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APPENDIXBLABORATORYANALYTICALRESULTS
ESI:y:
SEVERN
TRENT
ANALYTICALREPORT
JobNumber:680-24701-1
JobDescription:Hercules-Hattiesburg1Q07
For:Eco-SystemsInc6360155North
Suite330Jackson,MS39211
Attention:Mr.CharlesConey
(‘
L.Lf4—
LidyaGulizia
ProjectManagerI
03/20/2007
ProjectManager:LidyaGulizia
ThetestresultsinthisreportmeetallNELAPrequirementsforparametersforwhichaccreditationisrequiredoravailable.AnyexceptionstoNELAPrequirementsarenotedinthisreport.PursuanttoNELAP,thisreportmaynotbereproduced,exceptinfull,withoutthewrittenapprovalofthelaboratory.AllquestionsregardingthistestreportshouldbedirectedtotheSTLProjectManagerwhosignedthistestreport.
SevernTrentLaboratories,Inc.STLSavannah5102LaRocheAvenue,Savannah,GA31404Tel(912)354-7858Fax(912)351-3673www.stl-inc.com
Page1of103
STL
hehc
METHODSUMMARY
Client:Eco-SystemsIncJobNumber:680-24701-1
DescriptionLabLocationMethodPreparationMethod
Matrix:Water
VolatileOrganicCompoundsbyGCIMSSTLSAVSW8468260BPurge-and-TrapSTLSAVSW8465030B
LABREFERENCES:
STLSAV=STLSavannah
METHODREFERENCES:
SW846-“TestMethodsForEvaluatingSolidWaste,Physical/ChemicalMethods”,ThirdEdition,November1986AndItsUpdates.
STLSavannah
Page2of103
METHODIANALYSTSUMMARY
Client:Eco-SystemsIncJobNumber:680-24701-1
MethodAnalystAnalystID
SW8468260BBearden,RobertRB
STLSavannah
Page3of103
SAMPLESUMMARY
Client:Eco-SystemsIncJobNumber680-24701-1
Date/TimeDate/TimeLabSampleIDClientSampleIDClientMatrixSampledReceived
680-24701-1HER-CMOO-022607Water02126/2007140003/01/20070922
680-24701-2HER-CMO1-022607Water02/26/2007134503/01/20070922
680-24701-3HER-CMO2-022607Water02/26/2007133003/01/20070922
680-24701-4HER-CMO3-022607Water02/26/2007131003/01/20070922
680-24701-4MSHER-CMO3-022607Water02126/2007131003/01/20070922
680-24701-4MSDl—IER-CMO3-022607Water02/26/2007131003/01/20070922
680-24701-5HER-CMO4-022607Water02/26/2007125003/01/20070922
680-24701-6HER-CMO5-022607Water02/26/2007123003/01/20070922
680-24701-7HER-MWO2-022707Water02/27/2007101503/01/20070922
680-24701-8HER-MWO3-022707Water02/27/2007093003/01/20070922
680-24701-8MSHER-MWO3-022707Water02/27/2007093003/01/20070922
680-24701-8MSDHER-MWO3-022707Water02/27/2007093003/01/20070922
680-24701-9HER-MWO4-022707Water02/27/2007120503/01/20070922
680-24701-10HER-MWO5-022707Water02127/2007140503/01/20070922
680-24701-11HER-MWO6-022707Water02)27/2007152503/01/20070922
680-24701-12HER-MWO7-022807Water02)28/2007090003/01/20070922
680-24701-12MSHER-MWO7-022807Water02)28/2007090003/01/20070922
680-24701-12MSDHER-MWO7-022807Water02/28/2007090003/01/20070922
680-24701-13HER-MWO8-022807Water02/28/2007135003/01/20070922
680-24701-14HER-M\N09-022807Water02/28/2007123003/01/20070922
680-24701-15HER-MW1O-022707Water02/27/2007113003/01/20070922
680-24701-16HER-MW11-022707Water02/27/2007125003/01/20070922
680-24701-17HER-MW12-022707Water02/27/2007145003/01)20070922
680-24701-18HER-MW13-022807Water02/28/2007114503/01/20070922
680-24701-19HER-MW14-022807Water02/28/2007105503/01/20070922
680-24701-20HER-MW15-022807Water02/28/2007101503/01/20070922
680-24701-21HER-MW16-022807Water02/28/2007094003/01/20070922
680-24701-22HER-MW17-022807Water02/28/2007130503/01/20070922
680-24701-23HER-MW18-022707Water02/27/2007155503/01/20070922
680-24701-24HER-MW19-022707Water02/27/2007162503/01/20070922
680-24701-25RBHER-RSI-022607Water02/26/2007122003/01/20070922
680-24701-26RBHER-RS2-022707Water02/27/2007102003/01/20070922
680-24701-27RBHER-RS3-022807Water02/28/2007093003/01/20070922
680-24701-28FDHER-FDI-022707Water02)27/2007000003/01/20070922
680-24701-29FDHER-FD2-022807Water02/28/2007000003/01/20070922
680-24701-3OTBHER-TBWater02/28/2007000003/01/20070922
STLSavannah
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SAMPLERESULTS
STLSavannah
Page5of103
AnalyticalData
Client:Eco-SystemsIncJobNumber680-24701-1
ClientSampleID:HER-CMOO-022607
LabSampleID:680-24701-1DateSampled:02126/20071400ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2888.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/12/20071325FinalWeightNolume:5mLDatePrepared:03/12/20071325
AnalyteResult(ug/L)QualifierRLAcetone4225Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachlonde<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-1,3-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifiuoromethane<1.01.01,i-Dichloroethane<1.01.01,2-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0cis-1,2-Dichloroethene<1.01.0trans-12-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-13-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0lsobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage6of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMOO-022607
LabSampleID:680-24701-1DateSampled:02/26/20071400
ClientMatrix:WaterDateReceived:03/01/20070922
826DBVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69593InstwmentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2888.dDilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/12120071325FinalWeightNolume:5mLDatePrepared:03/12/20071325
