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6500 Sunplex Drive
Ocean Springs, MS 39564
228.875.6420 Phone
228.875.6423 Fax
LELAP Certification # 01960
MS Department of Environmental Quality
RE: Deepwater Horizon
Pearl, MS 39208
1542 Old Whitfield Road
Henry Folmar
Enclosed are Micro-Methods Laboratory, Inc. results of analyses performed on samples received
07/10/10 08:37. If you have any questions concerning this report, please feel free to contact the office.
Sincerely,
July 14, 2010
Harry P. Howell
President
Work Order # : 1007119
Purchase Order #: Deepwater Horizon
Micro-Methods Laboratory, Inc.
DISCLAIMER
The results only relate to the items or the sample and/or samples received by the laboratory. This report shall not be reproduced except in full,
without the approval of the laboratory. All test methods performed meet the requirements of NELAC 2003 Standards. Any variances and/or
deviations specific to this analytical report are referenced in the lab report using qualifiers and detailed explanations found in the case narrative.
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Sample ID Laboratory ID MatrixDate/Time Sampled
ANALYTICAL REPORT FOR SAMPLES
Date/Time Received
Sampled by
Biloxi Beach Waste Dumpster 1007119-01 Solid 07/09/10 11:30 07/10/10 08:37David Peacock
Sample Receipt Conditions
7/10/2010 8:37:00AM
Aaron Summerfield
7/10/2010 9:56:00AM Aaron Summerfield
Shipped by:Date/Time Received:
Received by:
Date/Time Logged: Logged by:
Gary HowardSubmitted by:
Default Cooler
Custody Seals
Containers Intact
COC/Labels Agree
Labels Complete
COC Complete
Received on Ice
No Ice, Short Trip
Obvious Contamination
Rush to meet HT
2.10 °C
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
No
Receipt Temperature:Cooler ID:
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 2 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
CASE NARRATIVE SUMMARY
All reported results are within Micro-Methods Laboratory, Inc.defined laboratory quality control objectives unless
detailed in narrative summary or identified as qualifications. NOTE: All results listed on this report are calculated
on a wet weight basis (as received by the laboratory) unless otherwise noted in the analysis qualification sections.
Summary Comments: No Summary Comments
Qualification: No Data Qualification
Analyte & Samples(s) Qualified:
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 3 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
ResultAnalyte MRL Batch
DateTime
Prepared
DateTime
Analyzed Method Notes DilUnits Analyst
Biloxi Beach Waste Dumpster
1007119-01 (Solid)
TCLP Semi-Volatile Organics by 1311/8270
ND 07/12/10
12:22
mg/L 0G120171Cresol(s) 0.050 TKM 07/14/10
13:14
EPA 8270C
ND "" ""1,4-Dichlorobenzene 0.050 TKM " "
ND "" ""2,4-Dinitrotoluene 0.050 TKM " "
ND "" ""Hexachlorobenzene 0.050 TKM " "
ND "" ""Hexachlorobutadiene 0.050 TKM " "
ND "" ""Hexachloroethane 0.050 TKM " "
ND "" ""Nitrobenzene 0.050 TKM " "
ND "" ""Pentachlorophenol 0.050 TKM " "
ND "" ""Pyridine 0.050 TKM " "
