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June 6, 2017 U.S. Environmental Protection Agency Office of Ecosystem Protection EPA/OEP RGP Applications Coordinator 5 Post Office Square – Suite 100 (OEP06-01) Boston, MA 02109 [email protected] Subject: NPDES General Permit for Remediation Activity Discharges in Massachusetts
(NPDES Permit No. MAG910000) Tennessee Gas Pipeline Company, L.L.C. Connecticut Expansion Project To Whom it May Concern: Tennessee Gas Pipeline Company, L.L.C. (“Tennessee”) has proposed the Connecticut Expansion Project (“Project”) to upgrade its existing pipeline system in New York, Massachusetts and Connecticut. The Project is being developed to help meet the increased demand in the northeastern United States for transportation capacity of natural gas. Project facilities include 3.81 miles of new 36-inch outside diameter pipeline looping co-located within or adjacent to Tennessee’s existing right-of-way in Sandisfield, Massachusetts (“Massachusetts Loop”); 8.26 miles of new 24-inch outside diameter pipeline looping co-located within or adjacent to Tennessee’s existing right-of-way between Agawam, Massachusetts, and East Granby, Connecticut (“Connecticut Loop”); as well as appurtenant facilities. Tennessee has received a FERC Certificate (CP14-529-000), USACE 404 permit (NAE-2013-02329), MADEP 401 permit (X265051), Town of Sandisfield Order of Conditions (278-130), Town of Agawam Order of Conditions (087-0610), and USEPA NPDES General Permit for Stormwater Discharges from Construction Activities for the Project (MAR10000H). Tennessee began construction of the Project facilities in the spring of 2017 and proposes to place the facilities in-service by fall 2017. Hydrostatic testing is anticipated to be completed in the late summer or fall 2017, prior to placing the facilities in-service. Tennessee has prepared the attached Notice of Intent (NOI) to be covered under the General Permit for Remediation Activity Discharges (NPDES Permit No. MAG910000). In compliance with United States Department of Transportation (“DOT”) specifications, Tennessee will conduct, or cause to be conducted, hydrostatic testing on all pipeline loops prior to placing those loops in service, including the 3.81-mile Massachusetts Loop and approximately 861 feet of 12-inch to 25-inch outside diameter piping within the existing Agawam Compressor Station (“Station 261”). Sources of hydrostatic test water for the proposed Project in Massachusetts are identified in Table 1 below. The water from Lower Spectacle Pond in Sandisfield, Massachusetts will be used to test the Massachusetts Loop pipeline. The water from the hydrant in Agawam will be used to test the Station 261 piping. The approximately 0.11-mile portion of the pipeline loop in Agawam will be tested with water from a hydrant in East Granby, Connecticut, which will be discharged in East Granby, and is thus not covered under this General Permit.
2
The pipeline will be tested hydrostatically in accordance with the DOT’s regulations, 49 CFR Part 192. The pipeline will be filled with water and maintained at a test pressure and duration in compliance with Tennessee’s engineering standards and applicable federal regulations. Upon satisfactory completion of the hydrostatic tests, the wastewater will be discharged to an upland area through a dewatering structure consisting of an energy dissipation device and water filtration structure. Discharge will overland flow towards Spectacle Pond Brook in Sandisfield, and towards an unnamed tributary to Worthington Brook in Agawam. Environmental impacts from withdrawal and discharge of test water will be minimized by utilizing the measures outlined in FERC’s Upland Erosion Control, Revegetation, and Maintenance Plan and Wetland and Waterbody Construction and Mitigation Procedures, as well as by complying with all applicable federal, state, and local permit requirements including the effluent limitations, monitoring and reporting requirements as specified in General Permit.
TABLE 1 - POTENTIAL SOURCES OF HYDROSTATIC PRESSURE TEST WATER FOR THE PROJECT IN MASSACHUSETTS
Potential Source(s) Approximate
Milepost Water Quantity
(Gallons) Manifold / Discharge Location
Lower Spectacle Pond, Sandisfield, MA
N/A 547,797 Intersection of Proposed Access Road #3 and Cold Spring Road
Municipal hydrant, at entrance to Station 261, 1615 Suffield, St., Agawam, MA
N/A 15,390 Upland area within workspace at
beginning of proposed loop
TOTAL 563,187 -- Tennessee does not anticipate the use of any additives within the hydrostatic test water. Should it be determined that additives are necessary based on the source and composition of the test water, Tennessee will submit detailed information on any chemicals to the USEPA for review and approval prior to use. Tennessee has also developed a Best Management Practices Plan (“BMPP”) in accordance with Section 2.5.1 of the General Permit. Tennessee certifies that the BMPP meets the requirements of the General Permit and will be implemented upon initiation of discharge. Attached to this correspondence, please find the aforementioned NOI, mapping depicting the Project’s proposed facilities including the proposed hydrostatic fill and discharge locations, a figure depicting the typical hydrostatic test dewatering structure, the StreamStats reports for Spectacle Pond Brook and an unnamed tributary to Worthington Brook, and influent and receiving water sampling results. Should you require further information to facilitate this request, please do not hesitate to contact me at [email protected] or 860-763-6052. Thank you for your continued attention to this Project. Sincerely,
Brian M. Benito, Jr. Environmental Project Manager Tennessee Gas Pipeline Company, L.L.C.
3
cc. Shauna Little, USEPA, [email protected] Shelley Puleo, USEPA, [email protected] Town of Sandisfield Conservation Commission, [email protected] Town of Agawam Conservation Commission, [email protected] Enclosures:
Remediation General Permit Notice of Intent – Massachusetts Loop Remediation General Permit Notice of Intent – Station 261
U.S.G.S. Site Location Maps Site Plan for Massachusetts Loop
Site Plan for Station 261 StreamStats Flow Statistics Ungauged Site Report (Spectacle Pond Brook, Sandisfield,
MA) StreamStats Flow Statistics Ungauged Site Report (Unnamed Tributary to Worthington
Brook, Agawam, MA) Correspondence with USFWS regarding ESA eligibility Correspondence with MASHPO regarding NHPA eligibility
Influent and Receiving Water Sampling Results
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 14 of 24
II. Suggested Format for the Remediation General Permit Notice of Intent (NOI)
A. General site information:
1. Name of site: Site address:
Street:
City: State: Zip:
2. Site owner
Owner is (check one): Federal State/Tribal Private
Other; if so, specify:
Contact Person:
Telephone: Email:
Mailing address:
Street:
City: State: Zip:
3. Site operator, if different than owner Contact Person:
Telephone: Email:
Mailing address:
Street:
City: State: Zip:
4. NPDES permit number assigned by EPA:
NPDES permit is (check one): RGP DGP CGP MSGP
Individual NPDES permit Other; if so, specify:
5. Other regulatory program(s) that apply to the site (check all that apply):
MA Chapter 21e; list RTN(s):
NH Groundwater Management Permit or
Groundwater Release Detection Permit:
CERCLA
UIC Program
POTW Pretreatment
CWA Section 404
Connecticut Expansion ProjectMassachusetts Loop
Town Hill Road to S Beech Plain Road
Sandisfield MA 01255
Tennessee Gas Pipeline Company, LLC
x
Brian M. Benito, Jr.
860-763-6052 [email protected]
8 Anngina Drive
Enfield CT 06082
Same
x
x x
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 15 of 24
B. Receiving water information: 1. Name of receiving water(s): Waterbody identification of receiving water(s):
Receiving water is (check any that apply): Outstanding Resource Water Ocean Sanctuary territorial sea Wild and Scenic River
2. Has the applicant attached a location map in accordance with the instructions in B, above? (check one): Yes No
Are sensitive receptors present near the site? (check one): Yes No
If yes, specify:
3. Indicate if the receiving water(s) is listed in the State’s Integrated List of Waters (i.e., CWA Section 303(d)). Include which designated uses are impaired, and any
pollutants indicated. Also, indicate if a final TMDL is available for any of the indicated pollutants. For more information, contact the appropriate State as noted in Part
4.6 of the RGP.
4. Indicate the seven day-ten year low flow (7Q10) of the receiving water determined in accordance with the instructions in
Appendix V for sites located in Massachusetts and Appendix VI for sites located in New Hampshire.
5. Indicate the requested dilution factor for the calculation of water quality-based effluent limitations (WQBELs) determined in
accordance with the instructions in Appendix V for sites in Massachusetts and Appendix VI for sites in New Hampshire.
6. Has the applicant received confirmation from the appropriate State for the 7Q10and dilution factor indicated? (check one): Yes No
If yes, indicate date confirmation received:
7. Has the applicant attached a summary of receiving water sampling results as required in Part 4.2 of the RGP in accordance with the instruction in Appendix VIII?
(check one): Yes No
C. Source water information:
1. Source water(s) is (check any that apply):
Contaminated groundwater
Has the applicant attached a summary of influent
sampling results as required in Part 4.2 of the RGP
in accordance with the instruction in Appendix
VIII? (check one):
Yes No
Contaminated surface water
Has the applicant attached a summary of
influent sampling results as required in Part 4.2
of the RGP in accordance with the instruction in
Appendix VIII? (check one):
Yes No
The receiving water Potable water; if so, indicate
municipality or origin:
A surface water other
than the receiving water; if
so, indicate waterbody: Other; if so, specify:
Spectacle Pond Brook
Classification of receiving water(s):
Class B, CWF
xx
Wetlands located on east side of stream
Spectacle Pond Brook is not listed in the State's Integrated List of Waters
0.084 ft3/s
None
x
x
The outlet of Lower Spectacle Pond, where water will be withdrawn from, is the headwaters of Spectacle Pond Brook, approximately 1,400 feet upstream of the dischare location.
x
x
Lower Spectacle Pond
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 16 of 24
2. Source water contaminants:
a. For source waters that are contaminated groundwater or contaminated
surface water, indicate are any contaminants present that are not included in
the RGP? (check one): Yes No If yes, indicate the contaminant(s) and
the maximum concentration present in accordance with the instructions in
Appendix VIII.
b. For a source water that is a surface water other than the receiving water, potable water
or other, indicate any contaminants present at the maximum concentration in accordance
with the instructions in Appendix VIII? (check one): Yes No
3. Has the source water been previously chlorinated or otherwise contains residual chlorine? (check one): Yes No
D. Discharge information
1.The discharge(s) is a(n) (check any that apply): Existing discharge New discharge New source
Outfall(s): Outfall location(s): (Latitude, Longitude)
Discharges enter the receiving water(s) via (check any that apply): Direct discharge to the receiving water Indirect discharge, if so, specify:
A private storm sewer system A municipal storm sewer system, if the discharge enters the receiving water via a private or municipal storm sewer system:
Has notification been provided to the owner of this system? (check one): Yes No
Has the applicant has received permission from the owner to use such system for discharges? (check one): Yes No, if so, explain, with an estimated timeframe for
obtaining permission:
Has the applicant attached a summary of any additional requirements the owner of this system has specified? (check one): Yes No
Provide the expected start and end dates of discharge(s) (month/year): August 2017
Indicate if the discharge is expected to occur over a duration of: less than 12 months 12 months or more x is a short-term discharge
Has the applicant attached a site plan in accordance with the instructions in D, above? (check one): Yes No
x
x
-73.122348, 42.158859
xThe discharge will occurr in an upland area approximately 600 feet from Spectacle Pond Brook. Flows will radiate out and overland towards Sprectacle Pond Brook.
x
x
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 17 of 24
2. Activity Category: (check all that apply) 3. Contamination Type Category: (check all that apply)
I – Petroleum-Related Site Remediation
II – Non-Petroleum-Related Site Remediation
III – Contaminated Site Dewatering
IV – Dewatering of Pipelines and Tanks
V – Aquifer Pump Testing
VI – Well Development/Rehabilitation
VII – Collection Structure Dewatering/Remediation
VIII – Dredge-Related Dewatering
a. If Activity Category I or II: (check all that apply)
A. Inorganics
B. Non-Halogenated Volatile Organic Compounds
C. Halogenated Volatile Organic Compounds
D. Non-Halogenated Semi-Volatile Organic Compounds
E. Halogenated Semi-Volatile Organic Compounds
F. Fuels Parameters
b. If Activity Category III, IV, V, VI, VII or VIII: (check either G or H)
G. Sites with Known
Contamination H. Sites with Unknown Contamination
c. If Category III-G, IV-G, V-G, VI-G,
VII-G or VIII-G: (check all that apply)
A. Inorganics
B. Non-Halogenated Volatile
Organic Compounds
C. Halogenated Volatile Organic
Compounds
D. Non-Halogenated Semi-Volatile
Organic Compounds
E. Halogenated Semi-Volatile
Organic Compounds
F. Fuels Parameters
d. If Category III-H, IV-H, V-H, VI-H, VII-H or
VIII-H Contamination Type Categories A through
F apply
x x
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 18 of 24
4. Influent and Effluent Characteristics
Parameter Believed
absent
Believed
present
# of
samples
Test
method
(#)
Detection
limit
(µg/l)
Influent Effluent
Daily
maximum
(µg/l)
Daily
average
(µg/l)
Daily
maximum
(µg/l)
Daily
average
(µg/l)
TBEL WQBEL
a. Inorganics
Ammonia Report mg/L ---
Chloride Report µg/l ---
Total Residual Chlorine 0.2 mg/L
Total Suspended Solids 30 mg/L
Antimony 206 µg/L
Arsenic 104 µg/L
Cadmium 10.2 µg/L
Chromium III 323 µg/L
Chromium VI 323 µg/L
Copper 242 µg/L
Iron 5,000 µg/L
Lead 160 µg/L
Mercury 0.739 µg/L
Nickel 1,450 µg/L
Selenium 235.8 µg/L
Silver 35.1 µg/L
Zinc 420 µg/L
Cyanide 178 mg/L
b. Non-Halogenated VOCs
Total BTEX 100 µg/L ---
Benzene 5.0 µg/L ---
1,4 Dioxane 200 µg/L ---
Acetone 7.97 mg/L ---
Phenol 1,080 µg/L
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 19 of 24
Parameter Believed
absent
Believed
present
# of
samples
Test
method
(#)
Detection
limit
(µg/l)
Influent Effluent
Daily
maximum
(µg/l)
Daily
average
(µg/l)
Daily
maximum
(µg/l)
Daily
average
(µg/l)
TBEL WQBEL
c. Halogenated VOCs
Carbon Tetrachloride 4.4 µg/L
1,2 Dichlorobenzene 600 µg/L ---
1,3 Dichlorobenzene 320 µg/L ---
1,4 Dichlorobenzene 5.0 µg/L ---
Total dichlorobenzene 763 µg/L in NH ---
1,1 Dichloroethane 70 µg/L ---
1,2 Dichloroethane 5.0 µg/L ---
1,1 Dichloroethylene 3.2 µg/L ---
Ethylene Dibromide 0.05 µg/L ---
Methylene Chloride 4.6 µg/L ---
1,1,1 Trichloroethane 200 µg/L ---
1,1,2 Trichloroethane 5.0 µg/L ---
Trichloroethylene 5.0 µg/L ---
Tetrachloroethylene 5.0 µg/L
cis-1,2 Dichloroethylene 70 µg/L ---
Vinyl Chloride 2.0 µg/L ---
d. Non-Halogenated SVOCs
Total Phthalates 190 µg/L
Diethylhexyl phthalate 101 µg/L
Total Group I PAHs 1.0 µg/L ---
Benzo(a)anthracene
As Total PAHs
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Chrysene
Dibenzo(a,h)anthracene
Indeno(1,2,3-cd)pyrene
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 20 of 24
Parameter Believed
absent
Believed
present
# of
samples
Test
method
(#)
Detection
limit
(µg/l)
Influent Effluent
Daily
maximum
(µg/l)
Daily
average
(µg/l)
Daily
maximum
(µg/l)
Daily
average
(µg/l)
TBEL WQBEL
Total Group II PAHs 100 µg/L ---
Naphthalene 20 µg/L ---
e. Halogenated SVOCs
Total PCBs 0.000064 µg/L ---
Pentachlorophenol 1.0 µg/L --- f. Fuels Parameters
Total Petroleum
Hydrocarbons 5.0 mg/L
---
Ethanol Report mg/L ---
Methyl-tert-Butyl Ether 70 µg/L
tert-Butyl Alcohol 120 µg/L in MA
40 µg/L in NH
---
tert-Amyl Methyl Ether90 µg/L in MA
140 µg/L in NH
---
Other (i.e., pH, temperature, hardness, salinity, LC50, additional pollutants present); if so, specify:
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 21 of 24
E. Treatment system information
1. 1. Indicate the type(s) of treatment that will be applied to effluent prior to discharge: (check all that apply)
Adsorption/Absorption Advanced Oxidation Processes Air Stripping Granulated Activated Carbon (“GAC”)/Liquid Phase Carbon Adsorption
Ion Exchange Precipitation/Coagulation/Flocculation Separation/Filtration Other; if so, specify:
2.2.
Identify each major treatment component (check any that apply):
Fractionation tanks Equalization tank Oil/water separator Mechanical filter Media filter
Chemical feed tank Air stripping unit Bag filter Other; if so, specify:
Indicate if either of the following will occur (check any that apply):
Chlorination De-chlorination
3. Provide the design flow capacity in gallons per minute (gpm) of the most limiting component.
Indicate the most limiting component:
Is use of a flow meter feasible? (check one): Yes No, if so, provide justification:
Provide the proposed maximum effluent flow in gpm.
Provide the average effluent flow in gpm.
If Activity Category IV applies, indicate the estimated total volume of water that will be discharged:
4. Has the applicant attached a schematic of flow in accordance with the instructions in E, above? (check one): Yes No
x
Energy diffusion device and water filtration structure
Provide a written description of all treatment system(s) or processes that will be applied to the effluent prior to discharge.
The discharge rate of the test water will be regulated using a gate valve and energy dissipation devices to control flow and prevent erosion or scouring. Tennessee will monitor the discharge flow with a continuous total flow meter to ensure that it does not exceed 694 gmp (1 mgd). See Attached figure No. 46 for detail of the dewatering structure.
x Energy diffusion device and water filtration structure
x
694 gpm
600 gpm
547,797 gal
x
2,200 gpm
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 22 of 24
F. Chemical and additive information 1. Indicate the type(s) of chemical or additive that will be applied to effluent prior to discharge or that may otherwise be present in the discharge(s):
(check all that apply)
Algaecides/biocides Antifoams Coagulants Corrosion/scale inhibitors Disinfectants Flocculants Neutralizing agents Oxidants Oxygen
scavengers pH conditioners Bioremedial agents, including microbes Chlorine or chemicals containing chlorine Other; if so, specify:
2. Provide the following information for each chemical/additive, using attachments, if necessary:
a. Product name, chemical formula, and manufacturer of the chemical/additive;
b. Purpose or use of the chemical/additive or remedial agent;
c. Material Safety Data Sheet (MSDS) and Chemical Abstracts Service (CAS) Registry number for each chemical/additive;
d. The frequency (hourly, daily, etc.), duration (hours, days), quantity (maximum and average), and method of application for the chemical/additive;
e. Any material compatibility risks for storage and/or use including the control measures used to minimize such risks; and
f. If available, the vendor's reported aquatic toxicity (NOAEL and/or LC50 in percent for aquatic organism(s)).
3. Has the applicant attached an explanation which demonstrates that the addition of such chemicals/additives may be authorized under this general permit in accordance
with the instructions in F, above? (check one): Yes No; if no, has the applicant attached data that demonstrates each of the 126 priority pollutants in CWA Section
307(a) and 40 CFR Part 423.15(j)(1) are non-detect in discharges with the addition of the proposed chemical/additive?
(check one): Yes No
G. Endangered Species Act eligibility determination
1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit:
Criterion A: No endangered or threatened species or critical habitat are in proximity to the discharge(s) or related activities or come in contact with the
“action area”.
Criterion B: Formal or informal consultation with the Services under section 7 of the ESA resulted in either a no jeopardy opinion (formal consultation) or a
written concurrence by the Services on a finding that the discharges and related activities are “not likely to adversely affect” listed species or critical habitat
(informal consultation). Has the applicant completed consultation with the Services? (check one): Yes No; if no, is consultation underway? (check
one): Yes No
Criterion C: Using the best scientific and commercial data available, the effect of the discharge(s) and related activities on listed species and critical habitat
have been evaluated. The discharge(s) and related activities will have “no affect” on any federally threatened or endangered listed species or designated
critical habitat under the jurisdiction of the Services. This determination was made by: (check one) the applicant EPA Other; if so, specify:
No additives will be used
N/A
x
x
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 23 of 24
2. Has the applicant attached supporting documentation of ESA eligibility in accordance with the instructions in G, above? (check one): Yes No
Does the supporting documentation include any written concurrence or finding provided by the Services? (check one): Yes No
H. National Historic Preservation Act eligibility determination 1. Indicate under which criterion the discharge(s) is eligible for coverage under this general permit:
Criterion A: No historic properties are present. The discharges and discharge-related activities (e.g., BMPs) do not have the potential to cause effects on
historic properties.
Criterion B: Historic properties are present. Discharges and discharge related activities do not have the potential to cause effects on historic properties.
Criterion C: Historic properties are present. The discharges and discharge-related activities have the potential to have an effect or will have an adverse
effect on historic properties.
2. Has the applicant attached supporting documentation of NHPA eligibility in accordance with the instructions in H, above? (check one): Yes No
Does the supporting documentation include any written agreement with the State Historic Preservation Officer (SHPO), Tribal Historic Preservation Officer (TPHO), or
other tribal representative that outlines measures the applicant will carry out to mitigate or prevent any adverse effects on historic properties? (check one): Yes No
I. Supplemental information
Describe any supplemental information being provided with the NOI. Include attachments if required or otherwise necessary.
Has the applicant attached data, including any laboratory case narrative and chain of custody used to support the application? (check one): Yes No
Has the applicant attached the certification requirement for the Best Management Practices Plan (BMPP)? (check one): Yes No
x
x
x
x
x
x
x
Tennessee Gas Pipeline Company, LLC (Tennessee) is seeking coverage to discharge of water resulting from a hydrostatic test of a new 3.81-mile section of 36" pipeline loop in Sandisfield, MA (Massachusetts Loop) and 861 feet of 12"-25" diameter pipe within the existing Agawam Compressor Station (Station 261). The intake for the Massachusetts Loop will occur from Lower Spectacle Pond, off Cold Spring Road. The discharge will occur in an upland area near where Proposed Temporary Access Road #3 enters the ROW. The intake for the Station 261 piping will occur from a Hydrant on Suffield Street. The discharge will occur in an upland area adjacet to Station 261. A seperate NOI for the Station 261 is included, however, Tennessee requests the use of one RGP for both discharges. These tests are necessary to evaluate the integrity of the pipeline.
MAG910000 Appendix IV – Part 1 – NOI
NHG910000 Page 24 of 24
J. Certification requirement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure
that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, I certify that the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I certify that I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing
violations.
Notification provided to the appropriate State, if required, including a copy of this NOI. Check one: Yes No NA
Notification provided to the municipality in which the discharge is located, including a copy of this NOI, if requested. Check one: Yes No
Notification provided to the owner of a private or municipal storm sewer system, if such system is used for site
discharges, including a copy of this NOI, if requested.
Permission obtained from the owner of a private or municipal storm sewer system, if such system is used for site
discharges. If yes, attach additional conditions. If no, attach explanation and timeframe for obtaining permission.