AnalyteResult(ugIL)QualifierRL
1,1,1,2-Tetrachloroethane<1.0*
1.01,1,2,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.01,1,1-Trichloroethane<1.01.011,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Thchlorofluoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofiuorobenzene10277-120Dibromofluoromethane10075-123Toluene-d8(Surr)10279-122
STLSavannahPage7of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMOI-022607
LabSampleID:680-24701-2DateSampled:02/26120071345ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69593InstrumentID:GCIMSVolatiles-0Preparation:5030BLabFileID:o2885.dDilution:1.0InitialWeight/Volume:5mLDateAnalyzed:03/12/20071225FinalWeight/Volume:5mLDatePrepared:03/12/20071225
Analyte
_______
Result(ug/L)QualifierRLAcetone4925Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-1,3-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i4-Dichloro-2-butene<2.02.0Dichlorodifiuoromethane<1.01.01,1-Dichloroethane<1.01.012-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0cis-1,2-Dichloroethene<1.01.0trans-i,2-Dichloroethene<1.01.01,2-Didloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Penlachloroethane<5.05.0Propionitnle<2020Styrene<1.01.0
STLSavannahPage8of103
AnalyticalData
Client:Eco-SystemsIncJobNumber680-24701-1
ClientSampleID:HER-CMOI-022607
LabSampleID:680-24701-2DateSampled:02/26/20071345ClientMatrix.WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0Preparation:50308LabFileID:o2885.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/12/20071225FinalWeightNolume:5mLDatePrepared:03/12/20071225
AnalyteResult(ug/L)QualifierRL
1,112-Tetrachloroethane<1.0*
1.01,12,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.01,1,1-Trichloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofiuorobenzene10277-120Dibromofluoromethane10175-123Toluene-d8(Surr)10279-122
STLSavannahPage9of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO2-022607
LabSampleID:680-24701-3DateSampled:02126/20071330
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69593InstrumentID:CC/MSVolatiles-0
Preparation:5030BLabFileID:o2886.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/12/20071245FinalWeight/Volume:5mL
DatePrepared:03/12)20071245
AnalyteResult(ugIL)QualifierRL
Acetone9225
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-1,3-butadiene<1.01.0
3-Chlorol-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
il-Dichloroethane<1.01.0
1,2-Dichloroethane<1.01.0
il-Dichloroethene<1.01.0
cis-12-Dichloroethene<1.01.0
trans-i,2-Dichloroethene<1.01.0
12-Dichloropropane<1.01.0
cis-1,3-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage10of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO2-022607
LabSampleID:680-24701-3DateSampled:02126120071330
ClientMatrix:WaterDateReceived:03101/20070922
826DBVolatileOrganicCompoundsbyGCIMS
Method:82606AnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2886.d
Dilution:1.0InitialWeightNolurne:5mL
DateAnalyzed:03/12/20071245FinalWeightNolume:5mL
DatePrepared:03/12/20071245
AnalyteResult(ug/L)QualifierRL
1,1,12-Tetrachloroethane<1.0*
1.0
1,1,2,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
11,1-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
12,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofiuorobenzene10277-120
Dibromofluoromethane10075-123
Toluene-d8(Surr)10179-122
STLSavannahPage11of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO3-022607
LabSampleID:680-24701-4DateSampled:02/26/20071310
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:02831.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20071419FinalWeightNolume:5mL
DatePrepared:03/11/20071419
AnalyteResultug/LQualifierRL
Acetone6325
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<10.10
Carbondisulfide<2.02.0
Carbontetrachlonde<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-13-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0
Dichloroditluoromethane<1.01.0
i,1-Dichloroethane<1.01.0
1,2-Dichloroethane<1.01.0
1,1-Dichloroethene<1.01.0
cis-1,2-Dichloroethene<1.01.0
trans-i,2-Dichloroethene<1.01.0
1,2-Dichloropropane<1.01.0
cis-1,3-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonilrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
Page12of103STLSavannah
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO3-022607
LabSampleID:680-24701-4DateSampled:02)26/20071310ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC!MS
Method:82608AnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:50308LabFileID:02831,dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071419FinalWeightNolume:5mLDatePrepared;03/11/20071419
AnalyteResult(ug/L)QualifierRL
1,1,1,2-Tetrachloroethane<1.0*
1.01,1,2,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.01,1,1-Trichloroethane<1.01.01,1,2-Tiichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofluorobenzene10177-120Dibromofluoromethane10275-123Toluene-d8(Sun)10179-122
STLSavannahPage13of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO4-022607