ND "" ""2,4,5-Trichlorophenol 0.050 TKM " "
ND "" ""2,4,6-Trichlorophenol 0.050 TKM " "
% Rec Rec Limits Batch
DateTime
Prepared
DateTime
Analyzed Method Notes Surrogate
"" " "10-12082.0 % TKMPhenol-d5 0.410
"" " "10-13197.9 % TKM2,4,6-Tribromophenol 0.489
"" " "10-12582.3 % TKM2-Fluorobiphenyl 0.206
"" " "10-12085.5 % TKM2-Fluorophenol 0.428
"" " "10-13091.7 % TKMNitrobenzene-d5 0.229
"" " "15-13543.8 % TKMTerphenyl-dl4 0.109
TCLP Metals by 1311/6010B
ND 07/12/10
09:00
mg/L 0G120121Arsenic 0.100 AKS 07/13/10
14:40
SW 6010B
ND "" ""Barium 0.100 AKS " "
ND "" ""Cadmium 0.100 AKS " "
ND "" ""Chromium 0.100 AKS " "
ND "" ""Lead 0.100 AKS " "
ND "" ""Selenium 0.100 AKS " "
ND "" ""Silver 0.100 AKS 07/13/10
14:51
"
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 4 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
ResultAnalyte MRL Batch
DateTime
Prepared
DateTime
Analyzed Method Notes DilUnits Analyst
Biloxi Beach Waste Dumpster
1007119-01 (Solid)
TCLP Mercury by 1311/7470A
ND 07/13/10
13:30
mg/L 0G130151Mercury 0.010 AKS 07/13/10
16:41
SW 7470A
TCLP Volatile Organic Compounds by EPA Method 1311/8260B
ND 07/12/10
11:30
mg/L 0G140151Benzene 0.125 KRL 07/12/10
21:00
EPA 8260B
ND "" ""2-Butanone 0.250 KRL " "
ND "" ""Carbon Tetrachloride 0.125 KRL " "
ND "" ""Chlorobenzene 0.125 KRL " "
ND "" ""Chloroform 0.125 KRL " "
ND "" ""1,2-Dichloroethane 0.125 KRL " "
ND "" ""1,1-Dichloroethene 0.125 KRL " "
ND "" ""Tetrachloroethene 0.125 KRL " "
ND "" ""Trichloroethene 0.125 KRL " "
ND "" ""Vinyl chloride 0.125 KRL " "
% Rec Rec Limits Batch
DateTime
Prepared
DateTime
Analyzed Method Notes Surrogate
"" " "83-12896.8 % KRLDibromofluoromethane 1.21
"" " "83.1-126105 % KRL1,2-Dichloroethane-d4 1.31
"" " "82.3-11297.2 % KRLToluene-d8 1.22
"" " "78.4-11492.9 % KRL4-Bromofluorobenzene 1.16
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 5 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Semi-Volatile Organics by 1311/8270 - Quality Control
Batch 0G12017 - EPA 3510C Prepared: 07/12/10 Analyzed: 07/14/10
Blank (0G12017-BLK1)
Cresol(s) mg/LND 0.050
1,4-Dichlorobenzene "ND 0.050
2,4-Dinitrotoluene "ND 0.050
Hexachlorobenzene "ND 0.050
Hexachlorobutadiene "ND 0.050
Hexachloroethane "ND 0.050
Nitrobenzene "ND 0.050
Pentachlorophenol "ND 0.050
Pyridine "ND 0.050
2,4,5-Trichlorophenol "ND 0.050
2,4,6-Trichlorophenol "ND 0.050
" 0.500 10-120Surrogate: Phenol-d5 71.20.356
" 0.500 10-131Surrogate: 2,4,6-Tribromophenol 71.20.356
" 0.250 10-125Surrogate: 2-Fluorobiphenyl 72.80.182
" 0.500 10-120Surrogate: 2-Fluorophenol 69.20.346
" 0.250 10-130Surrogate: Nitrobenzene-d5 80.40.201
" 0.250 15-135Surrogate: Terphenyl-dl4 81.30.203
LCS (0G12017-BS1)
Cresol(s) mg/L1.17 0.050 1.50 3510-12578.0
1,4-Dichlorobenzene "0.324 0.050 0.500 3520-12464.9
2,4-Dinitrotoluene "0.410 0.050 0.500 3539-13981.9
Hexachlorobenzene "0.294 0.050 0.500 3510-15258.9
Hexachlorobutadiene "0.292 0.050 0.500 3524-11658.5
Hexachloroethane "0.336 0.050 0.500 3540-13067.3
Nitrobenzene "0.403 0.050 0.500 3535-18080.6
Pentachlorophenol "0.243 0.050 0.500 3514-17648.7
