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Polymer Micromachining Packaging of MEMS sensors Mikrosensorer

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Page 1: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Polymer Micromachining

Packaging of MEMS sensors

Mikrosensorer

Project meeting 1

Sensor Time

Accelerometer 184 915

Pressure sensor 184 1015

Flow sensor 184 1115

Polymer Micromechanics

Cheaper materials

Low cost fabrication

Allow single use

rdquothermal recyclingrdquo

Rapid prototyping

Very flexible electronic

components (design amp state)

Polymer Micromachining

Polymer Micromechanics

bull Thin Film Litography

bull Hot Embossing

bull Injection Moulding

bull Laser Fabrication

bull 3D-printing

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 2: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Project meeting 1

Sensor Time

Accelerometer 184 915

Pressure sensor 184 1015

Flow sensor 184 1115

Polymer Micromechanics

Cheaper materials

Low cost fabrication

Allow single use

rdquothermal recyclingrdquo

Rapid prototyping

Very flexible electronic

components (design amp state)

Polymer Micromachining

Polymer Micromechanics

bull Thin Film Litography

bull Hot Embossing

bull Injection Moulding

bull Laser Fabrication

bull 3D-printing

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 3: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Polymer Micromechanics

Cheaper materials

Low cost fabrication

Allow single use

rdquothermal recyclingrdquo

Rapid prototyping

Very flexible electronic

components (design amp state)

Polymer Micromachining

Polymer Micromechanics

bull Thin Film Litography

bull Hot Embossing

bull Injection Moulding

bull Laser Fabrication

bull 3D-printing

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 4: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Cheaper materials

Low cost fabrication

Allow single use

rdquothermal recyclingrdquo

Rapid prototyping

Very flexible electronic

components (design amp state)

Polymer Micromachining

Polymer Micromechanics

bull Thin Film Litography

bull Hot Embossing

bull Injection Moulding

bull Laser Fabrication

bull 3D-printing

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 5: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Polymer Micromechanics

bull Thin Film Litography

bull Hot Embossing

bull Injection Moulding

bull Laser Fabrication

bull 3D-printing

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 6: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Polymer classes

Plastic materials that can be formed into shapes

Thermoplastic materials that can be shaped more than once

Thermosetting plastic material that can only be shaped once

Elastomer material that is elastic in some way If a moderate amount of deforming force is added the elastomer will return to its original shape Useful for fibers

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 7: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Properties of Polymers

bull Chain length

bull Structure orientation of chains

bull Identity of side groups

bull Degree of cross‐linking

ndash Cross linking with covalent bonds formed

between chains make the polymer stiffer

more crystalline

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 8: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Thermoplastics

Melting (Tm)

Rubbery flow

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 9: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

OSTE(+)

Saharil F et al microTAS 2012Carlborg et al Lab on a chip 2011

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 10: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Particle doped polymers

bull Magnetic particles

bull Silver

bull Carbon graphene

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 11: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Hot Embossing

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 12: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Nano Imprint Litography (NIL)

Thin Films

Higher Temperatures

Curable Polymers

Limit in aspect ratio rather than linewidth

Very high resolution

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 13: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Injection Moulding

High throughput massfabrication

Expensive initial cost

Limited resolution (10 microm)

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 14: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

3D printing

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 15: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Stereolitography

bull Polymerisation by

multi photon

absorption

bull High energy density

achieved by fs-

pulses

bull Resolution down to

120nm

bull Completely arbitrary

3D -structures

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 16: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Microfluidic filters

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 17: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Cell Gym

Adv Mater 23 (2011)

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 18: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Microrobots

Adv Materials 24 2012

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 19: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Laser Ablation

bull Evaporation

ndash Long wavelength (~1microm)

ndash Gaussian profile

ndash Condensation rdquobumpsrdquo

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 20: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Laser Ablation

bull Ionisation

ndash Short wavelength (200 ndash 300 nm)

ndash High power bursts

ndash Smaller spot size (5 microm)

ndash High aspect ratio

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 21: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Materials

bull Metals

bull Polymers

bull Semiconductors

bull Glass

bull Ceramics

bull Crystalline materials

bull Delicate materials

bull Flammablesexplosives

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 22: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Cutting

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 23: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Drilling

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 24: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Structuring in 25 D

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 25: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Packaging

bull MEMS Packaging Issues

bull MEMS Packaging Approaches

bull Electrical connections

bull Sealing

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 26: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Recommended Literature