LabSampleID:680-24701-5DateSampled:02/26/20071250ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2887.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/12/20071305FinalWeightNolume:5mLDatePrepared:03/12/20071305
AnalyteResult(ug/L)QualifierRLAcetone16025Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene1.31.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-1,3-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01,01,1-Dichloroethane<1.01.012-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0cis-i,2-Dichloroethene<1.01.0trans-i2-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage14of103
AnalyticalData
Client:Eco-SystemsIncJobNumber680-24701-1
ClientSampleID:HER-CMO4-022607
LabSampleID:680-24701-5DateSampled:02/26/20071250ClientMatrix:WaterDateReceived:03/01/20070922
826DBVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC!MSVolatiles-0Preparation:5030BLabFileID:o2887.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/12/20071305FinalWeightNolume:5mLDatePrepared:03/12120071305
AnalyteResult(ug/L)QualifierRL1,1,12-Tetrachloroethane<1.01.01,1,22-Tetrachloroethane<1.01.0TetracNoroethene<1.01.0Toluene<1.01.01,11-Thchloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofluorobenzene10277-120Dibromotluoromethane10175-123Toluene-d8(Surr)10379-122
STLSavannahPage15of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMO5-022607
LabSampleID:680-24701-6DateSampled.02/26/20071230
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2841.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071739FinalWeightNolume:5mLDatePrepared:03/11/20071739
AnalyteResult(ug/L)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene2.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-i3-butadiene<1.01.03-Chloro-i-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.011-Dichloroethane<1.01.012-Dichloroethane<1.01.011-Dichloroethene<1.01,0cis-1,2-Dichloroethene<1.01.0trans-i,2-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodometharie<5.05.0Isobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STISavannahPage16of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-CMD5-022607
LabSampleID:680-24701-6DateSampled:02126120071230ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2841.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071739FinalWeightNolume:5mLDatePrepared:03/11/20071739
AnalyteResult(ug/L)QualifierRL
111,2-Tetrachloroethane<1.0*
1.01,1,2,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.011,1-Trichloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofiuoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofiuorobenzene9877-120Dibromofluoromethane10175-123Toluene-d8(Surr)9879-122
STLSavannahPage17of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO2-022707
LabSampleID:680-24701-7DateSampled:02/27/20071015
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2842.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071759FinalWeightNolume:5mLDatePrepared:03/11/20071759
AnalyteResult(ug/L)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-i-propene<1.01.0Chlorodibromomethane<1.01.012-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.0i,i-Dichloroethene<1.01.0cis-1,2-Dichloroethene<1.01.0trans-i2-Dichloroethene<1.01.01,2-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i,3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0lsobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitnle<2020Styrene<1.01.0
STLSavannahPage18of103
AnalyticalData
QClient:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO2-022707
LabSampleID:680-24701-7DateSampled:02/27/20071015ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:50308LabFileID:o2842.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03111/20071759FinalWeightNolume:5mLDatePrepared:03/11/20071759
AnalyteResult(ugIL)QualifierRL
1,1,1,2-Tetrachloroethane<1.0*
1.01,1,2,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.01,1,1-Trichloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,2,3-Thchloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofluorobenzene10177-120Dibromofluoromethane10175-123Toluene-dS(Surr)10079-122
Page19of103 STLSavannah
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER..MWO3-022707
LabSampleID:680-24701-8DateSampled:02/27/20070930ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2892.dDilution:1.0InitialWeight/Volume:5mLDateAnalyzed:03/12120071446FinalWeight/Volume:5mLDatePrepared:03/12/20071446
AnalyteResult(ugIL)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.011-Dichloroethene<1.01.0cis-12-Dichloroethene<1.01.0trans-i2-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutanol<4040Methacrylonhtrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage20of103
AnalyticalData
QClient:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO3-022707
LabSampleID:680-24701-8DateSampled:02127/20070930ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:826GBAnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0Preparation:503DBLabFileID:o2892.dDilution:1.0InitialWeight/Volume:5mLDateAnalyzed:03/12120071446FinalWeight/Volume:5mLDatePrepared:03/12120071446
