as follows:trace 1 - 10%little 11 - 20%some 21 - 35%and 35 - 49%

O£ 3

DPL CONSULTANTS

TEST PITi DESCRIPTIVE LOG


CLIENT: Tybouts Trust DATE: 26 March 1990REVIEWED BY: EWR

DepthRange (ft.) Generalized Soil Description

:D

J

0.0 - 4.7 Brown, fine sand; some silt; littlegravel (wet)

4,7 - 7,5 Varicolored, high plasticity clay;trace very fine sand; stiff

7.5 - — Varicolored, low plasticity clay;trace very fine to fine sand

Notes: i. Test pit terminated at 9.7 ft. depth.2. Water seepage at 4,7 ft. depth level (top of clay

stratum); approx. 0.2 ft. water in bottom atcompletion.

3. Caved to 8.3 ft., water level 6.7 ft. depth level afterapprox. 1.5 hours; backfilled.

TP-J 0.0 - — Brown and gray, fine sand and clayeysilt; trace gravel; contains burledtree trunks, branches (moist) — fill

Notes: l. Test pit terminated at •'. ft.: depth.2. Caving badly below 3,0 ::,; cannot keep hole open;

backfilled.3. Wet at 6.5 ft.

TP-K 0.0 - 3.0 Brown, fine sand; some silt; littlegravel; few red clay blocks —possible f i l l

3,0 - —. Brown, fine sand and gravel; some silt(wet)

Notes: l. Test pit terminated at approx. 6.5 ft. depth.2. Caving, cannot keep sides open; backfilled.

•a 1 of 5

DPL CONSULTANTS


PROJECT: Hard Clay Evaluation w.o. NO.: 323.HH.08CLIENT: Tybouts Trust DATE: 26 March 1990

REVIEHED BY! EHR_______________________________

Test Pit DepthNo. Range fft.) Generalized Soil Description

TP-L 0.0 - 0.1 Brown silt; gravel; rootsO.l - — Varicolored, low plasticity clay;

trace very fine sand; stiffNotes: l. Test pit terminated at 9.2 ft. depth.

2. No groundwater seepage apparent at completion.3. Pit open and dry to 9.2 ft. after 1 hour; backfilled.

TP-M 0.0 - 44 Brown, fine sand; some silt; somegravel (moist) — grades downward to

4 _ - — Gray, fine sand; some silt; somegravel; red clay blocks (wet) —possible fill

Notes: l. Test pit terminated at approx. 7.5 ft. depth.2. Wet, caving, cannot keep open; backfilled.

TP-N 0.0 - 1.5± Brown, fine sand; some silt, somegravel (irregular bottom surface)

1.54- — Varicolored, low plasticity clay;little fine sand; friable; hard (dry)

Notes: 1. Test pit terminated at 6.3 ft. depth.2. No groundwater seepage apparent at completion;

backfilled.

80000807'**°

DPL CONSULTANTS


PROJECT: Hard Clay Evaluation H.O. NO.: 323.HH.08


REVIEWED BY: EWR_______________________________________

Test Pit DepthNo. jRqnge (ft.) Generalized Soil Description

TP-0 0.0 - 1.6 Yellow brown, fine sand and gravel,some silt (moist)

1.6 - 6.0 Varicolored, high plasticity clay-silt; trace fine sand; very stiff

6.0 - — Varicolored, low plasticity clay,trace fine sand

Notes: 1. Test pit terminated at 9.6 ft. depth; backfilled.2. Hater seepage at 1.6 ft. depth level (top of clay

stratum) at completion.

TP-P 0.0 - 24 Brown, fine sand; some silt; somegravel — bottom of stratum sloped

2 ± - — varicolored, low plasticity clay;trace very fine sand

Notes: 1. Test pit terminated at 10.l ft. depth; backfilled.2. No groundwater seepage apparent at completion.

TP-Q 0.0 - 6.54 Brown, fine sand and silt; some graveland cobbles; red clay blocks (wet) —fill

@ 6.54 Varicolored silt-clay

Notes: 1. Test pit terminated at approx. 6.5 ft. depth.2. Hole caving badly, approx. 12 ft. diameter; backfilled.

O

DPL CONSULTANTS




REVIEWED BY: EWR________________________________

Test Pit DepthNo. Rqnge (ft.) Generalized Soil Description

TP-R 0.0 - 8.0 Brown, fine sand and clayey silt; somegravel-cobbles; red clay blocks(moist, becomes wet at approx. 7.0ft.) ~ fill

8.0 - — Varicolored, high plasticity clay-silt; trace very fine to fine sand

Notes: 1. Test pit terminated at 10.5 ft. depth.2. Hater seepage at 7.0-8.0 ft. depth interval (top of

clay stratum); approx. 0.7 ft. water in bottom atcompletion.

3. Caved to 5.S ft., water level 3.7 ft. after 1 hour;backfilled.

TP-S 0.0 - o.l Small gravel, rootsVaricolored, high plasticity clay-silt; trace very fine sand; very stiff

Notes: l. Test pit terminated at 9.9 ft. depth.2. Hole dry after 1.5 hours; backfilled.

TP-T 0.0 - 2.0 Light yellow-orange, very fine sand;little silt; little rounded gravel

2.0 - 5.8 Brown, fine sand; some silt; somerounded gravel (wet)

5.8 - — Varicolored, low plasticity clay;trace very fine sand; few fineIronstone fragments

Notes: 1. Test pit terminated at 9.8 ft. depth.2. Hater seepage and sides caving above 5.8 ft. depth

level; approx. 0.6 ft. water in bottom at completion.3. Caved to 3.5 ft., water level at 2.2 ft. after 1.5

hours; backfilled.

5.

DPL CONSULTANTS


PROJECT: Hard Clay Evaluation W.o. NO.: 323.HH.08'IS


REVIEHED BY; EWR__________________________________

Test Pit DepthNo. Range (ft.) Generalized Soil Description

TP-U 0.0 - —• Brown, fine sand and silt; somegravel, blocks of clay (wet) — fill?

Notes: 1. Test pit terminated approx. 7.5 ft. depth.2. Hole caving badly; water flowing in from surface;

backfilled.

TP-V 0.0 - 4.1 Brown, fine sand and silt; somegravel; blocks of clay (moist) —fill?

^~ 4.1 - — Varicolored, low plasticity clay,. j trace very fine sand; very stiff

'N«_X

Notes: l. Test pit terminated at 11.0 ft. depth.2. Water seepage at 4.1 ft. depth (along top of clay

stratum); approx. 0.5 ft. water in bottom atcompletion; backfilled.

TP-H 0.0 - 5.0 Brown, fine sand; some silt; somegravel (moist)

5.0 - — Brown, fine sand; some silt; somelarge gravel (wet)

Notes: 1. Test pit terminated at 10.5 ft. depth.2. Caving badly below approx. 7 ft. depth.* * * * * * * * *

GENERAL NOTES:

1.) Textural gradation classes (e.g., silt, sand, gravel) aredefined on the basis of the Unified Soil ClassificationSystem (ASTM: D 2487).

"'••• 2.) Component amounts delimited as follows:v j trace 1 - 10%^ little 11 - 20%

some 21 - 35%and 35 - 49%

HR0008IO

APPENDIX B

Standard Proctor Test Moisture-Density Curves

\ 109

101

IW

1A 103

101

3 «>• q-]32Ua •«Bg

81

851

//-

3 IZ 1 1

Minimum Dry OiniliyOptimum Moltturt CoMolituri Conlinl ol SDiiqrlpllon ol MilarlPOPPLE*) HIG

/

100.2.

PCF

/

£Cj___

•irt

s~+*.\

(kj«ftl

COMPJ

COMP

V

\

CTlSJ

/ cno

V>

L

gift

\?«

V\j\

Va 18 20 22 24 16 28 ?o 32 34

MOISTURE (%)in.*,w,w,iM irwr *— k tSPPIUlPAPUl ITV

105. S (P.C.F.) TEST SAMPLEnl.nl 21.1 %

impli ii Rio*il VAEICC

vid 2<p.g %LOPED c'YELLOW, BED BBOWU , &EEY, •

14 PLASTICITY SILT« CLAYProolor Till Typi STAUPAgP ! A.8.T.M. :

. .. Proctor Curve 'MOISTURE-DENSITY RELATIONSHIP

ForWARD CLAY EVALUATION

TEST PIT S-1(1-3 FT. DEPTH)TYBOUTS LANDFILL

D (o°>& . Miihod - —

©DUFFIELD ASSOCIATES, INC,CONSULTING (SEC-TECHNICAL ENGINEERS

Drawn; DHP ChK'd; GKE Dili: 1 MAY 1^0Soili: fft 'iHOVVKl WjJ,RftfflfllftCJ8pFill No.; ' PIOI;

120

118

11(0

114

112

I noo!W

£ 106a5o lOfcBQ

104

10?

100

98

•

mmJA

•• MBM*

/

/W_,f

JftL

/

/

'JSSL

PCFs.

//

L25_»

3&

XM>N

S9MFA

COIrtP

\

-rToTT

A£U£b

•

\«

1

)kj-i(e

^)

m

\

DW

,1;

4 to 8 10 17 14 |(a Id 20 22 Z4 2(o _8MOISTURE (%) @ pEpMEAB,UTV

Mixlmum Dry Dinilly II'Z.Z (P.C.F.) TEST SAMPLEOptimum Moliluri CoMolitur* Conlini ol £Duorlpllon ol Mitorl

PLASTICITY CL;

ntint 11.9 *•moll ii Rtoilvtd U.i »il I/AEICOLOEED fEED, 6PEY, YELLOW^ LOWW, LITTLE <5AMD

Proolor Tut Typi STAK1DAPD } A.8.T.M. ;

Proctor CurveMOISTURE-DENSITY RELATIONSHIP


TEST PIT N-1(4-6 FT. DEPTH)

TYBOUTS LANDFILL

0 (W9fl . Mithod ---

P^DUFFIELP ASSOCIATES, llfjL P CONSULTING QEOTECHNICAL ENQINEEW

Driwic DHP Chk'd: GKE DScili: A*i SHOWU WFill No.; P

iti: . I WAV RSO(,0,i 323HH-OB•O n n n n n O 1 O

lie

114

112

110

3 108oj

HzU° 104

§102.

100

1

V7/__

I/io?3"

._*&

5 14 15 K

Minimum Dry OinillyOptimum Moliturt CoMolitun Conlint ol 8Diiorlptlon ol MilirlPLASTICITY CU

c0

L-ltf)pcpT

PPL

\\

5?%"

z2&.

\

COMP

TiO-liS

&IL0I

L-l ^

\\

J ———

V

\

V •M

a 1 IB fl 20 U 22 29 2 2<j

MOISTURE (%) 0 p_RMEA|_|UTy

II 1.3 (P.C.F.) TEST SAMPLEnl.nl I-.5 »

implt ii Riotil VARICO

Ivid 2$, 4 ftLOPED f&BEY. BED, PURPLE^ LOW

W. TBACE VEEY FIWE SAMDProotor Tut Typi ^TAUDABD ! A.SJ.M. :

Proctor CurveMOISTURE-DENSITY RELATIONSHIP


TEST PIT L-1(7-9 FT. DEPTH)TYBOUTS LANDFILL

P <f°>% t Method - ——

ISVoUFFIELD ASSOCIATES, INC.L* V CONSULTING QEOTECHNICAL ENGINEERS

Driwn; PHP ChK'd: G.E DScili: A'i SHOWU YiFfli No,: P

»ti; 1 MAY WO$'R EPB'flliy'f Uigi:

102

101

100

3 <)8oa!>• 9-7auO °)fo

aa

94

1

mmm

I

I

'

,JU:4

/

j!?£i.

JfiE.

y

/

/

3 PCF

,

• •— JB*B

yO

f

'•2&.

\SMrK r_3_\_ m

/7\

\

~"T "~

Vlip)

——— TT~- ••M

8

2 14 I6> 18 20 22 'A :te 18 90 3Z 34 3b

MOISTURE (%) /j\ pEEMEABILrrYMixlmum Dry Oinilly (01. la (P.C.F.) TES"T SAMPLEODtlmum Maliturt Contint 2?.=, %Molilur* Contint ol CDeiorlptlon ol MilirlHIGH PLASTIC)!

impli ii Reoilvid ?0.fil VABICOL

% %DEED CED. &BEY, YELLOW

'Y CLAY. TBACP UfPY PIME 5AUDProotor Tut Typi ^TAMDAPH ; A.S.T.M. :

. ..Proctor CurveMOISTURE-DENSITY RELATIONSHIP


TESTPITI-1(5-7 FT. DEPTH)

TYBOUTS, LANDFILL

PpOWKl)

Method _, -,———

F^DUFFIELD ASSOCIATES, \CjL* V CONSULTING QEOTECHNICAL EHQINEeBs

Drawn; DHP ChK'diSKGScut: M SHOWNFHt No,:

Dili: 1 MAY 1 90Wj)fl Q H <1&FiPIQI;

APPENDIX C

Laboratory Analysis Reports

by

Lancaster Laboratories, Inc.

O 'Aftoooeie

> ANALYSIS REPORT

\.Caucaster.Cabomtones.., „•i, LLI Sample No. SU 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilralngton DB 19808-1296 Discard Date 6/2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unspiked Grab Soil Time Collected 0905Sample P.O. 323-BH-08

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUAOTITATION LAB CODEAluminum 3,130. mg/kg 20. 014301400Antimony < 5. mg/kg 5. 014401400Barium 60. mg/kg 20. 014601400Beryllium 1.0 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 770. mg/kg 10. 015001400Chromium 25. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 14. mg/kg 2. 015301400Iron 32,200. mg/kg 5. 015401400Magnesium 320. mg/kg 10. 015701400Manganese 147. mg/kg 1. 015801400Mercury < 0.04 mg/kg 0.04 015903500Nickel 4. mg/kg 4. 016101400Potassium 770. rag/kg 50. 016201400Silver < 1. mg/kg 1. 016601400Sodium < 50. mg/kg 50. 016701400Vanadium 40. mg/kg 5. 017101400Zinc 16. mg/kg 2. 017201400Cyanide, Total < 0.1 mg/kg 0.1 023704000

> VOA GC/MS Library Search attached 089005500Semivolatlle Library Search attached 089309500Arsenic (furnace method) < 1. mg/kg 1. 114504000Lead (furnace method) 2.7 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000Thallium (furnace method) < 1. mg/kg 1. 117304000TCL Volatiles (Soil) attached 117827000TCL Semi-Volatiles (Soil) attached 120154000TCL Semi-Volatiles (Soil) cont attached 120200000TCL Pesticides attached 122528000Moisture 19.0 J by we. 0.1 135301200pB 5.51 0.01 144101000

Note)The pH was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized vater) after being tumbled for one hour.

3 COPIES TO Duffield Associates, Inc. ATTNt Glenn K. Elliott

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by;Ss.flsv.rstSkt. For Explanation Nelson B. RlSSer fi.pt.OQ 08 I 7Of Symbols And Abbreviations And Manauor GC/MS F\nvw"wOur SUndardTtrnw And Condition Manager, liUMh

1 'k BH irVZlMwfcwi Amncw Council ot

ANALYSIS REPORT

III Sample No. SV 1505027Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vllmington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unspiked Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT Of

ANALYSIS DRY WT. BASIS QUANTITATION LAB CODEAluminum 3,860. mg/kg 20. 014301000Antimony < 6. mg/kg 6. 014401000Barium 70. mg/kg 20. 014601000Beryllium 1.3 mg/kg 0.6 014701000Cadmium < 0.6 mg/kg 0.6 014901000Calcium 950. mg/kg 10. 015001000Chromium 30. mg/kg 1. 015101000Cobalt < 6. mg/kg 6. 015201000Copper 17. mg/kg 2. 015301000Iron 39,700. mg/kg 6. 015401000Magnesium 400. ng/kg 10. 015701000Manganese 181. mg/kg 1. 015801000Mercury < 0.05 mg/kg 0.05 015901000Nickel 5. mg/kg 5. 016101000Potassium 950. mg/kg 60. 016201000Silver < 1. mg/kg 1. 016601000Sodium < 60. mg/kg 60. 016701000Vanadium 49. mg/kg 6. 017101000Zinc 20. fflg/kg 2. 017201000Cyanide, Total < 0.1 mg/kg 0.1 023701000VOA GC/MS Library Search attached 089001000Arsenic (furnace method) < 1. mg/kg 1. 114504500Lead (furnace method) 3.4 mg/kg 0.6 115504500Selenium (furnace method) < 0.6 mg/kg 0.6 116404500Thallium (furnace method) < 1. mg/kg 1. 117304500TCL Volatiles (Soil) attached 117827000TCL Serai-Volatiles (Soil) attached 120127000TCL Semi-Volatiles (Soil) cont attached 120227000TCL Pesticides attached 122527000Moisture *AS RECEIVED* 19.0 X by wt. 0.1 135327000pB 6.80 0.01 144127000

Note:The pB was performed on a hi slurry (50 gns. of sample and 50 ml.of deionized vater) after being tumbled for one hour.

2)

3 COPIES TO Duffield Associates, Inc. ATTNi Glenn K. Blliott1 COPT TO Data Package Group


Reviewed and Approved bytSt»Rtvers« Skit For Explanation Nelson B. Risser01 Symbols And Abbrtvlttlont And timnmaa* £f/uQOurSttnmrdTirmiAmiCondlllont Manager > GC/HS

> ANALYSIS REPORT

Lancaster L mm tonesLLI Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Ullmington DB 19808-1296 Discard Date 6/ 2/90


Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODE1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.12° °1963 330.00 207900 Reviewed and Approved byt

s«R.vars.si<jt For Explanation Nelson B. Rlsser Eflfl Q 0 0 fl I 9ot Symbol. And Abbr.vl«lton« And Manager, GC/MS ^"wuuw'-'Our StindtrtTtrm. And Condition. nBnuB«iir» ui->na

.> ANALYSIS REPORT1

I Lancaster. Caboratvrie?LLI Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unsplked Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride < 5. ug/kg 5. 083100000NAcetone < 10. ug/kg 10. 091400000NCarbon Disulflde < 5. ug/kg 5. 091500000N1,1-Dichloroethene < 5. ug/kg 5. 118000000N1,1-Dlchloroethane < 5. ug/kg 5. 083300000N1,2-Dichloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dichloroethane < 5. ug/kg 5. . 083600000N2-Butanone < 10. ug/kg 10. ' 091600000N1,1,1-Trichloroethane < 5. ug/kg 5. 083700000NCarbon Tetrachloride < 5. ug/kg 5. OB3800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodichloromethane < 5. ug/kg 5. 083900000N1,2-Dichloropropane < 5. ug/kg 5. 084000000N

' cis-l,3-Dichloropropene < 5. ug/kg 5. 084400000NTrichloroethene < 5. ug/kg 5. 118100000NDlbromochloromethane < 5. ug/kg 5. 084600000N1,1,2-Trichloroethane < 5. 'ig/kg 5. 084500000NBenzene < 5. ^/kg 5. 118200COONCrans'l,3-Dichloropcopene < 5. ug/kg 5. 084100000NBromoform < 5. ug/kg 5. 084700000N4-Methyl-2-Pentanone < 10. :i{/kg 10. 091900000N2-Bexanone . < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene < 5. ug/kg 5. 118300000NChlorobenzene < 5. ug/kg . 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N

3 COPIES TO Duffield Associates, Inc. AXTO: Glenn K. Blllott1 COPT TO Data Package Group


Reviewed and Approved byiSttR.v.rs.SW. For Explanation Nelson B. Rlsse/f St n n o o n01 Symbol. And Abbreviation. And Manarar f!fi/M<» H H U U U 0 /Our standard Ttrms And Conditions nanager, uwna nnvuwut,u

.> ANALYSIS REPORT

i LancasterLaboftttoriesLLI Sample No. Stf 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Ullmington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unspiked Grab Soil Time Collected 0905Sample P.O. 323-BB-OB

Rel.RESULT LIMIT OP

TCL Volatiles (Soil) DRY VT, BASIS QUANTITATION LAB CODEChloromethane < 12. ug/kg 12. 082700000NBromomethane < 12. ug/kg 12. 082800000NVinyl Chloride < 12. ug/kg 12. . 082900000NChloroethane < 12. ug/kg 12. 083000000NMethylene Chloride < 6. ug/kg 6. 083100000NAcetone < 12. ug/kg 12. 091400000NCarbon Bisulfide < 6. ug/kg 6. 091500000N1,1-Dichloroethene < 6. ug/kg 6. 118000000N1,1-Dichloroethane < 6. ug/kg 6. 083300000N1,2-Dichloroethene (total) < 6. ug/kg 6. 117900000NChloroform < 6. ug/kg 6. 083500000N1,2-Dlchloroethane < 6. ug/kg 6. OB3600000N2-Butanone < 12. ug/kg 12. 091600000N1,1,1-Trichloroethane < 6. ug/kg 6. 083700000NCarbon Tetrachloride < 6. ug/kg 6. 083800000NVinyl Acetate < 12. ug/kg 12. 091700000NBromodlchloromethane < 6. ug/kg 6. 083900000N1,2-Dichloropropane < 6. ug/kg 6. 084000000Ncls-l,3-Dlchloropropene < 6. ug/kg 6. 084400000NTrlchloroethene < 6. ug/kg 6. 118100000NDibromochloromethane < 6. ug/kg 6. OS4600QOON1,1,2-Trichloroethane < 6. ug/kg 6. 084500000NBenzene < 6. ug/kg 6. 118200000NtranS'l,3-Dichloropropene < 6. ug/kg 6. 084100000NBromoform < 6. ug/kg 6. 084700000N4-Methyl-2-Pentanone < 12. ug/kg 12. 091900000N2-Bexanone < 12. ug/kg 12. 091800000NTetrachloroethene < 6. ug/kg 6. 084800000N1,1,2,2-Tetrachloroethane . < 6. ug/kg 6. 084900000NToluene < 6. ug/kg 6. 11830QOOONChlorobenzene < 6. ug/kg 6. 118400000NEthylbenzene < 6. ug/kg 6. 085200000NStyrene < 6. ug/kg 6. 092000000NXylenes (total) < 6. ug/kg 6. 092100000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blllott1 COPT TO Data Package Group


Reviewed and Approved byi

s.iRtvtr.tSidtForEiipiin.tion Nelson B. Risser B(UROQ082 I01 Symbol. And Abbnvlitkmi And Manager. GC/MS*__, Our Standard Tmms And Condition. n«u««w;, uwna

Mtfflw. AnwuMn Couroi elntxxAlomi. ino

• J"-

ANALYSIS REPORT

II BPA SAMPLE NO.

TENTATIVELY IDENTIFIED COMPOUNDS !! 01

,,ab Name: LANCASTER LABS Contract: I.Lab Code: LANCAS Case No.: 253212 SAS No.: SDGNo.:TYB2Matrix! (soil/water) SOIL Lab Sample ID: C1505027Liample wt/voli 5.0 (g/mL) G Lab Pile ID: C1505027Llevel: (low/med) LOW Date Received: 03/29/90I Moisture: not dec. 19 Date Analyzed: 04/04/90lolumn (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/KG

!I CAS NUMBER ! COMPOUND NAME ! RT ! EST. CONC. ! Q !^ .............. .a.....,..a................. ,..,„.. „.„....„.. „„.

FORM I VGA-TIC 1/87 Rev.I AfflUXM MHMKOfl to,

K1W

Respectfully SubmittedSMRavtr.«S(d« For Explanation Lancaster Labofl

mental Reviewed and656-2301 Nelson B. Rlsser B.A.

> ANALYSIS REPORT

l LancasterLabomtories , ,«, LLI Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90tfilmington DE 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unsplked Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT OF

TCL Semi'Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEphenol < 330. ug/kg 330. 118500000Nbis (2.chloroethyl) ether < 330. ug/kg 330. 066700000N2-chlorophenol < 330. ug/kg 330. 118600000N1,3-dlchlorobenzene < 330. ug/kg 330. 067700000N1,4-dichlorobenzene < 330. ug/kg 330. 118700000Nbenzyl alcohol < 330. ug/kg 330. 092600000N1,2-dichlorobenzene < 330. ug/kg 330. 067600000N2-methylphenol < 330. ug/kg 330. 092700000Nbis (2-chloroisopropyl) ether < 330. ug/kg 330. 066800000N4-methylphenol < 330. ug/kg 330. 092800000NN-nitrosodl-n-propylamine < 330. ug/kg 330. 11B800000Nhexachloroethane < 330. ug/kg 330. 069200000N

^nitrobenzene < 330. ug/kg 330. 069600000Nsi*/ isophorone < 330. ug/kg 330. 069400000N

2-nitrophenol < 330. ug/kg 330. 06S100000N2,4-dimethylphenol < 330. ug/kg 330. 064800000Nbenzole acid < 1,700. ug/kg 1,700. 092900000Nbis (2-chloroethoxy) methane < 330. ug/kg 330. 066600000N2,4-dichlorophenol < 330. ug/kg 330. 064700000N1,2,4-trichlorobenzene < 330. ug/kg 330. 11B900000Nnaphthalene < 330. ug/kg 330. 069500000N4-chloroaniline < 330. >jg/kg 330. 093000000Nhexachlorobutadlene < 330. ;;g/kg 330. 069000000N4-chloro-3-methylphenol < 330. '.rf/kg 330. 119000QOON2-methylnaphthalene < 330. ug/kg 330. 093100000Nhexachlorocyclopentadiene < 330. '/«/kg 330. 069100000N2,4,6-trichlorophenol < 330. ug/kg 330. 065600000N2,4,5-trichlorophenol < 1,700. ug/kg 1,700. 093200000N2-chloronaphthalene < 330. ug/kg 330. 067200000N2-nitroaniline < 1,700. ug/kg 1,700. 093300000Ndimethyl phthalate < 330. ug/kg 330. 068100000Nacenaphthylene < 330. ug/kg 330. , 065800000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliott1 COPY TO Data Package Group

. J Questions? Contact Environmental Respectfully SubmittedS SSS11" Technical Services at (717) 656-2301 Lancaster Laboratories, Inc.

i iKaLMgpsuenwniiMii Reviewed and Approved bysflfll et IMtin9,

SttRevarstSld. For Explanation Timothy S. Oostdyk, B.ftfl fl 0 0 8 2 301 Symbol. And Abbreviation. And Grouo Leader. GC/MS.,„_„„ OurSt.ndifdT.rm.AndCondllloni " "H uianm, uwna

MmMrAmncinCoiinMtl

ANALYSIS REPORTiM'l-A

I Lancaster Laboratories , \LLI Sample No. SV 1505027


Collected 3/29/90 by DSSTybouts Landfill TTP-TP-Ol-Ol Unspiked Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Semi- Volatiles (Soil) cont AS RECEIVED QUANTITATION LAB CODE3-nitroanillne < 1,700. ug/kg 1,700. 093400000Nacenaphthene < 330. ug/kg 330. 119100000N2,4-dinltrophenol < 1,700. ug/kg 1,700. 065000000N4-nitrophenol < 1,700. ug/kg 1,700. 119200000Ndibenzofuran < 330. ug/kg 330. 093500000N2,4-dinitrotoluene < 330. ug/kg 330. 119300000N2,6-dlnltrotoluene < 330. ug/kg 330. 068400000Ndlethyl phthalate < 330. ug/kg 330. 06BOOOOOON4-chlorophenyl phenyl ether < 330. ug/kg 330. 067300000Nfluorene < 330. ug/kg 330. 068800000N4-nitroanlline < 1,700. ug/kg 1,700. 093600000N2-methyl-4,6-dlnitrophenol < 1,700. ug/kg 1,700. 064900000P**,,N-nitrosodiphenylamine < 330. ug/kg 330. 069900000')4-bromophenyl phenyl ether < 330. ug/kg 330. 067000000ft-**hexachlorobenzene < 330. ug/kg 330. 068900000Npentachlorophenol < 1,700. ug/kg 1,700. 119400000Nphenanthrene < 330. ug/kg 330. 070000000Nanthracene < 330. ug/kg 330. 065900000Ndl-n-butyl phthalate < 330. ug/kg 330. 068200000Nfluoranthene < 330. ug/kg 330. 068700000Npyrene < 330. ug/kg 330. 119500000Nbutyl benzyl phthalate < 330. ug/kg 330. 067100000N3,3'-dlchlorobenzidine < 670. ug/kg 670. 067900000Nbenzo (a) anthracene < 330. ug/kg 330. 066100000Nbis (2-ethylhexyl) phthalate < 330. ug/kg 330. 066900000Nchrysene < 330. ug/kg 330. 067400000Ndl-n-octyl phthalate < 330. ug/kg 330. 068500000Nbenzo (b) fluoranthene < 330. ug/kg 330. 066300000Nbenzo (K) fluoranthene < 330. ug/kg 330. 066500000Nbenzo (a) pyrene < 330. ug/kg 330. 066200000Nindeno (1,2,3-cd) pyrene < 330. ug/kg 330. 069300000Ndibenz (a,h) anthracene < 330. ug/kg 330. 067500000Nbenzo (ghl) perylene < 330. ug/kg 330. 066400000N

3 COPIES TO Duffield Associates, Inc. ATTNi Glenn K. Elllott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services ac (717) 656-2301 Lancaster Laboratories, Inc.

' Reviewed and Approved bytSwR.v.rs.Slda For Explanation Timothy S. OOStdyk,GC/MS

M«mn«imncinCwnpi«f

' ANALYSIS REPORT

Lancaster, Laboratorm, „

••«, Duffield Associates, Inc5350 Limestone Road

,

Vilmington DE 19808-1296

Tybouts Landfill TTP-TP-01-01Sample

TCL Seml-Volatiles (Soil)phenolbis (2.chloroethyl) ether2-chlorophenol1,3'dichlorobenzene1,4-dichlorobenzenebenzyl alcohol1,2-dichlorobenzene2-methylphenolbis (2-chlorolsopropyl) ether4-methylphenolN-nitrosodi-n-propylamine

__ hexachloroethane\^ nitrobenzeneJ isophorone

2-nitrophenol2,4-dimethylphenolbenzole acidbis (2-chloroethoxy) methane2,4-dichlorophenol1,2,4- trlchlorobenzenenaphthalene4-chloroanllinehexachlorobutadiene4 • chloco • 3 • me thylphenol2-methylnaphthalenehexachlorocyclopen tadiene2,4,6-trichlorophenol2,4,5- trichlorophenol2.chloronaphthalene2-nitroanilinedimethyl phthalateacenaphthylene

Unsplked Grab Soil

RESULTDRY UT. BASIS< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.

< 2,100.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.< 410.

< 2,100.< 410.

< 2,100.< 410.< 410.

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

LLI Sample No. SV 1505027Date Reported 5/ 2/90Date Submitted 3/29/90Discard Date 6/ 2/90Collected 3/29/90 by DSSTime Collected 0905P.O. 323-HB-08Rel.

LIMIT OFQUANTITATION LAB CODE

410. 118500000N410. 066700000N410. 118600000N410. 067700000N410. 118700000N410. 092600000N410. 067600000N410. 092700000N410. 066800000N410. 092BOOOOON410. 118800000N410. 069200000N410. 069600000N410. 069400000N410. 065100000N410. 064800000N

2,100. 092900000N410. 066600000N410. 064700000N410. 118900000N410. 069500000N410. 093000000N410. 069000000N410. 119000000N410. 093100000N410, 069100000N410. 065600000N

2,100. 093200000N410. 067200000N

2,100. 093300000N410. 068100000N410. 065800000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliott1 COPT TO Data Package Group


Reviewed and Approved by:Sat RavtrstSldt For Explanation Timothy S. Oostdyk01 Symbol! And Abbravlallons And (;* f e»d«pOur Standard Ttriti. And Condition. "Imf «*«™«i

ANALYSIS REPORTAll!

