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8/10/2019 laporan resmi distilasi, Kimia Dasar 1

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EXPERIMENT REPORT

DISTILLATION

GROUP V :

PUTRI MEGA ANANDA (123194205)

ZAIMATUL UMAH (123194232)

RADIAN DANY APRILIA (123194236)

THE STATE UNIVERSITY OF

SURABAYA

A!ULTY O MATHEMATI!S AND NATURAL S!IEN!ES

DEPARTMENT O !HEMISTRY

2012


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A. TITLE : DISTILLATION

B. DATE OF EXPERIMENT : October, 9th2012

C. PRPOSE : 1. Se!"r"t#$% "$& !'r#()#$% the *#+'#&

2. Deter#$#$% bo#*#$% !o#$t o( the *#+'#&

D. BASIC T-EOR:

D#/t#**"t#o$ #/ " #&e*) '/e& etho& (or /e!"r"t#$% #t're/ b"/e& o$

((ere$ce/ #$ the co$t#o$/ re+'#re& to ch"$%e the !h"/e o( co!o$e$t/ o(

the #t're. To /e!"r"te " #t're o( *#+'#&/, the *#+'#& c"$ be he"te& to (orce

co!o$e$t/, h#ch h"e ((ere$t bo#*#$% !o#$t/, #$to the %"/ !h"/e. The %"/

#/ the$ co$&e$/e& b"c3 #$to *#+'#& (or "$& co**ecte&. A*tho'%h the ter #/

o/t coo$*) "!!*#e& to *#+'#&/, the reer/e !roce// c"$ be '/e& to /e!"r"te

%"/e/ b) *#+'e()#$% co!o$e$t/ '/#$% ch"$%e/ #$ te!er"t're "$&4or

!re//'re. D#/t#**"t#o$ #/ '/e& (or "$) coerc#"* !roce//e/, /'ch "/

!ro&'ct#o$ o( %"/o*#$e, /t#**e& "ter, )*e$e, "*coho*, !"r"((#$, 3ero/e$e,"$& "$) other *#+'#&/. D#/t#**"t#o$ #/ '/e& to "#$%&' *+"*#,- b)

/e!"r"t#$% #t (ro " $o$5o*"t#*e or *e//5o*"t#*e "ter#"*. 6he$ ((ere$t

co!o'$&/ #$ " #t're h"e ((ere$t bo#*#$% !o#$t/, the) /e!"r"te #$to

#$#&'"* co!o$e$t/ he$ the #t're #/ c"re('**) /t#**e&.

D%./%/%*, &*$ !*+"*#,- I-,/%&%/%*,: *%%, P*%,/ D/$+%,/%*,

D#/t#**"t#o$ #/ '/e& to !'r#() " co!o'$& b) /e!"r"t#$% #t (ro " $o$5o*"t#*e

or *e//5o*"t#*e "ter#"*. Bec"'/e ((ere$t co!o'$&/ o(te$ h"e ((ere$t

bo#*#$% !o#$t/, the co!o$e$t/ o(te$ /e!"r"te (ro " #t're he$ the

#t're #/ /t#**e&.

The bo#*#$% !o#$t #/ the te!er"t're "t h#ch the "!or !re//'re o( the *#+'#&

!h"/e o( " co!o'$& e+'"*/ the eter$"* !re//'re "ct#$% o$ the /'r("ce o( the

*#+'#&. The eter$"* !re//'re #/ '/'"**) the "to/!her#c !re//'re. For

#$/t"$ce, co$/#&er " *#+'#& he"te& #$ "$ o!e$ (*"/3. The "!or !re//'re o( the

*#+'#& #** #$cre"/e "/ the te!er"t're o( the *#+'#& #$cre"/e/, "$& he$ the

"!or !re//'re e+'"*/ the "to/!her#c !re//'re, the *#+'#& #** bo#*. D#((ere$t

co!o'$&/ bo#* "t ((ere$t te!er"t're/ bec"'/e e"ch h"/ " ((ere$t,

ch"r"cter#/t#c "!or !re//'re: co!o'$&/ #th h#%her "!or !re//'re/ #**

bo#* "t *oer te!er"t're/.

Bo#*#$% !o#$t/ "re '/'"**) e"/'re& b) recor$% the bo#*#$% !o#$t 7or r"$%e8

o$ " theroeter h#*e !er(or#$% " /t#**"t#o$. Th#/ etho& #/ '/e&

he$eer there #/ e$o'%h o( the co!o'$& to !er(or " /t#**"t#o$. The

/t#**"t#o$ etho& o( bo#*#$% !o#$t &eter#$"t#o$ e"/'re/ the te!er"t're

o( the "!or/ "boe the *#+'#&. S#$ce the/e "!or/ "re #$ e+'#*#br#' #th the

bo#*#$% *#+'#&, the) "re the /"e te!er"t're "/ the bo#*#$% *#+'#&. The "!or

te!er"t're r"ther th"$ the !ot te!er"t're #/ e"/'re& bec"'/e #( )o' !'t "

theroeter "ct'"**) #$ the bo#*#$% *#+'#& #t're, the te!er"t're re"$%

o'*& *#3e*) be h#%her th"$ th"t o( the "!or/. Th#/ #/ bec"'/e the *#+'#& c"$


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be /'!erhe"te& or co$t"#$"te& #th other /'b/t"$ce/, "$& there(ore #t/

te!er"t're #/ $ot "$ "cc'r"te e"/'ree$t o( the bo#*#$% te!er"t're.

E. DESIN OF EXPERIMENT :


4/13

"8 E+'#!e$t "$& M"ter#"*/

E+'#!e$t :

D#/t#**"t#o$ (*"/3 : 1!#ece

Be"3er %*"// ;00 L : 1!#ece

Be"3er %*"// 100 L : 1!#ece

L#+'e(#er : 1!#ece

Theroeter : 1!#ece

Bo#*#$% /to$e/ :

P#!ette &ro!/ :

6#re %"'=e : 2!#ece

B'$/e$ : 1!#ece

Tr#!o& : 1!#ece

S!"t'*" : 1!#ece

M"ter#"*/ :

N"C* 1 %r"

A%NO< 0,1 M

A+'"&e/

b8 E!er#e$t Ste!/

1. Pre!"re the /t#**"t#o$ /et

2. E$ter#$% bo#*#$% /to$e/ #$to /t#**"t#o$ (*"/3 b) 3ee* oer the

/t#**"t#o$ (*"/3


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11. Po'r#$% ;L N"C* /o*'t#o$ 7/o*'t#o$ be(ore /t#**"t#o$8 #$ te/t t'be 1

12. Po'r#$% ;L /t#**"te #$ te/t t'be 2

1


6/13

PROCEDRE

E$tere& to be"3er %*"// 7//o*e&8

1. A&& /oe o( bo#*#$% /to$e/2. E$ter to /t#**"t#o$ (*"/3

1. R'$ "ter thro'%h the L#+'e(#er2. Bo#*e& /t#**"t#o$ (*"/3 '$t#* the

te!er"t're #$cre"/e "$& co$/t"$t

Te/t T'be 1 Te/t T'be 2 Te/t T'be

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