Pyridine "0.377 0.050 0.500 355-12575.4
2,4,5-Trichlorophenol "0.414 0.050 0.500 3514-13082.7
2,4,6-Trichlorophenol "0.405 0.050 0.500 3537-14481.1
" 0.500 10-120Surrogate: Phenol-d5 71.90.359
" 0.500 10-131Surrogate: 2,4,6-Tribromophenol 90.50.453
" 0.250 10-125Surrogate: 2-Fluorobiphenyl 80.90.202
" 0.500 10-120Surrogate: 2-Fluorophenol 63.10.315
" 0.250 10-130Surrogate: Nitrobenzene-d5 87.70.219
" 0.250 15-135Surrogate: Terphenyl-dl4 86.80.217
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 6 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Semi-Volatile Organics by 1311/8270 - Quality Control
Batch 0G12017 - EPA 3510C Prepared: 07/12/10 Analyzed: 07/14/10
Matrix Spike (0G12017-MS1) Source: 1007119-01
Cresol(s) mg/L1.33 0.050 1.50 ND 405-13588.3
1,4-Dichlorobenzene "0.370 0.050 0.500 ND 4015-12974.0
2,4-Dinitrotoluene "0.478 0.050 0.500 ND 4034-14495.6
Hexachlorobenzene "0.305 0.050 0.500 ND 405-15761.1
Hexachlorobutadiene "0.324 0.050 0.500 ND 4019-12464.7
Hexachloroethane "0.386 0.050 0.500 ND 4030-13577.2
Nitrobenzene "0.448 0.050 0.500 ND 4030-18589.6
Pentachlorophenol "0.507 0.050 0.500 ND 409-181101
Pyridine "0.433 0.050 0.500 ND 405-13086.5
2,4,5-Trichlorophenol "0.491 0.050 0.500 ND 409-13598.2
2,4,6-Trichlorophenol "0.473 0.050 0.500 ND 4032-14994.6
" 0.500 10-120Surrogate: Phenol-d5 88.30.441
" 0.500 10-131Surrogate: 2,4,6-Tribromophenol 1100.551
" 0.250 10-125Surrogate: 2-Fluorobiphenyl 96.50.241
" 0.500 10-120Surrogate: 2-Fluorophenol 83.30.417
" 0.250 10-130Surrogate: Nitrobenzene-d5 1010.253
" 0.250 15-135Surrogate: Terphenyl-dl4 69.80.175
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 7 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Metals by 1311/6010B - Quality Control
Batch 0G12012 - EPA 3010A Prepared: 07/12/10 Analyzed: 07/13/10
Blank (0G12012-BLK1)
Arsenic mg/LND 0.100
Barium "ND 0.100
Cadmium "ND 0.100
Chromium "ND 0.100
Lead "ND 0.100
Selenium "ND 0.100
Silver "ND 0.100
LCS (0G12012-BS1)
Arsenic mg/L0.199 0.100 0.200 2085-11599.4
Barium "0.205 0.100 0.200 2085-115102
Cadmium "0.193 0.100 0.200 2085-11596.6
Chromium "0.190 0.100 0.200 2085-11595.1
Lead "0.203 0.100 0.200 2085-115101
Selenium "0.200 0.100 0.200 2085-115100
Silver "0.106 0.100 0.100 2085-115106
LCS Dup (0G12012-BSD1)
Arsenic mg/L0.212 0.100 0.200 2085-115106 6.21
Barium "0.206 0.100 0.200 2085-115103 0.784
Cadmium "0.197 0.100 0.200 2085-11598.3 1.75
Chromium "0.197 0.100 0.200 2085-11598.3 3.34
Lead "0.195 0.100 0.200 2085-11597.3 3.99
Selenium "0.196 0.100 0.200 2085-11598.2 2.05
Silver "0.104 0.100 0.100 2085-115104 1.98
Matrix Spike (0G12012-MS1) Source: 1007119-01
Arsenic mg/L0.177 0.100 0.200 ND 2075-12588.3
Barium "0.323 0.100 0.200 0.091 2075-125116
Cadmium "0.168 0.100 0.200 ND 2075-12584.1
Chromium "0.179 0.100 0.200 ND 2075-12589.5
Lead "0.192 0.100 0.200 ND 2075-12595.9
Selenium "0.203 0.100 0.200 ND 2075-125102
Silver "0.110 0.100 0.100 ND 2075-125110
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 8 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Mercury by 1311/7470A - Quality Control