•.ancaster. LaboratoriesIII Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Unspikcd Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Sen!•Volatiles (Soil) cent DRY UT. BASIS QUANTITATION LAB CODE3-nitroanillne < 2,100. ug/kg 2,100. 093400000Nacenaphthene < 410. ug/kg 410. 119100000N2,4-dlnltrophenol < 2,100. ug/kg 2,100. 065000000N4-nitrophenol < 2,100. ug/kg 2,100. 119200000Ndibenzofucan < 410. ug/kg 410. 093500000N2,4-dlnitrotoluene < 410. ug/kg 410. 119300000N2,6-dlnitrotoluene < 410. ug/kg 410. 068400000Ndlethyl phthalate < 410. ug/kg 410. 068000000N4-chlorophenyl phenyl ether < 410. ug/kg 410. 067300000Nfluorene < 410. ug/kg 410. 068800000N4-nitroanlline < 2,100. ug/kg 2,100. 093600000N2-methyl-4,6-dlnitrophenol < 2,100. ug/kg 2,100. 064900000fXN-nltrosodlphenylamine < 410. ug/kg 410. 069900000.. J4-bromophenyl phenyl ether < 410. ug/kg 410. 067000000H™1"hexachlorobenzene < 410. ug/kg 410. 068900000Npentachlorophenol < 2,100. ug/kg 2,100. 119400000Nphenanthrene < 410. ug/kg 410. 070000000Nanthracene < 410. ug/kg 410. 065900000Ndi-n-butyl phthalate < 410. ug/kg 410. 068200000Nfluoranthene < 410. ug/kg 410. 068700000Npyrene < 410. ug/kg 410. 1195000QONbutyl benzyl phthalate < 410. ug/kg 410. 067100000N3,3'-dlchlorobenzidine < 830. ug/kg 830. 067900000Nbenzo (a) anthracene < 410. ug/kg 410. 066100000Nbis (2-ethylhexyl) phthalate < 410. ug/kg 410. 0669000QONchrysene < 410. ug/kg 410. 0674000QONdi-n-octyl phthalate < 410. ug/kg 410. 06B500000Nbenzo (b) fluoranthene < 410. ug/kg 410. 066300000Nbenzo (K) fluoranthene < 410. ug/kg 410. 066500000Nbenzo (a) pyrene < 410. ug/kg 410. 066200000Nindeno (1,2,3-cd) pyrene < 410. ug/kg 410. 069300000Ndibenz (a,h) anthracene < 410. ug/kg 410. 067500000Nbenzo (ghi) perylene < 410. ug/kg 410. 066400000N3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blllott1 COPY TO Data Package Group


Reviewed and Approved byiSM Ravers. Sldt For Explanation Timothy. S. Oostdyk| 9$Q 0826Of Syroboli And Abtofivlilloni And Group Lo&dcf* GC/H»

MmOfTArrwiMn Council cK

> ANALYSIS REPORT

I Lancaster Laboratories .-t, I -

! P0101USLab Name: LANCASTER LABS Contract: __. !Lab Code: LANCAS Case No.: ___. SAS No.: __. SDG No.: ___.Matrix: (soil/water) SOIL Lab Sample ID: 1505027Sample wt/vol: 30.0(g/mL) G Lab File ID: >E5603Level: (low/ned) LOW Date Received: 03/29/90X Moisture: not dec. 19,0 dec. __. Date Extracted: 04/03/90Extraction: (SepP/Cont/Sonc) SONC Date Analyzed: 04/03/90GPC Cleanup: (Y/N) N pfl: 5.51 Dilution Factor: 1.000


CAS NUMBER

1. 6258652.3.

I 4. 4436753V-V 6.7.8.9.10.11.12.13.14.15.16.17.ia.19.20.21.22.23.24.25.

!! COMPOUND NAME

Fur an, 2,5-dlmethyl-2-Pentene, 3,4-dlmethyl-,

t Unknown3-Bexene-2,5-dloneUnknown alicycllc hydrocarbo

RT4.907.218.3211.0134.45

!EST. CONC.

700.160.

2100.290.330.

_

Q

JB,11,IBJB.IB

"I" • isomer ofFORM I SV-TIC 1/87 Rev.

"-"•"wwwn AIMUKWIWI Inxxiwy At«Hiuim—* eavfai t Envinxinwiui

Respectfully Submitted _Lancaster LaboratorjOpRilMclJ Q _, /Reviewed and Approved byi

656-2301 Tlnothy S. Oostdyk, B.A.

V ( ANALYSIS REPORT

Lancaster Laboratories.Ill Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/2/90

Collected 3/29/90 by DSSTybouts Landfill TTF-TP-01-01 Unsplked Grab Soil Time Collected 0905Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. 061200000NGamma BBC • Llndane < 8. ug/kg 8. 121800000NHeptachlor < 8. ug/kg 8. 121900000NAldrln < 8. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NBndosulfan I < 8. ug/kg 8. 062700000NDleldrin < 16. ug/kg 16. 122200000NDDB < 16. ug/kg 16. 061600000NBndrin < 16. ug/kg 16. 122300000NBndosulfan II < 16. ug/kg 16. 062800000N<?XODD , < 16. ug/kg 16. 061700000^^Bndosulfan Sulfate < 16. ug/kg 16. 062900000N1*DOT < 16. ug/kg 16. 122100000NBndrln Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCB-1232 < 80. ug/kg 80. 064100000NPCB-1242 < 80. ug/kg 80. 0642QQOQONPCB-1248 < 80. ug/kg 80. 064300000NPCS-1254 < 160. ug/kg 160. 064400000NPCB-1260 . < 160. ug/kg 160. 064500QQON

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. ElliotC1 COPY TO Data Package Group

'.WWW Am*™ Carol of


Reviewed and Approved by:

s««fl.v.rs.skJ. For Expiration Charles J. Neslu01 Symbol.AndAbbrtvlitlon. And Grouo Leader. PaOur SUnd.rdT.rm. And Condition. " """""•'

.> 4 ANALYSIS REPORT

.ancaster.Laboratories .LLI Sample No. SV 1505027

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/2/90


Rel.RESULT LIMIT OP

TCL Pesticides DRY VT. BASIS QUANTITATION LAB CODEAlpha BBC < 10. ug/kg 10. 060900000NBeta BBC < 10. ug/kg 10. 061000000NDelta BRC < 10. ug/kg 10. 061200000NGamma BBC • Llndane < 10. ug/kg 10. 121800000NHeptachlor < 10. ug/kg 10. 12190000011Aldrin < 10. ug/kg 10. 122000000NBeptachlor Epoxide < 10. ug/kg 10. 061500000NEndosulfan I < 10. ug/kg 10. 062700000NDleldrin < 20. ug/kg 20. 122200000NDDE < 20. ug/kg 20. 061600000NEndrin < 20. ug/kg 20. 122300000NEndosulfan II < 20. ug/kg 20. 062800000NODD < 20. ug/kg 20. 061700000NEndosulfan Sulfate < 20. ug/kg 20, 062900000NDOT < 20. ug/kg 20. 122100000NEndrin Ketone < 20. ug/kg 20. 093800000NHethoxychlor < 100. ug/kg 100. 062100000NAlpha Chlordane < 100. ug/kg 100. 136100000NGamma Chlordane < 100. ug/kg 100. 136200000NToxaphene < 200. ug/kg 200. 094200000NPCB-1016 < 100. ug/kg 100. 063900000NPCS-1221 < 100. ug/kg 100. 064000000NPCB-1232 < 100. ug/kg 100. 064100000NPCB.1W2 < 100. ug/kg 100. 064200000NPCB-1248 < 100. ug/kg 100. 064300000NPCB-1254 < 200. ug/kg 200. 064400000NPCB-1260 . < 200. ug/kg 200. 064500000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPY TO Data Package Group

VVWKW, TWHOfv A0

Mmw: Amman Coral M



Sat R.v.rstSldt For Explanationj Charles J. Neslund,«...._....-.-..*,.,. ..,-.i .-j Group Leader,

1 ANALYSIS REPORT

I Lancaster Laboratories.LLI Sample No. TL 1505030


Collected 3/29/90 by DSSEP Toxlcicy Leachate of Tybouts Landfill Time Collected 0905TTF-TP-Ol-Ol Unspiked Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODE3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully Submitted\l StoSSS?* Technical Services at (717) 656-2301 Lancaster Laboratories, Inc.l,S«i"5M«S!r"El1v""wn'" °44 °1963 230'00 06270° Reviewed and Approved by:

SttRavarstsidtForExpHnaikm Nelson B. RlsserrJfin n 0 o nOt Symbols And Abbravlallona And Hansaer GC/HS "H U U UO J UOur stind.rdT.rm. And Condition. Manager, uwna «wu

> ANALYSIS REPORT

Lancaster Laboratories, . .,,„HI Sample No. TL 1505030


Collected 3/29/90 by DSSEP Toxicity Leachate of Tybouts Landfill Time Collected 0905TTF-TP-01-01 Unsplked Grab Soil Sample P.O. 323-BH-OB

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum < 0.1 mg/l 0.1 024301400Antimony < 0.05 mg/l 0.05 024401400Barium 0.2 mg/l 0.1 024601400Beryllium < 0.005 mg/l 0.005 024701400Cadmium < 0.005 mg/l 0.005 024901400Calcium 0.9 mg/l 0.5 025001400Chromium < 0.01 mg/l 0.01 025101400Cobalt < 0.05 mg/l 0.05 025201400Copper < 0.02 mg/l 0.02 025301400Iron < 0.05 mg/l 0.05 025401400Magnesium 0.39 mg/l 0.05 025701400Manganese < 0.01 mg/l 0.01 025801400Mercury < 0.0002 mg/l 0.0002025902500Nickel < 0.04 mg/l 0.04 026101400Potassium 1. mg/l 1. 026201400Silver < 0.01 mg/l 0.01 026601400Sodium 2.0 mg/l 0.5 026701400Vanadium < 0.05 mg/l 0.05 027101400Zinc 0.11 mg/l 0.02 027201400Arsenic (furnace method) ' <~0.01~ mg/1 ' 0.01 104503000Lead (furnace method) < 0.005 mg/l 0.005 105503000Selenium (furnace method) < 0.005 mg/l 0.005 106403000Thallium (furnace method) < 0.01 mg/l 0.01 107303000

The above analyses were performed on an EP Toxicity leachate of thesubmitted waste prepared according to the procedure specified inFederal Register May 19 1980 p. 33127.A sample is considered EP Toxic if any of the contaminant concentra-tions (mg/l) in the leachate exceed the following maxima (100 times thePrimary Drinking Vater Standards):

Arsenic 5.0, Barium 100.0, Cadmium 1.0, Chromium 5.0, Lead 5.0,Mercury 0.2, Selenium 1.0, Silver 5.0, Endrin 0.02, Llndane 0.4,Methoxychlor 10.0, Toxaphene 0.5, 2,4-D 10.0, 2,4,5-TP 1.0.

Based on the determinations performed, the submitted sample DOBS NOTexhibit the characteristic of EP Toxicity as defined in Section 261.24Federal Register 1980 p. 33122.


Reviewed and Approved byiSM Ravtrst skit For Explanation Nelson B. Rlsser B. A§ R 0 0 8 3 IOt Symbols And Abbrtvlalloni And MmiaovrOur Standard Ttrm. And Condition! Manager,

.> ANALYSIS REPORT

I Lancaster LaboratoriesIII Sample No. SV 1505033

Duffield Associates, Inc. . Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTF-TP-02-05 Grab Soil Sample Time Collected 1035

P.O. 323-BB-08Rel.

RESULT LIMIT OFANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 2,740. mg/kg 20. 014301400Antimony < 5. mg/kg 5. 014401400Barium 30. mg/kg 20. 014601400Beryllium 1.6 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 940. mg/kg 10. 015001400Chromium 25. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 17. mg/kg 2. 015301400Iron 30,300. mg/kg 5. 015401400Magnesium 300. mg/kg 10. 015701400Manganese 5. mg/kg 1. 015801400Mercury < 0.04 mg/kg 0.04 015903500Nickel < 4. mg/kg 4. 016101400Potassium 580. mg/kg 50. 016201400Silver < 1. mg/kg 1. 016601400Sodium < 50. mg/kg 50. 016701400Vanadium 46. mg/kg 5. 017101400Zinc 9. mg/kg 2. 017201400Cyanide, Total <0.1 ug/kg 0.1 023704000VOA GC/MS Library Search Attached 089005500Arsenic (furnace method) < 1. ng/kg 1. 114504000Lead (furnace method) 4.4 ig/kg 0.5 115504000Selenium (furnace method) < 0.5 sg/kg 0.5 116404000Thalllun (furnace method) < 1. ug/kg 1. 117304000TCL Volatiles (Soil) attached 117827000TCL Pesticides attached 122528000Moisture 16.9 5 by we. 0.1 135301200pB 5,42 0.01 144101000

Note:The pfl was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.


Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.120 01963 235.00 134900 Reviewed and Approved byi

Sn RtytratSldt For Explication Nelson H. Rlsser B.A.01 Symbol. And Abbreviation. And Manaaeri GC/MS flRfiflfiQoiOur Standard Ttrmt And Condition. iwnnjjmi «wn» HnUUUgo2'

> ANALYSIS REPORT

I', Lancaster L \iboralorm, .LLI Sample No. SV 1505033

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-02-05 Grab Soil Sample Time Collected 1035

P.O. 323-BB-08Rel.

RESULT LIMIT OPANALYSIS DRY VT. BASIS QUANTITATION LAB CODEAluminum 3,300. mg/kg 20. 014301000Antimony < 6. rag/kg 6. 014401000Barium 30. mg/kg 20. 014601000Beryllium 2.0 mg/kg 0.6 014701000Cadmium < 0.6 mg/kg 0.6 014901000Calcium 1,130. mg/kg 10. 015001000Chromium 30. mg/kg 1. 015101000Cobalt < 6. mg/kg 6. 015201000Copper 21. mg/kg 2. 015301000Iron 36,500. mg/kg 6. 015401000Magnesium 360. mg/kg 10. 015701000Manganese 6. mg/kg 1. 015801000Mercury < 0.05 mg/kg 0.05 015901000Nickel < 5. mg/kg 5. 016101000Potassium 690. mg/kg 60. 016201000Silver < 1. mg/kg 1. 016601000Sodium < 60. mg/kg 60. 016701000Vanadium 55. mg/kg 6. 017101000Zinc 11. ag/kg 2. 017201000Cyanide, Total < 0.1 ug/kg 0.1 023701000VOA GC/MS Library Search attached 089005500Arsenic (furnace method) < 1. •ng/kg 1. 114505500Lead (furnace method) 5.3 ?g/kg 0.6 115505500Selenium (furnace method) < 0.6 sg/kg 0.6 116405500Thallium (furnace method) < 1. ug/kg 1. 117305500TCL Volatiles (Soil) .mached 117827000TCL Pesticides attached 122527000Moisture "AS RECEIVED* 16.9 * by wt. 0.1 135327000pB 6.52 0.01 144127000

Note:The pB was performed on a 1:1 slurry (50 gms. of sample and 50 ml,of deionized water) after being tumbled for one hour.

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPT TO Data Package Group

S__<CcWAiQuestions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:St» flavors. Skit For Explanation Nelson B. Rlsser B.A.0) Symbol. And Abbreviation. And Manager. GC/rtSD 0 n n n ~Our SlandtrdTtrm. And Condition. nanager, "''flTl (J 0 0 8 3 3

> ANALYSIS REPORT

Lancaster Laboratories

LLI Sample No. SV 1505033Duffield Associates, Inc. • Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10, 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. OB3000000NMethylene Chloride < 5. ug/kg 5. 083100000NAcetone 20. ug/kg 10. 091400000NCarbon Disulflde < 5. ug/kg 5. 091500000N1,1-Dichloroethene < 5. ug/kg 5. 118000000N1,1-Dlchloroethane < 5. ug/kg 5. 083300000N1,2-Dlchloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dlchloroethane < 5. ug/kg 5. OB3600000W .,2-Butanone < 10. ug/kg 10. 091600000 1')1,1,1-Trichloroethane < 5. ug/kg 5. 083700000 "Carbon Tetrachlorlde < 5. ug/kg 5. 083800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodichloromethane < 5. ug/kg 5. 083900000N1,2-Dichloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dlchloropropene < 5. ug/kg 5. 084400000NTrichloroethene < 5. ug/kg 5. 118100000NDibromochloromethane < 5. ug/kg 5. OB4600000N1,1,2-Trichloroethane < 5. ug/kg 5. 084500000NBenzene < 5. ug/kg 5. 1182QOOOONtrans-l,3-Dlchloropropene < 5. ug/kg 5. 084100000NBromoform < 5. ug/kg 5. OB4700000N4-Methyl-2-Pentanone < 10. ug/kg 10. 091900000N2-Bexanone . < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. OB4900000NToluene < 5. ug/kg 5. 11830QOOONChlorobenzene < 5. ug/kg 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N

3 COPIES TO Duffield Associates, Inc. ATTN; Glenn K. Elllott1 COP? TO Data Package Group


Reviewed and Approved by:SttRiv.ritSldtForEiiplin.tlon Nelson B. Risser .B.A.01 Symbol. And Abbreviation. And Manager. GC/MS flR LTl) Oft 91,Our Standard Ttrmt And Condition. nanager, uw/nsMlluiJU004

> ANALYSIS REPORT




P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Volatiles (Soil) DRY VT. BASIS QUANTITATION LAB CODEChloromethane < 12. ug/kg 12. 082700000NBromomethane < 12. ug/kg 12. 082800000NVinyl Chloride < 12. ug/kg 12. 082900000NChloroethane < 12. ug/kg 12. 083000000NMethylene Chloride < 6. ug/kg 6. 083100000NAcetone 24. ug/kg 12. 091400000NCarbon Disulflde < 6. ug/kg 6. 091500000N1,1-Dlchloroethene < 6. ug/kg 6. 118000000N1,1-Dlchloroethane < 6. ug/kg 6. 083300000N1,2-Dlchloroethene (total) < 6. ug/kg 6. 117900000NChloroform < 6. ug/kg 6. 083500000N1,2-Dichloroethane < 6. ug/kg 6. 083600000N2-Butanone < 12. ug/kg 12. 091600000N1,1,1-Trichloroethane < 6. ug/kg 6. 083700000NCarbon Tetrachloride < 6. ug/kg 6. 083800000NVinyl Acetate < 12. ug/kg 12. 091700000NBromodlchloromethane < 6. ug/kg 6. 083900000N1,2-Dlchloropropane < 6. ug/kg 6. 084000000Ncis-l,3-Dlchloropropene < 6. ug/kg 6. OB4400000NTrlchloroethene < 6. ug/kg 6. 118100000NDibromochloromethane < 6. ug/kg 6. 084600000N1,1,2-Trichloroethane < 6. ug/kg 6. 084500000NBenzene < 6. ug/kg 6. 118200000Ncrans-l,3'Dlchloropropene < 6. ug/kg 6. 084100000NBromoform < 6. ug/kg 6. OB4700000N4-Methyl-2-Pentanone < 12. ug/kg 12. 091900000N2-Bexanone • < 12. ug/kg 12. 091800000NTetrachloroethene < 6. ug/kg 6. 084800000N1,1,2,2-Tetrachloroethane < 6. ug/kg 6. OB4900000NToluene < 6. ug/kg 6. 118300000NChlorobenzene < 6. ug/kg 6. 118400000NEthylbenzene < 6. ug/kg 6. 085200000NStyrene < 6. ug/kg 6. 092000000NXylenes (total) < 6. ug/kg 6. 092100000N3 COPIES TO Duffield Associates, Inc. ATTNs Glean K. Blllott1 COPY TO Data Package Group


Reviewed and Approved by:SttRtvtrit Skit For EKpliMtlon Nelson B. Risser B.A01 Symbol. And Abbrevlatloni And Manager. GC/MSOur Stand.rdT.rm. And Condition* ' ' nanngar,, uwna.,

: MmlncAmmanCainoliK

.> ANALYSIS REPOP1

I Lancaster Ldbomtones,'«, TBNTATIVELy IDENTIFIED COMPOUNDS I I

! 02 !_ab Name: LANCASTER LABS Contract: !_______!Lab Code: LANCAS Case No.: 253212 SAS No.: SDG No.: HB2•'itrix: (soil/water) SOIL Lab Sample ID: C1505033Lample wt/vol: 5.0 (g/mL) G Lab Pile ID: C1505033L

Level: (low/med) LOV Date Received: 03/29/90K Moisture: not dec. 17 Date Analyzed: 04/04/90)lumn (pack/cap) PACK Dilution Factor: 1.0


! ! I ! ! !'! CAS NUMBER ! COMPOUND NAME ! RT ! EST. CONC. I Q !

'OA-TIC 1/87 Rev.nni»v Atcmiiuton

sil. BUopui I Enwtnmnil

Respectfully SubmittedSM Rtvtr.1 sut For Explanation Lancaster Laboratories., Inc^ n,mWdW)inental , ., Reviewed; and ApproSMJB 3 6:cal Services at (717) 656-2301' Nelson B. Rlsser B.A.

> ANALYSIS REPORT

\incaster LaboratoriesgPT is&isyffifl ^

LLI Sample No. SV 1505033Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. 061200000NGamma BBC • Llndane < 8. ug/kg 8. 121800000NBeptachlor < 8. ug/kg 3. 121900000NAldrin < 8. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NEndosulfan I < 8. ug/kg 8. 062700000NDleldrln < 16. ug/kg 16. 122200000NDDE < 16. ug/kg 16. 061600000NBndrin < 16. ug/kg 16. 122300000NBndosulfan II < 16. ug/kg 16. 062800000NDDD < 16. ug/kg 16. 061700000NBndosulfan Sulfate < 16. ug/kg 16. 062900000NDOT < 16. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093BOOOOONMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCS-1232 < 80. ug/kg 80. 064100000NPCB-1242 < 80. ug/kg 80. 0642000QONPCS-1248 <80. ug/kg 80. 064300000NPCB-1254 < 160. ug/kg 160, 064400000NPCS-1260 . < 160. ug/kg 160. 064500000N


s _/mm' TwiwvAci

Mmm Amman Mral ol'nowiwniutioiiBniiino.



SMRav.ratSldt For Explanation Charles J. Neslu3flSZffl£Z?8Sy£.- '•" G««P "*»«•• i

> ' ANALYSIS REPORT

I Lancaster LaboratoriesLLI Sample No. SV 1505033



P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Pesticides DRY VT. BASIS QUANTITATION LAB CODEAlpha BBC < 10. ug/kg 10. 060900000NBeta BBC < 10. ug/kg 10. 061000000NDelta BBC < 10. ug/kg 10. 061200000NGamma BBC • Lindane < 10. ug/kg 10. 121800000NBeptachlor < 10. ug/kg 10. 121900000NAldrin < 10. ug/kg 10. 122000000NBeptachlor Epoxide < 10. ug/kg 10. 061500000NEndosulfan I < 10. ug/kg 10. 062700000NDleldrin < 19. ug/kg 19. 122200000NDDE < 19. ug/kg 19. 061600000NEndrin < 19. ug/kg 19. 122300000NEndosulfan II < 19. ug/kg 19. 062800000N/->ODD < 19. ug/kg 19. 061700000r: >:•)Endosulfan Sulfate < 19. ug/kg 19. 062900000Ns«d'DOT < 19. ug/kg 19. 122100000NBndrln Ketone < 19. ug/kg 19. 093800000NMethoxychlor < 100. ug/kg 100. 062100000N •Alpha Chlordane < 100. ug/kg 100. 136100000NGamma Chlordane < 100. ug/kg 100. 136200000NToxaphene < 190. ug/kg 190. 094200000NPCS-1016 < 100. ug/kg 100. 063900000NPCB-1221 < 100. ug/kg 100. 064000000NPCS-1232 < 100. ug/kg 100. 064100000NPCB-1242 < 100. ug/kg 100. 064200000NPCB-1248 < 100. ug/kg 100. 064300000NPCB-1254 < 190. ug/kg 190. 064400000NPCB-1260 . < 190. ug/kg 190. 064500000N


'.ooitltimno.

Momotfl Anwrew Cowiwl ot

if'jQuestions? Contact Environmental Respectfully Sub-1 t':sd fTechnical Services at (717) 656*2301 Lancaster Laboratories, Inc.


s« Rntru skit For Explanation Charles J. Neslund, B.S.01 Symbol. AndAbbrevlttlont And ' •;. ; .. Group L«id«r Pt.tlcidjs/PCB'Our StandtrdTtrm. And Condition. . ' •HW.I

,^> ANALYSIS REPORT

incasier Laboratories^ ^ j»r£HS

LLI Sample No. SV 1505034Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilolngton DB 19808-1296 Discard Date 6/2/90


P.O. 323-RB-08Rel.

RESULT LIMIT OFANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 1,840. mg/kg 20. 014301400Antimony < 5. mg/kg 5. 014401400Barium < 20. mg/kg 20. 014601400Beryllium 0.9 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 600. mg/kg 10. 015001400Chromium 10. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 14. mg/kg 2. 015301400Iron 14,700. mg/kg 5. 015401400Magnesium 350. mg/kg 10. 015701400Manganese < 1. mg/kg 1. 015801400Mercury < 0.04 mg/kg 0.04 015903500Nickel < 4. mg/kg 4. 016101400Potassium 170. mg/kg 50. 016201400Sliver < 1. mg/kg 1. 016601400Sodium < 50. mg/kg 50. 016701400Vanadium 23. mg/kg 5. 017101400Zinc < 2. mg/kg 2. 017201400Cyanide, Total < 0.1 mg/kg 0.1 023704000VOA GC/MS Library Search attached 089005500Semivolatlle Library Search attached 089309500Arsenic (furnace method) < 2. mg/kg 2. 114504000Lead (furnace method) 4.4 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000Thallium (furnace method) < 1. mg/kg 1. 117304000TCL Volatiles (Soil) attached 117827000TCL Semi-Volatiles (Soil) attached 120154000TCL Semi-Volatiles (Soil) cont attached 120200000TCL Pesticides attached 122528000Moisture 11.2 % by wt. 0.1 135301200pB 5.32 0.01 144101000

Note:The pH was performed on a 1:1 slurry (50 gas. of sample and 50 ml.of deionized water) after being tumbled for one hour.

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blliott



Stt Rivsts. Sld. For Explanation Nelsun B. Rlsser B.A.01 Symbol. AndAbbnvtatlon.And Manager,. GC/MSOur sundurd Torn™ And Condition.

•'•MAI.VSIS REPORT

I Lancaster Laboratories

LLI Sample No. SV 1505034Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90


P.O. 323-BB-OBRel.

RESULT LIMIT OFANALYSIS DRY VT. BASIS QUANTITATION LAB CODEAluminum 2,070. mg/kg 20. 014301000Antimony < 6. mg/kg 6. 014401000Barium < 20. mg/kg 20. • 014601000Beryllium 1.0 mg/kg 0.6 014701000Cadmium < 0.6 mg/kg 0.6 014901000Calcium 670. mg/kg 10. 015001000Chromium 11. mg/kg 1. 015101000Cobalt < 6. mg/kff 6. 015201000Copper 15. mg/kg 2. 015301000Iron 16,600. mg/kff 6. 015401000Magnesiua 390. ng/kg 10. 015701000Manganese . < 1. mg/kg 1. 015801000-K.Mercury < 0.05 mg/kff 0.05 01590100(1Nickel < 5. mg/kg 5. 01610100CS*'Potassium 190. mg/kff 60. 016201000Silver < 1. mg/kg 1. 016601000Sodium < 60. mg/kg 60. 016701000Vanadium 26. mg/kg 6. 017101000Zinc < 2. mg/kg 2. 017201000Cyanide, Total < 0.1 mg/kg ' 0.1 023701000VOA GC/MS Library Search attached 089001000Arsenic (furnace method) < 2. mg/kg 2. 114504500Lead (furnace method) 5.0 mg/kg 0.6 115504500Selenium (furnace method) < 0.6 mg/kg 0.6 116404500Thallium (furnace method) < 1. mg/kg 1. 117304500TCL Volatiles (Soil) attached 117827000TCL Semi-Volatiles (Soil) attached 120127000TCL Semi-Volatiles (Soil) cont ' attached 120227000TCL Pesticides attached 122527000Moisture *AS RECEIVED* 11.2 X by wt. 0.1 135327000pB 6.56 0.01 144127000

Note:The pB was performed on a 1:1 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.

3 COPIBS TO Duffield Associates, Inc. ATTNt Glenn K. Blllott1 COPY TO Data Package Group


Reviewed and Approved by:Stt R.vsrs. Skit For Explanation . Nelson B. Rlsser B* 4> (1 fi fl fl (i fl01 Symbol. And Abbreviations And Hanaaer GC/MS ftlfUUUOHUOur SUnd.rdT.rrai And Condition. nanager, uwn»

> . "*N'/\i VS!S REPORT


LU Sample No. SV 1505034Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OPANALYSIS AS RECEIVED QUANTITATION LAB CODE1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.120 01963 330.00 207900 Reviewed and Approved by:

Sttfltvtist Sld. For Explanation Nelson B. RtsserOt Symbols And Abbravlallona And Hanafltir.Our Sltnd.rdT.rnn And Condition. n«nog«,

-,4p> ANALYSIS REPORT

ancastcrLaboratoriesIJrgSffiffi ff ^ .frjaarjf-V '-.Jg

LLI Sample No. SV 1505034Duffield Associates, Inc. Date Repotted 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90


P.O. 323-BB-OBRel.

