Paradise Marsh Contaminants Investigation - U.S. Fish and … · 2017-08-30 · Paradise Marsh Refuge Cleanup Project ... in our analysis of the Bight 1998 data from San Diego Bay)

CA – San Diego Bay National Wildlife Refuge Sweetwater Marsh Unit

Paradise Marsh Refuge Cleanup Project

Paradise Marsh Contaminants Investigation

Carol Gorbics, Environmental Contaminants Specialist and

Catherine Zeeman, PhD, Resource Contaminants Specialist Environmental Contaminants Division

Carlsbad Fish and Wildlife Office Carlsbad, California

USFWS Region 8/CNO

Congressional Districts 52 and 53 FFS#: 1C59

DEC ID: 1261-1C59

April 2008

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AbstractParadise Marsh, located in San Diego Bay National Wildlife Refuge, provides intertidal habitat for wildlife of San Diego Bay in California. The quality of this habitat may be influenced by contaminants from multiple sources including San Diego Bay, Paradise Creek, and fill material located along the northern bluff area and eastern bluff area of the marsh. Several contaminants of concern for the San Diego Bay region have been identified by various state and federal agencies. These include chlordane, chromium, copper, lead, mercury, tributyltin, zinc, polycyclic aromatic hydrocarbons (PAHs), and polychlorinated biphenyls (PCBs). The presence of these and other contaminants in the Bay and within Paradise Marsh may result in a degraded habitat for wildlife species.Additionally, fill material placed along the periphery of Paradise Marsh may have provided a source of contaminated material into Paradise Marsh. The goals and objectives of this project were to evaluate sediment contamination in Paradise Marsh using the Sediment Quality Triad approach to determine the potential for adverse effects to benthic invertebrates using this area of the refuge by evaluating (1) sediment contaminant levels; (2) benthic community structure; and (3) pore water toxicity. In addition, we compared conditions in Paradise Marsh with available San Diego Bay data. We collected surface sediments and benthic invertebrate samples at nine stations within Paradise Marsh and at one reference station in nearby Sweetwater Marsh. Sediments were analyzed for PAHs, metals, organochlorine pesticides, and PCBs. Sediment contaminant concentrations were compared to effects-based screening levels found from the literature. Bulk sediment samples and pore water samples were tested for toxicity to invertebrates. Benthic community structure was analyzed for evidence of impairment. We found that habitat quality was diminished throughout the Paradise Marsh area when compared to the reference site. Sites closest to the north bluff, east bluff, and Paradise Creek inflow tended to be more clearly associated with known sources of contamination, although this relationship was not statistically significant. Contaminants found to be of concern in San Diego Bay in previous studies were also present at levels of concern in Paradise Marsh. Specifically, antimony, cadmium, copper, lead, mercury, silver, and zinc were found in high concentrations in the Bay and in Paradise Marsh (although sediment guidelines were exceeded only for antimony (T20), copper (ERL), and mercury (ERL) in our analysis of the Bight 1998 data from San Diego Bay). Petroleum hydrocarbon contamination is of serious concern. It is possible that a source of contamination is entering the marsh from upstream. It is also possible that contamination from the upstream source is ongoing. Additional investigation is recommended, specifically related to the inflow of Paradise Creek into Paradise Marsh. Sediment clean-up is warranted, however, the source of contamination in the inflow needs to be substantiated, identified and halted prior to the initiation of cleanup activities. Also, the delineation of the contaminated areas will require additional sampling.

Keywords San Diego Bay, Paradise Marsh, contamination, metals, organic pollutants, San Diego Bay National Wildlife Refuge, DEC ID 1261-1C59, Congressional District 52, Congressional District 53, FFS 1C59

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Table of Contents

1.0 Introduction............................................................................................................................... 1 2.0 Background and Environmental Setting ................................................................................... 3

2.1 Summary of Previous Investigations .............................................................................. 3 2.2 San Diego Bay Habitat Values ....................................................................................... 3 2.3 Paradise Marsh Species of Special Concern................................................................... 4

3.0 Methods..................................................................................................................................... 4 3.1 Study Design and Field Methods.................................................................................... 4 3.2 Laboratory Methods........................................................................................................ 5

4.0 Data Analysis and Results ........................................................................................................ 8 4.1 Sediment Characterization .............................................................................................. 8 4.2 Toxicity Assessments.................................................................................................... 11 4.3 Benthic Community Structure Assessments................................................................. 12 4.4 Results........................................................................................................................... 16

5.0 Discussion ............................................................................................................................... 16 5.1 Sediment Characterization ............................................................................................ 16 5.2 Toxicity Assessments.................................................................................................... 19 5.3 Benthic Assemblages .................................................................................................... 19 5.4 Sediment Quality Triad Assessment............................................................................. 20 5.5 Reference Site ............................................................................................................... 21

6.0 Management Recommendations and Conclusions ................................................................. 22 7.0 References............................................................................................................................... 23

Figure 1. Location Map................................................................................................................ 29 Figure 2. Sampling Locations. ..................................................................................................... 30 Figure 3. Sediment Characterization Based on Sediment Chemistry. ......................................... 31 Figure 4. Comparison of Sediment Chemistry Results................................................................ 32 Figure 5. Overall SQT Rank Compared with Distance from Potential Contamination............... 32

Table 1. Surveys of breeding Belding's Savannah sparrows in San Diego Bay, 1977-2001....... 33 Table 2. Sampling Location Information..................................................................................... 33 Table 3. Bioassay Testing Performed on Paradise Marsh Samples............................................. 33 Table 4. Sediment Characterization using Sediment Chemistry Guidelines.. ............................. 34 Table 5. ER-Mqs and corresponding ranks for sediments from Paradise Marsh.. ...................... 35 Table 6. SQT Rank for Physical Sediment Characteristics.. ....................................................... 35 Table 7. Overall SQT Score for Sediment Chemistry Characterization.. .................................... 35 Table 8. Overall SQT Rank for Sediment Toxicity.. ................................................................... 35 Table 9. Summary of Species Richness. ...................................................................................... 36 Table 10. Biodiversity Indicators with indexed values in parentheses........................................ 36 Table 11. SQT Rank for Relative Benthic Index.. ....................................................................... 36 Table 12. SQT Rank for Proportional Abundance of Pollution Tolerant Indicator Species.. ..... 37 Table 13. Overall SQT Rank for Benthic Community Indices.................................................... 37 Table 14. Overall Sediment Quality Triad Assessment Rank.. ................................................... 37 Table 15. Possible Contaminant Sources..................................................................................... 38 Table 16. PAHs exceeding T20 (bolded italics) or T50 (gray highlight). ................................... 38

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Appendix A. Contractors Report ................................................................................................. 39 Appendix B. Raw Data ................................................................................................................ 56 Appendix C. List of Indicator Species and their Classifications ............................................... 143

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List of Acronyms/Abbreviations bgs: below ground surface cm: centimeters D’: Simpson diversity index EPA: Environmental Protection Agency ER-L: effects range-low ER-M: effects range-median ER-Mq: effects range-median quotient H’: Shannon-Wiener index m: meters mL: milliliter MLLW: mean lower low water PAH: polycyclic aromatic hydrocarbons PCB: polychlorinated biphenyl PEL: probable effects level RBI: relative benthic indexRL: reporting limit S: species richnessSCB: Southern California Bight SQT: sediment quality triad T20: denotes the probability that 20 percent of samples would be toxic T50: denotes the probability that 50 percent of samples would be toxic TEL: threshold effects level TOC: total organic carbon USACE: U.S. Army Corps of Engineers

Acknowledgements The project’s authors wish to acknowledge the efforts of Emilie Luciani, Scott Sobiech, Judy Gibson and Sharon Taylor for their contributions to this report.

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Section 1.0 Introduction

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1.0 Introduction Paradise Creek is a small tidal creek on south San Diego Bay in National City, California.Upstream from the bay, it is almost completely paved over or channelized, but just east of the coastal freeway (Interstate 5) a half-mile-long stretch flows through a residential neighborhood, welding shop, auto repair and detailing operation, storage yard for heavy equipment, and school. The U.S. Army Corps of Engineers straightened this stretch of the creek in the 1950s but did not cover it.

Paradise Creek flows into Paradise Marsh which is a small, vegetated, tidally influenced estuarine marsh located south of West 24th Street and west of Interstate Highway 5 at the Sweetwater Channel freeway overpass. Paradise Marsh is part of the Sweetwater Marsh Unit of the San Diego Bay National Wildlife Refuge and is administered by the U.S. Fish and Wildlife Service (Service).

The marsh is surrounded by commercial and industrial-zoned land. The southern edge of Paradise Marsh connects directly to the Sweetwater River flood channel (Figure 1 and Figure 2).This channel has a constructed concrete tide-gate opening that can be closed with fitted planks.The marsh is situated at an elevation of approximately 1 meter (m) above mean lower low water (MLLW). The western and northern edge of the Paradise Marsh study area is a bluff that ranges from approximately 4 m to 6 m above MLLW. The eastern edge of the Paradise Marsh study area is bounded by Interstate 5.

Several contaminants of concern have been identified in San Diego Bay by various state and federal agencies including the California Regional Water Quality Control board and others (Fairey et al. 1996, Bay and Greenstein 2002, U.S. Department of the Navy 2000). These include chlordane, chromium, copper, lead, mercury, tributyltin, zinc, polycyclic aromatic hydrocarbons (PAHs), and polychlorinated biphenyls (PCBs). The presence of these and other contaminants in the Bay and within Paradise Marsh may result in a degraded habitat for wildlife species using Bay habitats.

The majority of the contaminants of concern likely enter this site through the surface water flow associated with Paradise Creek and the tidal inflow from Sweetwater Channel. The contaminants are carried into the tidal channel and associated wetland area where they become associated with the sediment particles. Fill material on the northern and eastern edges of the marsh is another potential source of contaminants. Along the northern edge of the marsh is a developed commercial area that included contaminated fill material that had previously been subject to some remediation. Also, along the eastern edge is a fill area believed to be contaminated with ash and petroleum waste (C. Zeeman, personal communication).

Contaminants associated with sediments may be toxic to directly exposed benthic biota including microbes, invertebrates, vegetation, bottom-dwelling fish, and other wildlife species. Certain sediment-borne contaminants may also enter and accumulate in the food chain to levels that are unsafe to upper trophic level predators such as birds that consume benthic invertebrates or fish.

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Many of the contaminants that become associated with the sediments may not be biologically available, making it difficult to predict toxicity to benthic biota based on analytical chemistry information alone. One tool for determining the degree to which contaminants are contributing to the degradation of sediment quality is the Sediment Quality Triad (SQT) approach (Chapman 1986, Chapman et al. 1997).

The SQT is used to assess impacts of sediment-borne contaminants on directly exposed benthic invertebrates. The health of the benthic invertebrate community is important by itself, and for Service trust resources that rely on benthic invertebrates as a primary source of nutrition. Benthic invertebrates also constitute an important route of exposure by fish and wildlife to sediment-borne contaminants. Tools, other than the SQT (i.e. bioaccumulation studies), are needed to characterize sediment quality in terms of contaminant exposure for fish and wildlife.

The SQT is a “weight of evidence” effects-based approach for evaluating and assessing pollution-induced degradation consisting of three components: sediment chemistry (a measure of contamination), sediment toxicity tests with benthic invertebrates (measures of bioavailability and biological effects), and in situ biological effects (benthic invertebrate community assemblages). The analysis of contaminant loads as well as the percentages of fine sediments and total organic carbon (TOC) provide useful information on sediment conditions, which also influence the distribution of organisms. Therefore, we describe the physical sediment characteristics, as well.

This study was conducted to determine if contaminants are present and if there is any evidence of potential impacts on benthic biota. The goals and objectives of this project include:

A. To evaluate sediment contamination using the Sediment Quality Triad approach in Paradise Marsh to assess the potential for adverse effects among benthic invertebrates that constitute an important source of food for wildlife using this area of the refuge.

a. Collect and analyze sediment contaminant and toxicity levels b. Collect and analyze benthic communities and their structures c. Collect and analyze pore water toxicity d. Consider sediment contamination, benthic community structure and pore water

toxicity in the context of the Sediment Quality Triad approach B. To compare sediment contamination in Paradise Marsh and San Diego Bay to sediment

contamination in other bays and harbors sampled during the Bight 1998 Project.1

1 The Bight ’98 Project is a multi-agency regional marine monitoring survey of the Southern California Bight (SCB). The overall goal of Bight '98 Project is to assess the condition of the bottom environment and the health of the biological resources in the SCB. The project includes the measurement of a variety of indicators at roughly 300 sites between Point Conception and just south of the Mexican Border. The indicators measured include benthic invertebrate assemblages, sediment contaminant concentrations, sediment toxicity, demersal fish assemblages, demersal fish gross pathology, bioacummulation of contaminants by demersal fish, dissolved oxygen, temperature, salinity, transmissivity, and marine debris. The data are available from the Southern California Coastal Water Research Project Authority Web Site http://www.sccwrp.org/data/1998_bight_survey.html.

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Section 2.0 Background and Environmental Setting

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2.0 Background and Environmental Setting

2.1 Summary of Previous Investigations A limited subsurface soil and groundwater investigation was conducted in May and June 2000 by JE Assessment Services, Inc. (Rancho Cucamonga, CA) at the direction of Community Development Commission of National City in the northern bluff, eastern bluff, and within the marsh. Three borings were installed in the northern bluff to depths up to 7 m below ground surface (bgs). Four borings were installed in the eastern bluff to depths up to 2 m bgs. Six borings were installed in the marsh to depths of 1.5 m bgs. Two sediment samples were collected from Paradise Creek. Three monitoring wells were also installed in the marsh.

An additional limited subsurface soil and groundwater investigation was conducted in January 2001 also by JE Assessment Services, Inc. in the eastern bluff and within the marsh. Two additional borings were installed in the eastern bluff to depths up to 0.25 m bgs. Four additional borings were installed in the marsh to depths up to 0.6 m bgs. Two additional sediment samples were collected from Paradise Creek and two additional monitoring wells were installed in the marsh.

These studies reported that there were: (1) elevated levels of total California and federally-regulated metals in the subsurface soil in the marsh, northern and eastern bluffs, and in Paradise Creek sediments; (2) elevated metal concentrations near the surface (to 0.15 m) in the marsh and the creek, and from 2 m bgs to 5 m bgs in the eastern and northern bluff, respectively; and (3) elevated metal concentrations, including soluble metals, detected in the groundwater beneath the marsh. Unfortunately, these investigations did not provide data or specify the standards used to make these determinations.

2.2 San Diego Bay Habitat Values San Diego Bay is one of few natural deepwater bays on the Pacific Coast. The Bay is located in the Southern California Bight (SCB) just north of the Mexican/United States border, and is sheltered by the overlapping peninsulas of Point Loma and Coronado. San Diego Bay is an important commercial port that accommodates substantial military holdings, recreational vessels, and a commercial fishing fleet. The Bay also harbors several types of important natural resources, including salt Marshes, tidal flats, bird nesting and foraging sites, and essential fish and sea turtle habitats such as eelgrass beds. Many of these resources are located within two components of the San Diego Bay National Wildlife Refuge, the Sweetwater Marsh Unit (316 acres) and the South San Diego Bay Unit (3,940 acres). San Diego Bay’s coastal wetlands and the indigenous fish and wildlife that utilize them are biologically, physically, and economically valuable resources. San Diego Bay is a spawning and nursery area for over 80 species of ocean and bay fish. Over 180 species of birds have been reported to be utilizing the Bay for nesting, foraging, and resting. Additionally, nine federal and state listed endangered or threatened species are found in various habitats scattered about the Bay including the California least tern (Sternula (Sterna) antillarum browni), light-footed clapper rail (Rallus longirostris levipes),California brown pelican (Pelecanus occidentalis), peregrine falcon (Falco peregrinus), western snowy plover (Charadrius alexandrinus nivosus), Beldings savannah sparrow (Passerculus

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sandwichensis beldingi), green sea turtle (Chelonia mydas), and the salt marsh bird’s beak (Cordylanthus maritimus ssp. maritimus) (an estuarine plant).

Several “contaminants of concern for the San Diego Bay Region” have been identified by various state and federal agencies. These include chlordane, chromium, copper, lead, mercury, tributyltin, zinc, polycyclic aromatic hydrocarbons (PAHs), and polychlorinated biphenyls (PCBs). The presence of these and other contaminants in the Bay and within Paradise Marsh may result in a degraded habitat for wildlife using the area.

2.3 Paradise Marsh Species of Special Concern The federally endangered California least tern and threatened western snowy plover may be nesting at the D Street fill area from April to September (Figure 2). These birds feed in Sweetwater channel which drains Paradise Marsh and in the San Diego Bay adjacent to the outflow from Sweetwater Channel (Figure 2).

In addition, refuge biologists report that the California brown pelican use this area (Paradise Marsh) throughout the year for resting and feeding in the channel.

The state protected Belding’s savannah sparrows are present in Paradise Marsh throughout the year and are likely nesting in the marsh vegetation during summer months. There were five surveys of breeding Belding’s savannah sparrows in San Diego Bay between 1977 and 2001. The number of breeding pairs at Paradise Marsh has declined over time and only seven territories were identified in the most recent survey (Table 1). There are currently only a few high spots of thick pickleweed suitable to support nesting Belding’s savannah sparrows. However, they may not be consistently occupied because the wetland is small, very narrow and heavily impacted by the noise of Interstate 5 which may impair predator avoidance by the sparrows. There are also abundant signs of people, cats, and dogs in the marsh and on its edge.

3.0 Methods

3.1 Study Design and Field Methods Sediments from nine locations in Paradise Marsh and one reference station were collected and analyzed for contaminant levels and evidence of potential contaminant impacts on benthic biota using the triad approach described by Chapman (1986) and Chapman et al. (1997). Coordinates and general features of each station were recorded and are summarized in Table 2. Sample locations are identified in Figure 2. Sample location Sed-10 is a reference station in the main area of the San Diego National Wildlife Refuge located on the south side of the Sweetwater Channel. Sediment samples were collected for chemical analysis, laboratory toxicity tests, and benthic macroinvertebrate community analysis. Detailed sampling methods are provided in the Southern California Bight 2003 Regional Marine Monitoring Survey Field Operations Manual (Bight 2003a) and all samples were collected in accordance with the protocols established for that study.

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Section 3.0 Methods

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Sampling protocols in the field followed accepted procedures and included methods to avoid cross-contamination; methods to avoid contamination by the sampling activities and crew; and careful temperature control, homogenization, and subsampling.

Sediment samples for chemistry and toxicity tests consisted of the top two centimeters (cm) of material and were collected using a 0.1 m Van Veen grab. General features of each station were recorded in the field. Sediment samples were analyzed for grain-size, total organic carbon (TOC), trace metal, and trace organic analyses. Sediment samples collected for chemical analysis were placed in a glass I-Chem container cleaned to EPA specifications and kept on ice for transport to the lab and storage at -20 degrees Celsius.

Similar sampling procedures were used to collect samples evaluated for toxicity. At each sampling station, surface (upper 2 cm) sediment was collected using a clean stainless-steel spoon. The sediment sample at each station was mixed in a decontaminated stainless-steel bowl using a large stainless-steel spoon to achieve a uniform texture and color. Sub-samples were then transferred to pre-cleaned glass containers with Teflon® lined lids with no head space, and then stored in the dark at 4°C until bulk sediment and pore water tests were conducted.

Samples for benthic infaunal analyses were collected in accordance with the Bight 2003 Monitoring Survey Macrobenthic (Infaunal) Sample Analysis Laboratory Manual (Bight 2003b).

3.2 Laboratory Methods

Sediment Characterization - Chemistry Chemical analyses and toxicity tests were performed by MEC Analytical Systems, Incorporated using protocols detailed in the Bight 2003 Coastal Ecology Workplan (Bight 2003c). Laboratory procedures were in accordance with quality assurance/quality control criteria established for Bight 2003 studies (Bight 2003d).

Sediments were analyzed for grain size, TOC, 23 major and trace elements (aluminum, antimony, arsenic, barium, beryllium, cadmium, chromium, cobalt, copper, iron, lead, manganese, mercury, molybdenum, nickel, selenium, silver, strontium, thallium, tin, titanium, vanadium, and zinc), five classes of organic compounds--total chlordanes ( and isomers), total DDTs (o, p- and p,p-isomers of DDT, DDD, and DDE), other chlorinated pesticides (20 compounds), total PAHs (24 compounds), and PCBs as congeners (46 congeners) and as aroclors (7 aroclors). All laboratory analyses were performed in accordance with the protocols established for the Southern California Bight 2003 Regional Monitoring Survey (Bight 03 2003b) including Quality Assurance and Quality Control standards (Bight 2003d). The target analytes and corresponding reporting limits are in Appendices A and C.

Sediment Characterization - Toxicity Assessments Two different sediment toxicity tests were selected for use. The first method measured whole sediment toxicity to the amphipod, Eohaustorius estuarius. Amphipods are among the first species to disappear from benthic communities impacted by pollution (Swartz et al. 1994).Sediment toxicity tests with amphipods are widely used in a variety of monitoring programs and

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standardized methods have been developed to improve data reliability (ASTM 1991). Survival of amphipods following a 10-day exposure period is the endpoint for this test. This bioassay minimizes many of the limitations of sediment toxicity tests by measuring a clearly adverse response (death), requiring relatively little manipulation of the sample, and using a species representative of an ecologically important group.

An interstitial water toxicity test using sand dollar (Dendraster excentricus) embryos was selected to provide a more sensitive measure of toxicity than offered by bulk sediment tests (and thus better discrimination between sites). In this test, sand dollar embryos are exposed to several dilutions of interstitial water for three days and then examined for abnormalities in development. Echinoderm embryos such as the sand dollar are often more sensitive to contaminants than the adult life stages of fish or crustaceans (Bay et al. 1993). This test provides an evaluation of a sediment compartment (interstitial water) considered very important for contaminant bioavailability and toxicity.

Bioassays performed for this project are summarized in Table 3.

a. Solid Phase Toxicity Tests Sediment toxicity tests for Eohaustorius estuarius were performed as specified in the Bight 2003 Sediment Toxicity Test Interlaboratory Comparison Study Final Workplan (Bight 2003a). All participating laboratories are following these protocols.