Check one: Yes No NA
Check one: Yes No NA Notification provided to the owner/operator of the area associated with activities covered by an additional discharge
permit(s). Additional discharge permit is (check one): RGP DGP CGP MSGP Individual NPDES permit
Other; if so, specify:
Check one: Yes No NA
Signature: Date:
Print Name and Title:
x
x
Brian M. Benito, Jr., Project Manager
Tennessee Gas Pipeline Company, LLC, NPDES ID MAR10000H
June 6, 2017
U.S.G.S. SITE LOCATION MAPS
PA
NH
CT
VT
NJ
RI
ME
NY
Tennessee Gas Pipeline Company
CT Expansion Project
Site Location
January 2016
Path: Y:\Projects\Tennessee_Gas\CT_Expansion_Project\Maps\Pipeyards\2015_02_10\CT_Expansion_Pipeyards_aerial.mxd
!( !(
!(!(
!(
!(!(
!( !(
South BeechPlain Pipeyard
BerkshireCounty
HampdenCounty
Otis
Monterey
Sandisfield
Tolland
MP 0 MP 0.5MP 1 MP 1.5
MP 2
MP 2.5MP 3 MP 3.5 MP 3.81
1 inch = 2,000 feet0 2,000 4,0001,000Feet
.Figure 1
Legend!( Mileposts
Access Roads
Proposed Project Centerline
Pipeyards
County Boundary
Town Boundary
Massachusetts Loop
Tennessee Gas Pipeline Company, L.L.C.Connecticut Expansion ProjectUSGS Site Topographic Map
Connecticut
Site Location
April 15, 2015
Path: Y:\Projects\Tennessee_Gas\CT_Expansion_Project\Maps\Topos\CT_Expansion_CT_Loop_Topo.mxd
!(
!(
!(
!(
!(
!(
!(
!(
!.
CT-5CT-1
CT-4
CT-2CT-3
CT-4A
Hickory StreetPipeyard
CompressorStation 261
Muddy BrookCrossing
HampdenCounty
HartfordCounty
Suffield
Enfield
Agawam
Longmeadow
Copyright:© 2013 National Geographic Society, i-cubed
NY
MA
CT
VT NH
1 inch = 2,000 feet0 2,000 4,0001,000
Feet
.
Legend!( Mileposts
!. Existing Compressor StationCenterline RouteAccess RoadsRivers and StreamsPipeyardsTown BoundaryCounty Boundary
Figure 1
Page 1
SITE PLAN FOR MASSACHSUETTS LOOP
WORKSPACE
MATERIAL
REVISIONSPIPE SUMMARY
ALI
GN
ME
NT
STR
IP M
AP
PIP
ELI
NE
STA
TIO
NIN
G
OWNERSHIPL.L. NO.
PROFILE
ENVIRONMENTAL
REFERENCE DRAWINGS
LINE LIST
PROTECTIONEASEMENT
RODS
SOIL TYPE
COATING/PADDING SUMMARY
SCHEMATIC
a Kinder Morgan company
Tennessee Gas PipelineCompany, L.L.C.
LIMITS OF
DISTURBANCE
1" = 200'
TO-T12-200-3-142A
75B Pillsbury loam, 0 to 8 percent slopes, extremelystony
905C Peru-Marlow association, rolling, extremely stony
901E Berkshire-Marlow association, 15 to 45 percentslopes, steep, extremely stony
904E Lyman-Tunbridge association, steep, very stony
CONNECTICUT EXPANSION PROJECTMASSACHUSETTS LOOP 200-3
PROPOSED 36" NATURAL GAS PIPELINE
BERKSHIRE COUNTY,MASSACHUSETTS
67158
WORKSPACE INSETS
K
Flow
Influent monitoring location
Effluent monitoring location
Receiving water monitoring location
SITE PLAN FOR STATION 261
STREAM STATS FLOW STATISTICS FOR UNGAUGED SITE REPORT (SPECTACLE POND BROOK, SANDISFIELD, MA)
StreamStats Report for Spectacle Pond Brook
Flow-Duration Statistics Parameters [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 3.36 square miles 1.61 149
DRFTPERSTR Stratified Dri埔 per StreamLength
0 square mile permile
0 1.29
MAREGION Massachusetts Region 1 dimensionless 0 1
BSLDEM250 Mean Basin Slope from 250KDEM
4.294 percent 0.32 24.6
Region ID:MAWorkspace ID:MA20170523125413378000Clicked Point (Latitude, Longitude):42.15793, -73.12099Time:2017-05-23 14:54:38 -0400
Flow-Duration Statistics Flow Report [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value UnitAverage standard error (ofeither estimate or prediction)
LowerPredictionInterval
UpperPredictionInterval
50 PercentDuration
3.29 埔^3/s 17.6 1.47 7.3
60 PercentDuration
2.05 埔^3/s 19.8 0.734 5.7
70 PercentDuration
1.29 埔^3/s 23.5 0.47 3.5
75 PercentDuration
1 埔^3/s 25.8 0.374 2.65
80 PercentDuration
0.685 埔^3/s 28.4 0.236 1.96
85 PercentDuration
0.507 埔^3/s 31.9 0.159 1.59
90 PercentDuration
0.325 埔^3/s 36.6 0.101 1.02
95 PercentDuration
0.201 埔^3/s 45.6 0.0569 0.685
98 PercentDuration
0.137 埔^3/s 60.3 0.0342 0.52
99 PercentDuration
0.0999 埔^3/s 65.1 0.0234 0.401
Flow-Duration Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
Low-Flow Statistics Parameters [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 3.36 square miles 1.61 149
DRFTPERSTR Stratified Dri埔 per StreamLength
0 square mile permile
0 1.29
BSLDEM250 Mean Basin Slope from 250KDEM
4.294 percent 0.32 24.6
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
MAREGION Massachusetts Region 1 dimensionless 0 1
Low-Flow Statistics Flow Report [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value UnitAverage standard error (ofeither estimate or prediction)
LowerPredictionInterval
UpperPredictionInterval
7 Day 2 YearLow Flow
0.222 埔^3/s 49.5 0.0578 0.819
7 Day 10 YearLow Flow
0.084 埔^3/s 70.8 0.0174 0.377
Low-Flow Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
August Flow-Duration Statistics Parameters [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 3.36 square miles 1.61 149
DRFTPERSTR Stratified Dri埔 per StreamLength
0 square mile permile
0 1.29
BSLDEM250 Mean Basin Slope from 250KDEM
4.294 percent 0.32 24.6
MAREGION Massachusetts Region 1 dimensionless 0 1
August Flow-Duration Statistics Flow Report [100 Percent (3.36 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value UnitAverage standard error (ofeither estimate or prediction)
LowerPredictionInterval
UpperPredictionInterval
August 50PercentDuration
0.559 埔^3/s 33.2 0.179 1.71
August Flow-Duration Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
Bankfull Statistics Parameters [100 Percent (3.36 square miles) Bankful l Statewide SIR2013 5155]
Parameter Code Parameter Name Value Units Min Limit Max Limit
DRNAREA Drainage Area 3.36 square miles 0.6 329
BSLDEM10M Mean Basin Slope from 10m DEM 9.409 percent 2.2 23.9
Bankfull Statistics Flow Report [100 Percent (3.36 square miles) Bankful l Statewide SIR2013 5155]
Statistic Value Unit Average standard error of prediction
Bankfull Width 25.4 埔 21.3
Bankfull Depth 1.4 埔 19.8
Bankfull Area 35.3 埔^2 29
Bankfull Streamflow 115 埔^3/s 55
Bankfull Statistics Citations
Bent, G.C., and Waite, A.M.,2013, Equations for estimating bankfull channel geometry anddischarge for streams in Massachusetts: U.S. Geological Survey Scientific Investigations Report2013–5155, 62 p., (http://pubs.usgs.gov/sir/2013/5155/)
Probability Statistics Parameters [100 Percent (3.36 square miles) Perennial Flow Probabil i ty]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 3.36 square miles 0.01 1.99
PCTSNDGRV Percent Underlain By Sand AndGravel
0 percent 0 100
FOREST Percent Forest 78.58 percent 0 100
MAREGION Massachusetts Region 1 dimensionless 0 1
Probability Statistics Disclaimers [100 Percent (3.36 square miles) Perennial Flow Probabil i ty]
One or more of the parameters is outside the suggested range. Estimates were extrapolated with unknownerrors
Probability Statistics Flow Report [100 Percent (3.36 square miles) Perennial Flow Probabil i ty]
Statistic Value Unit
Probability Stream Flowing Perennially 0.949 dim
Probability Statistics Citations
Bent, G.C., and Steeves, P.A.,2006, A revised logistic regression equation and an automatedprocedure for mapping the probability of a stream flowing perennially in Massachusetts: U.S.Geological Survey Scientific Investigations Report 2006–5031, 107 p.(http://pubs.usgs.gov/sir/2006/5031/pdfs/SIR_2006-5031rev.pdf )
STREAM STATS FLOW STATISTICS FOR UNGAUGED SITE REPORT (UNNAMED TRIBUTARY TO WORTHINGTON BROOK,
AGAWAM, MA)
StreamStats Report for Unnamed Tributary to Worthington Brook
Flow-Duration Statistics Parameters [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 0.66 square miles 1.61 149
DRFTPERSTR Stratified Driퟬ per StreamLength
0.14 square mile permile
0 1.29
MAREGION Massachusetts Region 1 dimensionless 0 1
BSLDEM250 Mean Basin Slope from 250KDEM
1.089 percent 0.32 24.6
Region ID:MAWorkspace ID:MA20170523130055542000Clicked Point (Latitude, Longitude):42.03474, -72.63469Time:2017-05-23 15:01:22 -0400
Flow-Duration Statistics Disclaimers [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
One or more of the parameters is outside the suggested range. Estimates were extrapolated with unknownerrors
Flow-Duration Statistics Flow Report [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value Unit
50 Percent Duration 0.625 ퟬ^3/s
60 Percent Duration 0.414 ퟬ^3/s
70 Percent Duration 0.309 ퟬ^3/s
75 Percent Duration 0.252 ퟬ^3/s
80 Percent Duration 0.172 ퟬ^3/s
85 Percent Duration 0.118 ퟬ^3/s
90 Percent Duration 0.077 ퟬ^3/s
95 Percent Duration 0.0416 ퟬ^3/s
98 Percent Duration 0.0305 ퟬ^3/s
99 Percent Duration 0.0211 ퟬ^3/s
Flow-Duration Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
Low-Flow Statistics Parameters [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 0.66 square miles 1.61 149
DRFTPERSTR Stratified Driퟬ per StreamLength
0.14 square mile permile
0 1.29
BSLDEM250 Mean Basin Slope from 250KDEM
1.089 percent 0.32 24.6
MAREGION Massachusetts Region 1 dimensionless 0 1
Low-Flow Statistics Disclaimers [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
One or more of the parameters is outside the suggested range. Estimates were extrapolated with unknownerrors
Low-Flow Statistics Flow Report [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value Unit
7 Day 2 Year Low Flow 0.0515 ퟬ^3/s
7 Day 10 Year Low Flow 0.0174 ퟬ^3/s
Low-Flow Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
August Flow-Duration Statistics Parameters [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 0.66 square miles 1.61 149
DRFTPERSTR Stratified Driퟬ per StreamLength
0.14 square mile permile
0 1.29
BSLDEM250 Mean Basin Slope from 250KDEM
1.089 percent 0.32 24.6
MAREGION Massachusetts Region 1 dimensionless 0 1
August Flow-Duration Statistics Disclaimers [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
One or more of the parameters is outside the suggested range. Estimates were extrapolated with unknownerrors
August Flow-Duration Statistics Flow Report [100 Percent (0.657 square miles) Statewide Low Flow WRIR00 4135]
Statistic Value Unit
August 50 Percent Duration 0.146 ퟬ^3/s
August Flow-Duration Statistics Citations
Ries, K.G., III,2000, Methods for estimating low-flow statistics for Massachusetts streams: U.S.Geological Survey Water Resources Investigations Report 00-4135, 81 p.(http://pubs.usgs.gov/wri/wri004135/)
Bankfull Statistics Parameters [100 Percent (0.657 square miles) Bankful l Statewide SIR2013 5155]
Parameter Code Parameter Name Value Units Min Limit Max Limit
DRNAREA Drainage Area 0.66 square miles 0.6 329
BSLDEM10M Mean Basin Slope from 10m DEM 4.025 percent 2.2 23.9
Bankfull Statistics Flow Report [100 Percent (0.657 square miles) Bankful l Statewide SIR2013 5155]
Statistic Value Unit Average standard error of prediction
Bankfull Width 11.6 ퟬ 21.3
Bankfull Depth 0.781 ퟬ 19.8
Bankfull Area 8.9 ퟬ^2 29
Bankfull Streamflow 17.5 ퟬ^3/s 55
Bankfull Statistics Citations
Bent, G.C., and Waite, A.M.,2013, Equations for estimating bankfull channel geometry anddischarge for streams in Massachusetts: U.S. Geological Survey Scientific Investigations Report2013–5155, 62 p., (http://pubs.usgs.gov/sir/2013/5155/)
Probability Statistics Parameters [100 Percent (0.657 square miles) Perennial Flow Probabil i ty]
ParameterCode Parameter Name Value Units
MinLimit
MaxLimit
DRNAREA Drainage Area 0.66 square miles 0.01 1.99
PCTSNDGRV Percent Underlain By Sand AndGravel
47.31 percent 0 100
FOREST Percent Forest 10.99 percent 0 100
MAREGION Massachusetts Region 1 dimensionless 0 1
Probability Statistics Flow Report [100 Percent (0.657 square miles) Perennial Flow Probabil i ty]
Statistic Value UnitPercentCorrect
Lower PredictionInterval
Upper PredictionInterval
Probability Stream FlowingPerennially
0.968 dim 71
Probability Statistics Citations
Bent, G.C., and Steeves, P.A.,2006, A revised logistic regression equation and an automatedprocedure for mapping the probability of a stream flowing perennially in Massachusetts: U.S.
CORRESPONDENCE WITH USFWS REGARDING ESA ELIGIBILITY
1
Miller, Shannon
From: Miller, ShannonSent: Wednesday, April 13, 2016 2:04 PMTo: Miller, ShannonSubject: FW: CT Expansion Project
-------- Original message -------- From: "Tur, Maria" <[email protected]> Date: 4/12/16 16:42 (GMT-05:00) To: "Benito, Brian" <[email protected]> Subject: CT Expansion Project Dear Mr. Benito, We have received and reviewed the Northern Long-Eared Bat 4(d) Rule Streamlined Consultation Form for the Connecticut Expansion Project. By signing the form, you (as the designated non-federal representative for FERC for this project), have indicated that any resulting incidental take of the northern long-eared bat is not prohibited by the final 4(d) rule. Maria E. Tur U.S. Fish and Wildlife Service New England Field Office 70 Commercial Street, Suite 300 Concord, NH 03301 Phone (603) 223-2541 x6419 FAX (603) 223-0104 http://www.fws.gov/newengland/
Northern Long-Eared Bat 4(d) Rule Streamlined Consultation Form
Federal agencies should use this form for the optional streamlined consultation framework for the northern long-eared bat (NLEB). This framework allows federal agencies to rely upon the U.S. Fish and Wildlife Service’s (USFWS) January 5, 2016, intra-Service Programmatic Biological Opinion (BO) on the final 4(d) rule for the NLEB for section 7(a)(2) compliance by: (1) notifying the USFWS that an action agency will use the streamlined framework; (2) describing the project with sufficient detail to support the required determination; and (3) enabling the USFWS to track effects and determine if reinitiation of consultation is required per 50 CFR 402.16.
This form is not necessary if an agency determines that a proposed action will have no effect to the NLEB or if the USFWS has concurred in writing with an agency's determination that a proposed action may affect, but is not likely to adversely affect the NLEB (i.e., the standard informal consultation process). Actions that may cause prohibited incidental take require separate formal consultation. Providing this information does not address section 7(a)(2) compliance for any other listed species.
Information to Determine 4(d) Rule Compliance: YES NO 1. Does the project occur wholly outside of the WNS Zone1? 2. Have you contacted the appropriate agency2 to determine if your project is near
known hibernacula or maternity roost trees?
3. Could the project disturb hibernating NLEBs in a known hibernaculum? 4. Could the project alter the entrance or interior environment of a known
hibernaculum?
5. Does the project remove any trees within 0.25 miles of a known hibernaculum at any time of year?
6. Would the project cut or destroy known occupied maternity roost trees, or any other trees within a 150-foot radius from the maternity roost tree from June 1 through July 31.
You are eligible to use this form if you have answered yes to question #1 or yes to question #2 and no to questions 3, 4, 5 and 6. The remainder of the form will be used by the USFWS to track our assumptions in the BO.
Agency and Applicant3 (Name, Email, Phone No.): Brian Benito Jr., [email protected], 860-763-6052
Project Name: Connecticut Expansion Project
Project Location (include coordinates if known): Along an existing pipeline corridor in Bethlehem, NY between 42.591222, -73.872989 & 42.589802, -73.836526; Sandisfield, MA between 42.178203, -73.145388 42.139793, -73.092106; Agawam, MA between 42.034026, -72.634128 & 41.929292, -72.715990 in East Granby, CT.
Basic Project Description (provide narrative below or attach additional information): Tennessee Gas Pipeline Company, L.L.C. (“Tennessee”) is proposing the construction and operation of the Connecticut Expansion Project (the “Project”) in Hartford County, Connecticut, Albany County, New York, and Berkshire and Hampden Counties, Massachusetts. The proposed Project involves the construction of two sections 1 http://www.fws.gov/midwest/endangered/mammals/nleb/pdf/WNSZone.pdf 2 See http://www.fws.gov/midwest/endangered/mammals/nleb/nhisites.html 3 If applicable - only needed for federal actions with applicants (e.g., for a permit, etc.) who are party to the consultation.
of new 36-inch outside diameter (“OD”) pipeline looping, totaling 1.35 miles in New York (“New York Loop”), 3.81 miles in Massachusetts (“Massachusetts Loop”), and one section of new 24-inch OD pipeline looping totaling 8.26 miles in Massachusetts and Connecticut (“Connecticut Loop”), as well as appurtenant facilities, including one new main line valve (“MLV”), cathodic protection, and pig launchers and receivers. To the extent that it is practicable, feasible, and in compliance with existing law, Tennessee proposes to locate the pipeline loops within or adjacent to its rights-of-way (“ROW”) associated with its existing pipelines designated as the 200 and 300 Lines.
General Project Information YES NO Does the project occur within 0.25 miles of a known hibernaculum? Does the project occur within 150 feet of a known maternity roost tree? Does the project include forest conversion4? (if yes, report acreage below)
Estimated total acres of forest conversion NY Loop: 3.81 MA Loop: 38.96 CT Loop: 33.97
If known, estimated acres5 of forest conversion from April 1 to October 31 Same as above If known, estimated acres of forest conversion from June 1 to July 316 None
Does the project include timber harvest? (if yes, report acreage below) Estimated total acres of timber harvest See above If known, estimated acres of timber harvest from April 1 to October 31 See above If known, estimated acres of timber harvest from June 1 to July 31 See above
Does the project include prescribed fire? (if yes, report acreage below) Estimated total acres of prescribed fire If known, estimated acres of prescribed fire from April 1 to October 31 If known, estimated acres of prescribed fire from June 1 to July 31
Does the project install new wind turbines? (if yes, report capacity in MW below) Estimated wind capacity (MW)
Agency Determination:
By signing this form, the action agency determines that this project may affect the NLEB, but that any resulting incidental take of the NLEB is not prohibited by the final 4(d) rule.
If the USFWS does not respond within 30 days from submittal of this form, the action agency may presume that its determination is informed by the best available information and that its project responsibilities under 7(a)(2) with respect to the NLEB are fulfilled through the USFWS January 5, 2016, Programmatic BO. The action agency will update this determination annually for multi-year activities.
The action agency understands that the USFWS presumes that all activities are implemented as described herein. The action agency will promptly report any departures from the described activities to the appropriate USFWS Field Office. The action agency will provide the appropriate USFWS Field Office with the results of any surveys conducted for the NLEB. Involved parties will promptly notify the appropriate USFWS Field Office upon finding a dead, injured, or sick NLEB.
Signature: Date Submitted: 04/12/16
4 Any activity that temporarily or permanently removes suitable forested habitat, including, but not limited to, tree removal from development, energy production and transmission, mining, agriculture, etc. (see page 48 of the BO). 5 If the project removes less than 10 trees and the acreage is unknown, report the acreage as less than 0.1 acre. 6 If the activity includes tree clearing in June and July, also include those acreage in April to October.
United States Department of the Interior
FISH AND WILDLIFE SERVICE
~%$4%URIS
New England Field Offic70 Commercial Street, Suite 300
Concord, NH 03301-5087http: //www.fws.gov/newengland
Subject: Connecticut Expansion Project (Docket I/ CP14-529-000)
Kimberly D. Bose, SecretaryFederal Energy Regulatory Commission888 First Street, N.E., Room 1A 5ORIGINALWashington, DC 20426
Dear Ms. Bose:
eII
Kl ~~pnm
Ilco~I Q
20+
This responds to your letter, dated May 3, 2016, regarding the Tennessee Gas PipelineCompany's Connecticut Expansion Project (Project), requesting that we concur with yourdetermination that the Project may effect, but is not likely to adversely affect, the federallyendangered Indiana bat (Myotis sodalist). Your request and our response are provided inaccordance with section 7 of the Endangered Species Act (87 Stat. 884, as amended; 16 U.S.C.1531,et set/.).
The purpose of the Project is to upgrade an existing pipeline system in New York,Massachusetts, and Connecticut, to transport natural gas. The Project would install
approximately 13,3 miles of pipeline looping (installation of new pipeline along existing pipelinewithin active rights-of-way). This concurrence request is for 1.4 miles of a new 36-inch-diameternatural gas pipeline loop in Albany County, New York. Due to the extremely low likelihood thatIndiana bats would be present within the project area, Tennessee Gas is not proposing any time-
of-year restrictions on project activities.
The U.S. Fish and Wildlife Service does not anticipate any adverse impacts to the Indiana bat asa result of this Project. While there is a historical occurrence record for this species within theproposed project area, and suitable roosting and/or foraging habitat also may be present, adverseeffects to Indiana bats are highly unlikely, because exceedingly low numbers of individuals, ifany, remain in the project area subsequent to white nose syndrome. Therefore, we concur with
your determination that the Project may affect, but is not likely to adversely affect the Indianabat. Further consultation with our office is not required at this time. If the proposed actionchanges, which may affect a listed species or critical habitat in a manner not considered by ouroflice, please contact us immediately to determine if additional consultation is required.
20160628-0029 FERC PDF (Unofficial) 06/28/2016
Kimberly D. BoseJune 24, 2016
Thank you for your coordination on this project. Please contact Ms. Maria Tur of this office at603-223-2541 with any additional information or for further assistance.
Sincerely yours,
Thomas R. ChapmanSupervisorNew England Field Office
20160628-0029 FERC PDF (Unofficial) 06/28/2016
Kimberly D. BoseJune 24, 2016
CC:
ES:
Reading fileShannon Jones (shannon. jones(@fere.gov)Elaine P. Baum (elaine.baumfere.gov)NYFO, Patricia Cole, Noelle Rayman, David StilwellMTur:6-24-16:603-223-2541
20160628-0029 FERC PDF (Unofficial) 06/28/2016
Document Content(s)
14288197.tif..........................................................1-3
20160628-0029 FERC PDF (Unofficial) 06/28/2016
CORRESPONDENCE WITH MASHPO REGARDING NHPA ELIGIBILITY
INFLUENT AND RECEIVING WATER SAMPLING RESULTS
Report Date:
07-Apr-17 13:56
ü Final Report
Re-Issued Report
Revised Report
Laboratory Report
AECOM Environment
10 Orms Street; Suite 405
Providence, RI 02904
Attn: Eric Olson
Project:
Project #:
Agawam Comp Station & Pond Stream, MA
60306709-452
Laboratory ID Client Sample ID Matrix Date Sampled Date Received
SC32894-01 ACS-1 (Hydrant) Drinking Water 28-Mar-17 08:45 28-Mar-17 15:43
SC32894-02 ACS-2 (Stream) Surface Water 28-Mar-17 09:30 28-Mar-17 15:43
SC32894-03 SPB-1 (Brook) Surface Water 28-Mar-17 12:30 28-Mar-17 15:43
SC32894-04 LSP-1 (Pond) Surface Water 28-Mar-17 13:30 28-Mar-17 15:43
SC32894-05 Reagent Blank Aqueous 28-Mar-17 00:00 28-Mar-17 15:43
SC32894-06 Trip Blank Aqueous 28-Mar-17 00:00 28-Mar-17 15:43
I attest that the information contained within the report has been reviewed for accuracy and checked against the quality control
requirements for each method. These results relate only to the sample(s) as received.