AnalyteResult(ug/L)QualifierRL1,1,1,2-Tetrachloroethane<1.0
*
1.01,1,2,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.01,11-Trichloroethane<1.01.01,1,2-Tiichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits4-Bromofluorobenzene10377-120Dibromofluoromethane10075-123Toluene-d8(Surr)9879-122
STLSavannahPage21of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO4-022707
LabSampleID:680-24701-9DateSampled:02)27/20071205ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2846.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071919FinalWeightlVolume:5mLDatePrepared:03/11/20071919
AnalyteResult(ug/L)QualifierRL
Acetone<2525Acetonhtrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-i-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.012-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0cis-1,2-Dichloroethene<1.01.0trans-i2-Dichloroethene<1.01.01,2-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i,3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrhle<2020Styrene<1.01.0
STLSavannahPage22of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO4-022707
LabSampleID:680-24701-9DateSampled:02/27/20071205ClientMatrix:WaterDateReceived:03/01/20070922
826DBVolatileOrganicCompoundsbyGCIMS
Method:826DBAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:503DBLabFileID:o2846.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071919FinalWeightNolume:5mLDatePrepared:03/11/20071919
AnalyteResult(ug/L)QualifierRL
1,112-Tetrachloroethane<1.0*
1.01,1,22-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.011,1-Trichloroethane<1.01.011,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,23-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofiuorobenzene9777-120Dibromofluoromethane10075-123Toluene-d8(Surr)10179-122
STLSavannahPage23of103
AnalyticalData
Client:Eco-SystemsIncJobNumber680-24701-1
ClientSampleID:HER-MWOS-022707
LabSampleID:680-24701-10DateSampled:02/27/20071405
ClientMatrix:WaterDateReceived:03/01)20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2847.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20071939FinalWeight/Volume:5mL
DatePrepared:03/11/20071939
AnalyteResult(ug/L)QualifierRL
Acetone5225Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0
MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0Chloroethane<1.01.0
Chloroform<1.01.0Chloromethane<1.01.02-Chloro-i3-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.0
1,1-Dichloroethane<1.01.012-Dichloroethane<1.01.0il-Dichloroethene<1.01.0
cis-12-Dichloroethene<1.01.0trans-i2-Dichloroethene<1.01.01,2-Dichloropropane<1.01.0
cis-i,3-Dichloropropene<1.01.0
trans-i3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.02-Hexanone<1010
lodomethane<5.05.0Isobutanol<4040
Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage24of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO5-022707
LabSampleID:680-24701-10DateSampled:02/27)20071405ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2847.dDilution:1.0InitialWeightNolume:5mLDateAnalyzed:03/11/20071939FinalWeight/Volume:5mLDatePrepared:03/11/20071939
AnalyteResult(ug/L)QualifierRL
1,1,1,2-Tetrachloroethane<1.0*
1.01,12,2-Tetrachloroethane<1.01.0Tetrachloroethene<1.01.0Toluene<1.01.0111-Trichloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.01,23-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0Xylenes,Total<2.02.0
Surrogate%RecAcceptanceUmits
4-Bromofluorobenzene10077-120Dibromofluoromethane10275-123Toluene-d8(Surr)10179-122
STLSavannahPage25of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO6-022707
LabSampleID:680-24701-11DateSampled:02/27/20071525ClientMatrix:WaterDateReceived:03/01/20070922
826DBVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0Preparation:5030BLabFileID:o2848.dDilution:1.0InitialWeight/Volume:5mLDateAnalyzed:03/11/20071959FinalWeight/Volume:5mLDatePrepared:03/11/20071959
AnalyteResult(ugIL)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloricle<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0ChloTcfcrrn<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.01,2-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0ds-12-Dichloroethene<1.01.0trans-i,2-Dichloroethene<1.01.01,2-Dichloropropane<1.01.0cis-i,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010loclomethane<5.05.0Isobutanol<4040Methacrylonitrfle<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage26of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO6-022707
LabSampleID:680-24701-11DateSampled:02/27/20071525
ClientMatrix:WaterDateReceived:03/01)20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:CC/MSVolatiles-0
Preparation:5030BLabFileID:o2848.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20071959FinalWeightNolume:5mL
DatePrepared:03/11/20071959
Analy!eResult(ug/L)QualifierRL
1,1,12-Tetrachloroethane<•o*
1.01,12,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.01,1,1-Trichloroethane<1.01.01,1,2-Trichloroethane<1.01.0Trichloroethene<1.010Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0Vinylacetate<2.02.0Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate.
