J64994-1 Std Tal L3 Package Mini Final Report - dtsc-ssfl.com fileexceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval

ANALYTICAL REPORT

Job Number: 280-64994-1

Job Description: MWH - Boeing SSFL GW 1Q15

For:MWH Americas Inc

2121 N California BlvdSuite 600

Walnut Creek, CA 94597

Attention: Sarah E VonRaesfeld

_____________________________________________

Approved for release.Jamie N IdeProject Manager I2/18/2015 3:43 PM

Jamie N Ide, Project Manager I4955 Yarrow Street, Arvada, CO, 80002

(303)736-0126 [email protected]

02/18/2015

cc: Boeing EDMS

The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with anyexceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval ofthe laboratory. All questions regarding this report should be directed to the TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

TestAmerica Laboratories, Inc.

TestAmerica Denver 4955 Yarrow Street, Arvada, CO 80002

Tel (303) 736-0100 Fax (303) 431-7171 www.testamericainc.com

02/18/2015Page 1 of 101

mailto:[email protected]://www.testamericainc.comhttp://

Table of ContentsCover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93

Subcontracted Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 96

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99

02/18/2015Page 2 of 101

CASE NARRATIVE

Client: MWH Americas Inc

Project: MWH - Boeing SSFL GW 1Q15

Report Number: 280-64994-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

RECEIPT

The samples were received on 2/4/2015 10:00 AM; the samples arrived in good condition, properly preserved and, where required, on

ice. The temperatures of the 4 coolers at receipt time were 1.1 C, 2.8 C, 3.9 C and 5.9 C.

The requested 1,2,3-TCP 524.2 SIM, and 314.0_LL Perchlorate analyses were performed by TestAmerica's Irvine laboratory.

The requested 8315 Formaldehyde analyses were performed by TestAmerica's North Canton laboratory.

The samples requesting "Extract and Hold" on the Chain of Custody will be reported under a separate cover (280-64994-2). All other

samples/analyses requested on the Chain of Custody will be found in this report.

The volume submitted for 314 Perchorate analysis for sample RD-78_020315_01 (280-64994-11) was received with approximately 1/4

inch of headspace. For water samples, headspace should be about one-third of the container in order to reduce potential anaerobic

biodegradation.

VOLATILE ORGANIC COMPOUNDS (GC/MS SIM) - 524.2 SIM

Sample RD-60_020315_01 (280-64994-5)[2.5X] required dilution prior to analysis. The reporting limits have been adjusted accordingly.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

VOLATILE ORGANIC COMPOUNDS (GC-MS)

Methylene Chloride was detected in method blank MB 280-263200/8 at a level that was above the method detection limit but below the

reporting limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the

MDL and/or RL, the result has been flagged.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

VOLATILE ORGANIC COMPOUNDS (GC-MS SIM)

1,4-Dioxane exceeded the RPD limit for LCSD 280-263242/4. The associated LCS/LCSD spike recoveries were in control and

demonstrate that operating procedures were in control. No further action was required.


SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)


SEMIVOLATILE ORGANIC COMPOUNDS - GC/MS SIM LL


GAS RANGE ORGANICS


DIESEL RANGE ORGANICS


PERCHLORATE (IC) - 314.0_LL


FORMALDEHYDE

Formaldehyde was detected in method blank MB 240-166845/2-A at a level exceeding the reporting limit. If the associated sample

reported a result above the MDL and/or RL, the result has been flagged.

02/18/2015Page 3 of 101


PERCHLORATE - 6860


ANIONS (48 HOURS) - Nitrate as NO3


ANIONS (28 DAYS) - Fluoride


AMMONIA


CORROSIVITY (PH)


HYDRAZINE/UDMH/MMH

1,1-dimethylhydrazine (or unsymmetrical dihydrazine, UDMH)- eluted outside the retention time window on the matrix spike or matrix

spike duplicate for the following samples and parent samples: (280-64994-6 MS), (280-64994-6 MSD), RD-39B_020315_01

(280-64994-6). When reviewing the samples for target compounds, this retention time shift was taken into account. Individual samples

were compared to neighboring QC as well as individual matrix retention time spikes.