Solid phase bioassays were performed using 10-day acute exposure test (USEPA and USACE 1998) to estimate the potential toxicity of the project sediment to benthic organisms using the marine amphipod E. estuarius. Prior to testing, the project and control sediments were press sieved through a 2.0-millimeter (mm) stainless steel mesh screen to remove any larger or native organisms that could impact the test. The test used five replicates for each sample and laboratory controls.

Test animals and laboratory control sediment were supplied by Northwestern Aquatics of Newport, Oregon. The project and laboratory control sediment were placed in 1-L glass jars to a thickness of 2 cm (150 mL), to which was added approximately 900 mL of seawater. Additional replicates with no animals for each sample were set up to obtain measurements of pore water ammonia at test initiation and termination. The test was run under continuous light at a temperature of 15 ± 2°C and under gentle aeration. After 1 day of acclimation, an initial set of water quality parameter measurements were made including temperature, dissolved oxygen, pH, and salinity for each replicate (ammonia was measured in the overlying water of a composite of replicates in each sample and control). In addition, one of the replicates with no animals from each test treatment was broken down, and sediment pore water was extracted via centrifugation for subsequent analysis of ammonia. Test organisms then were randomly distributed to test chambers (20 animals per chamber). Animals remaining in the water column and exhibiting abnormal behavior after 1 hour were replaced. The chambers were covered with petri dishes to minimize evaporation. Water quality measurements were taken on day 0 and 10, and the number of dead and surfaced animals was noted for each replicate daily. On day 10, the sediments from the chambers were sieved through a 0.5-mm screen, and the number of survivors was recorded. Test acceptability criteria was 90 percent mean control survival. A reference toxicant test was

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Section 3.0 Methods

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conducted using cadmium chloride to establish sensitivity of test organisms used in the evaluation of Sweetwater Marsh sediments. An additional reference toxicant test was also conducted using ammonium chloride to evaluate potential influence of ammonia toxicity on the test results obtained with study sediments.

b. Pore Water Toxicity Tests Sediment pore water was extracted by centrifugation of the project sediment. After homogenization, approximately 750 mL of sediment from each station was placed into 1000-mL Teflon® containers. Containers were loaded into the centrifuge in a manner that created a balanced mass, and the sediment was spun for 15 minutes at a g-force of approximately 1,000 X g. Upon completion of centrifugation, containers were gently removed from the centrifuge to prevent sediment from the pellet became suspended in the supernatant. The overlying water, representing the 100 percent test concentration, was then decanted into labeled glass containers.All pore water from a given site was combined into a single container prior to splitting off into sub-samples for toxicity testing. If pore water was not used immediately for analysis, the samples were stored in the dark at 4 ± 2°C.

Protocols for the echinoderm fertilization test are from the EPA’s West Coast Manual (USEPA 1995). Pore water from each sample location and a seawater control were tested. This test examined the impact the project pore water samples had on echinoderm sperm cells and their ability to fertilize viable eggs. Adult Sand Dollars (Dendraster excentricus) were obtained from A. K. Siewers, Santa Cruz, California. Spawning was induced by injection of 0.5M potassium chloride. Eggs and sperm were collected and held separately to ensure that eggs were not prematurely fertilized. Prior to test initiation, a trial fertilization test was performed to determine the appropriate sperm-to-egg ratio for conducting this test. D. excentricus sperm cells were then placed into vials containing 10mL of project area pore water. After an exposure period of 20 minutes, D. excentricus eggs were then added. The eggs were given 20 minutes to fertilize after which the vials were preserved with 0.5 mL of 5% formalin for future enumeration under a microscope. The test was run using four replicates for each treatment and control at 15 ± 1°C. Temperature, pH, dissolved oxygen, and salinity were taken once at test initiation. The first 100 eggs in each sample were counted in a Sedgwick-Rafter cell and the proportion of fertilized and unfertilized eggs was determined. Test acceptability criteria for the test was 70% fertilization in controls. A reference toxicant test was conducted using copper sulfate. A reference toxicant test was also conducted using ammonia chloride.

Benthic Community Structure Assessments Benthic infaunal analyses were performed in accordance with the Bight 2003 Macrobenthic (Infaunal) Sample Analysis Laboratory Manual (Bight 2003b). The large amount of small organic (plant) particles made it necessary to split the sample material for sorting. Taxonomists that analyzed these samples participated in the intercalibration meetings required by the protocols.

All data were reviewed and verified to determine whether all data quality objectives were met, and that appropriate corrective actions were taken, if necessary. Infauna data were written on taxonomic bench sheets and double-key entered by a professional data entry service. The data were then processed through error screening computer programs that perform range checks and

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name verification. Additionally, a minimum of 10% of entries were visually verified to the bench sheets.

4.0 Data Analysis and Results

General sampling information is provided in Table 2.

Each of the components of the sediment quality triad approach was analyzed and is summarized in the tables and figures that follow. Tables 4 though 7 summarize the data of sediment characteristics. Table 8 summarizes the data analysis approaches associated with consideration of the toxicity assessments. Tables 9 through 13 summarize the data analysis approaches associated with consideration of the benthic community structure. Table 14 provides an overall summary of all of the sediment quality triad components combined.

4.1 Sediment Characterization Sediment chemistry results were evaluated by comparison to effects-based screening levels from the literature and compared generally to the reference station and San Diego Bay sediments. The data for the San Diego sediments were from Bight 1998 (see footnote 1). Effects-based screening levels from the literature were used to evaluate contaminant levels measured in study sediment (Long et al. 1995, Long and Morgan 1990, MacDonald 1994, Field et al. 2002).

Although contaminant loads provide useful information on sediment conditions, it is also important to evaluate the percentage of fine sediments and TOC since these factors may influence the distribution of organisms and contaminant levels in the sediments and may affect the outcome of the toxicity tests and contaminant availability to organisms. Therefore, potential impacts of fine sediments (<63 um) or TOC on benthic abundance and biomass regardless of sediment chemistry were also evaluated.

TOC levels were compared with ranges recommended by EPA (Hyland et al. 1999). Grain size did not vary, so it was not used in our analysis. While results for all target analytes are provided in the report (Appendices A and C), no effort was made to evaluate chemicals for which sediment quality guidelines are not available.

Comparison of Chemistry with Sediment Quality Guidelines Sediment Quality Guidelines have been developed to predict adverse biological effects on estuarine bottom dwelling invertebrates. Three sets of guidelines were used in this study.

"Effects Range-Low or ER-L” and "Effects Range-Medium or ER-M" are two guideline values which delineate three concentration ranges for each of several chemicals. Adverse effects are expected to be rare when contaminant concentrations fall below ER-L values. Concentrations between the ER-L and ER-M values represent a range within which adverse effects will occasionally occur, and toxic effects are frequently observed in the range of concentrations above the ER-M (Long et al. 1995). An ER-L and an ER-M for each chemical were derived arithmetically from a database consisting of matched chemical and biological effects data, including field data and laboratory bioassays, and equilibrium partitioning models (Long and

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Morgan 1990). A “Probable Effects Level or PEL” and “Threshold Effects Level or TEL” were derived for selected contaminants by the state of Florida using the same methods as described above, except for inclusion of data showing “no effects” and the use of a geometric mean instead of an arithmetic mean to define effects levels (MacDonald 1994). Finally, T20 and T50 values were derived for each of 37 chemicals by Field et al. (2002). These values denote concentrations that have a 20 percent or 50 percent probability of exhibiting toxicity.

Concentrations of chemicals measured in Paradise Marsh were compared to respective values from all three sets of guidelines. The three sets of metrics were considered equally as measures of the potential for adverse effects.

Each sediment sample was assigned a SQT-chemistry rank based on the number of compounds present at concentrations exceeding guidelines. The following rankings were considered based on exceedances by contaminants with sediment quality guidelines. Chemicals that exceeded guidelines are shown in Figure 3 and Table 4.

Poor: Concentrations of ten or more substances exceed the ER-L, T20, or TEL OR concentrations of two or more substances exceeded the ER-M, T50, or PEL. Sediments from stations Sed-1, Sed-3, Sed-4, Sed-6, Sed-8, and Sed-9 received a SQT-chemistry rank of poor.

Fair: Concentrations of five to ten substances exceeded the ER-L, T20 or TEL OR the concentration of one substance exceeded the ER-M or T50 or PEL. Sediments from stations Sed-2, Sed-5, and Sed-7 received a SQT-chemistry rank of fair.

Good: Concentrations of four or fewer substances exceeded ER-L, T20 or TEL, and no substances exceeded the ER-M, T50 or PEL. The reference station is the only location that received a SQT-chemistry rank of good.

These poor, fair, and good rankings were assigned a SQT-chemistry score of 1, 2, or 3, respectively for subsequent “scoring” of results.

One site (Sed-1) is clearly the most contaminated site as it exceeds ER-M or T50 or PEL for metals and numerous organic compounds. Other stations were ranked as poor (Sed-3, Sed-4, Sed-6, and Sed-9) due primarily to exceedances of ER-M or T50 or PEL for metals rather than excessive organic contaminants.

Mean ER-M Quotient Evaluation The use of the Mean ER-M Quotient (mER-Mq) is a simple approach for addressing overall chemical pollution where there were multiple pollutants at a station, and is used in addition to the standard chemical by chemical approach discussed earlier. This approach provides a measure of the potential combined toxicity of multiple contaminants. The mER-Mq for a station reflects both the number and degree of guideline exceedances.

The mER-Mq is described in detail in Long et al. (1998). Briefly, ER-Ms, which are concentrations “frequently” associated with biological effects (Long et al. 1995), were used to

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calculate the mER-Mq for each sample. Concentrations of the 24 contaminants for which ER-M values exist, were considered. These include eight trace metals (Ag, As, Cd, Cr, Cu, Hg, Pb, Zn), 13 PAH compounds (acenapthene, acenaphthylene, anthracene, benzo[a]pyrene, benzo[a] anthracene, chrysene, dibenz[a,h]anthracene, fluoranthene, fluorene, 2-methylnaphthalene, naphthalene, phenanthrene, pyrene), p,p’-DDE, total DDTs, and total PCBs. Mean ER-Mqs computed for the 24 chemicals have been used in previous studies of benthic impacts (Carr et al.1996a and b, Hyland et al. 1999).

The mER-Mq for each sample is calculated as follows: concentrations of individual chemicals were divided by their respective ER-Ms to produce an ER-M quotient for each chemical. The quotients for each station were summed and divided by the number of quotients to produce the mean quotient. In cases where concentrations of these chemicals were below the reporting limit (RL), a value of one-half the RL was used in the derivation of the mER-Mq.

The use of mER-Mq values was designed to assist with screening samples in which multiple compounds contributed to the overall level of chemical pollution, and was intended for use in conjunction with the standard chemical-specific method discussed in the previous section. Although interactive effects are possible with the mixtures of contaminants, none are implied by the use of mER-Mq. Quotients are presented as a method for comparing relative degree of contamination at various locations to aid management efforts.

A mER-Mq above 0.5 is considered elevated based on an analysis by Long et al. (1995) that indicated at least 50% of samples in a nationwide survey exhibited toxicity when the ER-Mq was greater than 0.5. Sediments with an ER-Mq >= 0.5 were classified as poor, sediments with an ER-Mq between 0.5 and 0.2 were classified as fair, and sediments with an ER-Mq <= 0.2 were classified as good.

The estimated ER-Mqs and ranks for Paradise Marsh sediments are shown in Table 5.

Percent Fine Sediments Evaluation The percentage of fine sediments in Paradise Marsh ranged only from 53 to 73%, with the median phi size ranging between 4.7 and 5.8. This relatively low variation indicates a relatively homogeneous study area with the proportion of fine sediments not likely to explain variations in contaminant levels or toxicity for sediments in this study area.

For this study, the threshold for “excessive fine sediments” and a poor score was greater than 75% fine sediments and “excessive coarse sediments” and a poor score was less than 40% fine sediments. All sampling locations were within these thresholds; and were therefore assigned a rank of fair and a score of 2. Because all stations had the same score for grain size, this parameter was not considered further.

Total Organic Carbon Evaluation Hyland et al. (1999) found that TOC levels below 0.5 mg/g (0.05%) and above 30 mg/g (3.0%) were related to decreased benthic abundance and biomass. The National Coastal Assessment Program (USEPA, 2004) has used TOC concentrations of above 2% and above 5% to indicate good or poor sediment quality, respectively. For this study, a rank of poor was assigned to

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sediments with TOC <=0.05% or >=3%. A rank of fair was used when TOC was between 0.05% and 2% and a rank of good was used when TOC was between 2% and 3%. One sampling site (Sed-1) had a TOC concentration high enough to indicate poor conditions. Five of the locations (Sed-3, 5, 6, 8, and 9) were in the good category and four (Sed-2, 4, 7, and 10) were in the fair category.

The ranks and scores based on TOC are shown in Table 6.

Sediment Quality Triad Score based on Sediment Characteristics Each of the Sediment Characterization Evaluations was individually scored and then the scores were averaged. The results are shown in Table 7. Overall, sediments from each station were assigned scores of 1, 2, or 3 for each of three factors. The average of these three was used to assign an overall SQT-chemistry rank of poor, fair or good. These were, in turn, assigned a numeric score to be factored into the final assessment.

4.2 Toxicity Assessments Results of bulk sediment and pore-water tests for all Paradise Marsh study locations are found in Appendices A and C.

Solid Phase Toxicity Tests Sediment samples were defined as toxic if there was a significant difference (p<0.05) in mean organism response (e.g. percentage survival) between a sample and its corresponding laboratory control. Statistical significance was determined using a separate variance t test. Survival among amphipods exposed to sediment from stations sed-2, -4, -5, -6, -8, and -9 was significantly lower than survival in their respective controls.

Pore Water Toxicity Tests Pore water bioassays were performed to estimate the toxicity of the water occupying the pore spaces of the Paradise Marsh sediment to echinoderm gametes at the sediment-water interface.

Toxicity to echinoderm gametes was determined by comparing results obtained with study area pore water to laboratory controls. Sediment samples were defined as toxic if there was a significant difference (p<0.05) in mean toxicity test organism response (e.g. percentage fertilization) between a sample and its corresponding laboratory control. Statistical significance was determined using a separate variance t test. However, because dissolved oxygen was low and salinity was high in test waters, these results likely are not an accurate portrayal of potential contaminant-related impacts at Paradise Marsh.

We cannot draw conclusions from these results since the dissolved oxygen and salinity failed their performance criteria for tests with the echinoderm larvae, so results of pore-water tests are not considered further.

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Sediment Quality Triad Score based on Toxicity Toxicity results of bulk sediment tests with amphipods were given an individual “rank” of good (>=90-percent survival), fair (between 70- and 90-percent survival) or poor (significantly lower than their respective controls).

The SQT-toxicity ranks and scores for bulk sediment toxicity tests are shown in Table 8.

4.3 Benthic Community Structure Assessments Because no one measure to assess the benthic community “health” at each sampling location is totally descriptive and wholly adequate, several methods were used for this analysis and are described below. Each measure was given an individual rank of good, fair, or poor. These ranks were assigned scores that were then averaged to produce a single average score to assess benthic community health at each study location.

The benthic community structure approach has several advantages: (a) the approach has been used extensively as an assessment tool to examine the ecological effects of potentially contaminated sediments; (b) it is an in situ method and therefore establishes an empirical relationship between benthic community structure and sediment quality; and (c) the method is well suited for assessing the spatial and temporal effects of toxic chemical contamination and/or organic carbon enrichment in a variety of sediment types. Limitations to this approach include: (a) the large number of factors that influence benthic community structure at a given site makes it difficult to isolate chemical-specific effects; and (b) it is a descriptive method and can not be used alone to generate numerical sediment quality criteria.

Measures of Biodiversity Overall, there were 13,847 individuals, representing 72 macrobenthic invertebrate species and 1 fish species collected from 10 benthic cores (Table 9). Polychaetes were more numerous than any other taxon. Great numbers of mollusks in Sed-1 and Sed-9 were due to the bivalve Musculista senhousei which generally occurs as a large aggregate. The number of species found per location ranged from 18 (Sed-10) to 35 (Sed-9).

A comparison of one or all of the following measures of biodiversity can illustrate the condition of the benthic community at each study location. Each measure can be used for comparisons between stations, one of which is a reference.

1. Species Richness (S) - the total number of different taxa present. It does not take into account the proportion and distribution of each species within the local aquatic community.

2. Shannon-Wiener index (H’) - similar to the Simpson's index, this measurement takes into account species richness and proportion of each species within the local aquatic community. Shannon-Weaver (H') puts statistical weight on rare species.

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3. Simpson Diversity Index (D’) - a measurement that accounts for the richness and the percent of each species from a biodiversity sample within a local aquatic community. The index assumes that the proportion of individuals in an area indicate their importance to diversity. Simpson's diversity index (D') emphasizes more common species.

Index values for each of the ten sample locations are shown in Table 10. Most sample locations within the study area had relatively diverse community assemblages and were similar to each other. The results showed differences in the range of diversity values between the study area and the reference site (Sed-10).

The results from the Species Richness, ShannonWeiner Index, and Simpson’s Diversity Index were standardized to the total range for each diversity value (classified between a minimum and maximum assigned to 0 and 10, respectively) for all sites and averaged to derive an overall rank which is shown as the “Combined Index Rank” and scored as follows: < 3 is poor; >=3 and <6 is fair; and >=6 is good. Poor, fair, and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations. Additional detail is provided in Chapman et al. 1997.

Ranks for individual measures and average ranks for each station are shown in Table 10.

Relative Benthic Index A detailed description of the methods used to calculate the relative benthic index (RBI) is provided in Anderson et al. (1998) and Fairey et al. (1996). It is based on responses of marine benthic communities to anthropogenic and natural disturbances. It does not require the presence of unpolluted reference stations and does not refer to data beyond that collected in each study.The metrics used in the RBI include number of species and individuals (total number of all taxa, total number of mollusk species, total number of mollusk individuals, total number of crustacean species and total number of crustacean individuals) the abundance of species indicative of relatively disturbed benthic habitats, and the abundance of species indicative of relatively undisturbed benthic habitats.

The overall RBI value for each station was calculated by summing the values of the total fauna, total mollusks, crustacean species, and indicator species (described later in this section) and standardized to the total range (described below).

The maximum and minimum values for total number of species, number of mollusk species and number of crustacean species, over all the stations were identified. For each station, the total number of species, total mollusk species, and total number of crustacean species were then converted to the percentage of the total range for each parameter. The number of crustacean individuals at each station was similarly converted to a percentage of the total range, and was added to the total species, mollusk, and crustacean species numbers. The community numbers, thus represent two thirds of the RBI for each station.

Equation: (Number of Mollusk Species at a station) / (Number of Mollusk Species Overall) + (Number of Crustacean Species at a station) / (Number of Crustacean Species Overall) + (Total Number of Species at a Station) / (Total Number of Species Overall) = Community Number for RBI calculation

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For the positive and negative indicator indices, the final index was weighted toward presence and absence of key indicator species, with abundance of each species given additional incremental weight. Accordingly, the abundance of each indicator species was transformed using a double square-root transformation to compress the range of values. For each species, the transformed abundance was converted to a percentage of the total range. The transformed values of the negative indicator species were summed and that sum was subtracted from the sum of the values for the positive indicator species.

Indicator species for the San Diego Bay area are not well described. Therefore, indicator species for other regions of California were also considered. The identification of representative positive indicator species was particularly problematic. Species commonly used elsewhere were not represented in this study. Therefore, less commonly used indicator species were included as positive indicator species and an additional diversity index was also considered (see “Proportional Abundance of Negative Indicator Species” section below). Appendix B lists the indicator species evaluated for this study.

a. Negative (pollution tolerant) indicator speciesThe polychaete annelid, Capitella capitata, is one of the most well known marine pollution indicators and has been found to be tolerant of a wide variety of contaminants including trace metals, hydrocarbons, and general pollution (Bridges et al. 1994; Chapman et al. 1987; Daan etal. 1994; Daan et al. 1996; Holte et al. 1996; Levin et al. 1996; Milbrink 1980; Pearson and Rosenberg 1978; Peterson et al. 1996; Plante-Cuny et al. 1993; Raman 1995; Reish 1957; and Tetra Tech 1990). The Capitella species complex is a cosmopolitan group that lives in a wide range of conditions including fouled or low oxygen, high organic matter and fine sediments. They have a rapid (1 to 2 month) life cycle, and are abundant around outfalls discharging biological wastes. Capitella sp. are capable of surviving for days with little or no oxygen, and are often considered the best example of a "weedy,” opportunistic species (Grassle and Grassle 1974; Grassle and Grassle 1976; Lenihan and Oliver 1995; McCall 1977; Okey 1997; Oliver et al. 1977; Pearson and Rosenberg 1978). This species was found at all sites except Sed-10 (reference site) at abundances ranging from four individuals (Sed-5) to 118 individuals (Sed-1) (Appendix B, Table 7).

Another polychaete, Streblospio benedicti, has been found to tolerate hydrocarbon contamination (Bridges et al. 1994; Chandler et al. 1997; Chapman et al. 1987; Dauer 1993; Levin et al. 1996; Pearson and Rosenberg 1978). Polychaete distributions and dominance patterns are often used as indicators of pollution, as many species (including S. benedicti) are relatively tolerant to high levels of sediment organics (Reish and Bernard 1979). Often, pollution-tolerant polychaetes remain in areas where more sensitive species have left or died, though heavily polluted areas eventually become completely devoid of life. S. benedicti was found at Sed-1 through Sed-8 at abundances ranging from two individuals (Sed-7) to 276 individuals (Sed-3).

Oligochaetes are an important indicator of pollution because of their tolerance to organic enrichment. In enriched or oxygen-deficient areas, there are typically high densities of tubificids. For example, tubificids made up 98 percent of the fauna in highly polluted areas of San Francisco Bay in 1968 (Cook and Brinkhurst 1973). Tubificid worms in the class

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Oligochaeta were found at all sites ranging from four individuals (Sed-10) to 776 individuals (Sed-4).