-
AcceptanceLimits
4-Bromofiuorobenzene10477-120
Dibromofluoromethane10475-123
Toluene-d8(Surr)10179-122
STLSavannahPage27of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO7-022807
LabSampleID:680-24701-12DateSampled:02/28/20070900
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2849.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072020FinalWeightNolume:5mL
DatePrepared:03/11/20072020
AnalyteResult(ug/L)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoforrn<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.012-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.0i,1-Dichloroethene<1.01.0cis-i,2-Dichloroethene<1.01.0trans-i,2-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-i,3-Dichloropropene<1.01.0trans-i,3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage28of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO7-022807
LabSampleID:680-24701-12DateSampled:02/28/20070900
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:50308LabFileID:o2849.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072020FinalWeightNolume:5mL
DatePrepared:03/11/20072020
AnalyteResult(ug/L)QualifierRL
1,1,1,2-Tetrachloroethane<1.01.0
1,12,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,1,1-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0Trichloroethene<1.01.0Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene9977-120
Dibromofluoromethane10175-123
Toluene-d8(Surr)10179-122
STLSavannahPage29of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO8-022807
LabSampleID:680-24701-13DateSampled:02/28/20071350
ClientMatrix:WaterDateReceived:03/01(20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680—69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2850.d
Dilution:10InitialWeightNolume:5mL
DateAnalyzed:03/11/20072040FinalWeightNolume:5mL
DatePrepared:03/11/20072040
AnalyteResult(ug/L)QualifierRL
Acetone<250250
Acetonitrile<400400
Acrolein<200200
Acrylonitrile<200200
Benzene99010
Dichlorobromomethane<1010
Bromoform<1010
Bromomethane<1010
MethylEthylKetone<100100
Carbondisulfide<2020
Carbontetrachloride84010
Chlorobenzene2410
Chloroethane<1010
Chloroform10010
Chloromethane<1010
2-Chloro-1,3-butadiene<1010
3-Chloro-1-propene<1010
Chlorodibromomethane<1010
1,2-Dibromo-3-Chloropropane<1010
EthyleneDibromide<1010
Dibromomethane<1010
trans-i,4-Dichloro-2-butene<2020
Dichlorodifluoromethane<1010
1,1-Dichloroethane<1010
1,2-Dichloroethane<1010
1,1-Dichloroethene<1010
cis-i2-Dichloroethene<1010
trans-i2-Dichloroethene<1010
1,2-Dichloropropane<1010
cis-1,3-Dichloropropene<1010
trans-1,3-Dichloropropene<1010
Ethylbenzene1210
Ethylmethacrylate<1010
2-Hexanone<100100
lodomethane<5050
Isobutanol<400400
Methacrylonitrile<200200
MethyleneChloride<5050
Methylmethacrylate<1010
methylisobutylketone<100100
Pentachloroethane<5050
Propionitrile<200200
Styrene<1010
STLSavannahPage30of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO8-022807
LabSampleID:680-24701-13DateSampled:02/28/20071350
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2850.d
Dilution:10InitialWeightNolume:5mL
DateAnalyzed:03/11/20072040FinalWeightlVolume:5mL
DatePrepared:03/11/20072040
AnalyteResult(ugIL)QualifierRL
111,2-Tetrachloroethane<10*
10
112,2-Tetrachloroethane<1010
Tetrachloroethene<1010
Toluene1110
1,1,1-Trichloroethane<1010
1,1,2-Trichloroethane<1010
Trichloroethene<1010
Trichlorofluoromethane<1010
1,2,3-Thchloropropane<1010
Vinylacetate<2020
Vinylchloride<1010
Xylenes,Total2220
Surrogate%RecAcceptanceLimits
4-Bromofiuorobenzene10777-120
Dibromofluoromethane9375-123
Toluene-d8(Surr)10679-122
STLSavannahPage31of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO9-022807
LabSampleID:680-24701-14DateSampled:02/28/20071230
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GCIMSVolatiles-0
Preparation:5030BLabFileID:02851.dDilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072100FinalWeightNolume:5mL
DatePrepared:03/11/20072100
AnalyteResult(ug/L)QualifierRL
Acetone<2525Acetonitrile<4040Acrolein<2020Acrylonitrile<2020Benzene7.61.0Dichlorobromomethane<1.01.0Bromoform<1.01.0Bromomethane<1.01.0MethylEthylKetone<1010Carbondisulfide<2.02.0Carbontetrachloride<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-13-butadiene<1.01.03-Chloro-1-propene<1.01.0Chlorodibromomethane<1.01.012-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-I4-Dichloro-2-butene<2.02.0Dichlorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.011-Dichloroethene4.61.0ds-1,2-Dichloroethene<1.01.0trans-l,2-Dichloroethene<1.01.012-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-13-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0lsobutanol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.0methylisobutylketone<1010Peritachloroethane<5.05.0Propionitrile<2020Styrene<1.01.0