RESULT LIMIT OFTCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. OB3000000NMethylene Chloride < 5. ug/kg 5. 083100000NAcetone 25. ug/kg 10. 091400000NCarbon Disulfide < 5. ug/kg 5. 091500000N1,1-Dlchloroethene < 5. ug/kg 5. 11BOOOOOON1,1-Dlchloroethane < 5. ug/kg 5. 083300000N1,2-Dichloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N '1,2-Dichloroethane < 5. ug/kg 5. 083600000N-'K2-Butanone < 10. ug/kg 10. 0916000001 ;.;)1,1,1-Trichloroethane < 5. ug/kg 5. 083700000N>*'Carbon Tetrachlorlde < 5. ug/kg 5. 083800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodlchloromethane < 5. ug/kg 5. 083900000N1,2-Dlchloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dichloropropene < 5. ug/kg 5. 084400000NTrlchloroethene < 5. ug/kg 5. H8100000NDlbromochloromethane < 5. ug/kg 5. 084600QOON1,1,2-Trichloroethane < 5. ug/kg 5. 084500000NBenzene < 5. ug/kg 5. 118200000Ntrans-l,3-Dichloropropene < 5. ug/kg 5. 084100000NBromoforn < 5. ug/kg 5. OB4700000N<t-Methyl.2'Pentanone < 10. ig/kg 10. 091900000N2-Uexanone . < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5, 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5, 084900000NToluene < 5. ug/kg 5. 118300000NChlorobenzene < 5. ug/kg 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Billott1 COPY TO Data Package Group


Reviewed and Approved byiSMRtvtrttsidtForExpunoiion Nelson B. Rlsser01 Symbol. And AbtoravMIon. And

. —„„ Our 8t.nd.rd TirnwAnd ConditionsMtmwrAmioMnCwnalcl '•-••

• v >"MAI VCIC; Rppppj, f, > \ • - - -

11. Ldtiiasti y • uibotuioi lesLU Sample No. SV 1505034


Collected 3/29/90 by DSS.Tybouts Landfill TTP-TP-03-04 Grab Soil Sample Time Collected 1125

P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Volatiles (Soil) DRY VT. BASIS QUANTITATION LAB CODEChloromethane < 11. ug/kg 11. 082700000NBronomethane < 11. ug/kg 11. 082800000NVinyl Chloride < 11. ug/kg 11. - 082900000NChloroethane < 11. ug/kg 11. 083000000NMethylene Chloride < 6. ug/kg 6. 083100000NAcetone 28. ug/kg 11. 091400000NCarbon Disulfide < 6. ug/kg 6. 091500000N1,1-Dlchloroethene < 6. ug/kg 6. 118000000N1,1-Dichloroethana < 6. ug/kg 6. 083300000N1,2-Dichloroethene (total) < 6. ug/kg 6. 117900000NChloroform < 6. Uff/kg 6. 083500000N1,2-Dlchloroethane < 6. ug/kg 6. 083600000N2-Butanone < 11. ug/kg 11. 091600000N1,1,1-Trichloroethane < 6. ug/kg 6. OB3700000NCarbon Tetrachloride < 6. ug/kg 6. 083800000NVinyl Acetate < 11. ug/kg 11. 091700000NBromodlchloromethane < 6. ug/kg 6. OB3900000N1,2-Dichloropropane < 6. ug/kg 6. 084000000Ncis-l,3-Dichloropropene < 6. ug/kg 6. 084400000NTrlchloroethene ... < ug/kg ^ naiOOOOONDibromochloromethane < 6. ug/kg 6. 084600000N1,1,2-Trlchloroethane < 6. ug/kg 6. 084500000NBenzene < 6. ug/kg 6. 118200000Ntrans-l,3-Dichloropropene < 6. ug/kg 6. OB4100000NBromoform < 6. ug/kff 6. 084700000N4-Hethyl-2-Pentanone < 11. ug/kg 11. 091900000N2-Bexanone. < 11. ug/kg 11. 091800000NTetrachloroethene < 6. ug/kg 6. 084800000N1,1,2,2-Tetrachloroethane < 6. ug/kg 6. 084900000NToluene < 6. ug/kff 6. 11B300000NChlorobenzene < 6. ug/kg 6. 118400000NEthylbenzene < 6. ug/kff 6. 085200000NStyrene < 6. ug/kg 6. 092000000NXylenes (total) < 6. ug/kg 6. 092100000N

3

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blllott1 COPY TO Data Package Group

)sSSKSSS


Reviewed and Approved byisttRtvirH swt For Explanation Nelson B. Rlsser i04 Symbol. And Abbnvlatloni And Miuunmr fiC/HSOur SUtiKHrdTtrmt And Condition. Banagee, WIUS

> VN/M vcic pppopf~v ' '

.incastcr .Laboratories?mmmmTENTATIVELY IDENTIFIED COMPOUNDS !

! 03,ab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: 253212 SAS No.: SDG No.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: C1505034Liample wt/vol: 5.0 (s/fflL) G Lab File ID: C1505034Luevel: (low/med) LOV Date Received: 03/29/90X Moisture: not dec. 11 Date Analyzed: 04/04/90lolumn (pack/cap) PACK Dilution Factor: 1.0


! ! I l l11 CAS NUMBER I COMPOUND NAME I RT I EST. CONC. II |............... | „.„...„....„..„»....„! „„»... U»..»a.a... I ..

,—————— PORMXVOA-TIC 1/87 Rev.Mnmr AsenMMionifmieil. Betoken t GnvironmfrKU

ivui o( luting, Respectfully Submitted.SS E?-!!!!!!!!.'1!!!!. Lancaster Laboratories, Inc.

56-2301 Nelson B. Rissec B-AV1Manager. GC/HS




P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Semi-Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEPhenol < 330. ug/kg 330. 118500000Nbis (2'Chloroethyl) ether < 330. ug/kg 330. 066700000N2-chlorophenol < 330. ug/kg 330. 118600000N1,3-dichlorobenzene < 330. ug/kg 330. 067700000N1,4-dlchlorobenzene < 330. ug/kg 330. 118700000Nbenzyl alcohol < 330. ug/kg 330, 092600000N1,2-dichlorobenzene < 330. ug/kg 330. 067600000N2-methylphenol < 330. ug/kg 330. 092700000Nbis (2-chlorolsopropyl) ether < 330. ug/kg 330. 066BOOOOON4-methylphenol < 330. ug/kg 330. 092800000NN-nltrosodl-n-propylamlne < 330. ug/kg 330. 118800000Nhexachloroethane < 330. ug/kg 330. C69200000Nnitrobenzene < 330. ug/kg 330. 069600000Nisophorone < 330. ug/kg 330. 069400000N2-nltrophenol < 330. ug/kg 330. 065100000N2,4-dlmethylphenol < 330. ug/kg 330. 064800000Nbenzole acid < 1,700. ug/kg 1,700. 092900000Nbis (2-chloroethoxy) methane < 330. ug/kg 330. 066600000N2,4-dichlorophenol < 330. ug/kg 330. 064700000N1,2,4-trichlorobenzene < 330. ug/kg 330. 118900000Nnaphthalene < 330. ug/kg 330. 069500000N4-chloroanillne < 330. ;g/kg 330. 093000000Nhexachlorobutadiene < 330. .g/kg 330. 069000000N4-chloro-3.methylphenol < 330. .g/kg 330. 119000000N2-methylnaphthalene < 330. <;g/kg 330. 093100000Nhexachlorocyclopentadlene < 330. n/kg 330. 069100000N2,4,6-trlchlorophenol < 330. . ^g/kg 330. 065600000N2,4,5-trlchiorophenol < 1,700. ,;g/kg 1,700. 093200000N2-chloronaphthalene < 330. >ig/kg 330. 067200000N2-nltroaniline < 1,700. ug/kg 1,700. 093300000Ndimethyl phthalate < 330. ug/kg 330. 068100000Nacenaphthylene < 330. ug/kg 330. 065800000N



Reviewed and Approved byiSMfi.varatSld. For Explanation Timothy S. Oostdyk,01 Symbols And Abbftvlaltons And Group Leader, GC/IOur SUnd.nl Tarm. And Condition. '

.incaster LaboratoriesLLI Sample No. SV 1505034



P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Semi-Volatiles (Soil) cont AS RECEIVED QUANTITATION LAB CODE3-nitroanlllne < 1,700. ug/kg 1,700. 093400000Nacenaphthene < 330. ug/kg 330. 119100000N2,4-dinitrophenol < 1,700. ug/kg 1,700. 065000000N4-nltrophenol < 1,700. ug/kg 1,700. 119200000Ndlbenzofuran < 330. ug/kg 330. 093500000N2,4-dinltrotoluene < 330. ug/kg 330. 119300000N2,6-dlnitrotoluene < 330. ug/kff 330. 068400000Ndiethyl phthalate < 330. ug/kg 330. 068000000N4-chlorophenyl phenyl ether < 330. ug/kg 330. 067300000Nfluorene < 330. ug/kg 330. 068800000N4-nltroaniline < 1,700. ug/kg 1,700. 093600000N2-methyl-4,6-dinitrophenol < 1,700. ug/kg 1,700. 064900000ttr»vN-nitrosodiphenylamine < 330. ug/kg 330. 06990000C .v' j4-bromophenyl phenyl ether < 330. ug/kg 330. 067000000hexachlorobenzene < 330. ug/kg 330. 068900000Npentachlorophenol < 1,700. ug/kg 1,700. 119400000Nphenanthrene < 330. ug/kg 330. 070000000Nanthracene < 330. ug/kg 330. 065900000Ndi-n-butyl phthalate < 330. ug/kg 330. 068200000Nfluoranthene < 330. ug/kg 330. 068700000Npyrene < 330. ug/kg 330. 119500000Nbutyl benzyl phthalate < 330. ug/kg 330. 067100000N3,3'-dichlorobenzidine < 670. ug/kg 670. 067900000Nbenzo (a) anthracene < 330. ug/kg 330. 066100000Nbis (2-ethylhexyl) phthalate < 330. ug/kg 330. 066900000Nchrysene < 330. ug/kg 330. 067400000Ndl-n-octyl phthalate < 330. ug/kg 330. 068500000Nbenzo (b) fluoranthene < 330. ug/kg 330. 066300000Nbenzo (K) fluoranthene < 330. ug/kg 330. 066500000Nbenzo (a) pyrene < 330. ug/kg 330. 066200000Nindeno (1,2,3-cd) pyrene < 330, ug/kg 330. 069300000Ndibenz (a,h) anthracene , < 330. ug/kg 330. 067500000Nbenzo (ghl) perylene < 330. ug/kg 330. 066400000N


Questions? Contact Bnvironmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved byiStt_Ravars._SK)t For Explanation Timothy S. OostdykjEi

MtmotrAmmanCwnolot ":J

* W1-LYSIS REPORT

ncaster Laboratories ^, LLI Sample No. SV 1505034



P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Semi-Volatlles (Soil) DRY VT. BASIS QUANTITATION LAB CODBphenol < 370. ug/kg 370. 11B500000Nbis (2-chloroethyl) ether < 370. ug/kg 370. 066700000N2-chlorophenol < 370. ug/kg 370. 118600000N1,3-dichlorobenzene < 370. ug/kg 370. OS7700000N1,4-dlchlorobenzene < 370. ug/kg 370. 118700000Nbenzyl alcohol < 370. ug/kg 370. 092600000N1,2-dichlorobenzene < 370. ug/kg 370. 067600000N2-methylphenol < 370. ug/kg 370. 092700000Nbis (2-chloroisopropyl) ether < 370. ug/kg 370. 066800000N4-methylphenol < 370. ug/kg 370. 092BOOOOONN-nltrosodl-n-propylamlne < 370. ug/kg 370. 118800000Nhexachloroethane < 370. ug/kg 370. 069200000Nnitrobenzene < 370. ug/kg 370. 069600000Nisophorone < 370. ug/kg 370. 069400000N2-nltrophenol < 370. ug/kff 370. 065100000N2,4-dlmethylphenol < 370. ug/kg 370. 064800000Nbenzole acid < 1,900. ug/kg 1,900. 092900000Nbis (2-chloroethoxy) methane < 370. ug/kg 370. 066600000N2,4-dichlorophenol < 370. ug/kg 370. 064700000N1,2,4-trichlorobenzene ' < 370. ug/kg 370. 118900000Nnaphthalene < 370. ug/kg 370. 069500000N4-chloroanillne < 370. ug/kg 370. 093000000Nhexachlorobutadlene < 370. ug/kg 370. 069000000N4>chloro-3<methylphenol < 370. ug/kg 370. 1190QOOOON2.methylnaphthalene < 370. ug/kg 370. 093100000Nhexachlorocyclopentadiene < 370. ug/kg 370. 069100000N2,4,6-trlchlorophenol < 370. ug/kg 370. 065600000N2,4,5-trichlorophenol < 1,900. ug/kg 1,900. 093200000N2-chloronaphthalene < 370. ug/kg 370. 067200000N2-nitroaniline < 1,900. ug/kg 1,900. 093300000Ndimethyl phthalate < 370. ug/kg 370. 068100000Nacenaphthylene < 370. ug/kg 370. 065800000N



Reviewed and Approved byirr '

SttR.v.r.1 sid.ForExplication Timothy S. Oostdykh B.A.01 Symbols, MdAbbtivtolonii And , ." ; .. Group Leadigr, GcAfi U 008^7Our Standard Tttmi And Condition. . , , w v u " '

ncaster Labaratories• .'. -..'.I;'.. .'•TTC'*!.-' .''l r f m ^ ffjfjff Sfimffjff'.

\Duffield Associates, Inc.5350 Limestone RoadVilmington DB 19808-1296

Tybouts Landfill TTP-TP-03-04 Git

TCL Semi- Volatiles (Soil) cont3-nltroanlllneacenaphthene2,4-dlnitrophenol4-nitrophenoldl benzo fur an2,4-dlnitrotoluene2, 6-dinltro toluenedlethyl phthalate4-chlorophenyl phenyl etherfluorene4-nitroanlline2-methyl-4,6-dlnltrophenolN-nitrosodlphenylamine4-bromophenyl phenyl etherhexachlorobenzenepentachlorophenolphenanthreneanthracenedi-n-butyl phthalatefluoranthenepyrenebutyl benzyl phthalate3,3'-dichloroben.idlnebenzo (a) anthracenebis (2-ethylhexyl) phthalate

1 chrysenedi-n-octyl phthalatebenzo (b) fluoranthenebenzo (K) fluoranthenebenzo (a) pyreneindeno (1,2,3-cd) pyrenedlbenz (a,h) anthracene

i benzo (ghi) perylenei 3 COPIES TO Duffield Associates,

1 COPT TO Data Package Group

SlflUS ijn»J!'r!W.«iP

ib Soil Sample

RESULTDRY VT. B/

< 1,900.< 370.

< 1,900.< 1,900.< 370.< 370.< 370.< 370.< 370.< 370.

< 1,900.< 1,900.

< 370.< 370.< 370.

< 1,900.< 370.< 370.< 370.< 370.< 370.< 370.< 750.< 370.< 370.< 370.< 370.< 370.< 370.< 370.< 370.< 370.< 370.

Inc. ATTNi

1 JEW.... l-iR<

ISISug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kffug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguff/kg

Glenn K.

raw V'«Tnwt«fl«»i»r '!.' irmm «•«*' u.nn..-wt *

LLI Sample No. SV 1505034Date Reported 5/ 2/90Date Submitted 3/29/90Discard Date 6/ 2/90Collected 3/29/90 by DSSTime Collected 1125P.O. 323-BB-08Rel.

LIMIT OFQUANTITATION LAB CODE

1,900. 093400000N370. 119100000N

1,900. 065000000N1,900. 119200000N

370. 093SOOOOON370. 119300000N370. 068400000N370. 068000000N370. 067300000N370. 068BOOOOON

1,900. 093600000N1,900. 064900000N-TK

370. 069900000! '',•,;)370. 0670000001M'370. 06B900000N

1,900. 119400000N370. 070000000N370. 065900000N370. 068200000N370. 068700000N370. 119500000N370. 067100000N750. 067900000N370. 066100QOON370. 066900000N370. 067400000N370. 068500QOON370. 066300000N370. 066500000N370. 066200000N370. 069300000N370. 067500000N370. 066400000N

Elliot t

Question.? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.' ' Reviewed and Approved byi

St. Rtvtrtt Skit For Expitnttion Timothy S. Oosti01 Symbol! And Abfcnvlilloin And Grau "OurStanftirtlkmiAMCtndltlom.. •

ANALYSIS REPORT

ncaster LdMiitonesspffi ^ mi mmm tvmm

I P0304Lab Name: LANCASTER LABS Conttact:Lab Code: LANCAS Case No.: __. SAS No.: __. SDG No.: __.Matrix: (soil/water) SOIL Lab Sample ID: 1505034Sample wt/vol: 30.0(g/mL) G Lab Pile ID: >B5606Level: (low/med) LOV Date Received: 03/29/90X Moisture! not dec. 11.0 dec. __. Date Extracted: 04/03/90Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 04/03/90GPC Cleanup: (Y/N) N pB: 5.82 Dilution Factor: 1.000


!! CAS NUMBER

1. 6258652. 22163003.4. 3074713

"V-•>•-1?.

B.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.

CONFOUND NAME

Furan, 2,5-dimethyl-Beptane, 2,5-dimethyl-UnknownBexane, 2, 3 -dimethyl •Unknown aliphatic hydrocarboUnknown aromaticUnknown carboxylic acidUnknown phthalate esterUnknown carboxylic acid este

RT

4.888.208.308.768.9510.9915.5624.0328.06

EST. CONC.

260.150.1900.190.190.860.230.530.190.

0

JBJJBJBJBJBJjJ

FORK I SV-TIC 1/87 Rev.

Respectfully SubmittedLancaster Laboratorie

• Reviewed and Approv656-2301 Timothy S. Oostdyk, B.A.

Grouo Leader, GC/MS

"NAi YSIS REPORT"~"

Mil/ones'

LLI Sample No. SV 1505034Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilnington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. - 061200000NGamma BBC • Lindane < B. ug/kff 8. 121800000NBeptachlor < 8. ug/kg 8. 121900000NAldrin < 8. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NEndosulfan I < 8. ug/kg 8. 062700000NDleldrin < 16. ug/kff 16. 122200000NDDE < 16. ug/kg 16. 061600000NEndrin < 16. ug/kff 16. 122300000NBndosulfan II < 16. ug/kg 16. 062800000K*,ODD < 16. ug/kg 16. 061700000 '"')Endosulfan Sulfate < 16. ug/kg 16. 062900000DOT < 16. ug/kff 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane ' < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCB-1232 < 80. ug/kg 80. 064100000NPCB-1242 < 80. ug/kg 80. 064200QOONPCS-1248 < 80. ug/kg 80. 064300000NPCB<1254 < 160. ug/kg 160. 064400000NPCB-1260 < 160. ug/kg 160. 064500000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliot!1 COPY TO Data Package Group


Reviewed and Approved byiS«t Ravarst Slda For Enplanallon Charles J. Neslund,01 Symbol. And Abbnsvlitlon. And Grnun LeaderOur SUndtrdTtrm. And Condition. Group Maaer,,

> -'.MALYSIS REPORT


LLI Sample No. SV 1505034Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vlloington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides DRY VT. BASIS QUANTITATION LAB CODEAlpha BBC < 9. ug/kg 9. 060900000NBeta BBC < 9. ug/kg 9. 061000000NDelta BBC < 9. ug/kg 9. 061200000NGamma BBC • Llndane < 9. ug/kg 9. 121800000NHeptachlor < 9. ug/kg 9. 121900000NAldrin < 9. ug/kg 9. 122000000NBeptachlor Epoxlde < 9. ug/kg 9. 061500000NEndosulfan I < 9. ug/kff 9. 062700000NDleldrin < IB. ug/kg 18. 122200000NDDE < 18. ug/kff 18. 061600000NBndrln < IB. ug/kff 18. 122300000NEndosulfan II < 18. ug/kg 18. 062800000NODD < 18. ug/kg 18. 061700000NEndosulfan Sulfate < IS. ug/kg 18. 062900000NDOT < IB. ug/kff 18. 122100000NBndrln Ketone < 18. ug/kg 18. 093BOOOOONMethoxychlor < 90. ug/kg 90. 062100000NAlpha Chlordane < 90. ug/kg 90. 136100000NGamma Chlordane < 90. ug/kg 90. 136200000NToxaphene < 180. ug/kg 180. 094200000NPCB-1016 < 90. ug/kg 90. 063900000NPCB-1221 < 90. ug/kg 90. 064000000NPCB-1232 < 90. ug/kg 90. 064100000NPCB-1242 < 90. ug/kg 90. 064200000NPCB-1248 < 90. ug/kg 90. 064300000NPCB-1254 < 180. ug/kg 180. 064400000NPCB-1260 < 180. ug/kg 180. 064500000N


—Ifewn*

Mmtttn Anwcwi Cwnal ol


Reviewed and Approved by:Sit Rtvtnt SId. For Explanation Charles J. Neslund, nBmSn n n n r-,0f Symbol. And AttwMkmi And Jv«im r_.«i«r »«H ftKUytirQ & 51 our Standtrtf Tim. And Condition.. Group Leader, PestinW«/Wa<i J

ANALYSIS REPORT

Lancaster Laboratories . .LLI Sample No. TL 1505035


Collected 3/29/90 by DSSBP Toxicity Leachate of Tybouts Landfill Time Collected 1125TTF-TP-03-04 Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUANTITATION LAB CODE3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliott1 COPY TO Data Package Group

O,,,- - Technical services at (717) 656-2301 Lancaster Laboratories, Inc.

044 01963 230.00 062700 Reviewed and Approved bytSat R.vtrst Skit For Explanation Nelson B. Rlsseh I>A.,_ „01 Symbol. And Abbr.vl.tlon. And Manner GO/MS fl R 0 0 0 fi R 9our standsrdTarma And condition. nanager, uwns TIVUYQJ^

> ANALYSIS REPORT

I Lancaster. Laboratories.,.,.....IZSNflW/HoHiindPikn, L.UII;.'

LLI Sample No. TL 1505035Duffield Associates, Inc. Date Reported 5/ 7/905350 Limestone Road Date Submitted 3/29/90Vlloington DB 19808-1296 Discard Date 6/7/90

Collected 3/29/90 by DSSEP Toxicity Leachate of Tybouts Landfill Time Collected 1125TTF-TP-03-04 Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUANTISATION LAB CODBAluminum < 0.1 mg/l 0.1 024301400Antimony < 0.05 mg/l 0.05 024401400Barium 0.2 mg/l 0.1 024601400Beryllium < O.OOS mg/l 0.005 024701400Cadoium < 0.005 mg/l 0.005 024901400Calcium 1.4 mg/l 0.5 025001400Chromium < 0.01 mg/l 0.01 025101400Cobalt < 0.05 mg/l 0.05 025201400Copper < 0.02 mg/l 0.02 025301400Iron < 0.05 mg/l 0.05 025401400Magnesium 0.93 mg/l 0.05 025701400Manganese ' . 0.02 mg/l 0.01 025801400

•" .Mercury 0.0002 mg/l 0.0002025902500'Nickel < 0.04 mg/l 0.04 026101400Potassium < 1. mg/l 1. 026201400Silver < 0.01 mg/l 0.01 026601400Sodium 3.0 mg/l 0.5 026701400Vanadium < 0.05 mg/l 0.05 027101400Zinc 0.20 mg/l 0.02 027201400Arsenic (furnace method) < 0.01 mg/l 0.01 104503000Lead (fucnace method) < 0.005 rag/1 0.005 105503000Selenium (furnace method) < 0.005 mg/l 0.005 106403000Thallium (furnace method) < 0.01 mg/l 0.01 107303000


Arsenic 5.0, Barium 100.0, Cadmium 1.0, Chromium 5.0, Lead 5.0,Mercury 0.2, Selenium 1.0, Sliver 5.0, Endrin 0.02, Lindane 0.4,Methoxychlor 10.0, Toxaphene 0.5, 2,4-0 10.0, 2,4,5-TP 1.0.

Based on the determinations performed, the submitted sample DOES NOTexhibit the characteristic of BP Toxicity as defined in Section 261.24Federal Register 1980 p. 33122.

TflflO1* A


Reviewed and Approved by:SMflmiritSWiForExpltnitlon Nelson fl. RlsserOf Symbols And Abbreviation. And Minmrnr PP/IWOur Standard T.rmi And Condition! Manager, GC/MS

MmwrAmmanCow»l<x "S

ncaster LaboratoriesTsliMB

III Sample No. SV 1505037Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 2,620. mg/kg 20. 014301400Antimony < 5. rag/kg 5. 014401400Barium 20. mg/kg 20. 014601400Beryllium 1.6 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 800. mg/kg 10. 015001400Chromium 24. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 24. mg/kg 2. 015301400Iron 50,100. mg/kg 5. 015401400Magnesium 260. mg/kg 10. 015701400Manganese 2. mg/kg 1. 015801400/«7>,Mercury < 0.04 mg/kg 0.04 0159035001Nickel < 4. mg/kg 4. 016101400Potassium 470. mg/kg 50. 016201400Silver < 1. mg/kg 1. 016601400Sodium < 50. Jig/kg 50. 016701400Vanadium 42. ?g/kg 5. 017101400Zinc 31. ng/kg .2. 017201400Cyanide, Total < 0.1 ug/kg 0.1 023704000VOA GC/MS Library Search attached 089005500Arsenic (furnace method) < 5. ig/kg 5. 114504000Lead (furnace method) 10.5 Tin/kg 0.5 115504000Selenium (furnace method) < 0.5 sg/kg 0.5 116404000Thallium (furnace method) < 1. ig/kg 1. 117304000TCL Volatiles (Soil) uuched 117827000TCL Pesticides attached 122528000Moisture 21.5 t by ut. 0.1 135301200pB 5.28 0.01 144101000

Note:The pB was performed on a 1:1 slurry (50 gms. of sample and 50 ml,,of deionized water) after being tumbled for one hour,


Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc."0 01963 235.00 134900 Reviewed and Approved byi

..Our8tatid«rdTtrm»AndiC»ndaiioi«jt "

j__±"-Bgj£lt BtA> A R 0 0 0 8 5 1»_ _ BManager, GC/MS

> i.MAI.VCIS PFPOPT

'.metier LaboratoriesLLI Sample No. SV 1505037



P.O. 323-BB-OBRel.

RESULT LIMIT OFANALYSIS DRY VT. BASIS QUANTITATION LAB CODEAluminum 3,340. mg/kg 30. 014301000Antimony < 6. mg/kg 6. 014401000Barium 30. mg/kg 30. 014601000Beryllium 2.0 mg/kg 0.6 014701000Cadmium < 0.6 mg/kg 0.6 014901000Calcium 1,020. mg/kg 10. 015001000Chromium 31. tig/kg 1. 015101000Cobalt < 6. mg/kg 6. 015201000Copper > 31. rag/kg 3. 015301000Iron 63,800. mg/kg 6. 015401000Magnesium 330. mg/kg 10. 015701000Manganese 2. mg/kg 1. 015801000Mercury < 0.05 mg/kg 0.05 015901000Nickel < 5. mg/kg 5. 016101000Potassium 600. mg/kg 60. 016201000Silver < 1. mg/kg 1. 016602000Sodium < 60. ag/kg 60. 016701000Vanadium 53. ag/kg 6. 017101000Zinc 40. ag/kg 3. 017201000Cyanide, Total < 0.1 ag/kg 0.1 023701000VOA GC/MS Library Search attached 089005500Arsenic (furnace method) < 6. ag/kg 6. 114505500Lead (furnace method) 13.3 ng/kg 0.6 115505500Selenium (furnace method) < 0.6 ig/kg 0.6 116405500Thallium (furnace method) < 1. ag/kg 1. 117305500TCL Volatiles (Soil) mached 117827000TCL Pesticides attached 122527000Moisture *AS RECEIVED* 21.5 C by wt. 0.1 135327000pB 6.72 0.01 144127000


3 COPIES TO Duffield Associates, Inc. ATTN; Glenn K. Elliott1 COPY TO Data Package Group


•• Reviewed and Approved byj

. AR00085Ogr Standard Ttrmi Ana CondrtkMvi ..

> • ANALYSIS REPORT

il Lancaster LaboratoriesLLI Sample No. SV 1505037



P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. OB2800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride 6. ug/kg 5. 083100000NAcetone 10. ug/kg 10. 091400000NCarbon Disulfide < 5. ug/kg 5. 091500000N1,1-Dichloroethene < 5. ug/kg 5. 118000000N1,1-Dlchloroethane < 5. ug/kg 5. 083300000N1,2-Dichloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kff 5. 083500000N1,2-Dlchloroethane < 5. ug/kg 5. 083600000N.-V2-Butanone < 10. ug/kg 10. 0916000001 .:! )1,1,1-Trichloroethane < 5. uff/kg 5. 083700000 *Carbon Tetrachloride < 5. ug/k* 5. 083800000NVinyl Acetate < 10. us/kg 10. 091700000NBromodichloromethane < 5. ug/kg 5. 083900000N1,2'Dichloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dichloropropene < 5. ug/kff 5. 084400000NTrichloroethene ' ' < 5. ug/kg 5. 118100000NDibcomochloromethane < 5. ug/kg 5. 084600000N1,1,2-Trlchloroethane < 5. ug/kg 5. 084500QOONBenzene < 5. ug/kg 5. 118200000Ntrans-l,3-Dlchloropropene < 5. ug/kg 5. 084100000NBromoform < 5. ug/kg 5. 084700000N4-Methyl-2-Pentanone < 10. ug/kg 10. 091900000N2-Bexanone . < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene < 5. ug/kg 5. 118300000NChlorobenzene < 5. ug/kg 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N



Reviewed and Approved byiSat R.y«rs.SW. For Explanation Nelson B. Rlsser B.A, _ n ^ ......Of Symbol. And Abbr.vl.tton. And Manager. GC/MS Q R I) J U O h nOur Standard T.rm» And Condition. noimaio*, »v» u- H 11 v u v u w u

MmiMrAmMnCoumiol

.> ANALYSIS REPORT

I Lancaster LaboratoriesLLI Sample No. SV 1505037


Collected 3/29/90 by DSSTybouts Landfill TTF-TP-OS-OS Grab Soil Sample Time Collected 1320

P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Volatiles (Soil) DRY VT. BASIS QUANTITATION LAB CODEChloromethane . < 13. ug/kg 13. 082700000NBroraomethane < 13. ug/kg 13. 082800000NVinyl Chloride < 13. ug/kg 13. 082900000NChloroethane < 13. ug/kg 13. 083000000NMethylene Chloride 7. ug/kg 6. 083100000NAcetone 13. ug/kg 13. 091400000NCarbon Disulfide < 6. ug/kg 6. 091500000N1,1-Dichloroethene < 6. ug/kg 6. 118000000N1,1-Dlchloroethane < 6. ug/kg 6. 083300000N1,2-Dlchloroethene (total) < 6. ug/kg 6. 117900000NChloroform < 6. ug/kg 6. 083500000N1,2-Dlchloroethane < 6. ug/kg 6. 083600000N2-Butanone < 13. ug/kg 13. 091600000N1,1,1-Trichloroethane < 6. ug/kg 6. 083700000NCarbon Tetrachlorlde < 6. ug/kg 6. 083800000NVinyl Acetate < 13. ug/kg 13. 091700000NBromodlchloromethane < 6. ug/kg 6. 083900000N1,2-Dlchloropropane < 6. ug/kg 6. 084000000Ncis-l,3-Dlchloropropene < 6. ug/kg 6. 084400000NTrichloroethene " < 6. ug/kg 6. 118100000NDibromochloromethane < 6. ug/kg 6. 0846000QON1,1,2-Trichloroethane < 6. ug/kg 6. 084500000NBenzene < 6. ug/kg 6. 118200000Ntrans.l,3-Dlchloropropene < 6. ug/kg 6. 084100000NBromoform < 6. ug/kg 6. 084700000N4-Methyl.2-Pentanone < 13. us/kg 13. 091900000N2-Bexanone < 13. ug/kg 13. 091800000NTetrachloroethene < 6. ug/kg 6. 084800000N1,1,2,2-Tetrachloroethane < 6. ug/kg 6. 084900000NToluene < 6. ug/kg 6. 118300000NChlorobenzene < 6. ug/kg 6. 118400000NEthylbenzene < 6. ug/kg 6. OB5200000NStyrene < 6. ug/kg 6. 092000000NXylenes (total) < 6. ug/kg 6. . 092100000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blllott1 COPT TO Data Package Group


Reviewed and Approved byiSa. R.vars. SWt For Explanation Nelson B. RlsserOf Symbol. And Abbr.vl.tton. And Manaaer. GC/MS___,_ Our SI«nd«rdT.rm. And Condition. nwmgur, uwna

, Wmbtr Anwiwi Carol of

> y v ANALYSIS REPORT

I Lancaster Laboratories.\ TENTATIVELY IDENTIFIED COMPOUNDS !

! 05ab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: 253212 SAS No.: SDG No.: TYB2"atrix: (soil/water) SOIL Lab Sample ID: C1505037LRample wt/vol: 5.0. (g/mL) G Lab File ID: C1505037LRLevel: (low/med) LOV Date Received: 03/29/90t Moisture: not dec. 22 Date Analyzed: 04/05/90olumn (pack/cap) PACK Dilution Factor: 1.0


t ! ! ! ! I!! CAS NUMBER ! COMPOUND NAME ! RT ! E.T. CONC. ! Q !!! a............... I „..„«„...„..».....»»_»!»»»»!..» ».»»...!»»_!