Unlike most other amphipods, Grandidierella japonica is tolerant of many contaminants (Carr etal. 1996a; Ferraro and Cole 1990; Swartz et al. 1994). This species was found at all sites except Sed-10 (reference site) at abundances ranging from 16 individuals (Sed-9) to 284 individuals (Sed-4).

b. Positive (pollution intolerant species) Indicator Species The bivalves in the genus Tellina live in clean, well-oxygenated sands of shallow water (Oliver et al. 1980). Species in Southern California attain great enough densities to be a major component of the shallow water, benthic infaunal community (Barnard 1963). They are not known to be early colonists in disturbed sedimentary habitats (Oliver et al. 1977). Tellina was found in low numbers at only two sites (Sed-2 and Sed-3).

Gammaridea (crustacea) are amphipods that are generally indicative of clean sediment (Fairey etal. 1996). Gammaridea was found at Sed-10 only (2 individuals).

The clam Macoma is small and lives shallowly under the sediment surface. Macoma generally favor finer sediment, including bays. Some Macoma species filter feed, while others deposit feed by vacuuming sediment surface with their incurrent siphon (Reid and Reid 1969). They are typically absent in a disturbed habitat. Where present, Macoma abundance ranged from four to 32 individuals. Macoma was found at sites Sed-4, 5, 6, 7, 8, and 9.

The overall RBI was calculated by summing the values of the total fauna, total molluscs, crustacean species, and indicator species (positive and negative), and standardizing it to the total range. This resulted in a range of values from 0.00 (most impacted) to 1.00 (least impacted). For this study, the threshold for significantly impacted benthic community structure was set at an RBI value of less than or equal to 0.30. The threshold for unimpacted benthic community structure was set at 0.50. Based on best professional judgment, stations having an RBI less than or equal to 0.30 had few species and individuals, few numbers of positive indicator species, and relatively large numbers of negative indicator species, while stations having an RBI greater than or equal to 0.50 had a robust number of species, more positive indicator species, and few negative indicator species. Sites with an RBI value <=0.3 were subsequently ranked as poor, those with an RBI value between 0.3 and 0.5 were ranked as fair, and those with an RBI value >=0.5 were ranked good.

The SQT results based on RBI calculations are shown in Table 11.

Proportional Abundance of Negative Indicator Species Because it was difficult to determine with confidence a suite of species that occur in unimpacted areas of San Diego Bay, we also evaluated the proportional abundance of negative indicator species based on literature review of species that are pollution tolerant. The ranking based on pollution tolerant species was assigned as follows: 0 to 25% good; 26 to 50% fair; 51 to 100% poor.

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The SQT results based on proportional abundance of pollution tolerant (negative) indicator species are shown in Table 12.

Sediment Quality Triad Score Results from the RBI and the Proportion Abundance of Pollution Tolerant Indicator Species were given individual rank of good, fair, or poor as described above. These ranks were assigned scores of 1, 2, or 3 which were then averaged to produce a single score for that sample. The average score for each station was assigned a rank of poor, fair or good.

The individual and average ranks for benthic community structure at each location are shown in Table 13.

4.4 Results

Analytical Results Results of chemical analyses for sediment chemistry, toxicity tests, and benthic community structure analysis are presented in Appendices A and C.

Overall Sediment Quality Triad Rank by Sampling Location Results from the sediment characterization, toxicity assessment, and benthic community analyses were given individual rank of good, fair, or poor as described above. These poor, fair, and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations. These values were then averaged to derive a single score for the overall Sediment Quality Triad Assessment. An average score of less than 1.75 is poor, >=1.75 and <2.5 is fair, and >=2.5 is good.

Final SQT ranks for sediments from 9 locations in Paradise Marsh and one reference station are shown in Table 14.

5.0 Discussion

5.1 Sediment Characterization The quality of sediments in San Diego Bay has historically been altered by human activity (USDoN, SWDIV, and SDUPD 2000). Similarly, Paradise Marsh has had similar alterations from adjacent development, upstream development, and tidal flux from the San Diego Bay. Major anthropogenic disturbances have included the removal and displacement of sediments by filling, channel dredging, and the direct input of sewage, industrial wastes, and pesticides. For example, the use and disposal of petroleum products (e.g., oils, paint sludge, diesel fuel, asphalt, and creosote) throughout the Bay introduced high levels of polycyclic aromatic hydrocarbons (PAHs) into the sediments. Moreover, various metals have been released to the water and sediments through air deposition, the leaching of hull paints, and disposal of industrial wastes.Sediment distribution within bays is affected by a complexity of factors, such as tidal influence, current velocity, sedimentary input, the presence or absence of large structures (e.g., piers or

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docks), channel dredging, breakwaters (USDoN, SWDIV, and SDUPD 2000), and upland runoff (Table 15).

Sediments from Paradise Marsh have clearly been impacted by activities in the San Diego Bay and upstream along Paradise Creek. Urban stormwater flushes debris and contaminants from roads, parking lots, sidewalks, rooftops, lawns, and other surfaces. Stormwater can contain suspended solids, nutrients, bacteria, oil and grease, trace metals, and organic contaminants such as pesticides, polychlorinated biphenyls (PCBs), and polycyclic aromatic hydrocarbons (PAHs). Additionally, sediment deposition occurs episodically, with flooding of tributaries causing fine marine sediments to be carried in from the Bay mainly through tidal action.

Clearly, Sed-1, which is closest to the upstream drain of Paradise Creek and close to both the north and east bluffs, collects the most profound contamination coming from off-site. Stormwater run-off and surface flow into Paradise Creek throughout the creek’s watershed appear to provide sources of contamination including hydrocarbons, metals, and pesticides.

Sediments at Sed-1 had the highest concentrations of cadmium, chromium, copper, mercury nickel, silver, and zinc and the second highest concentrations of arsenic and lead measured in Paradise Marsh sediments. Concentrations of the metals exceed effects-based guidelines for benthic invertebrates, as well as the calculated means for the sediments in San Diego Bay Bight 1998 data (Figure 4). Concentrations for all but arsenic and lead at Sed-1 were two to five times greater than the mean concentration for all sampling locations. The data indicated that sediments at Sed-1 were more influenced by upstream sources than by the Bay.

Every site sampled had at least four contaminants that exceeded the ER-L, TEL or T20. Sites Sed-1, -3, -4, -6, and -9 had two or more contaminants that exceeded more severe reference values (ER-M, PEL or T50) (Figure 3 and Table 4). Twenty-two contaminants exceeded the ER-M, PEL or T50 at Sed-1.

Metals Inorganic contaminants of concern for Paradise Marsh are also contaminants of concern for San Diego Bay overall. Metal contamination was widespread in San Diego Bay sediments in the Bight 1998 investigation, with every station containing measurable quantities of at least 15 different metals. The highest concentrations of certain metals (i.e., aluminum, arsenic, barium, chromium, copper, iron, manganese, nickel, zinc) were found where the percent of fine sediments was high. These included sites near Naval Station San Diego and within or near small boat marinas and commercial piers.

Fairey et al. (1996) concluded that five metals (i.e., chromium, copper, lead, mercury, zinc) should be considered contaminants of concern in San Diego Bay based on their concentrations in sediments or their potential for causing detrimental effects. Stations with the highest concentrations of these five metals occurred near naval shipyards and marinas. Copper, mercury, and zinc were the most prevalent of these metals in the Bay. They also occurred at highest concentrations relative to effects-based guidelines.

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The contaminants of concern in San Diego Bay identified by Fairey et al. (1996) were present at elevated levels in Paradise Marsh sediments. Although mean concentrations of these contaminants in San Diego Bay did not exceed ER-Ms, with the exception of chromium, these contaminants did exceed the ER-M guidelines in Paradise Marsh (Figure 3 and Figure 4). The reference site (Sed-10) had ER-M exceedances only for zinc, silver and copper. Metals that exceeded the ER-M, PEL or T50 at one or more locations included antimony, cadmium and silver in addition to the four identified in San Diego Bay (copper, lead, mercury and zinc).

Polycyclic Aromatic Hydrocarbons (PAHs) PAHs were detected in the sediments at 34 of the 46 stations sampled in San Diego Bay (Bight 1998 data, see footnote 1) and in all of the samples from Paradise Marsh. In San Diego Bay, total PAH concentrations ranged from 16 to 10,768 parts per billion (ppb), with the highest concentrations occurring primarily within naval installations and large shipyards. In contrast, the lowest PAH concentrations generally occurred in sediments in open areas of the Bay where tidal flushing is relatively strong.

In Paradise Marsh, Sed-1 had the highest Total PAH concentrations (26,098 ppb), more than double the highest concentrations found in other parts of San Diego Bay. The Total PAH values ranged from 64.8 ppb (Sed-10, reference site) to 26,098 ppb (Sed-1). The concentrations of individual PAHs in Sed-1 are seriously elevated. Table 4 and Table 16 show the PAH analytes measured in Paradise Marsh that were detected and those that exceeded the sediment guidelines.

Although Sed-1 is not located next to the shipyards and naval installations that occur within other portions of San Diego Bay, it is located immediately adjacent to the inflow from the urbanized and industrial watershed of Paradise Creek which may explain the nature of contamination at this site. Proximity to Interstate 5 and contaminated fill materials found in the east bluff and north bluff may also help to explain contaminant levels at this location.

Polychlorinated Biphenyl Compounds (PCBs) PCBs were detected in sediments at 12 of the 46 stations sampled in San Diego Bay. These stations were located primarily in large shipyards, naval facilities, and along downtown waterfronts. Total PCB levels ranged from 1.5 ppb to 123.8 ppb. The highest concentrations were found near the NASSCO shipyard, the mouth of Las Chollas Creek, and in Harbor Island East Basin near the mouth of Convair Basin, a PCB cleanup site.

PCBs were detected at seven of the ten sampling locations in Paradise Marsh with concentrations ranging from 5.6 ppb to 111 ppb (Sed-1), similar to concentrations found in the Bay. PCB concentrations exceeded the ER-L at sites Sed-1, Sed-3, and Sed-4. PCBs were not detected at the reference site (Sed-10).

PesticidesAlthough DDT was detected in San Diego Bay sediments in 1998, it only occurred at seven of the 46 San Diego Bay stations. Neither DDT nor its metabolites were detected in Paradise Marsh using the methods described in this report. However, chlordanes were detected in Paradise Marsh. This was not surprising because chlordanes are often detected at the mouth of upland drainages such as Paradise Creek (Bay and Greenstein 2002). Chlordanes were found at

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sites Sed-1 (>ERM), Sed-3 (>ER-L), and Sed-8 (>ER-L). Residues of chlordanes are likely due to past use for controlling termites and other insects in residential settings prior to the 1988 ban on chlordane use in the U.S. Chlordane is quite stable in the soil environment and may continue to be transported for years from soils near treated buildings upstream of Paradise Marsh and into the watershed.

Data from Bight 1998 indicate that chlordane pollution is pervasive along the north shore of San Diego Bay, San Diego River, and northern Mission Bay. Areas which receive storm runoff, such as Chollas Creek, Seventh St. Channel, and urban storm drains appear to be the most heavily contaminated.

5.2 Toxicity Assessments Sediment toxicity testing on field collected sediments is an essential line-of-evidence that the contaminants present in the sediments may produce adverse effects in the benthic community.The composition of interstitial waters in sediments is another indicator of the potential for sediment-borne contaminants to adversely affect benthic organisms. However, in this study, pore water test results were discarded because they did not meet performance criteria

Some conclusions from a SETAC review of toxicity testing of pore water, including recommendations for future areas of research, were as follows (Carr and Nipper 2001):

Sampling, extraction, and storage techniques are critically important for achieving the most field-representative samples of pore water.

It is nearly impossible to avoid artifacts and chemical changes when removing pore water from sediment and using it in a toxicity test. Determination of chemical concentrations in pore waters is recommended, in addition to the regular contaminant measurements conducted in the whole sediment, as a means of providing information on routes and levels of exposure, aiding in the interpretation of test results, and identifying sources of toxicity.

The measurement of several pore-water features, a number of which can act as confounding factors (e.g., salinity, alkalinity, pH, conductivity, dissolved oxygen concentrations, ammonia, hydrogen sulfide, and oxidation potential (Eh)), should be recorded shortly after pore-water collection and after storage. This would help in interpreting test results, understanding the contribution of these factors to concordance or discordance between solid phase and pore-water test methods.

In this study, it is likely that dissolved oxygen and hypersalinity acted as confounding factors, limiting our understanding of the contribution of the contamination to the results of the tests.

5.3 Benthic Assemblages Sites and stations which are categorized as undegraded (or in this case “good”) have high species diversity, high proportional abundance of amphipods and other crustaceans, with a few

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exceptions (e.g., the crustacean G. japonica, was used as an indicator of a stressed habitat in this study.). Undegraded areas generally contain species which are known to be sensitive to pollutants.

The approach we used in the study assumes that the integration of data from laboratory toxicity tests, chemical analyses, and benthic community assessments provides complementary evidence of the degree of pollution-induced degradation in aquatic communities. However, species within a community may vary broadly in their response to contaminants (some may decrease in abundance due to the direct effects of a toxicant while other may increase in abundance; Coull and Chandler 1992), and, thus, the total abundance of a major taxon may obscure significant changes in community composition.

Environmental contamination acts as a selective force against sensitive individuals. The Paradise Marsh study area had a large proportion of species that have been identified in the literature as tolerant of stressors (“pollution tolerant” or “indicator species”) (see list in Appendix B). In the Paradise Marsh study area, 25 percent (n = 17) of the species identified in Sed-1 through Sed-9 were indicative of a stressed environment. Those made up 35% of the total abundance. In Sed-10, only one in 15 species were indicative of a stressed environment. That species made up less than 1 percent of the total abundance in the reference site.

5.4 Sediment Quality Triad Assessment While the three types of data from the triad concept provide complementary measures of sediment quality, the data from the three measures may not necessarily parallel each other. Each component measures different properties of the sediments. For example, sites that are relatively contaminated may not be the most toxic, or sites with relatively altered benthic communities may not be most contaminated. If each of the components mimicked each other in the classification of sites, there would be no need to measure all three. The strength of the triad approach is the use of both chemical and biological measures that can be used in an ecological evaluation of sediment quality. The triad concept can provide the data needed to interpret and use in characterizing sediment quality.

The Sediment Quality Triad approach allows us to delineate between sites where observed effects are more or less severe. At moderately impacted sites, this delineation may be difficult to see and may confound the interpretation of the results.

In the present study, a combination of measures through the SQT approach allows us to determine that conditions are poor at multiple locations in Paradise Marsh (Table 14). Based on individual measures, it can be concluded that sediments are most impacted at the locations nearest the inflow of Paradise Creek and two fill areas. The influences from Paradise Creek and fill areas are greater than those from San Diego Bay.

In this study, there was evidence of contamination throughout the study area. This was possibly due to the presence of the contaminated fill material on the north and the inflow of Paradise Creek on the northwest. The possible trend of decreasing contamination from north to south was not statistically significant; however, three of the five poor sites (Sed-1, Sed-2, and Sed-4) were

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the closest to the north bluff. Additionally, two of those (Sed-1 and Sed-2) were also the closest to the inflow and the east bluff. (See Figure 5)

It became apparent that all the sampling locations within the study area exhibit harmful sediment contamination to some degree. These sites are located within an urban and industrial development with multiple known and potential sources of contamination. Sed-1, located nearest to the Paradise Creek inflow and Sed-3 and Sed-4, located nearest to the north bluff fill showed some serious contamination problems. Sed-6 and Sed-8 also showed some serious contamination problems; however, their relationship to contamination sources was less clear.

Groundwater studies in the area have shown that groundwater moves to the north from the wetland to the north bluff. This suggests that surface phenomena are potentially responsible for transporting contaminants into the marsh. The inflow of Paradise Creek is possibly a source of contamination due to the urban and industrial nature of the watershed. Chlordane is often linked to urban run-off areas, and its presence in Paradise Marsh further indicates potential evidence of the contribution of contamination via Paradise Creek (Bay and Greenstein 2002).

5.5 Reference Site The reference station (Sed-10) used in this study was determined to be acceptable. No ER-M guideline values were exceeded and the mER-Mq was the lowest of all the sites evaluated. No significant toxicity was observed in the reference station sediments. In addition, benthic community structure at the reference site had few “pollution tolerant species.” TOC and grain size were within the range found in the study sites, so conditions were considered to be comparable.

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6.0 Management Recommendations and Conclusions

Conclusions Sediment quality throughout the sampled areas of Paradise Marsh showed evidence of

contamination from multiple chemicals (see Figure 3). All of the sites in Paradise Marsh were more contaminated than the reference site in

Sweetwater Marsh (Sed-10) based on the results of the Sediment Quality Triad approach.

Sites closest to known sources of contamination (north bluff, east bluff and Paradise Creek inflow) tended to have higher levels of contamination and impacts, although this relationship was not statistically significant based on the methods we used.

Contaminants found to be of concern in San Diego Bay in previous studies were also present at levels of concern in Paradise Marsh.

Petroleum hydrocarbon contamination in Sed-1 is of serious concern for the Refuge. The source of this contamination is unknown.

Recommendations Additional investigation upstream of Paradise Marsh is recommended, specifically to

characterize inputs into Paradise Creek that are being transported into Paradise Marsh. Sediment clean-up of Paradise Marsh is warranted especially with respect to PAHs. Further

research on the contamination in the inflow needs to be conducted and the source identified and halted prior to the initiation of cleanup activities.

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Section 7.0 References

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7.0 References ASTM (American Society for Testing and Materials). 1991. E 1367 guide for conducting 10-d static sediment toxicity tests with estuarine and marine amphipods. In: 1991 Annual Book of ASTM Standards. Vol. 11.04. Am. Soc. Test. Materials, Philadelphia, PA. pp 1052-1075.

Anderson B, P Nicely, B Phillips, and J Hunt. 2004. Sediment Quality Assessment Study at the B Street/Broadway Piers, Downtown Anchorage, and Switzer Creek, San Diego Bay Phase I Draft Report. Prepared by Marine Pollution Studies Laboratory, University of California, Davis, CA. In cooperation with San Diego Regional Water Quality Control Board, Port of San Diego, City of San Diego. 190 pp.

Anderson B, J Hunt, B Phillips, J Newman, R Tjeerdema, CJ Wilson, G Kapahi, RA Sapudar, M Stephenson, M Puckett, R Fairey, J Oakden, M Lyons, and S Birosik. 1998. Sediment Chemistry, Toxicity, and Benthic Community Conditions in Selected Water Bodies of the Los Angeles Region, Final Report. California State Water Resources Control Board, Division of Water Quality, Bay Protection, and Toxic Cleanup Program. 232 pp.

Barnard, JL. 1963. Relationship of benthic Amphipoda to invertebrate communities of inshore sublittoral sands of southern California. Pac. Natur. 3: 439-466.

Bay, S, R Burgess, and D Nacci. 1993. Status and applications of echinoid (phylum Echinodermata) toxicity test methods. In: W.G. Landis, J.S. Hughes, and M.A. Lewis (eds.), Environmental toxicology and risk assessment, Std. Tech. Publ. 1179 Am. Soc. Test. Materials, Philadelphia, PA. pp. 281-302.

Bay, S and D Greenstein. 2002. Preliminary Characterization of Sediment Toxicity in the Chollas Creek Channel. Southern California Coastal Water Research Project Technical Report #362, SCCWRP, Westminster, CA. 19 pp.

Bight Report. 2003a. Southern California Bight 2003 Regional Marine Monitoring Survey, Field Operations Manual. Prepared for the Commission of Southern California Coastal Water Research Project. July 2003. 147 pp.

Bight Report. 2003b. Southern California Bight 2003 Regional Marine Monitoring Survey, Macrobenthic (Infaunal) Sample Analysis Laboratory Manual. Prepared for the Commission of Southern California Coastal Water Research Project. June 2003. 31 pp.

Bight Report. 2003c. Southern California Bight 2003 Regional Marine Monitoring Survey, Coastal Ecology Workplan. Prepared for the Commission of Southern California Coastal Water Research Project. June 2003. 28 pp.

Bight Report. 2003d. Southern California Bight 2003 Regional Marine Monitoring Survey, Quality Assurance Manual. Prepared for the Commission of Southern California Coastal Water Research Project. June 2003. 58 pp.

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Bridges TS, LA Levin, D Cabrera, G Plaia. 1994. Effects of sediment amended with sewage, algae, or hydrocarbons on growth and reproduction in two opportunistic polychaetes. J Exper Mar Biol Ecol 177: 99–119.

Carr, RS, DC Chapman, CL Howard, and J Biedenbach. 1996a. Sediment Quality Triad assessment survey in the Galveston Bay Texas system. Ecotoxicology 5: 341-364.

Carr, RS, ER Long, DC Chapman, G Thursby, JM Biedenbach, H Windom, G Sloane, and DA Wolfe. 1996b. Toxicity assessment studies of contaminated sediments in Tampa Bay, Florida. Environ. Toxicol. Chem. 15: 1218-1231.

Carr, RS and M Nipper. 2001. Summary of a SETAC Technical Workshop. Porewater Toxicity Testing: Biological, Chemical, and Ecological Considerations with a Review of Methods and Applications, and Recommendations for Future Areas of Research.

Chandler, GT, MR Shipp, and TL Donelan. 1997. Bioaccumulation, growth and larval settlement effects of sediment-associated polynuclear aromatic hydrocarbons on the estuarine polychaete, Streblospio benedicti (Webster). Journal of Experimental Marine Biology and Ecology 213: 95-110.

Chapman, PM. 1986. Sediment quality criteria from the sediment quality triad: An example. Environ. Toxicol. Chem. 5: 957-964.

Chapman, PM, B Anderson, S Carr, M Engle, R Green, J Hameedi, M Harmon, P Haverland, J Hayland, C Ingersoll, E Long, J Rogers Jr, M Salazar, PK Sibley, PJ Smith, RC Swartz, B Thompson, and H Windom. 1997. General Guidance for Using the Sediment Quality Triad. Marine Pollution Bulletin, 34(6): 368-372.

Chapman, PM, RN Dexter, and ER Long. 1987. Synoptic measures of sediment contamination, toxicity and infaunal community composition (the sediment quality triad) in San Francisco Bay.Mar. Ecol. Prog. Ser. 37: 75-96.