All applicable NELAC requirements have been met.
Massachusetts # M-MA138/MA1110
Connecticut # PH-0777
Florida # E87936
Maine # MA138
New Hampshire # 2972/2538
New Jersey # MA011
New York # 11393
Pennsylvania # 68-04426/68-02924
Rhode Island # LAO00348
USDA # P330-15-00375
Vermont # VT-11393
Authorized by:
June O'Connor
Laboratory Director
Eurofins Spectrum Analytical holds primary certification in the State of Massachusetts for the analytes as indicated with an X in the
"Cert." column within this report. Please note that the State of Massachusetts does not offer certification for all analytes. Please refer to
our website for specific certification holdings in each state.
Please note that this report contains 50 pages of analytical data plus Chain of Custody document(s). When the Laboratory Report is
indicated as revised, this report supersedes any previously dated reports for the laboratory ID(s) referenced above. Where this report
identifies subcontracted analyses, copies of the subcontractor's test report are available upon request. This report may not be
reproduced, except in full, without written approval from Eurofins Spectrum Analytical, Inc.
Eurofins Spectrum Analytical, Inc. is a NELAC accredited laboratory organization and meets NELAC testing standards. Use of the NELAC logo
however does not insure that Eurofins Spectrum Analytical, Inc. is currently accredited for the specific method or analyte indicated. Please refer to
our "Quality" web page at www.spectrum-analytical.com for a full listing of our current certifications and fields of accreditation. States in which
Eurofins Spectrum Analytical, Inc. holds NELAC certification are New York, New Hampshire, New Jersey, Pennsylvania and Florida. All analytical
work for Volatile Organic and Air analysis are transferred to and conducted at our 830 Silver Street location (PA-68-04426).
Please contact the Laboratory or Technical Director at 800-789-9115 with any questions regarding the data contained in this laboratory report.
Eurofins Spectrum Analytical, Inc. 830 Silver Street T | 413-789-9018
Agawam, MA 01001 F | 413-789-4076
www.EurofinsUS.com/Spectrum Page 1 of 50
MassDEP Analytical Protocol Certification Form
Laboratory Name: Eurofins Spectrum Analytical, Inc. Project #: 60306709-452
Project Location: Agawam Comp Station & Pond Stream, MA RTN:
This form provides certifications for the following data set: SC32894-01 through SC32894-06
Matrices: Aqueous
Drinking Water
Surface Water
CAM Protocol
8260 VOC
CAM II A
7470/7471 Hg
CAM III B
MassDEP VPH
CAM IV A
8081 Pesticides
CAM V B
7196 Hex Cr
CAM VI B
MassDEP APH
CAM IX A
8270 SVOC
CAM II B
7010 Metals
CAM III C
MassDEP EPH
CAM IV B
8151 Herbicides
CAM V C
8330 Explosives
CAM VIII A
TO-15 VOC
CAM IX B
6010 Metals
CAM III A
6020 Metals
CAM III D
8082 PCB
CAM V A
9014 Total
Cyanide/PAC
CAM VI A
6860 Perchlorate
CAM VIII B
ü
ü
ü
ü
ü
Affirmative responses to questions A through F are required for "Presumptive Certainty" status
Were all samples received in a condition consistent with those described on the Chain of Custody, properly
preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding
times?
Were the analytical method(s) and all associated QC requirements specified in the selected CAM
protocol(s) followed?
Were all required corrective actions and analytical response actions specified in the selected CAM
protocol(s) implemented for all identified performance standard non-conformances?
Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality
Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?
a. VPH, EPH, and APH Methods only: Was each method conducted without significant modification(s)?
b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?
Were all applicable CAM protocol QC and performance standard non-conformances identified and
evaluated in a laboratory narrative (including all "No" responses to questions A through E)?
Responses to questions G, H and I below are required for "Presumptive Certainty" status
Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?
Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness
requirements described in 310 CMR 40. 1056 (2)(k) and WSC-07-350.
Were all QC performance standards specified in the CAM protocol(s) achieved?
Were results reported for the complete analyte list specified in the selected CAM protocol(s)?
All negative responses are addressed in a case narrative on the cover page of this report.
I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the
information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete.
June O'Connor
Laboratory Director
Date: 4/7/2017
A
B
C
D
E
F
G
H
I
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
ü
ü
ü
ü
ü
ü
ü
ü
Yes No
ü
9012 Total
Cyanide/PAC
CAM VI A
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 2 of 5007-Apr-17 13:56
CASE NARRATIVE:
Data has been reported to the RDL. This report excludes estimated concentrations detected below the RDL and above the MDL
(J-Flag).
All non-detects and all results below the reporting limit are reported as < (less than) the reporting limit in this report.
The samples were received 5.1 degrees Celsius, please refer to the Chain of Custody for details specific to temperature upon receipt.
An infrared thermometer with a tolerance of +/- 1.0 degrees Celsius was used immediately upon receipt of the samples.
If a Matrix Spike (MS), Matrix Spike Duplicate (MSD) or Duplicate (DUP) was not requested on the Chain of Custody, method
criteria may have been fulfilled with a source sample not of this Sample Delivery Group.
MADEP has published a list of analytical methods (CAM) which provides a series of recommended protocols for the acquisition,
analysis and reporting of analytical data in support of MCP decisions. "Presumptive Certainty" can be established only for those
methods published by the MADEP in the MCP CAM. The compounds and/or elements reported were specifically requested by the
client on the Chain of Custody and in some cases may not include the full analyte list as defined in the method. Regulatory limits may
not be achieved if specific method and/or technique was not requested on the Chain of Custody.
According to WSC-CAM 5/2009 Rev.1, Table 11 A-1, recovery for some VOC analytes have been deemed potentially difficult.
Although they may still be within the recommended recovery range, a range has been set based on historical control limits.
Some target analytes which are not listed as exceptions in the Summary of CAM Reporting Limits may exceed the recommended RL
based on sample initial volume or weight provided, % moisture content, or responsiveness of a particular analyte to purge and trap
instrumentation.
Analyses for Total Hardness, pH, and Total Residual Chlorine fall under the state of Pennsylvania code Chapter 252.6 accreditation by
rule.
See below for any non-conformances and issues relating to quality control samples and/or sample analysis/matrix.
EPA 1664B
Laboratory Control Samples:
1705552 BS
Non-polar material (SGT-HEM) percent recovery 46 (64-132) is outside individual acceptance criteria, but within overall method
allowances. All reported results of the following samples are considered to have a potentially low bias:
ACS-2 (Stream)
LSP-1 (Pond)
SPB-1 (Brook)
1705552-BS1
Data for this analyte may be biased low based on QC spike recoveries.
Non-polar material (SGT-HEM)
Samples:
SC32894-02 ACS-2 (Stream)
Data for this analyte may be biased low based on QC spike recoveries.
Non-polar material (SGT-HEM)
SC32894-03 SPB-1 (Brook)
Data for this analyte may be biased low based on QC spike recoveries.
Non-polar material (SGT-HEM)
SC32894-04 LSP-1 (Pond)
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* Reportable Detection Limit Page 3 of 5007-Apr-17 13:56
EPA 1664B
Samples:
SC32894-04 LSP-1 (Pond)
Data for this analyte may be biased low based on QC spike recoveries.
Non-polar material (SGT-HEM)
EPA 200.7
Samples:
SC32894-01 ACS-1 (Hydrant)
MRL raised to correlate to batch QC reporting limits.
Iron
SC32894-02 ACS-2 (Stream)
MRL raised to correlate to batch QC reporting limits.
Iron
SC32894-03 SPB-1 (Brook)
MRL raised to correlate to batch QC reporting limits.
Iron
SC32894-04 LSP-1 (Pond)
MRL raised to correlate to batch QC reporting limits.
Iron
EPA 200.8
Blanks:
1705512-BLK1
The method blank contains analyte at a concentration above the MRL, however no reportable concentration is present in the
sample.
Lead
Duplicates:
1705512-DUP1 Source: SC32894-01
MRL raised to correlate to batch QC reporting limits.
Lead
Samples:
SC32894-01 ACS-1 (Hydrant)
MRL raised to correlate to batch QC reporting limits.
Lead
SC32894-02 ACS-2 (Stream)
MRL raised to correlate to batch QC reporting limits.
Lead
SC32894-03 SPB-1 (Brook)
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* Reportable Detection Limit Page 4 of 5007-Apr-17 13:56
EPA 200.8
Samples:
SC32894-03 SPB-1 (Brook)
MRL raised to correlate to batch QC reporting limits.
Lead
SC32894-04 LSP-1 (Pond)
MRL raised to correlate to batch QC reporting limits.
Lead
SM3500-Cr-B (11)/7196A
Duplicates:
1705285-DUP1 Source: SC32894-01
The Reporting Limit has been raised to account for matrix interference.
Hexavalent Chromium
Samples:
SC32894-01 ACS-1 (Hydrant)
The Reporting Limit has been raised to account for matrix interference.
Hexavalent Chromium
SC32894-02 ACS-2 (Stream)
The Reporting Limit has been raised to account for matrix interference.
Hexavalent Chromium
SC32894-03 SPB-1 (Brook)
The Reporting Limit has been raised to account for matrix interference.
Hexavalent Chromium
SC32894-04 LSP-1 (Pond)
The Reporting Limit has been raised to account for matrix interference.
Hexavalent Chromium
SW846 8260C
Calibration:
1703038
Analyte quantified by quadratic equation type calibration.
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
Bromoform
Carbon tetrachloride
cis-1,3-Dichloropropene
Dibromochloromethane
Naphthalene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
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* Reportable Detection Limit Page 5 of 5007-Apr-17 13:56
SW846 8260C
Calibration:
1703038
This affected the following samples:
1705468-BLK1
1705468-BS1
1705468-BSD1
ACS-1 (Hydrant)
ACS-2 (Stream)
LSP-1 (Pond)
S703389-ICV1
S703413-CCV1
SPB-1 (Brook)
Trip Blank
Laboratory Control Samples:
1705468 BS/BSD
trans-1,4-Dichloro-2-butene percent recoveries (131/134) are outside individual acceptance criteria, but within overall method
allowances. All reported results of the following samples are considered to have a potentially high bias:
ACS-1 (Hydrant)
Samples:
S703413-CCV1
Analyte percent drift is outside individual acceptance criteria (20), but within overall method allowances.
1,1,2,2-Tetrachloroethane (-25.9%)
This affected the following samples:
1705468-BLK1
1705468-BS1
1705468-BSD1
ACS-1 (Hydrant)
SW846 8270D
Calibration:
1701045
Analyte quantified by quadratic equation type calibration.
2,4-Dinitrophenol
2,4-Dinitrotoluene
4,6-Dinitro-2-methylphenol
4-Nitrophenol
Benzidine
Benzoic acid
Carbazole
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 6 of 5007-Apr-17 13:56
SW846 8270D
Calibration:
1701045
This affected the following samples:
1705460-BLK1
1705460-BS1
1705460-BSD1
ACS-1 (Hydrant)
ACS-2 (Stream)
LSP-1 (Pond)
S701962-ICV1
S703498-CCV1
SPB-1 (Brook)
Laboratory Control Samples:
1705460 BS/BSD
4-Chloroaniline percent recoveries (38/43) are outside individual acceptance criteria, but within overall method allowances. All
reported results of the following samples are considered to have a potentially low bias:
ACS-1 (Hydrant)
Aniline percent recoveries (34/38) are outside individual acceptance criteria, but within overall method allowances. All reported
results of the following samples are considered to have a potentially low bias:
ACS-1 (Hydrant)
Benzidine percent recoveries (38/56) are outside individual acceptance criteria, but within overall method allowances. All
reported results of the following samples are considered to have a potentially low bias:
ACS-1 (Hydrant)
1705460 BSD
2,4-Dinitrophenol RPD 21% (20%) is outside individual acceptance criteria.
Benzidine RPD 39% (20%) is outside individual acceptance criteria.
1705460-BSD1
RPD out of acceptance range. The batch is accepted based upon LCS and/or LCSD recovery.
2,4-Dinitrophenol
Benzidine
Samples:
S703498-CCV1
Analyte percent difference is outside individual acceptance criteria (20), but within overall method allowances.
3,3´-Dichlorobenzidine (-26.3%)
3-Nitroaniline (-39.5%)
4-Chloroaniline (-21.0%)
Aniline (-34.7%)
Bis(2-chloroethyl)ether (22.4%)
Hexachlorocyclopentadiene (21.7%)
Pyridine (-54.1%)
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* Reportable Detection Limit Page 7 of 5007-Apr-17 13:56
SW846 8270D
Samples:
S703498-CCV1
Analyte percent drift is outside individual acceptance criteria (20), but within overall method allowances.
2,4-Dinitrophenol (25.1%)
4,6-Dinitro-2-methylphenol (37.1%)
4-Nitrophenol (20.1%)
Benzidine (-85.8%)
Carbazole (-45.3%)
This affected the following samples:
1705460-BLK1
1705460-BS1
1705460-BSD1
ACS-1 (Hydrant)
ACS-2 (Stream)
LSP-1 (Pond)
SPB-1 (Brook)
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* Reportable Detection Limit Page 8 of 5007-Apr-17 13:56
Sample Acceptance Check Form
Client:
Work Order:
Project:
Sample(s) received on:
AECOM Environment - Providence, RI
Agawam Comp Station & Pond Stream, MA / 60306709-452
SC32894
3/28/2017
Yes No N/A
Were samples received at a temperature of 6°C?
Were custody seals present?
Were custody seals intact?
ü
ü
ü
The following outlines the condition of samples for the attached Chain of Custody upon receipt.
Were samples cooled on ice upon transfer to laboratory representative? ü
Were samples properly labeled (labels affixed to sample containers and include sample ID, site
location, and/or project number and the collection date)?
ü
Were sample containers received intact?
Were samples accompanied by a Chain of Custody document?
Did sample container labels agree with Chain of Custody document?
Were samples received within method-specific holding times?
ü
ü
ü
ü
Does Chain of Custody document include proper, full, and complete documentation, which shall
include sample ID, site location, and/or project number, date and time of collection, collector's name,
preservation type, sample matrix and any special remarks concerning the sample?
ü
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 9 of 5007-Apr-17 13:56
Summary of Hits
Client ID: ACS-1 (Hydrant)Lab ID: SC32894-01
ResultParameter Units Analytical MethodReporting LimitFlag
Calcium EPA 200.70.1003.97 mg/l
Copper EPA 200.70.00500.0080 mg/l
Iron EPA 200.70.04008.32 mg/lR06
Magnesium EPA 200.70.01001.22 mg/l
Nickel EPA 200.70.00500.0094 mg/l
Zinc EPA 200.70.00500.136 mg/l
Lead EPA 200.80.001300.00133 mg/lR06
Chloride EPA 300.01.0020.8 mg/l
Hardness SM 2340B (11)0.29114.9 mg/l CaCO3
Total Suspended Solids SM2540D (11)1.730.7 mg/l
Bromodichloromethane SW846 8260C0.503.48 µg/l
Chloroform SW846 8260C1.0041.2 µg/l
Dibromochloromethane SW846 8260C0.500.66 µg/l
Client ID: ACS-2 (Stream)Lab ID: SC32894-02
ResultParameter Units Analytical MethodReporting LimitFlag
Non-polar material (SGT-HEM) EPA 1664B1.02.0 mg/lBsL
Calcium EPA 200.70.10012.3 mg/l
Copper EPA 200.70.00500.0053 mg/l
Iron EPA 200.70.04001.35 mg/lR06
Magnesium EPA 200.70.01004.48 mg/l
Zinc EPA 200.70.00500.0062 mg/l
Chloride EPA 300.01.0018.9 mg/l
Hardness SM 2340B (11)0.29149.1 mg/l CaCO3
Total Suspended Solids SM2540D (11)0.58.8 mg/l
Client ID: SPB-1 (Brook)Lab ID: SC32894-03
ResultParameter Units Analytical MethodReporting LimitFlag
Non-polar material (SGT-HEM) EPA 1664B1.02.3 mg/lBsL
Calcium EPA 200.70.1005.30 mg/l
Iron EPA 200.70.04000.178 mg/lR06
Magnesium EPA 200.70.01001.68 mg/l
Chloride EPA 300.01.0014.0 mg/l
Hardness SM 2340B (11)0.29120.2 mg/l CaCO3
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 10 of 5007-Apr-17 13:56
Client ID: LSP-1 (Pond)Lab ID: SC32894-04
ResultParameter Units Analytical MethodReporting LimitFlag
Calcium EPA 200.70.1005.30 mg/l
Iron EPA 200.70.04000.233 mg/lR06
Magnesium EPA 200.70.01001.66 mg/l
Chloride EPA 300.01.0013.6 mg/l
Hardness SM 2340B (11)0.29120.1 mg/l CaCO3
Total Suspended Solids SM2540D (11)0.50.6 mg/l
Please note that because there are no reporting limits associated with hazardous waste characterizations or micro analyses , this
summary does not include hits from these analyses if included in this work order.