STLSavannahPage32of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWO9-022807
LabSampleID:680-24701-14DateSampled:02128120071230
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:82608AnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:02851.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072100FinalWeightNolume:5mL
DatePrepared:03/11120072100
AnalyteResult(ug/L)QualifierRL
1,1,12-Tetrachloroethane<1.0*
1.0
1,1,2,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
11,1-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene10177-120
Dibromofluoromethane10075-123
Toluene-d8(Surr)10079-122
STLSavannahPage33of103
AnalyticalData
Client:Eco-SystemsIncJobNumber.680-24701-1
ClientSampleID:HER-MWIO-022707
LabSampleID:680-24701-15DateSampled:02/27/20071130
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2852.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072120FinalWeightNolume:5mL
DatePrepared:03/11/20072120
AnalyteResult(ug/L)QualifierRL
Acetone<2525
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-13-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dicliloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
i,i-Dichloroethane<1.01.0
12-Dichloroethane<1.01.0
1,1-Dichloroethene<1.01.0
cis-1,2-Dichloroethene<1.01.0
trans-i2-Dichloroethene<1.01.0
12-Dichloropropane<1.01.0
cis-1,3-Dichloropropene<1.01.0
trans-i3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.010
STLSavannahPage34of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWIO-022707
LabSampleID.680-24701-15DateSampled:02/27/20071130
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2852.d
Dilution:1.0InitialWeight/Volume:5mL
DateAnalyzed:03/11/20072120FinalWeight/Volume:5mL
DatePrepared:03/11/20072120
AnalyteResult(ug/L)QualifierRL
11,12-Tetrachloroethane<1.010
1,12,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,1,1-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0
Thchloroethene<1.01.0
Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene9877-120
Dibromofluoromethane10175-123
Toluene-d8(Surr)10279-122
STLSavannahPage35of103
AnaIyticaData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWII-022707
LabSampleID:680-24701-16DateSampled:02/27/20071250
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC!MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GCIMSVolatiles-0
Preparation:50308LabFileID:o2853.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20072140FinalWeightNolume:5mL
DatePrepared:03/11/20072140
AnalyteResult(ug/L)QualifierRL
Acetone<2525
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-13-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
12-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
1,1-Dichloroethane<1.01.0
1,2-Dichloroethane<1.01.0
1,1-Dichloroethene<1.01.0
cis-i2-Dichloroethene<1.01.0
trans-i2-Dichloroethene<1.01.0
1,2-Dichloropropane<1.01.0
cis-13-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage36of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER.MWII-022707
LabSampleID:680-24701-16DateSampled:02/27/20071250
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2853.d
Dilution:1.0InitialWeight/Volume:5mL
DateAnalyzed:03/11/20072140FinalWeightNolume:5mL
DatePrepared:03/11/20072140
AnalyteResult(ug/L)QualifierRL
1,1,12-Tetrachloroethane<1.0*
1.0
112,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,11-Trichloroethane<1.01.0
112-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
123-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene9877-120
Dibromofluoromethane10075123
Toluene-d8(Surr)10079-122
Page37of103STLSavannah
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI2-022707
LabSampleID:680-24701-17DateSampled:02)27/20071450
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69593InstrumentID:GC!MSVolatiles-0
Preparation:5030BLabFileID:o2898.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/12/20071646FinalWeight/Volume:5mL
DatePrepared:03/12/20071646
AnalyteResult(ug/L)QualifierRL
Acetone<2525
Acetonitrile<4040
Acrolein<2020
Acrylonitnle<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-1,3-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
1,1-Dichloroethane<1.01.0
1,2-Dichloroethane<1.01.0
1,1-Dichloroethene<1.01.0