02/18/2015Page 4 of 101

SAMPLE SUMMARY

Client: MWH Americas Inc Job Number: 280-64994-1

Client Sample IDLab Sample ID Client Matrix Sampled Received

Date/Time Date/Time

280-64994-1 RD-32_020315_01 Water 02/03/2015 1111 02/04/2015 1000

280-64994-4TB TB_RD-32_020315 Water 02/03/2015 0700 02/04/2015 1000

280-64994-5 RD-60_020315_01 Water 02/03/2015 0933 02/04/2015 1000

280-64994-6 RD-39B_020315_01 Water 02/03/2015 1008 02/04/2015 1000

280-64994-9TB TB_RD-39B_020315 Water 02/03/2015 0700 02/04/2015 1000

280-64994-10 RD-66_020315_01 Water 02/03/2015 1201 02/04/2015 1000

280-64994-11 RD-78_020315_01 Water 02/03/2015 1334 02/04/2015 1000

TestAmerica Denver 02/18/2015Page 5 of 101

EXECUTIVE SUMMARY - Detections


Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

280-64994-5 RD-60_020315_01

0.013 ug/L 524.2M_CA-SRL0.0301,2,3-Trichloropropane

1.0 ug/L 8260B0.28 J1,1,2-Trichloroethane

1.0 ug/L 8260B2.31,1-Dichloroethane

1.0 ug/L 8260B1.71,1-Dichloroethene

0.50 ug/L 8260B2.31,2-Dichloroethane

1.0 ug/L 8260B0.29 JChloroform

1.0 ug/L 8260B14cis-1,2-Dichloroethene

1.0 ug/L 8260B0.19 JToluene

1.0 ug/L 8260B0.45 Jtrans-1,2-Dichloroethene

10 ug/L 8260B230Trichloroethene

0.50 mg/L 300.00.38 JFluoride

280-64994-6 RD-39B_020315_01

100 ug/L 8260B51 JIsopropanol

0.50 mg/L 300.00.47 JFluoride

0.100 SU 9040B8.33 HFpH adj. to 25 deg C

50 ug/L 8315A7.8 J BFormaldehyde

280-64994-11 RD-78_020315_01

2.0 ug/L 8260B SIM9.1 *1,4-Dioxane


METHOD SUMMARY


Preparation MethodMethodLab LocationDescription

Matrix: Water

Volatile Organic Compounds (GC/MS) TAL DEN SW846 8260B

Purge and Trap TAL DEN SW846 5030B

Volatile Organic Compounds (GC/MS) TAL DEN SW846 8260B SIM


Semivolatile Organic Compounds (GC/MS) TAL DEN SW846 8270C

Liquid-Liquid Extraction (Continuous) TAL DEN SW846 3520C

Semivolatile Organic Compound (GC/MS SIM LL) TAL DEN SW846 8270D SIM

Liquid-Liquid Extraction (Continuous) TAL DEN SW846 3520C

Gasoline Range Organics - (GC) TAL DEN SW846 8015B


Diesel Range Organics TAL DEN SW846 8015B

Liquid-Liquid Extraction (Separatory Funnel) TAL DEN SW846 3510C

Silica Gel Cleanup TAL DEN SW846 3630M

Perchlorate by IC/MS or IC/MS/MS TAL DEN EPA 6860

Anions, Ion Chromatography TAL DEN MCAWW 300.0

Nitrogen, Ammonia TAL DEN MCAWW 350.1

pH TAL DEN SW846 9040B

Hydrazine by Ion Chromatography TAL DEN TAL-DEN DV-WC-0077

Sample Filtration TAL DEN TestAmerica SOP Filtration

Carbonyl Compounds (HPLC) TAL CAN SW846 8315A

Solid-Phase Extraction (SPE) TAL CAN SW846 8315_W_Prep

Volatile Organic Compounds (GC/MS SIM) TAL IRV CADHS 524.2M_CA-SRL

Perchlorate (IC) TAL IRV EPA 314.0 LL

Lab References:

TAL CAN = TestAmerica Canton

TAL DEN = TestAmerica Denver

TAL IRV = TestAmerica Irvine

Method References:

CADHS = California Department of Health Services

EPA = US Environmental Protection Agency

MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its

Updates.

TAL-DEN = TestAmerica Laboratories, Denver, Facility Standard Operating Procedure.

TestAmerica SOP = TestAmerica, Inc., Standard Operating Procedure


METHOD / ANALYST SUMMARY


Method Analyst Analyst ID

Farag, Mina MFCADHS 524.2M_CA-SRL

Kwong, Gina GKCADHS 524.2M_CA-SRL

Berger, Brent B BBBSW846 8260B

Lines, Jeremy N JNLSW846 8260B

Moan, Matthew R MRMSW846 8260B SIM

Kiekel, Daniel C DCKSW846 8270C

Vasquez, Karla G KGVSW846 8270D SIM

Redman, Erin E EERSW846 8015B

Moore, Tegan E TEMSW846 8015B

Fiedler, Heather K HKFEPA 6860

Benson, Alex F AFBMCAWW 300.0

Newcome, Robin S RSNMCAWW 350.1

Simons, Nicole A NASSW846 9040B

Smith, Matthew P MPSTAL-DEN DV-WC-0077

Hoang, Christina chEPA 314.0 LL

Colon, Olguita OCRSW846 8315A

TestAmerica Denver

02/18/2015Page 8 of 101

Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111

Date Received: 02/04/2015 1000

524.2M_CA-SRL Volatile Organic Compounds (GC/MS SIM)

Dilution:

02/09/2015 1828

1.0

524.2M_CA-SRL

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID:

D0209011.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-234998

N/A

N/A

Analysis Method:

Analyte Result (ug/L) Qualifier MDL RL

0.0017 U 0.00500.00171,2,3-Trichloropropane


Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-32_020315

Client Matrix:

280-64994-4TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/09/2015 1859

1.0

524.2M_CA-SRL



Lab File ID:

Instrument ID:

D0209012.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-234998

N/A

N/A

Analysis Method:




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-60_020315_01

Client Matrix:

280-64994-5

Water

Date Sampled: 02/03/2015 0933



Dilution:

02/10/2015 1648

2.5

524.2M_CA-SRL



Lab File ID:

Instrument ID:

D0210011.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-235281

N/A

N/A

Analysis Method:


0.030 0.0130.00431,2,3-Trichloropropane


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008



Dilution:

02/09/2015 2002

1.0

524.2M_CA-SRL



Lab File ID:

Instrument ID:

D0209014.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-234998

N/A

N/A

Analysis Method:




Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-39B_020315

Client Matrix:

280-64994-9TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/10/2015 1719

1.0

524.2M_CA-SRL



Lab File ID:

Instrument ID:

D0210012.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-235281

N/A

N/A

Analysis Method:




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-78_020315_01

Client Matrix:

280-64994-11

Water

Date Sampled: 02/03/2015 1334



Dilution:

02/10/2015 1750

1.0

524.2M_CA-SRL



Lab File ID:

Instrument ID:

D0210013.D

25 mL

25 mL

N/A

GCMS74

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-235281

N/A

N/A

Analysis Method:




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111


8260B Volatile Organic Compounds (GC/MS)

Dilution:

02/05/2015 0020

02/05/2015 0020

1.0

8260B



Lab File ID:

Instrument ID:

R2757.D

20 mL

20 mL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:


0.16 U 1.00.161,1,1-Trichloroethane


0.42 U 5.00.421,1,2-Trichloro-1,2,2-trifluoroethane

0.22 U 1.00.221,1-Dichloroethane

0.23 U 1.00.231,1-Dichloroethene


1.9 U 101.9Acetone

0.16 U 1.00.16Benzene

0.19 U 1.00.19Carbon tetrachloride

0.16 U 1.00.16Chloroform

0.15 U 1.00.15cis-1,2-Dichloroethene

0.16 U 1.00.16Ethylbenzene

2.0 U 102.0Methyl ethyl ketone (MEK)

0.32 U 5.00.32Methylene Chloride

0.34 U 2.00.34m-Xylene & p-Xylene

0.19 U 1.00.19o-Xylene

0.20 U 1.00.20Tetrachloroethene

0.17 U 1.00.17Toluene

0.15 U 1.00.15trans-1,2-Dichloroethene

0.16 U 1.00.16Trichloroethene

0.29 U 1.00.29Trichlorofluoromethane

0.10 U 1.00.10Vinyl chloride

Surrogate %Rec Acceptance LimitsQualifier

95 70 - 1271,2-Dichloroethane-d4 (Surr)

101 78 - 1204-Bromofluorobenzene (Surr)

91 77 - 120Dibromofluoromethane (Surr)

97 80 - 125Toluene-d8 (Surr)


Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-32_020315

Client Matrix:

280-64994-4TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/05/2015 0040

02/05/2015 0040

1.0

8260B



Lab File ID:

Instrument ID:

R2758.D

20 mL

20 mL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene








0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene











Analytical Data


Client Sample ID:

Lab Sample ID:

RD-60_020315_01

Client Matrix:

280-64994-5

Water

Date Sampled: 02/03/2015 0933



Dilution:

02/05/2015 0100

02/05/2015 0100

1.0

8260B



Lab File ID:

Instrument ID:

R2759.D

20 mL

20 mL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:



0.28 J 1.00.271,1,2-Trichloroethane


2.3 1.00.221,1-Dichloroethane

1.7 1.00.231,1-Dichloroethene

2.3 0.500.131,2-Dichloroethane

1.9 U 101.9Acetone

0.16 U 1.00.16Benzene


0.29 J 1.00.16Chloroform

14 1.00.15cis-1,2-Dichloroethene





0.19 U 1.00.19o-Xylene


0.19 J 1.00.17Toluene

0.45 J 1.00.15trans-1,2-Dichloroethene









Analytical Data


Client Sample ID:

Lab Sample ID:

RD-60_020315_01

Client Matrix:

280-64994-5

Water

Date Sampled: 02/03/2015 0933



Dilution:

02/05/2015 0120

02/05/2015 0120

1.0

8260B



Lab File ID:

Instrument ID:

R2760.D

2 mL

20 mLRun Type: DL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:


230 101.6Trichloroethene







Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008



Dilution:

02/05/2015 2237

02/05/2015 2237

1.0

8260B



Lab File ID:

Instrument ID:

P0670.D

20 mL

20 mL

5030B

VMS_P

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263200

N/A

Analysis Method:

Prep Method:








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene





51 J 10013Isopropanol




0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene











Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-39B_020315

Client Matrix:

280-64994-9TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/05/2015 2257

02/05/2015 2257

1.0

8260B



Lab File ID:

Instrument ID:

P0671.D

20 mL

20 mL

5030B

VMS_P

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263200

N/A

Analysis Method:

Prep Method:








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene





13 U 10013Isopropanol




0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene











Analytical Data


Client Sample ID:

Lab Sample ID:

RD-66_020315_01

Client Matrix:

280-64994-10

Water

Date Sampled: 02/03/2015 1201



Dilution:

02/05/2015 0219

02/05/2015 0219

1.0

8260B



Lab File ID:

Instrument ID:

R2763.D

20 mL

20 mL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene








0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene











Analytical Data


Client Sample ID:

Lab Sample ID:

RD-78_020315_01

Client Matrix:

280-64994-11

Water

Date Sampled: 02/03/2015 1334



Dilution:

02/05/2015 0239

02/05/2015 0239

1.0

8260B



Lab File ID:

Instrument ID:

R2764.D

20 mL

20 mL

5030B

VMS_R1

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263047

N/A

Analysis Method:

Prep Method:








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene








0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene











Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111


8260B SIM Volatile Organic Compounds (GC/MS)

Dilution:

02/06/2015 0907

02/06/2015 0907

1.0

8260B SIM



Lab File ID:

Instrument ID:

E7464.D

20 mL

20 mL

5030B

VMS_E

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263242

N/A

Analysis Method:

Prep Method:


0.22 U * 2.00.221,4-Dioxane




Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-32_020315

Client Matrix:

280-64994-4TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/06/2015 1216

02/06/2015 1216

1.0

8260B SIM



Lab File ID:

Instrument ID:

E7474.D

20 mL

20 mL

5030B

VMS_E

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263242

N/A

Analysis Method:

Prep Method:


0.22 U * 2.00.221,4-Dioxane




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008



Dilution:

02/06/2015 1235

02/06/2015 1235

1.0

8260B SIM



Lab File ID:

Instrument ID:

E7475.D

20 mL

20 mL

5030B

VMS_E

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263242

N/A

Analysis Method:

Prep Method:


0.22 U * 2.00.221,4-Dioxane




Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-39B_020315

Client Matrix:

280-64994-9TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

02/06/2015 1253

02/06/2015 1253

1.0

8260B SIM



Lab File ID:

Instrument ID:

E7476.D

20 mL

20 mL

5030B

VMS_E

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263242

N/A

Analysis Method:

Prep Method:


0.22 U * 2.00.221,4-Dioxane




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-78_020315_01

Client Matrix:

280-64994-11

Water

Date Sampled: 02/03/2015 1334



Dilution:

02/06/2015 1312

02/06/2015 1312

1.0

8260B SIM



Lab File ID:

Instrument ID:

E7477.D

20 mL

20 mL

5030B

VMS_E

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263242

N/A

Analysis Method:

Prep Method:


9.1 * 2.00.221,4-Dioxane




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008


8270C Semivolatile Organic Compounds (GC/MS)

Dilution:

02/09/2015 1535

02/12/2015 1638

1.0

8270C

Injection Volume:



Lab File ID:

Instrument ID:

K10187.D

1055.3 mL

1 mL

0.5 uL

3520C

SMS_K

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-264097

280-263603

Analysis Method:

Prep Method:


1.9 U 9.51.91,3-Dinitrobenzene

0.53 U 9.50.53Bis(2-ethylhexyl) phthalate

0.95 U 9.50.95Butyl benzyl phthalate

0.36 U 9.50.36Diethyl phthalate

0.20 U 9.50.20Dimethyl phthalate

1.1 U 9.51.1Di-n-butyl phthalate

0.33 U 9.50.33Di-n-octyl phthalate

0.77 U 9.50.77Nitrobenzene


72 48 - 1352,4,6-Tribromophenol

83 48 - 1352-Fluorobiphenyl

84 41 - 1352-Fluorophenol

86 42 - 135Nitrobenzene-d5

88 46 - 135Phenol-d5

90 20 - 135Terphenyl-d14


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111


8270D SIM Semivolatile Organic Compound (GC/MS SIM LL)

Dilution:

02/07/2015 0952

02/12/2015 1007

1.0

8270D SIM

Injection Volume:



Lab File ID:

Instrument ID:

G5_4267.D

1005.9 mL

1 mL

5 uL

3520C

SMS_G5

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-264019

280-263420

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier RL

ND U 0.0050N-Nitrosodimethylamine


112 18 - 142N-Nitrosodimethylamine-d6 (Surr)


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008



Dilution:

02/07/2015 0952

02/12/2015 1028

1.0

8270D SIM

Injection Volume:



Lab File ID:

Instrument ID:

G5_4268.D

1053.6 mL

1 mL

5 uL

3520C

SMS_G5

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-264019

280-263420

Analysis Method:

Prep Method:






Analytical Data


Client Sample ID:

Lab Sample ID:

RD-78_020315_01

Client Matrix:

280-64994-11

Water

Date Sampled: 02/03/2015 1334



Dilution:

02/07/2015 0952

02/12/2015 1049

1.0

8270D SIM

Injection Volume:



Lab File ID:

Instrument ID:

G5_4269.D

990.6 mL

1 mL

5 uL

3520C

SMS_G5

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-264019

280-263420

Analysis Method:

Prep Method:






Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111


8015B Gasoline Range Organics - (GC)

Dilution:

8015B

5030B

1.0

02/05/2015 1637

02/05/2015 1637

Instrument ID:



Injection Volume:

Result Type: PRIMARY

5 mL

5 mL

5 mL

VGC_Q

Analysis Date:

Prep Date:

Analysis Batch: 280-263126

N/A

Analysis Method:

Prep Method:


10 U 10010C6-C12


89 82 - 110a,a,a-Trifluorotoluene


Analytical Data


Client Sample ID:

Lab Sample ID:

TB_RD-32_020315

Client Matrix:

280-64994-4TB

Water

Date Sampled: 02/03/2015 0700



Dilution:

8015B

5030B

1.0

02/05/2015 1702

02/05/2015 1702

Instrument ID:



Injection Volume:


5 mL

5 mL

5 mL

VGC_Q

Analysis Date:

Prep Date:


N/A

Analysis Method:

Prep Method:


10 U 10010C6-C12


87 82 - 110a,a,a-Trifluorotoluene


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008


8015B Diesel Range Organics

Dilution:

8015B

3510C

1.0

02/11/2015 1451

02/09/2015 2141

Instrument ID:



Injection Volume:


1037.2 mL

1 mL

1 uL

SGC_U2a

Analysis Date:

Prep Date:


280-263658Prep Batch:

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

0.096 U 0.240.096C12-C14

0.096 U 0.240.096C15-C20

0.096 U 0.240.096C8-C11

0.096 U 0.240.096C8-C30

0.096 U 0.240.096C21-C30


94 50 - 115o-Terphenyl


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-78_020315_01

Client Matrix:

280-64994-11

Water

Date Sampled: 02/03/2015 1334


314.0 LL Perchlorate (IC)

Dilution:

02/17/2015 1509

1.0

314.0 LL

Injection Volume:



Lab File ID:

Instrument ID:

20150217_23.d

1 mL

1 uL

N/A

IC-24

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

440-236706

N/A

N/A

Analysis Method:


0.50 U 2.00.50Perchlorate


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008


8315A Carbonyl Compounds (HPLC)

Dilution:

02/05/2015 0810

02/06/2015 1045

1.0

8315A

Injection Volume:



Lab File ID:

Instrument ID:

L1020617.D

100 mL

5 mL

10 uL

8315_W_Prep

A2HPL2

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

240-167018

240-166845

Analysis Method:

Prep Method:


7.8 J B 505.0Formaldehyde


Analytical Data


Client Sample ID:

Lab Sample ID:

RD-32_020315_01

Client Matrix:

280-64994-1

Water

Date Sampled: 02/03/2015 1111


6860 Perchlorate by IC/MS or IC/MS/MS

Dilution:

02/10/2015 1434

1.0

6860

Injection Volume:



Lab File ID:

Instrument ID:

IC215B10009.d

5 mL

250 uL

N/A

LC_LCMS2

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263734

N/A

N/A

Analysis Method:




Analytical Data


Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008


6860 Perchlorate by IC/MS or IC/MS/MS

Dilution:

02/10/2015 1503

1.0

6860

Injection Volume:



Lab File ID:

Instrument ID:

IC215B10010.d

5 mL

250 uL

N/A

LC_LCMS2

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

280-263734

N/A

N/A

Analysis Method:




Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

RD-60_020315_01

Client Matrix:

280-64994-5

Water

Date Sampled: 02/03/2015 0933


Analyte Result Qual Units MDL RL Dil Method

Fluoride 0.38 J mg/L 0.060 0.50 1.0 300.0

Analysis Date: 02/04/2015 1941Analysis Batch: 280-262933


Analytical Data


General Chemistry

Client Sample ID:

Lab Sample ID:

RD-39B_020315_01

Client Matrix:

280-64994-6

Water

Date Sampled: 02/03/2015 1008


Analyte Result Qual Units MDL RL Dil Method

Fluoride 0.47 J mg/L 0.060 0.50 1.0 300.0


Nitrate as NO3 0.19 U mg/L 0.19 2.5 1.0 300.0


Ammonia 0.022 U mg/L 0.022 0.50 1.0 350.1


1,1-Dimethylhydrazine 1.9 U ug/L 1.9 10 1.0 DV-WC-0077


Prep Batch: 280-263039 Prep Date: 02/04/2015 1940

Hydrazine 0.67 U ug/L 0.67 5.0 1.0 DV-WC-0077



Monomethyl Hydrazine 0.25 U ug/L 0.25 10 1.0 DV-WC-0077



Analyte Result Qual Units RL RL Dil Method

pH adj. to 25 deg C 8.33 HF SU 0.100 0.100 1.0 9040B



Quality Control Results

Job Number: 280-64994-1Client: MWH Americas Inc

Surrogate Recovery Report


Client Matrix: Water


DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

280-64994-1 RD-32_020315_01 91 95 97 101

280-64994-4 TB_RD-32_020315 88 92 88 99

280-64994-5 RD-60_020315_01 87 93 90 100

280-64994-5 DL RD-60_020315_01

DL

92 99 100 99

280-64994-6 RD-39B_020315_01 102 87 99 98

280-64994-9 TB_RD-39B_020315 102 89 98 98

280-64994-10 RD-66_020315_01 93 98 92 101

280-64994-11 RD-78_020315_01 95 100 92 102

MB 280-263047/6 79 83 82 90

MB 280-263200/8 100 87 98 99

LCS 280-263047/4 87 92 90 90

LCS 280-263200/6 105 92 108 102

LCSD 280-263047/5 87 92 88 91

LCSD 280-263200/7 97 85 99 92

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane (Surr) 77-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-127

TOL = Toluene-d8 (Surr) 80-125

BFB = 4-Bromofluorobenzene (Surr) 78-120

TestAmerica Denver

02/18/2015Page 41 of 101







DCA

%Rec

280-64994-1 RD-32_020315_01 93

280-64994-4 TB_RD-32_020315 96

280-64994-6 RD-39B_020315_01 96

280-64994-9 TB_RD-39B_020315 94

280-64994-11 RD-78_020315_01 97

MB 280-263242/5 95

LCS 280-263242/3 101

LCSD 280-263242/4 97

280-64994-1 MS RD-32_020315_01

MS

94

280-64994-1 MSD RD-32_020315_01

MSD

97


DCA = 1,2-Dichloroethane-d4 (Surr) 70-127

TestAmerica Denver

02/18/2015Page 42 of 101




8270C Semivolatile Organic Compounds (GC/MS)



2FP PHL NBZ FBP TBP TPH

%Rec %Rec %Rec %Rec %Rec %Rec

280-64994-6 RD-39B_020315_01 84 88 86 83 72 90

MB 280-263603/1-A 91 94 92 87 83 96

LCS 280-263603/2-A 80 82 84 85 79 84

LCSD

280-263603/3-A

79 80 80 80 75 82


2FP = 2-Fluorophenol 41-135

PHL = Phenol-d5 46-135

NBZ = Nitrobenzene-d5 42-135

FBP = 2-Fluorobiphenyl 48-135

TBP = 2,4,6-Tribromophenol 48-135

TPH = Terphenyl-d14 20-135

TestAmerica Denver

02/18/2015Page 43 of 101







DMA (S)

%Rec

280-64994-1 RD-32_020315_01 112

280-64994-6 RD-39B_020315_01 118

280-64994-11 RD-78_020315_01 110

MB 280-263420/1-A 113

LCS 280-263420/2-A 119

LCSD

280-263420/3-A

114


DMA (S) = N-Nitrosodimethylamine-d6 (Surr) 18-142

TestAmerica Denver

02/18/2015Page 44 of 101







TFT1

%Rec

280-64994-1 RD-32_020315_01 89

280-64994-4 TB_RD-32_020315 87

MB 280-263126/4 82

LCS 280-263126/5 82

LCSD 280-263126/21 90


TFT = a,a,a-Trifluorotoluene 82-110

TestAmerica Denver

02/18/2015Page 45 of 101




8015B Diesel Range Organics



OTPH1

%Rec

280-64994-6 RD-39B_020315_01 94

MB 280-263658/1-B 96

LCS 280-263658/2-B 93

LCSD

280-263658/3-B

90


OTPH = o-Terphenyl 50-115

TestAmerica Denver

02/18/2015Page 46 of 101



WaterClient Matrix:

1.0Dilution:

Lab Sample ID:

Method Blank - Batch: 440-234998

Instrument ID:

Lab File ID:



D0209003.D

25 mL

25 mLUnits: ug/L

Method: 524.2M_CA-SRL

Preparation: N/A

GCMS74MB 440-234998/3

Analysis Date: 02/09/2015 1339

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

440-234998

Prep Date:

Leach Date:

N/A

N/A

Analyte RLMDLQualResult


Water

1.0

Lab Control Sample - Batch: 440-234998

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:



D0209002.D

25 mL

25 mLUnits: ug/L


Preparation: N/A

GCMS74LCS 440-234998/2


Analysis Batch:

Prep Batch:

Leach Batch:

440-234998

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte QualLimit% Rec.ResultSpike Amount

0.00500 0.00433 87 J80 - 1201,2,3-Trichloropropane




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



D0210003.D

25 mL

25 mLUnits: ug/L


Preparation: N/A

GCMS74MB 440-235281/3


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

440-235281

Prep Date:

Leach Date:

N/A

N/A



Water

1.0

Lab Control Sample - Batch: 440-235281

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:



D0210002.D

25 mL

25 mLUnits: ug/L


Preparation: N/A

GCMS74LCS 440-235281/2


Analysis Batch:

Prep Batch:

Leach Batch:

440-235281

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte QualLimit% Rec.ResultSpike Amount

0.00500 0.00561 112 80 - 1201,2,3-Trichloropropane




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



R2751.D

20 mL

20 mLUnits: ug/L

Method: 8260B

Preparation: 5030B

VMS_R1MB 280-263047/6


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

280-263047

Prep Date:

Leach Date:

02/04/2015 2216

N/A








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene








0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene





Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 83 70 - 127

4-Bromofluorobenzene (Surr) 90 78 - 120

Dibromofluoromethane (Surr) 79 77 - 120

Toluene-d8 (Surr) 82 80 - 125




Dilution:

Dilution:

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 280-263047

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:




Units:

Instrument ID:

Lab File ID:



ug/L

R2749.D

20 mL

20 mL

20 mL

R2750.D

20 mL

20 mL

20 mL

ug/L

Method: 8260B

Preparation: 5030B

VMS_R1

VMS_R1

LCS 280-263047/4

LCSD 280-263047/5

Analysis Date:

Prep Date:

Leach Date:

02/04/2015 2137

02/04/2015 2137

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263047

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

02/04/2015 2156

02/04/2015 2156

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263047

N/A

N/A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

101102 65 - 135 1 201,1,1-Trichloroethane

98100 65 - 140 1 20 J J1,1,2-Trichloro-1,2,2-trifluoroethane


112111 65 - 135 0 211,1-Dichloroethane

10199 65 - 136 1 201,1-Dichloroethene

109105 65 - 135 3 201,2-Dichloroethane

9488 39 - 156 6 23Acetone

9897 65 - 135 1 20Benzene

103101 65 - 135 2 21Carbon tetrachloride

105105 65 - 135 0 20Chloroform

9799 65 - 135 2 20cis-1,2-Dichloroethene

9596 65 - 135 1 20Ethylbenzene

11099 44 - 177 10 32Methyl ethyl ketone (MEK)

102101 54 - 141 0 26Methylene Chloride

9394 65 - 135 0 20m-Xylene & p-Xylene

9496 65 - 135 2 20o-Xylene

9495 65 - 135 0 20Tetrachloroethene

9898 65 - 135 1 20Toluene

106107 65 - 135 1 24trans-1,2-Dichloroethene

10098 65 - 135 2 20Trichloroethene

117121 53 - 137 3 27Trichlorofluoromethane

119120 40 - 137 1 24Vinyl chloride

Surrogate LCS % Rec LCSD % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 92 92 70 - 127

4-Bromofluorobenzene (Surr) 90 91 78 - 120

Dibromofluoromethane (Surr) 87 87 77 - 120

Toluene-d8 (Surr) 90 88 80 - 125




Water

02/04/2015 2137

Dilution: Dilution:1.0 1.0

Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/

Laboratory Duplicate Data Report - Batch: 280-263047

Method: 8260B

Preparation: 5030B

Units: ug/LLCS 280-263047/4 LCSD 280-263047/5LCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

02/04/2015 2137

Analysis Date:

Prep Date:

Leach Date:

02/04/2015 2156

02/04/2015 2156

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

5.065.125.00 5.001,1,1-Trichloroethane

J J4.924.985.00 5.001,1,2-Trichloro-1,2,2-trifluoroethane


5.595.565.00 5.001,1-Dichloroethane

5.044.975.00 5.001,1-Dichloroethene


18.817.620.0 20.0Acetone

4.914.845.00 5.00Benzene

5.155.045.00 5.00Carbon tetrachloride

5.255.255.00 5.00Chloroform

4.844.935.00 5.00cis-1,2-Dichloroethene

4.764.825.00 5.00Ethylbenzene

22.019.920.0 20.0Methyl ethyl ketone (MEK)

5.085.075.00 5.00Methylene Chloride

4.674.685.00 5.00m-Xylene & p-Xylene

4.704.795.00 5.00o-Xylene

4.724.735.00 5.00Tetrachloroethene

4.924.905.00 5.00Toluene

5.305.375.00 5.00trans-1,2-Dichloroethene

4.994.915.00 5.00Trichloroethene

5.846.035.00 5.00Trichlorofluoromethane

5.976.025.00 5.00Vinyl chloride




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



P0663.D

20 mL

20 mLUnits: ug/L

Method: 8260B

Preparation: 5030B

VMS_PMB 280-263200/8


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

280-263200

Prep Date:

Leach Date:

02/05/2015 2019

N/A








1.9 U 101.9Acetone

0.16 U 1.00.16Benzene





13 U 10013Isopropanol


0.769 J 5.00.32Methylene Chloride


0.19 U 1.00.19o-Xylene


0.17 U 1.00.17Toluene







4-Bromofluorobenzene (Surr) 99 78 - 120

Dibromofluoromethane (Surr) 100 77 - 120

Toluene-d8 (Surr) 98 80 - 125




Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:




Units:

Instrument ID:

Lab File ID:



ug/L

P0661.D

20 mL

20 mL

20 mL

P0662.D

20 mL

20 mL

20 mL

ug/L

Method: 8260B

Preparation: 5030B

VMS_P

VMS_P

LCS 280-263200/6

LCSD 280-263200/7

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1939

02/05/2015 1939

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263200

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1959

02/05/2015 1959

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263200

N/A

N/A


% Rec.


121132 65 - 140 8 201,1,2-Trichloro-1,2,2-trifluoroethane


97108 65 - 135 11 211,1-Dichloroethane

118131 65 - 136 11 201,1-Dichloroethene

8695 65 - 135 10 201,2-Dichloroethane

7072 39 - 156 3 23Acetone

103114 65 - 135 10 20Benzene

92103 65 - 135 11 21Carbon tetrachloride

91101 65 - 135 11 20Chloroform

106118 65 - 135 10 20cis-1,2-Dichloroethene

104117 65 - 135 12 20Ethylbenzene

10597 44 - 177 8 32Methyl ethyl ketone (MEK)