Batch 0G13015 - SW 7470A Prepared & Analyzed: 07/13/10
Blank (0G13015-BLK1)
Mercury mg/LND 0.010
LCS (0G13015-BS1)
Mercury mg/L0.021 0.010 0.0200 2085-115103
LCS Dup (0G13015-BSD1)
Mercury mg/L0.021 0.010 0.0200 2085-115106 2.87
Matrix Spike (0G13015-MS1) Source: 1007119-01
Mercury mg/L0.021 0.010 0.0200 ND 2075-125104
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 9 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Volatile Organic Compounds by EPA Method 1311/8260B - Quality Control
Batch 0G14015 - EPA 5030B Prepared & Analyzed: 07/12/10
Blank (0G14015-BLK1)
Benzene mg/LND 0.125
2-Butanone "ND 0.250
Carbon Tetrachloride "ND 0.125
Chlorobenzene "ND 0.125
Chloroform "ND 0.125
1,2-Dichloroethane "ND 0.125
1,1-Dichloroethene "ND 0.125
Tetrachloroethene "ND 0.125
Trichloroethene "ND 0.125
Vinyl chloride "ND 0.125
" 1.25 83-128Surrogate: Dibromofluoromethane 98.71.23
" 1.25 83.1-126Surrogate: 1,2-Dichloroethane-d4 1011.26
" 1.25 82.3-112Surrogate: Toluene-d8 1011.26
" 1.25 78.4-114Surrogate: 4-Bromofluorobenzene 98.61.23
LCS (0G14015-BS1)
Benzene mg/L0.526 0.125 0.500 3591.8-113105
2-Butanone "0.498 0.250 0.500 3573-12399.5
Carbon Tetrachloride "0.507 0.125 0.500 3583.2-122101
Chlorobenzene "0.506 0.125 0.500 3589.5-111101
Chloroform "0.511 0.125 0.500 3589.8-126102
1,2-Dichloroethane "0.518 0.125 0.500 3581.9-130104
1,1-Dichloroethene "0.518 0.125 0.500 3583.8-132104
Tetrachloroethene "0.550 0.125 0.500 3576-128110
Trichloroethene "0.529 0.125 0.500 3587.2-117106
Vinyl chloride "0.413 0.125 0.500 3565.9-13282.5
" 1.25 83-128Surrogate: Dibromofluoromethane 1031.29
" 1.25 83.1-126Surrogate: 1,2-Dichloroethane-d4 1031.29
" 1.25 82.3-112Surrogate: Toluene-d8 95.61.20
" 1.25 78.4-114Surrogate: 4-Bromofluorobenzene 96.11.20
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 10 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Result MRL Units LevelSpike
ResultSource
%REC%RECLimits RPD
RPDLimit Notes Analyte
TCLP Volatile Organic Compounds by EPA Method 1311/8260B - Quality Control
Batch 0G14015 - EPA 5030B Prepared & Analyzed: 07/12/10
LCS Dup (0G14015-BSD1)
Benzene mg/L0.509 0.125 0.500 3591.8-113102 3.14
2-Butanone "0.451 0.250 0.500 3573-12390.1 9.92
Carbon Tetrachloride "0.488 0.125 0.500 3583.2-12297.5 3.87
Chlorobenzene "0.507 0.125 0.500 3589.5-111101 0.148
Chloroform "0.485 0.125 0.500 3589.8-12697.0 5.17
1,2-Dichloroethane "0.505 0.125 0.500 3581.9-130101 2.64
1,1-Dichloroethene "0.504 0.125 0.500 3583.8-132101 2.79
Tetrachloroethene "0.522 0.125 0.500 3576-128104 5.13
Trichloroethene "0.500 0.125 0.500 3587.2-11799.9 5.69
Vinyl chloride "0.429 0.125 0.500 3565.9-13285.8 3.86
" 1.25 83-128Surrogate: Dibromofluoromethane 99.51.24
" 1.25 83.1-126Surrogate: 1,2-Dichloroethane-d4 1021.28
" 1.25 82.3-112Surrogate: Toluene-d8 97.51.22
" 1.25 78.4-114Surrogate: 4-Bromofluorobenzene 97.61.22
Matrix Spike (0G14015-MS1) Source: 1007119-01
Benzene mg/L0.503 0.125 0.500 ND 4085.9-121101
2-Butanone "0.410 0.250 0.500 ND 4069-13682.0