Cook, DG and RO Brinkhurst. 1973. "Marine Flora and Fauna of the Northeastern United States, Annelida: Oligochaeta." National Oceanic and Atmospheric Administration and National Marine Fisheries Service, U.S. Department of Commerce. Seattle, Washington. 22 pp.

Coull, BC and GT Chandler. 1992. Pollution and meiofauna: field, laboratory, and mesocosm studies. Oceanogr. Mar. Biol. Annu. Rev. 30: 191-271.

Daan, R, M Mulder, and A van Leeuwen. 1994. Differential sensitivity of macrozoobenthic species to discharges of oil-contaminated drill cuttings in the North Sea. Netherlands Journal of Sea Research 33: 113-127.

Daan, R, K Booij, M Mulder, and EM van Weerlee. 1996. Environmental effects of a discharge of drill cuttings contaminated with ester-based drilling muds in the North Sea. Environmental Toxicology and Chemistry 15(10): 1709-1722.

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Dauer DM. 1993. Biological criteria, environmental health, and estuarine macrobenthic community structure. Mar Pollut Bull 26: 249–257.

Fairey, R, C Bretz, S Lamerdin, J Hunt, B Anderson, S Tudor, C Wilson, F La Caro, M Stephenson, M Puckett, and E Long. 1996. Chemistry, Toxicity, and Benthic Community Conditions in Sediments of the San Diego Bay Region. Final Report. California State Water Resources Control Board. Sacramento, CA. 203 pp.

Ferraro, SP and FA Cole. 1990. Taxonomic level and sample size sufficient for assessing pollution impacts on the Southern California bight macrobenthos. Mar. Ecol. Prog. Ser. 67: 251-262.

Field, LJ, DD MacDonald, SB Norton, CG Ingersoll, CG Severn, D Smorong, and R Lindskoog. 2002. Predicting amphipod toxicity from sediment chemistry using logistic regression models. Environmental Toxicology and Chemistry 21: 1993-2005.

Grassle, JF and JP Grassle. 1974. Opportunistic life histories and genetic systems in marine benthic polychaetes. Journal of Marine Research. 32(2): 253-283.

Grassle, JP and JF Grassle. 1976. Sibling species in the marine pollution indicator Capitella(Polychaeta). Science 192: 567-569.

Holte, B, S Dahle, B Gulliksen, and N Naes. 1996. Some macrofaunal effects of local pollution and glacier-induced sedimentation, with indicative chemical analyses in the sediments of two Arctic fjords. Polar Biology 16: 549-557.

Hyland JL, RF Van Dolah, and TR Snoots. 1999. Predicting stress in benthic communities of southeastern U.S. estuaries in relation to chemical contamination of sediments. Environ Toxicol Chem 18: 2557–2564.

ICES Advisory Committee on Ecosystems. 2004. Report of the Study Group on Ecological Quality Objectives for Sensitive and for Opportunistic Benthos Species. ICES CM 2004/ACE:01 Ref. E, WGECO, BEWG. ICES, Copenhagen. 83 pp.

Jacobi M, R Fairey, C Roberts, E Landrau, J Hunt, B Anderson, B Phillips, CJ Wilson, G Kapahi, F LaCaro, B Gwynne, M Stephenson, and M Puckett. 1998. Chemical and Biological Measures of Sediment Quality and Tissue Bioaccumulation in the North Coast Region. Final Report. CSWRCB; NOAA; CDF&G, Marine Pollution Studies Laboratory; Moss Landing Marine Laboratories; UC Santa Cruz. 79 pp.

Lenihan, HS and JS Oliver. 1995. Anthropogenic and natural disturbances to marine benthic communities in Antarctica. Ecological Applications 5(2): 311-326.

Levin, L, H Caswell, T Bridges, C Dibacco, D Cabrera, and G Plaia. 1996. Demographic responses of estuarine polychaetes to pollutants: Life table response experiments. Ecological Applications 6: 1295-1313.

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Long ER, DD MacDonald, SL Smith, and FD Calder. 1995. Incidence of adverse biological effects within ranges of chemical concentrations in marine and estuarine sediments. Environ Manag 19: 81–97.

Long ER, LJ Field, and DD MacDonald. 1998. Predicting toxicity in marine sediments with numerical sediment quality guidelines. Environ Toxicol Chem 17: 714–727.

Long, ER and LG Morgan. 1990. The Potential for Biological Effects of Sediment-sorbed Contaminants Tested in the National Status and Trends Program. NOAA Tech. Memo. NOS OMA 52, 175 pp.

MacDonald, D. 1994. Approach to the Assessment of Sediment Quality Guidelines in Florida Coastal Waters. Volume 1- Development and Evaluation Of Sediment Assessment Guidelines. Prepared for the Florida Department of Environmental Regulation. MacDonald Environmental Services, Ltd., Ladysmith, British Columbia. 52 pp.

McCall, PL. 1977. Community patterns and adaptive strategies of the infaunal benthos of Long Island Sound. Journal of Marine Research 35: 221-226.

Milbrink G. 1980. Oligochaete communities in pollution biology: The European situation with special references to lakes in Scandia, Drottningholm, Sweden. Uppsala University and Institute of Freshwater Research, Uppsala, Sweden. pp. 433–455.

Okey, TA. 1997. Sediment flushing observations, earthquake slumping, and benthic community changes in Monterey Canyon head. Continental Shelf Research 17: 877-897.

Oliver, JS, PN Slattery, LW Hulberg, and JW Nybakken. 1977. Patterns of Succession in Benthic Infaunal Communities Following Dredging and Dredged Material Disposal in Monterey Bay. Dredged Material Research Program, U.S. Army Engineers Waterways Experiment Station, Technical Report 0-77-27, Vicksberg, Mississippi. 186 pp.

Oliver, JS, PN Slattery, LW Hulberg, and JW Nybakken. 1980. Relationships between wave disturbance and zonation of benthic invertebrate communities along a subtidal high energy beach in Monterey Bay, California. Fishery Bulletin 78: 437-45.

Pearson TH and Rosenberg R. 1978. Macrobenthic succession in relation to organic enrichment and pollution of the marine environment. Oceanogr Mar Biol Annu Rev 16: 229-311.

Peterson, CH, MC Kennicutt II, RH Green, P Montagna, DE Harper Jr, EN Powell, and PF Roscigno. 1996. Ecological consequences of environmental perturbations associated with offshore hydrocarbon production: A perspective on long-term exposures in the Gulf of Mexico.Canadian Journal of Fisheries and Aquatic Sciences 53: 2637-2654.

Plante-Cuny, MR, C Salen-Picard, C Grenz, R Plante, E Alliot, and C Barranguet. 1993.Experimental field study of the effects of crude oil drill cuttings and natural biodeposits on microphyto- and macrozoobenthic communities in a Mediterranean area. Marine Biology (Berlin) 117: 355-366.

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Raman, AV. 1995. Pollution effects in Visakhapatnam harbour in India: An overview of 23 years of investigations and monitoring. Helgolaender Meeresuntersuchungen 49: 633-645.

Ranasinghe, JA, DE Montagne, RW Smith, TK Mikel, SB Weisberg, D Cadien, R Velarde, and A Dalkey. 2003. Southern California Bight 1998 Regional Monitoring Program: VII. Benthic Macrofauna. Southern California Coastal Water Research Project. Westminster, CA. 100 pp.

Reid, RG and A Reid. 1969. Feeding processes of members of the genus Macoma (Mollusca: Bivalvia). Can. J. Zool. 47: 649-657.

Reish DJ. 1957. The relationship of the polychaetous annelid Capitella capitata (Fabricius) to waste discharges of biological origin. In: Tarzwell D, ed. Biological Problems in Water Pollution. U.S. Public Health Service, Washington DC, pp 195-200.

Reish, DJ and JL Barnard, 1979. "Amphipods." In: CW Hart and SLH Fuller, Jr, eds. Pollution Ecology of Estuarine Invertebrates. Academic Press. New York. pp 345-370.

SFEI. 1999. 1997 Annual Report: San Francisco Estuary Regional Monitoring Program for Trace Substances. San Francisco Estuary Institute, Oakland, CA. 389 pp.

Smith RW, M Bergen, SB Weisberg, D Cadien, A Dalkey, D Montagne, JK Stull, and RG Velarde. 2001. Benthic Response Index for Assessing Infaunal Communities on the Mainland Shelf of Southern California. Ecological Applications: 11(4): 1073-1087.

Swartz, RC, FA Cole, JO Lamberson, SP Ferraro, DW Schults, WA DeBen, H Lee II, and RJ Ozretich. 1994. Sediment toxicity, contamination, and amphipod abundance at a DDT- and dieldrin-contaminated site in San Francisco Bay. Environ. Toxicol. Chem. 13: 949-962.

Tetra Tech. 1990. Puget Sound Ambient Monitoring Program 1989: Marine Sediment Monitoring. Prepared for Washington Dept. of Ecology, Ambient Monitoring Section. Tetra Tech, Inc. Bellevue, WA. 279 pp.

U.S. Department of the Navy, Southwest Division (USDoN, SWDIV) and San Diego Unified Port District (SDUPD). 2000. San Diego Bay Integrated Natural Resources Management Plan, September 2000. San Diego, Ca. Prepared by Tierra Data Systems, Escondido, CA. 705 pp.

U.S. Environmental Protection Agency, United States; and Department of the Army, United States Army Corps of Engineers (EPA and USACE). 1998. Evaluation of Dredged Material Proposed for Discharge in Waters of the U.S.: Testing Manual (Inland Testing Manual). EPA-823-B-98- 004. EPA Office of Water. February 1998. 409 pp.

U.S. Environmental Protection Agency, United States (EPA) 1995. West Coast Manual. EPA/600/R-95/136. 15 pp.

U.S. Environmental Protection Agency. 2004. National Coastal Condition Report II. Office of Research and Development, Office of Water, Washington D.C. EPA-620/R-03/002. 290 pp.

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Zembal, R and SM Hoffman. 2002. A Survey of the Beldings Savannah Sparrow (Passerculus sandwichensis beldingi) in California 2001. Species Conservation and Recovery Program Report No. 2002-01. California Department of Fish and Game. 16 pp.

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Figures and Tables

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Figure 1. Location Map for Paradise Marsh, San Diego, CA.

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Figures and Tables

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Figure 2. Sampling Locations for the Paradise Marsh Contaminants Investigation, San Diego, CA 2004.

Sed-# = denotes sampling location number

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Figures and Tables

- 31 -

Figure 3. Sediment Characterization Based on Sediment Chemistry Showing Contaminants that Exceed Guidelines at Sampling Locations Ranked Poor and Fair for the Paradise Marsh Contaminants Investigation, San Diego, CA 2004.

0

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2

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4

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c. Sampling Locations Ranked as Fair Due to between Five and Ten ER-L / TEL / T20 Exceedances

a. Sampling locations sed-1, -3, -4, -6, and -9 received a poor SQT ranking with >=2 ER-M or PEL or T50 exceedances b. Sampling locations sed-1, -3, -6, and -8 received a poor SQT ranking with >10 ER-L or TEL or T20 exceedances c. Sampling locations sed-2, -5, and -7 received a fair SQT ranking with >5 and <= 10 ER-L or TEL or T20 exceedances Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Sed-# = denotes sampling location number ER-L = effects range-low ER-M = effects range-median PEL = probable effects level TEL = threshold effects level T20 = denotes the probability that 20 percent of samples would be toxic T50 = denotes the probability that 50 percent of samples would be toxic

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Figures and Tables

- 32 -

Figure 4. Comparison of Sediment Chemistry Results from this study (Paradise Marsh Contaminants Investigation, San Diego, CA) to the San Diego Bay Bight 1998 project.

0

1

10

100

SED-1

SED-2

SED-3

SED-4

SED-5

SED-6

SED-7

SED-8

SED-9

SED-10

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arsh

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cent

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UCL SD Bay Bight 98 Mean

Inde

xed

Dat

a

Paradise Marsh sediment chemistry results are shown relative to the upper confidence level of the Bight 1998 Mean.

Note: Because these data include an array of contaminants, the data set is indexed so that you can compare two locations (Paradise Marsh and San Diego Bay) and the eight contaminants of concern on one chart. The results for the Paradise Marsh sediments are indexed against the UCL of the mean for each of the contaminants of concern identified in the San Diego Bay Bight 1998 study calculated as:

(Paradise Marsh sediment concentration) / (UCL mean San Diego Bay Bight 1998 sediment concentration)

Results for each Paradise Marsh sampling station shown as >Index 1 and above the line exceed the Bight 1998 Mean UCL, while those below the line do not.


Figure 5. Overall SQT Rank Compared with Distance from Potential Sources of Contamination for the Paradise Marsh Contaminants Investigation, San Diego, CA.

0200400600800

10001200140016001800

dist

ance

(m)

Poor Fair Good

inflow north bluff east bluff

See Figure 2 for locations of the Inflow, North Bluff and East Bluff.

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Figures and Tables

- 33 -

Table 1. Surveys of breeding Belding's Savannah sparrows in San Diego Bay, 1977-2001 for the Paradise Marsh Contaminants Investigation, San Diego, CA.

LOCATION NUMBER OF PAIRS

1977 1986 1991 1996 2001

Paradise Marsh 16 19 14 6 7

Sweetwater Marsh NWR 40 118 141 78 93

F Street Marsh 18 8 15 12 9

Western Salt Company Dikes/Otay River 100 70 29 71 102

South Bay Marina Reserve 25 15 42 31 26

San Diego Bay Totals 199 230 241 198 237

State-Wide Totals 1610 2274 1844 2350 2902

Source: Zembal and Hoffman 2002

Table 2. Sampling Station Information for the Paradise Marsh Contaminants Investigation, San Diego, CA 2004.

Station Date Latitude Longitude Depth(m)

Salinity(psu) pH

DissolvedOxygen(mg/L)

Comment

SED 1 7/21/2004 32.659 -117.108 0.46 36.43 7.95 10.1 90% algal cover SED 2 7/21/2004 32.658 -117.109 1.26 35.64 8.08 12.0 90% algal cover concrete rubble SED 3 7/21/2004 32.658 -117.109 0.59 36.53 8.00 12.3 100% algal cover concrete rubble SED 4 7/21/2004 32.658 -117.109 1.20 36.49 8.03 12.5 100% algal cover concrete rubble SED 5 7/22/2004 32.657 -117.108 0.30 36.71 7.91 9.9 90% algal cover SED 6 7/22/2004 32.656 -117.109 0.90 36.73 7.93 10.8 40% algal cover SED 7 7/22/2004 32.655 -117.107 0.98 36.53 7.80 9.1 80% mussel cover SED 8 7/22/2004 32.654 -117.107 0.90 35.55 7.68 7.7 80% algal cover SED 9 7/22/2004 32.651 -117.105 0.38 36.15 7.51 6.3 80% algal and eelgrass cover

SED 10 7/21/2004 32.644 -117.107 0.56 36.04 7.64 8.0 75% algal and eelgrass cover Sed-# = denotes sampling location number

Table 3. Bioassay Testing Performed on Samples for the Paradise Marsh Contaminants Investigation, San Diego, CA 2004.

Associated QA/QC TestsTest Type Type of

Organism Taxon Test Duration Reference Toxicant

Solid Phase –Survival Amphipod Eohaustorius estuarius 10 Days Copper / Ammonia

Echinoderm Fertilization Echinoderm gametes Dendraster excentricus 40-Minute Copper / Ammonia

QA/QC = Quality Assurance / Quality Control

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Figures and Tables

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Table 4. Sediment Characterization using Sediment Chemistry Guidelines for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED

-1

SED

-2

SED

-3

SED

-4

SED

-5

SED

-6

SED

-7

SED

-8

SED

-9

SED

-10

Antimony (Sb) ++ + ++ + + + + Arsenic (As) + + + Cadmium (Cd) ++ + + + + + + Chromium (Cr) + + + Copper (Cu) ++ + ++ + + + + + ++ + Lead (Pb) ++ ++ ++ + + + + Mercury (Hg) ++ + + ++ + Nickel (Ni) + + + + Silver (Ag) ++ + + + + + + + ++ + Zinc (Zn) ++ + ++ + + ++ + + ++ + 1-Methylphenanthrene + + Acenaphthene + Acenaphthylene + + Anthracene + Benz[a]anthracene ++ + + + Benzo[a]pyrene ++ + + + + + + Benzo[b]fluoranthene ++ + Benzo[g,h,i]perylene ++ + + + Benzo[k]fluoranthene ++ + + + Chlordane-alpha ++ + Chlordane-gamma ++ + Chrysene ++ + Dibenz[a,h]anthracene ++ + + + + Fluoranthene ++ + + Fluorene + + Indeno[1,2,3-c,d]pyrene ++ + + + Perylene ++ Phenanthrene ++ ++ Pyrene ++ + Total Detectable PAHs ++ + Total Detectable PCBs + + + ERL or TEL or T20 Exceedances (+) 31 5 18 8 6 22 7 13 9 4

ERM or PEL or T50 Exceedances (++) 22 0 3 2 0 3 0 0 3 0

SEDIMENT RANKING poor fair poor poor fair poor fair poor poor good “+” indicates ERL or TEL or T20 exceedances and “++” indicates ER-M or PEL or T50 exceedances. Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Sed-# = denotes sampling location number ER-L = effects range-low ER-M = effects range-median PEL = probable effects level TEL = threshold effects level T20 = denotes the probability that 20 percent of samples would be toxic T50 = denotes the probability that 50 percent of samples would be toxic

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Figures and Tables

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Table 5. ER-Mqs and corresponding ranks for sediments for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10 ER-Mq 0.69 0.06 0.16 0.55 0.05 0.17 0.06 0.08 0.08 0.04 ER-Mq SQT Score poor good good poor good good good good good good Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Sed-# = denotes sampling location number ER-Mq = effects range-median quotient SQT = sediment quality triad

Table 6. SQT Rank for Physical Sediment Characteristics for the Paradise Marsh Contaminants Investigation, San Diego, CA.

Parameter Units SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10percent 5.194 1.178 2.763 1.398 2.192 2.426 1.82 2.091 2.483 1.142 Total Organic

Carbon rank poor fair good fair good good fair good good Fair Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Sed-# = denotes sampling location number SQT = sediment quality triad

Table 7. Overall SQT Score for Sediment Chemistry Characterization for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10Sediment Guideline Exceedances poor fair poor poor fair poor fair poor poor good

ER-Mq poor good good poor good good good good good good Total Organic Carbon poor fair good fair good good fair good good fair Average Overall SQT Score for Sediment Guidelines poor fair fair poor good fair fair fair fair Good An average Score of less than 1.75 = poor, >=1.75 and <2.5 = fair and >=2.5 = good. Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Percent fines were not included in the calculation of the Overall SQT Rank for Sediment Guidelines because it is unlikely that the variation in percent fines affected the sediment toxicity.

Sed-# = denotes sampling location number ER-Mq = effects range-median quotient SQT = sediment quality triad

Table 8. Overall SQT Rank for Sediment Toxicity for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10 Mean % Survival 86 63 84 65 57 73 71 79 71 72 OVERALL SQT Rank for Sediment Toxicity fair poor fair poor poor poor fair poor poor Fair Highlighted values are significantly lower than their respective controls and were ranked as poor. Poor and fair rankings were assigned a value of 1 or 2, respectively for subsequent calculations.


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Figures and Tables

- 36 -

Table 9. Summary of Species Richness (number of species) and Abundance (number of individuals) for major taxa for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10 Total

Taxon

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

l Abu

ndan

ce

# of

Spe

cies

Tota

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ndan

ce

# of

Spe

cies

Tota

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ndan

ce

# of

Spe

cies

Tota

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ndan

ce

# of

Spe

cies

Tota

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Crustaceans 9 157 6 199 8 194 8 420 5 176 4 232 9 292 8 248 8 316 5 128 22 2362Fish 1 2 1 2Minor Phyla 2 3 2 6 3 8 1 4 3 60 2 8 1 28 1 20 6 137Molluscs 7 1331 10 172 6 316 5 168 5 144 6 208 5 298 4 520 7 1404 5 508 17 5069Polychaetes 6 210 13 153 9 598 9 1228 10 236 14 2072 9 194 11 500 19 1052 7 34 27 6277

Total 24 1701 31 530 26 1116 23 1820 20 556 27 2572 24 786 25 1276 35 2800 18 690 73 13847Sed-# = denotes sampling location number

Table 10. Biodiversity Indicators with standardized values (1-10 scale) in parentheses for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10Species Richness 24 (4) 31 (8) 26 (5) 23 (3) 20 (1) 27 (5) 24 (4) 25 (4) 35 (10) 18 (0)

ShannonWeiner Index (H’) 1.76 (5) 2.39 (9) 2.48 (10) 1.99 (6) 2.33 (9) 2.15 (8) 2.21 (8) 2.28 (9) 2.24 (8) 1.13 (0) Simpson Diversity Index

(D') 0.76 (6) 0.73 (8) 0.72 (7) 0.70 (5) 0.73 (6) 0.71 (6) 0.72 (6) 0.69 (6) 0.70 (8) 0.63 (0)

Combined Index Ranking 6.0 8.0 7.0 5.0 6.0 6.0 6.0 6.0 8.0 0.0 Biodiversity Sediment

Quality Rank fair good good fair fair fair fair fair good poor A Score of less than 3 is poor; >=3 and <=6 is fair; and >6 is good.


Table 11. SQT Rank for Relative Benthic Index for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10Relative Benthic Index 0.00 0.54 0.24 0.18 0.09 0.11 0.42 0.39 1.00 0.56

Relative Benthic Index Sediment Quality Rank

poor good poor poor poor poor fair fair good good

An index <=0.3 is poor, between 0.3 and 0.5 is fair, >=0.5 is good. Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.


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- 37 -

Table 12. SQT Rank for Proportional Abundance of Pollution Tolerant Indicator Species for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10

Pollution Tolerant Species 17% 55% 51% 76% 37% 25% 36% 31% 16% 1%

Other Species 83% 45% 49% 24% 63% 75% 64% 69% 84% 99% Proportional Abundance Sediment Quality Rank good poor poor poor fair good fair fair good good The ranking was assigned as follows: 0 to 25% good; 26 to 50% fair; 51 to 100% poor. Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.