cis-i,2-Dichloroelhene<1.01.0
trans-i,2-Dichloroethene<1.01.0
1,2-Dichloropropane<1.01.0
cis-i3-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
tsobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage38of103
AnalyticalData
Client:Eco-SystemsIncJobNumber680-24701-1
ClientSampleID:HER-MWI2-022707
LabSampleID:680-24701-17DateSampled:02127120071450
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCiMS
Method:82606AnalysisBatch:680-69593InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2898.d
Dilution:1.0InitialWeight.Nolume:5mL
DateAnalyzed:03/12/20071646FinalWeightNolume:5mL
DatePrepared:03112120071646
AnalyteResult(ugIL)QualifierRL
1,1,12-Tetrachloroethane<1.0*
10
1,1,22-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
11,1-Trichloroethane<1.01.0
1,12-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene10477-120
Dibromofluoromethane10175-123
Toluene-d8(Surr)9979-122
STLSavannahPage39of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI3-022807
LabSampleID:680-24701-18DateSampled:02128/20071145
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:82608AnalysisBatch:680-69519InstrumentID:GC/MSVolatiles-0
Preparation:503GBLabFileID:o2819.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/09/20071842FinalWeighlNolume:5mL
DatePrepared:03/09/20071842
AnalyteResult(ugIL)QualifierRL
Acetone<2525
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene1601.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride680E1.0
Chlorobenzene141.0
Chloroethane<1.01.0
Chloroform1201.0
Chloromethane<1.01.0
2-Chloro-i3-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
1,1-Dichloroethane<1.01.0
i,2-Dichloroethane<101.0
1,i-Dichloroethene<1.01.0
cis-i,2-Dichloroethene2.51.0
trans-i,2-Dichloroethene<1.01.0
12-Dichloropropane<1.01.0
cis-i,3-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage40of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI3-022807
LabSampleID:680-24701-18DateSampled:02/28/20071145
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69519InstrumentID:GCIMSVolatiles-0
Preparation:5030BLabFileID:o2819.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/09/20071842FinalWeight/Volume:5mL
DatePrepared:03/09/20071842
AnalyteResult(ugiL)QualifierRL
11,1,2-Tetrachloroethane<1.01.0
1,1,22-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,11-Trichloroethane<1.01.0
1,1,2-Tiichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride1.61.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene10077-120
Dibromofluoromethane11075-123
Toluene-d8(Surr)10579-122
STLSavannahPage41of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI3-022807
LabSampleID:680-24701-18DateSampled:02128120071145
ClientMatrixWaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2833.d
Dilution:5.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20071459RunType:DLFinalWeight/Volume:5mL
DatePrepared:03/11/20071459
AnalyteResult(ug/L)QualifierRL
Acetone<130130
Acetonitrile<200200
Acrolein<100100
Acrylonitrile<100100
Benzene170D5.0
Dichlorobromomethane<5.05.0
Bromoform<5.05.0
Bromomethane<5.05.0
MethylEthylKetone<5050
Carbondisulfide<1010
Carbontetrachloride580D5.0
Chlorobenzene14D5.0
Chloroethane<5.05.0
Chloroform110D5.0
Chloromethane<5.05.0
2-Chloro-1,3-butadiene<5.05.0
3-Chloro-1-propene<5.05.0
Chlorodibromomethane<5.05.0
1,2-Dibromo-3-Chloropropane<5.05.0
EthyleneDibromide<5.05.0
Dibromomethane<5.05.0
trans-i4-Dichloro-2-butene<1010
Dichloroditluoromethane<5.05.0
11-Dichloroethane<5.05.0
12-Dichloroethane<5.05.0
1,1-Dichloroethene<5.05.0
cis-12Dichloroethene<5.05.0
trans-1,2-Dichloroelhene<5.05.0
12-Dichloropropane<505.0
cis-1,3-Dichloropropene<5.05.0
trans-i3-Dichloropropene<5.05.0
Ethylbenzene<5.05.0
Ethylmethacrylate<5.05.0
2-Hexanone<5050
lodomethane<2525
Isobutanol<200200
Methacrylonitrile<100100
MethyleneChloride<2525
Methylmethacrylate<5.05.0
methylisobutylketone<5050
Pentachloroethane<2525
Propionitrile<100100
Styrene<5.05.0
STLSavannahPage42of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI3-022807
LabSampleID:680-24701-18DateSampled:02/28/20071145
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC/MS
Method:8260BAnalysisBatch:680-69521InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2833.d
Dilution:5.0InitialWeightNolume:5mL
DateAnalyzed:03/11/20071459RunType:DLFinalWeightNolume:5mL
DatePrepared:03111/20071459
AnalyteResult(ug/L)QualifierRL
1,11,2-Tetrachloroethane<5.0*
5.0
1,122-Tetrachloroethane<5.05.0
Tetrachloroethene<5.05.0
Toluene<5.05.0