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 11 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
Prepared by method SW846 5030 Water MS
SW846 8260C 01-Apr-1731-Mar-17µg/l 1.00< 1.0076-13-1 1,1,2-Trichlorotrifluoroetha
ne (Freon 113)
1 1705468GMA0.53
" ""µg/l 10.0< 10.067-64-1 Acetone 1 ""0.80
" ""µg/l 0.50< 0.50107-13-1 Acrylonitrile 1 ""0.47
" ""µg/l 1.00< 1.0071-43-2 Benzene 1 ""0.28
" ""µg/l 1.00< 1.00108-86-1 Bromobenzene 1 ""0.33
" ""µg/l 1.00< 1.0074-97-5 Bromochloromethane 1 ""0.34
" ""µg/l 0.503.4875-27-4 Bromodichloromethane 1 ""0.42
" ""µg/l 1.00< 1.0075-25-2 Bromoform 1 ""0.42
" ""µg/l 2.00< 2.0074-83-9 Bromomethane 1 ""0.90
" ""µg/l 2.00< 2.0078-93-3 2-Butanone (MEK) 1 ""1.07
" ""µg/l 1.00< 1.00104-51-8 n-Butylbenzene 1 ""0.41
" ""µg/l 1.00< 1.00135-98-8 sec-Butylbenzene 1 ""0.33
" ""µg/l 1.00< 1.0098-06-6 tert-Butylbenzene 1 ""0.32
" ""µg/l 2.00< 2.0075-15-0 Carbon disulfide 1 ""0.41
" ""µg/l 1.00< 1.0056-23-5 Carbon tetrachloride 1 ""0.44
" ""µg/l 1.00< 1.00108-90-7 Chlorobenzene 1 ""0.25
" ""µg/l 2.00< 2.0075-00-3 Chloroethane 1 ""0.59
" ""µg/l 1.0041.267-66-3 Chloroform 1 ""0.33
" ""µg/l 2.00< 2.0074-87-3 Chloromethane 1 ""0.37
" ""µg/l 1.00< 1.0095-49-8 2-Chlorotoluene 1 ""0.32
" ""µg/l 1.00< 1.00106-43-4 4-Chlorotoluene 1 ""0.32
" ""µg/l 2.00< 2.0096-12-8 1,2-Dibromo-3-chloroprop
ane
1 ""0.86
" ""µg/l 0.500.66124-48-1 Dibromochloromethane 1 ""0.32
" ""µg/l 0.50< 0.50106-93-4 1,2-Dibromoethane (EDB) 1 ""0.20
" ""µg/l 1.00< 1.0074-95-3 Dibromomethane 1 ""0.31
" ""µg/l 1.00< 1.0095-50-1 1,2-Dichlorobenzene 1 ""0.28
" ""µg/l 1.00< 1.00541-73-1 1,3-Dichlorobenzene 1 ""0.31
" ""µg/l 1.00< 1.00106-46-7 1,4-Dichlorobenzene 1 ""0.27
" ""µg/l 2.00< 2.0075-71-8 Dichlorodifluoromethane
(Freon12)
1 ""0.58
" ""µg/l 1.00< 1.0075-34-3 1,1-Dichloroethane 1 ""0.32
" ""µg/l 1.00< 1.00107-06-2 1,2-Dichloroethane 1 ""0.28
" ""µg/l 1.00< 1.0075-35-4 1,1-Dichloroethene 1 ""0.69
" ""µg/l 1.00< 1.00156-59-2 cis-1,2-Dichloroethene 1 ""0.33
" ""µg/l 1.00< 1.00156-60-5 trans-1,2-Dichloroethene 1 ""0.38
" ""µg/l 1.00< 1.0078-87-5 1,2-Dichloropropane 1 ""0.29
" ""µg/l 1.00< 1.00142-28-9 1,3-Dichloropropane 1 ""0.21
" ""µg/l 1.00< 1.00594-20-7 2,2-Dichloropropane 1 ""0.42
" ""µg/l 1.00< 1.00563-58-6 1,1-Dichloropropene 1 ""0.58
" ""µg/l 0.50< 0.5010061-01-5 cis-1,3-Dichloropropene 1 ""0.36
" ""µg/l 0.50< 0.5010061-02-6 trans-1,3-Dichloropropene 1 ""0.35
" ""µg/l 1.00< 1.00100-41-4 Ethylbenzene 1 ""0.33
" ""µg/l 0.50< 0.5087-68-3 Hexachlorobutadiene 1 ""0.47
" ""µg/l 2.00< 2.00591-78-6 2-Hexanone (MBK) 1 ""0.53
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 12 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
SW846 8260C 01-Apr-1731-Mar-17µg/l 1.00< 1.0098-82-8 Isopropylbenzene 1 1705468GMA0.36
" ""µg/l 1.00< 1.0099-87-6 4-Isopropyltoluene 1 ""0.28
" ""µg/l 1.00< 1.001634-04-4 Methyl tert-butyl ether 1 ""0.24
" ""µg/l 2.00< 2.00108-10-1 4-Methyl-2-pentanone
(MIBK)
1 ""0.52
" ""µg/l 2.00< 2.0075-09-2 Methylene chloride 1 ""0.66
" ""µg/l 1.00< 1.0091-20-3 Naphthalene 1 ""0.35
" ""µg/l 1.00< 1.00103-65-1 n-Propylbenzene 1 ""0.34
" ""µg/l 1.00< 1.00100-42-5 Styrene 1 ""0.40
" ""µg/l 1.00< 1.00630-20-6 1,1,1,2-Tetrachloroethane 1 ""0.38
" ""µg/l 0.50< 0.5079-34-5 1,1,2,2-Tetrachloroethane 1 ""0.33
" ""µg/l 1.00< 1.00127-18-4 Tetrachloroethene 1 ""0.57
" ""µg/l 1.00< 1.00108-88-3 Toluene 1 ""0.30
" ""µg/l 1.00< 1.0087-61-6 1,2,3-Trichlorobenzene 1 ""0.38
" ""µg/l 1.00< 1.00120-82-1 1,2,4-Trichlorobenzene 1 ""0.38
" ""µg/l 1.00< 1.00108-70-3 1,3,5-Trichlorobenzene 1 ""0.30
" ""µg/l 1.00< 1.0071-55-6 1,1,1-Trichloroethane 1 ""0.51
" ""µg/l 1.00< 1.0079-00-5 1,1,2-Trichloroethane 1 ""0.33
" ""µg/l 1.00< 1.0079-01-6 Trichloroethene 1 ""0.50
" ""µg/l 1.00< 1.0075-69-4 Trichlorofluoromethane
(Freon 11)
1 ""0.49
" ""µg/l 1.00< 1.0096-18-4 1,2,3-Trichloropropane 1 ""0.29
" ""µg/l 1.00< 1.0095-63-6 1,2,4-Trimethylbenzene 1 ""0.36
" ""µg/l 1.00< 1.00108-67-8 1,3,5-Trimethylbenzene 1 ""0.43
" ""µg/l 1.00< 1.0075-01-4 Vinyl chloride 1 ""0.47
" ""µg/l 2.00< 2.00179601-23-1 m,p-Xylene 1 ""0.38
" ""µg/l 1.00< 1.0095-47-6 o-Xylene 1 ""0.28
" ""µg/l 2.00< 2.00109-99-9 Tetrahydrofuran 1 ""1.06
" ""µg/l 1.00< 1.0060-29-7 Ethyl ether 1 ""0.37
" ""µg/l 1.00< 1.00994-05-8 Tert-amyl methyl ether 1 ""0.49
" ""µg/l 1.00< 1.00637-92-3 Ethyl tert-butyl ether 1 ""0.33
" ""µg/l 1.00< 1.00108-20-3 Di-isopropyl ether 1 ""0.29
" ""µg/l 10.0< 10.075-65-0 Tert-Butanol / butyl alcohol 1 ""5.90
" ""µg/l 20.0< 20.0123-91-1 1,4-Dioxane 1 ""11.4
" ""µg/l 5.00< 5.00110-57-6 trans-1,4-Dichloro-2-buten
e
1 ""0.82
" ""µg/l 200< 20064-17-5 Ethanol 1 ""30.9
Surrogate recoveries:
70-130 % " " ""4-Bromofluorobenzene 95 "460-00-4
70-130 % " " ""Toluene-d8 99 "2037-26-5
70-130 % " " ""1,2-Dichloroethane-d4 104 "17060-07-0
70-130 % " " ""Dibromofluoromethane 103 "1868-53-7
Microextractable Organic Compounds
Microextractables
Prepared by method General Preparation SVOC
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.010096-12-8 1,2-Dibromo-3-chloroprop
ane
1 1705548DS0.00362
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* Reportable Detection Limit Page 13 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Microextractable Organic Compounds
Microextractables
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.0100106-93-4 1,2-Dibromoethane (EDB) 1 1705548DS0.00336
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
Prepared by method SW846 3510C
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.05< 5.0583-32-9 Acenaphthene 1 1705460SM1.19
" ""µg/l 5.05< 5.05208-96-8 Acenaphthylene 1 ""1.10
" ""µg/l 5.05< 5.0562-53-3 Aniline 1 ""1.42
" ""µg/l 5.05< 5.05120-12-7 Anthracene 1 ""1.17
" ""µg/l 5.05< 5.05103-33-3 Azobenzene/Diphenyldiaz
ene
1 ""1.04
" ""µg/l 5.05< 5.0592-87-5 Benzidine 1 ""2.89
" ""µg/l 5.05< 5.0556-55-3 Benzo (a) anthracene 1 ""1.14
" ""µg/l 5.05< 5.0550-32-8 Benzo (a) pyrene 1 ""1.02
" ""µg/l 5.05< 5.05205-99-2 Benzo (b) fluoranthene 1 ""1.03
" ""µg/l 5.05< 5.05191-24-2 Benzo (g,h,i) perylene 1 ""1.34
" ""µg/l 5.05< 5.05207-08-9 Benzo (k) fluoranthene 1 ""1.36
" ""µg/l 5.05< 5.0565-85-0 Benzoic acid 1 ""2.01
" ""µg/l 5.05< 5.05100-51-6 Benzyl alcohol 1 ""1.76
" ""µg/l 5.05< 5.05111-91-1 Bis(2-chloroethoxy)metha
ne
1 ""1.00
" ""µg/l 5.05< 5.05111-44-4 Bis(2-chloroethyl)ether 1 ""1.13
" ""µg/l 5.05< 5.05108-60-1 Bis(2-chloroisopropyl)ethe
r
1 ""1.21
" ""µg/l 5.05< 5.05117-81-7 Bis(2-ethylhexyl)phthalate 1 ""1.41
" ""µg/l 5.05< 5.05101-55-3 4-Bromophenyl phenyl
ether
1 ""1.19
" ""µg/l 5.05< 5.0585-68-7 Butyl benzyl phthalate 1 ""1.33
" ""µg/l 5.05< 5.0586-74-8 Carbazole 1 ""1.25
" ""µg/l 5.05< 5.0559-50-7 4-Chloro-3-methylphenol 1 ""1.24
" ""µg/l 5.05< 5.05106-47-8 4-Chloroaniline 1 ""1.32
" ""µg/l 5.05< 5.0591-58-7 2-Chloronaphthalene 1 ""1.20
" ""µg/l 5.05< 5.0595-57-8 2-Chlorophenol 1 ""1.27
" ""µg/l 5.05< 5.057005-72-3 4-Chlorophenyl phenyl
ether
1 ""1.16
" ""µg/l 5.05< 5.05218-01-9 Chrysene 1 ""1.05
" ""µg/l 5.05< 5.0553-70-3 Dibenzo (a,h) anthracene 1 ""1.20
" ""µg/l 5.05< 5.05132-64-9 Dibenzofuran 1 ""1.09
" ""µg/l 5.05< 5.0595-50-1 1,2-Dichlorobenzene 1 ""1.61
" ""µg/l 5.05< 5.05541-73-1 1,3-Dichlorobenzene 1 ""1.21
" ""µg/l 5.05< 5.05106-46-7 1,4-Dichlorobenzene 1 ""1.14
" ""µg/l 5.05< 5.0591-94-1 3,3´-Dichlorobenzidine 1 ""1.57
" ""µg/l 5.05< 5.05120-83-2 2,4-Dichlorophenol 1 ""1.22
" ""µg/l 5.05< 5.0584-66-2 Diethyl phthalate 1 ""1.54
" ""µg/l 5.05< 5.05131-11-3 Dimethyl phthalate 1 ""1.49
" ""µg/l 5.05< 5.05105-67-9 2,4-Dimethylphenol 1 ""1.42
" ""µg/l 5.05< 5.0584-74-2 Di-n-butyl phthalate 1 ""1.12
" ""µg/l 5.05< 5.05534-52-1 4,6-Dinitro-2-methylphenol 1 ""1.89
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 14 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.05< 5.0551-28-5 2,4-Dinitrophenol 1 1705460SM2.17
" ""µg/l 5.05< 5.05121-14-2 2,4-Dinitrotoluene 1 ""1.85
" ""µg/l 5.05< 5.05606-20-2 2,6-Dinitrotoluene 1 ""1.66
" ""µg/l 5.05< 5.05117-84-0 Di-n-octyl phthalate 1 ""1.28
" ""µg/l 5.05< 5.05206-44-0 Fluoranthene 1 ""1.20
" ""µg/l 5.05< 5.0586-73-7 Fluorene 1 ""1.20
" ""µg/l 5.05< 5.05118-74-1 Hexachlorobenzene 1 ""1.06
" ""µg/l 5.05< 5.0587-68-3 Hexachlorobutadiene 1 ""1.19
" ""µg/l 5.05< 5.0577-47-4 Hexachlorocyclopentadien
e
1 ""2.10
" ""µg/l 5.05< 5.0567-72-1 Hexachloroethane 1 ""1.53
" ""µg/l 5.05< 5.05193-39-5 Indeno (1,2,3-cd) pyrene 1 ""1.30
" ""µg/l 5.05< 5.0578-59-1 Isophorone 1 ""1.07
" ""µg/l 5.05< 5.0591-57-6 2-Methylnaphthalene 1 ""1.22
" ""µg/l 5.05< 5.0595-48-7 2-Methylphenol 1 ""1.46
" ""µg/l 10.1< 10.1108-39-4,
106-44-53 & 4-Methylphenol 1 ""1.46
" ""µg/l 5.05< 5.0591-20-3 Naphthalene 1 ""1.06
" ""µg/l 5.05< 5.0588-74-4 2-Nitroaniline 1 ""1.40
" ""µg/l 5.05< 5.0599-09-2 3-Nitroaniline 1 ""1.56
" ""µg/l 5.05< 5.05100-01-6 4-Nitroaniline 1 ""2.16
" ""µg/l 5.05< 5.0598-95-3 Nitrobenzene 1 ""1.03
" ""µg/l 5.05< 5.0588-75-5 2-Nitrophenol 1 ""1.46
" ""µg/l 20.2< 20.2100-02-7 4-Nitrophenol 1 ""2.95
" ""µg/l 5.05< 5.0562-75-9 N-Nitrosodimethylamine 1 ""1.39
" ""µg/l 5.05< 5.05621-64-7 N-Nitrosodi-n-propylamine 1 ""1.32
" ""µg/l 5.05< 5.0586-30-6 N-Nitrosodiphenylamine 1 ""1.47
" ""µg/l 20.2< 20.287-86-5 Pentachlorophenol 1 ""1.89
" ""µg/l 5.05< 5.0585-01-8 Phenanthrene 1 ""1.25
" ""µg/l 5.05< 5.05108-95-2 Phenol 1 ""0.993
" ""µg/l 5.05< 5.05129-00-0 Pyrene 1 ""1.44
" ""µg/l 5.05< 5.05110-86-1 Pyridine 1 ""1.56
" ""µg/l 5.05< 5.05120-82-1 1,2,4-Trichlorobenzene 1 ""1.28
" ""µg/l 5.05< 5.0590-12-0 1-Methylnaphthalene 1 ""1.10
" ""µg/l 5.05< 5.0595-95-4 2,4,5-Trichlorophenol 1 ""1.20
" ""µg/l 5.05< 5.0588-06-2 2,4,6-Trichlorophenol 1 ""1.09
" ""µg/l 5.05< 5.0582-68-8 Pentachloronitrobenzene 1 ""1.29
" ""µg/l 5.05< 5.0595-94-3 1,2,4,5-Tetrachlorobenzen
e
1 ""1.05
Surrogate recoveries:
30-130 % " " ""2-Fluorobiphenyl 51 "321-60-8
15-110 % " " ""2-Fluorophenol 31 "367-12-4
30-130 % " " ""Nitrobenzene-d5 58 "4165-60-0
15-110 % " " ""Phenol-d5 19 "4165-62-2
30-130 % " " ""Terphenyl-dl4 63 "1718-51-0
15-110 % " " ""2,4,6-Tribromophenol 63 "118-79-6
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 15 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
Prepared by method SW846 3510C
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.204< 0.20412674-11-2 Aroclor-1016 1 1705401IMR0.106
" ""µg/l 0.204< 0.20411104-28-2 Aroclor-1221 1 ""0.117
" ""µg/l 0.204< 0.20411141-16-5 Aroclor-1232 1 ""0.113
" ""µg/l 0.204< 0.20453469-21-9 Aroclor-1242 1 ""0.0710
" ""µg/l 0.204< 0.20412672-29-6 Aroclor-1248 1 ""0.139
" ""µg/l 0.204< 0.20411097-69-1 Aroclor-1254 1 ""0.118
" ""µg/l 0.204< 0.20411096-82-5 Aroclor-1260 1 ""0.0868
" ""µg/l 0.204< 0.20437324-23-5 Aroclor-1262 1 ""0.0914
" ""µg/l 0.204< 0.20411100-14-4 Aroclor-1268 1 ""0.0934
Surrogate recoveries:
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr)
70 "10386-84-2
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr) [2C]
70 "10386-84-2
30-150 % " " ""Decachlorobiphenyl (Sr) 70 "2051-24-3
30-150 % " " ""Decachlorobiphenyl (Sr)
[2C]
60 "2051-24-3
Total Metals by EPA 200/6000 Series Methods
Prepared by method General Prep-Metal
EPA 200/6000
methods
30-Mar-17N/AField
Preserved;
pH<2
confirmed
Preservation 1 1705413AS
Total Metals by EPA 200 Series Methods
EPA 200.7 05-Apr-1703-Apr-17mg/l 0.0050< 0.0050 X7440-22-4 Silver 1 1705511EDT0.0035
" ""mg/l 0.0040< 0.0040 X7440-38-2 Arsenic 1 ""0.0028
" 07-Apr-17"mg/l 0.1003.97 X7440-70-2 Calcium 1 ""0.0340
" 05-Apr-17"mg/l 0.0025< 0.0025 X7440-43-9 Cadmium 1 ""0.0004
" ""mg/l 0.0050< 0.0050 X7440-47-3 Chromium 1 ""0.0019
" 05-Apr-17"mg/l 0.00500.0080 X7440-50-8 Copper 1 ""0.0029
" 06-Apr-17"mg/l 0.04008.32 X7439-89-6 Iron 1 ""0.0100R06
EPA
245.1/7470A
03-Apr-17"mg/l 0.00020< 0.00020 X7439-97-6 Mercury 1 1705513lnb0.00013
EPA 200.7 05-Apr-17"mg/l 0.01001.22 X7439-95-4 Magnesium 1 1705511EDT0.0074
" ""mg/l 0.00500.0094 X7440-02-0 Nickel 1 ""0.0010
EPA 200.8 03-Apr-17"mg/l 0.001300.00133 X7439-92-1 Lead 1 1705512edt0.00005R06
EPA 200.7 05-Apr-17"mg/l 0.0060< 0.0060 X7440-36-0 Antimony 1 1705511EDT0.0026
" ""mg/l 0.0150< 0.0150 X7782-49-2 Selenium 1 ""0.0072
" ""mg/l 0.00500.136 X7440-66-6 Zinc 1 ""0.0027
General Chemistry Parameters
Prepared by method EPA 200 Series
Calculation 07-Apr-1703-Apr-17mg/l 0.0100< 0.010016065-83-1 Trivalent Chromium 1 1705511EDT0.0053
SM 2340B (11) 07-Apr-17"mg/l
CaCO3
0.29114.9Hardness 1 [CALC]EDT0.115
Prepared by method SM4500-NH3 B (11)
SM4500-NH3 C.
(11)
05-Apr-1704-Apr-17mg/l 0.200< 0.200 XAmmonia as N 1 1705665AHK0.118
EPA 300.0 30-Mar-1730-Mar-17mg/l 1.0020.8 X16887-00-6 Chloride 1 1705419AHK0.0897
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 16 of 5007-Apr-17 13:56
ACS-1 (Hydrant)
Sample IdentificationMatrix
28-Mar-17 08:45
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Drinking WaterSC32894-01
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
General Chemistry Parameters
SM3500-Cr-B
(11)/7196A
28-Mar-17
17:26
28-Mar-17
17:09
mg/l 0.025< 0.02518540-29-9 Hexavalent Chromium 1 1705285TY0.014R01,LIV
EPA 335.4 /
SW846 9012B
31-Mar-1731-Mar-17mg/l 0.00500< 0.00500 X57-12-5 Cyanide (total) 1 1705518RLT0.00426
SM2540D (11) 31-Mar-1730-Mar-17mg/l 1.730.7 XTotal Suspended Solids 1 1705388CMB0.6
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 17 of 5007-Apr-17 13:56
ACS-2 (Stream)
Sample IdentificationMatrix
28-Mar-17 09:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-02
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
Prepared by method SW846 5030 Water MS
SW846 8260C 01-Apr-1731-Mar-17µg/l 10.0< 10.067-64-1 Acetone 1 1705468GMA0.80
" ""µg/l 1.00< 1.0071-43-2 Benzene 1 ""0.28
" ""µg/l 1.00< 1.0056-23-5 Carbon tetrachloride 1 ""0.44
" ""µg/l 0.50< 0.50106-93-4 1,2-Dibromoethane (EDB) 1 ""0.20
" ""µg/l 1.00< 1.0095-50-1 1,2-Dichlorobenzene 1 ""0.28
" ""µg/l 1.00< 1.00541-73-1 1,3-Dichlorobenzene 1 ""0.31
" ""µg/l 1.00< 1.00106-46-7 1,4-Dichlorobenzene 1 ""0.27
" ""µg/l 1.00< 1.0075-34-3 1,1-Dichloroethane 1 ""0.32
" ""µg/l 1.00< 1.00107-06-2 1,2-Dichloroethane 1 ""0.28
" ""µg/l 1.00< 1.0075-35-4 1,1-Dichloroethene 1 ""0.69
" ""µg/l 1.00< 1.00156-59-2 cis-1,2-Dichloroethene 1 ""0.33
" ""µg/l 1.00< 1.00100-41-4 Ethylbenzene 1 ""0.33
" ""µg/l 1.00< 1.001634-04-4 Methyl tert-butyl ether 1 ""0.24
" ""µg/l 2.00< 2.0075-09-2 Methylene chloride 1 ""0.66
" ""µg/l 1.00< 1.0091-20-3 Naphthalene 1 ""0.35
" ""µg/l 1.00< 1.00127-18-4 Tetrachloroethene 1 ""0.57
" ""µg/l 1.00< 1.00108-88-3 Toluene 1 ""0.30
" ""µg/l 1.00< 1.0071-55-6 1,1,1-Trichloroethane 1 ""0.51
" ""µg/l 1.00< 1.0079-00-5 1,1,2-Trichloroethane 1 ""0.33
" ""µg/l 1.00< 1.0079-01-6 Trichloroethene 1 ""0.50
" ""µg/l 1.00< 1.0075-01-4 Vinyl chloride 1 ""0.47
" ""µg/l 2.00< 2.00179601-23-1 m,p-Xylene 1 ""0.38
" ""µg/l 1.00< 1.0095-47-6 o-Xylene 1 ""0.28
" ""µg/l 1.00< 1.00994-05-8 Tert-amyl methyl ether 1 ""0.49
" ""µg/l 10.0< 10.075-65-0 Tert-Butanol / butyl alcohol 1 ""5.90
" ""µg/l 20.0< 20.0123-91-1 1,4-Dioxane 1 ""11.4
Surrogate recoveries:
70-130 % " " ""4-Bromofluorobenzene 94 "460-00-4
70-130 % " " ""Toluene-d8 100 "2037-26-5
70-130 % " " ""1,2-Dichloroethane-d4 105 "17060-07-0
70-130 % " " ""Dibromofluoromethane 99 "1868-53-7
Microextractable Organic Compounds
Microextractables
Prepared by method General Preparation SVOC
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.010096-12-8 1,2-Dibromo-3-chloroprop
ane
1 1705548DS0.00362
" ""µg/l 0.0100< 0.0100106-93-4 1,2-Dibromoethane (EDB) 1 ""0.00336
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
Prepared by method SW846 3510C
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.15< 5.1583-32-9 Acenaphthene 1 1705460SM1.22
" ""µg/l 5.15< 5.15208-96-8 Acenaphthylene 1 ""1.12
" ""µg/l 5.15< 5.15120-12-7 Anthracene 1 ""1.20
" ""µg/l 5.15< 5.1556-55-3 Benzo (a) anthracene 1 ""1.16
" ""µg/l 5.15< 5.1550-32-8 Benzo (a) pyrene 1 ""1.04
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 18 of 5007-Apr-17 13:56
ACS-2 (Stream)
Sample IdentificationMatrix
28-Mar-17 09:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-02
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.15< 5.15205-99-2 Benzo (b) fluoranthene 1 1705460SM1.05
" ""µg/l 5.15< 5.15191-24-2 Benzo (g,h,i) perylene 1 ""1.37
" ""µg/l 5.15< 5.15207-08-9 Benzo (k) fluoranthene 1 ""1.39
" ""µg/l 5.15< 5.15117-81-7 Bis(2-ethylhexyl)phthalate 1 ""1.44
" ""µg/l 5.15< 5.1585-68-7 Butyl benzyl phthalate 1 ""1.36
" ""µg/l 5.15< 5.1559-50-7 4-Chloro-3-methylphenol 1 ""1.27
" ""µg/l 5.15< 5.1595-57-8 2-Chlorophenol 1 ""1.30
" ""µg/l 5.15< 5.15218-01-9 Chrysene 1 ""1.07
" ""µg/l 5.15< 5.1553-70-3 Dibenzo (a,h) anthracene 1 ""1.23
" ""µg/l 5.15< 5.15120-83-2 2,4-Dichlorophenol 1 ""1.25
" ""µg/l 5.15< 5.1584-66-2 Diethyl phthalate 1 ""1.57
" ""µg/l 5.15< 5.15131-11-3 Dimethyl phthalate 1 ""1.53
" ""µg/l 5.15< 5.15105-67-9 2,4-Dimethylphenol 1 ""1.45
" ""µg/l 5.15< 5.1584-74-2 Di-n-butyl phthalate 1 ""1.14
" ""µg/l 5.15< 5.15534-52-1 4,6-Dinitro-2-methylphenol 1 ""1.93
" ""µg/l 5.15< 5.1551-28-5 2,4-Dinitrophenol 1 ""2.22
" ""µg/l 5.15< 5.15117-84-0 Di-n-octyl phthalate 1 ""1.31
" ""µg/l 5.15< 5.15206-44-0 Fluoranthene 1 ""1.23
" ""µg/l 5.15< 5.1586-73-7 Fluorene 1 ""1.23
" ""µg/l 5.15< 5.15193-39-5 Indeno (1,2,3-cd) pyrene 1 ""1.33
" ""µg/l 5.15< 5.1595-48-7 2-Methylphenol 1 ""1.49
" ""µg/l 10.3< 10.3108-39-4,
106-44-53 & 4-Methylphenol 1 ""1.49
" ""µg/l 5.15< 5.1591-20-3 Naphthalene 1 ""1.08
" ""µg/l 5.15< 5.1588-75-5 2-Nitrophenol 1 ""1.49
" ""µg/l 20.6< 20.6100-02-7 4-Nitrophenol 1 ""3.01
" ""µg/l 20.6< 20.687-86-5 Pentachlorophenol 1 ""1.93
" ""µg/l 5.15< 5.1585-01-8 Phenanthrene 1 ""1.28
" ""µg/l 5.15< 5.15108-95-2 Phenol 1 ""1.01
" ""µg/l 5.15< 5.15129-00-0 Pyrene 1 ""1.47
" ""µg/l 5.15< 5.1595-95-4 2,4,5-Trichlorophenol 1 ""1.23
" ""µg/l 5.15< 5.1588-06-2 2,4,6-Trichlorophenol 1 ""1.11
Surrogate recoveries:
30-130 % " " ""2-Fluorobiphenyl 51 "321-60-8
15-110 % " " ""2-Fluorophenol 32 "367-12-4
30-130 % " " ""Nitrobenzene-d5 50 "4165-60-0
15-110 % " " ""Phenol-d5 21 "4165-62-2
30-130 % " " ""Terphenyl-dl4 50 "1718-51-0
15-110 % " " ""2,4,6-Tribromophenol 57 "118-79-6
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
Prepared by method SW846 3510C
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.211< 0.21112674-11-2 Aroclor-1016 1 1705401IMR0.109
" ""µg/l 0.211< 0.21111104-28-2 Aroclor-1221 1 ""0.121
" ""µg/l 0.211< 0.21111141-16-5 Aroclor-1232 1 ""0.117
" ""µg/l 0.211< 0.21153469-21-9 Aroclor-1242 1 ""0.0733
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 19 of 5007-Apr-17 13:56
ACS-2 (Stream)
Sample IdentificationMatrix
28-Mar-17 09:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-02
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.211< 0.21112672-29-6 Aroclor-1248 1 1705401IMR0.143
" ""µg/l 0.211< 0.21111097-69-1 Aroclor-1254 1 ""0.122
" ""µg/l 0.211< 0.21111096-82-5 Aroclor-1260 1 ""0.0896
" ""µg/l 0.211< 0.21137324-23-5 Aroclor-1262 1 ""0.0943
" ""µg/l 0.211< 0.21111100-14-4 Aroclor-1268 1 ""0.0963
Surrogate recoveries:
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr)
65 "10386-84-2
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr) [2C]
70 "10386-84-2
30-150 % " " ""Decachlorobiphenyl (Sr) 80 "2051-24-3
30-150 % " " ""Decachlorobiphenyl (Sr)
[2C]
75 "2051-24-3
Extractable Petroleum Hydrocarbons
Prepared by method SW846 3510C
EPA 1664B 04-Apr-1703-Apr-17mg/l 1.02.0Non-polar material
(SGT-HEM)
1 1705552KK0.3BsL
Total Metals by EPA 200/6000 Series Methods
Prepared by method General Prep-Metal
EPA 200/6000
methods
29-Mar-17N/AField
Preserved;
pH<2
confirmed
Preservation 1 1705326BK
Total Metals by EPA 200 Series Methods
EPA 200.7 05-Apr-1703-Apr-17mg/l 0.0050< 0.0050 X7440-22-4 Silver 1 1705511EDT0.0035
" ""mg/l 0.0040< 0.0040 X7440-38-2 Arsenic 1 ""0.0028
" 07-Apr-17"mg/l 0.10012.3 X7440-70-2 Calcium 1 ""0.0340
" 05-Apr-17"mg/l 0.0025< 0.0025 X7440-43-9 Cadmium 1 ""0.0004
" ""mg/l 0.0050< 0.0050 X7440-47-3 Chromium 1 ""0.0019
" 05-Apr-17"mg/l 0.00500.0053 X7440-50-8 Copper 1 ""0.0029
" 06-Apr-17"mg/l 0.04001.35 X7439-89-6 Iron 1 ""0.0100R06
EPA
245.1/7470A
03-Apr-17"mg/l 0.00020< 0.00020 X7439-97-6 Mercury 1 1705513lnb0.00013
EPA 200.7 05-Apr-17"mg/l 0.01004.48 X7439-95-4 Magnesium 1 1705511EDT0.0074
" ""mg/l 0.0050< 0.0050 X7440-02-0 Nickel 1 ""0.0010
EPA 200.8 03-Apr-17"mg/l 0.00130< 0.00130 X7439-92-1 Lead 1 1705512edt0.00005R06
EPA 200.7 05-Apr-17"mg/l 0.0060< 0.0060 X7440-36-0 Antimony 1 1705511EDT0.0026
" ""mg/l 0.0150< 0.0150 X7782-49-2 Selenium 1 ""0.0072
" ""mg/l 0.00500.0062 X7440-66-6 Zinc 1 ""0.0027
General Chemistry Parameters
Prepared by method EPA 200 Series
Calculation 07-Apr-1703-Apr-17mg/l 0.0100< 0.010016065-83-1 Trivalent Chromium 1 1705511EDT0.0053
SM 2340B (11) 07-Apr-17"mg/l
CaCO3
0.29149.1Hardness 1 [CALC]EDT0.115
Prepared by method SM4500-NH3 B (11)
SM4500-NH3 C.