KMIOry ASHMllllOTm«l. Baogai I EfMnmtnM

'

FORM I VOA-TIC 1/87 Rev.

Respectfully SubmittedsttRmrstsid.ForExpisnation Lancaster Laboratories, Inc.

u ™ wia W®SfflP8""1 Reviewed 'and Appijcft3 (W) ft Cf u A.MMt. fgr f nSSfVff 656-2301 Nelson I. Rlsser B.A. "V° °

'•" -« rfl . Monn'mi- HP/MS

> ANALYSIS REPORT

''MasterL''1™ '®!!^ :-./ •r

LLI Sample No. SV 1505037Duf£ield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Wllmington DB 19808-1296 Discard Date 6/2/90

Collected 3/29/90 by DSSTybouts Landfill HP-TP-OS-OS Grab Soil Sample Time Collected 1320

P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. 061200000NGamma BBC • Lindane < 8. ug/kg 8. 121800000NReptachlor < 8. ug/kg 8. 121900000NAldrin < B. ug/kg 8. 122000000NBeptachlor Epoxlde < 8. ug/kg 8. 061500000NEndosulfan I < 8. ug/kg 8. 062700000NDleldrin < 16. ug/kg 16. 122200000NDDE < 16. ug/kg 16. 061600000NEndrin < 16. ug/kg 16. 122300000NEndosulfan II < 16. ug/kg 16. 062800000NODD < 16. ug/kg 16. 061700000NEndosulfan Sulfate < 16. ug/kg 16. 062900000NDOT < 16. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB- 1016 < 80. ug/kg 80. 063900000NPCB- 1221 < 80. ug/kg 80. 064000000NPCS- 1232 < 80. ug/kg 80. 064100000NPCB -1242 < 80. ug/kg 80. 0642000QONPCB- 1248 < 80. ug/kg 80. 064300000NPCB- 1254 < 160. ug/kg 160. 064400000NPCB- 1260 < 160. ug/kg 160. 064500000N


Nv*ftmin«n Ai

Mtrnmr. Amman Carol ol


Reviewed and Approved by:Sat Rty.raa SWt For Explanation Charles J. Neal01 Symbols And Abbr.vlstlon. And Grniin Leaderour St.nd.rdT.rm. And Condition. MOUP M«™«»

> ANALYSIS REPORT




P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides DRY VT. BASIS QUANTITATION LAB CODEAlpha BBC < 10. ug/kg 10. 060900000NBeta BBC < 10. ug/kg 10. 061000000NDelta BBC < 10. ug/kg 10. 061200000NGamma BBC • Lindane < 10. ug/kg 10. 121800000NBeptachlor < 10. ug/kg 10. 121900000NAldrin < 10. ug/kg 10. 122000000NBeptachlor Epoxide < 10. ug/kg 10. 061500000NEndosulfan I < 10. ug/kg 10. 062700000NDieldrin < 20. ug/kff 20. 122200000NDDB < 20. ug/kg 20. 061600000NEndrin < 20. ug/kg 20. 122300000NEndosulfan II < 20. ug/kg 20. 062800CW",DDD < 20. ug/kg 20. 06170000& )Endosulfan Sulfate < 20. ug/kg 20. 062900000ft**'DOT < 20. ug/kg 20. 122100000NEndrin Ketone < 20. ug/kg 20. 093800000NMethoxychlor < 100. ug/kg 100. 062100000NAlpha Chlordane < 100. ug/kg 100. 136100000NGamma Chlordane < 100. ug/kg 100. 136200000NToxaphene < 200. ug/kg 200. 094200000NPCB-1016 < 100. ug/kg 100. 063900000NPCB-1221 < 100. ug/kg 100. 064000000NPCB-1232 < 100. ug/kg 100. 064100000NPCB-1242 < 100. ug/kg 100. 064200000NPCB-1248 < 100. ug/kg 100. 064300000NPCB-1254 < 200. ug/kg 200. 064400000NPCS-1260 . < 200. ug/kg 200. 064500000N

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliot:1 COPY TO Data Package Group

fwi d tilling,

MunMrAmrwn Counol ol


Reviewed and Approved by:SttRavaratSkJt For Explanation ' Charles J. NelOf Symbol. And Abbnviitloni And Grouo Leader.Our SUndirdTtrm. And Condition. tatoup """"*'

\ III Sample No. SV 1505036Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-OBRel.

RESULT LIMIT OPANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 2,500. mg/kg 20. 014301400Antimony < 5. mg/kg 5. 014401400Barium < 20. mg/kg 20. 014601400Beryllium < 0.5 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 550. mg/kg 10. 015001400Chromium 9. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 8. mg/kff 2. 015301400Iron 4,300. mff/kg 5. 015401400Magnesium 160. mg/kg 10. 015701400Manganese 1. mg/kg 1. 015801400

3 Mercury < 0.04 mg/kg 0.04 015903500Nickel < 4. mg/kg 4. 016101400Potassium 100. mg/kg 50. 016201400Silver < 1. mg/kg 1. 016601400Sodium < 50. ' mg/kg 50. 016701400Vanadium 34. mg/ks 5. 017101400Zinc 3. mg/kg 2. 017201400Cyanide, Total < 0.1 ng/kg 0.1 023704000VOA GC/MS Library Search attached 089005500Arsenic (furnace method) < 1. mg/kg 1. 114504000Lead (furnace method) 3.7 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000Thallium (furnace method) < 1. mg/kg 1. 117304000TCL Volatiles (Soil) attached 117827000TCL Pesticides attached 122528000Moisture ' 15.4 X by wt. 0.1 135301200pB 5.49 0.01 144101000

Note:The pB was performed on a 1:1 slurry (50 gas. of sample and 50 ml.of deionized water) after being tumbled for one hour.

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Blliott1 COPY TO Data Package Group


SttR.y.r.tSid.ForE;plin.iton Nelson B. Rlsser•Of Symbols And AbbrtirlanonrAndi ••••<• . u.nBu»i- ftp/weOur stind.riT«rmMrW condition. •• i. ••• ..... Manager,, GC/NS

Laboratories


Collected 3/29/90 by DSSTybouts Landfill TTP-TP.04-07 Grab Soil Sample Time Collected 1230

P.O. 323-BB-08Rel.

RESULT LIMIT OPANALYSIS DRY UT. BASIS QUANTITATION LAB CODEAluminum 2,950. mg/kg 20. 014301000Antimony < 6. mg/kg 6. 014401000Barium < 20. mg/kg 20. 014601000Beryllium < 0.6 mg/kff 0.6 014701000Cadmium < 0.6 mg/kg 0.6 014901000Calcium 650. rag/kg 10. 015001000Chromium 11. mg/kg 1. 015101000Cobalt < 6. og/kff 6. 015201000Copper 9. mg/kff 2. 015301000Iron 5,090. mi/kg 6. 015401000Magnesium 190. mg/kg 10. 015701000Manganese 1. mg/kg 1. 01580l(XXK>sMercury < 0.05 og/kg 0.05 015901000. i)Nickel < 5. mg/kg 5. OieiOlOOO "*Potassium 120. n>ff/kff 60. 016201000Silver < 1. mg/kg 1. 016601000Sodium < 60. mg/kg 60.' 016701000Vanadium 40. fflg/kg 6. 017101000Zinc 3. mg/kg 2. 017201000Cyanide, Total < 0.1 mg/kg 0.1 023701000VOA GC/MS Library Search attached 089005500Arsenic (furnace method) < 1. mg/kg 1. 114505500Lead (furnace method) 4.4 mg/kg 0.6 115505500Selenium (furnace method) < 0.6 mg/kg 0.6 116405500Thallium (furnace method) < 1. mg/kg 1. 117305500TCL Volatiles (Soil) attached 117827000TCL Pesticides , attached 122527000Moisture "AS RECEIVED* 15.4 X by wt. 0.1 135327000pB 6.49 0.01 144127000




ToniSS"""™™"1*"1 Reviewed and Approved byiStt R.vera. SKtt For Explanation Nelson H. Rlsser B.Of Symbolt And Abbr.vl.tkxia And, • u_.,.,,_r tV/M"!__ _ Our sttndard Term. And condition. . .• . Miiager,,,, uwns

1 wroiw! Amman Cownl olI innnwn". Ino

I Lamasicr



P.O. 323-BB-08Rel.

RESULT LIMIT OPTCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODSChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride < 5. ug/kg 5. 083100000NAcetone 11. ug/kg 10. 091400000NCarbon Disulfide < 5. ug/kg 5. 091500000N1,1-Dlchloroethene < 5. ug/kg 5. 118000000N1,1-Dlchloroethane < 5. ug/kg 5. 083300000N1,2-Dichloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dlchloroethane . < 5. ug/kg 5. OB3600000N2-Butanone < 10. ug/kg 10. 091600000N1,1,1-Trichloroethane < 5. ug/kg 5. 083700000NCarbon Tetrachloride < 5. ug/kg 5. OB3800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodlchloromethane < 5. ug/kg 5. 083900000N1,2-Dichloropropane < 5. ug/kg 5. 084000000NciS;l,3-Dichloropropene < 5. ug/kg 5. 084400000NTrlchloroethene < 5. ug/kg 5. 118100000NDlbromochloromethane < 5. ug/kg 5. 084600000N1,1,2-Trichloroethane < 5. ug/kg 5. 084500000NBenzene < 5. ug/kg 5. 118200000Ntrans-l,3>Dichloropropene < 5. ug/kg 5. 084100QOONBromoform < 5. ug/kg 5. 084700000N4-Methyl-2-Pentanone < 10. ug/kg 10. 091900000N2-flexanone < 10. ug/kg 10. 091800000NTetrachloroethene ' < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene < 5. ug/kg 5. 11B300000NChlorobenzene < 5. ug/kg 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N


I'

Mmnr. Amman Comic*


Reviewed and Approved by:SwRavari.Sldt For Explanation Nelson B. Risser B.A. fl R fl fl fl fl f. 101 Symbol.AndAbbniylttton.And Manaaer, GC/MS Hl\UUUOOJOur SUnd.rdT.rmi And Condition! nonages, uwna

amaster Laboratories

LU Sample No. SV 1505036Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90


P.O. 323-HB-08Rel.

RESULT LIMIT OFTCL Volatiles (Soil) DRY VT. BASIS QUANTITATION LAB CODEChloromethane < 12. ug/kg 12. 082700000NBromomethane < 12. ug/kg 12. 082800000NVinyl Chloride < 12. ug/kg 12. OB2900000NChloroethane < 12. ug/kg 12. 083000000NMethylene Chloride < 6. ug/kg 6. 083100000NAcetone 13. ug/kg 12. 091400000NCarbon Disulflde < 6. ug/kg 6. 091500000N1,1-Dichloroethene < 6. ug/kg 6. 118000000N1,1-Dlchloroethane < 6. ug/kff 6. 083300000N1,2-Dlchloroethene (total) < 6. ug/kg 6. 117900000NChloroform < 6. ug/kg 6. 083500000N1,2-Dlchloroethane < 6. ug/kg 6. 083600000N/~H,2-Butanone < 12. ug/kg 12. 0916000001; : )1,1,1-Trichloroethane < 6. ug/kg 6. 083700000NS*"Carbon Tetrachlorlde < 6. ug/kg 6. 083800000NVinyl Acetate < 12. ug/kg 12. 091700000NBromodichloromethane < 6. ug/kg 6. 083900000N1,2-Dlchloropropane < 6. ug/kg 6. 084000000Ncis-l,3-Dichloropropene < 6. ug/kg 6. 084400000NTrlchloroethene < 6. ug/kg 6. 118100000NDibromochloromethane < 6. ug/kg 6. 084600000N1,1,2-Trlchloroethane < 6. 'ig/kg 6. 084500000NBenzene < 6. ig/kg 6. 118200000Ntrans-l,3-Dlchloropropene < 6. ig/kg 6. 084100000NBromoform < 6. ug/kg 6. 084700000NA.Methyl.2-Pentanone < 12. ;g/kg 12. 091900000N2-Bexanone . < 12. ug/kg 12. 091800000NTetrachloroethene < 6. ug/kg 6. 084800000N1,1,2,2-Tetrachloroethane < 6. ug/kg 6. OB4900000NToluene < 6. ug/kg 6. 118300000NChlorobenzene < 6. ug/kg 6. 118400000NEthylbenzene < 6. ug/kg 6. 085200000NStyrene < 6. ug/kg 6. 092000000NXylenes (total) < 6. ug/kg 6. 092100000N


Questions? Contact Environmental Respectfully Submitted V^fTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

• • • Revleved and Approved bytSttRav.raa Slot For Explanation Nelson B. Rlsser B.Afl R 0 0 0 8 6 kOf Symbol. Arid Abbmlttton.Artdi " • •• • Munamr GC/MS^___ wrst«nardlt«TitAn« condition*;! Manager, uwna

Mwotc Amman Counolol

.VQm pppnoj

"*, TENTATIVELY IDENTIFIED COMPOUNDS I !! 04 !

-ab Name: LANCASTER LABS Contract: !________.!Lab Code: LANCAS Case No.: 253212 SAS No.: SDG No.: TYB2'latrix: (soil/water) SOIL Lab Sample ID: C1505036LSSample wt/vol: 5.0 (g/mL) G Lab File 10: C1505036LSLevel: (low/med) LOW Date Received: 03/29/90X Moisture: not dec. 15 Date Analyzed: 04/05/90lolumn (pack/cap) PACK Dilution Factor: 1.0


! ! t i l l!! CAS NUMBER ! COMPOUND NAME I RT ! EST. CONC. 1 Q II ! »>•••»»»»-» | a»»i»»i«aa»BBM«Baa_aa | aaaaaaaa | aaaaiiaaaaaBaa! aaa» I

, T»«»Y Aconowtion»mal, BWvul t EnwonmmM

Services at (717) 656-2301

1/87Respectfully Submitted. _„.«««•«« Laboratorflfi ftM 8 6 5Reviewed and Approved byt. ,Nelson B. Rlsser B.A.

I Lancaster Laboratories



P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides AS RECEIVED QUANTITATMN LAB CODEAlpha BBC < 8. ug/kff 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. 061200000NGamma BBC • Undone < B. ug/kff 8. 121UOOOOONBeptachlor < 8. ug/kg 8. 121900000NAldrin < 8. ug/kg 8. 122000000NBeptachlor Epoxide < B. ug/kg 8. 061500000NBndosulfan I < 8. ug/kg 8. 062700000NDleldrin < 16. ug/kg 16. 122200000NDDB < 16. ug/kg 16. 061600000NEndrin < 16. ug/kg 16. 122300000NEndosulfan II < 16. ug/kg 16. 062800000tf \ODD < 16. us/kg 16. 0617000001 i!JEndosulfan Sulfate < 16. ug/kg 16. 062900000N"1*'DOT < 16. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 13620QOOONToxaphene < 160. ug/kg ' 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCB-1232 < 80. ug/kg 80. 064100000NPCB-1242 < 80. ug/kg 80. 064200000NPCB-1248 < 80. ug/kg 80. 064300000NPCB-1254 < 160. ug/kg 160. 064400000NPCB-1260 • < 160. ug/kg 160. 064500000N


lAmmMA| Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved byj

> i 'NAI_Y9I<3 RFDO

I LancasterLaboiiiiones

•i LLI Sample No. SV 1505036Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90


P.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Pesticides DRY VT. BASIS QUANTITATION LAB CODEAlpha BBC < 9. ug/kg 9. 060900000NBeta BBC < 9. ug/kg 9. 061000000NDelta BBC < 9. ug/kg 9. 061200000NGamma BBC • Llndane < 9. ug/kg 9. 121800000NBeptachlor < 9. ug/kg 9. 121900000NAldrln < 9. ug/kg 9. 122000000NBeptachlor Epoxide < 9. ug/kg 9. 061500000NBndosulfan I < 9. ug/kff 9. 062700000NDleldrin < 19. ug/kg 19. 122200000NDDE < 19. ug/kg 19. 061600000NBndrln < 19. ug/kg 19. 122300000N

._ Endosulfan II < 19. uff/kg 19. 062800000N] ODD < 19. ug/kg 19. 061700000N

,_„/ Endosulfan Sulfate < 19. ug/kg 19. 062900000NDOT < 19. ug/kg 19. 122100000NEndrin Ketone < 19. ug/kg 19. 093800000NMethoxychlor < 90. ug/kg 90. 06210QOOONAlpha Chlordane < 90. ug/kg 90. 136100000NGamma Chlordane < 90. ug/kg 90. 136200000NToxaphene < 190. ug/kg 190. 094200000NPCB-1016 < 90. ug/kg 90. 063900000NPCB-1221 < 90. ug/kg 90. 064000000NPCB-1232 < 90. ug/kg 90. 064100000NPCB-1242 < 90. ug/kg 90. 064200000NPCB-1248 < 90. ug/kg 90. 064300000NPCB-1254 < 190. ug/kg 190. 064400000NPCB-1260 . < 190. ug/kg 190. 064500000N


Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc...... .• Reviewed and Approved by:

St. Rsurst Sld. For Explanation Charles J. Nealund.,,.„ 01 SymtxH.MdAbbr.yl.tlon. And r™"*?„_; "oir'Sumd.rd'iit(mi'A(Ktcona:itiont,, "rouP Leader,

ANALYSIS REPORT

.ancaster. Laboratories.

Ill Sample No. SV 1505028Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vllmlngton DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Matrix Spike Grab Time Collected 0905Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 2,820. mg/kg 20. 014301400Antimony 18. mg/kg 5. 014401400Barium 150. mg/kg 20. • 014601400Beryllium 3.8 mg/kg 0.5 014701400Cadmium 2.8 rag/kg 0.5 014901400Calcium 1,050. mg/kg 10. 015001400Chromium 26. mg/kg 1. 015101400Cobalt 30. mg/kg 5. 015201400Copper 24. mg/kff 2. 015301400Iron 16,400. mg/kg 5. 015401400Magnesium 460. mg/kg 10. 015701400Manganese 36. mg/kg 1. 01580140Q/-VMercury 0.18 mg/kg 0.04 015903501-y!)Nickel 32. mg/kg 4. 016101400s"*1Potassium 890. mg/kg 50. 016201400Silver 3. mg/kg 1. 016601400Sodium 260. mg/kg 50. 016701400Vanadium 48. mg/kg 5. 017101400Zinc 39. mg/kff 2. 017201400Cyanide, Total 9.0 ng/kg 0.1 023704000VOA GC/MS Library Search attached 089005500Semivolatlle Library Search attached 089309500Arsenic (furnace method) 5, mg/kff 1. 114504000Lead (furnace method) 8.3 mg/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000Thallium (furnace method) 3. mg/kg 1, 117304000TCL Volatiles (Soil) attached 117827000TCL Semi-Volatiles (Soil) attached 120154000TCL Semi.Volatiles (Soil) cont attached 120200000TCL Pesticides attached 122528000

3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliot!1 COPY TO Data Package Group


S..R.vara.Sldt For Explanation Nelson B. Rlsser B.A.Of Symbol. And Abbreviations And M.n.»« TP/MQOur sundtrdTtrmi And Condition! Manager, i«wnsAROQ0868

.> ANALYSIS REPORT

I .Lancaster Laboratories-. ....

•<•, LLI Sample No. SV 1505028Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Matrix Spike Grab Time Collected 0905Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kff 10. '082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride 7. ug/kg 5. 083100000NAcetone 17. ug/kg 10. 091400000NCarbon Dlsulfide < 5. us/kg 5. 091500000N1,1-Dichloroethene 70. ug/kg 5. 118000000N1,1-Dlchloroethane < 5. ug/kff 5. 083300000N1,2-Dlchloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dichloroethane < 5. ug/kg 5. 083IJOOOOON

^ 2-Butanone < 10. ug/kg 10. 091600000N.„_/ 1,1,1-Trichloroethane < 5. ug/kg 5. 083700000N

Carbon Tetrachlorlde < 5. ug/kg 5. 083800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodichloromethane < 5. ug/kg 5. 083900000N1,2-Dlchloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dichloropropene < 5. ug/kg 5. 084400000NTrlchloroethene 58. ug/kff 5. 118100000NDlbromochloromethane < 5. ug/kg 5. OB4600000N1,1,2-Trichloroethane < 5. ug/kg 5. 084500000NBenzene 59. ug/kg 5. 118200000Ntrans-l,3-Dichloropropene < 5. ug/kg 5. 084100000NBromoform < 5. ug/kff 5. 084700000N4-Methyl-2-Pentanane < 10. ug/kg 10. 091900000N2-Bexanone • < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene 62. ug/kg 5. 118300000NChlocobenzene 58. ug/kg 5. 11B400000NEthylbenzene < 5. ug/kg 5. 08520QOOONStyrene ' < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N

3 COPIES TO Duffield Associates, Inc. ATTNt Glenn K. Blllott1 COPY TO Data Package Group


Reviewed and Approved byiSttRavera. SkttForExpl.n.llon Nelson H. Risaer01 Symbol. And AbbmvHUon! And u!i.».. VJVMC___ Our Standard Ttrni. And Condition. Manager, GC/HS

f MmMn Amman Council ol

1 ANALYSIS REPORT

, Lancaster LaboratoriesNO.

TENTATIVELY IDENTIFIED COMPOUNDS I! 01MS

.ab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: 253212 SAS No.: SDG No.; TYB2"atrix: (soil/water) SOIL Lab Sample ID: C1505028LMample wt/vol: 5.0 (g/mL) G Lab Pile ID: C1505028LMLevel: (low/med) LOV Date Received: 03/29/90X Moisture: not dec. 19 Date Analyzed: 04/04/90olumn (pack/cap) PACK Dilution Factor: 1.0


!! CAS NUMBER I COMPOUND NAME ! RT . ! EST. CONC. !

„„ FORM I VOA-TIC 1/87 Rev.(imyAccimninnl(n««. BOOQ.CII & Environnwiul

11 ol tunng,Respectfully SubmittedLancaster LaboraReviewed and A

Technical Services at (717) 656-2301 Nelson B..Rlsjer B.A.irsKotnflwiutwrninntu ino "'•'•'' ' M«n«««•*'f»n /Mp '

> ANALYSIS REPORT

Lancaster Laboratories•J"1"""""™1

Duffield Associates, Inc.5350 Limestone RoadVilmington DE 19808-1296

Tybouts Landfill TTP-TP-01-01 MatrixSoil Sample

TCL Semi- Volatiles (Soil)phenolbis (2-chloroethyl) ether2'Chlorophenol1,3-dichlorobenzene1,4-dlchlorobenzenebenzyl alcohol1,2-dlchlorobenzene2-methylphenolbis (2-chloroisopropyl) ether4-methylphenolN-nitrosodi-n-propylaminehe'xachloroethane

} nitrobenzenes Isophorone

2-nitrophenol2,4-dlmethylphenolbenzole acidbis (2-chloroethoxy) methane2,4-dichlorophenol1,2,4-trichlorobenzenenaphthalene4-chloroanllinehexachlorobutadlene4 • chloro • 3 • me thylphenol2-methylnaphthalenehexachlorocvclopentadiene2,4,6-trichlorophenol2,4,5-trichlorophenol2-chloronaphthalene2-nitroanilinedimethyl phthalateacenaphthylene

Spike Grab

RESULTAS RECEIVED4,770.< 330.4,720.< 330.2,400.< 330.< 330.< 330.< 330.< 330.3,180.< 330.< 330.< 330.< 330.< 330.

< 1,700.< 330.< 330.2,670.< 330.< 330.< 330.3,620.< 330.< 330.< 330.

< 1,700.< 330.

< 1,700.< 330.< 330.


LLI Sample No. SV 1505028Date Reported 5/ 2/90Date Submitted 3/29/90Discard Date 6/ 2/90Collected 3/29/90 by DSSTime Collected 0905P.O. 323-BB-08Rel.

LIMIT OPQUANTITATION LAB CODB

330. 118500000N330. 066700000N330. - 118600000N330. 067700000N330. 118700000N330. 092600000N330. 067600000N330. 092700000N330. 066800000N330. 092800000N330. 118800000N330. 069200000N330. 069600000N330. 069400000N330. 065100000N330. 064800000N

1,700. 092900000N330. 066600000N330. 064700000N330. 118900000N330. 069500000N330. 093000000N330. 069000000N330. 119000000N330. 093100000N330. 069100000N330. 065600000N

1,700. 093200000N330. 067200000N

1,700. 093300000N330. 068100000N330. 065800000N


\__>nein' TSimyAo



MWw: Amman wmrtol} m tol XKA ***** i«i«.

> ANALYSIS REPORT

Lancaster Laboratories... ....MMNowllollarelPiko. I..IIB

LLI Sample No. SV 1505028Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTF-TP-01-01 Matrix Spike Grab Time Collected 0905Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Semi-Volatiles (Soil) cont AS RECEIVED QUANTITATION LAB CODE3-nitroanlllne < 1,700. ug/kg 1,700. 093400000Nacenaphthene 2,760. ug/kg 330. 119100000N2,4-dinitrophenol < 1,700. ug/kg 1,700. 065000000N4-nitrophenol 5,900. ug/kg 1,700. 119200000Ndlbenzofuran < 330. ug/kg 330. 093500000N2,4-dinitrotoluene 3,280. ug/kg 330. 119300000N2,6-dlnitrotoluene < 330. ug/kg 330. 068400000Ndiethyl phthalate < 330. ug/kg 330. 068000000N4-chlorophenyl phenyl ether < 330. ug/kg 330. 067300000Nfluorene < 330. ug/kg 330. 068800000N4-nltroanlline < 1,700. ug/kg 1,700. 093600000N2-methyl-4,6-dinltrophenol • < 1,700. ug/kg 1,700. 0649000001.,,N-nitrosodlphenylamine < 330. ug/kg 330. 069900000Pi•)4-bromophenyl phenyl ether < 330. ug/kg 330. 0670000001 'hexachlorobenzene < 330. ug/kg 330. 068900000Npentachlorophenol 4,000. ug/kg 1,700. 119400000Nphenanthrene < 330. ug/kg 330. 070000000Nanthracene < 330. ug/kg 330. 065900000Ndi-n-butyl phthalate < 330. ug/kg 330. 068200000Nfluoranthene < 330. ug/kg 330. 068700000Npyrene 3,610. ug/kg 330. 119500000Nbutyl benzyl phthalate < 330. ug/kg 330. 067100000N3,3'-dlchlorobenzidlne < 670. ug/kg 670. 067900000Nbenzo (a) anthracene < 330. ug/kg 330. 0661000QONbis (2-ethylhexyl) phthalate < 330. ug/kg 330. 066900000Nchrysene < 330. ug/kg 330. 067400000Ndi-n-octyl phthalate < 330. ug/kg 330. 068500000Nbenzo (b) fluoranthene ' < 330. ug/kg 330. 066300000Nbenzo (K) fluoranthene < 330. ug/kg 330. 066500000Nbenzo (a) pyrene < 330. ug/kg 330. 066200000Nindeno (1,2,3-cd) pyrene < 330. ug/kg 330. 069300000Ndibenz (a,h) anthracene < 330. ug/kg 330. 067500000Nbenzo (ghl) perylene < 330. ug/kg 330. 066400000N


, An™™ A.MMi»ni« Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved by:S.tR.v.ra.Sld. For Explanation Timothy S. OostdvlOf Symbol. And Abbr.vl.tlon. And " „ { „ " :,„',Our SUndtrd Ttrmt And Condition. <«oup Leafier, GC/

irwotnMnl UDoifllonni ira

> ' v ANALYSIS REPORT

.ancaster. L oratories

! T0101MS ILab Name: LANCASTER LABS Contract: __. !________!Lab Code: LANCAS Case No.: __. SAS No.: __. SDG No.: __.Matrix: (soil/water) SOIL Lab Sample ID: 1505028Sample wt/vol: 30.0(g/mL) G Lab Pile IDi >E5604Level: (low/med) LOV Date Received: 03/29/90% Moisture: not dec. 19.0 dec. __. Date Extracted: 04/30/90Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 04/03/90GPC Cleanup: (Y/N) N pB: 5.51 Dilution Factor: 1.000

CONCENTRATION UNITS:Number TICs found: 3 (ug/L oc ug/Kg) UG/KG

!CAS NUMBER

1.2.3./>.

^ 5l) «•.i 7.

8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.

COMPOUND NAME

UnknownUnknown alicyclic compoundUnknown

RT

8.3134.4340.49

EST. CONC.

660.450.290.

Q

JBJBJ

FORM I SV-TIC 1/87 Rev.

Mwcuion lorAccfWiiaiion

Respectfully SubmittedswRtwriiSWiForEapliMtlon Lancaster Laboratories. Inc.sr'T656-2301 Timothy S. Oo,

Pi*nitn TniHor f\F /UC

> ANALYSIS REPORT

Lancaster Laboratories, Hw lloll.inil 1'iMl

LLI Sample No. SV 1505028Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilnington DB 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Matrix Spike Grab Time Collected 0905Soil Sample P.O. 323-BB-OB

Rel.RESULT LIMIT OF

TCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BHC < 8. ug/kg 8. 061200000NGamma BBC • Lindane 24. ug/kg 8. 121BOOOOONBeptachlor 25. ug/kg 8. 121900000NAldrin 26. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NBndosulfan I < 8. ug/kg 8. 062700000NDleldrin 63. ug/kg 16. 122200000NDDE < 16. ug/kg 16. 061600000NEndrin 69. ug/kg 16. 122300000NEndosulfan II < 16. ug/kg 16. 062800000NDDD < 16. ug/kg 16. 061700000NEndosulfan Sulfate < 16. ug/kg 16. 062900000NDDT 59. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCS-1232 < 80. ug/kg 80. 064100000NPCB.1242 < 80. ug/kg 80. 064200000NPCB-1248 < 80. ug/kg 80. 064300000NPCB-1254 < 160. ug/kg 160. 064400000NPCS-1260 < 160. ug/kg 160. 064500000N



Reviewed and Approved byiStt Ravara. SWt For Explanation Charles J. Neslund. BOf Symbolt And Abbr.vl.tlon. And p""* ?._i " il_II P7,Our Srtn<HrdT«mi And Condition. GMUP Leader, Pesticli

> ANALYSIS REPORT

I LancasterLdboratories ...••OSNnwillollandPikn.Liru-.;

LLI Sample No. TL 1505031Duffield Associates, Inc. Date Reported 5/ 7/905350 Lines tone Road Date Submitted 3/29/90Viluinjton DB 19808-1296 Discard Date 6/7/90

Collected 3/29/90 by DSSEP Toxicity Leachate of Tybouts Landfill Tine Collected 0905TTP-TP-01-01 Matrix Spike Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUANTITATION LAB CODE3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elliott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.°** °1963 230l°° 06270° Reviewed and Approved by:

St. Rtvtrtt SW. For Explanation Nelson B. Rlsser B. A> n n n n -i r-/TO 0 0 0 8 7 5

t ANALYSIS REPORT

Lancaster. Laboratories,.,..,, „4 25 Now Holland Piko,Ui"<

LLI Sample No. TL 1505031Duffield Associates, Inc. Date Reported 5/ 7/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/7/90

Collected 3/29/90 by DSSBP Toxicity Leachate of Tybouts Landfill Time Collected 0905TTP-TP-01-01 Matrix Spike Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

ANALYSIS AS RECEIVED QUANTITATION LAB CODBAluminum 2.0 rag/1 0.1 024301400Antimony 0.47 mg/l 0.05 024401400Barium 1.9 ng/1 0.1 024601400Beryllium 0.048 rag/1 0.005 024701400Cadmium 0.052 mg/l 0.005 024901400Calcium 3.0 mg/l 0.5 025001400Chromium 0.18 mg/l 0.01 025101400Cobalt 0.50 mg/l 0.05 025201400Copper 0.25 mg/l 0.02 025301400Iron 1.01 mg/l 0.05 025401400Magnesium 2.27 og/1 0.05 025701400Manganese 0.49 ng/1 0.01 025801400Mercury 0.0010 mg/l 0.0002 025902500Nickel ' 0.49 rag/1 0.04 026101400Potassium 3. mg/l 1. 026201400Silver 0.05 rag/1 0.01 026601400Sodium 5.6 mg/l 0.5 026701400Vanadium 0.48 mg/l 0.05 027101400Zinc 0.35 rag/1 0.02 027201400Arsenic (furnace method) ~ 0.04 mg/l ' 0.01 104503000Lead (furnace method) 0.021 rag/1 0.005 105503000Selenium (furnace method) 0.010 rag/1 0.005 106403000Thallium (furnace method) 0.05 mg/l 0.01 107303000

The above analyses were performed on an EP Toxicity leachate of thesubmitted waste prepared according to the procedure specified inFederal Register May 19 1980 p. 33127.A sample is considered EP Toxic if any of the contaminant concentra-tions (rag/1) in the leachate exceed the following maxima (100 times thePrimacy Drinking Vater Standards))

Arsenic 5.0, Barium 100.0, Cadmium 1.0, Chromium 5.0, Lead 5.0,Mercury 0.2, Selenium 1.0, Silver 5.0, Endrin 0.02, Llndane 0.4,Methoxychlor 10.0, Toxaphene 0.5, 2,4-D 10.0, 2,4,5-TP 1.0.