118127 54 - 141 8 26Methylene Chloride

109119 65 - 135 8 20m-Xylene & p-Xylene

105116 65 - 135 10 20o-Xylene

110122 65 - 135 10 20Tetrachloroethene

107120 65 - 135 11 20Toluene

111123 65 - 135 10 24trans-1,2-Dichloroethene

102114 65 - 135 12 20Trichloroethene

7684 53 - 137 9 27Trichlorofluoromethane

8694 40 - 137 9 24Vinyl chloride



4-Bromofluorobenzene (Surr) 102 92 78 - 120

Dibromofluoromethane (Surr) 105 97 77 - 120

Toluene-d8 (Surr) 108 99 80 - 125




Water

02/05/2015 1939


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8260B

Preparation: 5030B


Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1939

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1959

02/05/2015 1959

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte


6.056.595.00 5.001,1,2-Trichloro-1,2,2-trifluoroethane



5.906.575.00 5.001,1-Dichloroethene


14.114.520.0 20.0Acetone

5.155.715.00 5.00Benzene

4.615.165.00 5.00Carbon tetrachloride

4.535.055.00 5.00Chloroform

5.325.885.00 5.00cis-1,2-Dichloroethene

5.205.835.00 5.00Ethylbenzene

21.119.420.0 20.0Methyl ethyl ketone (MEK)

5.886.345.00 5.00Methylene Chloride

5.465.935.00 5.00m-Xylene & p-Xylene

5.255.825.00 5.00o-Xylene

5.516.125.00 5.00Tetrachloroethene

5.375.985.00 5.00Toluene

5.566.175.00 5.00trans-1,2-Dichloroethene

5.095.715.00 5.00Trichloroethene

3.824.185.00 5.00Trichlorofluoromethane

4.304.705.00 5.00Vinyl chloride




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



E7463.D

20 mL

20 mLUnits: ug/L

Method: 8260B SIM

Preparation: 5030B

VMS_EMB 280-263242/5


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

280-263242

Prep Date:

Leach Date:

02/06/2015 0848

N/A


0.22 U 2.00.221,4-Dioxane



Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:




Units:

Instrument ID:

Lab File ID:



ug/L

E7461.D

20 mL

20 mL

20 mL

E7462.D

20 mL

20 mL

20 mL

ug/L

Method: 8260B SIM

Preparation: 5030B

VMS_E

VMS_E

LCS 280-263242/3

LCSD 280-263242/4

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 0811

02/06/2015 0811

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263242

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 0829

02/06/2015 0829

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263242

N/A

N/A


% Rec.

12193 25 - 141 26 20 *1,4-Dioxane






Water

02/06/2015 0811


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8260B SIM

Preparation: 5030B


Analysis Date:

Prep Date:

Leach Date:

02/06/2015 0811

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 0829

02/06/2015 0829

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

*6.054.665.00 5.001,4-Dioxane

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:



Instrument ID:

Lab File ID:




E7466.D

20 mL

20 mL

20 mL

E7467.D

20 mL

20 mL

20 mL

Method: 8260B SIM

Preparation: 5030B

VMS_E

VMS_E

280-64994-1

280-64994-1

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 280-263242

02/06/2015 0948

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

280-263242

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 1006

02/06/2015 1006

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263242

N/A

N/A

02/06/2015 0948

Analyte RPD LimitRPDLimit

% Rec.

MS MSD MS Qual MSD Qual

95 113 25 - 141 18 201,4-Dioxane

Surrogate Acceptance LimitsMS % Rec MSD % Rec





Water

02/06/2015 0948 02/06/2015 1006


Client Matrix: Client Matrix: Water

Method: 8260B SIM

Preparation: 5030B

Units: ug/L280-64994-1 280-64994-1MS Lab Sample ID: MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 280-263242

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 0948

N/A

Analysis Date:

Prep Date:

Leach Date:

02/06/2015 1006

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS MSDMS Spike MSD Spike

0.22 U 5.00 5.00 4.74 5.671,4-Dioxane




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



K10178.D

1000 mL

1 mLUnits: ug/L

Method: 8270C

Preparation: 3520C

SMS_KMB 280-263603/1-A


Analysis Batch:

Prep Batch:

Leach Batch: N/A

280-264097

280-263603

Prep Date: Injection Volume: 0.5 uL

Leach Date:

02/09/2015 1535

N/A


2.0 U 102.01,3-Dinitrobenzene

0.56 U 100.56Bis(2-ethylhexyl) phthalate

1.0 U 101.0Butyl benzyl phthalate

0.38 U 100.38Diethyl phthalate

0.21 U 100.21Dimethyl phthalate

1.2 U 101.2Di-n-butyl phthalate

0.35 U 100.35Di-n-octyl phthalate

0.81 U 100.81Nitrobenzene


2,4,6-Tribromophenol 83 48 - 135

2-Fluorobiphenyl 87 48 - 135

2-Fluorophenol 91 41 - 135

Nitrobenzene-d5 92 42 - 135

Phenol-d5 94 46 - 135

Terphenyl-d14 96 20 - 135




Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

K10179.D

1000 mL

1 mL

0.5 uL

K10180.D

1000 mL

1 mL

0.5 uL

ug/L

Method: 8270C

Preparation: 3520C

SMS_K

SMS_K

LCS 280-263603/2-A

LCSD 280-263603/3-A

Analysis Date:

Prep Date:

Leach Date:

02/12/2015 1257

02/09/2015 1535

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-264097

280-263603

N/A

Analysis Date:

Prep Date:

Leach Date:

02/12/2015 1324

02/09/2015 1535

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-264097

280-263603

N/A


% Rec.