(11)
05-Apr-1704-Apr-17mg/l 0.200< 0.200 XAmmonia as N 1 1705665AHK0.118
EPA 300.0 29-Mar-1729-Mar-17mg/l 1.0018.9 X16887-00-6 Chloride 1 1705349AHK0.0897
SM3500-Cr-B
(11)/7196A
28-Mar-17
17:39
28-Mar-17
17:10
mg/l 0.050< 0.05018540-29-9 Hexavalent Chromium 1 1705288TY0.028R01,LIV
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 20 of 5007-Apr-17 13:56
ACS-2 (Stream)
Sample IdentificationMatrix
28-Mar-17 09:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-02
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
General Chemistry Parameters
EPA 335.4 /
SW846 9012B
31-Mar-1731-Mar-17mg/l 0.00500< 0.00500 X57-12-5 Cyanide (total) 1 1705518RLT0.00426
SM2540D (11) 31-Mar-1730-Mar-17mg/l 0.58.8 XTotal Suspended Solids 1 1705388CMB0.2
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 21 of 5007-Apr-17 13:56
SPB-1 (Brook)
Sample IdentificationMatrix
28-Mar-17 12:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-03
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
Prepared by method SW846 5030 Water MS
SW846 8260C 01-Apr-1731-Mar-17µg/l 10.0< 10.067-64-1 Acetone 1 1705468GMA0.80
" ""µg/l 1.00< 1.0071-43-2 Benzene 1 ""0.28
" ""µg/l 1.00< 1.0056-23-5 Carbon tetrachloride 1 ""0.44
" ""µg/l 0.50< 0.50106-93-4 1,2-Dibromoethane (EDB) 1 ""0.20
" ""µg/l 1.00< 1.0095-50-1 1,2-Dichlorobenzene 1 ""0.28
" ""µg/l 1.00< 1.00541-73-1 1,3-Dichlorobenzene 1 ""0.31
" ""µg/l 1.00< 1.00106-46-7 1,4-Dichlorobenzene 1 ""0.27
" ""µg/l 1.00< 1.0075-34-3 1,1-Dichloroethane 1 ""0.32
" ""µg/l 1.00< 1.00107-06-2 1,2-Dichloroethane 1 ""0.28
" ""µg/l 1.00< 1.0075-35-4 1,1-Dichloroethene 1 ""0.69
" ""µg/l 1.00< 1.00156-59-2 cis-1,2-Dichloroethene 1 ""0.33
" ""µg/l 1.00< 1.00100-41-4 Ethylbenzene 1 ""0.33
" ""µg/l 1.00< 1.001634-04-4 Methyl tert-butyl ether 1 ""0.24
" ""µg/l 2.00< 2.0075-09-2 Methylene chloride 1 ""0.66
" ""µg/l 1.00< 1.0091-20-3 Naphthalene 1 ""0.35
" ""µg/l 1.00< 1.00127-18-4 Tetrachloroethene 1 ""0.57
" ""µg/l 1.00< 1.00108-88-3 Toluene 1 ""0.30
" ""µg/l 1.00< 1.0071-55-6 1,1,1-Trichloroethane 1 ""0.51
" ""µg/l 1.00< 1.0079-00-5 1,1,2-Trichloroethane 1 ""0.33
" ""µg/l 1.00< 1.0079-01-6 Trichloroethene 1 ""0.50
" ""µg/l 1.00< 1.0075-01-4 Vinyl chloride 1 ""0.47
" ""µg/l 2.00< 2.00179601-23-1 m,p-Xylene 1 ""0.38
" ""µg/l 1.00< 1.0095-47-6 o-Xylene 1 ""0.28
" ""µg/l 1.00< 1.00994-05-8 Tert-amyl methyl ether 1 ""0.49
" ""µg/l 10.0< 10.075-65-0 Tert-Butanol / butyl alcohol 1 ""5.90
" ""µg/l 20.0< 20.0123-91-1 1,4-Dioxane 1 ""11.4
Surrogate recoveries:
70-130 % " " ""4-Bromofluorobenzene 94 "460-00-4
70-130 % " " ""Toluene-d8 100 "2037-26-5
70-130 % " " ""1,2-Dichloroethane-d4 104 "17060-07-0
70-130 % " " ""Dibromofluoromethane 99 "1868-53-7
Microextractable Organic Compounds
Microextractables
Prepared by method General Preparation SVOC
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.010096-12-8 1,2-Dibromo-3-chloroprop
ane
1 1705548DS0.00362
" ""µg/l 0.0100< 0.0100106-93-4 1,2-Dibromoethane (EDB) 1 ""0.00336
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
Prepared by method SW846 3510C
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.05< 5.0583-32-9 Acenaphthene 1 1705460SM1.19
" ""µg/l 5.05< 5.05208-96-8 Acenaphthylene 1 ""1.10
" ""µg/l 5.05< 5.05120-12-7 Anthracene 1 ""1.17
" ""µg/l 5.05< 5.0556-55-3 Benzo (a) anthracene 1 ""1.14
" ""µg/l 5.05< 5.0550-32-8 Benzo (a) pyrene 1 ""1.02
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 22 of 5007-Apr-17 13:56
SPB-1 (Brook)
Sample IdentificationMatrix
28-Mar-17 12:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-03
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.05< 5.05205-99-2 Benzo (b) fluoranthene 1 1705460SM1.03
" ""µg/l 5.05< 5.05191-24-2 Benzo (g,h,i) perylene 1 ""1.34
" ""µg/l 5.05< 5.05207-08-9 Benzo (k) fluoranthene 1 ""1.36
" ""µg/l 5.05< 5.05117-81-7 Bis(2-ethylhexyl)phthalate 1 ""1.41
" ""µg/l 5.05< 5.0585-68-7 Butyl benzyl phthalate 1 ""1.33
" ""µg/l 5.05< 5.0559-50-7 4-Chloro-3-methylphenol 1 ""1.24
" ""µg/l 5.05< 5.0595-57-8 2-Chlorophenol 1 ""1.27
" ""µg/l 5.05< 5.05218-01-9 Chrysene 1 ""1.05
" ""µg/l 5.05< 5.0553-70-3 Dibenzo (a,h) anthracene 1 ""1.20
" ""µg/l 5.05< 5.05120-83-2 2,4-Dichlorophenol 1 ""1.22
" ""µg/l 5.05< 5.0584-66-2 Diethyl phthalate 1 ""1.54
" ""µg/l 5.05< 5.05131-11-3 Dimethyl phthalate 1 ""1.49
" ""µg/l 5.05< 5.05105-67-9 2,4-Dimethylphenol 1 ""1.42
" ""µg/l 5.05< 5.0584-74-2 Di-n-butyl phthalate 1 ""1.12
" ""µg/l 5.05< 5.05534-52-1 4,6-Dinitro-2-methylphenol 1 ""1.89
" ""µg/l 5.05< 5.0551-28-5 2,4-Dinitrophenol 1 ""2.17
" ""µg/l 5.05< 5.05117-84-0 Di-n-octyl phthalate 1 ""1.28
" ""µg/l 5.05< 5.05206-44-0 Fluoranthene 1 ""1.20
" ""µg/l 5.05< 5.0586-73-7 Fluorene 1 ""1.20
" ""µg/l 5.05< 5.05193-39-5 Indeno (1,2,3-cd) pyrene 1 ""1.30
" ""µg/l 5.05< 5.0595-48-7 2-Methylphenol 1 ""1.46
" ""µg/l 10.1< 10.1108-39-4,
106-44-53 & 4-Methylphenol 1 ""1.46
" ""µg/l 5.05< 5.0591-20-3 Naphthalene 1 ""1.06
" ""µg/l 5.05< 5.0588-75-5 2-Nitrophenol 1 ""1.46
" ""µg/l 20.2< 20.2100-02-7 4-Nitrophenol 1 ""2.95
" ""µg/l 20.2< 20.287-86-5 Pentachlorophenol 1 ""1.89
" ""µg/l 5.05< 5.0585-01-8 Phenanthrene 1 ""1.25
" ""µg/l 5.05< 5.05108-95-2 Phenol 1 ""0.993
" ""µg/l 5.05< 5.05129-00-0 Pyrene 1 ""1.44
" ""µg/l 5.05< 5.0595-95-4 2,4,5-Trichlorophenol 1 ""1.20
" ""µg/l 5.05< 5.0588-06-2 2,4,6-Trichlorophenol 1 ""1.09
Surrogate recoveries:
30-130 % " " ""2-Fluorobiphenyl 63 "321-60-8
15-110 % " " ""2-Fluorophenol 35 "367-12-4
30-130 % " " ""Nitrobenzene-d5 71 "4165-60-0
15-110 % " " ""Phenol-d5 22 "4165-62-2
30-130 % " " ""Terphenyl-dl4 66 "1718-51-0
15-110 % " " ""2,4,6-Tribromophenol 69 "118-79-6
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
Prepared by method SW846 3510C
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.204< 0.20412674-11-2 Aroclor-1016 1 1705401IMR0.106
" ""µg/l 0.204< 0.20411104-28-2 Aroclor-1221 1 ""0.117
" ""µg/l 0.204< 0.20411141-16-5 Aroclor-1232 1 ""0.113
" ""µg/l 0.204< 0.20453469-21-9 Aroclor-1242 1 ""0.0710
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 23 of 5007-Apr-17 13:56
SPB-1 (Brook)
Sample IdentificationMatrix
28-Mar-17 12:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-03
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.204< 0.20412672-29-6 Aroclor-1248 1 1705401IMR0.139
" ""µg/l 0.204< 0.20411097-69-1 Aroclor-1254 1 ""0.118
" ""µg/l 0.204< 0.20411096-82-5 Aroclor-1260 1 ""0.0868
" ""µg/l 0.204< 0.20437324-23-5 Aroclor-1262 1 ""0.0914
" ""µg/l 0.204< 0.20411100-14-4 Aroclor-1268 1 ""0.0934
Surrogate recoveries:
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr)
65 "10386-84-2
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr) [2C]
70 "10386-84-2
30-150 % " " ""Decachlorobiphenyl (Sr) 75 "2051-24-3
30-150 % " " ""Decachlorobiphenyl (Sr)
[2C]
70 "2051-24-3
Extractable Petroleum Hydrocarbons
Prepared by method SW846 3510C
EPA 1664B 04-Apr-1703-Apr-17mg/l 1.02.3Non-polar material
(SGT-HEM)
1 1705552KK0.2BsL
Total Metals by EPA 200/6000 Series Methods
Prepared by method General Prep-Metal
EPA 200/6000
methods
29-Mar-17N/AField
Preserved;
pH<2
confirmed
Preservation 1 1705326BK
Total Metals by EPA 200 Series Methods
EPA 200.7 05-Apr-1703-Apr-17mg/l 0.0050< 0.0050 X7440-22-4 Silver 1 1705511EDT0.0035
" ""mg/l 0.0040< 0.0040 X7440-38-2 Arsenic 1 ""0.0028
" 07-Apr-17"mg/l 0.1005.30 X7440-70-2 Calcium 1 ""0.0340
" 05-Apr-17"mg/l 0.0025< 0.0025 X7440-43-9 Cadmium 1 ""0.0004
" ""mg/l 0.0050< 0.0050 X7440-47-3 Chromium 1 ""0.0019
" 06-Apr-17"mg/l 0.0050< 0.0050 X7440-50-8 Copper 1 ""0.0029
" 06-Apr-17"mg/l 0.04000.178 X7439-89-6 Iron 1 ""0.0100R06
EPA
245.1/7470A
03-Apr-17"mg/l 0.00020< 0.00020 X7439-97-6 Mercury 1 1705513lnb0.00013
EPA 200.7 05-Apr-17"mg/l 0.01001.68 X7439-95-4 Magnesium 1 1705511EDT0.0074
" ""mg/l 0.0050< 0.0050 X7440-02-0 Nickel 1 ""0.0010
EPA 200.8 03-Apr-17"mg/l 0.00130< 0.00130 X7439-92-1 Lead 1 1705512edt0.00005R06
EPA 200.7 05-Apr-17"mg/l 0.0060< 0.0060 X7440-36-0 Antimony 1 1705511EDT0.0026
" ""mg/l 0.0150< 0.0150 X7782-49-2 Selenium 1 ""0.0072
" ""mg/l 0.0050< 0.0050 X7440-66-6 Zinc 1 ""0.0027
General Chemistry Parameters
Prepared by method EPA 200 Series
Calculation 07-Apr-1703-Apr-17mg/l 0.0100< 0.010016065-83-1 Trivalent Chromium 1 1705511EDT0.0053
SM 2340B (11) 07-Apr-17"mg/l
CaCO3
0.29120.2Hardness 1 [CALC]EDT0.115
Prepared by method SM4500-NH3 B (11)
SM4500-NH3 C.
(11)
05-Apr-1704-Apr-17mg/l 0.200< 0.200 XAmmonia as N 1 1705665AHK0.118
EPA 300.0 29-Mar-1729-Mar-17mg/l 1.0014.0 X16887-00-6 Chloride 1 1705349AHK0.0897
SM3500-Cr-B
(11)/7196A
28-Mar-17
17:40
28-Mar-17
17:10
mg/l 0.025< 0.02518540-29-9 Hexavalent Chromium 1 1705288TY0.014R01,LIV
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 24 of 5007-Apr-17 13:56
SPB-1 (Brook)
Sample IdentificationMatrix
28-Mar-17 12:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-03
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
General Chemistry Parameters
EPA 335.4 /
SW846 9012B
31-Mar-1731-Mar-17mg/l 0.00500< 0.00500 X57-12-5 Cyanide (total) 1 1705518RLT0.00426
SM2540D (11) 31-Mar-1730-Mar-17mg/l 0.5< 0.5 XTotal Suspended Solids 1 1705388CMB0.2
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 25 of 5007-Apr-17 13:56
LSP-1 (Pond)
Sample IdentificationMatrix
28-Mar-17 13:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-04
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
Prepared by method SW846 5030 Water MS
SW846 8260C 01-Apr-1731-Mar-17µg/l 10.0< 10.067-64-1 Acetone 1 1705468GMA0.80
" ""µg/l 1.00< 1.0071-43-2 Benzene 1 ""0.28
" ""µg/l 1.00< 1.0056-23-5 Carbon tetrachloride 1 ""0.44
" ""µg/l 0.50< 0.50106-93-4 1,2-Dibromoethane (EDB) 1 ""0.20
" ""µg/l 1.00< 1.0095-50-1 1,2-Dichlorobenzene 1 ""0.28
" ""µg/l 1.00< 1.00541-73-1 1,3-Dichlorobenzene 1 ""0.31
" ""µg/l 1.00< 1.00106-46-7 1,4-Dichlorobenzene 1 ""0.27
" ""µg/l 1.00< 1.0075-34-3 1,1-Dichloroethane 1 ""0.32
" ""µg/l 1.00< 1.00107-06-2 1,2-Dichloroethane 1 ""0.28
" ""µg/l 1.00< 1.0075-35-4 1,1-Dichloroethene 1 ""0.69
" ""µg/l 1.00< 1.00156-59-2 cis-1,2-Dichloroethene 1 ""0.33
" ""µg/l 1.00< 1.00100-41-4 Ethylbenzene 1 ""0.33
" ""µg/l 1.00< 1.001634-04-4 Methyl tert-butyl ether 1 ""0.24
" ""µg/l 2.00< 2.0075-09-2 Methylene chloride 1 ""0.66
" ""µg/l 1.00< 1.0091-20-3 Naphthalene 1 ""0.35
" ""µg/l 1.00< 1.00127-18-4 Tetrachloroethene 1 ""0.57
" ""µg/l 1.00< 1.00108-88-3 Toluene 1 ""0.30
" ""µg/l 1.00< 1.0071-55-6 1,1,1-Trichloroethane 1 ""0.51
" ""µg/l 1.00< 1.0079-00-5 1,1,2-Trichloroethane 1 ""0.33
" ""µg/l 1.00< 1.0079-01-6 Trichloroethene 1 ""0.50
" ""µg/l 1.00< 1.0075-01-4 Vinyl chloride 1 ""0.47
" ""µg/l 2.00< 2.00179601-23-1 m,p-Xylene 1 ""0.38
" ""µg/l 1.00< 1.0095-47-6 o-Xylene 1 ""0.28
" ""µg/l 1.00< 1.00994-05-8 Tert-amyl methyl ether 1 ""0.49
" ""µg/l 10.0< 10.075-65-0 Tert-Butanol / butyl alcohol 1 ""5.90
" ""µg/l 20.0< 20.0123-91-1 1,4-Dioxane 1 ""11.4
Surrogate recoveries:
70-130 % " " ""4-Bromofluorobenzene 95 "460-00-4
70-130 % " " ""Toluene-d8 100 "2037-26-5
70-130 % " " ""1,2-Dichloroethane-d4 105 "17060-07-0
70-130 % " " ""Dibromofluoromethane 101 "1868-53-7
Microextractable Organic Compounds
Microextractables
Prepared by method General Preparation SVOC
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.010096-12-8 1,2-Dibromo-3-chloroprop
ane
1 1705548DS0.00362
" ""µg/l 0.0100< 0.0100106-93-4 1,2-Dibromoethane (EDB) 1 ""0.00336
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
Prepared by method SW846 3510C
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.10< 5.1083-32-9 Acenaphthene 1 1705460SM1.20
" ""µg/l 5.10< 5.10208-96-8 Acenaphthylene 1 ""1.11
" ""µg/l 5.10< 5.10120-12-7 Anthracene 1 ""1.18
" ""µg/l 5.10< 5.1056-55-3 Benzo (a) anthracene 1 ""1.15
" ""µg/l 5.10< 5.1050-32-8 Benzo (a) pyrene 1 ""1.03
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 26 of 5007-Apr-17 13:56
LSP-1 (Pond)
Sample IdentificationMatrix
28-Mar-17 13:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-04
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GCMS
Semivolatile Organic Compounds
SW846 8270D 03-Apr-1731-Mar-17µg/l 5.10< 5.10205-99-2 Benzo (b) fluoranthene 1 1705460SM1.04
" ""µg/l 5.10< 5.10191-24-2 Benzo (g,h,i) perylene 1 ""1.36
" ""µg/l 5.10< 5.10207-08-9 Benzo (k) fluoranthene 1 ""1.38
" ""µg/l 5.10< 5.10117-81-7 Bis(2-ethylhexyl)phthalate 1 ""1.43
" ""µg/l 5.10< 5.1085-68-7 Butyl benzyl phthalate 1 ""1.35
" ""µg/l 5.10< 5.1059-50-7 4-Chloro-3-methylphenol 1 ""1.26
" ""µg/l 5.10< 5.1095-57-8 2-Chlorophenol 1 ""1.29
" ""µg/l 5.10< 5.10218-01-9 Chrysene 1 ""1.06
" ""µg/l 5.10< 5.1053-70-3 Dibenzo (a,h) anthracene 1 ""1.21
" ""µg/l 5.10< 5.10120-83-2 2,4-Dichlorophenol 1 ""1.23
" ""µg/l 5.10< 5.1084-66-2 Diethyl phthalate 1 ""1.55
" ""µg/l 5.10< 5.10131-11-3 Dimethyl phthalate 1 ""1.51
" ""µg/l 5.10< 5.10105-67-9 2,4-Dimethylphenol 1 ""1.44
" ""µg/l 5.10< 5.1084-74-2 Di-n-butyl phthalate 1 ""1.13
" ""µg/l 5.10< 5.10534-52-1 4,6-Dinitro-2-methylphenol 1 ""1.91
" ""µg/l 5.10< 5.1051-28-5 2,4-Dinitrophenol 1 ""2.19
" ""µg/l 5.10< 5.10117-84-0 Di-n-octyl phthalate 1 ""1.30
" ""µg/l 5.10< 5.10206-44-0 Fluoranthene 1 ""1.21
" ""µg/l 5.10< 5.1086-73-7 Fluorene 1 ""1.21
" ""µg/l 5.10< 5.10193-39-5 Indeno (1,2,3-cd) pyrene 1 ""1.32
" ""µg/l 5.10< 5.1095-48-7 2-Methylphenol 1 ""1.48
" ""µg/l 10.2< 10.2108-39-4,
106-44-53 & 4-Methylphenol 1 ""1.48
" ""µg/l 5.10< 5.1091-20-3 Naphthalene 1 ""1.07
" ""µg/l 5.10< 5.1088-75-5 2-Nitrophenol 1 ""1.48
" ""µg/l 20.4< 20.4100-02-7 4-Nitrophenol 1 ""2.98
" ""µg/l 20.4< 20.487-86-5 Pentachlorophenol 1 ""1.91
" ""µg/l 5.10< 5.1085-01-8 Phenanthrene 1 ""1.27
" ""µg/l 5.10< 5.10108-95-2 Phenol 1 ""1.00
" ""µg/l 5.10< 5.10129-00-0 Pyrene 1 ""1.46
" ""µg/l 5.10< 5.1095-95-4 2,4,5-Trichlorophenol 1 ""1.21
" ""µg/l 5.10< 5.1088-06-2 2,4,6-Trichlorophenol 1 ""1.10
Surrogate recoveries:
30-130 % " " ""2-Fluorobiphenyl 57 "321-60-8
15-110 % " " ""2-Fluorophenol 36 "367-12-4
30-130 % " " ""Nitrobenzene-d5 66 "4165-60-0
15-110 % " " ""Phenol-d5 22 "4165-62-2
30-130 % " " ""Terphenyl-dl4 68 "1718-51-0
15-110 % " " ""2,4,6-Tribromophenol 68 "118-79-6
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
Prepared by method SW846 3510C
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.200< 0.20012674-11-2 Aroclor-1016 1 1705401IMR0.104
" ""µg/l 0.200< 0.20011104-28-2 Aroclor-1221 1 ""0.115
" ""µg/l 0.200< 0.20011141-16-5 Aroclor-1232 1 ""0.111
" ""µg/l 0.200< 0.20053469-21-9 Aroclor-1242 1 ""0.0696
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 27 of 5007-Apr-17 13:56
LSP-1 (Pond)
Sample IdentificationMatrix
28-Mar-17 13:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-04
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Semivolatile Organic Compounds by GC
Polychlorinated Biphenyls
SW846 8082A 31-Mar-1730-Mar-17µg/l 0.200< 0.20012672-29-6 Aroclor-1248 1 1705401IMR0.136
" ""µg/l 0.200< 0.20011097-69-1 Aroclor-1254 1 ""0.116
" ""µg/l 0.200< 0.20011096-82-5 Aroclor-1260 1 ""0.0851
" ""µg/l 0.200< 0.20037324-23-5 Aroclor-1262 1 ""0.0896
" ""µg/l 0.200< 0.20011100-14-4 Aroclor-1268 1 ""0.0915
Surrogate recoveries:
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr)
45 "10386-84-2
30-150 % " " ""4,4-DB-Octafluorobiphenyl
(Sr) [2C]
45 "10386-84-2
30-150 % " " ""Decachlorobiphenyl (Sr) 65 "2051-24-3
30-150 % " " ""Decachlorobiphenyl (Sr)
[2C]
65 "2051-24-3
Extractable Petroleum Hydrocarbons
Prepared by method SW846 3510C
EPA 1664B 04-Apr-1703-Apr-17mg/l 1.0< 1.0Non-polar material
(SGT-HEM)
1 1705552KK0.2BsL
Total Metals by EPA 200/6000 Series Methods
Prepared by method General Prep-Metal
EPA 200/6000
methods
29-Mar-17N/AField
Preserved;
pH<2
confirmed
Preservation 1 1705326BK
Total Metals by EPA 200 Series Methods
EPA 200.7 05-Apr-1703-Apr-17mg/l 0.0050< 0.0050 X7440-22-4 Silver 1 1705511EDT0.0035
" ""mg/l 0.0040< 0.0040 X7440-38-2 Arsenic 1 ""0.0028
" 07-Apr-17"mg/l 0.1005.30 X7440-70-2 Calcium 1 ""0.0340
" 05-Apr-17"mg/l 0.0025< 0.0025 X7440-43-9 Cadmium 1 ""0.0004
" ""mg/l 0.0050< 0.0050 X7440-47-3 Chromium 1 ""0.0019
" 06-Apr-17"mg/l 0.0050< 0.0050 X7440-50-8 Copper 1 ""0.0029
" 06-Apr-17"mg/l 0.04000.233 X7439-89-6 Iron 1 ""0.0100R06
EPA
245.1/7470A
03-Apr-17"mg/l 0.00020< 0.00020 X7439-97-6 Mercury 1 1705513lnb0.00013
EPA 200.7 05-Apr-17"mg/l 0.01001.66 X7439-95-4 Magnesium 1 1705511EDT0.0074
" ""mg/l 0.0050< 0.0050 X7440-02-0 Nickel 1 ""0.0010
EPA 200.8 03-Apr-17"mg/l 0.00130< 0.00130 X7439-92-1 Lead 1 1705512edt0.00005R06
EPA 200.7 05-Apr-17"mg/l 0.0060< 0.0060 X7440-36-0 Antimony 1 1705511EDT0.0026
" ""mg/l 0.0150< 0.0150 X7782-49-2 Selenium 1 ""0.0072
" ""mg/l 0.0050< 0.0050 X7440-66-6 Zinc 1 ""0.0027
General Chemistry Parameters
Prepared by method EPA 200 Series
Calculation 07-Apr-1703-Apr-17mg/l 0.0100< 0.010016065-83-1 Trivalent Chromium 1 1705511EDT0.0053
SM 2340B (11) 07-Apr-17"mg/l
CaCO3
0.29120.1Hardness 1 [CALC]EDT0.115
Prepared by method SM4500-NH3 B (11)
SM4500-NH3 C.