Carbon Tetrachloride "0.459 0.125 0.500 ND 4072.3-12691.8
Chlorobenzene "0.496 0.125 0.500 ND 4084.6-11699.1
Chloroform "0.497 0.125 0.500 ND 4076.4-13099.4
1,2-Dichloroethane "0.499 0.125 0.500 ND 4077.5-13699.8
1,1-Dichloroethene "0.482 0.125 0.500 ND 4079.1-12996.4
Tetrachloroethene "0.463 0.125 0.500 ND 4071.6-11992.5
Trichloroethene "0.498 0.125 0.500 ND 4086.2-11799.6
Vinyl chloride "0.435 0.125 0.500 ND 4064.2-12587.0
" 1.25 83-128Surrogate: Dibromofluoromethane 99.21.24
" 1.25 83.1-126Surrogate: 1,2-Dichloroethane-d4 99.41.24
" 1.25 82.3-112Surrogate: Toluene-d8 97.21.21
" 1.25 78.4-114Surrogate: 4-Bromofluorobenzene 96.31.20
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 11 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Laboratory Accreditations/Certifications
Code Description Number Expires
01960La Environmental Lab Accreditation Program 06/30/2011C01
National Environmental Lab Accreditation Program 06/30/2011C02
MS00007Ms Dept of Health (Coliform) 11/25/2010C03
MS00021-2009Ms Dept of Health (Drinking Water Certificate) 12/31/2010C04
PBF-00000028Ms DEQ Lead Firm Certification 10/08/2010C05
ABI-00001348MsDEQ Asbestos Inspector : C.D. Bingham 04/22/2010C06
AM-011572MsDEQ Air Monitor : C.D. Bingham 04/23/2010C07
ABI-00001821MsDEQ Asbestos Inspector: C. W. Meins 09/04/2010C08
AM-011189MsDEQ Air Monitor : C.W. Meins 04/23/2011C09
ABI-00002378MsDEQ Asbestos Inspector : C.E.Harris 01/14/2011C10
ABM-00002015MsDEQ Air Monitor : C.E. Harris 10/30/2010C11
ABI-00001345MsDEQ Asbestos Inspector : H.P. Howell 04/22/2010C12
ABM-00001344MsDEQ Air Monitor: H.P. Howell 04/23/2010C13
Report Definitions
DET Analyte DETECTED
ND Analyte NOT DETECTED at or above the minimum reporting limit
NR Not Reported
RPD Relative Percent Difference
ICV Initial Calibration Verfiication
CCV Continuing Calibration Verification Standard
SSV Secondary Source Verfication Standard
LCS Lab Control Spike - Lab matrix prepared with known concentration of analyte/s of interest analyzed by method.
MS Matrix Spike - Sample prepared with known concentration of analyte/s of interest analyzed by method.
MSD Matrix Spike Duplicate - Duplicate sample prepared with known concentration of anlayte/s of interest analyzed by method.
MRL Minimum Reporting Limit
%REC Percentage Recovery of known concentration added to matrix
Batch Group of samples prepared for analysis not to exceed 20 samples.
Matrix Material containing analyte/s of interest
Surrogate Analyte added to sample to determine extraction efficiency of method.
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 12 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
COC Goes Here
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 13 of 14
Project:
Project Number:
Project Manager:
Reported:
MS Department of Environmental Quality
1542 Old Whitfield Road [none]
Henry Folmar
Deepwater Horizon
07/14/10 15:53Pearl MS, 39208
6500 Sunplex Drive
Ocean Springs, MS 39564
228-875-6420 Phone
228-875-6423 Fax
Micro-Methods Laboratory, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 14 of 14