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Peltier, Hannah
From: Ahrendsen, BlakeSent: Friday, December 12, 2014 9:55 AMTo: Peltier, HannahSubject: FW: NPDES Permit Renewal Application - AR0046116Attachments: WF-06_NPDES_Form_2C_Amendment_121214.pdf; ATT00001..htm; 678528.pdf;
ATT00002..htm
Importance: High
From: Seth Pickens [mailto:[email protected]] Sent: Friday, December 12, 2014 9:49 AM To: Fuller, Kim Cc: Ahrendsen, Blake; Ahrendsen, Blake; Bruce Shackleford; GREG HICKS; [email protected] Subject: Re: NPDES Permit Renewal Application - AR0046116 Importance: High Blake, As requested in Item 3 of the email sent on December 3, 2014, please find attached to this email the updated Section V.A of EPA Form 2C for Outfall 001 for the West Fraser Huttig, AR Facility and the associated lab report test data. As we have now addressed all 4 items from the email below, our application should now be complete. Please let me know if the Department requires any additional information or has any further questions. Cordially, Seth Pickens, B.S., CPSWPPP, CCSI Environmental Scientist Environmental Consulting Operations, Inc Integrating ECOnomy and ECOlogy since 1990 17724 I‐30 Suite 5A Benton, AR 72019 Office ‐ 1‐501‐315‐9009 Cell ‐ 1‐479‐518‐1819 [email protected]
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS.
EPA I.D. NUMBER (copy from Item 1 of Form 1)
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) OUTFALL NO.
PART A –You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT 3. UNITS
(specify if blank) 4. INTAKE (optional)
a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE
(if available) c. LONG TERM AVRG. VALUE
(if available) a. LONG TERM
AVERAGE VALUE
1. POLLUTANT (1)
CONCENTRATION (2) MASS (1)
CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF
ANALYSES a. CONCEN-
TRATION b. MASS (1)
CONCENTRATION (2) MASS b. NO. OF
ANALYSES
a. Biochemical Oxygen Demand (BOD) b. Chemical Oxygen Demand (COD) c. Total Organic Carbon (TOC) d. Total Suspended Solids (TSS)
e. Ammonia (as N)
f. Flow VALUE VALUE VALUE
VALUE
g. Temperature (winter)
VALUE VALUE VALUE °C
VALUE
h. Temperature (summer)
VALUE VALUE VALUE °C
VALUE
i. pH MINIMUM MAXIMUM MINIMUM MAXIMUM
STANDARD UNITS PART B – Mark “X” in column 2-a for each pollutant you know or have reason to believe is present. Mark “X” in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK “X” 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE
(if available) c. LONG TERM AVRG. VALUE
(if available) a. LONG TERM AVERAGE
VALUE 1. POLLUTANT
AND CAS NO.
(if available)
a. BELIEVED PRESENT
b. BELIEVED ABSENT
(1) CONCENTRATION (2) MASS
(1) CONCENTRATION (2) MASS
(1) CONCENTRATION (2) MASS
d. NO. OF ANALYSES
a. CONCEN-TRATION b. MASS
(1) CONCENTRATION (2) MASS
b. NO. OF ANALYSES
a. Bromide (24959-67-9)
b. Chlorine, Total Residual
c. Color
d. Fecal Coliform
e. Fluoride (16984-48-8)
f. Nitrate-Nitrite (as N)
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE
ITEM V-B CONTINUED FROM FRONT 2. MARK “X” 3. EFFLUENT 4. UNITS 5. INTAKE (optional)
a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE
(if available) c. LONG TERM AVRG. VALUE
(if available) a. LONG TERM
AVERAGE VALUE 1. POLLUTANT
AND CAS NO.
(if available)
a. BELIEVED PRESENT
b. BELIEVED ABSENT
(1) CONCENTRATION (2) MASS
(1) CONCENTRATION (2) MASS
(1) CONCENTRATION (2) MASS
d. NO. OF ANALYSES
a. CONCEN-TRATION b. MASS
(1) CONCENTRATION (2) MASS
b. NO. OF ANALYSES
g. Nitrogen, Total Organic (as N)
h. Oil and Grease i. Phosphorus (as P), Total (7723-14-0)
j. Radioactivity
(1) Alpha, Total
(2) Beta, Total
(3) Radium, Total
(4) Radium 226, Total
k. Sulfate (as SO4) (14808-79-8)
l. Sulfide (as S)
m. Sulfite (as SO3) (14265-45-3)
n. Surfactants
o. Aluminum, Total (7429-90-5)
p. Barium, Total (7440-39-3)
q. Boron, Total (7440-42-8)
r. Cobalt, Total (7440-48-4)
s. Iron, Total (7439-89-6)
t. Magnesium, Total (7439-95-4)
u. Molybdenum, Total (7439-98-7)
v. Manganese, Total (7439-96-5)
w. Tin, Total (7440-31-5)
x. Titanium, Total (7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Page 1 of 112/10/2014Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Account Project
678528WFS2 -L
Report To
West Fraser, Inc.