Table 13. Overall SQT Rank for Benthic Community Indices for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10Biodiversity Sediment Quality Rank fair good good fair fair fair fair fair good poor

RBI Sediment Quality Rank poor good poor poor poor poor fair fair good good Proportional Abundance Sediment Quality Rank good poor poor poor fair good fair fair good good Overall SQT Rank for Benthic Community Indices fair fair fair poor fair fair fair fair good fair Poor, fair and good rankings were assigned a value of 1, 2, or 3 respectively for “scoring” of individual measures. An average score of less than 1.5 = poor, >=1.5 and <2.5 = fair and >=2.5 = good. Poor, fair and good rankings were assigned a value of 1, 2, or 3, respectively for subsequent calculations.

Sed-# = denotes sampling location number RBI: Relative Benthic Index SQT = sediment quality triad

Table 14. Overall Sediment Quality Triad Assessment Rank for the Paradise Marsh Contaminants Investigation, San Diego, CA.

SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-10SQT Rank for Sediment Chemistry Guidelines poor fair fair poor good fair fair fair fair good SQT Rank for Bulk Sediment Toxicity fair poor fair poor poor poor fair poor poor fair SQT Rank for Benthic Community Indices fair fair fair poor fair fair fair fair good fair

Overall SQT Ranking poor poor fair poor fair poor fair poor fair fair Poor, fair and good rankings were assigned a value of 1, 2, or 3 respectively for calculations. A Score of less than 1.75 = poor, >=1.75 and <2.5 = fair and >=2.5 = good.


OU 1 001223

Figures and Tables

- 38 -

Table 15. Possible Contaminant Sources for the Paradise Marsh Contaminants Investigation, San Diego, CA.

Shipyard facilities in San Diego Bay Shipping activities in San Diego Bay Stormwater runoff into Paradise Creek – non-point Ash/Road material disposal (PAHs and metals) runoff into Paradise Creek – non-point Upstream agricultural and residential run-off into Paradise Creek – non-point Air deposition (including automobile emissions) from regional activities Redistribution of adjacent sediments from San Diego Bay Airport runoff from San Diego Bay Antifouling paints from San Diego Bay

Table 16. PAHs exceeding T20 (bolded italics) or T50 (gray highlight) Sediment Chemistry Guidelines for the Paradise Marsh Contaminants Investigation, San Diego, CA.

Analyte SED-1 SED-2 SED-3 SED-4 SED-5 SED-6 SED-7 SED-8 SED-9 SED-101-Methylnaphthalene 6.2 1.5 8.4 1.3 1.5 1.3 1-Methylphenanthrene 97.2 8.2 3.0 2.0 90.3 2,6-Dimethylnaphthalene 12.5 2.5 2.9 13.1 2.5 3.2 2.4 2-Methylnaphthalene 12.7 2.0 3.0 9.8 2.3 3.3 2.1 Acenaphthene 26.0 1.5 1.7 3.7 1.4 1.5 Acenaphthylene 6.4 1.2 23.3 1.3 Anthracene 111.0 4.2 6.5 3.1 27.2 4.2 6.0 Benz[a]anthracene 1930.0 44.3 77.4 36.6 10.9 308.0 43.1 62.4 10.7 5.30 Benzo[a]pyrene 3340.0 70.6 152.0 56.6 23.5 450.0 80.5 129.0 16.0 8.10 Benzo[b]fluoranthene 2560.0 55.8 128.0 46.8 17.6 279.0 68.4 115.0 21.2 7.00 Benzo[g,h,i]perylene 2110.0 57.0 120.0 42.8 15.8 321.0 61.2 119.0 20.0 6.40 Benzo[k]fluoranthene 2450.0 54.3 114.0 43.5 19.0 275.0 59.6 98.0 15.9 8.30 Biphenyl 5.5 1.6 3.6 7.1 1.9 1.9 2.5 Chrysene 1790.0 41.7 81.0 35.2 11.4 301.0 45.9 71.0 11.9 5.50 Dibenz[a,h]anthracene 726.0 30.3 15.6 72.7 30.4 Fluoranthene 2530.0 75.0 116.0 58.2 14.9 581.0 70.3 102.0 19.3 7.00 Fluorene 31.7 2.2 2.3 22.0 2.3 2.1 1.0 Indeno[1,2,3-c,d]pyrene 2480.0 58.3 129.0 48.4 17.6 326.0 56.5 119.0 16.9 Naphthalene 19.2 1.5 2.7 8.2 2.0 2.8 1.6 Perylene 810.0 20.4 32.6 13.2 5.2 70.0 19.8 29.8 Phenanthrene 685.0 21.2 29.7 17.5 3.9 616.0 14.4 24.5 6.6 Pyrene 2780.0 102.0 123.0 56.0 17.4 926.0 71.6 111.0 19.9 11.50 Total Detectable PAHs* 26098.2 664.5 1244.0 499.0 169.7 5010.7 656.4 1108.8 184.1 64.20 PEL and TEL guidelines were used for Total Detectable PAHs because T20 and T50 guidelines were not available. Sed-# = denotes sampling location number

PAH = Petroleum Aromatic Hydrocarbons T20 = denotes the probability that 20 percent of samples would be toxic T50 = denotes the probability that 50 percent of samples would be toxic PEL = probable effects level TEL = threshold effects level

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Appendix A Page A-39

Appendix A. Contractors Report

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Appendices

Appendix B – Raw Data Page B-56

Appendix B. Raw Data

Appendix B: Table 1. Pore Water Toxicity Test Results........................................................... 57 Appendix B: Table 2. Pore Water Toxicity Tests – Water Quality Results. ............................. 59 Appendix B: Table 3. Pore Water Toxicity Tests – Batch Information. ................................... 62 Appendix B: Table 4. Solid Phase Toxicity Tests – Results ..................................................... 62 Appendix B: Table 5. Solid Phase Toxicity Tests – Water Quality Results.............................. 65 Appendix B: Table 6. Solid Phase Toxicity Tests – Batch Information.................................... 72 Appendix B: Table 7. Infauna Test Results ............................................................................... 72 Appendix B: Table 8. Sediment Chemistry Results .................................................................. 78 Appendix B: Table 9. Sediment Chemistry – Batch Information............................................ 127 Appendix B: Table 10. Grain Size and Total Organic Carbon Results. .................................. 129

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*list of acronyms found at end of table Appendix B – Raw Data

Page B-57

This is a paragraph this is a paragraph Appendix B: Table 1. Pore Water Toxicity Test Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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0000 12-Aug-04 CNEG Paradise Marsh MEC DE NA NA FP 1 89 A 0000 12-Aug-04 CNEG Paradise Marsh MEC DE NA NA FP 2 95 A 0000 12-Aug-04 CNEG Paradise Marsh MEC DE NA NA FP 3 90 A 0000 12-Aug-04 CNEG Paradise Marsh MEC DE NA NA FP 4 91 A SED-1 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 43 A SED-1 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 46 A SED-1 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 38 A SED-1 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 45 A SED-2 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 65 A SED-2 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 62 A SED-2 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 69 A SED-2 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 52 A SED-3 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 84 A SED-3 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 90 A SED-3 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 78 A SED-3 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 91 A SED-4 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 75 A SED-4 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 77 A SED-4 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 93 A SED-4 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 82 A SED-5 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 60 A SED-5 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 62 A SED-5 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 61 A SED-5 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 76 A SED-6 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 51 A SED-6 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 73 A SED-6 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 56 A SED-6 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 73 A SED-7 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 77 A SED-7 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 68 A SED-7 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 79 A SED-7 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 71 A SED-8 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 11 A SED-8 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 21 A SED-8 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 44 A SED-8 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 41 A SED-9 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 38 A SED-9 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 29 A SED-9 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 35 A SED-9 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 33 A SED-10 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 1 42 A SED-10 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 2 41 A SED-10 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 3 45 A SED-10 12-Aug-04 RESULT Paradise Marsh MEC DE NA NA FP 4 56 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 0 ug/l FP 1 89 A

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Appendix B: Table 1. Pore Water Toxicity Test Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 0 ug/l FP 2 95 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 0 ug/l FP 3 90 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 0 ug/l FP 4 91 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 3.5 ug/l FP 1 68 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 3.5 ug/l FP 2 61 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 3.5 ug/l FP 3 89 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 7.5 ug/l FP 1 77 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 7.5 ug/l FP 2 63 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 7.5 ug/l FP 3 57 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 15 ug/l FP 1 48 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 15 ug/l FP 2 75 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 15 ug/l FP 3 63 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 30 ug/l FP 1 47 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 30 ug/l FP 2 55 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 30 ug/l FP 3 45 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 60 ug/l FP 1 50 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 60 ug/l FP 2 50 A 0000 12-Aug-04 RFCU Paradise Marsh CURT MEC DE 60 ug/l FP 3 38 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 0 mg/l FP 1 89 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 0 mg/l FP 2 95 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 0 mg/l FP 3 90 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 0 mg/l FP 4 91 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 6.25 mg/l FP 1 65 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 6.25 mg/l FP 2 58 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 6.25 mg/l FP 3 61 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 12.5 mg/l FP 1 58 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 12.5 mg/l FP 2 45 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 12.5 mg/l FP 3 43 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 25 mg/l FP 1 42 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 25 mg/l FP 2 28 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 25 mg/l FP 3 46 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 50 mg/l FP 1 27 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 50 mg/l FP 2 37 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 50 mg/l FP 3 25 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 100 mg/l FP 1 29 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 100 mg/l FP 2 28 A 0000 12-Aug-04 RFNH3 Paradise Marsh NH3RT MEC DE 100 mg/l FP 3 38 A A = Acceptable data for analysis CU = Copper DE = Dendraster excentricus FP = fertilization product MEC = MEC Analytical Systems, Inc. mg/l = milligrams per liter NA = not applicable

NH3 = Ammonia QA = Quality Assurance RT or RF = Reference Toxicant Sampling Location 0000 = Reference Sample Sed-# = sampling location number ug/l = microgram per liter

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Appendix B: Table 2. Pore Water Toxicity Tests – Water Quality Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA DO None 8.8 mg/l MEC 0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA NH3T < 0.1 mg/l MEC 0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA NH3U < 0.003 mg/l MEC 0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA pH None 8.1 pH MEC 0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CNEG SEAWATER NA NA NA TEMP None 15.5 C MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 2.7 mg/l MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 12.7 mg/l MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.146 mg/l MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.73 pH MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-1 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 15.8 C MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.3 mg/l MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 7.65 mg/l MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.089 mg/l MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.7 pH MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-2 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.1 mg/l MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 9.15 mg/l MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.087 mg/l MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.61 pH MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-3 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.2 mg/l MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 11.4 mg/l MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.119 mg/l MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.65 pH MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-4 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.2 mg/l MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 7.9 mg/l MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0 mg/l MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 0.072 pH MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-5 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 15.8 C MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.3 mg/l MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 11.1 mg/l MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.102 mg/l MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.58 pH MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 37 ppt MEC SED-6 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 15.9 C MEC SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.2 mg/l MEC SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 8.61 mg/l MEC SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.08 mg/l MEC SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.59 pH MEC SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC

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SED-7 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 1.6 mg/l MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 12.4 mg/l MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.073 mg/l MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.43 pH MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-8 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 2.6 mg/l MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 26.9 mg/l MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.158 mg/l MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.36 pH MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 36 ppt MEC SED-9 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA DO None 8.1 mg/l MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3T None 5.74 mg/l MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA NH3U None 0.038 mg/l MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA pH None 7.49 pH MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA SAL None 52 ppt MEC SED-10 12-Aug-04 Paradise Marsh RESULT SEAWATER 1 NA NA TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 0 ug/l DO None 8.8 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 0 ug/l pH None 8.1 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 0 ug/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 0 ug/l TEMP None 15.5 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 3.5 ug/l DO None 9.1 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 3.5 ug/l pH None 8.09 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 3.5 ug/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 3.5 ug/l TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 7.5 ug/l DO None 9.2 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 7.5 ug/l pH None 8.1 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 7.5 ug/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 7.5 ug/l TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 15 ug/l DO None 9.3 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 15 ug/l pH None 8.11 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 15 ug/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 15 ug/l TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 30 ug/l DO None 9.4 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 30 ug/l pH None 8.11 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 30 ug/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 30 ug/l TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 60 ug/l DO None 9.5 mg/l MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 60 ug/l pH None 8.11 pH MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 60 ug/l SAL None 30 ppt MEC 0000 12-Aug-04 Paradise Marsh CURT RFCU RT NA 60 ug/l TEMP None 15.4 C MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l DO None 8.8 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l NH3T < 0.1 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l NH3U < 0.003 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l pH None 8.1 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 0 mg/l TEMP None 15.5 C MEC

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0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l DO None 9.2 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l NH3T None 9.92 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l NH3U None 0.236 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l pH None 8.04 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 6.25 mg/l TEMP None 16 C MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l DO None 9.2 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l NH3T None 12.1 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l NH3U None 0.286 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l pH None 8.04 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 12.5 mg/l TEMP None 15.9 C MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l DO None 9.4 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l NH3T None 25.4 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l NH3U None 0.599 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l pH None 8.01 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 25 mg/l TEMP None 15.9 C MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l DO None 9.4 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l NH3T None 52.5 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l NH3U None 1.239 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l pH None 7.94 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 50 mg/l TEMP None 15.9 C MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l DO None 9.3 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l NH3T None 90.1 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l NH3U None 1.343 mg/l MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l pH None 7.83 pH MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l SAL None 31 ppt MEC 0000 12-Aug-04 Paradise Marsh NH3RT RFNH3 RT NA 100 mg/l TEMP None 15.8 C MEC C = Celsius CNEG = Lab Negative Control CU = Copper DE = Dendraster excentricus DO = Dissolved Oxygen FP = Fertilization Product H2S = Hydrogen Sulfide MEC = MEC Analytical Systems, Inc. mg/l = milligrams per liter NA = Not Applicable NH3 = Ammonia

NH3T = Total Ammonia NH3U = Unionized Ammonia ppt = parts per thousand QA = Quality Assurance RF or RT = Reference Toxicant SAL = Salinity Sampling Location 0000 = Reference Sample Sed-# = sampling location number ST = Total Sulfide TEMP = Temperature ug/l = microgram per liter

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Appendix B: Table 3. Pore Water Toxicity Tests – Batch Information for the Paradise Marsh Contaminants Investigation, San Diego, CA.*

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Paradise Marsh MEC DE EPA 1995 12/Aug/2004 SEAWATER 0.33 HOURS 15

Paradise Marsh CURT MEC DE EPA 1995 12/Aug/2004 RT 0.33 HOURS 15

Paradise Marsh NH3RT MEC DE EPA 1995 12/Aug/2004 RT 0.33 HOURS 15 C = Celsius DE = Dendraster excentricus MEC = MEC Analytical Systems, Inc. NH3 = Ammonia RT = Reference Toxicant

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Appendix B: Table 4. Solid Phase Toxicity Tests – Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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0000 CNEG Paradise Marsh MEC EE NA PERCENT SP 1 100 A 0000 CNEG Paradise Marsh MEC EE NA PERCENT SP 2 90 A 0000 CNEG Paradise Marsh MEC EE NA PERCENT SP 3 100 A 0000 CNEG Paradise Marsh MEC EE NA PERCENT SP 4 85 A 0000 CNEG Paradise Marsh MEC EE NA PERCENT SP 5 95 A SED-1 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 85 A SED-1 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 100 A SED-1 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 90 A SED-1 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 60 A SED-1 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 95 A SED-2 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 60 A SED-2 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 65 A SED-2 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 65 A SED-2 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 85 A SED-2 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 40 A SED-3 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 85 A SED-3 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 90 A SED-3 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 95 A SED-3 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 90 A SED-3 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 60 A SED-4 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 60 A SED-4 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 70 A SED-4 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 60 A SED-4 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 70 A SED-4 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 65 A

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SED-5 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 30 A SED-5 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 55 A SED-5 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 50 A SED-5 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 75 A SED-5 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 75 A SED-6 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 75 A SED-6 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 90 A SED-6 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 75 A SED-6 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 65 A SED-6 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 60 A SED-7 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 100 A SED-7 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 60 A SED-7 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 70 A SED-7 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 55 A SED-7 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 70 A SED-8 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 70 A SED-8 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 90 A SED-8 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 75 A SED-8 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 75 A SED-8 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 85 A SED-9 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 75 A SED-9 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 65 A SED-9 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 60 A SED-9 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 80 A SED-9 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 75 A SED-10 RESULT Paradise Marsh MEC EE NA PERCENT SP 1 0 A SED-10 RESULT Paradise Marsh MEC EE NA PERCENT SP 2 80 A SED-10 RESULT Paradise Marsh MEC EE NA PERCENT SP 3 95 A SED-10 RESULT Paradise Marsh MEC EE NA PERCENT SP 4 100 A SED-10 RESULT Paradise Marsh MEC EE NA PERCENT SP 5 85 A 0000 RFCD Paradise Marsh RFCD MEC EE 0 mg/l SP 1 100 A 0000 RFCD Paradise Marsh RFCD MEC EE 0 mg/l SP 2 100 A 0000 RFCD Paradise Marsh RFCD MEC EE 0 mg/l SP 3 90 A 0000 RFCD Paradise Marsh RFCD MEC EE 2.5 mg/l SP 1 60 A 0000 RFCD Paradise Marsh RFCD MEC EE 2.5 mg/l SP 2 50 A 0000 RFCD Paradise Marsh RFCD MEC EE 2.5 mg/l SP 3 60 A 0000 RFCD Paradise Marsh RFCD MEC EE 5 mg/l SP 1 20 A 0000 RFCD Paradise Marsh RFCD MEC EE 5 mg/l SP 2 40 A 0000 RFCD Paradise Marsh RFCD MEC EE 5 mg/l SP 3 40 A 0000 RFCD Paradise Marsh RFCD MEC EE 10 mg/l SP 1 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 10 mg/l SP 2 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 10 mg/l SP 3 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 20 mg/l SP 1 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 20 mg/l SP 2 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 20 mg/l SP 3 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 40 mg/l SP 1 0 A 0000 RFCD Paradise Marsh RFCD MEC EE 40 mg/l SP 2 0 A

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0000 RFCD Paradise Marsh RFCD MEC EE 40 mg/l SP 3 0 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 0 mg/l SP 1 90 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 0 mg/l SP 2 80 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 0 mg/l SP 3 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 15.625 mg/l SP 1 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 15.625 mg/l SP 2 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 15.625 mg/l SP 3 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 31.25 mg/l SP 1 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 31.25 mg/l SP 2 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 31.25 mg/l SP 3 100 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 62.5 mg/l SP 1 80 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 62.5 mg/l SP 2 80 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 62.5 mg/l SP 3 80 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 125 mg/l SP 1 10 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 125 mg/l SP 2 10 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 125 mg/l SP 3 0 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 250 mg/l SP 1 0 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 250 mg/l SP 2 0 A 0000 RFNH3 Paradise Marsh RFNH3 MEC EE 250 mg/l SP 3 0 A A = Acceptable data for analysis CNEG = Lab Negative Control EE = Eohaustorius estuariusMEC = MEC Analytical Systems, Inc. mg/l = milligrams per liter NA = Not Applicable NH3 = Ammonia

QA = Quality Assurance Sed-# = sampling location number RF or RT = Reference Toxicant CD = Cadmium Sampling Location 0000 = Reference Sample SP = Survival Percent

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Appendix B: Table 5. Solid Phase Toxicity Tests – Water Quality Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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0000 Paradise Marsh MEC OL NA NA 0 DO None 8.9 mg/l 0 0000 Paradise Marsh MEC OL NA NA 0 TEMP None 17.2 C 0 0000 Paradise Marsh MEC OL NA NA 0 SAL None 22.1 PPT 0 0000 Paradise Marsh MEC OL NA NA 0 pH None 8.0 pH 0 0000 Paradise Marsh MEC OL NA NA 0 NH3T None 0.115 mg/l 0 0000 Paradise Marsh MEC IW NA NA 0 NH3T None 0.107 mg/l 0 0000 Paradise Marsh MEC OL NA NA 0 NH3U None 0.003 mg/l 0 0000 Paradise Marsh MEC IW NA NA 0 NH3U None 0.001 mg/l 0 0000 Paradise Marsh MEC IW NA NA 0 SAL None 25.0 PPT 0 0000 Paradise Marsh MEC IW NA NA 0 pH None 7.4 pH 0 0000 Paradise Marsh MEC OL NA NA 10 DO None 7.9 mg/l 0 0000 Paradise Marsh MEC OL NA NA 10 TEMP None 17.0 C 0 0000 Paradise Marsh MEC OL NA NA 10 SAL None 22.2 PPT 0 0000 Paradise Marsh MEC OL NA NA 10 pH None 8.2 pH 0 0000 Paradise Marsh MEC OL NA NA 10 NH3T None 0.450 mg/l 00000 Paradise Marsh MEC IW NA NA 10 NH3T None 0.342 mg/l 00000 Paradise Marsh MEC OL NA NA 10 NH3U None 0.019 mg/l 00000 Paradise Marsh MEC IW NA NA 10 NH3U None 0.004 mg/l 00000 Paradise Marsh MEC IW NA NA 10 SAL None 22.0 PPT 0 0000 Paradise Marsh MEC IW NA NA 10 pH None 7.6 pH 0 SED-1 Paradise Marsh MEC OL NA NA 0 DO None 8.5 mg/l 0 SED-1 Paradise Marsh MEC OL NA NA 0 TEMP None 17.1 C 0 SED-1 Paradise Marsh MEC OL NA NA 0 SAL None 22.4 PPT 0 SED-1 Paradise Marsh MEC OL NA NA 0 pH None 8.0 pH 0 SED-1 Paradise Marsh MEC OL NA NA 0 NH3T None 0.214 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 0 NH3T None 4.330 mg/l 0SED-1 Paradise Marsh MEC OL NA NA 0 NH3U None 0.006 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 0 NH3U None 0.029 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 0 SAL None 31.0 PPT 0 SED-1 Paradise Marsh MEC IW NA NA 0 pH None 7.4 pH 0 SED-1 Paradise Marsh MEC OL NA NA 10 DO None 7.5 mg/l 0 SED-1 Paradise Marsh MEC OL NA NA 10 TEMP None 16.9 C 0 SED-1 Paradise Marsh MEC OL NA NA 10 SAL None 23.3 PPT 0 SED-1 Paradise Marsh MEC OL NA NA 10 pH None 8.2 pH 0 SED-1 Paradise Marsh MEC OL NA NA 10 NH3T None 1.730 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 10 NH3T None 3.060 mg/l 0SED-1 Paradise Marsh MEC OL NA NA 10 NH3U None 0.072 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 10 NH3U None 0.041 mg/l 0SED-1 Paradise Marsh MEC IW NA NA 10 SAL None 25.0 PPT 0 SED-1 Paradise Marsh MEC IW NA NA 10 pH None 7.7 pH 0 SED-2 Paradise Marsh MEC OL NA NA 0 DO None 8.9 mg/l 0 SED-2 Paradise Marsh MEC OL NA NA 0 TEMP None 17.0 C 0 SED-2 Paradise Marsh MEC OL NA NA 0 SAL None 22.0 PPT 0 SED-2 Paradise Marsh MEC OL NA NA 0 pH None 8.0 pH 0 SED-2 Paradise Marsh MEC OL NA NA 0 NH3T None 0.227 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 0 NH3T None 3.920 mg/l 0SED-2 Paradise Marsh MEC OL NA NA 0 NH3U None 0.006 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 0 NH3U None 0.032 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 0 SAL None 31.0 PPT 0