Based on the determinations performed, the submitted sample DOBS NOTexhibit the characteristic of BP Toxicity as defined in Section 261.24Federal Register 1980 p. 33122.


Reviewed and Approved by:SttR»vtr.tSldiForExpl«n«tlon Nelson B. Risser B.A.Of Symbol. And Abbrtyl.llon. And Hammer RC/MQ 0 fl fl fl 0 0 1 rour Sttndtrd Ttrmt And Condition. Manager, GC/NS HnUUUo/6

ANALYSIS REPORT

LLI Sample No. SV 1505029Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Viloington DE 19808-1296 Discard Date 6/ 2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Matrix Spike Dup. Time Collected 0905Grab Soil Sample P.O. 323-HB-08

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum 3,100. mg/kg 20. 014301400Antimony < 5. mg/kg 5. 014401400Barium 30. rag/kg 20. 014601400Beryllium 1.1 mg/kg 0.5 014701400Cadmium < 0.5 mg/kg 0.5 014901400Calcium 780. mg/kg 10. 015001400Chromium 28. mg/kg 1. 015101400Cobalt < 5. mg/kg 5. 015201400Copper 13. mg/kg 2. 015301400Iron 34,800. mg/kg 5. 015401400Magnesium 320. tag/kg 10. 015701400Manganese 22. mg/kg 1. 015801400Mercury < 0.04 tog/kg 0.04 015903500Nickel 5. mg/kg 4. 016101400Potassium 700. mg/kg 50. 016201400Silver < 1. ng/kg 1. 016601400Sodium < 50. mg/kg 50. 016701400Vanadium 45. ng/kg 5. 017101400Zinc 19. mg/kg 2. 017201400Cyanide, Total < 0.1 mg/kg 0.1 023704000VOA GC/MS Library Search attached 089005500Semivolatlle Library Search attached 089309500Arsenic (furnace method) < 1. ng/kg 1. 114504000Lead (furnace method) 4.5 rag/kg 0.5 115504000Selenium (furnace method) < 0.5 mg/kg 0.5 116404000Thallium (furnace method) < 1. rag/kg 1. 117304000TCL Volatiles (Soil) attached 117827000TCL Semi.Volatiles (Soil) attached 120154000TCL Semi.Volatiles (Soil) cont attached 120200000TCL Pesticides attached 122528000Moisture 19.2 Z by wt. 0.1 135301200pB 5.43 0.01 144101000



H . r G c H / i n n o ,Our sundird T.rmi And Condition. • Manager, GC/MS flflU00877

.> ' ANALYSIS REPORT

, Lancaster L Iworatones

'«, LLI Sample No. SV 1505029Duffield Associates, Inc. Date Reported 5/ 2/905350 Linestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90

Collected 3/29/90 by DSSTybouts Landfill TTP-TP-01-01 Matrix Spike Dup. Time Collected 0905Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OP

TCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChlororaethane < 10. ug/kg 10. OB2700000NBrononie thane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. - 082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride 6. ug/kg 5. 083100000NAcetone 20. ug/kg 10. 091400000NCarbon Dlsulfide < 5. ug/kg 5. 091500000N1,1-Dlchloroethene 67. ug/kg 5. 11BOOOOOON1,1-Dlchloroethane < 5. ug/kg 5. 083300000Nl,2-Dlchloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dichloroethane . < 5. ug/kg 5. 083600000N

" \ 2-Butanone < 10. ug/kg 10. 091600000NJ 1,1,1-Trlchloroethane < 5. ug/kg 5. OB3700000N

Carbon Tetrachloride < 5. ug/kg 5. 083800000NVinyl Acetate < 10. ug/kg 10. 091700000NBromodichloromethane < 5. ug/kg 5. 083900000N1,2-Dichloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dlchloropropene < 5. ug/kg 5. OB4400000NTrlchloroethene 54. ug/kg 5. 11B100000NDibrotnochloromethane < 5. ug/kg 5. 084600000N1,1,2-Trichloroethane < 5. ug/kg 5. 084500000NBenzene 57. ug/kg 5. 118200000Ntcans-l,3.Dichloropropene < 5. ug/kg 5. 08410QOOONBromoform < 5. ug/kg 5. 084700000N4-Kethyl-2.Pentanone < 10. ug/kg 10. 091900000N2-Hexanone. < 10. ug/kg 10. 091800000NTetrachloroethene ' < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene 59. ug/kg 5. 118300000NChlorobenzene 54. ug/kg 5. 118400000NEthylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenes (total) < 5. ug/kg 5. 092100000N



Reviewed and Approved byiSt«R.ytr«tSldtForE»pl.nillonj Nelson B. Rlssi

Mtrnw. Amman Cwrolol'IXMOWQWI UMf imnm ire

SttRtvtntSldtForExplan.llon Nelson B. Rlssei iB.A,<*Of Symbol.AndAbbr.»Utlont And • MmiMer GC/MS flniTDflft 7 fiour at.nd.rd T.rm. And Condition. nanager, w,/ns.n " w u U 0 / Q

ANALYSIS REPORl

botulones^

4 TENTATIVELY IDENTIFIED COMPOUNDS !! 01MSD

ib Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: 253212 SAS No.: SDGNo.:TYB2

! "itrlx; (soil/water) SOIL Lab Sample ID: C1505029LPmple wt/vol: 5.0 (g/mL) G Lab Pile ID: C1505029LP

_avel: (low/med) LOV Date Received: 03/29/90X Moisture: not dec. 19 Date Analyzed: 04/04/90)lunn (pack/cap) PACK Dilution Factor: 1.0


CAS NUMBER ! COMPOUND NAME ! RT 1 EST. CONC. !...............|........................a...|........|a............|.

.!.

——AHOC., ««» I VOA-T1C 1/87 Rev.XKlwy AceilCitawn---"'• '" ronmfflu

Respectfully SubmittedsttRtvOTtsidtForEwifnttio^ Lancaster Laboratojc Iqc

Reviewed and656-2301 Nelson B. Risser B.A.

Manager,

> ANALYSIS REPORT

Lancaster.Laboratories ...

LLI Sample No. Stf 1505029Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vllnington DB 19808-1296 Discard Date 6/2/90


Rel.RESULT LIMIT OP

TCL Seal.Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEphenol 4,850. ug/kg 330. 118500000Nbis (2-chloroethyl) ether < 330. ug/kg 330. 066700000N2-chlorophenol 4,900. ug/kg 330. 118600000N1,3-dichlorobenzene < 330. ug/kg 330. 0«7700000N1,4-dichlorobenzene 2,450. ug/kg 330. 118700000Nbenzyl alcohol < 330. ug/kg 330. 092600000N1,2-dichlorobenzene < 330. ug/kg 330. 067600000N2-methylphenol < 330. ug/kg 330. 092700000Nbis (2-chlorolsopropyl) ether < 330. ug/kg 330. 066BOOOOON4-methylphenol < 330. ug/kg 330. 092800000NN-nitrosodl-n-propylamlne 3,280. ug/kg 330. 118800000Nhexachloroethane < 330. ug/kg 330. 069200000N

""""S nitrobenzene < 330. ug/kg 330. 069600000Nisophorone < 330. ug/kg 330. 069400000N2-nltrophenol < 330. ug/kg 330. 065100000N2,4-dimethylphenol < 330. ug/kg 330. 064800000Nbenzole acid < 1,700. ug/kg 1,700. 092900000Nbis (2-chloroethoxy) methane < 330. ug/kg 330. 066600000N2,4-dichlorophenol < 330. ug/kg 330. 064700000N1,2,4-trlchlorobenzene 2,670. ug/kg 330. 118900000Nnaphthalene < 330. >ig/k« 330. 069500000N4-chloroanlllne < 330. ig/kg 330. 093000000Nhexachlorobutadlene < 330. ^/kg 330. 069000000N4-chloro-3.inethylphenol 5,810. ^/icg 330. 119000000N2-methylnaphthalene < 330. ig/kg 330. 093100000Nhexachlorocyclopentadlene < 330. ig/kg 330. 069100000N2,4,6-trlchlorophenol < 330. ig/kg 330. 065600000N2,4,5-trichlorophenol < 1,700. ug/kg 1,700. 093200000N2-chloronaphthalene < 330. ug/kg 330. 0672QOOOON2-nitroaniline < 1,700. ug/kg 1,700. 093300000Ndimethyl phthalate < 330. ug/kg 330. 068100000Nacenaphthylene < 330. ug/kg 330. 065800000N

3 COPIES TO Duffield Associates, Inc. ATTN; Glenn K. Elliott1 COPY TO Data Package Group

JnonAiKMiwiio) Questions? Contact Environmental Respectfully Submittedx~- 0«««««im__.. Technical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved byiSMfl.vtrs. SldtForExpl.n.llon Tlmochv S. OostdvlOf Symbol. And Abbrtvl.ttona And """nf *' "os™>1!

i __^ Our Slsnd.rd T.rms And Conditions Group Leader, GO,MmMr Anwicin Cwnol of'"'"" ' ' omlonii.lnc.

* \NALYSIS REPORT. __^——i:——^—————————————————, La wtcr L aboratones

LLI Sample No. SV 1505029Duffield Associates, Inc. Date Reported 5/ 2/905350 Lines tone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90


Rel.RESULT LIMIT OP

TCL Semi-Volatiles (Soil) cont AS RECEIVED QUANTITATION LAB CODE3-nitroanlline < 1,700. ug/kg 1,700. 093400000Nacenaphthene 2,620. ug/k_ 330. 119100000N2,4-dinitrophenol < 1,700. ug/kg 1,700. • 065000000N4-nltrophenol 6,200. ug/kg 1,700. 119200000Ndibenzofuran < 330. ug/kg 330. 093500000N2,4.dinitrotoluene 3,340. ug/kg 330. 119300000N2,6-dinitrotoluene < 330. ug/kg 330. 068400000Ndiethyl phthalate < 330. ug/kg 330. 068000000N4-chlorophenyl phenyl ether < 330. ug/kg 330. 067300000Nfluorene < 330. ug/kg 330. 068800000NA.nltroanillne < 1,700. ug/kg 1,700. 093600000N2-methyl.4,6-dlnltrophenol .< 1,700. ug/kg 1,700. 0649000001 •N-nitrosodlphenylamine < 330. ug/kg 330. 0699000001' )4-bronophenyl phenyl ether < 330. ug/kg 330. 067000000(N«'hexachlorobenzene < 330. ug/kg 330. 068900000Npentachlorophenol 4,000. ug/kg 1,700. 119400000Nphenanthrene < 330. ug/kg 330. 070000000Nanthracene < 330. ug/kg 330. 065900000Ndi-a-butyl phthalate < 330. ug/kg 330. 06B200000Nfluoranthene < 330. ug/kg ' 330. 06B700000Npyrene 3,280. ug/kg 330. 119500000Nbutyl benzyl phthalate < 330. ug/kg 330. 067100000N3,3'.dlchlorobenzldine < 670. ug/kg 670. 067900000Nbenzo (a) anthracene < 330. ug/kg 330. 066100000Nbis (2-ethylhexyl) phthalate < 330. ug/kg 330. 066900000Nchrysene < 330. ug/kg 330. 067400000Ndl-n-octyl phthalate < 330. ug/kg 330. 068500000Nbenzo (b) fluoranthene ' < 330. ug/kg 330. 066300000Nbenzo (K) fluoranthene < 330. ug/kg 330. 066500000Nbenzo (a) pyrene < 330. ug/kg 330. 066200000Nindeno (1,2,3-cd) pyrene < 330. ug/kg 330. 069300000Ndibenz (a,h) anthracene • < 330. ug/kg 330. 067500000Nbenzo (ghl) perylene < 330. ug/kg 330. 066400000N3 COPIBS TO Duffield Associates, Inc. ATTN: Glenn K. Blllott1 COPY TO Data Package Group


Reviewed and Approved byiSMRavtrst Slot For Explanation TlOOthy S. Oostdyk, B.A.Of Symbol. And Abbnvlttloni And Grouo Leader. G"""J 'Our SUnd.rdT.rm. And Condition. u v "*"'""•• "

MunMr. Armnwn Coinal olironpffifflml UMf'trm" IF"

> v ANALYSIS REPORT

.ancaster Laboratories

! TP101MSDLab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: __, SAS No.: __. SDG No.: __.Matrix: (soil/water) SOIL Lab Sample ID: 1505029Sample wt/vol: 30.0(g/mL) G Lab Pile ID: >E5605Level: (low/med) LOV Date Received: 03/29/90X Moisture: not dec. 19.0 dec. __. Date Extracted: 04/30/90Extraction: (SepP/Cont/Sonc) SONC Date Analyzed: 04/03/90GPC Cleanup: (Y/N) N pB: 5.51 Dilution Factor: 1.000


CAS NUMBER

1.2.3.4-

V-J6.1 7.

8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.

COMPOUND NAME

UnknownUnknown alicyclic hydrocarboUnknown

RT

8.3134.4340.50

EST. CONC.

620.290.210.

Q

JBJBJ


Respectfully SubmittedLancaster LaboratorlMr, Inc.Reviewed and ApprovM tyl) 0882.

2301 Timothy S. Oostdyk, B.A. °£

> ANALYSIS REPORT

'Master Laboratories-<s LLI Sample No. SV 1505029

Duffield Associates, Inc. Date Reported 5/ 2/905350 Lines tone Road Date Submitted 3/29/90Vllmlngton DB 19808-1296 Discard Date 6/ 2/90


Rel.RESULT LIMIT OP

TCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 061000000NDelta BBC < 8. ug/kg 8. 061200000NGamut BBC • Llndane 26. ug/kg 8. 121800000NBeptachlor 27. ug/kg 8. 121900000NAldrln 27. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NEndosulfan I < 8. ug/kg B. 062700000NDieldrin 68. ug/kg 16. 122200000NDDB < 16. ug/kg 16. 061600000NEndrin 73. ug/kg 16. 122300000NEndosulfan II < 16. ug/kg 16. 062800000N/~SODD < 16. ug/kg 16. 0617000001V"Bndosulfan Sulfate < 16. ug/kg 16. 062900000N>DOT 66. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093800000NMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB-1016 < 80. ug/kg 80. 063900000NPCB-1221 < 80. ug/kg 80. 064000000NPCB-1232 < 80. u_/kg 80. 064100000NPCB-1242 < 80. ug/kg 80. 064200000NPCB-1248 < 80. ug/kg 80. 064300000NPCB-1254 < 160. •in/kg 160. 0644000QONPCB-1260 . < 160. ig/kg 160. 064500000N

3 COPIES TO Duffield Associates, Inc. • ATTN: Glenn K. Elllott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully Submitted'££$£££?* Technical Services at (717) 656-2301 Lancaster Laboratories, Inc.TSftimT**6™™™1' Reviewed and Approved by:"!HrV .rj_j_fo SMR.v.rs.SldtForExplan.tlon Charles J. Nes

WmMr, Amman Coral M

Of Symbol. And Abbr.vl.tlon. And Grouo Leader, Ft)Our SUndtrdTtrmt And Condition. ' 9 wouor, *o

> ANALYSIS REPORT

I Lancaster Laboratories......425 Now Holland Rko,

LLI Sample No. TL 1505032Duffield Associates, Inc. Date Reported 5/ 7/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/7/90

Collected 3/29/90 by DSSBP Toxicity Leachate of Tybouts Landfill Tine Collected 0905TTF-TP-Ol-Ol Matrix Spike Dup. Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODE3 COPIES TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.°** °1963 230>0° 06270° Reviewed and Approved by«

Nelson B. RlsserJiMMKS. u' oymoon mia ADDr.vi.inna ma•iWJW.'l Our s""dlrd Ttrml And Condition.

Mwimr Amman Caiwlot

Sit RavtritSldt For Explanation Nelson B. Rlsser BuAa n n n n mOf symbol. And Abbr.yl.tton. And Mnna»4r rr/iw ™ n U 0 0 8 8 kOur SUndardTarms And Conditions Manager, GC/MS nnwuwuU4

> ANALYSIS REPORT

I Lancaster Laboratories ....•IM New Mland Pikt>

LLI Sample No. TL 1505032Duffield Associates, Inc. Date Reported 5/ 7/905350 Limestone Road Date Submitted 3/29/90Vilmington DE 19808-1296 Discard Date 6/7/90

Collected 3/29/90 by DSSBP Toxicity Leachate of Tybouts Landfill Time Collected 0905TTF-TP-01-01 Matrix Spike Dup. Grab Soil Sample P.O. 323-BB-08

Rel.RESULT LIMIT OF

ANALYSIS AS RECEIVED QUANTITATION LAB CODBAluminum < 0.1 ng/1 0.1 024301400Antimony < 0.05 mg/l 0.05 024401400Barium < 0.1 mg/l 0.1 024001400Beryllium < 0.005 ng/1 0.005 024701400Cadmium < 0.005 mg/l 0.005 024901400Calcium 0.9 ng/1 0.5 025001400Chromium 0.02 ng/1 0.01 025101400Cobalt < 0.05 mg/l 0.05 025201400Copper < 0.02 ng/1 0.02 025301400Iron 0.06 mg/l 0.05 025401400Magnesium 0.35 mg/l 0.05 025701400Manganese < 0.01 ng/1 0.01 025801400 ,Mercury < 0.0002 mg/l 0.0002 025902500 r': )Nickel < 0.04 ng/1 0.04 026101400Potassium < 1. ng/1 1. • 026201400Silver < 0.01 mg/l 0.01 026601400Sodium 1.6 ng/1 0.5 026701400Vanadium < 0.05 rag/1 0.05 027101400Zinc 0.14 mg/l 0.02 027201400Arsenic (furnace method) " < 0.01 ng/1 0.01 104503000Lead (furnace method) < 0.005 mg/l 0.005 105503000Selenium (furnace method) < 0.005 mg/l 0.005 106403000Thallium (furnace method) < 0.01 ng/1 0.01 107303000


Arsenic 5.0, Barium 100.0, Cadmium 1.0, Chromium 5.0, Lead 5.0,Mercury 0.2, Selenium 1.0, Silver 5.0, Endrin 0.02, Lindane 0.4,Methoxychlor 10.0, Toxaphene 0.5, 2,4-D 10.0, 2,4,5-TP 1.0.

Based on the determinations performed, the submitted sample DOBS NOTexhibit the characteristic of BP Toxicity as defined in Section 261.24Federal Register 1980 p. 33122.


Reviewed and Approved byi •Sat Rtvtrst 3Wt For Explanation Nelson B. Rissermm " " '

WmwrAmnan Council ol

Of Symbol. And Abbrtvltttons And Manager, GC/MSOur Sttndird Tarm. And Condition. ntwMnni;, uwna

Lancaster Laboratories^ ^ SigigglgWffgg ^'*• LLI Sample No. SV 1505038

Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilnington DE 19808-1296 Discard Date 6/ 2/90

Tybouts Landfill Method BlankP.O. 323-HB-08Rel.

RESULT LIMIT OFANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum < 20. ng/kg 20. 014300000Antinony < 5. mg/kg 5. 014400000Barium < 20. mg/kg 20. ' 014600000Beryllium < 0.5 mg/kg 0.5 014700000Cadmium < 0.5 ng/kg -0.5 014900000Calcium < 10. rag/kg 10. 015000000Chromium < 1. mg/kg 1. 015100000Cobalt < 5. mg/kg 5. 015200000Copper < 2. mg/kg 2. 015300000Iron < 5. ng/kg 5. 015400000Magnesium < 10. mg/kg 10. 015700000

--x Manganese < 1. rag/kg 1. 015800000. j Mercury < 0.04 mg/kg 0.04 015900000

—/ Nickel < 4. rag/kg 4. 016100000Potassium < 50. mg/kg 50. 016200000Silver < 1. ng/kg 1. 016600000Sodium < 50. rag/kg 50. 016700000Vanadium < 5. ng/kg 5. 017100000Zinc < 2. rag/kg 2. 017200000Cyanide, Total < 0.1 mg/kg 0.1 023700000VOA GC/MS Library Search attached 089000000Semivolatlle Library Search attached 089300000Arsenic (furnace method) < 1. mg/kg 1, 114500000Lead (furnace method) < 0.5 mg/kg 0.5 115500000Selenium (furnace method) < 0.5 mg/kg 0.5 116400000Thallium (furnace method) < 1, mg/kg 1, 117300000TCL Volatiles (Soil) attached 117800000TCL Semi-Volatiles (Soil) attached 120100000TCL Serai-Volatiles (Soil) cent attached 120200000TCL Pesticides attached 122500000pB 6.62 0.01 144100000

Note:The pB was performed on a 111 slurry (50 gms. of sample and 50 ml.of deionized water) after being tumbled for one hour.


, 'x**ffl(nMnA Questions? Contact Environmental Respectfully Submitted. ......... Technical Services at (717) 656-2301 Lancaster Laboratories, Inc.

r,««»7M"e"v"ai™n11' 12001963 0.00 000000 Reviewed and Approved by:St. Rav.nt aid. For Explanation Nelson B. .._.Of Symbol. And Abbnvlitkmi And M.naoAr W/M<J___ our siindsrdTtrm. And Condition. Manager, GC/HS

I Mmwn Amman cowolol

•\MA!YS!S REPORT

I Lancaskr Laboratories

LLI Sample No. SV 1505038Duffield Associates, Inc. Date Reported 5/ 2/905350 Lines tone Road Date Submitted 3/29/90Wllmington DE 19808-1296 Discard Date 6/2/90

Tybouts Landfill Method BlankP.O. 323-BB-08Rel.

RESULT LIMIT OFTCL Volatiles (Soil) AS RECEIVED QUANTITATION LAB CODEChloromethane < 10. ug/kg 10. 082700000NBromomethane < 10. ug/kg 10. 082800000NVinyl Chloride < 10. ug/kg 10. 082900000NChloroethane < 10. ug/kg 10. 083000000NMethylene Chloride < 5. ug/kg 5. 083100000NAcetone < 10. ug/kg 10. 091400000NCarbon Disulfide < 5. ug/kg 5. 091500000N1,1-Dlchloroethene < 5. ug/kg 5. 118000000N1,1-D1chloroethane < 5. ug/kg 5. 083300000N1,2-Dlchloroethene (total) < 5. ug/kg 5. 117900000NChloroform < 5. ug/kg 5. 083500000N1,2-Dichloroethane < 5. ug/kg 5. 083600000N/*?'.,2-Butanone < 10. ug/kg 10. 091600000N, ' !.1,1,1-Trichloroethane < 5. ug/kg 5. 083700000NN;*i''Carbon Tetrachloride < 5. ug/kg 5. 083800000NVinyl Acetate < 10. ug/kg 10. 091700000NBronodlchloronethane < 5. ug/kg 5. 083900000N1,2-Dlchloropropane < 5. ug/kg 5. 084000000Ncis-l,3-Dlchloropropene < 5. ug/kg 5. 084400000NTrlchloroethene < 5. ug/kg 5. 118100000NDlbromochloronethane < 5. ug/kg 5. 084600000N1,1,2-Trlchloroethane < 5. ug/kg 5. 084500000NBenzene < 5. ug/kg 5. 118200000Ntcans-l,3-Dichloropropene < 5. ug/kg 5. 084100000NBromoform < 5. ug/kg 5. 084700000N4.Methyl.2.Pentanone < 10. ug/kg 10. 091900000N2-Bexanone < 10. ug/kg 10. 091800000NTetrachloroethene < 5. ug/kg 5. 084800000N1,1,2,2-Tetrachloroethane < 5. ug/kg 5. 084900000NToluene < 5. ug/kg 5. 118300000NChlorobenzene < 5. ug/kg 5. 118400000N •Ethylbenzene < 5. ug/kg 5. 085200000NStyrene < 5. ug/kg 5. 092000000NXylenea (total) < 5. ug/kg 5. 092100000N

3 COPIBS TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPT TO Data Package Group

,(*i,Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.

Reviewed and Approved byiSat Rtvara. SMt For Explanation Nelson B. RlssernB-.Ai „01 Symbol. And Abbr.yl.llon. And M.naoer GC/MS AnDfiflflft?_____ our Stind.rdl.rm. And condition.. Manager, W/tlS HnuUUOO/

M«r»»c Amman Council ol

> \ M\|AIYSIS REPORTV > \

ancasiei '9>jw/uiM 'ies

TENTATIVELY IDENTIFIED COMPOUNDS

.ab Name: LANCASTER LABS Contract: _____Lab Code: LANCAS Case No.i 253212 SAS No.: SDG No.: TYB2"atrlx: (soil/water) SOIL Lab Sample ID: C150503BLample wt/vol: 5.0 (g/mL) G Lab Pile ID: C1505038LLevel: (low/med) LOW Date Received: 03/29/90f. Moisture: not dec. 0 Date Analyzed; 04/04/90olunn (pack/cap) PACK Dilution Factor: 1.0

CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/KG! ! I I I !

11 CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q I"'"""""""""'•'""""""""""""""""-"•-•"•"• •"•—"—• "-"

PORM J VOA'TIC 1/fl7

Respectfully SubmittedLancaster LaboratoiReviewed and

echnicaT'Services'at (717)" 656-2301 Nelson B. Rlsser B.A.

W^LYSIS REPORT

ancaster Laboratories•*,

Duffield Associates, Inc.5350 Limestone RoadVilmington DE 19808-1296

Tybouts Landfill Method Blank

TCL Semi- Volatiles (Soil)phenolbis (2-chloroethyl) ether2-chlorophenol1,3-dichlorobenzene1,4-dichlorobenzenebenzyl alcohol1,2-dichlorobenzene2-methylphenolbis (2-chlorolsopropyl) ether4-methylphenolN-nltrosodi-n-propylaminehexachloroethanenitrobenzeneisophorone2-nltrophenol2,4-dlmethylphenolbenzole acidbis (2-chloroethoxy) methane2,4-dichlorophenol1,2,4- trlchlorobenzenenaphthalene4-chloroanilinehexachlorobutadlene4 • chloro - 3 • me thylphenol2-nethylnaphthalenehexachlorocyclopen tadiene2,4,6-trichloi'ophenol2,4,5-trichlorophenol2-chloronaphthalene2-nitroanilinedimethyl phthalateacenaphthylene

LLI Sample No. SV 1505038

RESULTAS RECEIVED< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.

< 1,700.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.< 330.

< 1,700.< 330.

< 1,700.< 330.< 330.


Date ReportedDate SubmittedDiscard Date

P.O. 323-BB-08Rel.

LIMIT OPQUANTITATION

330.330.330.330.330.330.330.330.330.330.330.330.330.330.330.330.

1,700.330.330.330.330.330.330.330.330.330.330.

1,700.330.

1,700.330.330.

5/ 2/903/29/906/ 2/90

LAB CODE118500000N066700000N' 118600000N067700000N118700000N092600000N067600000N092700000N066800000N092800000N118800000N

0696WOOOrt_jD069400000N**065100000N064BOOOOON092900000N066600000N064700000N118900000N069500000N093000000N069000000N119000000N093100000N069100000N065600000N093200000N067200000N093300000N068100000N065800000N

3 COPIES TO Duffield Associates, Inc. ATTNt Glenn K. Blllott1 COPY TO Data Package Group


iSiy Em"°"™™1 Reviewed and Approved byiS..Rav.rs.9ld.ForEiplsnallon Tlnothy S. Oostdyk,Of Symbol. And Abbrtvl.llon. And firnim Leader 'GC/x___ Our Standard T.rma And Condition. . Group fceaoer, (aC/

MimOfr. Amtncm Council of

> ANALYSIS REPORT

jncastcr Laboratories

LLI Sample No. SV 1505038Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vllnington DB 19808-1296 Discard Date 6/2/90


RESULT LIMIT OFTCL Serai-Volatiles (Soil) cont AS RECEIVED QUANTITATION LAB CODE3-nitroanillne < 1,700. ug/kg 1,700. . 093400000Nacenaphthene < 330. ug/kg 330. 119100000N2,4-dinitrophenol < 1,700. ug/kg 1,700. 065000000N4-nitrophenol < 1,700. ug/kg 1,700. 119200000Ndibenzofuran < 330. ug/kg 330. 093500000N2,4-dinltrotoluene < 330. ug/kg 330. 119300000N2,6-dinltrotoluene < 330. ug/kg 330. 06B400000Ndlethyl phthalate < 330. ug/kg 330. 068000000N4-chlorophenyl phenyl ether < 330. ug/kg 330. 067300000Nfluorene < 330. ug/kg 330. 068BOOOOON4-nitroanlline < 1,700. ug/kg 1,700. 093600000N2-methyl-4,6-dinltrophenol < 1,700. ug/kg 1,700. 064900000NN-nitrosodiphenylaoine < 330. ug/kg 330. 069900000N4-bromophenyl phenyl ether < 330. ug/kg 330. 067000000Nhexachldrobenzene < 330. ug/kg 330. 068900000Npentachlorophenol < 1,700. ug/kg 1,700. 119400000Nphenanthrene < 330. ug/kg 330. 070000000Nanthracene < 330. ug/kg 330. 065900000Ndi-n-butyl phthalate < 330. ug/kg 330. 068200000Nfluoranthene ' < 330. ug/kg 330. 068700000Npyrene < 330. ug/kg 330. 119500000Nbutyl benzyl phthalate < 330. ug/kg 330. 067100000N3,3'-dichlorobenzidine < 670. ug/kg 670. 067900000Nbenzo (a) anthracene < 330, ug/kg 330. 066100000Nbis (2-ethylhexyl) phthalate < 330. ug/kg 330. 066900000Nchrysene < 330. m/kg 330. 067400000Ndi.n-octyl phthalate < 330. ug/kg 330. 068500000Nbenzo (b) fluoranthene < 330, ug/kg 330. 066300000Nbenzo (K) fluoranthene < 330. ug/kg 330. 066500000Nbenzo (a) pyrene < 330. ug/kg 330. 066200000Nindeno (l,2,3.cd) pyrene < 330. ug/kg 330. 069300000Ndlbenz (a,h) anthracene < 330. ug/kg 330. 067500000Nbenzo (ghl) perylene < 330. ug/kg 330. 066400000N




'"Wwwniuooritontiino.

o, Symbol. AndAbbr.yl.tton. And ?ln°th!r S>. Oos«^ »•*•UT symoon «no flODmitiion. «w p-nnn r /tor- e/vucOur Standard Torm.,,, id Condition. GrouP "ader, CC/HS p - - .