Greg Hicks
PO Box 384
Huttig, AR 71742
Report
Employee Owned Integrity Caring Continual Improvement
Table of Contents
PagesDescriptionReport Name
This report consists of this Table of Contents and the following pages:
678528_r03_03_ProjectResults_1355090 Ana-Lab Project P:678528 C:WFS2 1355090 Outfall 001 Permit Renewal 2 678528_r10_05_ProjectQC Ana-Lab Project P:678528 C:WFS2 Project Quality Control Groups 4 678528_r99_09_CoC__1_of_1 Ana-Lab CoC WFS2 678528_1_of_1 2
8 Total Pages:
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptTOC Created 10/06/2004 v1.1LDSClient v1.5.50.962
NELAP-accredited #T104704201
Report Page 1 of 9
1
2
3
4
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results12/10/2014Printed: Page 1 of 2
Report To
West Fraser, Inc.
Greg Hicks
PO Box 384
Huttig, AR 71742
678528WFS2-LAccount Project
Results
BottleCASFlagsRLUnitsResultsParameter
1355090 Outfall 001 Permit Renewal
12/04/2014 10:30:00M MatthewsCollected by:
12/04/2014Received:
Non-Potable Water Affiliation: West Fraser, Inc.
Prepared: 592828 12/05/2014 09:15:00
EPA 200.7 4.4 12/05/2014 15:29:28LPS QCgroup 592997Analyzed
2.40 mg/L 0.500 7439-95-4Magnesium, Total 05N
Prepared: 592833 12/05/2014 09:30:00
EPA 350.1 2 12/08/2014 10:00:00RSV QCgroup 593136Analyzed
0.111 mg/L 0.020Ammonia Nitrogen 06N
Prepared: 592807 12/10/2014 11:07:06
SM 5210 B-2001 12/10/2014 11:07:06MKC QCgroup 592807Analyzed
8.35 mg/L D2.00 1026-3Biochemical Oxygen Demand (BOD5) 01N
Prepared: 593365 12/09/2014 13:50:33
SM 5310 C-96 12/09/2014 13:50:33ALH QCgroup 593365Analyzed
6.87 mg/L 0.500Total Organic Carbon 03N
The above methods that we used are approved for NPDES reporting as listed in 40 CFR 136 Table 1B or Ana-Lab has specific approval from EPA to use
these methods for NPDES reporting.
Sample Preparation for Sample 1355090
1355090 Outfall 001 Permit Renewal 12/04/2014Received:
Prepared: 592828 12/05/2014 09:15:00
EPA 200.2 2.8 12/05/2014 09:15:00TES QCgroup 592828Analyzed
50/50 mlLiquid Metals Digestion 02N
Prepared: 592833 12/05/2014 09:30:00
EPA 350.2, Rev. 2.0 12/05/2014 09:30:00CDB QCgroup 592833Analyzed
50/50 mlAmmonia Distillation 04N
Prepared: 592807 12/05/2014 07:01:13
SM 5210 B-2001 12/05/2014 07:01:13MKC QCgroup 592807Analyzed
StartedBOD Set StartedN
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 2 of 9
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2
3
4
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement
Results12/10/2014Printed: Page 2 of 2
Qualifiers:
D - Duplicate RPD was higher than expected
We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's
corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US
Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate
TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking
Water Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of
Environmental Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana
Department of Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals
Drinking Water (NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment
Waste Water and Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not
covered under NELAC scope of accreditation.
These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of
Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.
RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical
Abstract Service number.
C. H. Whiteside, Ph.D., President
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 3 of 9
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3
4
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 1 of 412/10/2014Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
WFS2 -LAccount Project
West Fraser, Inc.