Handbook of silicon based MEMS

Materials amp technologies

Author Lindroos Veikko

Available as eBook on

httpwwwlubluseensearchlubsearchhtml

Part V

Encapsulation of MEMS Components

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 27: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Packaging

bull One of least explored MEMS components

bull Litterature is scarce

bull No unique and generally applicable packaging method for

MEMS

bull Each device works in a special environment

bull Each device has unique operational specs

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 28: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Design Issues in MEMS

packaging

bull Up to and exceeding 80 of total cost

bull Sensors need direct access to the environment

bull Package must be specifically designed for device

bull Reliability

bull Media compatibility

bull Modularity

bull Small quantities

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 29: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Example Accelerometerbull Key Issues

- Free standing microstructures

- Temperature sensitive microelectronics

- Hermetic sealing

- Alignment

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 30: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Example Pressure Sensor

Key Issues

ndash Exposure to external pressure

ndash Housing for harsh environment

ndash Interface coating

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 31: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Example Microfluidic DeviceKey Issues

ndash Micro-to-Macro interconnections

ndash Good sealing

ndash Temperature sensitive materials

ndash Optical access

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 32: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Packaging serves

two main functions

bull Protection from environment

ndash Electrical isolation from electrolytes and moisture

ndash Mechanical protection to ensure structural integrity

ndash Optical and thermal protection to prevent undesired effects

on performance

ndash Chemical isolation from harsh chemical environment

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 33: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Packaging serves

two main functions

bull Protection from device

ndash Material selection to eliminate or reduce host response

ndash Device operation to avoid toxic products

ndash Device sterilization

ndash Size and contacts

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 34: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Major Issues in MEMS

packaging

bull Release and stiction

bull Die handling and dicing

bull Stress

bull Outgassing

bull Testing

bull Electrical contacts

bull Encaptulation Hermetic seals

bull Integration

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 35: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Die Packaging Operations

bull Die separation (dicing)

bull Die pick

bull Die attach (a)

bull Inspection

bull Wire Bonding (b)

bull Preseal inspection

bull Packaging and Sealing (c)

bull Plating

bull Lead trim

bull Final Tests

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 36: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Packaging levels

bull Wafer

bull Die

bull Device

bull System

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 37: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Wafer Level Packaging

bull To adopt IC packaging processes

as much as possible

bull Stay in Batch process as long as

possible

bull Includes both interconnections

and Encapsulations

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 38: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Electrical ContactsWire bonding

bull Wire bonding

ndash Most common method

ndash Uses variety of metals

depending on bondpad

Ball bond Wedge bond

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 39: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Electrical ContactsWire bonding

Wedge bonding

ndash Aluminium or Gold wire

ndash Aluminium is ultrasonically bonded at room temperature

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 40: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Electrical ContactsWire bonding

Ball bonding

ndash Gold or Copper (Need inert atmosphere)

ndash Ball is formed with high voltage arc or hydrogen torch

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 41: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Electrical Contactsbull Flip chips

ndash Solder bumps used to attach flipped chip

ndash Quick universal connection

ndash Allows individual chip optimization

ndash Connect dissimilar materials

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 42: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Anisotropic Conductive Film

bull Polyester film with 10microm Particles of Gold coated polymer

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 43: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Sealing Methods

bull Hermetic

ndash Soldering Brazing Welding (Metals)

ndash Anodic bonding Glass frit (Glass)

ndash Wafer bonding (Silicon)

bull Nonhermetic

ndash Epoxy molding

ndash Blob top (polymers)

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 44: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Sealing Methods

Issues

bull Thermal expansion

bull Permeability

bull Surface Roughness

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 45: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Package Encapsulation

bull Protection from corrosion mechanical damage

bull Moisture is one of the major sources of corrosion

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 46: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Metal sealing methods

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 47: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Soldering and Brazing

bull Soldering

ndash Tin-Lead solder (indium and

silver are sometimes added)

ndash Tin-Lead oxidizes easily and

should be stored in nitrogen

bull Brazing

ndash Eutectic Au-Sn (8020) at 280oC

ndash 350oC for stronger more

corrosion-resistant seal and the

use of flux can be avoided

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 48: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Eutectic Bondingbull Formed by heating two

materials (Au and Si)

so they diffuse

together

bull The resulting alloy

composition melts at a

lower temperature than

the base materials

(97Au - 3Si eutectic

melts at 363degC)

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 49: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Eutectic Bonding

bull Benefits

bull Good thermal conductivity

bull Electrically conducting

bull Good fatiguecreep

resistance

bull Low contamination

bull High processoperating

temperature capability

bull Limitations bull High stresses on Si chip due to

CTE mismatch on larger dies

bull Relatively high processing

temperatures

bull Die back metallisation may be

required

bull Rework is difficult

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 50: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Metal sealing methods