111-Trichloroethane<5.05.0
1,12-Trichloroethane<5.05.0
Tnchloroethene<5.05.0
Trichlorofluoromethane<5.05.0
12,3-Trichloropropane<5.05.0
Vinylacetate<1010
Vinylchloride<5.05.0
Xylenes,Total<1010
Surrogate%RecAcceptanceLimits
4-Bromofiuorobenzene10077-120
Dibromofluoromethane10175-123
Toluene-d8(Surr)10379-122
STLSavannahPage43of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI4-022807
LabSampleID:680-24701-19DateSampled:02/28/20071055
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGC!MS
Method:8260BAnalysisBatch:680-69519InstrumentID:GC/MSVolatiles-0
Preparation5030BLabFileID:o2820.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03109/20071902FinalWeightNolume:5mL
DatePrepared:03/09/20071902
AnalyteResult(ug/L)QualifierRL
Acetone<2525
Acetonitrile<4040
Acrolein<2020
Acrylonitñle<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-13-butadiene<1.01.0
3-Chloro-i-propene<1.01.0
Chlorodibromomethane<1.01.0
12-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i,4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
il-Dichloroethane<1.01.0
1,2-Dichloroethane<1.01.0
1,1-Dichloroethene<1.01.0
cis-1,2-Dichloroethene<1.01.0
trans-i2-Dichloroethene<1.01.0
1,2-Dichloropropane<1.01.0
cis-1,3-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroethane<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage44of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI4-022807
LabSampleID:680-24701-19DateSampled:02128/20071055
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69519InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2820.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/09/20071902FinalWeightNolume:5mL
DatePrepared:03/09/20071902
AnalyteResult(ug/L)QualifierRL
1,1,12-Tetrachloroethane<1.01.0
1,1,2,2-Tetrachloroethane1.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,1,1-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
1,2,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene9977-120
Dibromofluoromethane10175-123
Toluene-d8(Surr)10179-122
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AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI5-022807
LabSampleID680-24701-20DateSampled:02)28/20071015
ClientMatrix:WaterDateReceived:03/01/20070922
8260BVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69519InstrumentID:GCIMSVolatiles-0
Preparation:50308LabFileID:o2821.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03)09/20071922FinalWeightNolume:5mL
DatePrepared:03/09/20071922
AnalyteResult(ug/L)QualifierRL
Acetone35025
Acetonitrile<4040
Acrolein<2020
Acrylonitrile<2020
Benzene<1.01.0
Dichlorobromomethane<1.01.0
Bromoform<1.01.0
Bromomethane<1.01.0
MethylEthylKetone<1010
Carbondisulfide<2.02.0
Carbontetrachloride<1.01.0
Chlorobenzene<1.01.0
Chloroethane<1.01.0
Chloroform<1.01.0
Chloromethane<1.01.0
2-Chloro-1,3-butadiene<1.01.0
3-Chloro-1-propene<1.01.0
Chlorodibromomethane<1.01.0
1,2-Dibromo-3-Chloropropane<1.01.0
EthyleneDibromide<1.01.0
Dibromomethane<1.01.0
trans-i4-Dichloro-2-butene<2.02.0
Dichlorodifluoromethane<1.01.0
11-Dichloroethane<1.01.0
12-Dichloroethane<1,01.0
1,1-Dichloroethene<1.01.0
cis-1,2-Dichloroethene<1.01.0
trans-i,2-Dichloroethene<1.01.0
1,2-Dichloropropane<1.01.0
cis-13-Dichloropropene<1.01.0
trans-i,3-Dichloropropene<1.01.0
Ethylbenzene<1.01.0
Ethylmethacrylate<1.01.0
2-Hexanone<1010
lodomethane<5.05.0
Isobutanol<4040
Methacrylonitrile<2020
MethyleneChloride<5.05.0
Methylmethacrylate<1.01.0
methylisobutylketone<1010
Pentachloroefharie<5.05.0
Propionitrile<2020
Styrene<1.01.0
STLSavannahPage46of103
AnalyticalData
Client:Eco-SystemsIncJobNumber:680-24701-1
ClientSampleID:HER-MWI5-022807
LabSampleID:680-24701-20DateSampled:02128120071015
ClientMatrix:WaterDateReceived:03/01/20070922
826GBVolatileOrganicCompoundsbyGCIMS
Method:8260BAnalysisBatch:680-69519InstrumentID:GC/MSVolatiles-0
Preparation:5030BLabFileID:o2821.d
Dilution:1.0InitialWeightNolume:5mL
DateAnalyzed:03/09/20071922FinalWeightNolume:5mL
DatePrepared:03/09/20071922
AnalyteResult(ug/L)QuatierRL
1,1,1,2-Tetrachloroethane<1.01.0
1,12,2-Tetrachloroethane<1.01.0
Tetrachloroethene<1.01.0
Toluene<1.01.0
1,11-Trichloroethane<1.01.0
1,1,2-Trichloroethane<1.01.0
Trichloroethene<1.01.0
Trichlorofluoromethane<1.01.0
12,3-Trichloropropane<1.01.0
Vinylacetate<2.02.0
Vinylchloride<1.01.0
Xylenes,Total<2.02.0
Surrogate%RecAcceptanceLimits
4-Bromofluorobenzene10077-120
Dibromofluoromethane10275-123
Toluene-d8(Surr)9979-122
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