9093 65 - 135 3 30Bis(2-ethylhexyl) phthalate

8791 65 - 135 4 30Butyl benzyl phthalate

8690 65 - 135 5 30Diethyl phthalate

8691 65 - 135 5 30Dimethyl phthalate

8790 65 - 135 3 30Di-n-butyl phthalate

8488 65 - 135 4 30Di-n-octyl phthalate

8188 65 - 135 8 39Nitrobenzene


2,4,6-Tribromophenol 79 75 48 - 135

2-Fluorobiphenyl 85 80 48 - 135

2-Fluorophenol 80 79 41 - 135

Nitrobenzene-d5 84 80 42 - 135

Phenol-d5 82 80 46 - 135

Terphenyl-d14 84 82 20 - 135




Water

02/12/2015 1257


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8270C

Preparation: 3520C

Units: ug/LLCS 280-263603/2-A LCSD 280-263603/3-ALCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

02/09/2015 1535

Analysis Date:

Prep Date:

Leach Date:

02/12/2015 1324

02/09/2015 1535

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

72.174.580.0 80.0Bis(2-ethylhexyl) phthalate

69.772.880.0 80.0Butyl benzyl phthalate

68.472.180.0 80.0Diethyl phthalate

69.072.780.0 80.0Dimethyl phthalate

69.872.380.0 80.0Di-n-butyl phthalate

67.470.380.0 80.0Di-n-octyl phthalate

64.970.380.0 80.0Nitrobenzene




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



G5_4254.D

1000 mL

1 mLUnits: ug/L

Method: 8270D SIM

Preparation: 3520C

SMS_G5MB 280-263420/1-A


Analysis Batch:

Prep Batch:

Leach Batch: N/A

280-263708

280-263420

Prep Date: Injection Volume: 5 uL

Leach Date:

02/07/2015 0952

N/A

Analyte RLQualResult



N-Nitrosodimethylamine-d6 (Surr) 113 18 - 142

Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

ug/L

G5_4255.D

1000 mL

1 mL

5 uL

G5_4256.D

1000 mL

1 mL

5 uL

ug/L

Method: 8270D SIM

Preparation: 3520C

SMS_G5

SMS_G5

LCS 280-263420/2-A

LCSD 280-263420/3-A

Analysis Date:

Prep Date:

Leach Date:

02/10/2015 1725

02/07/2015 0952

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263708

280-263420

N/A

Analysis Date:

Prep Date:

Leach Date:

02/10/2015 1746

02/07/2015 0952

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263708

280-263420

N/A


% Rec.

7272 68 - 124 0 30N-Nitrosodimethylamine


N-Nitrosodimethylamine-d6 (Surr) 119 114 18 - 142




Water

02/10/2015 1725


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8270D SIM

Preparation: 3520C

Units: ug/LLCS 280-263420/2-A LCSD 280-263420/3-ALCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

02/07/2015 0952

Analysis Date:

Prep Date:

Leach Date:

02/10/2015 1746

02/07/2015 0952

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

0.01800.01790.0250 0.0250N-Nitrosodimethylamine




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



004F0401.D

5 mL

5 mLUnits: ug/L

Method: 8015B

Preparation: 5030B

VGC_QMB 280-263126/4


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

280-263126

Prep Date: Injection Volume: 5 mL

Leach Date:

02/05/2015 1112

N/A PRIMARYColumn ID:


10 U 10010C6-C12


a,a,a-Trifluorotoluene 82 82 - 110

Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

ug/L

005F0501.D

5 mL

5 mL

5 mL

PRIMARY

020F2001.D

5 mL

5 mL

5 mL

PRIMARY

ug/L

Method: 8015B

Preparation: 5030B

VGC_Q

VGC_Q

LCS 280-263126/5

LCSD 280-263126/21

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1137

02/05/2015 1137

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263126

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1752

02/05/2015 1752

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263126

N/A

N/A


% Rec.

9489 79 - 149 6 27 J JC6-C12


a,a,a-Trifluorotoluene 82 90 82 - 110




Water

02/05/2015 1137


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8015B

Preparation: 5030B


Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1137

Analysis Date:

Prep Date:

Leach Date:

02/05/2015 1752

02/05/2015 1752

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

J J95.089.3101 101C6-C12




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



02110007.D

1000 mL

1 mLUnits: mg/L

Method: 8015B

Preparation: 3510C

SGC_U2aMB 280-263658/1-B


Analysis Batch:

Prep Batch:

Leach Batch: N/A

280-263879

280-263658


Leach Date:

02/09/2015 1951

N/A PRIMARYColumn ID:


0.10 U 0.250.10C12-C14

0.10 U 0.250.10C15-C20

0.10 U 0.250.10C8-C11

0.10 U 0.250.10C8-C30

0.10 U 0.250.10C21-C30


o-Terphenyl 96 50 - 115

Dilution:

Dilution:

Lab Control Sample/


1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:


Units:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

mg/L

02110008.D

1000 mL

1 mL

1 uL

PRIMARY

02110009.D

1000 mL

1 mL

1 uL

PRIMARY

mg/L

Method: 8015B

Preparation: 3510C

SGC_U2a

SGC_U2a

LCS 280-263658/2-B

LCSD 280-263658/3-B

Analysis Date:

Prep Date:

Leach Date:

02/11/2015 1338

02/09/2015 1951

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263879

280-263658

N/A

Analysis Date:

Prep Date:

Leach Date:

02/11/2015 1402

02/09/2015 1951

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

280-263879

280-263658

N/A


% Rec.

94104 24 - 115 10 30C12-C14

103109 69 - 115 6 30C15-C20

7078 10 - 115 11 30C8-C11

100105 80 - 120 5 30C8-C30

108109 75 - 115 1 30C21-C30


o-Terphenyl 93 90 50 - 115




Water

02/11/2015 1338


Client Matrix:

LCSD Lab Sample ID:


Laboratory Control/


Method: 8015B

Preparation: 3510C

Units: mg/LLCS 280-263658/2-B LCSD 280-263658/3-BLCS Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

02/09/2015 1951

Analysis Date:

Prep Date:

Leach Date:

02/11/2015 1402

02/09/2015 1951

N/AN/A

LCSD

Result/Qual

LCS

Result/Qual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

0.7060.7770.750 0.750C12-C14

1.151.221.13 1.13C15-C20

0.2610.2920.375 0.375C8-C11

3.753.943.75 3.75C8-C30

1.621.641.50 1.50C21-C30




WaterClient Matrix:

1.0Dilution:

Lab Sample ID:


Instrument ID:

Lab File ID:



20150217_3.d

1 mL

Units: ug/L

Method: 314.0 LL

Preparation: N/A

IC-24MB 440-236706/3


Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

440-236706