Greg Hicks
PO Box 384
Huttig, AR 71742
Report To001
678528
SM 5210 B-2001Non-Potable Water 592807
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Biochemical Oxygen
Demand (BOD5)
592807 0.11 0.200 0.500 mg/L 115028382
Biochemical Oxygen
Demand (BOD5)
592807 0.12 0.200 0.500 mg/L 115028431
Biochemical Oxygen
Demand (BOD5)
592807 0.18 0.200 0.500 mg/L 115028478
Biochemical Oxygen
Demand (BOD5)
592807 -0.04 0.200 0.500 mg/L 115028525
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Biochemical Oxygen
Demand (BOD5)
1354701 Duplicate 3.97 2.97 mg/L 28.8 20.0
Biochemical Oxygen
Demand (BOD5)
1354743 Duplicate 253 314 mg/L 21.5 20.0
Biochemical Oxygen
Demand (BOD5)
1354766 Duplicate 4.20 4.24 mg/L 0.948 20.0
Biochemical Oxygen
Demand (BOD5)
1354947 Duplicate 35.4 34.2 mg/L 3.45 20.0
Biochemical Oxygen
Demand (BOD5)
1354982 Duplicate 14.0 12.0 mg/L 15.4 20.0
Biochemical Oxygen
Demand (BOD5)
1355016 Duplicate 8.76 8.32 mg/L 5.15 20.0
Biochemical Oxygen
Demand (BOD5)
1355090 Duplicate 32.0 8.35 mg/L 117 20.0
Seed Drop
FileOutUnitsMQLMDLReadingPrepSetParameter
Biochemical Oxygen
Demand (BOD5)
592807 0.957 0.200 0.500 mg/L 115028383
Biochemical Oxygen
Demand (BOD5)
592807 1.03 0.200 0.500 mg/L 115028432
Biochemical Oxygen
Demand (BOD5)
592807 0.980 0.200 0.500 mg/L 115028479
Biochemical Oxygen
Demand (BOD5)
592807 1.02 0.200 0.500 mg/L 115028526
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Biochemical Oxygen
Demand (BOD5)
194 198 mg/L 98.0 83.7 - 116 115028384
Biochemical Oxygen
Demand (BOD5)
196 198 mg/L 99.0 83.7 - 116 115028433
Biochemical Oxygen
Demand (BOD5)
192 198 mg/L 97.0 83.7 - 116 115028480
Biochemical Oxygen
Demand (BOD5)
191 198 mg/L 96.5 83.7 - 116 115028527
EPA 350.1 2Non-Potable Water 593136
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 4 of 9
1
2
3
4
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 2 of 412/10/2014Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Ammonia Nitrogen 592833 ND 0.00974 0.020 mg/L 115035005
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115034983
Ammonia Nitrogen 1.96 2.00 mg/L 98.0 90.0 - 110 115034994
Ammonia Nitrogen 2.03 2.00 mg/L 102 90.0 - 110 115035002
Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115035011
Ammonia Nitrogen 1.98 2.00 mg/L 99.0 90.0 - 110 115035022
Ammonia Nitrogen 1.99 2.00 mg/L 99.5 90.0 - 110 115035029
Ammonia Nitrogen 2.02 2.00 mg/L 101 90.0 - 110 115035037
Ammonia Nitrogen 1.99 2.00 mg/L 99.5 90.0 - 110 115035050
Ammonia Nitrogen 2.00 2.00 mg/L 100 90.0 - 110 115035064
Ammonia Nitrogen 1.97 2.00 mg/L 98.5 90.0 - 110 115035071
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Ammonia Nitrogen 1354824 Duplicate 0.178 0.181 mg/L 1.67 20.0
Ammonia Nitrogen 1354837 Duplicate 0.265 0.279 mg/L 5.15 20.0
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Ammonia Nitrogen 2.17 2.00 mg/L 108 90.0 - 110 115034982
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Ammonia Nitrogen 592833 2.03 2.00 mg/L 101 90.0 - 110 115035006
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Ammonia Nitrogen 592833 2.03 2.11 2.00 90.0 - 110 101 106 mg/L 3.86 20.0
Mat. Spike
FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter
Ammonia Nitrogen 1354824 2.45 0.181 2.00 mg/L 113 80.0 - 120 115035010
Ammonia Nitrogen 1354837 2.43 0.279 2.00 mg/L 108 80.0 - 120 115035014
EPA 200.7 4.4Non-Potable Water 592997
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Magnesium, Total 592828 ND 0.0102 0.500 mg/L 115032566
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Magnesium, Total 26.4 25.0 mg/L 106 90.0 - 110 115032552
Magnesium, Total 25.8 25.0 mg/L 103 90.0 - 110 115032554
Magnesium, Total 25.2 25.0 mg/L 101 90.0 - 110 115032562
Magnesium, Total 24.6 25.0 mg/L 98.4 90.0 - 110 115032572
Magnesium, Total 24.7 25.0 mg/L 98.8 90.0 - 110 115032576
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Magnesium, Total 50.3 50.0 mg/L 101 95.0 - 105 115032547
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 5 of 9
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4
Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 3 of 412/10/2014Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Magnesium, Total 25.5 25.0 mg/L 102 90.0 - 110 115032551