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 51: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Glass Sealing

bull Hermetic glass-to-metal seals or glass-ceramic seal

bull Chemical inertness oxidation resistance electrical

insulation impermeability to moisture and other gasses

wide choice of thermal characteristics

bull Soft glass sealing are made by lead-zinc-borate glasses

below 420oC -gtlow water content good chemical

durability thermal expansion closely matched to that of

the ceramic

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 52: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Glass Sealing

Disadvantages

bull low strength and brittleness

bull Water is absorbed on glass network and may get

released into the sealed cavity

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 53: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Anodic bondning

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 54: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Anodic Bonding

bull Sodium-rich glass (Pyrex)

bull Operation temperature is well below the melting

temperature of glass

bull Surface roughness lt 1 microm

bull Native oxide on Si must be thinner than 02 microm

bull Bonding temperature below 500oC or the

thermal properties of materials begin to deviate

seriously

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 55: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Glass Frit Bonding

bull Low melting point glass (lead-glass 430C)

bull Screen printed as grained glass paste

bull Burn-out (melting to real glass)

bull Bonding (Melting)

bull Excellent Hermetic sealing to most materials

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 56: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Silicon Fusion Bondingbull Clean surface roughness lt 4 nm

bull Activated (Hydrated) in warm sulfuric acid

bull Weak Hydrogen bond

bull Dehydration in 1000oC

bull Forms stable

silicondioxide bond

bull Possible to do

hydrophobic bond

with weak H-F binding

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 57: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Low temperature Si bonding

bull Plasma Activation Based Low-

Temperature Bonding

bull UHV Low-Temperature Hydrophobic

Bonding

bull Direct Bonding of CVD Oxides

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 58: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Wafer Bonding Processes

bull Anodic Bonding

ndash Temperature ~450oC voltage ~1000 volts

ndash Silicon (metal) to glass

bull Glass Frit Bonding

ndash Temperature ~450oC voltage

ndash Silicon (metal) to glass

bull Fusion Bonding

ndash Temperature ~1000oC

ndash Silicon to silicon (glass oxide)

bull Eutectic Bonding

ndash Silicon to metal (silicon-to-gold ~363oC)

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 59: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

LPCVD encapsulation

(a) Standard surface

micromachining

process

(b) Additional thick PSG

(phosphosilicate glass)

deposition to define

encapsulation regions

(c) Additional thin PSG

deposition to define

etch channels

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 60: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

LPCVD encapsulation

(d) Nitride shell deposition

etch hole definition

(e) Removal of all sacrificial

PSG inside the shell

supercritical CO2 drying

global LPCVD sealing

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 61: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

CVDChemical Vapor Deposition

bull Chemical reaction in vapor phase forms a solid film

bull Pressure and temperature dependent

bull Activation energy (heat radiation plasma)

Polysilicon Nitrides Oxides Semiconductors (III - V)

Metals Polymers Diamond

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 62: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

CVDChemical Vapor Deposition

Critical deposition temperature of niobium as a function of NbCl5 initial pressure

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 63: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

CVDChemical Vapor Deposition

bull Atmospheric-pressure CVD (APCVD)

bull Low-pressure CVD (LPCVD)

bull Plasma-enhanced CVD (PECVD)

bull Photo-enhanced CVD (PHCVD)

bull Laser-induced CVD (PCVD)

bull Metalorganic CVD (MOCVD)

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 64: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Polymer Sealing

bull Advantages

ndash Low bonding temperature

ndash No metal ions

ndash Elastic property of polymer can reduce bonding stress

bull Disadvantages

ndash Not a good material for hermetic sealing

ndash High vapor pressure

ndash Poor mechanical properties

bull Examples

ndash Silicone (Blob top)

ndash UV-curable encapsulant resins

ndash Thick ultraviolet photoresists such as polyimides AZ-4000

and SU-8

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 65: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Thermal bonding of polymers

The substrates are heated above Tg and pressed together

Melting (Tm)

Rubbery flow

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 66: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Laser bonding of polymers

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 67: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Other bonding methods

bull UV Curable Materials

bull Photoresists

bull Adhesives (Glues Silicones)

bull Waxes

bull Chemical Bonding

bull Hydrophilic bond

Adhesive application on

structured surfaces

Page 68: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4

Adhesive application on

structured surfaces

Page 69: Mikrosensorer Polymer Micromachining Packaging of MEMS …bme.lth.se/fileadmin/biomedicalengineering/Courses/Mikrosensorer/Packaging.pdfAccelerometer 18/4 , 9.15 Pressure sensor 18/4