(11)
05-Apr-1704-Apr-17mg/l 0.200< 0.200 XAmmonia as N 1 1705665AHK0.118
EPA 300.0 29-Mar-1729-Mar-17mg/l 1.0013.6 X16887-00-6 Chloride 1 1705349AHK0.0897
SM3500-Cr-B
(11)/7196A
28-Mar-17
17:42
28-Mar-17
17:10
mg/l 0.025< 0.02518540-29-9 Hexavalent Chromium 1 1705288TY0.014R01,LIV
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 28 of 5007-Apr-17 13:56
LSP-1 (Pond)
Sample IdentificationMatrix
28-Mar-17 13:30
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 Surface WaterSC32894-04
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
General Chemistry Parameters
EPA 335.4 /
SW846 9012B
05-Apr-1705-Apr-17mg/l 0.00500< 0.00500 X57-12-5 Cyanide (total) 1 1705670RLT0.00426
SM2540D (11) 31-Mar-1730-Mar-17mg/l 0.50.6 XTotal Suspended Solids 1 1705388CMB0.2
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 29 of 5007-Apr-17 13:56
Reagent Blank
Sample IdentificationMatrix
28-Mar-17 00:00
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 AqueousSC32894-05
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Microextractable Organic Compounds
Microextractables
Prepared by method General Preparation SVOC
SW846 8011 03-Apr-1703-Apr-17µg/l 0.0100< 0.010096-12-8 1,2-Dibromo-3-chloroprop
ane
1 1705548DS0.00362
" ""µg/l 0.0100< 0.0100106-93-4 1,2-Dibromoethane (EDB) 1 ""0.00336
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 30 of 5007-Apr-17 13:56
Trip Blank
Sample IdentificationMatrix
28-Mar-17 00:00
Collection Date/Time Received
28-Mar-17
Client Project #
60306709-452 AqueousSC32894-06
Result AnalyzedMethod Ref. Cert.BatchPreparedDilutionAnalyte(s) Units *RDLFlagCAS No. AnalystMDL
Volatile Organic Compounds
Volatile Organic Compounds by SW846 8260
Prepared by method SW846 5030 Water MS
SW846 8260C 01-Apr-1731-Mar-17µg/l 10.0< 10.067-64-1 Acetone 1 1705468GMA0.80
" ""µg/l 1.00< 1.0071-43-2 Benzene 1 ""0.28
" ""µg/l 1.00< 1.0056-23-5 Carbon tetrachloride 1 ""0.44
" ""µg/l 0.50< 0.50106-93-4 1,2-Dibromoethane (EDB) 1 ""0.20
" ""µg/l 1.00< 1.0095-50-1 1,2-Dichlorobenzene 1 ""0.28
" ""µg/l 1.00< 1.00541-73-1 1,3-Dichlorobenzene 1 ""0.31
" ""µg/l 1.00< 1.00106-46-7 1,4-Dichlorobenzene 1 ""0.27
" ""µg/l 1.00< 1.0075-34-3 1,1-Dichloroethane 1 ""0.32
" ""µg/l 1.00< 1.00107-06-2 1,2-Dichloroethane 1 ""0.28
" ""µg/l 1.00< 1.0075-35-4 1,1-Dichloroethene 1 ""0.69
" ""µg/l 1.00< 1.00156-59-2 cis-1,2-Dichloroethene 1 ""0.33
" ""µg/l 1.00< 1.00100-41-4 Ethylbenzene 1 ""0.33
" ""µg/l 1.00< 1.001634-04-4 Methyl tert-butyl ether 1 ""0.24
" ""µg/l 2.00< 2.0075-09-2 Methylene chloride 1 ""0.66
" ""µg/l 1.00< 1.0091-20-3 Naphthalene 1 ""0.35
" ""µg/l 1.00< 1.00127-18-4 Tetrachloroethene 1 ""0.57
" ""µg/l 1.00< 1.00108-88-3 Toluene 1 ""0.30
" ""µg/l 1.00< 1.0071-55-6 1,1,1-Trichloroethane 1 ""0.51
" ""µg/l 1.00< 1.0079-00-5 1,1,2-Trichloroethane 1 ""0.33
" ""µg/l 1.00< 1.0079-01-6 Trichloroethene 1 ""0.50
" ""µg/l 1.00< 1.0075-01-4 Vinyl chloride 1 ""0.47
" ""µg/l 2.00< 2.00179601-23-1 m,p-Xylene 1 ""0.38
" ""µg/l 1.00< 1.0095-47-6 o-Xylene 1 ""0.28
" ""µg/l 1.00< 1.00994-05-8 Tert-amyl methyl ether 1 ""0.49
" ""µg/l 10.0< 10.075-65-0 Tert-Butanol / butyl alcohol 1 ""5.90
" ""µg/l 20.0< 20.0123-91-1 1,4-Dioxane 1 ""11.4
Surrogate recoveries:
70-130 % " " ""4-Bromofluorobenzene 92 "460-00-4
70-130 % " " ""Toluene-d8 99 "2037-26-5
70-130 % " " ""1,2-Dichloroethane-d4 105 "17060-07-0
70-130 % " " ""Dibromofluoromethane 98 "1868-53-7
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* Reportable Detection Limit Page 31 of 5007-Apr-17 13:56
Volatile Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8260C
Batch 1705468 - SW846 5030 Water MS
Blank (1705468-BLK1) Prepared & Analyzed: 31-Mar-17
µg/l< 1.001,1,2-Trichlorotrifluoroethane (Freon 113) 1.00
µg/l< 10.0Acetone 10.0
µg/l< 0.50Acrylonitrile 0.50
µg/l< 1.00Benzene 1.00
µg/l< 1.00Bromobenzene 1.00
µg/l< 1.00Bromochloromethane 1.00
µg/l< 0.50Bromodichloromethane 0.50
µg/l< 1.00Bromoform 1.00
µg/l< 2.00Bromomethane 2.00
µg/l< 2.002-Butanone (MEK) 2.00
µg/l< 1.00n-Butylbenzene 1.00
µg/l< 1.00sec-Butylbenzene 1.00
µg/l< 1.00tert-Butylbenzene 1.00
µg/l< 2.00Carbon disulfide 2.00
µg/l< 1.00Carbon tetrachloride 1.00
µg/l< 1.00Chlorobenzene 1.00
µg/l< 2.00Chloroethane 2.00
µg/l< 1.00Chloroform 1.00
µg/l< 2.00Chloromethane 2.00
µg/l< 1.002-Chlorotoluene 1.00
µg/l< 1.004-Chlorotoluene 1.00
µg/l< 2.001,2-Dibromo-3-chloropropane 2.00
µg/l< 0.50Dibromochloromethane 0.50
µg/l< 0.501,2-Dibromoethane (EDB) 0.50
µg/l< 1.00Dibromomethane 1.00
µg/l< 1.001,2-Dichlorobenzene 1.00
µg/l< 1.001,3-Dichlorobenzene 1.00
µg/l< 1.001,4-Dichlorobenzene 1.00
µg/l< 2.00Dichlorodifluoromethane (Freon12) 2.00
µg/l< 1.001,1-Dichloroethane 1.00
µg/l< 1.001,2-Dichloroethane 1.00
µg/l< 1.001,1-Dichloroethene 1.00
µg/l< 1.00cis-1,2-Dichloroethene 1.00
µg/l< 1.00trans-1,2-Dichloroethene 1.00
µg/l< 1.001,2-Dichloropropane 1.00
µg/l< 1.001,3-Dichloropropane 1.00
µg/l< 1.002,2-Dichloropropane 1.00
µg/l< 1.001,1-Dichloropropene 1.00
µg/l< 0.50cis-1,3-Dichloropropene 0.50
µg/l< 0.50trans-1,3-Dichloropropene 0.50
µg/l< 1.00Ethylbenzene 1.00
µg/l< 0.50Hexachlorobutadiene 0.50
µg/l< 2.002-Hexanone (MBK) 2.00
µg/l< 1.00Isopropylbenzene 1.00
µg/l< 1.004-Isopropyltoluene 1.00
µg/l< 1.00Methyl tert-butyl ether 1.00
µg/l< 2.004-Methyl-2-pentanone (MIBK) 2.00
µg/l< 2.00Methylene chloride 2.00
µg/l< 1.00Naphthalene 1.00
µg/l< 1.00n-Propylbenzene 1.00
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 32 of 5007-Apr-17 13:56
Volatile Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8260C
Batch 1705468 - SW846 5030 Water MS
Blank (1705468-BLK1) Prepared & Analyzed: 31-Mar-17
µg/l< 1.00Styrene 1.00
µg/l< 1.001,1,1,2-Tetrachloroethane 1.00
µg/l< 0.501,1,2,2-Tetrachloroethane 0.50
µg/l< 1.00Tetrachloroethene 1.00
µg/l< 1.00Toluene 1.00
µg/l< 1.001,2,3-Trichlorobenzene 1.00
µg/l< 1.001,2,4-Trichlorobenzene 1.00
µg/l< 1.001,3,5-Trichlorobenzene 1.00
µg/l< 1.001,1,1-Trichloroethane 1.00
µg/l< 1.001,1,2-Trichloroethane 1.00
µg/l< 1.00Trichloroethene 1.00
µg/l< 1.00Trichlorofluoromethane (Freon 11) 1.00
µg/l< 1.001,2,3-Trichloropropane 1.00
µg/l< 1.001,2,4-Trimethylbenzene 1.00
µg/l< 1.001,3,5-Trimethylbenzene 1.00
µg/l< 1.00Vinyl chloride 1.00
µg/l< 2.00m,p-Xylene 2.00
µg/l< 1.00o-Xylene 1.00
µg/l< 2.00Tetrahydrofuran 2.00
µg/l< 1.00Ethyl ether 1.00
µg/l< 1.00Tert-amyl methyl ether 1.00
µg/l< 1.00Ethyl tert-butyl ether 1.00
µg/l< 1.00Di-isopropyl ether 1.00
µg/l< 10.0Tert-Butanol / butyl alcohol 10.0
µg/l< 20.01,4-Dioxane 20.0
µg/l< 5.00trans-1,4-Dichloro-2-butene 5.00
µg/l< 200Ethanol 200
50.0 70-130Surrogate: 4-Bromofluorobenzene 47.5 µg/l 95
50.0 70-130Surrogate: Toluene-d8 49.8 µg/l 100
50.0 70-130Surrogate: 1,2-Dichloroethane-d4 49.8 µg/l 100
50.0 70-130Surrogate: Dibromofluoromethane 44.7 µg/l 89
LCS (1705468-BS1) Prepared & Analyzed: 31-Mar-17
20.0 70-130µg/l17.6 881,1,2-Trichlorotrifluoroethane (Freon 113)
20.0 70-130µg/l21.0 105Acetone
20.0 70-130µg/l18.3 91Acrylonitrile
20.0 70-130µg/l19.8 99Benzene
20.0 70-130µg/l20.4 102Bromobenzene
20.0 70-130µg/l19.0 95Bromochloromethane
20.0 70-130µg/l16.7 84Bromodichloromethane
20.0 70-130µg/l17.2 86Bromoform
20.0 70-130µg/l17.8 89Bromomethane
20.0 70-130µg/l21.5 1082-Butanone (MEK)
20.0 70-130µg/l17.8 89n-Butylbenzene
20.0 70-130µg/l19.5 98sec-Butylbenzene
20.0 70-130µg/l19.4 97tert-Butylbenzene
20.0 70-130µg/l16.0 80Carbon disulfide
20.0 70-130µg/l17.8 89Carbon tetrachloride
20.0 70-130µg/l19.4 97Chlorobenzene
20.0 70-130µg/l17.5 88Chloroethane
20.0 70-130µg/l18.1 91Chloroform
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* Reportable Detection Limit Page 33 of 5007-Apr-17 13:56
Volatile Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8260C
Batch 1705468 - SW846 5030 Water MS
LCS (1705468-BS1) Prepared & Analyzed: 31-Mar-17
20.0 70-130µg/l18.1 90Chloromethane
20.0 70-130µg/l20.2 1012-Chlorotoluene
20.0 70-130µg/l19.0 954-Chlorotoluene
20.0 70-130µg/l17.2 861,2-Dibromo-3-chloropropane
20.0 70-130µg/l17.5 88Dibromochloromethane
20.0 70-130µg/l19.4 971,2-Dibromoethane (EDB)
20.0 70-130µg/l19.1 95Dibromomethane
20.0 70-130µg/l20.1 1011,2-Dichlorobenzene
20.0 70-130µg/l20.7 1031,3-Dichlorobenzene
20.0 70-130µg/l18.7 931,4-Dichlorobenzene
20.0 70-130µg/l16.9 85Dichlorodifluoromethane (Freon12)
20.0 70-130µg/l19.4 971,1-Dichloroethane
20.0 70-130µg/l18.4 921,2-Dichloroethane
20.0 70-130µg/l18.0 901,1-Dichloroethene
20.0 70-130µg/l20.1 101cis-1,2-Dichloroethene
20.0 70-130µg/l18.2 91trans-1,2-Dichloroethene
20.0 70-130µg/l19.1 961,2-Dichloropropane
20.0 70-130µg/l19.5 981,3-Dichloropropane
20.0 70-130µg/l19.1 952,2-Dichloropropane
20.0 70-130µg/l18.1 901,1-Dichloropropene
20.0 70-130µg/l20.5 102cis-1,3-Dichloropropene
20.0 70-130µg/l20.9 105trans-1,3-Dichloropropene
20.0 70-130µg/l19.0 95Ethylbenzene
20.0 70-130µg/l20.8 104Hexachlorobutadiene
20.0 70-130µg/l17.1 852-Hexanone (MBK)
20.0 70-130µg/l19.3 97Isopropylbenzene
20.0 70-130µg/l18.2 914-Isopropyltoluene
20.0 70-130µg/l20.3 101Methyl tert-butyl ether
20.0 70-130µg/l17.4 874-Methyl-2-pentanone (MIBK)
20.0 70-130µg/l17.3 87Methylene chloride
20.0 70-130µg/l21.1 106Naphthalene
20.0 70-130µg/l18.8 94n-Propylbenzene
20.0 70-130µg/l18.2 91Styrene
20.0 70-130µg/l18.1 901,1,1,2-Tetrachloroethane
20.0 70-130µg/l15.9 791,1,2,2-Tetrachloroethane
20.0 70-130µg/l19.8 99Tetrachloroethene
20.0 70-130µg/l19.3 96Toluene
20.0 70-130µg/l20.6 1031,2,3-Trichlorobenzene
20.0 70-130µg/l20.2 1011,2,4-Trichlorobenzene
20.0 70-130µg/l18.3 921,3,5-Trichlorobenzene
20.0 70-130µg/l19.5 981,1,1-Trichloroethane
20.0 70-130µg/l19.8 991,1,2-Trichloroethane
20.0 70-130µg/l19.0 95Trichloroethene
20.0 70-130µg/l18.9 95Trichlorofluoromethane (Freon 11)
20.0 70-130µg/l20.3 1021,2,3-Trichloropropane
20.0 70-130µg/l19.1 951,2,4-Trimethylbenzene
20.0 70-130µg/l18.9 941,3,5-Trimethylbenzene
20.0 70-130µg/l17.0 85Vinyl chloride
20.0 70-130µg/l19.2 96m,p-Xylene
20.0 70-130µg/l19.6 98o-Xylene
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 34 of 5007-Apr-17 13:56
Volatile Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8260C
Batch 1705468 - SW846 5030 Water MS
LCS (1705468-BS1) Prepared & Analyzed: 31-Mar-17
20.0 70-130µg/l18.6 93Tetrahydrofuran
20.0 70-130µg/l17.4 87Ethyl ether
20.0 70-130µg/l18.0 90Tert-amyl methyl ether
20.0 70-130µg/l18.2 91Ethyl tert-butyl ether
20.0 70-130µg/l18.0 90Di-isopropyl ether
200 70-130µg/l228 114Tert-Butanol / butyl alcohol
200 70-130µg/l244 1221,4-Dioxane
20.0 70-130µg/lQC226.2 131trans-1,4-Dichloro-2-butene
400 70-130µg/l475 119Ethanol
50.0 70-130Surrogate: 4-Bromofluorobenzene 51.3 µg/l 103
50.0 70-130Surrogate: Toluene-d8 50.0 µg/l 100
50.0 70-130Surrogate: 1,2-Dichloroethane-d4 47.0 µg/l 94
50.0 70-130Surrogate: Dibromofluoromethane 49.3 µg/l 99
LCS Dup (1705468-BSD1) Prepared & Analyzed: 31-Mar-17
20.0 2070-130 2µg/l17.2 861,1,2-Trichlorotrifluoroethane (Freon 113)
20.0 2070-130 8µg/l22.9 114Acetone
20.0 2070-130 4µg/l19.0 95Acrylonitrile
20.0 2070-130 0.2µg/l19.7 99Benzene
20.0 2070-130 2µg/l20.1 100Bromobenzene
20.0 2070-130 2µg/l19.4 97Bromochloromethane
20.0 2070-130 2µg/l17.1 85Bromodichloromethane
20.0 2070-130 2µg/l17.6 88Bromoform
20.0 2070-130 3µg/l18.4 92Bromomethane
20.0 2070-130 3µg/l22.2 1112-Butanone (MEK)
20.0 2070-130 3µg/l18.4 92n-Butylbenzene
20.0 2070-130 2µg/l19.1 95sec-Butylbenzene
20.0 2070-130 3µg/l18.8 94tert-Butylbenzene
20.0 2070-130 1µg/l16.2 81Carbon disulfide
20.0 2070-130 2µg/l17.5 87Carbon tetrachloride
20.0 2070-130 0.3µg/l19.4 97Chlorobenzene
20.0 2070-130 0.2µg/l17.5 88Chloroethane
20.0 2070-130 1µg/l18.3 92Chloroform
20.0 2070-130 0.9µg/l17.9 90Chloromethane
20.0 2070-130 0.2µg/l20.2 1012-Chlorotoluene
20.0 2070-130 0.6µg/l18.9 954-Chlorotoluene
20.0 2070-130 7µg/l18.4 921,2-Dibromo-3-chloropropane
20.0 2070-130 2µg/l17.9 89Dibromochloromethane
20.0 2070-130 2µg/l19.8 991,2-Dibromoethane (EDB)
20.0 2070-130 4µg/l19.8 99Dibromomethane
20.0 2070-130 2µg/l20.6 1031,2-Dichlorobenzene
20.0 2070-130 2µg/l20.3 1011,3-Dichlorobenzene
20.0 2070-130 3µg/l19.2 961,4-Dichlorobenzene
20.0 2070-130 1µg/l16.7 84Dichlorodifluoromethane (Freon12)
20.0 2070-130 1µg/l19.6 981,1-Dichloroethane
20.0 2070-130 3µg/l18.9 951,2-Dichloroethane
20.0 2070-130 1µg/l17.7 891,1-Dichloroethene
20.0 2070-130 0.3µg/l20.0 100cis-1,2-Dichloroethene
20.0 2070-130 1µg/l17.9 90trans-1,2-Dichloroethene
20.0 2070-130 2µg/l19.5 971,2-Dichloropropane
20.0 2070-130 3µg/l20.1 1011,3-Dichloropropane
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 35 of 5007-Apr-17 13:56
Volatile Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8260C
Batch 1705468 - SW846 5030 Water MS
LCS Dup (1705468-BSD1) Prepared & Analyzed: 31-Mar-17
20.0 2070-130 3µg/l18.4 922,2-Dichloropropane
20.0 2070-130 2µg/l17.8 891,1-Dichloropropene
20.0 2070-130 1µg/l20.7 104cis-1,3-Dichloropropene
20.0 2070-130 1µg/l21.2 106trans-1,3-Dichloropropene
20.0 2070-130 1µg/l18.8 94Ethylbenzene
20.0 2070-130 3µg/l21.3 107Hexachlorobutadiene
20.0 2070-130 5µg/l17.9 892-Hexanone (MBK)
20.0 2070-130 3µg/l18.8 94Isopropylbenzene
20.0 2070-130 1µg/l18.4 924-Isopropyltoluene
20.0 2070-130 3µg/l20.9 105Methyl tert-butyl ether
20.0 2070-130 6µg/l18.4 924-Methyl-2-pentanone (MIBK)
20.0 2070-130 2µg/l17.8 89Methylene chloride
20.0 2070-130 1µg/l21.4 107Naphthalene
20.0 2070-130 2µg/l18.4 92n-Propylbenzene
20.0 2070-130 0.7µg/l18.0 90Styrene
20.0 2070-130 2µg/l17.8 891,1,1,2-Tetrachloroethane
20.0 2070-130 3µg/l16.4 821,1,2,2-Tetrachloroethane
20.0 2070-130 4µg/l19.0 95Tetrachloroethene
20.0 2070-130 0.3µg/l19.4 97Toluene
20.0 2070-130 0.1µg/l20.6 1031,2,3-Trichlorobenzene
20.0 2070-130 0.8µg/l20.0 1001,2,4-Trichlorobenzene
20.0 2070-130 0.2µg/l18.4 921,3,5-Trichlorobenzene
20.0 2070-130 1µg/l19.3 961,1,1-Trichloroethane
20.0 2070-130 2µg/l20.3 1011,1,2-Trichloroethane
20.0 2070-130 0.6µg/l19.1 96Trichloroethene
20.0 2070-130 2µg/l18.6 93Trichlorofluoromethane (Freon 11)
20.0 2070-130 3µg/l20.9 1051,2,3-Trichloropropane
20.0 2070-130 2µg/l18.8 941,2,4-Trimethylbenzene
20.0 2070-130 2µg/l18.5 921,3,5-Trimethylbenzene
20.0 2070-130 0.7µg/l16.9 85Vinyl chloride
20.0 2070-130 2µg/l18.8 94m,p-Xylene
20.0 2070-130 1µg/l19.3 96o-Xylene
20.0 2070-130 5µg/l19.6 98Tetrahydrofuran
20.0 2070-130 2µg/l17.7 89Ethyl ether
20.0 2070-130 3µg/l18.6 93Tert-amyl methyl ether
20.0 2070-130 3µg/l18.9 94Ethyl tert-butyl ether
20.0 2070-130 3µg/l18.5 93Di-isopropyl ether
200 2070-130 5µg/l240 120Tert-Butanol / butyl alcohol
200 2070-130 0.5µg/l245 1231,4-Dioxane
20.0 2070-130 3µg/lQC226.9 134trans-1,4-Dichloro-2-butene
400 2070-130 7µg/l508 127Ethanol
50.0 70-130Surrogate: 4-Bromofluorobenzene 50.7 µg/l 101
50.0 70-130Surrogate: Toluene-d8 49.5 µg/l 99
50.0 70-130Surrogate: 1,2-Dichloroethane-d4 48.1 µg/l 96
50.0 70-130Surrogate: Dibromofluoromethane 49.8 µg/l 100
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 36 of 5007-Apr-17 13:56
Microextractable Organic Compounds - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8011
Batch 1705548 - General Preparation SVOC
Blank (1705548-BLK1) Prepared & Analyzed: 03-Apr-17
µg/l< 0.01001,2-Dibromo-3-chloropropane 0.0100
µg/l< 0.01001,2-Dibromoethane (EDB) 0.0100
LCS (1705548-BS1) Prepared & Analyzed: 03-Apr-17
0.200 60-140µg/l0.210 1051,2-Dibromoethane (EDB) 0.0100
0.200 60-140µg/l0.211 1061,2-Dibromo-3-chloropropane 0.0100
LCS Dup (1705548-BSD1) Prepared & Analyzed: 03-Apr-17
0.200 5060-140 11µg/l0.235 1181,2-Dibromo-3-chloropropane 0.0100
0.200 5060-140 10µg/l0.233 1161,2-Dibromoethane (EDB) 0.0100
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 37 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GCMS - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8270D