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SED-2 Paradise Marsh MEC IW NA NA 0 pH None 7.5 pH 0 SED-2 Paradise Marsh MEC OL NA NA 10 DO None 7.8 mg/l 0 SED-2 Paradise Marsh MEC OL NA NA 10 TEMP None 17.4 C 0 SED-2 Paradise Marsh MEC OL NA NA 10 SAL None 23.2 PPT 0 SED-2 Paradise Marsh MEC OL NA NA 10 pH None 8.5 pH 0 SED-2 Paradise Marsh MEC OL NA NA 10 NH3T None 1.020 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 10 NH3T None 2.530 mg/l 0SED-2 Paradise Marsh MEC OL NA NA 10 NH3U None 0.084 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 10 NH3U None 0.044 mg/l 0SED-2 Paradise Marsh MEC IW NA NA 10 SAL None 24.0 PPT 0 SED-2 Paradise Marsh MEC IW NA NA 10 pH None 7.8 pH 0 SED-3 Paradise Marsh MEC OL NA NA 0 DO None 8.8 mg/l 0 SED-3 Paradise Marsh MEC OL NA NA 0 TEMP None 17.2 C 0 SED-3 Paradise Marsh MEC OL NA NA 0 SAL None 22.0 PPT 0 SED-3 Paradise Marsh MEC OL NA NA 0 pH None 8.0 pH 0 SED-3 Paradise Marsh MEC OL NA NA 0 NH3T None 0.211 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 0 NH3T None 4.060 mg/l 0SED-3 Paradise Marsh MEC OL NA NA 0 NH3U None 0.006 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 0 NH3U None 0.042 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 0 SAL None 32.0 PPT 0 SED-3 Paradise Marsh MEC IW NA NA 0 pH None 7.6 pH 0 SED-3 Paradise Marsh MEC OL NA NA 10 DO None 7.8 mg/l 0 SED-3 Paradise Marsh MEC OL NA NA 10 TEMP None 16.9 C 0 SED-3 Paradise Marsh MEC OL NA NA 10 SAL None 23.6 PPT 0 SED-3 Paradise Marsh MEC OL NA NA 10 pH None 8.5 pH 0 SED-3 Paradise Marsh MEC OL NA NA 10 NH3T None 1.450 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 10 NH3T None 2.900 mg/l 0SED-3 Paradise Marsh MEC OL NA NA 10 NH3U None 0.115 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 10 NH3U None 0.049 mg/l 0SED-3 Paradise Marsh MEC IW NA NA 10 SAL None 25.0 PPT 0 SED-3 Paradise Marsh MEC IW NA NA 10 pH None 7.8 pH 0 SED-4 Paradise Marsh MEC OL NA NA 0 DO None 8.5 mg/l 0 SED-4 Paradise Marsh MEC OL NA NA 0 TEMP None 17.2 C 0 SED-4 Paradise Marsh MEC OL NA NA 0 SAL None 21.9 PPT 0 SED-4 Paradise Marsh MEC OL NA NA 0 pH None 8.0 pH 0 SED-4 Paradise Marsh MEC OL NA NA 0 NH3T None 0.209 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 0 NH3T None 4.410 mg/l 0SED-4 Paradise Marsh MEC OL NA NA 0 NH3U None 0.006 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 0 NH3U None 0.046 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 0 SAL None 32.0 PPT 0 SED-4 Paradise Marsh MEC IW NA NA 0 pH None 7.6 pH 0 SED-4 Paradise Marsh MEC OL NA NA 10 DO None 7.8 mg/l 0 SED-4 Paradise Marsh MEC OL NA NA 10 TEMP None 17.0 C 0 SED-4 Paradise Marsh MEC OL NA NA 10 SAL None 23.3 PPT 0 SED-4 Paradise Marsh MEC OL NA NA 10 pH None 8.4 pH 0 SED-4 Paradise Marsh MEC OL NA NA 10 NH3T None 1.300 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 10 NH3T None 2.600 mg/l 0SED-4 Paradise Marsh MEC OL NA NA 10 NH3U None 0.084 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 10 NH3U None 0.035 mg/l 0SED-4 Paradise Marsh MEC IW NA NA 10 SAL None 24.0 PPT 0

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SED-9 Paradise Marsh MEC IW NA NA 10 pH None 7.5 pH 0 SED-10 Paradise Marsh MEC OL NA NA 0 DO None 8.5 mg/l 0 SED-10 Paradise Marsh MEC OL NA NA 0 TEMP None 17.3 C 0 SED-10 Paradise Marsh MEC OL NA NA 0 SAL None 22.4 PPT 0 SED-10 Paradise Marsh MEC OL NA NA 0 pH None 8.1 pH 0 SED-10 Paradise Marsh MEC OL NA NA 0 NH3T None 0.239 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 0 NH3T None 3.120 mg/l 0SED-10 Paradise Marsh MEC OL NA NA 0 NH3U None 0.008 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 0 NH3U None 0.012 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 0 SAL None 43.0 PPT 0 SED-10 Paradise Marsh MEC IW NA NA 0 pH None 7.2 pH 0 SED-10 Paradise Marsh MEC OL NA NA 10 DO None 7.0 mg/l 0 SED-10 Paradise Marsh MEC OL NA NA 10 TEMP None 17.4 C 0 SED-10 Paradise Marsh MEC OL NA NA 10 SAL None 25.6 PPT 0 SED-10 Paradise Marsh MEC OL NA NA 10 pH None 8.4 pH 0 SED-10 Paradise Marsh MEC OL NA NA 10 NH3T None 0.850 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 10 NH3T None 3.560 mg/l 0SED-10 Paradise Marsh MEC OL NA NA 10 NH3U None 0.056 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 10 NH3U None 0.048 mg/l 0SED-10 Paradise Marsh MEC IW NA NA 10 SAL None 28.0 PPT 0 SED-10 Paradise Marsh MEC IW NA NA 10 pH None 7.7 pH 0 0000 Paradise Marsh RFCD MEC OL 0 mg/l 0 DO None 7.8 mg/l 00000 Paradise Marsh RFCD MEC OL 0 mg/l 0 TEMP None 16.8 C 00000 Paradise Marsh RFCD MEC OL 0 mg/l 0 SAL None 21.2 PPT 00000 Paradise Marsh RFCD MEC OL 0 mg/l 0 pH None 8.1 pH 0 0000 Paradise Marsh RFCD MEC OL 0 mg/l 4 DO None 8.2 mg/l 10000 Paradise Marsh RFCD MEC OL 0 mg/l 4 TEMP None 16.2 C 10000 Paradise Marsh RFCD MEC OL 0 mg/l 4 SAL None 21.1 PPT 10000 Paradise Marsh RFCD MEC OL 0 mg/l 4 pH None 7.8 pH 10000 Paradise Marsh RFCD MEC OL 2.5 mg/l 0 DO None 7.7 mg/l 00000 Paradise Marsh RFCD MEC OL 2.5 mg/l 0 TEMP None 16.7 C 00000 Paradise Marsh RFCD MEC OL 2.5 mg/l 0 SAL None 21.3 PPT 00000 Paradise Marsh RFCD MEC OL 2.5 mg/l 0 pH None 8.1 pH 00000 Paradise Marsh RFCD MEC OL 2.5 mg/l 4 DO None 8.1 mg/l 10000 Paradise Marsh RFCD MEC OL 2.5 mg/l 4 TEMP None 16.0 C 10000 Paradise Marsh RFCD MEC OL 2.5 mg/l 4 SAL None 21.3 PPT 10000 Paradise Marsh RFCD MEC OL 2.5 mg/l 4 pH None 7.9 pH 10000 Paradise Marsh RFCD MEC OL 5 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFCD MEC OL 5 mg/l 0 TEMP None 16.6 C 00000 Paradise Marsh RFCD MEC OL 5 mg/l 0 SAL None 21.1 PPT 00000 Paradise Marsh RFCD MEC OL 5 mg/l 0 pH None 8.1 pH 00000 Paradise Marsh RFCD MEC OL 5 mg/l 4 DO None 8.2 mg/l 10000 Paradise Marsh RFCD MEC OL 5 mg/l 4 TEMP None 15.7 C 10000 Paradise Marsh RFCD MEC OL 5 mg/l 4 SAL None 21.3 PPT 10000 Paradise Marsh RFCD MEC OL 5 mg/l 4 pH None 7.9 pH 10000 Paradise Marsh RFCD MEC OL 10 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFCD MEC OL 10 mg/l 0 TEMP None 17.0 C 00000 Paradise Marsh RFCD MEC OL 10 mg/l 0 SAL None 21.0 PPT 00000 Paradise Marsh RFCD MEC OL 10 mg/l 0 pH None 8.1 pH 00000 Paradise Marsh RFCD MEC OL 10 mg/l 4 DO None 8.1 mg/l 2

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0000 Paradise Marsh RFCD MEC OL 10 mg/l 4 TEMP None 15.6 C 2 0000 Paradise Marsh RFCD MEC OL 10 mg/l 4 SAL None 21.3 PPT 2 0000 Paradise Marsh RFCD MEC OL 10 mg/l 4 pH None 7.9 pH 2 0000 Paradise Marsh RFCD MEC OL 20 mg/l 0 DO None 7.4 mg/l 00000 Paradise Marsh RFCD MEC OL 20 mg/l 0 TEMP None 17.0 C 0 0000 Paradise Marsh RFCD MEC OL 20 mg/l 0 SAL None 21.0 PPT 00000 Paradise Marsh RFCD MEC OL 20 mg/l 0 pH None 8.1 pH 0

0000 Paradise Marsh RFCD MEC OL 20 mg/l 4 DO NA NA.0 mg/l NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 20 mg/l 4 TEMP NA NA.0 C NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 20 mg/l 4 SAL NA NA.0 PPT NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 20 mg/l 4 pH NA NA.0 pH NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 40 mg/l 0 DO None 7.4 mg/l 00000 Paradise Marsh RFCD MEC OL 40 mg/l 0 TEMP None 17.0 C 0 0000 Paradise Marsh RFCD MEC OL 40 mg/l 0 SAL None 21.0 PPT 00000 Paradise Marsh RFCD MEC OL 40 mg/l 0 pH None 8.1 pH 0

0000 Paradise Marsh RFCD MEC OL 40 mg/l 4 DO NA NA mg/l NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 40 mg/l 4 TEMP NA NA C NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 40 mg/l 4 SAL NA NA PPT NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFCD MEC OL 40 mg/l 4 pH NA NA pH NA All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 TEMP None 17.1 C 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 SAL None 21.0 PPT 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 pH None 8.2 pH 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 NH3T None 0.140 mg/l 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 0 NH3U None 0.006 mg/l 00000 Paradise Marsh RFNH3 MEC OL 0 mg/l 4 DO None 8.0 mg/l 10000 Paradise Marsh RFNH3 MEC OL 0 mg/l 4 TEMP None 16.4 C 10000 Paradise Marsh RFNH3 MEC OL 0 mg/l 4 SAL None 21.3 PPT 10000 Paradise Marsh RFNH3 MEC OL 0 mg/l 4 pH None 8.0 pH 10000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 TEMP None 17.0 C 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 SAL None 21.1 PPT 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 pH None 8.1 pH 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 NH3T None 13.500 mg/l 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 0 NH3U None 0.458 mg/l 00000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 4 DO None 8.1 mg/l 10000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 4 TEMP None 16.4 C 10000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 4 SAL None 21.6 PPT 10000 Paradise Marsh RFNH3 MEC OL 15.625 mg/l 4 pH None 8.0 pH 10000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 TEMP None 16.8 C 00000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 SAL None 21.3 PPT 00000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 pH None 8.0 pH 00000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 NH3T None 26.300 mg/l 0

OU 1 001256

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Page B-71


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0000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 0 NH3U None 0.702 mg/l 00000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 4 DO None 7.9 mg/l 10000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 4 TEMP None 16.4 C 10000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 4 SAL None 21.4 PPT 10000 Paradise Marsh RFNH3 MEC OL 31.25 mg/l 4 pH None 8.0 pH 10000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 DO None 7.6 mg/l 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 TEMP None 17.0 C 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 SAL None 21.3 PPT 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 pH None 7.9 pH 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 NH3T None 63.9 mg/l 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 0 NH3U None 1.382 mg/l 00000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 4 DO None 8.0 mg/l 10000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 4 TEMP None 16.4 C 10000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 4 SAL None 21.6 PPT 10000 Paradise Marsh RFNH3 MEC OL 62.5 mg/l 4 pH None 8.0 pH 10000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 DO None 7.5 mg/l 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 TEMP None 17.0 C 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 SAL None 21.5 PPT 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 pH None 7.7 pH 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 NH3T None 134.0 mg/l 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 0 NH3U None 1.842 mg/l 00000 Paradise Marsh RFNH3 MEC OL 125 mg/l 4 DO None 8.2 mg/l 10000 Paradise Marsh RFNH3 MEC OL 125 mg/l 4 TEMP None 16.4 C 10000 Paradise Marsh RFNH3 MEC OL 125 mg/l 4 SAL None 21.9 PPT 10000 Paradise Marsh RFNH3 MEC OL 125 mg/l 4 pH None 8.0 pH 10000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 DO None 7.6 mg/l 00000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 TEMP None 16.8 C 00000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 SAL None 22.1 PPT 00000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 pH None 7.5 pH 00000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 NH3T None 274.0 mg/l 00000 Paradise Marsh RFNH3 MEC OL 250 mg/l 0 NH3U None 2.345 mg/l 0

0000 Paradise Marsh RFNH3 MEC OL 250 mg/l 4 DO NA NA mg/l 1All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFNH3 MEC OL 250 mg/l 4 TEMP NA NA C 1All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFNH3 MEC OL 250 mg/l 4 SAL NA NA PPT 1All Organisms Dead, Parameter not measured

0000 Paradise Marsh RFNH3 MEC OL 250 mg/l 4 pH NA NA pH 1All Organisms Dead, Parameter not measured

C = Celsius CD = Cadmium DO = Dissolved Oxygen IW = Interstitial Water C = Celsius

mg/l = milligrams per liter MEC = MEC Analytical Systems, Inc. NA = Not Applicable NH3 = Ammonia NH3T = Total Ammonia

NH3U = Unionized Ammonia OL =ppt = parts per thousand RF = Reference Toxicant SAL = Salinity

Sampling Location 0000 = Reference SampleSed-# = sampling location number TEMP = Temperature ug/l = microgram per liter

OU 1 001257

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Appendix B: Table 6. Solid Phase Toxicity Tests – Batch Information for the Paradise Marsh Contaminants Investigation, San Diego, CA.*

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MEC EE EPA 1994 27-Jul-2004 BS 10 Days 15 C A MEC EE EPA 1994 27-Jul-2004 BS 4 Days 15 C A MEC EE EPA 1994 27-Jul-2004 BS 4 Days 15 C A A = Acceptable data for analysis BS = Bulk Sediment C = Celsius EE = Eohaustorius estuarius EPA = Environmental Protection Agency MEC = MEC Analytical Systems, Inc.

Appendix B: Table 7. Infauna Test Results for the Paradise Marsh Contaminants Investigation, San Diego, CA.* (continued from previous page)

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SED 1 7/21/2004 Crustaceans Ampithoe cf sectimanus 3 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Ampithoe longimana 3 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Grandidierella japonica 120 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Mayerella acanthopoda 4 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Monocorophium insidiosum 4 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Monocorophium sp 1 Y MEC 1.0 mm SED 1 7/21/2004 Crustaceans Nebalia pugettensis Cmplx 1 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Paracerceis sculpta 1 MEC 1.0 mm SED 1 7/21/2004 Crustaceans Tethygenia opata 20 MEC 1.0 mm SED 1 7/21/2004 Minor Phyla Rhabdocoela 2 MEC 1.0 mm SED 1 7/21/2004 Minor Phyla Sipuncula 1 MEC 1.0 mm SED 1 7/21/2004 Molluscs Acteocina inculta 525 MEC 1.0 mm SED 1 7/21/2004 Molluscs Alia carinata 1 MEC 1.0 mm SED 1 7/21/2004 Molluscs Barleeia sp 20 MEC 1.0 mm SED 1 7/21/2004 Molluscs Bulla gouldiana 1 MEC 1.0 mm SED 1 7/21/2004 Molluscs Cerithidea californica 169 MEC 1.0 mm SED 1 7/21/2004 Molluscs Musculista senhousia 7 MEC 1.0 mm SED 1 7/21/2004 Molluscs Tryonia imitator 608 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Capitella capitata Cmplx 118 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Exogone verugera 4 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Neanthes acuminata Cmplx 1 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Oligochaeta 11 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Polydora nuchalis 28 MEC 1.0 mm SED 1 7/21/2004 Polychaetes Streblospio benedicti 48 MEC 1.0 mm SED 10 7/21/2004 Crustaceans Ampithoe longimana 2 MEC 1.0 mm SED 10 7/21/2004 Crustaceans Bemlos macromanus 2 MEC 1.0 mm

OU 1 001258

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SED 10 7/21/2004 Crustaceans Gammaridea 2 Y MEC 1.0 mm SED 10 7/21/2004 Crustaceans Nebalia pugettensis Cmplx 6 MEC 1.0 mm SED 10 7/21/2004 Crustaceans Paracerceis sculpta 116 MEC 1.0 mm SED 10 7/21/2004 Minor Phyla Diadumene sp 20 MEC 1.0 mm SED 10 7/21/2004 Molluscs Acteocina inculta 6 MEC 1.0 mm SED 10 7/21/2004 Molluscs Alia carinata 2 MEC 1.0 mm SED 10 7/21/2004 Molluscs Barleeia sp 486 MEC 1.0 mm SED 10 7/21/2004 Molluscs Haminoea vesicula 6 MEC 1.0 mm SED 10 7/21/2004 Molluscs Musculista senhousia 8 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Exogone verugera 2 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Neanthes acuminata Cmplx 6 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Oligochaeta 4 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Pseudopolydora paucibranchiata 2 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Streblosoma uncinatus 8 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Syllis (Typosyllis) sp 2 MEC 1.0 mm SED 10 7/21/2004 Polychaetes Terebellidae 10 Y MEC 1.0 mm SED 2 7/21/2004 Crustaceans Ampithoe longimana 1 MEC 1.0 mm SED 2 7/21/2004 Crustaceans Ampithoe sp 2 Y MEC 1.0 mm SED 2 7/21/2004 Crustaceans Anoplodactylus viridintestinalis 1 MEC 1.0 mm SED 2 7/21/2004 Crustaceans Grandidierella japonica 182 MEC 1.0 mm SED 2 7/21/2004 Crustaceans Leptochelia dubia 6 MEC 1.0 mm SED 2 7/21/2004 Crustaceans Monocorophium acherusicum 7 MEC 1.0 mm SED 2 7/21/2004 Minor Phyla Diadumene sp 1 MEC 1.0 mm SED 2 7/21/2004 Minor Phyla Phoronida 5 MEC 1.0 mm SED 2 7/21/2004 Molluscs Acteocina inculta 46 MEC 1.0 mm SED 2 7/21/2004 Molluscs Barleeia sp 7 MEC 1.0 mm SED 2 7/21/2004 Molluscs Cerithidea californica 49 MEC 1.0 mm SED 2 7/21/2004 Molluscs Cryptomya californica 1 MEC 1.0 mm SED 2 7/21/2004 Molluscs Musculista senhousia 36 MEC 1.0 mm SED 2 7/21/2004 Molluscs Oleo hansineensis 1 MEC 1.0 mm SED 2 7/21/2004 Molluscs Tagelus subteres 9 MEC 1.0 mm SED 2 7/21/2004 Molluscs Tellina sp 2 MEC 1.0 mm SED 2 7/21/2004 Molluscs Theora lubrica 1 MEC 1.0 mm SED 2 7/21/2004 Molluscs Tryonia imitator 20 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Capitella capitata Cmplx 10 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Cirratulidae 1 Y MEC 1.0 mm SED 2 7/21/2004 Polychaetes Cirriformia sp 5 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Exogone verugera 12 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Fabriciola limnicola 8 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Marphysa sp 2 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Megalomma pigmentum 3 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Naineris uncinata 2 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Oligochaeta 71 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Polydora nuchalis 5 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Pseudopolydora paucibranchiata 10 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Streblosoma uncinatus 2 MEC 1.0 mm SED 2 7/21/2004 Polychaetes Streblospio benedicti 22 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Ampithoe cf sectimanus 38 MEC 1.0 mm