> «.. ANALYSIS REPORTi^' \ i.ancasier Laboratories

SBLKLlLab Name: LANCASTER LABS Contract:Lab Code: LANCAS Case No.: __. SAS No.: __. SDG No.: __,Matrix: (soil/water) SOIL Lab Sample ID: 1505038Sample wt/vol: 30.0(g/mL) G Lab Pile ID: >BS602Level: (low/med) LOV Date Received: 03/29/90X Moisture: not dec. __. dec. __. Date Extracted: 04/03/90Extraction: (SepP/Cont/Sonc) SONC Date Analyzed: 04/03/90GPC Cleanup: (Y/N) N pB: __. Dilution Factor: 1.000


CAS NUMBER

1. 6258652.3. 30747134. 9214715. 44367536. 1047677.8.9.10.11. .12.13.14.15.16.17.18.19.20.21.22.23.24.25.

COMPOUND NAME

Puran, 2,5-dimethyl-1 UnknownHeptane, 2,3-dimethyl-Bexane, 2,3,4-trloethyl-3-Bexene-2,5-dlone1-Bexanol, 2 -ethyl-Unknown allcyclic compound

•

RT

4.898.318.768.96

10.9912.9834.43

BST. CONC.

700.1800.170.170.170.200.130.

QJJJJJJJ


w Aswwien lotAGCWilaiion

Respectfully SubmittedSM Rivtn* 3Wi For Explanation Lancas ter Labocatorle

656-2301

iMfi! VSIS REPORT- -\


III Sample No. SV 1505038Duffield Associates, Inc. Date Reported 5/ 2/905350 Limestone Road Date Submitted 3/29/90Vilmington DB 19808-1296 Discard Date 6/2/90


RESULT LIMIT OFTCL Pesticides AS RECEIVED QUANTITATION LAB CODEAlpha BBC < 8. ug/kg 8. 060900000NBeta BBC < 8. ug/kg 8. 0610000000Delta BBC < 8. ug/kg 8. 061200000NGamma BBC - Lindane < 8. ug/kg B. 1218DOOOONBeptachlor < 8. ug/kg 8. 121900000NAldrin < 8. ug/kg 8. 122000000NBeptachlor Epoxide < 8. ug/kg 8. 061500000NEndosulfan I < 8. ug/kg 8. 062700000NDleldrln < 16. ug/kg 16. 122200000NDOB < 16. ug/kg 16. 061600000NEndrin < 16. ug/kg 16. 122300000NEndosulfan II < 16. ug/kg 16. 062800000NDDD < 16. ug/kg 16. 061700000NEndosulfan Sulf ate < 16. ug/kg 16. 062900000NDOT < 16. ug/kg 16. 122100000NEndrin Ketone < 16. ug/kg 16. 093BOOOOONMethoxychlor < 80. ug/kg 80. 062100000NAlpha Chlordane < 80. ug/kg 80. 136100000NGamma Chlordane < 80. ug/kg 80. 136200000NToxaphene < 160. ug/kg 160. 094200000NPCB- 1016 , < 80. ug/kg 80. 063900000NPCB- 1221 < 80. ug/kg 80. 064000000NPCB- 1232 < 80. ug/kg 80. 064100000NPCB. 1242 < 80. ug/kg 80. 064200QOONPCS- 1248 < 80. ug/kg 80. 064300000NPCS- 1254 < 160. ug/kg 160. 064400000NPCB- 1260 • < 160. ug/kg 160. 064500000N

,.~. )

3 COPIES TO Duffield Associates, Inc. ATTNi Glenn K. Elliott1 COPY TO Data Package Group

MKTIW Amman Council ol


Reviewed and Approved byiSet RaverstSWt For Explanation Charles J NeslunH H Soisymbol. AndADDnviition.And unarj.es J. Hesiund,_B.&.Our SUndirdflKmi And Condition. Group Leader,

> ANALYSIS REPORT

I Lancaster Laboratories, „„..,IM2S New Holland Piko, Unc.isi'

111 s««ple No. TL 1506697Duffield Associates, Inc. u ' » c u Date Reported 5/ 7/905350 Limestone Road u__ , „ Date Submitted 4/ 4/90Vilmington DE 19808-1296 "*" W 1990 Discard Date 4/ 4/90

Tybouts Landfill Method BlankP.O. 323-BB-OBRel.

RESULT LIMIT OPANALYSIS AS RECEIVED QUANTITATION LAB CODEAluminum < 0.1 mg/l 0.1 024300000Antimony < 0.05 mg/l 0.05 024400000Barium < 0.1 mg/l 0.1 024600000Beryllium < 0.005 ng/1 0.005 024700000Cadmium < 0.005 mg/l 0.005 024900000Calcium < 0.5 og/1 0.5 025000000Chromium < 0.01 ng/1 0.01 025100000Cobalt < 0.05 mg/l 0.05 025200000Copper < 0.02 mg/l 0.02 025300000Iron 0.13 ng/1 0.05 025400000Magnesium < 0.05 mg/l 0.05 025700000Manganese ' < 0.01 mg/l 0.01 025800000Mercury < 0.0002 ng/1 0.0002 025900000(? ; ! jNickel < 0.04 ng/1 0.04 026100000Potassium < 1. mg/l 1. 026200000Silver < 0.01 ng/1 0.01 026600000Sodium < 0.5 ng/1 0.5 026700000Vanadium < 0.05 ag/1 0.05 027100000Zinc 0.02 ng/1 0.02 027200000Arsenic (furnace method) < 0.01 ng/1 0.01 104500000Lead (furnace method) < 0.005 ng/1 0.005 105500000Selenium (furnace method) < 0.005 ng/1 0.005 106400000Thallium (furnace method) < 0.01 ig/1 0.01 107300000

The above analyses were performed on an EP Toxicity leachate of thesubmitted waste prepared according to the procedure specified in

"Federal Register May 19 1980 p. 33127. " ~~A sample is considered EP Toxic if any of the contaminant concentra-tions (ng/1) in the leachate exceed the following maxima (100 times thePrimary Drinking Vater Standards)!

Arsenic 5.0, Barium 100.0, Cadmlun 1.0, Chromium 5.0, Lead 5.0,Mercury 0.2, Selenium 1.0, Silver 5.0, Endrin 0.02, Lindane 0.4,Methoxychlor 10.0, Toxaphene 0.5, 2,4-D 10.0, 2,4,5-TP 1.0.

Based on the determinations performed, the submitted sample DOBS NOTexhibit the characteristic of BP Toxicity as defined in Section 261.24Pederal Register 1980 p. 33122.


Reviewed and Approved byiSttRtvtrttSldiForExplanillon Debora K. Glffordj,-)-

MmWf AnwwnCounolol

> ' ANALYSIS REPORT

I LancasterLaboratones., ,,.„„M35rta»Hollnre»Piket Unciuslia. I'A IIW l-bl)U4

LLI Sample No. TL 1506697Duffield Associates, Inc. Date Reported 5/ 7/905350 Limestone Road Date Submitted 4/ 4/90Vllnlngton DB 19808-1296 Discard Date 4/ 4/90

Tybouts Landfill Method Blank LeachateP.O. 323-BB-08Rel.

RESULT LIMIT OPANALYSIS AS RECEIVED QUANTITATION LAB CODE1 COPY TO Duffield Associates, Inc. ATTN: Glenn K. Elllott1 COPY TO Data Package Group

Questions? Contact Environmental Respectfully SubmittedTechnical Services at (717) 656-2301 Lancaster Laboratories, Inc.044 01963 0.00 000000 Reviewed and Approved byi

Sat Raver.. Skjt For Expl.nallonj Debora

iV lDj lF/nMmwrAmiriwn Carol of

GlffarA.Sf IBsw 91,

APPENDIX D

Laboratory Data Validation Report

by

ECHEM, Inc.

JIR000895

ECHEM INCORPORATEDENGINEERING CHEMISTRY CONSULTANTS

#32 Route 35Sebago Common

North Hindham, Maine 04062(207) 892-0002

FAX (207) 892-7499

13 June 1990

Ma Deirdre SmithDPL Consultantsa/o Duffield Associates Incorporated5350 Limestone RoadWilmington, DE 19808Re: Tybouts Corner Landfill SiteLaboratory: Lancaster Laboratories IncorporatedCase Ho: 253212Volatilea: P0101, P0205, P0304, P0407, P0505.Semivolatilea: P0101, P0304.Peaticides/PCBs: P0101, P0205, P0304, P0407, P0505.

Dear Ms Smith:Validation was performed on the organic analytical data for thesoil samples referenced above. The data were evaluated based onthe following parameters:

data completenessholding timesOC/MS tuningcalibrationablankssurrogate reooverieamatrix spike/matrix spike duplicatefield duplicatesinternal standard performancecompound Identificationcompound quantitation and reported detection limitstentatively identified compoundssystem performancepesticide instrument performance

* All criteria were met for this parameter.Table I provides a summary of the validation recommendations.

Table II provides a glossary of all data qualifiers used.

AR000896

Also attached are the validation log with sample identification >wicross-reference, completeness log and sample preparation andanalysis summaries on ECHEM standard forms.BLANKS!

1. VOA.

Positive blank results and associated action levels are tabulatedbelow:BLANK ID. CASE HO. COMPOUND CONCENTRATION ACTION LEVELVBLK01 253212 Acetone 9 90

2-Butanone 1 5

VBLK02 253212 Acetone 4 40

Associated Samples:BLANK ID. CASE NO. ASSOCIATED SAMPLESVBLK01 253212 P0101

P0205P0304T0101TP101

VBLK02 253212 P0407P0505

Action:

o For sample values < CRQL, and for sample values > CRQL and< action level, the result is flagged B.

NOTE: Blank action levels were corrected for aaaoclatedsample dilution factors, where necessary, prior tovalidation qualifications.

MATRIX SPIKES:

1. SVOA.

Samples with matrix spike and/or matrix spike duplicate recoveriesoutside the criteria specified in the CLP SOW are tabulated below:

RECOVERY (%)SAMPLE DNTP0101 98/100

Action:

/IR000897

o Nona, DNT waa not detected in the sample (CRQL u), andpositive biaa ia indicated.

FIELD DUPLICATES:

Field duplicate samples were not taken for this case, thereforesampling precision could not be addressed.TENTATIVELY IDENTIFIED COMPOUNDS;

1. SVOA

With the exception of low level carboxylic acida and a phthalateeater tentatively identified in sample P0304, all TICs present inboth samples were reported at similar levels in the method- blankand are typical method contaminants. Carboxylic aoida can benaturally occurring and phthalate esters are ubiquitous and knownlaboratory/method contaminants. Ho target anal vies were found ineither sample. The TICa idantified, therefore, are probably notindicative of the presence of environmental contamination.Sincerely,ECHEM INC.

Bruce K. Hall in, PhDVice President

enc.

cc: Mr. Terrance Haelen

:J •3

/1ROQQ898

Reilon.ORGANIC REGIONAL DATA ASSESSMENT

.

CASE NO. Af32.ll

SDG m r y B 2sow- rDPO: "ACTION, .,,,_FYI

SITE Jybwh Loftto. dao**!!NO. OF SAMPLES/ -,/<• ,/ $i,Lj *J,UATPIV *3 / Qtfi r&fi/fP*"/9 t*T *

REVIEWER (IP NOT Km

REVIEWER'S NAME "ff. / «/'M

COMPLETION DATE &JV»* 111*

DATl*! ASSESSMENT SUMMARY

1. HOLDING TIMES2. GC/MS TUNE/INSTR. PERFORM.3. CALIBRATIONS4. BLANKS5. SURROGATES6, MATRIX SMKZ/DUP7. OTHER QCt. INTERNAL STANDARDS9. COMPOUND IDENTIFICATION10. SYSTEM PERFORMANCE11. OVERALL ASSESSMENT

VOA BNA PEST OTHER

o o o__G O &• ___ __0 __ 0 0 ____

o/y o • o___r m m _/O 0 0 ___0 e> C>_Q Q 0 ___g> Q _0 _ ___d ^ d0 C> o. ___

0 • Dita had no pnblemi/or qutllfled dua to minor pnblemi.M • Data qualified dua to major pnblemi.Z • Dita uDicceptabli.X • Problem!, but do Dot affect data.

ACTION ITEMS; , p(___C«

AREAS OF CONCERN; , -nf,

.

NOTABLE PERFORMANCE. __ , ,.

; ;••>S»

w

Table II

GLOSSARY. OF DATA QUALIFIER CODES (ORGANIC)

CODES RELATIHQ TO IDEHTIPICATIOH

(confidence concerning presence or absence of compounds):0 = Not detected. The aasooiated number indicatea

approximate sample concentration neceaaary to bedetected,

(NO CODE) s Confirmed identification.

B = Not detected substantially above the level reportedin laboratory or field blanks.

R 3 unreliable reault. Analyte may or may not be presentin the sample. Supporting data necesaary to confirmreault.

H a Tentative identification. Consider present . Specialmethods may be needed to confirm its presence orabsence in future sampling efforts.

CODES RELATED TO QOAHTITATIOH

(can be used for both positive results and sample quantitationlimits):

J 3 Analyte present, Reported value may not be accurateor precise,

K = Analyte present. Reported value may be biased high.Actual value ia expected to be lower.

L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.

03 = Hot detected, quantitation limit may be inaccurateor imprecise.

UL a Not detected, quantitation limit is probably higher.

OTHER CODES

Q 3 No analytical result,

4AR00090Q

DATA VALIDATION LOO

CLIENT r!iW) tf&AlP* L)uPflE_iPROJECT ID V TTS

CASE NO. DATE REC'D VALIDATION UNITSVOA SVOA INORO PEST/ PCB DIOX SAS

{msup 5"- 3- 6 %% %

NOTE: UNITS ARE DEFINED AS HATER/SOIL (e.g.,5/6) INCLUDING BLANKS

COMMENTS: SAS for this project include

Turnaround time for these caaea ia standard/fast' days(circle one)

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AR000906

1A . EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET

b Name: LANCASTER LABS______ Contract:POlOl

•/S-LI-/.I

Lab Code: LANCAS Case No.: 263212 SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) SQIL_ Lab Sample ID: C1SOS027I.sample wt/vol: s.Q (g/mL) s_ Lab File ID: cisoso27LLevel: (low/med) LOW ._ Date Received: 03/29/90t Moisture: not dec, _19. Date Analyzed: 04/04/91}Column: (pack/cap) PACK._, Dilution Factor:

CONCENTRATION UNITS:CAS NO, COMPOUND (ug/L or ug/Kg) US/KG

74-87-3--——~Chloromethane_74-83-9--———-Bromomethane_75-01-4————Vinyl Chloride,75-00-3——'—Chloroethane75-09-2————Methylene chloride67-64-1—————Acetona_75-15-0—————Carbon Disulfide________75-35-4—————l,l-Dichloroethene______75-34-3—————1,1-Dichloroethane______540-59-0————1,2-Dichloroethene (total)_67-66-3————chloroform107-06-2————l,2-Dichloroethane_78-93-3———- -2-Butanone_____~71-55-6—————1,1, l-Trichloroethane_56-23-5————Carbon Tetrachlorida108-05-4————Vinyl Acetate______7S-27-4-———Bromodiohloromethana78-87-5———1,2-Dichloropropana__10061-01-5———cis-1,3-Dichloropropena_79-01-6———'Trichloroethene_____"124-48-1——•—Dibromochloromethane__79-00-5—————l, l, 2-Trichloroethane_71-43-2————'Benzene,____ _________10061-02-6———'trans-l,3-Dichloropropene_75-25-2————Bromoform108-10-1————4-Methyl-2?Pentanone___591-78-6————2-Hexanone__________127-18-4————Tetrachloroethene_____79-34-5—————l,l,2,2-Tetrachloroethane_108-88-3————Toluene108-90-7————-Chlorobenzene_100-41-4———'Ethvlbenzane100-42-5————Styrene____1330-20-7————Xylene (total)

1212121221266666612661266666666612126666666

UUUUJBJUUUUUUUUUUUUUUUUuuuuuuuuuuuu

I2.&

FORM I VOA

IE EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Name: LANCASTER LABS ______ contract: ______ _______ ,Si

P0101

Lab code: LANCAS case No.: 2S1212, SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) 3piL Lab Sample ID: C1SOS027LSample wt/vol: S . Q (g/mL) 5 _ Lab File ID: C1SOS027LLevel: (low/med) &pw Date Received: 03/29/90t Moisture: not dec. _ 12 Date Analyzed: 04/04/90Column (pack/cap) PftCK Dilution Factor: i.o

CONCENTRATION UNITS:Number Ties found: _ Q, (ug/L or ug/Kg) us/*;q

CAS NUMBER COMPOUND NAME RT•nova..'!.***'

EST. CONC.•••••••••••an

Q

FORM I VOA-TIC 1/87 Rev.

HR000908

IA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________

b Name: LANCASTER LABS______ contract:P0205. IH !_'••/

' Lab Code: LANCAS case No.: 253212 SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: Q1S05033CSample wt/vol: 5.0 (g/mL) S__ Lab File ID: C1SOS033L

Level: (low/raed) LOW Date Received: 03/29/90* Moisture: not dec. 17 Date Analyzed: Q4/04/9QColumn: (pack/cap) PACK Dilution Factor: l.Q

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3————'Chloromethane_74-83-9—————'Broraoraethane75-01-4—————Vinyl Chloride___75-00-3—-——-Chloroethane______75-09-2—————Methylene chloride,,67-64-1—————Acetone______"75-15-0—————Carbon Disulflde_75-35-4—————1,1-Dichloroethene75-34-3—————1,1-Dichloroethane______540-59-0————1,2-Dichloroethene (total)_67-66-3—————Chloroform107-06-2————•l,2-Dichloroethane_78-93-3-————'2-Butanone71-55-6-————•1,1,1-Trichloroethane56-23-5—————Carbon Tetrachloride_7108-05-4————Vinyl Acetate75-27-4—————Bromodichloromethane78-87-5—————1,2-Dichloropropane____10061-01-5———'Cis-1,3-Dichloropropene79-01-6————"Trichloroethene______124-48-1————Dibromochloromethane79-00-5—————1,1,2-Trichloroethane___71-43-2-————Benzene____________10061-02-6——trans-l,3-Dichloropropene_75-25-2———'—Broraoform108-10-1————4-Methyl-2-Pentanone_591-78-6————2-Hexanone___________127-18-4————Tetrachloroethene_____79-34-5—————1,1,2,2-Tetrachloroethane_108-88-3——'—Toluene108-90-7-———Chlorobenzene_100-41-4————Ethvlbenzene100-42-5————'Styrene_____1330-20-7————Xylene (total).

1212121252566666612661266666666612126666666

FORM I VOA ..„......_..„31

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________TENTATIVELY IDENTIFIED COMPOUNDS

uab Name: LANCASTER LABS______ contract:P0205

Lab Code: LANCAS Case No.: 253212 SAS No.: ____ SDG No.: TYB2•'*,Matrix: (soil/water) SOIL Lab Sample ID: C1S05033LSample wt/vol: s.o (g/mL) S_ Lab File ID: C1SOS033LLevel: (low/med) LOW Date Received: 03/29/90t Moisture: not dec. _IX Date Analyzed: 04/04/90Column (pack/cap) PACK L Dilution Factor:

CONCENTRATION UNITS:Number Ties found: _a (ug/L or ug/Kg) UG/KG

CAS NUMBERH B • BJI • ••• tV HM M • H aW>l

COMPOUND NAME«Baa.iaBBasaa«H«a»aaaanBEisaassi

RTsanaaBasiH

EST. CONC.•aamBnBBBKBBB

Q

FORM I VOA-TIC

IA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________

Name: LANCASTER LABS______ contract:P0304

..ab Code: LANCAS Case No.: 253212 SAS No.: ____ SDG No.: TYB2'*,latrix: (soil/water) SOIL , Lab Sample ID: cisoSQ34LSample wt/vol: 5.0 (g/mL) S_ Lab File ID: cisoso34i.,evel: (low/med) LOW , Date Received: 03/29/90* Moisture: not dec. _11 Date Analyzed: 04/04/90Joluran: (pack/cap) PACK , , Dilution Factor: i.o

CONCENTRATION UNITS:GAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3————-Chloromethane_________74-83-9-—————'Bromomethane________75-01-4—————Vinyl Chloride_______75-00-3—————Chloroethane __________75-09-2—————Methylene Chloride67-64-1—————Acetone____________75-15-0—————Carbon Disulfide______75-35-4—————1,1-Dichloroethene_____75-34-3—————1,1-Dichloroethane_____540-59-0————1,2-Dichloroethene (total)67-66-3—————chloroform107-06-2————'1,2-Dichloroethane____78-93-3———-2-Butanona_________71-55-6—————1,1,1-Trichloroethane56-23-5——•——Carbon Tetrachloride___108-05-4————Vinyl Acetate_______75-27-4————Bromodichloromethane___78-87-5-————1,2-Dichloropropane____10061-01-5———cis-l,3-Dichloropropene_79-01-6——•——'Trichloroethene______124-48-1————Dibromochloromethane___79-00-5—————1,1,2-Trichloroethane__71-43-2————'Benzene____________10061-02-6-——-trans-l,3-Dichloropropene_75-25-2————-Broraoform108-10-1————4-Methyl-2-Pentanone591-78-6—————2-Hexanone______127-18-4————Tetrachloroethene79-34-5—————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene___________"108-90-7———'Chlorobenzene_100-41-4————-Ethylbenzene_100-42-5————Styrene____1330-20-7————Xylene (total).

1111111142866666611661166666666611116666666

FORM I VOA


Lab Name: LANCASTER LABS______ Contract:P0304

Lab Code: LANCAS, Case No.: 2.5,3213 SAS No.: ____ SDG Ho.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: cisoso34LSample wt/vol: s.o (g/mL) S_ Lab File ID: C1SOS034LLevel: (low/raed) LOW Date Received: 03/29/90* Moisture: not dec. _U Date Analyzed: 04/04/90Column (pack/cap) PACK Dilution Factor: i.o

CONCENTRATION UNITS:Number Tics found: _a (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAMEasaBaaaaaaaBBHttaataaaBBaBBasiSB]

RTBBBKEBaa.

EST. CONC.BBBBBBaBBatfsVB

gBBBBSI

OFORM I VOA-TIC fl#&0&9.| 2

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET __________

Name: LANCASTER LABS______ contract:P0407

v ;••'.». •''Lab code: LANCAS^ case No.: 2S3212 SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: C1505036LSSample wt/vol: 5.0 (g/mL) G_ Lab File ID: C1SOS036LS

Level: (low/med) J_JH__ Data Received: 03/29/90

t Moisture: not dec. _15 Date Analyzed: 04/05/90Column: (pack/cap) PACK Dilution Factor: i.Q

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/Kq Q

•j

74-87-3-——-—'Chloromethane_74-83-9-—'——'Bromomethane75-01-4—————Vinyl Chloride,75-00-3—-'——Chloroethane75-09-2—————Methylene Chloride67-64-1—————Acetone_______75-15-0—————Carbon Disulfide______75-35-4—————1,1-Dichloroethene_____75-34-3—————1,1-Dichloroethane_____540-59-0————1,2-Dichloroethene (total).67-66-3—————Chlorofona107-06-2————1,2-Dichloroethane__78-93-3———2-Butanone_______71-55-6—————l,l,l-Trichloroethane_56-23-5————-Carbon Tetrachloride_108-05-4————Vinyl Acetate_____75-27-4—————Broraodichloromethane_78-87-5—————-1,2-Dichloropropane10061-01-5———cis-l,3-Dichloropropene79-01-6—————Trichloroethene_____124-48-1————Dibromochlororaethane__79-00-5—————1,1,2-Trichloroethane_71-43-2—————Benzene___________10061-02-6-———trans-l,3-Dichloropropene_75-25-2—————Broraoform108-10-1————4-Methyl-2-pentanone_591-78-6————2-Hexanone__________127-18-4———'Tetrachloroethene_____79-34-5——»——'1,1,2,2-Tetrachloroethane_108-88-3————Toluene___________108-90-7—•———Chlorobenzene_100-41-4————'Ethylbenzene_100-42-5————Styrene____1330-20-7————Xylene (total)

1212121231366666612661266666666612126666666

FORM I 0009 | 3 1/87 Rev.

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___________TENTATIVELY IDENTIFIED COMPOUNDS

_ub Name: LANCASTER LABS______ contract:P0407

"si;,.' Lab Code: LANCAS Case No.: 253212 SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: C1505036LSSample wt/vol: S.O, (g/raL) S_, Lab File ID: C1SOS036L3

Level: (low/med) LOW Date Received: 03/29/90t Moisture: not dec. _l£ Date Analyzed: Q4/OS/90column (pack/cap) PACK Dilution Factor: i.o

CONCENTRATION UNITS:Number TICs found: __a (ug/L or ug/Kg) US/KG

CAS NUMBER COMPOUND NAMEBBBBBBBBaaaaBCSSBBaaBBSSaBBBa

RTBasaaaan

EST. CONC. Q

FORM I VQft ' 1/87 Rev.ftjflf0Q09|lj

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___________

:b Name: LANCASTER LABS______ contract:P0505

Lab Code: I NCAS Case No.: 2S3212 SAS No.: ____ SDG No.: TYB2

Matrix: (soil/water) SOIL Lab Sample ID: C150S037LRsample wt/vol: s.q (g/mL) S_ Lab File ID: C1505037LRLevel: (low/med) LOW Date Received: 03/29/90t Moisture: not dec. _2i Date Analyzed: 04/05/90Column: (pack/cap) .PACK Dilution Factor: i.o

CONCENTRATION UNITS:CAS NO. COMPOUND (Ug/L or ug/Kg) UG/KG. Q

74-87-3————Chloromethane_74-83-9————-Bromomethane_75-01-4—————Vinyl Chloride,75-00-3——-—-Chloroethane75-09-2—————Methylene chloride,67-64-1—————-Acetone______~75-15-0—————Carbon Disulfide_75-35-4—————1,1-Dichloroethene75-34-3—————l,l-Dichloroethane~_______540-59-0————1,2-Dichloroethene (total)_67-66-3—————Chloroform________107-06-2———1,2-Dichloroethane__78-93-3—————2-Butanone_______71-55-6————-1,1, l-Trichloroethane_56-23-5——"——Carbon Tetrachloride_108-05-4—————Vinyl Acetate75-27-4—————Bromodichloromethane_78-87-5—————'l,2-Dichloropropane_10061-01-5———'Cis-l,3-Dichloropropene___79-01-6—————Trichloroethene______124-48-1'——'—Dibromochloromethane___79-00-5—————1.1.2-Trichloroethane71-43-2————Benzene_____________10061-02-6—•—trans-l,3-Dichloropropene_75-25-2—————Bromoform__________"108-10-1—————4-Methyl-2-Pentanone___591-78-6—————2-Hexanone__________127-18-4—————Tetrachloroethene_____79-34-5'——•——'1,1,2,2-Tetrachloroethane_108-88-3————'Toluene___________~108-90-7————Chlorobenzane_______100-41-4————-Ethylbenzene________100-42-5————styrene_1330-20-7————Xylene (total).

1313131371366666613661366666666613136666666

UUUU

B/UUUUUUUUUUuuuuuuuuuuuuuuuuuu

FORM I VOA /1ROOQ9I5 V87 Rev.


Lab Name: LANCASTER LABS______ Contract:P0505

•Lab Code: LANCAS case No.: 253212 SAS No.: ____. SDG No.: TYB2 ._' T»

Matrix: (soil/water) SOIL Lab Sample ID: cisoso37LRSample wt/vol: 5.0 (g/mL) S_ Lab File ID: cisoso37LRLevel: (low/med) LOW Date Received: 03/29/90* Moisture: not dec. _21 Date Analyzed: 04/05/90Column (pack/cap) PACK . Dilution Factor: i.o

CONCENTRATION UNITS:Number TICs found: 0 (ug/L or ug/Kg) UG/Kq

GAS NUMBER COMPOUND NAME RT EST. CONC. P.

e

«;.

FORM I VOA-TIC l / 8 7 H U U '•> ' «

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______

• .b Name: LANCASTER LABS______ contract:VBLKOl

lab Code: IANCAS_ case No.: 2S32\% SAS No.: ____ SDG No.: TYB2«,Matrix: (soil/water) SOIL Lab Sample ID: C1SOS038LSample wt/vol: 5.0 (g/mL) S_ Lab File ID: CISOSOSBLLevel: (low/raed) LOW Date Received: 03/29/9Q

t Moisture: not dec. __ Date Analyzed: 04/04/9Qcolumn: (pack/cap) PACK Dilution Factor: i. o

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/Kg Q

74-87-3———-chloromethane___74-83-9————Bromomethane____75-01-4—————Vinyl Chloride__75-00-3-—•-—-Chloroethane____;75-09-2—————Methylene chloride67-64-1—————Acetone_________~_75-15-0—————Carbon Disulfide_75-35-4—————1,1-Dichloroethene75-34-3—————1,1-Dichloroethane"540-59-0————1,2-Dichloroethene (total).67-66-3—————Chloroform107-06-2————1,2-Dichloroethane_78-93-3—————'2-Butanone71-55-6—————l,l,l-Trichloroethane_56-23-5-———-Carbon Tetrachloride_^108-05-4————Vinyl Acetate75-27-4—•——-Bromodichloromethane___78-87-5————'-1,2-Dichloropropane____10061-01-5——-cis-l,3-Dichloropropene_79-01-6—————Trichloroethene______124-48-1———'Dibromochloromethane___79-00-5————'1,1,2-Tr ichloroethane___71-43-2—————Benzene _________10061-02-6———trans-l,3-Dichloropropene_75-25-2'—-——'Broraoform108-10-1————4-Methyl-2-Pentanone_591-78-6————2-Hexanone127-18-4————Tetrachloroethene_____79-34-5—————1,1,2,2-Tetrachloroethane_108-88-3————'Toluene___________"108-90-7-————Chlorobenzene________

• 100-41-4-————Ethylbenzene________100-42-5————'Styrene___________1330-20-7————Xylene (total)_______

10101010595555551551055555555510105555555

FORM I VOA 1/87

IE EPA SAMPLE NOVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

tab Name: LANCASTER LABS______ Contract:VBLK01

Lab Code: LANCAS case No.: 253212 SAS No.: ____ SDG No.: TYB2••'*,Matrix: (soil/water) SOIL Lab Sample ID: cisoso38LSample wt/vol: S.O (g/mL) S_ Lab File ID: C1SOS038L

Level: (low/med) LOW Date Received: 03/29/90

t Moisture: not dec. __ Date Analyzed: 04/04/90column (pack/cap) PACK Dilution Factor: i.o

CONCENTRATION UNITS:Number Ties found: .___ (ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC fl ROD Od^Rev.I2,f

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ___________TENTATIVELY IDENTIFIED COMPOUNDS

b Name: LANCASTER LABS______ Contract:VBLK02

'iab Coda: .LANCAS , Case No.: 353212 SAS No.: ____ SDG No.: TYB2latrix: (soil/water) SOIL Lab Sample ID: CBLKAPSSample wt/vol: S.Q (g/mL) S_ Lab File ID: CBLKAPSvel: (low/med) LOW Date Received: 03/29/90

* Moisture: not dec. __ Date Analyzed: 04/05/90

Column (pack/cap) PACK Dilution Factor: l.o

CONCENTRATION UNITS:Number TICs found: ___ (ug/L or ug/Kg) _S/£S.