Batch 1705460 - SW846 3510C
Blank (1705460-BLK1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
µg/l< 5.00Acenaphthene 5.00
µg/l< 5.00Acenaphthylene 5.00
µg/l< 5.00Aniline 5.00
µg/l< 5.00Anthracene 5.00
µg/l< 5.00Azobenzene/Diphenyldiazene 5.00
µg/l< 5.00Benzidine 5.00
µg/l< 5.00Benzo (a) anthracene 5.00
µg/l< 5.00Benzo (a) pyrene 5.00
µg/l< 5.00Benzo (b) fluoranthene 5.00
µg/l< 5.00Benzo (g,h,i) perylene 5.00
µg/l< 5.00Benzo (k) fluoranthene 5.00
µg/l< 5.00Benzoic acid 5.00
µg/l< 5.00Benzyl alcohol 5.00
µg/l< 5.00Bis(2-chloroethoxy)methane 5.00
µg/l< 5.00Bis(2-chloroethyl)ether 5.00
µg/l< 5.00Bis(2-chloroisopropyl)ether 5.00
µg/l< 5.00Bis(2-ethylhexyl)phthalate 5.00
µg/l< 5.004-Bromophenyl phenyl ether 5.00
µg/l< 5.00Butyl benzyl phthalate 5.00
µg/l< 5.00Carbazole 5.00
µg/l< 5.004-Chloro-3-methylphenol 5.00
µg/l< 5.004-Chloroaniline 5.00
µg/l< 5.002-Chloronaphthalene 5.00
µg/l< 5.002-Chlorophenol 5.00
µg/l< 5.004-Chlorophenyl phenyl ether 5.00
µg/l< 5.00Chrysene 5.00
µg/l< 5.00Dibenzo (a,h) anthracene 5.00
µg/l< 5.00Dibenzofuran 5.00
µg/l< 5.001,2-Dichlorobenzene 5.00
µg/l< 5.001,3-Dichlorobenzene 5.00
µg/l< 5.001,4-Dichlorobenzene 5.00
µg/l< 5.003,3´-Dichlorobenzidine 5.00
µg/l< 5.002,4-Dichlorophenol 5.00
µg/l< 5.00Diethyl phthalate 5.00
µg/l< 5.00Dimethyl phthalate 5.00
µg/l< 5.002,4-Dimethylphenol 5.00
µg/l< 5.00Di-n-butyl phthalate 5.00
µg/l< 5.004,6-Dinitro-2-methylphenol 5.00
µg/l< 5.002,4-Dinitrophenol 5.00
µg/l< 5.002,4-Dinitrotoluene 5.00
µg/l< 5.002,6-Dinitrotoluene 5.00
µg/l< 5.00Di-n-octyl phthalate 5.00
µg/l< 5.00Fluoranthene 5.00
µg/l< 5.00Fluorene 5.00
µg/l< 5.00Hexachlorobenzene 5.00
µg/l< 5.00Hexachlorobutadiene 5.00
µg/l< 5.00Hexachlorocyclopentadiene 5.00
µg/l< 5.00Hexachloroethane 5.00
µg/l< 5.00Indeno (1,2,3-cd) pyrene 5.00
µg/l< 5.00Isophorone 5.00
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 38 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GCMS - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8270D
Batch 1705460 - SW846 3510C
Blank (1705460-BLK1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
µg/l< 5.002-Methylnaphthalene 5.00
µg/l< 5.002-Methylphenol 5.00
µg/l< 10.03 & 4-Methylphenol 10.0
µg/l< 5.00Naphthalene 5.00
µg/l< 5.002-Nitroaniline 5.00
µg/l< 5.003-Nitroaniline 5.00
µg/l< 5.004-Nitroaniline 5.00
µg/l< 5.00Nitrobenzene 5.00
µg/l< 5.002-Nitrophenol 5.00
µg/l< 20.04-Nitrophenol 20.0
µg/l< 5.00N-Nitrosodimethylamine 5.00
µg/l< 5.00N-Nitrosodi-n-propylamine 5.00
µg/l< 5.00N-Nitrosodiphenylamine 5.00
µg/l< 20.0Pentachlorophenol 20.0
µg/l< 5.00Phenanthrene 5.00
µg/l< 5.00Phenol 5.00
µg/l< 5.00Pyrene 5.00
µg/l< 5.00Pyridine 5.00
µg/l< 5.001,2,4-Trichlorobenzene 5.00
µg/l< 5.001-Methylnaphthalene 5.00
µg/l< 5.002,4,5-Trichlorophenol 5.00
µg/l< 5.002,4,6-Trichlorophenol 5.00
µg/l< 5.00Pentachloronitrobenzene 5.00
µg/l< 5.001,2,4,5-Tetrachlorobenzene 5.00
50.0 30-130Surrogate: 2-Fluorobiphenyl 39.8 µg/l 80
50.0 15-110Surrogate: 2-Fluorophenol 40.9 µg/l 82
50.0 30-130Surrogate: Nitrobenzene-d5 45.0 µg/l 90
50.0 15-110Surrogate: Phenol-d5 39.4 µg/l 79
50.0 30-130Surrogate: Terphenyl-dl4 46.5 µg/l 93
50.0 15-110Surrogate: 2,4,6-Tribromophenol 43.0 µg/l 86
LCS (1705460-BS1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
50.0 40-140µg/l37.5 75Acenaphthene 5.00
50.0 40-140µg/l40.1 80Acenaphthylene 5.00
50.0 40-140µg/lQC217.2 34Aniline 5.00
50.0 40-140µg/l34.6 69Anthracene 5.00
50.0 40-140µg/l42.5 85Azobenzene/Diphenyldiazene 5.00
50.0 40-140µg/lQC219.0 38Benzidine 5.00
50.0 40-140µg/l39.2 78Benzo (a) anthracene 5.00
50.0 40-140µg/l38.2 76Benzo (a) pyrene 5.00
50.0 40-140µg/l43.8 88Benzo (b) fluoranthene 5.00
50.0 40-140µg/l36.5 73Benzo (g,h,i) perylene 5.00
50.0 40-140µg/l36.6 73Benzo (k) fluoranthene 5.00
50.0 30-130µg/l37.9 76Benzoic acid 5.00
50.0 40-140µg/l36.2 72Benzyl alcohol 5.00
50.0 40-140µg/l31.8 64Bis(2-chloroethoxy)methane 5.00
50.0 40-140µg/l32.2 64Bis(2-chloroethyl)ether 5.00
50.0 40-140µg/l33.2 66Bis(2-chloroisopropyl)ether 5.00
50.0 40-140µg/l37.9 76Bis(2-ethylhexyl)phthalate 5.00
50.0 40-140µg/l36.5 734-Bromophenyl phenyl ether 5.00
50.0 40-140µg/l35.4 71Butyl benzyl phthalate 5.00
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* Reportable Detection Limit Page 39 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GCMS - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8270D
Batch 1705460 - SW846 3510C
LCS (1705460-BS1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
50.0 40-140µg/l49.9 100Carbazole 5.00
50.0 30-130µg/l37.1 744-Chloro-3-methylphenol 5.00
50.0 40-140µg/lQC218.9 384-Chloroaniline 5.00
50.0 40-140µg/l47.3 952-Chloronaphthalene 5.00
50.0 30-130µg/l37.3 752-Chlorophenol 5.00
50.0 40-140µg/l35.2 704-Chlorophenyl phenyl ether 5.00
50.0 40-140µg/l35.4 71Chrysene 5.00
50.0 40-140µg/l38.9 78Dibenzo (a,h) anthracene 5.00
50.0 40-140µg/l44.7 89Dibenzofuran 5.00
50.0 40-140µg/l42.5 851,2-Dichlorobenzene 5.00
50.0 40-140µg/l41.6 831,3-Dichlorobenzene 5.00
50.0 40-140µg/l41.4 831,4-Dichlorobenzene 5.00
50.0 40-140µg/l40.8 823,3´-Dichlorobenzidine 5.00
50.0 30-130µg/l36.4 732,4-Dichlorophenol 5.00
50.0 40-140µg/l34.5 69Diethyl phthalate 5.00
50.0 40-140µg/l35.0 70Dimethyl phthalate 5.00
50.0 30-130µg/l36.1 722,4-Dimethylphenol 5.00
50.0 40-140µg/l35.9 72Di-n-butyl phthalate 5.00
50.0 30-130µg/l52.1 1044,6-Dinitro-2-methylphenol 5.00
50.0 30-130µg/l40.6 812,4-Dinitrophenol 5.00
50.0 40-140µg/l48.5 972,4-Dinitrotoluene 5.00
50.0 40-140µg/l52.2 1042,6-Dinitrotoluene 5.00
50.0 40-140µg/l37.6 75Di-n-octyl phthalate 5.00
50.0 40-140µg/l37.5 75Fluoranthene 5.00
50.0 40-140µg/l34.1 68Fluorene 5.00
50.0 40-140µg/l47.2 94Hexachlorobenzene 5.00
50.0 40-140µg/l39.0 78Hexachlorobutadiene 5.00
50.0 40-140µg/l57.8 116Hexachlorocyclopentadiene 5.00
50.0 40-140µg/l46.3 93Hexachloroethane 5.00
50.0 40-140µg/l38.4 77Indeno (1,2,3-cd) pyrene 5.00
50.0 40-140µg/l33.8 68Isophorone 5.00
50.0 40-140µg/l44.2 882-Methylnaphthalene 5.00
50.0 30-130µg/l36.1 722-Methylphenol 5.00
50.0 30-130µg/l39.3 793 & 4-Methylphenol 10.0
50.0 40-140µg/l35.7 71Naphthalene 5.00
50.0 40-140µg/l36.8 742-Nitroaniline 5.00
50.0 40-140µg/l24.8 503-Nitroaniline 5.00
50.0 40-140µg/l41.0 824-Nitroaniline 5.00
50.0 40-140µg/l48.7 97Nitrobenzene 5.00
50.0 30-130µg/l38.4 772-Nitrophenol 5.00
50.0 30-130µg/l47.2 944-Nitrophenol 20.0
50.0 40-140µg/l31.8 64N-Nitrosodimethylamine 5.00
50.0 40-140µg/l35.2 70N-Nitrosodi-n-propylamine 5.00
50.0 40-140µg/l42.1 84N-Nitrosodiphenylamine 5.00
50.0 30-130µg/l27.2 54Pentachlorophenol 20.0
50.0 40-140µg/l38.3 77Phenanthrene 5.00
50.0 30-130µg/l34.8 70Phenol 5.00
50.0 40-140µg/l35.8 72Pyrene 5.00
50.0 40-140µg/l29.9 60Pyridine 5.00
50.0 40-140µg/l43.8 881,2,4-Trichlorobenzene 5.00
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 40 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GCMS - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8270D
Batch 1705460 - SW846 3510C
LCS (1705460-BS1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
50.0 40-140µg/l39.1 781-Methylnaphthalene 5.00
50.0 30-130µg/l39.8 802,4,5-Trichlorophenol 5.00
50.0 30-130µg/l38.5 772,4,6-Trichlorophenol 5.00
50.0 40-140µg/l44.0 88Pentachloronitrobenzene 5.00
50.0 40-140µg/l37.4 751,2,4,5-Tetrachlorobenzene 5.00
50.0 30-130Surrogate: 2-Fluorobiphenyl 44.0 µg/l 88
50.0 15-110Surrogate: 2-Fluorophenol 40.6 µg/l 81
50.0 30-130Surrogate: Nitrobenzene-d5 51.7 µg/l 103
50.0 15-110Surrogate: Phenol-d5 44.9 µg/l 90
50.0 30-130Surrogate: Terphenyl-dl4 39.8 µg/l 80
50.0 15-110Surrogate: 2,4,6-Tribromophenol 52.1 µg/l 104
LCS Dup (1705460-BSD1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
50.0 2040-140 1µg/l37.0 74Acenaphthene 5.00
50.0 2040-140 10µg/l36.3 73Acenaphthylene 5.00
50.0 2040-140 11µg/lQC219.2 38Aniline 5.00
50.0 2040-140 6µg/l36.6 73Anthracene 5.00
50.0 2040-140 3µg/l41.4 83Azobenzene/Diphenyldiazene 5.00
50.0 2040-140 39µg/lQR928.2 56Benzidine 5.00
50.0 2040-140 2µg/l38.3 77Benzo (a) anthracene 5.00
50.0 2040-140 1µg/l37.8 76Benzo (a) pyrene 5.00
50.0 2040-140 14µg/l38.1 76Benzo (b) fluoranthene 5.00
50.0 2040-140 2µg/l37.1 74Benzo (g,h,i) perylene 5.00
50.0 2040-140 1µg/l37.1 74Benzo (k) fluoranthene 5.00
50.0 2030-130 14µg/l33.1 66Benzoic acid 5.00
50.0 2040-140 2µg/l35.5 71Benzyl alcohol 5.00
50.0 2040-140 2µg/l31.1 62Bis(2-chloroethoxy)methane 5.00
50.0 2040-140 9µg/l29.4 59Bis(2-chloroethyl)ether 5.00
50.0 2040-140 5µg/l31.7 63Bis(2-chloroisopropyl)ether 5.00
50.0 2040-140 5µg/l36.1 72Bis(2-ethylhexyl)phthalate 5.00
50.0 2040-140 11µg/l32.5 654-Bromophenyl phenyl ether 5.00
50.0 2040-140 4µg/l36.8 74Butyl benzyl phthalate 5.00
50.0 2040-140 4µg/l48.1 96Carbazole 5.00
50.0 2030-130 0.8µg/l36.8 744-Chloro-3-methylphenol 5.00
50.0 2040-140 12µg/l21.3 434-Chloroaniline 5.00
50.0 2040-140 0.4µg/l47.5 952-Chloronaphthalene 5.00
50.0 2030-130 2µg/l36.4 732-Chlorophenol 5.00
50.0 2040-140 5µg/l36.8 744-Chlorophenyl phenyl ether 5.00
50.0 2040-140 9µg/l38.8 78Chrysene 5.00
50.0 2040-140 0.7µg/l39.2 78Dibenzo (a,h) anthracene 5.00
50.0 2040-140 5µg/l42.8 86Dibenzofuran 5.00
50.0 2040-140 6µg/l40.1 801,2-Dichlorobenzene 5.00
50.0 2040-140 2µg/l40.8 821,3-Dichlorobenzene 5.00
50.0 2040-140 0.2µg/l41.5 831,4-Dichlorobenzene 5.00
50.0 2040-140 11µg/l45.4 913,3´-Dichlorobenzidine 5.00
50.0 2030-130 0.1µg/l36.4 732,4-Dichlorophenol 5.00
50.0 2040-140 8µg/l37.2 74Diethyl phthalate 5.00
50.0 2040-140 1µg/l35.4 71Dimethyl phthalate 5.00
50.0 2030-130 3µg/l35.0 702,4-Dimethylphenol 5.00
50.0 2040-140 3µg/l34.7 69Di-n-butyl phthalate 5.00
50.0 2030-130 15µg/l45.0 904,6-Dinitro-2-methylphenol 5.00
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 41 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GCMS - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8270D
Batch 1705460 - SW846 3510C
LCS Dup (1705460-BSD1) Prepared: 31-Mar-17 Analyzed: 03-Apr-17
50.0 2030-130 21µg/lQR932.9 662,4-Dinitrophenol 5.00
50.0 2040-140 0.9µg/l48.9 982,4-Dinitrotoluene 5.00
50.0 2040-140 8µg/l48.2 962,6-Dinitrotoluene 5.00
50.0 2040-140 3µg/l36.4 73Di-n-octyl phthalate 5.00
50.0 2040-140 8µg/l34.6 69Fluoranthene 5.00
50.0 2040-140 12µg/l38.4 77Fluorene 5.00
50.0 2040-140 3µg/l45.8 92Hexachlorobenzene 5.00
50.0 2040-140 4µg/l40.6 81Hexachlorobutadiene 5.00
50.0 2040-140 4µg/l59.9 120Hexachlorocyclopentadiene 5.00
50.0 2040-140 5µg/l43.9 88Hexachloroethane 5.00
50.0 2040-140 3µg/l37.1 74Indeno (1,2,3-cd) pyrene 5.00
50.0 2040-140 5µg/l32.1 64Isophorone 5.00
50.0 2040-140 4µg/l42.5 852-Methylnaphthalene 5.00
50.0 2030-130 6µg/l33.9 682-Methylphenol 5.00
50.0 2030-130 4µg/l37.8 763 & 4-Methylphenol 10.0
50.0 2040-140 3µg/l36.9 74Naphthalene 5.00
50.0 2040-140 6µg/l39.0 782-Nitroaniline 5.00
50.0 2040-140 16µg/l29.1 583-Nitroaniline 5.00
50.0 2040-140 7µg/l44.2 884-Nitroaniline 5.00
50.0 2040-140 1µg/l48.2 96Nitrobenzene 5.00
50.0 2030-130 6µg/l36.2 722-Nitrophenol 5.00
50.0 2030-130 8µg/l43.5 874-Nitrophenol 20.0
50.0 2040-140 10µg/l28.8 58N-Nitrosodimethylamine 5.00
50.0 2040-140 0.4µg/l35.1 70N-Nitrosodi-n-propylamine 5.00
50.0 2040-140 5µg/l40.2 80N-Nitrosodiphenylamine 5.00
50.0 2030-130 19µg/l22.5 45Pentachlorophenol 20.0
50.0 2040-140 12µg/l33.8 68Phenanthrene 5.00
50.0 2030-130 4µg/l33.4 67Phenol 5.00
50.0 2040-140 1µg/l36.3 73Pyrene 5.00
50.0 2040-140 10µg/l27.0 54Pyridine 5.00
50.0 2040-140 0.9µg/l43.4 871,2,4-Trichlorobenzene 5.00
50.0 2040-140 5µg/l41.0 821-Methylnaphthalene 5.00
50.0 2030-130 5µg/l37.7 752,4,5-Trichlorophenol 5.00
50.0 2030-130 0.3µg/l38.6 772,4,6-Trichlorophenol 5.00
50.0 2040-140 3µg/l45.3 91Pentachloronitrobenzene 5.00
50.0 2040-140 5µg/l39.4 791,2,4,5-Tetrachlorobenzene 5.00
50.0 30-130Surrogate: 2-Fluorobiphenyl 43.1 µg/l 86
50.0 15-110Surrogate: 2-Fluorophenol 38.1 µg/l 76
50.0 30-130Surrogate: Nitrobenzene-d5 47.7 µg/l 95
50.0 15-110Surrogate: Phenol-d5 40.8 µg/l 82
50.0 30-130Surrogate: Terphenyl-dl4 42.2 µg/l 84
50.0 15-110Surrogate: 2,4,6-Tribromophenol 48.4 µg/l 97
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 42 of 5007-Apr-17 13:56
Semivolatile Organic Compounds by GC - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SW846 8082A
Batch 1705401 - SW846 3510C
Blank (1705401-BLK1) Prepared: 30-Mar-17 Analyzed: 31-Mar-17
µg/l< 0.200Aroclor-1016 0.200
µg/l< 0.200Aroclor-1016 [2C] 0.200
µg/l< 0.200Aroclor-1221 0.200
µg/l< 0.200Aroclor-1221 [2C] 0.200
µg/l< 0.200Aroclor-1232 0.200
µg/l< 0.200Aroclor-1232 [2C] 0.200
µg/l< 0.200Aroclor-1242 0.200
µg/l< 0.200Aroclor-1242 [2C] 0.200
µg/l< 0.200Aroclor-1248 0.200
µg/l< 0.200Aroclor-1248 [2C] 0.200
µg/l< 0.200Aroclor-1254 0.200
µg/l< 0.200Aroclor-1254 [2C] 0.200
µg/l< 0.200Aroclor-1260 0.200
µg/l< 0.200Aroclor-1260 [2C] 0.200
µg/l< 0.200Aroclor-1262 0.200
µg/l< 0.200Aroclor-1262 [2C] 0.200
µg/l< 0.200Aroclor-1268 0.200
µg/l< 0.200Aroclor-1268 [2C] 0.200
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr) 0.110 µg/l 55
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr)
[2C]
0.110 µg/l 55
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) 0.150 µg/l 75
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) [2C] 0.140 µg/l 70
LCS (1705401-BS1) Prepared: 30-Mar-17 Analyzed: 31-Mar-17
2.50 40-140µg/l2.06 82Aroclor-1016 0.200
2.50 40-140µg/l1.94 78Aroclor-1016 [2C] 0.200
2.50 40-140µg/l2.23 89Aroclor-1260 0.200
2.50 40-140µg/l1.93 77Aroclor-1260 [2C] 0.200
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr) 0.130 µg/l 65
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr)
[2C]
0.120 µg/l 60
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) 0.180 µg/l 90
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) [2C] 0.150 µg/l 75
LCS Dup (1705401-BSD1) Prepared: 30-Mar-17 Analyzed: 31-Mar-17
2.50 2040-140 1µg/l2.04 82Aroclor-1016 0.200
2.50 2040-140 0µg/l1.94 78Aroclor-1016 [2C] 0.200
2.50 2040-140 0µg/l2.23 89Aroclor-1260 0.200
2.50 2040-140 1µg/l1.95 78Aroclor-1260 [2C] 0.200
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr) 0.130 µg/l 65
0.200 30-150Surrogate: 4,4-DB-Octafluorobiphenyl (Sr)
[2C]
0.130 µg/l 65
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) 0.170 µg/l 85
0.200 30-150Surrogate: Decachlorobiphenyl (Sr) [2C] 0.150 µg/l 75
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 43 of 5007-Apr-17 13:56
Extractable Petroleum Hydrocarbons - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
EPA 1664B
Batch 1705552 - SW846 3510C
Blank (1705552-BLK1) Prepared: 03-Apr-17 Analyzed: 04-Apr-17
mg/l< 1.0Non-polar material (SGT-HEM) 1.0
LCS (1705552-BS1) Prepared: 03-Apr-17 Analyzed: 04-Apr-17
16.0 64-132mg/lBsL7.4 46Non-polar material (SGT-HEM) 1.0
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* Reportable Detection Limit Page 44 of 5007-Apr-17 13:56
Total Metals by EPA 200 Series Methods - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
EPA 200.7
Batch 1705511 - EPA 200 Series
Blank (1705511-BLK1) Prepared: 03-Apr-17 Analyzed: 05-Apr-17
mg/l< 0.0150Selenium 0.0150
mg/l< 0.0400Iron 0.0400
mg/l< 0.0060Antimony 0.0060
mg/l< 0.0025Cadmium 0.0025
mg/l< 0.0050Copper 0.0050
mg/l< 0.0050Zinc 0.0050
mg/l< 0.0050Nickel 0.0050
mg/l< 0.0100Magnesium 0.0100
mg/l< 0.0050Chromium 0.0050
mg/l< 0.100Calcium 0.100
mg/l< 0.0040Arsenic 0.0040
mg/l< 0.0050Silver 0.0050
LCS (1705511-BS1) Prepared: 03-Apr-17 Analyzed: 05-Apr-17
1.25 85-115mg/l1.32 105Antimony 0.0060
1.25 85-115mg/l1.36 109Selenium 0.0150
1.25 85-115mg/l1.28 102Iron 0.0400
6.25 85-115mg/l6.64 106Calcium 0.100
1.25 85-115mg/l1.29 103Silver 0.0050
1.25 85-115mg/l1.27 101Cadmium 0.0025