OU 1 001259

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SED 3 7/21/2004 Crustaceans Ampithoe longimana 12 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Grandidierella japonica 70 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Mayerella acanthopoda 4 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Monocorophium acherusicum 14 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Paracerceis sculpta 2 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Podocerus fulamus 44 MEC 1.0 mm SED 3 7/21/2004 Crustaceans Tethygenia opata 10 MEC 1.0 mm SED 3 7/21/2004 Minor Phyla Nemertea 2 MEC 1.0 mm SED 3 7/21/2004 Minor Phyla Phoronida 2 MEC 1.0 mm SED 3 7/21/2004 Minor Phyla Sipuncula 4 MEC 1.0 mm SED 3 7/21/2004 Molluscs Acteocina inculta 78 MEC 1.0 mm SED 3 7/21/2004 Molluscs Barleeia sp 140 MEC 1.0 mm SED 3 7/21/2004 Molluscs Cerithidea californica 30 MEC 1.0 mm SED 3 7/21/2004 Molluscs Musculista senhousia 62 MEC 1.0 mm SED 3 7/21/2004 Molluscs Tagelus subteres 2 MEC 1.0 mm SED 3 7/21/2004 Molluscs Tellina sp 4 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Capitella capitata Cmplx 58 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Exogone verugera 50 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Marphysa sp 2 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Neanthes acuminata Cmplx 2 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Oligochaeta 162 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Polydora nuchalis 36 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Pseudopolydora paucibranchiata 2 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Streblosoma uncinatus 10 MEC 1.0 mm SED 3 7/21/2004 Polychaetes Streblospio benedicti 276 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Ampithoe longimana 4 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Grandidierella japonica 284 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Leptochelia dubia 4 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Mayerella acanthopoda 44 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Monocorophium acherusicum 48 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Nebalia pugettensis Cmplx 12 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Podocerus fulamus 4 MEC 1.0 mm SED 4 7/21/2004 Crustaceans Tethygenia opata 20 MEC 1.0 mm SED 4 7/21/2004 Minor Phyla Leptoplanidae 4 MEC 1.0 mm SED 4 7/21/2004 Molluscs Acteocina inculta 92 MEC 1.0 mm SED 4 7/21/2004 Molluscs Barleeia sp 20 MEC 1.0 mm SED 4 7/21/2004 Molluscs Chione fluctifraga 4 MEC 1.0 mm SED 4 7/21/2004 Molluscs Macoma sp 8 MEC 1.0 mm SED 4 7/21/2004 Molluscs Musculista senhousia 44 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Capitella capitata Cmplx 80 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Chaetozone sp 4 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Exogone verugera 80 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Marphysa sanguinea 4 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Marphysa sp 4 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Oligochaeta 776 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Polydora nuchalis 48 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Pseudopolydora paucibranchiata 4 MEC 1.0 mm SED 4 7/21/2004 Polychaetes Streblospio benedicti 228 MEC 1.0 mm

OU 1 001260

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SED 5 7/22/2004 Crustaceans Grandidierella japonica 144 MEC 1.0 mm SED 5 7/22/2004 Crustaceans Leptochelia dubia 16 MEC 1.0 mm SED 5 7/22/2004 Crustaceans Monocorophium acherusicum 4 MEC 1.0 mm SED 5 7/22/2004 Crustaceans Paracerceis sculpta 8 MEC 1.0 mm SED 5 7/22/2004 Crustaceans Pyromaia tuberculata 4 MEC 1.0 mm SED 5 7/22/2004 Molluscs Acteocina inculta 52 MEC 1.0 mm SED 5 7/22/2004 Molluscs Barleeia sp 24 MEC 1.0 mm SED 5 7/22/2004 Molluscs Macoma sp 16 MEC 1.0 mm SED 5 7/22/2004 Molluscs Musculista senhousia 40 MEC 1.0 mm SED 5 7/22/2004 Molluscs Tagelus subteres 12 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Capitella capitata Cmplx 4 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Cirriformia sp 4 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Exogone verugera 48 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Fabriciola limnicola 116 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Marphysa sp 4 Y MEC 1.0 mm SED 5 7/22/2004 Polychaetes Marphysa sp B 4 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Naineris uncinata 8 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Oligochaeta 36 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Streblosoma uncinatus 4 MEC 1.0 mm SED 5 7/22/2004 Polychaetes Streblospio benedicti 8 MEC 1.0 mm SED 6 7/22/2004 Crustaceans Grandidierella japonica 160 MEC 1.0 mm SED 6 7/22/2004 Crustaceans Leptochelia dubia 32 MEC 1.0 mm SED 6 7/22/2004 Crustaceans Monocorophium acherusicum 24 MEC 1.0 mm SED 6 7/22/2004 Crustaceans Monocorophium insidiosum 16 MEC 1.0 mm SED 6 7/22/2004 Minor Phyla Diadumene sp 4 MEC 1.0 mm SED 6 7/22/2004 Minor Phyla Nemertea 4 MEC 1.0 mm SED 6 7/22/2004 Minor Phyla Phoronida 52 MEC 1.0 mm SED 6 7/22/2004 Molluscs Acteocina inculta 32 MEC 1.0 mm SED 6 7/22/2004 Molluscs Barleeia sp 16 MEC 1.0 mm SED 6 7/22/2004 Molluscs Cerithidea californica 4 MEC 1.0 mm SED 6 7/22/2004 Molluscs Macoma sp 32 MEC 1.0 mm SED 6 7/22/2004 Molluscs Musculista senhousia 120 MEC 1.0 mm SED 6 7/22/2004 Molluscs Tryonia imitator 4 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Capitella capitata Cmplx 24 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Cirriformia sp 40 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Exogone verugera 724 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Fabriciola limnicola 732 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Marphysa sp 4 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Mediomastus sp 24 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Naineris uncinata 4 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Neanthes acuminata Cmplx 4 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Oligochaeta 312 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Pherusa capulata 4 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Polydora nuchalis 16 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Pseudopolydora paucibranchiata 48 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Streblosoma uncinatus 12 MEC 1.0 mm SED 6 7/22/2004 Polychaetes Streblospio benedicti 124 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Ampithoe longimana 10 MEC 1.0 mm

OU 1 001261

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SED 7 7/22/2004 Crustaceans Bemlos macromanus 2 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Grandidierella japonica 148 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Leptochelia dubia 2 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Mayerella acanthopoda 2 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Nebalia pugettensis Cmplx 102 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Paracerceis sculpta 4 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Podocerus fulamus 4 MEC 1.0 mm SED 7 7/22/2004 Crustaceans Tethygenia opata 18 MEC 1.0 mm SED 7 7/22/2004 Fish Gobiidae 2 MEC 1.0 mm SED 7 7/22/2004 Molluscs Barleeia sp 106 MEC 1.0 mm SED 7 7/22/2004 Molluscs Cerithidea californica 2 MEC 1.0 mm SED 7 7/22/2004 Molluscs Chione fluctifraga 2 MEC 1.0 mm SED 7 7/22/2004 Molluscs Macoma sp 4 MEC 1.0 mm SED 7 7/22/2004 Molluscs Musculista senhousia 184 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Capitella capitata Cmplx 10 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Cirriformia sp 24 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Exogone verugera 14 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Fabriciola limnicola 2 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Neanthes acuminata Cmplx 14 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Oligochaeta 112 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Pseudopolydora paucibranchiata 10 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Streblospio benedicti 6 MEC 1.0 mm SED 7 7/22/2004 Polychaetes Streblospio sp 1 2 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Ampithoe sp 12 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Bemlos macromanus 88 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Grandidierella japonica 68 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Heptacarpus sp 4 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Leptochelia dubia 24 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Nebalia pugettensis Cmplx 4 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Paracerceis sculpta 44 MEC 1.0 mm SED 8 7/22/2004 Crustaceans Podocerus fulamus 4 MEC 1.0 mm SED 8 7/22/2004 Minor Phyla Nemertea 4 MEC 1.0 mm SED 8 7/22/2004 Minor Phyla Phoronida 4 MEC 1.0 mm SED 8 7/22/2004 Molluscs Alia carinata 4 MEC 1.0 mm SED 8 7/22/2004 Molluscs Barleeia sp 64 MEC 1.0 mm SED 8 7/22/2004 Molluscs Macoma sp 28 MEC 1.0 mm SED 8 7/22/2004 Molluscs Musculista senhousia 424 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Capitella capitata Cmplx 40 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Chaetozone sp 4 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Cirriformia sp 36 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Fabriciola limnicola 36 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Mediomastus sp 12 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Naineris uncinata 76 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Oligochaeta 260 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Pherusa capulata 16 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Pseudopolydora paucibranchiata 8 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Streblospio benedicti 4 MEC 1.0 mm SED 8 7/22/2004 Polychaetes Timarete luxuriosa 8 MEC 1.0 mm

OU 1 001262

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SED 9 7/22/2004 Crustaceans Ampithoe longimana 8 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Anoplodactylus erectus 4 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Bemlos sp 4 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Grandidierella japonica 16 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Paracerceis sculpta 212 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Paranthura elegans 4 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Podocerus fulamus 4 MEC 1.0 mm SED 9 7/22/2004 Crustaceans Synaptotanais notabilis 64 MEC 1.0 mm SED 9 7/22/2004 Minor Phyla Diadumene sp 28 MEC 1.0 mm SED 9 7/22/2004 Molluscs Acteocina inculta 8 MEC 1.0 mm SED 9 7/22/2004 Molluscs Alia carinata 8 MEC 1.0 mm SED 9 7/22/2004 Molluscs Barleeia sp 68 MEC 1.0 mm SED 9 7/22/2004 Molluscs Crepidula dorsata 4 MEC 1.0 mm SED 9 7/22/2004 Molluscs Macoma sp 32 MEC 1.0 mm SED 9 7/22/2004 Molluscs Musculista senhousia 1248 MEC 1.0 mm SED 9 7/22/2004 Molluscs Mytilus galloprovincialis 36 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Capitella capitata Cmplx 20 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Cirriformia sp SD1 56 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Dipolydora sp 8 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Drilonereis sp 4 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Exogone verugera 64 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Fabriciola limnicola 16 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Harmothoe imbricata Cmplx 16 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Marphysa sp 24 Y MEC 1.0 mm SED 9 7/22/2004 Polychaetes Marphysa sp B 4 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Mediomastus sp 112 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Naineris uncinata 28 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Neanthes acuminata Cmplx 112 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Oligochaeta 264 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Pherusa capulata 4 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Polydora nuchalis 32 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Prionospio heterobranchia 12 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Pseudopolydora paucibranchiata 228 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Streblosoma uncinatus 28 MEC 1.0 mm SED 9 7/22/2004 Polychaetes Syllis (Typosyllis) sp 20 MEC 1.0 mm MEC = MEC Analytical Systems, Inc. mm = millimeter Sed-# = sampling location number sp = species

OU 1 001263

App

endi

ces

*lis

t of a

cron

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ound

at e

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f tab

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App

endi

x B

– R

aw D

ata

Page

B-7

8

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

3 QA

QC

B1 A

roclo

r 101

6 ND

ng

/dry g

1020

8/18/0

48/2

3/04

DI W

ater

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%18

993

QAQC

B1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 DI

Wate

r

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1899

3 QA

QC

B1 A

roclo

r 123

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

DI W

ater

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%18

993

QAQC

B1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 DI

Wate

r

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1899

3 QA

QC

B1 A

roclo

r 124

8 ND

ng

/dry g

1020

8/18/0

48/2

3/04

DI W

ater

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%18

993

QAQC

B1

Aro

clor 1

254

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 DI

Wate

r

Ar

oclor

PCB

s 11

097-

61-1

65 -

135%

1899

3 QA

QC

B1 A

roclo

r 126

0 ND

ng

/dry g

1020

8/18/0

48/2

3/04

DI W

ater

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%18

994

SED-

1 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%18

994

SED-

1 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%18

994

SED-

1 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%18

994

SED-

1 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%18

994

SED-

1 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%18

994

SED-

1 R1

Aro

clor 1

254

15

1ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

097-

61-1

65 -

135%

1899

4 SE

D-1

R1 A

roclo

r 126

0 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

096-

82-5

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 101

6 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

674-

11-2

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 122

1 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 123

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

141-

16-5

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 124

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 124

8 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

672-

29-6

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 125

4 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

097-

61-1

65 -

135%

1899

5 SE

D-2

R1 A

roclo

r 126

0 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

096-

82-5

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 101

6 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

674-

11-2

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 122

1 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 123

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

141-

16-5

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 124

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 124

8 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

672-

29-6

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 125

4

63.79

9999

24ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

097-

61-1

65 -

135%

1899

6 SE

D-3

R1 A

roclo

r 126

0 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

096-

82-5

65 -

135%

1899

7 SE

D-4

R2 A

roclo

r 101

6 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

674-

11-2

65 -

135%

1899

7 SE

D-4

R1 A

roclo

r 101

6 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

674-

11-2

65 -

135%

1899

7 SE

D-4

R2 A

roclo

r 122

1 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1899

7 SE

D-4

R1 A

roclo

r 122

1 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1899

7 SE

D-4

R2 A

roclo

r 123

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

141-

16-5

65 -

135%

1899

7 SE

D-4

R1 A

roclo

r 123

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

141-

16-5

65 -

135%

1899

7 SE

D-4

R2 A

roclo

r 124

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1899

7 SE

D-4

R1 A

roclo

r 124

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1899

7 SE

D-4

R2 A

roclo

r 124

8 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

672-

29-6

65 -

135%

1899

7 SE

D-4

R1 A

roclo

r 124

8 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 12

672-

29-6

65 -

135%

OU 1 001264

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-7

9

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R2 A

roclo

r 125

4

26.5

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%18

997

SED-

4 R1

Aro

clor 1

254

E18

.7999

9924

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%18

997

SED-

4 R2

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%18

997

SED-

4 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%18

998

SED-

5 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%18

998

SED-

5 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%18

998

SED-

5 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%18

998

SED-

5 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%18

998

SED-

5 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%18

998

SED-

5 R1

Aro

clor 1

254

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%18

998

SED-

5 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%18

999

SED-

6 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%18

999

SED-

6 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%18

999

SED-

6 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%18

999

SED-

6 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%18

999

SED-

6 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%18

999

SED-

6 R1

Aro

clor 1

254

E19

.7000

0076

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%18

999

SED-

6 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%19

000

SED-

7 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%19

000

SED-

7 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%19

000

SED-

7 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%19

000

SED-

7 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%19

000

SED-

7 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%19

000

SED-

7 R1

Aro

clor 1

254

E17

.2999

9924

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%19

000

SED-

7 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%19

001

SED-

8 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%19

001

SED-

8 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%19

001

SED-

8 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%19

001

SED-

8 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%19

001

SED-

8 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%19

001

SED-

8 R1

Aro

clor 1

254

E16

.7000

0076

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%19

001

SED-

8 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%19

002

SED-

9 R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%19

002

SED-

9 R1

Aro

clor 1

221

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1110

4-28

-265

- 13

5%19

002

SED-

9 R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%19

002

SED-

9 R1

Aro

clor 1

242

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

5346

9-21

-965

- 13

5%19

002

SED-

9 R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%19

002

SED-

9 R1

Aro

clor 1

254

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

7-61

-165

- 13

5%19

002

SED-

9 R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%

OU 1 001265

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

0

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

R1

Aro

clor 1

016

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

4-11

-265

- 13

5%19

003

SED-

10

R1 A

roclo

r 122

1 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

104-

28-2

65 -

135%

1900

3 SE

D-10

R1

Aro

clor 1

232

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1114

1-16

-565

- 13

5%19

003

SED-

10

R1 A

roclo

r 124

2 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 53

469-

21-9

65 -

135%

1900

3 SE

D-10

R1

Aro

clor 1

248

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1267

2-29

-665

- 13

5%19

003

SED-

10

R1 A

roclo

r 125

4 ND

ng

/dry g

1020

8/18/0

48/2

3/04

Sedim

ent

Ar

oclor

PCB

s 11

097-

61-1

65 -

135%

1900

3 SE

D-10

R1

Aro

clor 1

260

ND

ng/dr

y g10

208/1

8/04

8/23/0

4 Se

dimen

t

Aroc

lor P

CBs

1109

6-82

-565

- 13

5%18

993

QAQC

B1

(PC

B030

)

59%

Rec

over

y

8/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

46

- 11

9%18

993

QAQC

B1

(PC

B112

)

73%

Rec

over

y

8/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

52

- 12

3%18

993

QAQC

B1

(PC

B198

)

80%

Rec

over

y

8/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

59

- 12

3%18

993

QAQC

B1

(TC

MX)

50

% R

ecov

ery

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

3 QA

QC

B1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

3 QA

QC

B1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%18

993

QAQC

B1

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%18

993

QAQC

B1

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%18

993

QAQC

B1

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%18

993

QAQC

B1

4,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

993

QAQC

B1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%18

993

QAQC

B1

BHC

-alph

a ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

993

QAQC

B1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%18

993

QAQC

B1

BHC

-delt

a ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

993

QAQC

B1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1899

3 QA

QC

B1 C

hlord

ane-

alpha

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

3 QA

QC

B1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1899

3 QA

QC

B1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%18

993

QAQC

B1

End

osulf

an S

ulfate

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1899

3 QA

QC

B1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%18

993

QAQC

B1

End

osulf

an-II

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1899

3 QA

QC

B1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%18

993

QAQC

B1

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%18

993

QAQC

B1

End

rin K

etone

ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

3 QA

QC

B1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1899

3 QA

QC

B1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

3 QA

QC

B1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%18

993

QAQC

B1

Mire

x ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

3 QA

QC

B1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

18

993

QAQC

B1

Tox

aphe

ne

ND

ng/dr

y g10

508/1

6/04

8/24/0

4 DI

Wate

r

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%18

993

QAQC

B1

tran

s-Non

achlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

DI W

ater

ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

4 SE

D-1

R1 (

PCB0

30)

10

0%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

OU 1 001266

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

1

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

4 SE

D-1

R1 (

PCB1

12)

11

9%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

4 SE

D-1

R1 (

PCB1

98)

94

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%18

994

SED-

1 R1

(TC

MX)

83

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

40

- 11

0%18

994

SED-

1 R1

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

4 SE

D-1

R1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1899

4 SE

D-1

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%18

994

SED-

1 R1

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1899

4 SE

D-1

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%18

994

SED-

1 R1

4,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1899

4 SE

D-1

R1 A

ldrin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%18

994

SED-

1 R1

BHC

-alph

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

84-6

60 -

123%

1899

4 SE

D-1

R1 B

HC-b

eta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%18

994

SED-

1 R1

BHC

-delt

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

86-8

29 -

113%

1899

4 SE

D-1

R1 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1899

4 SE

D-1

R1 C

hlord

ane-

alpha

9.100

0003

81ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-71-

964

- 11

7%18

994

SED-

1 R1

Chlo

rdan

e-ga

mma

11

.1000

0038

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1899

4 SE

D-1

R1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1899

4 SE

D-1

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1899

4 SE

D-1

R1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1899

4 SE

D-1

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1899

4 SE

D-1

R1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1899

4 SE

D-1

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%18

994

SED-

1 R1

End

rin K

etone

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5349

4-70

-550

- 13

0%18

994

SED-

1 R1

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1899

4 SE

D-1

R1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%18

994

SED-

1 R1

Meth

oxyc

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%18

994

SED-

1 R1

Mire

x ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

2385

-85-

556

- 12

3%18

994

SED-

1 R1

Tota

l Dete

ctable

DDT

s

0ng

/dry g

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

18

994

SED-

1 R1

Tox

aphe

ne

ND

ng/dr

y g10

508/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 80

01-3

5-2

65 -

135%

1899

4 SE

D-1

R1 tr

ans-N

onac

hlor

14

.3999

9962

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

5 SE

D-2

R1 (

PCB0

30)

71

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

46

- 11

9%18

995

SED-

2 R1

(PC

B112

)

94%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

5 SE

D-2

R1 (

PCB1

98)

84

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%18

995

SED-

2 R1

(TC

MX)

63

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

40

- 11

0%18

995

SED-

2 R1

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

5 SE

D-2

R1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1899

5 SE

D-2

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%18

995

SED-

2 R1

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1899

5 SE

D-2

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%

OU 1 001267

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

2

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

5 SE

D-2

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

995

SED-

2 R1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

1899

5 SE

D-2

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

995

SED-

2 R1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

5 SE

D-2

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

995

SED-

2 R1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 58

-89-

959

- 11

0%18

995

SED-

2 R1

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

5 SE

D-2

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%18

995

SED-

2 R1

Diel

drin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%18

995

SED-

2 R1

End

osulf

an S

ulfate

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1031

-07-

825

- 10

4%18

995

SED-

2 R1

End

osulf

an-I

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%18

995

SED-

2 R1

End

osulf

an-II

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3321

3-65

-9MD

L - 13

5%18

995

SED-

2 R1

End

rin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%18

995

SED-

2 R1

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 74

21-9

3-4

59 -

110%

1899

5 SE

D-2

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

5 SE

D-2

R1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%18

995

SED-

2 R1

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

5 SE

D-2

R1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1899

5 SE

D-2

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

5 SE

D-2

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1899

5 SE

D-2

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%18

995

SED-

2 R1

tran

s-Non

achlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3976

5-80

-547

- 14

3%18

996

SED-

3 R1

(PC

B030

)

87%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

1899

6 SE

D-3

R1 (

PCB1

12)

11

4%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

6 SE

D-3

R1 (

PCB1

98)

11

2%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

59 -

123%

1899

6 SE

D-3

R1 (

TCMX

)

85%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

6 SE

D-3

R1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

-19-

056

- 12

9%18

996

SED-

3 R1

2,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%18

996

SED-

3 R1

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1899

6 SE

D-3

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%18

996

SED-

3 R1

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

6 SE

D-3

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

996

SED-

3 R1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

1899

6 SE

D-3

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

996

SED-

3 R1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

6 SE

D-3

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

996

SED-

3 R1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 58

-89-

959

- 11

0%18

996

SED-

3 R1

Chlo

rdan

e-alp

ha

E1

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

6 SE

D-3

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%

OU 1 001268

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

3

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

6 SE

D-3

R1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1899

6 SE

D-3

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1899

6 SE

D-3

R1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1899

6 SE

D-3

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1899

6 SE

D-3

R1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1899

6 SE

D-3

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%18

996

SED-

3 R1

End

rin K

etone

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5349

4-70

-550

- 13

0%18

996

SED-

3 R1

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1899

6 SE

D-3

R1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%18

996

SED-

3 R1

Meth

oxyc

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%18

996

SED-

3 R1

Mire

x ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

2385

-85-

556

- 12

3%18

996

SED-

3 R1

Tota

l Dete

ctable

DDT

s

0ng

/dry g

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

18

996

SED-

3 R1

Tox

aphe

ne

ND

ng/dr

y g10

508/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 80

01-3

5-2

65 -

135%

1899

6 SE

D-3

R1 tr

ans-N

onac

hlor

E1.7

0000

0048

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

7 SE

D-4

MS1

(PCB

030)