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Magnesium, Total 592828 4.99 5.00 mg/L 99.7 85.0 - 115 115032567
LCS Dup
Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter
Magnesium, Total 592828 4.99 4.93 5.00 85.0 - 115 99.7 98.5 mg/L 1.21 25.0
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Magnesium, Total 1354973 5.70 0 0.988 5.00 75.0 - 125 94.2 mg/L 25.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Magnesium, Total 1354973 5.70 5.75 0.988 5.00 75.0 - 125 94.2 95.2 mg/L 1.06 25.0
SM 5310 C-96Non-Potable Water 593365
AWRL
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 2.22 2.00 mg/L 111 75.0 - 125 115040179
Blank
FileUnitsMQLMDLReadingPrepSetParameter
Total Organic Carbon 593365 0.110 0.0618 0.500 mg/L 115040178
Total Organic Carbon 593365 0.101 0.0618 0.500 mg/L 115040211
Total Organic Carbon 593365 0.0959 0.0618 0.500 mg/L 115040235
CCB
FileOutUnitsMQLMDLReadingPrepSetParameter
Total Organic Carbon 593365 0.137 0.0618 0.500 mg/L 115040172
Total Organic Carbon 593365 0.191 0.0618 0.500 mg/L 115040183
Total Organic Carbon 593365 0.148 0.0618 0.500 mg/L 115040188
Total Organic Carbon 593365 0.118 0.0618 0.500 mg/L 115040197
Total Organic Carbon 593365 0.0993 0.0618 0.500 mg/L 115040209
Total Organic Carbon 593365 0.175 0.0618 0.500 mg/L 115040222
Total Organic Carbon 593365 0.139 0.0618 0.500 mg/L 115040233
CCV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 10.4 10.0 mg/L 104 90.0 - 110 115040175
Total Organic Carbon 10.2 10.0 mg/L 102 90.0 - 110 115040184
Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040189
Total Organic Carbon 10.2 10.0 mg/L 102 90.0 - 110 115040198
Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040210
Total Organic Carbon 10.3 10.0 mg/L 103 90.0 - 110 115040223
Total Organic Carbon 10.6 10.0 mg/L 106 90.0 - 110 115040234
Duplicate
Limit%RPDUnitUnknownResultTypeSampleParameter
Total Organic Carbon 1355739 Duplicate 0.0885 0.0969 mg/L 9.06 20.0
Total Organic Carbon 1355739 Duplicate 0.0854 0.0969 mg/L 12.6 20.0
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 6 of 9
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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]
Quality Control Page 4 of 412/10/2014Printed
Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663
LELAP-accredited #02008
Employee Owned Integrity Caring Continual Improvement
ICL
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 20.7 20.0 mg/L 104 90.0 - 110 115040174
ICV
FileOutLimits%Recover%UnitsKnownReadingParameter
Total Organic Carbon 10.5 10.0 mg/L 105 90.0 - 110 115040176
LCS
OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter
Total Organic Carbon 593365 5.34 5.00 mg/L 107 85.0 - 115 115040177
Total Organic Carbon 593365 5.17 5.00 mg/L 103 85.0 - 115 115040212
Total Organic Carbon 593365 5.41 5.00 mg/L 108 85.0 - 115 115040236
MS
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Organic Carbon 1354322 14.3 0 4.28 10.0 70.0 - 130 100 mg/L 20.0
Total Organic Carbon 1354399 14.6 0 4.79 10.0 70.0 - 130 98.1 mg/L 20.0
Total Organic Carbon 1354454 12.0 0 1.89 10.0 70.0 - 130 101 mg/L 20.0
Total Organic Carbon 1354978 11.8 0 1.96 10.0 70.0 - 130 98.4 mg/L 20.0
MSD
Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter
Total Organic Carbon 1354322 14.3 14.1 4.28 10.0 70.0 - 130 100 98.2 mg/L 1.82 20.0
Total Organic Carbon 1354399 14.6 14.6 4.79 10.0 70.0 - 130 98.1 98.1 mg/L 0 20.0
Total Organic Carbon 1354454 12.0 11.7 1.89 10.0 70.0 - 130 101 98.1 mg/L 2.91 20.0
Total Organic Carbon 1354978 11.8 12.0 1.96 10.0 70.0 - 130 98.4 100 mg/L 1.61 20.0
Standard
FileOutLimits%Recover%UnitsKnownReadingSampleParameter
Total Organic Carbon 52.2 50.0 mg/L 104 90.0 - 110 115040173
RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%
Blank - Method Blank; LCS - Laboratory Control Sample; CCV - Continuing Calibration Verification; MS - Matrix Spike; ICV - Initial Calibration
Verification; CCB - Continuing Calibration Blank; AWRL - Ambient Water Reporting Limit
Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662
Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.5.50.962 www.ana-lab.com
Ark-La-Miss Region: 4720 Viking Dr. Suite A Bossier City LA 71111
NELAP-accredited #T104704201
Report Page 7 of 9
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