CAS NUMBER COMPOUND NAME RT EST. CONC. Q

,JFORM I VOA-TIC ft R 000 .M*? ReV< ,33

1A EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _________.

Lab Name: LANCASTER LABS______ Contract:Lab code: LANCAS Case No.: 253212 SAS No.: ____ SDG No.: TYB2

•'«,Matrix: (soil/water) SOIL Lab Sample ID: C1S05028LMSample wt/vol: s.o (g/raL) S_ Lab File ID: C1505028LMLevel: (low/med) LOW Date Received: 03/29/90

t Moisture: not dec. _12 Date Analyzed: 04/04/90.oluran: (pack/cap) PACK , Dilution Factor: i.o

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q

74-87-3—————Chlororaethane__74-83-9—'--——'Broraomethane_75-01-4—————Vinyl Chloride.75-00-3————-Chloroethana75-09-2—————Methylene Chloride_____67-64-1————Acetone____________75-15-0—————Carbon Disulfide______75-35-4—————1,1-Dichloroethene_____75-34-3—————1,1-Dichloroethane_____540-59-0————1,2-Dichloroethene (total).67-66-3—————Chloroform_________'_107-06-2————1,2-Dichloroethane_____78-93-3———'2-Butanone71-55-6—————1,1, l-Trichloroethane_56-23-5————Carbon TetrachlorideJ]108-05-4————Vinyl Acetate_75-27-4————'Broraodichloromethane__78-87-5——— 1,2-Dichloropropane__10061-01-5-——'cis-1,3-Dichloropropene_79-01-6-——-—Trichloroethene______124-48-1———Dibromochloromethane.___79-00-5————1, l, 2-Trichloroethane_71-43-2—---—'Benzene________"10061-02-6'——-trans-l,3-Dichloropropene_75-25-2'————Bromoform108-10-1————4-Methyl-2-Pentanone___591-78-6-——•—2-Hexanone__________127-18-4————Tetrachloroethene_____79-34-5—————l,l,2,2-Tetrachloroethane_108-88-3—-——Toluene,_________________108-90-7————Chlorobenzene ______,100-41-4————'Ethylbenzene________100-42-5————Styrene_____________1330-20-7————Xylene (total)_______

121212129216666662661266666666612126666666

UUUUUUBJUUUUUuuuuuuuuuuuuuuuu

FORM I VI&R00092Q 1/87 Rev.

IK ' EF'R SHWLE HU,SETMyULfVIILE CINGflNttS flNIILY.lS Ufirn SHEET ________

I I

Lab Name' LIINCflSTER LOBS Contract i ___ . | __________ ,|

l.ab Lodei LflNCflS , Case No," ___ , SflS No.i ___ , SOG No.i ___ ,

Matrix! (soil/water) SUIL Lab Sample I CM 1S0502/

Sample u t / u o l i 30,0(gAiiL) U Lab M le IU' >E5i5Q3

Leueli (low/rued I LOU Date Reoeluedi O.V29/70

X nolsture" not dec. 19,0 dec, ___ , Date Extraotedi 04/O.VVO

blxtractloni (SepF/Cont/Sonc) SUNC uate final yjedi 04/U.V9U

GPC Cleanup" (Y/N) N pHi 5.51 D i l u t i o n Factor* 1.000

UNil'SiNumber TIC* found! 5 ( ug/L or ug/Kg) Uli/KG

CHS NUMBER

'i.j ,4, 4436753S.6.? .B,','..10.11.\'i.13,14.15.16,17,IB.19.iJU,2.1,;> 2,.3.24..25,

CUMF'CIUNII NflME

Furan, 2,5-d Imethy 1-2-Pentene, 3,4-dlmethyl-,UnknownS-Hexene-Uif-rf loneUnknown a 1 (cyclic liydrccarbo

•

,

,„, ,

.„ , , „„.

Rf

4,907,218,32

11,0134,45

'

-

EST, CONC.

700,160.

2100,290,330.

N

JBJlJBJBJ«

"

.

"1" r I'soiner afFiiK'ii i sy-nc i/a/

flR00092

1C KF'fl !iHI1l'LK Ml),.t (JKGflNiCS HNflLYSlS Ufllfl SHEET __________ ,

I "lI P0101UJ! |

Lab Namei LflNCHSTER LflBS Contract" ___, |__________|

Lab Code" LflNCflS, Case No,' ___. SflS No," ___. SOB No," ___

Clatrlx" (scll/uater) SOIL Lab liampli* ID" 15050X7•'*,

Sample wt/ucl" 30,0(g/inL) G Lab F i l e ID" H5M>3

(low/med) LOW Date Receiucdi 03729/90

'/. Moisture' not'dec, 19,0 dec, ___. Date Extracted" 04/03790

Extraction' (SepF/Cont/Sonc) SUNC Date analysed" 04703/90

BMC Cleanup" (Y/N) N pH" 5.51 0 Hut Inn Factor" 1,000

i:UN-ENIRflT.CON UNITS*CMS Nl), COMPOUND (iig/L or ug/Kg) UG/KG q

3-NICroanl lineH3-32-9 ————— flcenaphtherifi

2,4-IMnltrophRnol100-02-7 —— — 4-Nltrophenol132-64-9 ——— - Dlben.ofurfln121-14-2 ———— 2,4-Olnltrntolnene_H4-66-2 ————— Olethylphthalat:s_700S-72-3 ——— - 4-Chloroph(?nyl-phnriy Inther_H6-73-7-- — — Muorene______________100-01-6 ——— - 4-Nltroanlllri(?__________534-SZ-l———— 4,6-Olnltro-Z--methvlph_nol_H6-30-6 —— -— N-Nltroso.llphenylamlne (!)__101-55-3------- 4-BromophenyI-phenylether_,118"74-1 ------- Hftxach lorobensene_______,07-06-5-------- f'antach loropheno I_______,U5-01-8————— Phenan throne___________120-12-7———— flnthracene_____________H4-74-2————— Ol-n-butylphthalate_206-44-0—-— Fluoranthene_____129-00-0———— Pyrene_8S-68-7 ————— Butylbe)riRvlphthalate

3,3'-Olchloroben.ldlne_56-55-3-------- B(!n2o(a)anthracene,21U-01-9 ———— Chrynene117-B4-0 ———— l)!"n-octylphthalote_205-99-2 ———— Senao(b)f liionirithr.'nR207-0(1-9--- —— tipnaoikjf Uioranthene

B(?nsij(a)pyrenis193-39-5 — ---•• lnd(-no(l,2,3-cd)pyrene_53-70-3 —— - — Dlbensla.hjanthracirnff^191-24-2 — —— Benso(g,h, I Jpery lene__

2100410

2100410410410410410

21002100410410410

21004104104104(041041082041041041041041041041041041U

1) - Cannot he separated from UIphenylam Ine

FUKtl J SV--Z J/EI7

AROQ0922 167

,|j Itl •SEM1UOLHIILE UKGHN1CS HllflLYSlS UllCfl SHtEl

Lab Name" LdNCflSTER LflBS Contract" ___.

Code" LUNCflS Case No," ___, SMS No,' ___, SDG No,"

•"' Hatrlx" (foil/water) SUIL Lab Sample 10" 1505UX7

'*• Sample wt7uol" 30,0(g/mL) G Lab F i l e lUi >_S603

LeueM (low/rued) LOU Date Received" 03729/90

V. Moisture" not dec, 19.0 dec, ___. Oate Extracted' 04/03/90

Extraction' (SepF/Cont/Sonc) SUNC Oate Analysed' 04/03/90

BPC Cleanup" (Y/N) N pH" 5.51 D i l u t i o n Factor" 1,000

CONCENTRATION UNITS'CHS NU, COMPOUND (ug/L or ug/Kg) UG/KG Q

108-95-2———— Phenol____________111-44-4———— bis(2-Chloroethy1)ether_95-57-H————— 2-Chlorophenol.541-73-1———— l,3-Dichlorob«nsene._106-46-7——— l,4-Ulch1arob«?naene_100-51-6———— Bensyl alcnhol95-50-1———--- 1.2-Ulchlorobenzene,.95-48-7————— t -Me thy I phono I.108-60-1-——— bls(2-L'hlorolj,opropyl)ether_106-44-5———— 4-riethy I phenol_________621-64-7------- N-Nltroso-dl-n-propy lamlne_67-72-1- — ---- Hexach loroethane________,98-95-3————-- Nitrobenzene___________78-59-1-------- Isophorone____________.88-75-5————— 2-Nltrophenol__________105-67-9———— 2,4-Dlmethyl phenol______.65-85-0————— Bensolc acid___________111-91-1———— bl*(2-Chloroethoxy)methane_120-83-2———— 2.4-Ulchlorophenol_______120-82-1——•— 1,2,4-Trlchlorobensene____91-20-3———— Naphthalene___________106-47-8-———— 4-Chloroanl I Ine_________87-68-3————— Hexach lorobutadlene______59-50-7————— 4-Chloro-3-methylphenol___91-57-6————- 2-l1ethy I naphthalene77-47-4-------- Hexach 1 orocycl open tad Iene__,88-06-2———— 2,4,6-Tr Ichloropheno I____95-95-4————— 2,4,5-rrlchlorophenol______91-1)8-7———•— 2-Chloronaphthalehe______88-74-4————— 2-Nltroanlllne_________131-11-3———— U Imethy Iphthalate_______208-96-9-- •—— flcenaphthy lene_________606-20-2———— 2,6-Olnltrotoluene_______

41041041041041041041041041041041041041041041041,02100410410410410410410410410410410

21004102100410410410

FORM 1 SV-1 1/B7 Row

flRQ00923 '-

l> KPA liflWLk HIJ,8EH1VUI.HI ILL UlUiANlCS IUIAI.YKIS Ulllfl BIIEU ___________.

I I| P030'4 |

Lob Nrtine' LANCASTER LABS ContMoti ___. |_________^J

Lab Codpi LflNCflS i Case No.i ___, BUS No , i ___, SDG No,' ___, 'i£J,-''

, Matrix! (TO I I/water) SOIL Lab Sample 10' IB05034'IS

Sample nt/uol" 30, 0(g/ml.) G Lab F i l e ID' J

Lf3i/Hl" (log/died) I.UH Date Received" 03/29/91)

K Moisture" not dec, 11.0 dec, ___. Date Extracted" 04/03/90

Extraction" (SepF/Cont/Sonr.) SONC Date Analyzed! 04/03/90

GF'C Cleanup" (Y/N) N pll" S.82 D i l u t i o n Factor" 1,000

aiNCKNIRIUIDN UNIPli"Number PICs found" 9 (ug/l. or ug/Kij) UG/KG

CDS NUMtlEK

1. 625H652. 2216300j.4, 30/4713S .6.7.H.9,

10.1 1 .12.H.14,IB.16,17,1H,19,20.21.22,23,24.KB.

COMPOUND NflME

Furnn, 2,5-dlmethy 1-Heptane, 2,5-dlmethy 1-UnknownHexane, ?., 3-dlmRthy 1-Unknaun a l i p h a t i c hydronarhoUnknown aromaticUnknown carbnxylic acidUnknown phthalate e*ter .Unknown carboxylic acid aste

R1

4,888.20B.308,7.00.98

10,9915,5624,0328.06„ ,.

,_.. ,.,.,

_,.,.,,„,„„.„ „

..... , , ,

ESI, CONC.

•M.150.r/oo,190,190.860,230,530,1 9'J ,

,

,.,

M

JMJJLX>m,)i,JF1.1 1JJ

FORM 1 Sy-flC 1/H7 Keu.

flftOQO_2l» 182

I1C FiPfl SIlhPLK MIJ.

SEMlVOLflllLt Uli'tiflNH'B ANALYSIS 1)111 A Sllt.ET ___________II POJ04 I

Lab Namei LANCASTER LAFIS Contraoti ___, I__________

. - l i b Code' LANCAS, Case No.' ___, SflS No.i ___, SUU Mo," ___,

Matrix' (soil/water) SU1I. Lob Sample ID" 1505034•i

Jiarnple wt7uoli 30,0(g/rdL) G l.ab Hie IDi >K560<5

Loufjl" (low/ined) LUH Date Rnceivedi 03729/90

't, llotftture" not dec. 11,0 disc, ___, Date Extracted! 04/03790

Extraction! (SepF/Cont/Sonc) SUNC Date Analyzed! 04/03/90

UPC Cleanup" (Y7N) N pH' 5.82 Dilut i o n Factor' 0,000

CUNCKNCRflTlUN UNITS"CAM NU. CunPOUNO (ug/l. or ug7Kg) IJI5/KG " Q

99-09-2--- — -•• 3-Nltroanl I lne_83-32-9————— Acenaphthenr?.51-28-5---—-- 2,4-Ulnltrophenol_100-02-7———— 4-Mltrophenol____132-64-9—---- Olbenzofuran,______121-14-2———— 2,4-Oln.ltrotoluene_84-66-2 ———— -- Dlethylphthnlate.700B-72-3- —— - 4-Chlori)phnny 1 -pheny lather.86-73-7 — --••••- FUiore!ne_______________100-01-6--——— 4-NltroaniIln<?_________534-52-1------- 4,6-Din Itro-2-methyIpheno I_IIA-30-6————-- N-Nltro'Sodlphenylanilne (t)_101-55-3———— 4-llromophenyl-phenylether__U8-74-1------- Hexachlorobnnnene___87-86-5————-- F'Rntachlorophenol____85-01-8————— Phenanthrenr_______120-12-7———— Anthracene————————84-74-2————— DI-n-buty I phthalate__206-44-0———— F luoranthene_________129-00-0———— Pyrene___________85-68-7————— Butyl benzyl phthalate_91-94-1————— 3,3'-Olchlorobenzldlne_56-55-3————— Benzol fl Jan thracerie___2111-01-9———— ChrysHntf,1.17-84-0———— DI-n-octy I phthalate__205-99-2———— flenzo(b) fluoranthene_207-OB-9-- —— - BenzojkjfUioran'fchene—50-if 2-8————— FjRnso(a)pyrerif?________193-39-ii———— 1 ndeno(l, 2,3-cd) pyrene,53-70-3———•— Qlb«!nz(a|h)anthracisne_191-24-2--- — - FJpnzotg.h, Dperylene—

1900380

190019003BO3803 CIO3803PO190019003UO3 BO:!i:io

19003UO35103803 £103803BO7503HO3803803803803003BO380380

(1) - Cannot be separated from DlpheriyInmlne

FIIRM 1 SV-2 1/B7 Hev

181flROQ0925

IB EF'fl SllMPLE IIM.UMANICS ANALYSIS D A I A SHEEI ______.

I lI I'D ;)04

108-95-2-——— Phenol____________111-44-4———— bls(2-Chloroethyl)ether_95-57-8————— 2-Chlorophenol.541-73-1———— l,3-0lchlorobenzene_106-46-7 —— — 1.4-Dlchlorobenzene_100-51-6--——— Benzyl alcohol____95-50-1---——— l,2-Dlchlorobenzene_95-48-7————— 2-Methylphenol.108-60-1------- bls(2-ChlorolsopropyI)ether_106-44-5-——— 4-Methy Iphonol__________621-64-7------- N-NI troso-d l-n-propy larnlne_(57-72-1-------- llraxach I or on thane________,98-95-3————— Nitrobenzene___________78-59-1 — ----- Isophorone____________88-75-5————— 2-Nltrnphenol__________105-67-9———— 2,4-Olmethy I phenol______65-85-0————— tlensolc acid___________111-91-1--——— bls(2-Chlorosthoxy)methane__120-83-2———— 2,4-Dlchlorophenol120-82-1———— l,2,4-Trlchlorobenzene_91-20-3————— Naphthalene.106-47-8——— 4-Chloroanl I Ine______87-68-3-----— HexachIorobutadlene59-50-7————— 4-Chlora-3-rnethylphenol.91-57-6—--— 2-Methylnaphthalene.77-47-4-----— Hexachlorocyclopentadlene_88-06-2————— 2.4.6-Trlohlorophenol95-95-4————— 2.4.5-Trtchlorophenol91-58-7-------- 2-Chloronaphthalene____88-74-4——•--- 2-NIt roan 11Ine____________131-11-3—-— Olnwthylphthalate______208-96-8———— Acenaphthylene________606-20-2———— 2,6-0 In I tro toluene_____

3803803803803803130380380380380380380380380380380

1900313038038038038038038038U38038019003801900380380380

Lab Name" LANCASTER LABS Contract' ___, I ^->---. ,..,|

Lab Code" LANCAS Case No." ___, SAS No," ___, BUG No , s ___,

'•'*<ri.itrlxi (soil/water) SOIL Lab Sample 10" 1505034

Sample Ht/vol" 30,Olg/mL) G Lab F i l e IDi >E!!.fi'Ji5

LeveM (low/med) LOU Date Received" 03/29790

'.'. Moisture" not dec, 11,0 dec, .___, Date Extracted" 04/OV90

Extraction" (SepF/Cont/Sonc) SUNC Oate Analyzed" 04/03/90

Gh'C Cleanup" (Y/N) N pll< 5.B2 Dilution Factor' 0.000

CIJNCENTRATIUN UNITS"CHS NU, CUMPDUMD (ug/L or ug/Kg) UG/KG I)

FORM I SV-1 flROQ0926

lf; EPH SAMPLE MIJ,SEM1VULAI1LE UKGAN1CS ANALYSIS Ofl'IH SHEET _______

I . II iiHLKll |

'~\_b Maine" LANCASTER LABS Contract" ___. |__________|

. ' Lab CoJe' LANCAS ' Case Ho.i ___, BUS No." ___, SDG Ho." ___,

•'«, Matrix' (soil/water) SOIL Lab Sample ID' 1505038

Sample wt/vol' 30,0(g/mL| G Lab F i l e ID' >fc',i602

Level" (Iou7med) LUU Date Received" 03729/90

'/, Moisture" not dec, ___, dec, ___. Date Extracted' 04/03/90

Extraction" (SepF/Cont/Sonc) SDNC Date Analyzed" 04/03/90

GPC Cleanup" (Y/N) N pH" ___, D i l u t i o n Factor' 1,000

CONCENTRATION UNITS"Number TICs found" 7 (ug/L or ug/Kg) UG/KG

CflS NUMBER

1, 6258652,3, 30747134, 921471S, 44367536. 1047677.B.9.

10,11,12.13.14.15.16,17.18,19.20.21.22.23.24,25.

1| COMPOUND NAME

IFuran, 2,5-dlmethy 1-UnknownHeptane, 2,3-dlmethy 1 -Hexane, 2,3,4-trlmethy 1-3-Hexene-2,5-dlone1-Hexanol, 2-ethyl-Unknoun a l l c y c l l c compound

. .... , , , ., „ ,

RT

4,898,318,768.9610,9912,9834.43

ES!', CQNC.

700,1800,170,170,170,200,130,

.

Q

JJJJ,'JJ,J

.

FORM 1 SV-T1C 1/87 Rev,

flR000927 "" 236

1C EPA 3W1PI.I- NU,SEMiyDLATILE ORGAN1CS ANALYSIS DAIA SHEfcl ___________,

I II SBI.KI.1 |

' ab Name" LANCASTER LABS Contract' ___. |__________|

99-09-2————— 3-Nltroanll Ine.H3-32-9————— Acenaphthene.SI-28-5————— 2,4-Dlnltrophenol_100-02-7 — -— 4-Nltrophenol____132-64-9———— Dlbenzofuran____121-14-2———— 2,4-DlnltroColiierie_B4-66-2————— I) I ethyl phthalate.7005-72-3——— 4-Chlorophenyl-phenylether.H6-73-7————— F'luorenei_____________100-01-6———— 4-Nltro.ifilllne_________534-52-1———— 4,6-l)lnltro-2-methylphenol.86-30-6————— N-Nltrosoillphenylarnlne (l)_101-55-3------- 4-Bron>opheny'l-pheny let her__,lit)-74-1 — ---- Hexach 1 orobenzene______H7-86-5-------- Pentachlorophenol______U5-01-8---——— Phenanthrene_________120-12-7———— Anthracene___________84-74-2————— Dl-n-butylphthalate_206-44-0———— Fluoranthene_____129--00-0---—— Pyrene.85-68-7————— Butyl benzyl phthalate____91-94-1————— 3,3'-Dlchloroben_ldlne___56-55-3—----- Benzol a(anthracene______2.1U-01-9———— Chrysene____________117-81-7———- Bls(2-ethylhexyI)phthalate.117-84-0—•—— 01-n-ootyIphthalate_____205-99-2 ——— -- Benzo(b)flunranthene____207-08-9—'—— BenzotMf luoranthnne_____50-32-8-------- Benzo(n)pyrene________193-39-5————• Indeno(l,2,3-cd)pyrene___53-70-3---——— DIbensia, h)anthracene____191-24-2------- Benzo(g,h( IJperylene,

170033017001700330330330330330170017003303303301700330330330330330330670330330330330330330330330330330

(1) - Cannot be separated from Olpheny lamlne

Lab Code' LANCAS , Case No," ___, SAS No.' ___. SUB No.i ___, >V|u)

Matrix' (soli/water) SOIL Lab Sample 10' I50503B\

Sample wt/vol' 30,0(g/ml.) G Lab F l i c ID' >ES<$02

Lewel" (low/mod) LUW Oate Received' 03/29/90

y, Moisture" not dec, ___, dec, • ... Date Extracted" 04/03/90

Extraction" (SepF/Cont/Sonc) SONC Oate Analyzed" 04/03/90

GPC Cleanup" (Y/N) N plH ___, Dilution Factor' 1,000

CONCENTRATION UNITS"CHS Ml). COMPOUND (ug/L or ug/Kg) U13/KG Q

FORM 1 SV-2 1/87 IJm

flROQ0928 "'.' 235

U) EPA SIIIIF'l.h mi.SEiUVULHHLK Uh'UANlCS ANALYSIS D A I A SIIEEI __________,

I II SBUH |

Name" LANCASTER LABS Contract" ___, |__________|

, Lab Code" LANCAS Case Mo." ___, SAS No," ___. SUG No.' ___,

"iiM.trlxi (soil/water) SOIL Lab Sample ID' 1505038

Sample wt/vol" 30,0(g/rnL) G Lab F i l e ID" >E5602

Leuel" (low/rued) LOW Date Received' 03/29/90

y, Molsturei not dec, ___, dec, ___, Date Extracted' 04/03/90

Extraction! (SepF/Cont/Sonc) SONC Date Analyzed! 04/03/90

BPC Cleanup' (Y/N) N pH' ___, Dil u t i o n Factor' 1,00(1

CONCENTRATION UNITS'CAS NU, CUMPUUND (ug/L or ug/Kg) UG/KG U

108-95-2———-- Phenol____________111-44-4———— bls|2-Chloroethy))ether.95-57-8———-- 2-Ch loropheno I______541-73-1-——— 1,3-Dlchlorobenzene___106-46-7------- 1,4-Olchlorobenzene___100-51-6———— Benzyl alcohol______95-50-1————— 1,2-Dlchlorobenzene___95-48-7————— 2-Methy Ipheno I______108-60-1 ——— - bls(2-C'h!orolsopropyl)ether_106-44-5———— 4-Methy Ipheno 1621-64-7—---- N-Nltroso-dl-n-propylamlne_67-72-1————— Hexach loroethane_______98-95-3 ——— -- Nitrobenzene____________78-59-1—----- Jsophorone___________88-75-5————— 2-Nltrophenol_________105-67-9———— 2,4-Olmethylphenol_____65-85-0-------- Benzole acid__________111-91-1———— bl»(2-Chloraethoxy)methane120-83-2———— 2,4-Dlchlorophenol______120-82-1———— 1,2,4-Trlchlorobenzene___91-20-3————— Naphthalene.106-47-8———— 4-Chloroanl line_____87-68-3--——-- Hexachlurobutadlene59-50-7 ——— -- 4-Chloro-3-methyIphenoI.91-57-6 ——— -- 2-Hethylnaphtha Iene_77-47-4- ——— -- Hexaehlorocyc I open tad I fine__88-06-2 ——— — 2,4,6-Tr Ich loropheno I____95-95-4————- 2,4,5-Tr I oh loropheno I____91-58-7-———-- 2-Chloronaphthalene______88-74-4————- 2-Nltroanll)ne___________131-11-3———— Dimethyl phthalate_______208-96-8———— flcenaphthylene_________606-20-2———— 2,6-Ulnltrotoluene_______

330330330330330330330330330330330330330330330330

1700330330330330330330330330330330

1700330

1700330330330

FORM i sv-i flRQQ0929 "~ J/8/234

99-09-2 ——— --- 3-Nltroanl line.83-32-9-------- AcenaphthRne.51-28-5- ——— - 2,4-Dlnltrophenol____•100-02-7———— 4-Nltropheno)_________132-64-9 ——— - Dlbenzofuran_________121-14-2 ——— - 2,4-Dlnltrotoluen-______84-66-2————- Die thy I phthalate_______7005-72-3 ——— - 4-Chloroph(!nyl-ph(!nylr!thRr.86-73-7————- Fluorene________________100-01-6———— 4-Nltro.anlllne____.____.534-52-1 ———— - 4,6-Dlnltro-2-rii(-ClivlpnffnoLU6-30-6 ———— - N-NltrosQillphenyl.'itiilne (!)„101-55-3------- 4-Elromopheny l-phpny If thnr_1UJ-74-1------- Hexach lorobenzene__87-86-5————— Ptsntachlorophpfiol__85-01-8-- — --- Phenanthrene_______120-12-7 ——— - Anthracene______114-74-2———.-- Dl-n-butylphthalaii?.206-44-0———- Fluoranthene.129-00-0———— Pyrene.U5-68-7————— Hutylbenzylphthol it-__91-94-1————— J,3'-Olchlorobensl.|lne.56-55-3-------- t)enzo(a)anthrflcerip___218-01-9 ——— - Chrysene.117-84-0 ——— - Dl-n-octylphthalfltp_205-99-2———— Benzo(b)f liioranthnni*.207-08-9-———- Benzojkjfluoranthene.b'0-32-8---- — - F5(?nzo(a)pyrene_193-39-5———— lndeno(l,2,3-cd)pyrpne.53-70-3 ———— - Dlbenz(a,h)flnthrar;Rne_191-24-2 —— --- Benzols,hi i)perylene__

2100410

21002100410410410410410

21002100410410410

2100410410410410410410820410410410410410410410410410

1C ERA SAMPLE Ml),I3EMIVULATILE ORGANICS ANALYSIS DATA SHEET __________,

I II IPKIIMSO |

Lab NiimRi LANCASTER LABS Contract i ___. |________'

l.nh Code" LANCAS, Case No," ___, SAS No,' ___, SDG Nn , i ___,

Matrix! (.soI l/watnr) SOIL Lab limuplc ID' 1505029,Hample Ht/yol' 30,0(g/mL) (i Lab F i l e IDi >F.!»60!>

Luueli (loM/med) LIJW Oate Rnoelweil" OV29/90

'/, Moisture' not dec, 19.0 doc, ___, Date Extracted' 04/03/90

Extract Inn' (SepK/Cont/Sonc) SIJNC Oate Analyzed' 04/03/90

(•PC Cleanup' (Y/N) N pM« 5.43 D i l u t i o n Factor' 1.000

CUNnENTRATIUN UNITS"CHS ND, CDMPOIJND (ug/L or ug/Kg) UU/KG U

1) - Cannot be separated from DI phony I amIne

FORM I SV-2 1/1:17 Rev

AR000930 ~ 257

IB EPA SAMPLESEMIVIJLAIILE ORGANICS ANALYSIS DATA SHEET ...........jol

_ I V IP101MSD\ab Naniei LANCASTER LABS Contract! ___, I_________

Lab Codei LANCAS Case No.i ___, SAS No.i ___. SDG No,' ___,

Matrix' (soil/water) SOIL Lab Sample ICM 1505029

Sample wt/voM 30,0(g/mL| G Lab F i l e ID' >E!>605

Level' (low/med) LOU Date Received' 03/29/90

"A Moisture' not dec, 19,0 dec, ___, Oate Extracted' 04/03/90

Extraction' (SepF/Cont/Sonc) SUNC Date Analyzed' 04/03/90

GI-'C Cleanup! (Y/N) N pll" 5,43 D i l u t i o n Factor i 1,000

COMCENTRATIUM UNITS iCAS NU, COMPOUND (ug/L or ug/Kg I UG/KG 0

108-95-2———— Phenol____________111-44-4-——— bls(2-Chloroethyl)ether.95-57-8————— 2-Ch loropheno I______541-73-1———— 1,3-Dlchlorobenzene___106-46-7———— 1,4-Olchlorobenaene___100-51-6——— Benzyl alcohol______95-50-1-———— 1,2-Dlchlorobenzene___95-48-7 ——— --- 2-MethyIphenoI.108-60-1———— bls(2-f;h1orolsopropyl)«?ther_106-44-5———— 4-Methy I phenol621-64-7---—— N-Nltroso-dl-n-propy lamlne_67-72-1-------- Hexaehloroethane________98-95-3————— Nitrobenzene___________78-59-1-------- Isophorone______________88-75-5————— 2-Nltrophenol__________105-67-9———— 2,4-D1 methyl phenol_______65-85-0————— Benzole acid___________111-91-1———— bls(2-Chloroethoxy)methane_120^83-2——— 2,4-01Qh loropheno I120-82-1———— 1,2,4-Trlchlorobenzene.91-20-3————— Naphthalene.106-47-8-——— 4-Chloroanlllne_____87-68-3- — ---- Hexachlorobutadlene___59-50-7————— 4-Ch1oro-3-rnethy Ipheno I.91-57-6————— 2-Methulnaphthalene.77-47-4-----— HexachI or OBycI open tad Iene__88-06-2————— 2,4,6-1 rich loropheno I____95-95-4————— 2,4,5-Trlchlorophenol____91-58-7-- ——— - 2-Chloronaphthalene______BB-74-4———-- Z-Nltroanl I Ine_________131-11-3———— Dimethyl phthalate_______208-96-8———— Acenaphthylene_________606-20-2---—— 2,6-Ulnitrotoluene______

410410410410410410410410410410410410410410410410

2100410410410410410410410410410410

2100410

2100410410410

FORM i sv-i flROQ093| 1/8/

.E NO.PESTICIDE OR'JUNICS ANALYSIS DATA SHEET ________

L.sb Hsm.1 LiWSTER LflBS Contract! | PQ101

ei LAMCAS Case No' SAS No' SDG NQI

(soli/water 1 SOIL Lab Sample IDi 150P02,'

Sample ut/uoli 30,0 (g/ml) G Lao File IDi fl900?2_037,RES

Laws I" (low/mad) LOU Data Received! 03/29/90

X Molsturei not da: 19 dec, Date Extracted" 04/02/90

Extraction" (SepF/Cont/Sonc) SQNC Date Analyzed' 04/03/90

GPC Cleanup' (Y/N) N pHi .5,5 Dilution Factor! 1,0

CONCENTRATION UNITSi(uq/L or uq/Kq) UG/KG

CflS NO, COMPOUND " " —-——— Q

319-84-6 ———— alpha-BHC319-85-7 ———— bata-BHC319-Si-fl ———— delta-BHC

74-M-a ————— Heptach lor309-00-2 ———— Aldrln1024-57-3 ———— Heptach lor epaxtde959-98-8 ———— Endosu 1 fan I60-57-1 ———— Dleldrln72-55-9— ——— 4,4' -DDE72-20-8 ————— Endrin33213-65-? ——— Endosulfan II72-54-3 ————— 4,4'-DDD1031 -07-B ——— Enrfosulfan aulfate50-29-3 ————— 4,4' -DOT72- 3-5 ————— Methoxychlor53494-70-5 ——— Endrin kefcane . „ ,5103-71-9 ———— alphfl-ChlnrdaneB103-74-2 — -- -qatma-Chlordane8001-35-2 ——— Toxaphene126i"4-ll-2 ——— Hroolor-101611104-23-2 ——— rtroclor-122111141-16-5 ——— Aroclor-123253449-21-9 ——— rtroclor-124212672-29-6 ——— flrocl or -12,491L097-.9-1 ——— Aroclor-126411096-82-5 ——— Hroclor-12^0

9,99,99,99,99.99.99,99,920,20,20,20,20.20,20-,99,20,99,99,

200,99,99,99,99,99,

200,200,

UIIUIIIIUUUUIIUUUUUuuuuuuuuU'uuu

FORM I PEST 1/87 Rev,

270AR000932

PESTICIDE OKGHN1CS ANALYSIS DATA SHEET _____________I i

Ldb Name i LANCASTER LABS Contract' | F'0205 |

.'-Nib Coca' LfiNCAS Case hlu" SAS No' SPG No'

.-i-atri* l*cii-'w-i™t) SOIL lab Sarnie ID' 1PO!"053

Sample ut/ijol' 30,0 (g/ml) G Lab File ID' fl90092_0?8.RES

Level' (luw/nwd) LOU Q*t« Received« 03/29/90

X Moisture' not deo 17 dec, Date Extracted' 04/02/90

Extraction" (SepF/Cunt/Sonc) SQNC Date Analyzed' 04/03/90

GPC Cleanup' (Y7N) N pH> 5,4 Dilution Factor' 1.0

CONCENTRATION UNITS'(uq/L or ug/Kg) UG/KG

CAS ISO, COMPOUND ————

—V6"rt-8———Heptach I or,

319-84-6————alpha-BHC.319-85-7————beta-BHC.319-8--3———delta-BHC______58-09-9————yawna-BHC (Lindane).