1.25 85-115mg/l1.39 112Chromium 0.0050
1.25 85-115mg/l1.34 107Magnesium 0.0100
1.25 85-115mg/l1.29 104Nickel 0.0050
1.25 85-115mg/l1.30 104Zinc 0.0050
1.25 85-115mg/l1.38 110Copper 0.0050
1.25 85-115mg/l1.32 106Arsenic 0.0040
EPA 200.8
Batch 1705512 - EPA 200 Series
Blank (1705512-BLK1) Prepared & Analyzed: 03-Apr-17
mg/lQB20.0157Lead 0.00130
LCS (1705512-BS1) Prepared & Analyzed: 03-Apr-17
0.100 85-115mg/lD0.112 112Lead 0.00650
Duplicate (1705512-DUP1) Prepared & Analyzed: 03-Apr-17Source: SC32894-01
208mg/lJ,R06 0.001330.00124Lead 0.00130
Matrix Spike (1705512-MS1) Prepared & Analyzed: 03-Apr-17Source: SC32894-01
0.100 70-130mg/lD 0.001330.115 114Lead 0.00650
Post Spike (1705512-PS1) Prepared & Analyzed: 03-Apr-17Source: SC32894-01
0.100 85-115mg/lD 0.001330.106 105Lead 0.00650
EPA 245.1/7470A
Batch 1705513 - EPA200/SW7000 Series
Blank (1705513-BLK1) Prepared & Analyzed: 03-Apr-17
mg/l< 0.00020Mercury 0.00020
LCS (1705513-BS1) Prepared & Analyzed: 03-Apr-17
0.00500 85-115mg/l0.00459 92Mercury 0.00020
Duplicate (1705513-DUP1) Prepared & Analyzed: 03-Apr-17Source: SC32894-02
20mg/l BRL< 0.00020Mercury 0.00020
Matrix Spike (1705513-MS1) Prepared & Analyzed: 03-Apr-17Source: SC32894-02
0.00500 80-120mg/l BRL0.00480 96Mercury 0.00020
Post Spike (1705513-PS1) Prepared & Analyzed: 03-Apr-17Source: SC32894-02
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 45 of 5007-Apr-17 13:56
Total Metals by EPA 200 Series Methods - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
EPA 245.1/7470A
Batch 1705513 - EPA200/SW7000 Series
Post Spike (1705513-PS1) Prepared & Analyzed: 03-Apr-17Source: SC32894-02
0.00500 85-115mg/l BRL0.00460 92Mercury 0.00020
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 46 of 5007-Apr-17 13:56
General Chemistry Parameters - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
EPA 300.0
Batch 1705349 - General Preparation
Blank (1705349-BLK1) Prepared & Analyzed: 29-Mar-17
mg/l< 1.00Chloride 1.00
LCS (1705349-BS1) Prepared & Analyzed: 29-Mar-17
20.0 90-110mg/l20.7 103Chloride 1.00
Duplicate (1705349-DUP1) Prepared & Analyzed: 29-Mar-17Source: SC32894-02
200.8mg/l 18.919.1Chloride 1.00
Matrix Spike (1705349-MS1) Prepared & Analyzed: 29-Mar-17Source: SC32894-02
8.00 90-110mg/l 18.926.6 96Chloride 1.00
Matrix Spike Dup (1705349-MSD1) Prepared & Analyzed: 29-Mar-17Source: SC32894-02
8.00 2090-110 1mg/l 18.927.0 100Chloride 1.00
Reference (1705349-SRM1) Prepared & Analyzed: 29-Mar-17
25.0 90-110mg/l25.5 102Chloride 1.00
Batch 1705419 - General Preparation
Blank (1705419-BLK1) Prepared & Analyzed: 30-Mar-17
mg/l< 1.00Chloride 1.00
LCS (1705419-BS1) Prepared & Analyzed: 30-Mar-17
20.0 90-110mg/l20.8 104Chloride 1.00
Duplicate (1705419-DUP2) Prepared & Analyzed: 30-Mar-17Source: SC32894-01
200.8mg/l 20.821.0Chloride 1.00
Matrix Spike (1705419-MS2) Prepared & Analyzed: 30-Mar-17Source: SC32894-01
8.00 90-110mg/l 20.828.2 92Chloride 1.00
Matrix Spike Dup (1705419-MSD2) Prepared & Analyzed: 30-Mar-17Source: SC32894-01
8.00 2090-110 2mg/l 20.828.7 99Chloride 1.00
Reference (1705419-SRM1) Prepared & Analyzed: 30-Mar-17
25.0 90-110mg/l24.7 99Chloride 1.00
EPA 335.4 / SW846 9012B
Batch 1705518 - General Preparation
Blank (1705518-BLK1) Prepared & Analyzed: 31-Mar-17
mg/l< 0.00500Cyanide (total) 0.00500
LCS (1705518-BS1) Prepared & Analyzed: 31-Mar-17
0.300 90-110mg/l0.310 103Cyanide (total) 0.00500
Reference (1705518-SRM1) Prepared & Analyzed: 31-Mar-17
0.388 65-135mg/l0.303 78Cyanide (total) 0.00500
Batch 1705670 - General Preparation
Blank (1705670-BLK1) Prepared & Analyzed: 05-Apr-17
mg/l< 0.00500Cyanide (total) 0.00500
LCS (1705670-BS1) Prepared & Analyzed: 05-Apr-17
0.300 90-110mg/l0.295 98Cyanide (total) 0.00500
Duplicate (1705670-DUP1) Prepared & Analyzed: 05-Apr-17Source: SC32894-04
20mg/l BRL< 0.00500Cyanide (total) 0.00500
Matrix Spike (1705670-MS1) Prepared & Analyzed: 05-Apr-17Source: SC32894-04
0.300 90-110mg/l BRL0.311 104Cyanide (total) 0.00500
Matrix Spike Dup (1705670-MSD1) Prepared & Analyzed: 05-Apr-17Source: SC32894-04
0.300 2090-110 5mg/l BRL0.296 99Cyanide (total) 0.00500
Reference (1705670-SRM1) Prepared & Analyzed: 05-Apr-17
0.388 65-135mg/l0.260 67Cyanide (total) 0.00500
SM2540D (11)
Batch 1705388 - General Preparation
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 47 of 5007-Apr-17 13:56
General Chemistry Parameters - Quality Control
Result Units
Spike
Level
Source
Result %REC
%REC
Limits RPD
RPD
LimitFlagAnalyte(s) *RDL
SM2540D (11)
Batch 1705388 - General Preparation
Blank (1705388-BLK1) Prepared: 30-Mar-17 Analyzed: 31-Mar-17
mg/l< 0.5Total Suspended Solids 0.5
LCS (1705388-BS1) Prepared: 30-Mar-17 Analyzed: 31-Mar-17
100 90-110mg/l94.0 94Total Suspended Solids 10.0
SM3500-Cr-B (11)/7196A
Batch 1705285 - General Preparation
Blank (1705285-BLK1) Prepared & Analyzed: 28-Mar-17
mg/l< 0.005Hexavalent Chromium 0.005
LCS (1705285-BS1) Prepared & Analyzed: 28-Mar-17
0.0500 90-111mg/l0.052 105Hexavalent Chromium 0.005
Duplicate (1705285-DUP1) Prepared & Analyzed: 28-Mar-17Source: SC32894-01
20mg/lR01 BRL< 0.025Hexavalent Chromium 0.025
Matrix Spike (1705285-MS1) Prepared & Analyzed: 28-Mar-17Source: SC32894-01
0.250 85-115mg/l BRL0.236 95Hexavalent Chromium 0.025
Matrix Spike Dup (1705285-MSD1) Prepared & Analyzed: 28-Mar-17Source: SC32894-01
0.250 2085-115 8mg/l BRL0.256 102Hexavalent Chromium 0.025
Reference (1705285-SRM1) Prepared & Analyzed: 28-Mar-17
0.0250 85-115mg/l0.026 106Hexavalent Chromium 0.005
Batch 1705288 - General Preparation
Blank (1705288-BLK1) Prepared & Analyzed: 28-Mar-17
mg/l< 0.005Hexavalent Chromium 0.005
LCS (1705288-BS1) Prepared & Analyzed: 28-Mar-17
0.0500 90-111mg/l0.052 105Hexavalent Chromium 0.005
Reference (1705288-SRM1) Prepared & Analyzed: 28-Mar-17
0.0250 85-115mg/l0.026 106Hexavalent Chromium 0.005
SM4500-NH3 C. (11)
Batch 1705665 - General Preparation
Blank (1705665-BLK1) Prepared: 04-Apr-17 Analyzed: 05-Apr-17
mg/l< 0.200Ammonia as N 0.200
LCS (1705665-BS1) Prepared: 04-Apr-17 Analyzed: 05-Apr-17
5.00 90-110mg/l4.90 98Ammonia as N 0.200
Duplicate (1705665-DUP1) Prepared: 04-Apr-17 Analyzed: 05-Apr-17Source: SC32894-02
200mg/lJ 0.1400.140Ammonia as N 0.200
Matrix Spike (1705665-MS1) Prepared: 04-Apr-17 Analyzed: 05-Apr-17Source: SC32894-03
5.00 80-120mg/l BRL4.90 98Ammonia as N 0.200
Reference (1705665-SRM1) Prepared: 04-Apr-17 Analyzed: 05-Apr-17
2.16 86-114mg/l2.03 94Ammonia as N 0.200
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 48 of 5007-Apr-17 13:56
Notes and Definitions
Data for this analyte may be biased low based on QC spike recoveries.BsL
Data reported from a dilutionD
The method blank contains analyte at a concentration above the MRL, however no reportable concentration is present in
the sample.
QB2
Analyte out of acceptance range in QC spike but no reportable concentration present in sample.QC2
RPD out of acceptance range. The batch is accepted based upon LCS and/or LCSD recovery.QR9
The Reporting Limit has been raised to account for matrix interference.R01
MRL raised to correlate to batch QC reporting limits.R06
RPD Relative Percent Difference
dry Sample results reported on a dry weight basis
Not ReportedNR
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
LIV The initial volume for this sample has been reduced due to sample matrix and/or historical data therefore elevating the
reporting limit.
HD Total Hardness is a calculation based on the reported values of Ca and Mg.
Interpretation of Total Petroleum Hydrocarbon Report
Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints
obtained from analyses of various petroleum products. Possible match categories are as follows:
Gasoline - includes regular, unleaded, premium, etc.
Fuel Oil #2 - includes home heating oil, #2 fuel oil, and diesel
Fuel Oil #4 - includes #4 fuel oil
Fuel Oil #6 - includes #6 fuel oil and bunker "C" oil
Motor Oil - includes virgin and waste automobile oil
Ligroin - includes mineral spirits, petroleum naphtha, vm&p naphtha
Aviation Fuel - includes kerosene, Jet A and JP-4
Other Oil - includes lubricating and cutting oil, and silicon oil
At times, the unidentified petroleum product is quantified using a calibration that most closely approximates the distribution of
compounds in the sample. When this occurs, the result is qualified as Calculated as.
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* Reportable Detection Limit Page 49 of 5007-Apr-17 13:56
Laboratory Control Sample (LCS): A known matrix spiked with compound(s) representative of the target analytes, which is used to
document laboratory performance.
Matrix Duplicate: An intra-laboratory split sample which is used to document the precision of a method in a given sample matrix.
Matrix Spike: An aliquot of a sample spiked with a known concentration of target analyte(s). The spiking occurs prior to sample
preparation and analysis. A matrix spike is used to document the bias of a method in a given sample matrix.
Method Blank: An analyte-free matrix to which all reagents are added in the same volumes or proportions as used in sample
processing. The method blank should be carried through the complete sample preparation and analytical procedure. The method blank
is used to document contamination resulting from the analytical process.
Method Detection Limit (MDL): The minimum concentration of a substance that can be measured and reported with 99% confidence
that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the
analyte.
Reportable Detection Limit (RDL): The lowest concentration that can be reliably achieved within specified limits of precision and
accuracy during routine laboratory operating conditions. For many analytes the RDL analyte concentration is selected as the lowest
non-zero standard in the calibration curve. While the RDL is approximately 5 to 10 times the MDL, the RDL for each sample takes
into account the sample volume/weight, extract/digestate volume, cleanup procedures and, if applicable, dry weight correction. Sample
RDLs are highly matrix-dependent.
Surrogate: An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical
process, but which is not normally found in environmental samples. These compounds are spiked into all blanks, standards, and
samples prior to analysis. Percent recoveries are calculated for each surrogate.
Continuing Calibration Verification: The calibration relationship established during the initial calibration must be verified at periodic
intervals. Concentrations, intervals, and criteria are method specific.
This laboratory report is not valid without an authorized signature on the cover page .
* Reportable Detection Limit Page 50 of 5007-Apr-17 13:56
Batch Summary
[CALC]
General Chemistry Parameters
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705285
General Chemistry Parameters
1705285-BLK1
1705285-BS1
1705285-DUP1
1705285-MS1
1705285-MSD1
1705285-SRM1
SC32894-01 (ACS-1 (Hydrant))
1705288
General Chemistry Parameters
1705288-BLK1
1705288-BS1
1705288-SRM1
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705326
Total Metals by EPA 200/6000 Series Methods
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705349
General Chemistry Parameters
1705349-BLK1
1705349-BS1
1705349-DUP1
1705349-MS1
1705349-MSD1
1705349-SRM1
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705388
General Chemistry Parameters
1705388-BLK1
1705388-BS1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705401
Semivolatile Organic Compounds by GC
1705401-BLK1
1705401-BS1
1705401-BSD1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705413
Total Metals by EPA 200/6000 Series Methods
SC32894-01 (ACS-1 (Hydrant))
1705419
General Chemistry Parameters
1705419-BLK1
1705419-BS1
1705419-DUP2
1705419-MS2
1705419-MSD2
1705419-SRM1
SC32894-01 (ACS-1 (Hydrant))
1705460
Semivolatile Organic Compounds by GCMS
1705460-BLK1
1705460-BS1
1705460-BSD1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705468
Volatile Organic Compounds
1705468-BLK1
1705468-BS1
1705468-BSD1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
SC32894-06 (Trip Blank)
1705511
Total Metals by EPA 200 Series Methods
1705511-BLK1
1705511-BS1
SC32894-01 (ACS-1 (Hydrant))
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
SC32894-04 (LSP-1 (Pond))
1705512
Total Metals by EPA 200 Series Methods
1705512-BLK1
1705512-BS1
1705512-DUP1
1705512-MS1
1705512-PS1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705513
Total Metals by EPA 200 Series Methods
1705513-BLK1
1705513-BS1
1705513-DUP1
1705513-MS1
1705513-PS1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705518
General Chemistry Parameters
1705518-BLK1
1705518-BS1
1705518-SRM1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
1705548
Microextractable Organic Compounds
1705548-BLK1
1705548-BS1
1705548-BSD1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
SC32894-05 (Reagent Blank)
1705552
Extractable Petroleum Hydrocarbons
1705552-BLK1
1705552-BS1
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705665
General Chemistry Parameters
1705665-BLK1
1705665-BS1
1705665-DUP1
1705665-MS1
1705665-SRM1
SC32894-01 (ACS-1 (Hydrant))
SC32894-02 (ACS-2 (Stream))
SC32894-03 (SPB-1 (Brook))
SC32894-04 (LSP-1 (Pond))
1705670
General Chemistry Parameters
1705670-BLK1
1705670-BS1
1705670-DUP1
1705670-MS1
1705670-MSD1
1705670-SRM1
SC32894-04 (LSP-1 (Pond))
S701962
Semivolatile Organic Compounds by GCMS
S701962-CAL1
S701962-CAL2
S701962-CAL3
S701962-CAL4
S701962-CAL5
S701962-CAL6
S701962-CAL7
S701962-CAL8
S701962-CAL9
S701962-CALA
S701962-ICV1
S701962-LCV1
S701962-LCV2
S701962-LCV3
S701962-TUN1
S702336
Semivolatile Organic Compounds by GC
S702336-CAL1
S702336-CAL2
S702336-CAL3
S702336-CAL4
S702336-CAL5
S702336-CAL6
S702336-CAL7
S702336-CAL8
S702336-CAL9
S702336-CALA
S702336-CALB
S702336-CALC
S702336-CALD
S702336-CALE
S702336-CALF
S702336-CALG
S702336-CALH
S702336-CALI
S702336-CALJ
S702336-CALK
S702336-CALL
S702336-CALM
S702336-CALN
S702336-CALO
S702336-CALP
S702336-CALQ
S702336-CALR
S702336-CALS
S702336-CALT
S702336-CALU
S702336-ICV1
S702336-ICV2
S702336-ICV3
S702336-ICV4
S702336-ICV5
S702336-ICV6
S702336-LCV1
S702336-LCV2
S702336-LCV3
S702336-LCV4
S702336-LCV5
S702336-LCV6
S703389
Volatile Organic Compounds
S703389-CAL1
S703389-CAL2
S703389-CAL3
S703389-CAL4
S703389-CAL5
S703389-CAL6
S703389-CAL7
S703389-CAL8
S703389-CAL9
S703389-ICV1
S703389-LCV1
S703389-LCV2
S703389-LCV3
S703389-TUN1
S703413
Volatile Organic Compounds
S703413-CCV1
S703413-TUN1
S703444
Microextractable Organic Compounds
S703444-CAL1
S703444-CAL2
S703444-CAL3
S703444-CAL4
S703444-CAL5
S703444-CAL6
S703444-CAL7
S703444-ICV1
S703444-LCV1
S703452
Semivolatile Organic Compounds by GC
S703452-CCV1
S703452-CCV2
S703452-IBL1
S703452-IBL2
S703464
Microextractable Organic Compounds
S703464-CCV1
S703464-CCV2
S703498
Semivolatile Organic Compounds by GCMS
S703498-CCV1
S703498-TUN1
(µS/cm3) (µS/cm)Agawam Compressor Station
(Hydrant),
Agawam, MA
03/28/17 @ 08:45 6.55 141 91 13.71 6.80 ‐98.0 58.7 0.79
UNT to Worthington Brook,
Agawam, MA03/28/17 @ 09:44 2.67 187 107 13.87 6.62 ‐117.8 21.5 0.02
Spectacle Pond Brook,
Sandisfield, MA03/28/17 @ 12:25 3.36 106 62 13.49 6.48 ‐114.3 ‐2.2 ‐
Lower Spectacle Pond,
Sandisfield, MA03/28/17 @ 13:13 2.28 76 43 12.36 6.68 ‐109.1 ‐2.3 ‐
ORPTurbidity(NTU)
Dissolved Oxygen(mg/L)
Total Chlorine(mg/L)
CT‐Expansion Project ‐ EPA Remediation General Permit (Pre‐Construction) Sampling (YSI and Chlorine Meter Readings)
Meter Readings ‐ Date and Time
ConductivitypH
Temp (oCelcius)
Location