309-00-2 ——— -Aldrtn.1024-57-5 ——— Heptachlor epoxlde.9P9-9B-3 ——— -Endosulfan I ____60-57-1— • —— Oteldrin ______72-55-? ———— 4,4' -DOE ______72-20-3 ———— Eridr In _______

5-9 —— Endosulfan II72-54-d ———— 4,4' -DDD1031-07-8 ——— Endosulfan sulfate_50-29-3 ———— 4,4' -DOT ______72-HJ-5 ———— tlethoxychlor ____53494-70-5 —— Endrin ketone _____5 103-7 1 -? ——— al pha-Ch lordane __5103-74-2 ——— garnna-Chlordane ___8001-35-2 —— -Toxaphene ______12674-11-2 —— Aroolor-1016 ____11104-26-2 —— -Aroclor-1221 ____11141-16-5 —— Aroclor-1232 ____53>*6?-21-9 —— Aroclor-1242 ____12672-29-6 —— Aruclor-1248 ___ .11097-6?-! —— Aroclor-1254 ____110?o-62-5 —— -Aroalor-1260 ____

9,69,69,69,69,69,69,69,619,19,19,19,1?,19,19,96,19,96,96,

190,96,96,?6,96,Pii.

190.190,

FORM I PEST 1/87 Rev.

"" 2*73AR000933

!'E«riCi:E OMilN!:JS ANALYSIS -V,TA SHEET

Lab N<_IRI LANCASTER LrtElS Contract' | P030«

b Co.:. i LHNMS il-se No' SAS Ns' MG Mo'

I'utru .soil, 'water) StIL -sb Simple 1C' 1F05074

S-riiple wt/ucili 30,1 (g/ml) G Lab Fl 1e ID' A96092J39.RES

Level' i;on,'n«d) LOW Date Receluedi 03/29/90

X Molsturei nod des 11 dec, Date Extracted' 04/02/90

Extraction' (SepF/Cont/Sonc) SUNC Date Analysed! 04/03/90

GF'C Cleanup! (Y/N) N pH' 5,8 Dilution Factor' 1,0

CONCENTRATION UNITS i(uq/L or ug/Kq) UG/KG

CflS NO, COTQUND " " —————— Q

319-84-6— —— fllpha-BHC319-SE-7 ———— heta-BHC319-E4-B ———— dclta-BHC59.99.9 —— „ —— qarnna-BHC (Llndanel , , .76-44-9 ———— Heptach lor _ ,,,...,309-00-2- ——— rtldrln10:,i-E7-? ———— Heptach 1 3 ;- apaxfris9El?-93-fl— —— Endosulfan I60-57-1—— —— D'.isldrln72-BE-9- ———— 4.4'-DDE72-20-9— • ——— Enjrlr,J3213-65-9 ——— Er,do«u Ifan 11 „ „., ,72-5,-a ————— ft,4'-DDD1051-07-3 ———— Enda*u1l1.!m sulfataBO-29-3- ———— 4T4'-DDT72-43-5 ————— Methcxyohlor , „53494-7C-5 ——— Endrln ketone5103-71-9- —— fllpha-Chlordans5103-74-2 ———— quma-ChlardaneS001-3S-2 ———— Toxaphene12674-11-2 ——— firoolor-1111611104-23-2 ——— ArDclor-122111U1-16-S-—— flroclor-123253469-21-9 ——— Hroclor-124212672-29-6 ——— Hroolor-1248, , , , ,.11097-69-1 ——— Aroclor-125411096-S2-S ——— rtroclar-1260

9,0?,09.09,09,09,09,09,0

18,13,18,18,18,18,18.90,16,70,90,180,90,90,90,90,90,180,180,

UUUIIIJUIJIIuIIIIuuuuuuuIJuuuuuuuu


:>. £F'i 'MPiK'i nu,PEsr::iDf CUVGHNICS ANALYSIS UHTA SHEET ________

lL,sb ,")««' LAMCHSTER LHC-IS Contract' | POP05

Cone i LAPH.HS Case No' !JAS Me' SDG No'

iK l soil, wetter) SOIL Lab Sample ID' 1POP037

••*,•sample wt/uol' ?0,0 (g/rnlj G Lab File ID' A90092J41.RES

L«,eli l'1ow/(ii*dj LQU Qaiw Received' 03/29/90

% Molsturei not deu 22 dec. Oate Extracted' 04/02/90

extraction' (SepF/Cont/Sonc) SONC Date Analyzed' 04/04/90

IK Cleanup' (Y/N) N pH' 5,3 Dilution Factor' 1,0

CONCENTRATION UNITSt.(uq/L or ug/Kq) UG/KG

CAS Ml), CDMP'uMC' ————

319-84-a — - — alpha-ElHC319-85-7 ———— beta-fiHC319-Bo-B ———— delta-BHC

^ 58-69-9 ———— adiAia-BHC (Llndanei ." '6-<W-fl ————— HepMchlorsJ-/30?-00-2 ———— rtldrlr,

1 1024-S"-.! ——— Heptdchiar ftpuxiijfl, „,,„,.„„,. . , .9B?-9S-Q ———— Endosulfan IiiO-57-1 ————— DlwliJrln

, ,-2-55-9 —— - — a, 4 '-DOE72-.0-8 ————— Endrin33213-o5-9 ——— Enrfosulfan II .| 72-Sa-d ————— 4,4'-DDDi 1051-07-3 ——— Endosulfan sulrisj., ,1 50-29-3 ————— _,4'-DDT1 72-43-!! ————— r-btihoxychlcr| 53454-70-5 ——— Endrin ketone5103-71-9 ———— alpha-Chlordane5103-74-2 — -— namma-Chloraane

1 SU01-3B-2 ———— Taxaphene12674-11-2 ——— Hro_lor~101,i11104-28-2 ——— Hruclor-122111141-16-5 ——— flruclar-'12»2,S34_*-:i-? ——— Ar.o<2lor-12«Jl_d72-2?-o ——— rtroclor-12«iS

1 110?7-_9-l ——— Hroclai"-12?4llC'/o-ilZ-5 — • — Brufllui'-l^dlJ. , ,, ,

1 -

10,10,10.10.10,10,10,10,20.20.20.20,20.20,20,

100,20,

100,100,200,100,100,100,100,100,200,200,

UUUUUuuuuuuuuuuuuuuuuuuuuuu

FORM I PEST ' 1/87 Rev,

flR000935 "" 306

:. . Sri-1 'jflpiri.i nuPESTICIDE ORCflNICG ANALYSIS DATA SHEET ________________

I IL_b Plane' LANCASTER LHES Contract' | METHO |

ib Code' LflMCflS Case No' SAS No' SDG No'

Matrix (:.o11/w_t_r) SOIL Lab Sample ID' 1505030

Sample Ht/voli 30,0 (g/mlj G Lao File ID' A90092J43.RES

Level' (lou/rned) LOU Date Received' 03/29/90

y, Moisture' not dec dec, Date Extracted' 04/02/90

Extraction' (SupF/Cont/Sonc) SONC Date Analyzed' 04/04/90

GPC Cleanup' (Y/N) N pH' 6,6 Dilution Factor' 1,0

CONCENTRATION UNITS'(ug/L or ug/Kg) UG/KG

CAS NO, COMPOUND ——-—— Q

| 319-84-6———alpha-BHC______I 319-85-7———beta-BHC______| 319-86-8———delta-BHC._______I 58-99-9————g_(nta-BHC (Llndane).76-44-8————Heptach lor_____309-00-2——-Aldrln_

I 1024-57-3———Heptach lor epoxlde_I 959-?8-8-———Endosulfan I____I 60-57-1————Oleldrln______I 72-55-9-——-4,4'-DDE______| 72-20-8————Endrin_______I 33213-65-9——Endosulfan II___| 72-54-3————4,4'-DOD______I 1031-07-8———Endosulfan sult'ate_i 50-29-3————4,4'-DOT_! 72-43-5————Methoxych1or__I 53494-70-5——Endrin ketone__i 5103-71-9———alpha-Chlordane.! 5103-74-2———gamna-Chlordane.i 8001-35-2———Toxaphene___I 12674-11-2——Aroclor-1016__11104-20-2——Aruclor-1221__11141-16-5-—-ArocI or-1232__

1 53469-21-9——Aroclor-1242__1 12672-29-6——Aroclor-1248__11097-69-1——Aroclor-1254__

I 11096-32-5——Aroclor-1260___

8,08,08,08,03,08,08,08,016,16,16,16,16,16,16,80,16,ao,80,160,80,ao,80,80,80,160,160,


AROG0936 ~ 494

r'S'STICIOE yMHNtiv WHL'.'SIS DATA SHEET

T0101 - P* TL-b tone i LANCASTER LHEii Contract;! |

Ccwe' LMCHS Case No' SAS No i SDG No'

»•*-i I/water) SOIL Lab Sample IDs 15050:6

Uvnple Ht/woli 30.0 (g/ml) G Lab Fi le ID' H!»0092_C34,RES

LeveM (law/rued) LOI4 Data Received! 03/29/90

! Moisture' not dec 19 dec. Date Extracted' 04/02/90

Extraction' (SepF/Cant/Sonc) SONC Oate flnalyzed' 04/03/90

.PC Cleanup! (Y/N) N pHi 5,5 Dilution Factor! 1,0

CONCENTRflTICN UNITS'(uq/L or uq,'Kq) UG/KG

CAS NO, COMPOUND

I II 319-84-6————alpha-BHC______________I 9,9319-35-7————beta-EHC ___________| 9,9

i 319-86-8———delta-BHC._____________! 9,9I 59-139.9——.—qamildl..!jHC (Lindane)________| 9,9— .44.3.—.—fi-ptacMar_____________I 9,9

9-00-2——-flldrln_______________I 9.9VJ24-F7-3-——Heptaohlor epaxlde________I 9.9959-9S-9———Endosulfan I____________I 9,940-57-1——-—Dleldrlr______________' 2'5,

I 72-55-9———-4,4'-DUE_______________I 20,1 72-20-8————Endrin________________I :0,

3rw:li-an II___________! 20,

| 79.54.3————4,4'-ODD_______________I 20.I 1031-07-8———EndasUfan jurats__________j TO.50-29-3————4,4'-DOT,______________I iO.72-43-5————Methoxyohlor,____________I "9.

I 53494-70-F——Endrin ketor.e.___________! 201 5103-71-9———alpha-Chlordane__________1 99.5103-74-2———qenma-Chlordane.__________I '9,

I 8001-35-2——toxaphene______________I 20D,I 12^74-11-2——Aroclor-1016______:_____! ?',11104-20-2-—Hroclor-1221,____________! '",

, 11141-16-5——flroslor-1232_______.__________1 '",

11097-o9-l——Arae lor-1254____________I 200,I U09a-32-5--—Aroclor-1260____________I 200.i I


flR000937 503

I'KSTICi'.'E OKfolNICS H"!flLY3IS L'llTA SHC.ETI .JJ r i?>l

ub name' LANCASTER LHBSr

Contract' I FP'JIOI * _.,) \ NT................ ! ML _'_;•" " Jf"

ib Cwe' '.HPICrtS Case No' SAS fto' SDG No'

r«ri.< (Mll.^-wr) SOIL Lao Sample 1C" lEOPO:?

Mt.-yijl' 30.0 la/'iiuj 13 uab File ID' AP0092_05E',RES

(low. iMdj LOW D..(e Revived' Os/29/PO

! not dec 19 . dun, Data Extracted' 04/02/90

Extraction' ('jtspF/CunVSonc) SOHC Date Analysed' 04/03/90

GPC Cleanup' (Y/N) N pH« 5,4 Dilution Factor' 1,0

CONCENTRATION UNITS'(ug/L or ug/Kq) UG/KG

CflS HO. COP1POUNO " ————— Q

1| 319-B4-0 ———— alpha-BHC| 319-195-7 ————— beta-tlHC| 319-!36-fi ———— delta-EHC| SB-3!>-9 —————— pqMfna-BHC (Lhidans)1 76-«u-3 ————— Heptach lor309-00-2 ———— flldrln

j 10i4-5/--3 ——— neptatihlor wpoxlds,.... ..... .1 959-98-S ———— Endosul-r_n I1 ,60-57-1 ————— Dlt-ldrin| 72-55-9- ——— -4,4'-UOE| 72-20-8- ———— Endrin! 3?21?-6R-9 ——— Endosulfan II| 72-54-6 ————— 4, 4' -ODD| 1031-07-E ——— End-sullen sulfata1 SO-29-3 ————— 4,4'-DDT72-43-P ————— Methoxychlor

, 53494-7CI-5 ——— Endrin ketune1 510:1-71-9 ———— alpha-Chlordane5103-74-2 ——— cianma-Chlorddine300 1-35-2 ———— Taxaphene

1 12674-11-2 ——— flroolor-lDla1 11104-28-2 — — Aroolor-122111141-14-5 ——— Aroolor-1232

l 53449-21-9 ——— Aroc lor-12421 12472-29-6 ——— Aniclar-12-GUJ'?7-(i9-l ——— Hruclur-1254

, 1109o-02-5- —— ftroclor-12401

9,9' 9,9

9,99 99,99,9?,?9,920.20,20,20,20,20,20,99,20,99,99,

200,99,?9,99,99,99.

200,200,

UIIUIIIJUIJIIIIuuuuuuuuuuuuuuuuuu

FORM I PEST 1/87 Rev.

flR000938 "" 512

J

ECHEM INC.ENGINEER I NO CHEMISTRY CONSULTANTS

132 Route 35Sebago Common

North Hindham, Maine 04062(207) 892-0002

PAX (207) 892-7499

25 June 1990

Ms Deirdre SmithDPL Consultantsa/o Duffield Associates5350 Limestone RoadWilmington, DE 19808

Re: Tybouts LandfillLaboratory: Lancaster LabsCase No: T.B2-IInorganics: Soils - TP0101, TP0101D, TP0101S, TP0205, TP0304,

TP0407, TP0505.Hater - TYB21T, TYB21TD, TYB21TS, TYB23T.

Dear Ms Smith:Validation was performed on the inorganic analytical data fromthe soil and water samples referenced above. The data wereevaluated based on the following parameters:

* o data completeness* o holding times* o calibrationo blanks

* o ICP interference check sampleo matrix spike sample analysiso duplicate sample analysis

* o laboratory control sample analysis* o furnace atomic absorption analysiso ICP serial dilution analysis

* o detection limits* o sample result verification

* All criteria were met for this parameter.

Table I provides a glossary of data qualifiers used.

Table II summarizes the validation recommendations in accordancewith USEPA Laboratory Data Validation Functional Guidelines forInorganics Analyses, June 13, 1988, and are based on thefollowing information.

flR000939

Also attached are the validation log, completeness log and samplepreparation and analysis summary with sample identificationcross-reference on ECHEM standard forms.CALIBRATION

a. Furnace AA linearity.Calibrations providing a correlation coefficient (r) of < 0.995are tabulated below:

CALIBRATION DATE/TIME ELEMENT (r)4-10-90 Selenium 0.9929

Associated samples:SAMPLE NO.TYB21TTYB21TSTYB21TDTYB23T

Action:o all associated positive results and non-detects are

flagged as estimated (J) and (UJ).BLANKS!

Blanks providing results above the IDL and their associated 5Xaction levels are tabulated below:SOIL BLANK ID. ELEMENT CONCENTRATION ACTION LEVEL

Cal 1 Aluminum 14.1 70.5Cal 2 Barium 12.3 61.5Initial Cal Cadmium 2.0 10.0Cal 2 Calcium 27.0 135Cal 3 Chromium 4.4 22Cal 1 Cobalt 6.2 31Cal 1 Copper 5.9 29.5Cal 1 Iron 217.3 1086.5Cal 2 Magnesium 26.9 134.5Cal 1 Manganese 5.4 27Initial Cal Mercury 0.1 0.5Cal 1 Nickel 29.2 145Cal 1 Selenium 1.3 6.5Cal 1 Silver 8.2 41Cal 2 Vanadium 10 50Prep Blank Zinc 0.751 3.76

Associated samples with positive values reported below the actionlevel are:SOIL SAMPLE NO. ElBMEHI CONCENTRATION

TP0407 Mercury 0.01Nickel 1.6Selenium 0.05

TP0505 Cobalt 0.47Mercury 0.28Selenium 0.06

TP0101 Cobalt 1.5Mercury 0.01

TP0101D Cobalt .1.5Mercury 0,01Selenium 0.05Silver 0.39

TP0205 Cobalt 0.70Mercury 0,07Selenium 0.06Silver 39.4

TP0304 Cobalt 0.44Mercury 0,07Nickel 1.3Selenium 0.06

HATER BLANK ID. ELEMENT CONCENTRATION ACTION LEVELPrep Blank Aluminum 48.8 244Prep Blank Barium 6.7 33.5Cal 1 Cadmium 4.2 21.0Prep Blank Calcium 166.8 834Prep Blank Chromium 7.1 35.5Prep Blank Copper 7.5 37.5Prep Blank Iron 125.7 628.5Prep Blank Lead 2.2 11Prep Blank Magnesium 32.4 162Cal 1 Manganese 4.4 22Prep Blank Mercury 0.2 1.0Cal 2 Nickel 6.1 30.5Prep Blank Potassium 985.5 4928.5Prep Blank Zinc 20.0 100

HR0009I)

0

Associated samples with positive values reported below the actionlevel are:

SAMPLE HO. ELEMENT CONCENTRATIONTYB21T Chromium 6.8

Copper 10.2Iron 40.7Manganese 5.7Mercury 0.12Nickel 7.5Potassium 1010

TYB21TD Copper 9.8Iron 57.3Manganese 7.4Mercury 0.16Nickel 10.3Potassium 840

TTB23T Cadmium > 3.3Chromium 7.0Copper 10.0Iron 31.4Manganese 17.1Mercury 0.21Potassium 467

Action:

o positive sample results less than the action level areflagged as non-detect at the sample value (U).

MATRIX SPIKE RECOVERIES

Samples providing matrix spike recoveries outside the 75-125%that contain native analyte at < 4X the spiking level aretabulated below:

SAMPLE HO. ELEMENT MB RECOVERY (»)TP0101 Antimony 58.0

Arsenic 180.1Barium 70.6Beryllium 870.5Cadmium 901.6Chromium 7.6Copper 61.0Lead 433.5Potassium 50.9Selenium 53.4Vanadium 26.0Zinc 70.4

flR00091)2

Action:o For MS recoveries > 125% and sample values non-detected,

no action ia taken,o for MS recoveries outside 75-125%, positive sample

results are flagged as estimated (J),o for MS recoveries from 30-74%, non-detec.s4 sample

results are flagged as estimated (UJ), ar.fio for MS recoveries < 30%, non-det.sct'jd sample results are

rejected (R).DUPLICATE SAMPLE ANALYSIS!

1. Field replicates.

Sample replicates containing > 5X CRQL of an analyte providing arelative percent difference (RPD) which exceeds the control limitof + 20% for water and ± 35% for soil, or when either the sampleor its replicate contains < 5X CRQL of an analyte and thedifference exceeds ± CRQL Cor water or _. 2X CRQL for soil aretabulated below:

SAMEIiE E1EMEHI RPpt%) CRQLTP0101D Barium 68.7 40

Lead 49.2 1Manganese 148.4 3

TYB21TD Zinc 28.3 20

Action:o positive results for all samples of the same matrix

associated with the analytical event are flagged asestimated (J).

ICP SERIAL DILUTION ANALYSIS!

Serial dilution results providing a %D of >15% are tabulatedbelow:

SAMPLE; ELEMENT 15TP0101 Barium 49.1

chromium 19,3Iron 10.2Vanadium 21.1Zinc 42.9

TYB21T Barium 23.5

Action:if results from the diluted sample are > the undilutedsample, all results for samples of the same matrix areflagged as estimated (J)/(UJ), and

if results from the diluted sample are < the undilutedsample, flag positive results from all samples of thesame matrix are flagged as estimated (J).

Very truly yours,ECHEM INC.

B.K. Hallin, PhDVice Presidentenc.

AR0009M

Table I

DATA QUALIFIER DEFINITIONS (INORGANICS)

U - The material was analyzed for, but was not detected abovethe level of the associated value. The associated value iaeither the sample quantitation limit or the sample detectionlimit.

J - The associated value is an estimated quantity,R - The data are unusable. (Note: Analyte may or may not be

present).

UJ- The material was analyzed for, but was not detected. Theassociated value is an estimate and may be inaccurate orimprecise.

«R0009l|5

IA EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ________

Name: LANCASTER LABS______ Contract:VBLK02

'._ab Code: LANCAS case No.: 253.212 SAS No.: ____ SDG No.: TYB2Matrix: (soil/water) SOIL Lab Sample ID: CBLKAPSSample wt/vol: s.o (g/mL) S_ Lab File ID: CBLKAPSlevels (low/med) LOW Data Received: 03/29/90% Moisture: not dec. __ Date Analyzed: 04/05/90.oluran: (pack/cap) PACK Dilution Factor:

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/Kfl

74-87-3—'———Chloromethane_74-83-9————Broraonethane_75-01-4—————Vinyl chloride,75-00-3———-Chloroethane75-09-2—————Methylene Chloride67-64-1—————Acetone75-15-0—————Carbon Disul.ida______75-35-4—————1,1-Dichloroethene_____75-34-3—————1,1-Dichloroethana_______540-59-0—————1,2-Dichloroethene (total).67-66-3————-Chloroform_________"107-06-2————1,2-Dichloroethane_____78-93-3'—-——-2-Butanone__________'71-55-6—————1,1,1-Trichloroethane___56-23-5—————Carbon Tetrachlorida____108-05-4————Vinyl Acetate________75-27-4———Bronodichloromethane___78-87-5——"—-1,2-Dichloropropana____10061-01-5-——-cis-l,3-Dichloropropene__79-01-6—————.richloroethene_______124-48-1————Dlbromochloromethane____79-00-5—————1,1,2-Trichloroathane___71-43-2-————'Benzene____________10061-02-6——-trans-l,3-Dichloropropene_75-25-2———-Bromoform108-10-1—————4-Methvl-2-Pantanona591-78-6-'———2-Hexanone__________127-18-4————Tetrachloroethena_____79-34-5—————1,1,2,2-Tetrachlo_oetnane_108-88-3————Toluene___________108-90-7——••——'Chlorobenzene_______100-41-4————Ethylbenzene________100-42-5—————Styrene1330-20-7————Xylena (total).

101010105455555510551055555555510105555555

NG 0(J9 If 6 V87 Rav. ,33

TAHIEII

Reaion JINORGANIC REGIONAL DATA ASSESSMENT ^_ •

DRAFT__ /"" UKttt*t*, CASE NO. ________________ SITE.

LABORATORY AHfA&TfK. ______ NO. OF SAMPLES/NO. OF SAMPL . / (MA-rant 4v/Al*./7 t

SDC« rygJ-JI __________ . REVIEWER (IF NOT ESD)_________________ REVIEWER'S NAME 3?-

DPO: ACTION ___ FYI _______ COMPLETION DATE.

DATA ASSESSMENT SUMMARY

1. HOLDING TIMES2. CALIBRATIONS3. BUNKS4. ICS5. LCS6. DUPLICATE ANALYSIS*1*7. MATRIX SPIKEI. MSA9. SERIAL DILUTION10. SAMPLE VERIFICATIONII. OTHER QC12. OVERALL ASSESSMENT

0 • Data hid no problemi/or qualified duo to minor problem.M • Din qualified due to oujor problem!.Z • Data unwetpable.X • Problenu, bat do not affect data.

ACTION ITEMS;,

,, - , , . D r ',AREAS OF CONCERN: * a a,*j/» n-Ux.i,... & At fw,t*

H-, , 7 »* «U TT,. , UJ -U ..I«U ' . P O r——• A1

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/) Cou--_ Jv/^ QtvlJ T\6h Jtf fli*tfll\. l/« l.itl't .____' " U U 3 4 /

DATA VALIDATION LOO

CLIEHT ft0 QlN> V\<CtOii= PROJECT ID "\l

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CASE HO. DATE REC'D VALIDATION DUITS

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tedzssnTAri .35?

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VOA SVGA IHORO PEST/ PCB DIOX SAS

S "Si-Id tit1

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(OTEi UNITS ARE DEFINED AS HATER/SOIL (s. 9. ,5/6) INCLUDING BLANKS

MMMENTS: SAS for this project includa - fJoiU^

Turnaround time for these caaaa i-fetandaiffi/faata days— Texrcle one)

9XNFUE PRDA1ATIOI AID AULT-I-

CM! BO TYB2-£ AIALITIOU. FMCTIOM (VSe.-W.Si

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1R000949

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U.S. EPA - CLPEPA SAMPLE NO.

1 /~\INORGANIC ANALYSIS DATA SHEET I I.'"'1 'I

I F'BS '""' ILab Name! Lancaster Laboratories Contract! I_______I

•'*,Lab Code: Case No.) SAS No.i SDB No.i TYBS-I

Matrix (soil/water)! SOIL Lab' Sample ID! 1505038

Level (low/med)i LOW Date Received! 03/59/90

'/. Solids: 1,00.0

Concentration Units (ug/L or mg/kg dry weight)! MG/KQ

I I I I I IICAS No. I Analyte IConcentratlonlCI Q IM

12_g2=22=§_I Aluminum.

25fffi=ii=g_ I -ESSE---

l2S_0-fta-ft I Cobalt__l2SS2=Se=§_IESEE9E_2S32=§2=6_IlE2n__

12532=22=6-1 Bgr._yEy_|7fj<*0-0a-0 INickejl__i2ft5i=22=2l i Esiiiliyffl

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Color Before! . Clarity Before! TeKturei

Color Afters Clarity Affcen Artifacts!

Commentsi

31FORM I - IN flR00095l 7/S1

Rev. IFB Amendment One


INORGANIC ANALYSIS DATA SHEET II -TYM04 I

Lab Names Lancaster Laboratories Contract! I _______ |

Lab Codei Case No.! SAS No.i SDQ No.! TYB2-I

Matrix (soil/water)! SOIL Lab Sample IDi 1505087

Level (low/med)! LOW Date Received! 03/89/90

'/, Solldsi 81.0

Concentration Units (ug/L or mg/l«g dry weight): ME/KB

)

Color Before:

Color After:

Comments!

1 1 1 1 1 1 1ICAS No. 1 Analyte IConcentrationlCI Q INI1 1 _ _ _ I I I I1 2Sg2=2!2=5_ 1 SlyfflisySL1 74<JO~36-0~ | Antimony"1 2__°-3a~a_ 1 firserj ji c '1 2_£t2=_2_i_ i ii-Iya!"i2SS2=5i=2_ liiE.Iilyffl1744. 0-43-9 1 Cadmium17440-70-S 1 Calcium1 2»52=42=__ 1 Chromium,1 74_0-_8-4_ 1 Coba 1 t __1 7440-50-i" 1 Co_oer174,39-89-6 IIron__ _17439-92-1 ILead1 2_32_9S=4_ 1 Maongsji u01 7<j3 9- 96-5~ 1 Ma noanese17439-97-6 IMercurvl7440-Oa-0_INicl(ei __17440-09-7 1 Potassium17783-59-3 1 Selenium,i2___=ga-_'_ I §ii_er _'25i2=g3=§- i§__iy~ _i _ii_2=Ii=i3l i Ibilliyffll

1 ICvaiiTd-""1 1

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959 i T • TP i>——— 32_|_ i __§_____!£_ i;___ _____ _ l__________

_____ 39700 I IE _S__J.P_I''____ |____ ..,__.__

TaT~r"E*" " TP i\____ o.oT iST \_C __j.cvi;

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Clarity Before: Texture:

Clarity Afters Artifacts!

34FORM I ~ IN 'flD/in-A-.-, 7/8'

Amendment Qni

U.S. EPA - CLPEPA SAMPLE N0.|

1 S*\INORGANIC ANALYSIS DATA SHEET Cfp'oi-t T| I

Lab Names Lancaster Laboratories Contracts I _______ I

Lab Code! Case No.! SAS No.i SDG No.! TYB2-l|

Matrix (soil/water): SOIL Lab Sample ID: 1505089

Level (low/med): LOW Date Received: 03/S9/90

'/. Solids: 80.8

Concentration Units (ug/L or mg/kg dry weight)! HE/KG

I I I I I IICAS No. I Analyte IConcentratlonlCI Q IMI______I____.

12ft-2=_'6=2_ 1Sotiffl£By_

I2S_2=SA=2_I__E____y_ll2fifi2=22=g_IS_IsAy__12__2=ft2=3_ I E&ESfflAHffl-12S_2=5_=5_lEe&ai-_

!=§2=9_ 'E__53E_«_l2*32=82=6J.lEe__12ft32=2g=i_ !_____12ft32=2_=S_ I Manganesel2532=22=6_lBscs_E*_l2fift2=2g=2_INi£L<Si.I22§g=ft2=g_is_is«iyffl_I2440-S3-4 I Silverl2_ft2=g3=5_ISodiuffl_

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Lab Codei Case No.i SAS No.i SDQNo.i TYB3-I


Level (low/med): LOW Date Received! 03/H9/90

'/, Solids! 81.0

Concentration Units (ug/L or mg/kg dry weight): MS/KB

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32FORM I - IN ~ i _ _

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Documents

•i r - Superfund Records Collections | US Environmental ... · IV CONCLUSION fi RECOMMENDATIONS 8 TABLES ... the top of the underlying silt-clay stratum. Test pits, performed in