65%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

46 -

119%

1899

7 SE

D-4

MS2

(PCB

030)

61%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

46 -

119%

1899

7 SE

D-4

R1 (

PCB0

30)

62

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

46

- 11

9%18

997

SED-

4 R2

(PC

B030

)

60%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

1899

7 SE

D-4

MS1

(PCB

112)

77%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

7 SE

D-4

MS2

(PCB

112)

83%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

7 SE

D-4

R1 (

PCB1

12)

82

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

52

- 12

3%18

997

SED-

4 R2

(PC

B112

)

80%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

7 SE

D-4

MS1

(PCB

198)

71%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

59 -

123%

1899

7 SE

D-4

MS2

(PCB

198)

97%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

59 -

123%

1899

7 SE

D-4

R1 (

PCB1

98)

85

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%18

997

SED-

4 R2

(PC

B198

)

83%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

59 -

123%

1899

7 SE

D-4

MS1

(TCM

X)

62

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

1000

ngCh

lorina

ted P

estic

ides

40

- 11

0%18

997

SED-

4 MS

2 (T

CMX)

49%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t10

00ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

7 SE

D-4

R1 (

TCMX

)

57%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

7 SE

D-4

R2 (

TCMX

)

56%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

7 SE

D-4

MS1

2,4'-D

DD

66

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

7 SE

D-4

MS2

2,4'-D

DD

61

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

7 SE

D-4

R1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

-19-

056

- 12

9%18

997

SED-

4 R2

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1899

7 SE

D-4

MS1

2,4'-D

DE

69

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%18

997

SED-

4 MS

2 2,4

'-DDE

62%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1899

7 SE

D-4

R1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1899

7 SE

D-4

R2 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1899

7 SE

D-4

MS1

2,4'-D

DT

64

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

OU 1 001269

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

4

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

MS2

2,4'-D

DT

72

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1899

7 SE

D-4

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%18

997

SED-

4 R2

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1899

7 SE

D-4

MS1

4,4'-D

DD

73

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1899

7 SE

D-4

MS2

4,4'-D

DD

79

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1899

7 SE

D-4

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%18

997

SED-

4 R2

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1899

7 SE

D-4

MS1

4,4'-D

DE

69

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

7 SE

D-4

MS2

4,4'-D

DE

69

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

7 SE

D-4

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%18

997

SED-

4 R2

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

7 SE

D-4

MS1

4,4'-D

DT

64

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1899

7 SE

D-4

MS2

4,4'-D

DT

84

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1899

7 SE

D-4

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

997

SED-

4 R2

4,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1899

7 SE

D-4

R1 A

ldrin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%18

997

SED-

4 R2

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

1899

7 SE

D-4

MS1

BHC-

alpha

60%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

997

SED-

4 MS

2 BH

C-alp

ha

60

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

319-

84-6

60 -

123%

1899

7 SE

D-4

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

997

SED-

4 R2

BHC

-alph

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

84-6

60 -

123%

1899

7 SE

D-4

MS1

BHC-

beta

58

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

7 SE

D-4

MS2

BHC-

beta

57

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

7 SE

D-4

R1 B

HC-b

eta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%18

997

SED-

4 R2

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

7 SE

D-4

MS1

BHC-

delta

64%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

997

SED-

4 MS

2 BH

C-de

lta

83

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

319-

86-8

29 -

113%

1899

7 SE

D-4

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

997

SED-

4 R2

BHC

-delt

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

86-8

29 -

113%

1899

7 SE

D-4

R1 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1899

7 SE

D-4

R2 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1899

7 SE

D-4

MS1

Chlor

dane

-alph

a

74%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

7 SE

D-4

MS2

Chlor

dane

-alph

a

78%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

7 SE

D-4

R1 C

hlord

ane-

alpha

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-71-

964

- 11

7%18

997

SED-

4 R2

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

7 SE

D-4

MS1

Chlor

dane

-gam

ma

79

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%18

997

SED-

4 MS

2 Ch

lorda

ne-g

amma

80%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1899

7 SE

D-4

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%18

997

SED-

4 R2

Chlo

rdan

e-ga

mma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

OU 1 001270

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

5

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1899

7 SE

D-4

R2 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1899

7 SE

D-4

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1899

7 SE

D-4

R2 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1899

7 SE

D-4

R1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1899

7 SE

D-4

R2 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1899

7 SE

D-4

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1899

7 SE

D-4

R2 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1899

7 SE

D-4

R1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1899

7 SE

D-4

R2 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1899

7 SE

D-4

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%18

997

SED-

4 R2

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 74

21-9

3-4

59 -

110%

1899

7 SE

D-4

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

7 SE

D-4

R2 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

7 SE

D-4

MS1

Hepta

chlor

58%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%18

997

SED-

4 MS

2 He

ptach

lor

49

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1899

7 SE

D-4

R1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%18

997

SED-

4 R2

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1899

7 SE

D-4

MS1

Hepta

chlor

Epo

xide

79

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

300

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%18

997

SED-

4 MS

2 He

ptach

lor E

poxid

e

77%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t30

0ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

7 SE

D-4

R1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%18

997

SED-

4 R2

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

7 SE

D-4

R1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1899

7 SE

D-4

R2 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1899

7 SE

D-4

MS1

Mire

x

61%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t15

0ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

7 SE

D-4

MS2

Mire

x

64%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t15

0ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

7 SE

D-4

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

7 SE

D-4

R2 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

7 SE

D-4

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1899

7 SE

D-4

R2 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1899

7 SE

D-4

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%18

997

SED-

4 R2

Tox

aphe

ne

ND

ng/dr

y g10

508/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 80

01-3

5-2

65 -

135%

1899

7 SE

D-4

MS1

trans

-Non

achlo

r

89%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t15

0ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

7 SE

D-4

MS2

trans

-Non

achlo

r

89%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t15

0ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

7 SE

D-4

R1 tr

ans-N

onac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

7 SE

D-4

R2 tr

ans-N

onac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

8 SE

D-5

R1 (

PCB0

30)

46

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

46

- 11

9%18

998

SED-

5 R1

(PC

B112

)

61%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1899

8 SE

D-5

R1 (

PCB1

98)

80

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%

OU 1 001271

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

6

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

8 SE

D-5

R1 (

TCMX

)

45%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

8 SE

D-5

R1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

-19-

056

- 12

9%18

998

SED-

5 R1

2,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%18

998

SED-

5 R1

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1899

8 SE

D-5

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%18

998

SED-

5 R1

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

8 SE

D-5

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

998

SED-

5 R1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

1899

8 SE

D-5

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

998

SED-

5 R1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

8 SE

D-5

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

998

SED-

5 R1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 58

-89-

959

- 11

0%18

998

SED-

5 R1

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

8 SE

D-5

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%18

998

SED-

5 R1

Diel

drin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%18

998

SED-

5 R1

End

osulf

an S

ulfate

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1031

-07-

825

- 10

4%18

998

SED-

5 R1

End

osulf

an-I

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%18

998

SED-

5 R1

End

osulf

an-II

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3321

3-65

-9MD

L - 13

5%18

998

SED-

5 R1

End

rin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%18

998

SED-

5 R1

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 74

21-9

3-4

59 -

110%

1899

8 SE

D-5

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

8 SE

D-5

R1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%18

998

SED-

5 R1

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

8 SE

D-5

R1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1899

8 SE

D-5

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

8 SE

D-5

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1899

8 SE

D-5

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%18

998

SED-

5 R1

tran

s-Non

achlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3976

5-80

-547

- 14

3%18

999

SED-

6 R1

(PC

B030

)

46%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

1899

9 SE

D-6

R1 (

PCB1

12)

56

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

52

- 12

3%18

999

SED-

6 R1

(PC

B198

)

59%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

59 -

123%

1899

9 SE

D-6

R1 (

TCMX

)

40%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1899

9 SE

D-6

R1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

-19-

056

- 12

9%18

999

SED-

6 R1

2,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%18

999

SED-

6 R1

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1899

9 SE

D-6

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%18

999

SED-

6 R1

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1899

9 SE

D-6

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%18

999

SED-

6 R1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

OU 1 001272

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

7

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

9 SE

D-6

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%18

999

SED-

6 R1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1899

9 SE

D-6

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%18

999

SED-

6 R1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 58

-89-

959

- 11

0%18

999

SED-

6 R1

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1899

9 SE

D-6

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%18

999

SED-

6 R1

Diel

drin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%18

999

SED-

6 R1

End

osulf

an S

ulfate

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1031

-07-

825

- 10

4%18

999

SED-

6 R1

End

osulf

an-I

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%18

999

SED-

6 R1

End

osulf

an-II

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3321

3-65

-9MD

L - 13

5%18

999

SED-

6 R1

End

rin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%18

999

SED-

6 R1

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 74

21-9

3-4

59 -

110%

1899

9 SE

D-6

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1899

9 SE

D-6

R1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%18

999

SED-

6 R1

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1899

9 SE

D-6

R1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1899

9 SE

D-6

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1899

9 SE

D-6

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1899

9 SE

D-6

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%18

999

SED-

6 R1

tran

s-Non

achlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3976

5-80

-547

- 14

3%19

000

SED-

7 R1

(PC

B030

)

76%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

1900

0 SE

D-7

R1 (

PCB1

12)

10

1%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1900

0 SE

D-7

R1 (

PCB1

98)

87

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%19

000

SED-

7 R1

(TC

MX)

71

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

40

- 11

0%19

000

SED-

7 R1

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1900

0 SE

D-7

R1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1900

0 SE

D-7

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%19

000

SED-

7 R1

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1900

0 SE

D-7

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%19

000

SED-

7 R1

4,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1900

0 SE

D-7

R1 A

ldrin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%19

000

SED-

7 R1

BHC

-alph

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

84-6

60 -

123%

1900

0 SE

D-7

R1 B

HC-b

eta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%19

000

SED-

7 R1

BHC

-delt

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

86-8

29 -

113%

1900

0 SE

D-7

R1 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1900

0 SE

D-7

R1 C

hlord

ane-

alpha

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-71-

964

- 11

7%19

000

SED-

7 R1

Chlo

rdan

e-ga

mma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1900

0 SE

D-7

R1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1900

0 SE

D-7

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

OU 1 001273

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

8

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

0 SE

D-7

R1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1900

0 SE

D-7

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1900

0 SE

D-7

R1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1900

0 SE

D-7

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%19

000

SED-

7 R1

End

rin K

etone

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5349

4-70

-550

- 13

0%19

000

SED-

7 R1

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1900

0 SE

D-7

R1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%19

000

SED-

7 R1

Meth

oxyc

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%19

000

SED-

7 R1

Mire

x ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

2385

-85-

556

- 12

3%19

000

SED-

7 R1

Tota

l Dete

ctable

DDT

s

0ng

/dry g

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

19

000

SED-

7 R1

Tox

aphe

ne

ND

ng/dr

y g10

508/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 80

01-3

5-2

65 -

135%

1900

0 SE

D-7

R1 tr

ans-N

onac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1900

1 SE

D-8

R1 (

PCB0

30)

77

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

46

- 11

9%19

001

SED-

8 R1

(PC

B112

)

97%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

52 -

123%

1900

1 SE

D-8

R1 (

PCB1

98)

74

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

59

- 12

3%19

001

SED-

8 R1

(TC

MX)

66

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

40

- 11

0%19

001

SED-

8 R1

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1900

1 SE

D-8

R1 2

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 34

24-8

2-9

60 -

129%

1900

1 SE

D-8

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%19

001

SED-

8 R1

4,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

4-8

46 -

138%

1900

1 SE

D-8

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%19

001

SED-

8 R1

4,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

50-2

9-3

34 -

136%

1900

1 SE

D-8

R1 A

ldrin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%19

001

SED-

8 R1

BHC

-alph

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

84-6

60 -

123%

1900

1 SE

D-8

R1 B

HC-b

eta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%19

001

SED-

8 R1

BHC

-delt

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

86-8

29 -

113%

1900

1 SE

D-8

R1 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1900

1 SE

D-8

R1 C

hlord

ane-

alpha

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-71-

964

- 11

7%19

001

SED-

8 R1

Chlo

rdan

e-ga

mma

E1.1

0000

0024

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1900

1 SE

D-8

R1 D

ieldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

60-5

7-1

46 -

125%

1900

1 SE

D-8

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1900

1 SE

D-8

R1 E

ndos

ulfan

-I ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

959-

98-8

54 -

141%

1900

1 SE

D-8

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1900

1 SE

D-8

R1 E

ndrin

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-2

0-8

32 -

141%

1900

1 SE

D-8

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%19

001

SED-

8 R1

End

rin K

etone

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5349

4-70

-550

- 13

0%19

001

SED-

8 R1

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1900

1 SE

D-8

R1 H

eptac

hlor E

poxid

e ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1024

-57-

356

- 12

2%19

001

SED-

8 R1

Meth

oxyc

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%

OU 1 001274

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-8

9

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

1 SE

D-8

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1900

1 SE

D-8

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1900

1 SE

D-8

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%19

001

SED-

8 R1

tran

s-Non

achlo

r E

1.200

0000

48ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3976

5-80

-547

- 14

3%19

002

SED-

9 R1

(PC

B030

)

46%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

46 -

119%

1900

2 SE

D-9

R1 (

PCB1

12)

56

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

52

- 12

3%19

002

SED-

9 R1

(PC

B198

)

67%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

59 -

123%

1900

2 SE

D-9

R1 (

TCMX

)

40%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

40 -

110%

1900

2 SE

D-9

R1 2

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

-19-

056

- 12

9%19

002

SED-

9 R1

2,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%19

002

SED-

9 R1

2,4'

-DDT

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

789-

02-6

39 -

130%

1900

2 SE

D-9

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%19

002

SED-

9 R1

4,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-5

5-9

69 -

116%

1900

2 SE

D-9

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%19

002

SED-

9 R1

Aldr

in ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

309-

00-2

45 -

128%

1900

2 SE

D-9

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%19

002

SED-

9 R1

BHC

-beta

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

319-

85-7

45 -

140%

1900

2 SE

D-9

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%19

002

SED-

9 R1

BHC

-gam

ma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 58

-89-

959

- 11

0%19

002

SED-

9 R1

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1900

2 SE

D-9

R1 C

hlord

ane-

gamm

a ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

5103

-74-

246

- 12

5%19

002

SED-

9 R1

Diel

drin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%19

002

SED-

9 R1

End

osulf

an S

ulfate

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

1031

-07-

825

- 10

4%19

002

SED-

9 R1

End

osulf

an-I

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%19

002

SED-

9 R1

End

osulf

an-II

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3321

3-65

-9MD

L - 13

5%19

002

SED-

9 R1

End

rin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%19

002

SED-

9 R1

End

rin A

ldehy

de

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 74

21-9

3-4

59 -

110%

1900

2 SE

D-9

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1900

2 SE

D-9

R1 H

eptac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 76

-44-

843

- 12

2%19

002

SED-

9 R1

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1900

2 SE

D-9

R1 M

ethox

ychlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

72-4

3-5

MDL -

157%

1900

2 SE

D-9

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1900

2 SE

D-9

R1 T

otal D

etecta

ble D

DTs

0

ng/dr

y g

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

1900

2 SE

D-9

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%19

002

SED-

9 R1

tran

s-Non

achlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3976

5-80

-547

- 14

3%19

003

SED-

10

R1 (

PCB0

30)

70

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

46

- 11

9%19

003

SED-

10

R1 (

PCB1

12)

94

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

52

- 12

3%19

003

SED-

10

R1 (

PCB1

98)

10

8%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s

59 -

123%

1900

3 SE

D-10

R1

(TC

MX)

63

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

40

- 11

0%

OU 1 001275

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

0

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

R1

2,4'

-DDD

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

53-1

9-0

56 -

129%

1900

3 SE

D-10

R1

2,4'

-DDE

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

3424

-82-

960

- 12

9%19

003

SED-

10

R1 2

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 78

9-02

-639

- 13

0%19

003

SED-

10

R1 4

,4'-D

DD

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-54-

846

- 13

8%19

003

SED-

10

R1 4

,4'-D

DE

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-55-

969

- 11

6%19

003

SED-

10

R1 4

,4'-D

DT

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 50

-29-

334

- 13

6%19

003

SED-

10

R1 A

ldrin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 30

9-00

-245

- 12

8%19

003

SED-

10

R1 B

HC-a

lpha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-84

-660

- 12

3%19

003

SED-

10

R1 B

HC-b

eta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-85

-745

- 14

0%19

003

SED-

10

R1 B

HC-d

elta

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 31

9-86

-829

- 11

3%19

003

SED-

10

R1 B

HC-g

amma

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

58-8

9-9

59 -

110%

1900

3 SE

D-10

R1

Chlo

rdan

e-alp

ha

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

1-9

64 -

117%

1900

3 SE

D-10

R1

Chlo

rdan

e-ga

mma

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 51

03-7

4-2

46 -

125%

1900

3 SE

D-10

R1

Diel

drin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 60

-57-

146

- 12

5%19

003

SED-

10

R1 E

ndos

ulfan

Sulf

ate

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

31-0

7-8

25 -

104%

1900

3 SE

D-10

R1

End

osulf

an-I

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 95

9-98

-854

- 14

1%19

003

SED-

10

R1 E

ndos

ulfan

-II

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 33

213-

65-9

MDL -

135%

1900

3 SE

D-10

R1

End

rin

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-20-

832

- 14

1%19

003

SED-

10

R1 E

ndrin

Alde

hyde

ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

7421

-93-

459

- 11

0%19

003

SED-

10

R1 E

ndrin

Keto

ne

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 53

494-

70-5

50 -

130%

1900

3 SE

D-10

R1

Hep

tachlo

r ND

ng

/dry g

15

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

76-4

4-8

43 -

122%

1900

3 SE

D-10

R1

Hep

tachlo

r Epo

xide

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 10

24-5

7-3

56 -

122%

1900

3 SE

D-10

R1

Meth

oxyc

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 72

-43-

5MD

L - 15

7%19

003

SED-

10

R1 M

irex

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 23

85-8

5-5

56 -

123%

1900

3 SE

D-10

R1

Tota

l Dete

ctable

DDT

s

0ng

/dry g

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

19

003

SED-

10

R1 T

oxap

hene

ND

ng

/dry g

1050

8/16/0

48/2

4/04

Sedim

ent

ngCh

lorina

ted P

estic

ides

8001

-35-

265

- 13

5%19

003

SED-

10

R1 tr

ans-N

onac

hlor

ND

ng/dr

y g1

58/1

6/04

8/24/0

4 Se

dimen

t ng

Chlor

inated

Pes

ticide

s 39

765-

80-5

47 -

143%

1899

3 QA

QC

B1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB02

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB03

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB04

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB05

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB07

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB07

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

OU 1 001276

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

1

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

3 QA

QC

B1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB08

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB09

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB10

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB11

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB12

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB12

8+16

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB13

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB14

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB15

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB15

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB15

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB15

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB16

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB17

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PCB

Cong

ener

s

65 -

135%

1899

3 QA

QC

B1 T

otal D

etecta

ble P

CBs

0

ng/dr

y g

8/1

6/04

8/23/0

4 DI

Wate

r

ngPC

B Co

ngen

ers

18

994

SED-

1 R1

PCB

018

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB02

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

031

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB03

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001277

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

2

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

4 SE

D-1

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB09

5

14.60

0000

38ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB09

9

14.80

0000

19ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

101

28

.7999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

110

18

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

114

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

119

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB12

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

126

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB12

8+16

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

138

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

149

16

.7000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB15

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

153

17

.6000

0038

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB15

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

157

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB15

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

168+

132

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB16

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

170

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB17

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

180

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

OU 1 001278

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

3

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

4 SE

D-1

R1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

PCB

201

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

4 SE

D-1

R1 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

994

SED-

1 R1

Tota

l Dete

ctable

PCB

s

111

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

1899

5 SE

D-2

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

101

E2.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

110

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

123

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB13

8 E

4.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB14

9 E

1.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB15

3 E

2.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001279

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

4

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

5 SE

D-2

R1 P

CB16

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

170

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB17

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

180

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

PCB

201

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

5 SE

D-2

R1 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

995

SED-

2 R1

Tota

l Dete

ctable

PCB

s

10.5

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

1899

6 SE

D-3

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB09

5 E

5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

101

13

.6000

0038

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

110

7.8

0000

0191

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

123

10

.1999

9981

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB13

8

56.59

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001280

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

5

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

6 SE

D-3

R1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

149

6.5

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB15

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

153

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB15

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

157

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB15

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

168+

132

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB16

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

170

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB17

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

180

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

PCB

201

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

6 SE

D-3

R1 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

996

SED-

3 R1

Tota

l Dete

ctable

PCB

s

99.80

0003

05ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

18

997

SED-

4 R1

PCB

018

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B018

76%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

18

65

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

28

81

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B028

74%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB02

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

031

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

31

76

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

031

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

31

73

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB03

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B033

79%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

33

76

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

037

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

37

92

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B037

75%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

OU 1 001281

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

6

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R2 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

44

88

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B044

68%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB04

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

049

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

49

87

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B049

69%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB04

9 E

1.399

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

52

88

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B052

73%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB05

2 E

1.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

066

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

66

83

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B066

68%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

70

91

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B070

76%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB07

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

074

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB0

74

10

0%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

74

81

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

074

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB07

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B077

94%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

77

89

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B081

94%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

81

91

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

081

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB08

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B087

112

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B087

110

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB09

5 E

1.200

0000

48ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B095

86%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

OU 1 001282

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

7

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

MS2

PCB0

95

69

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

095

E1.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB09

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B097

97%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB0

97

82

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B099

100

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B099

87%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

101

E2.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

01

92

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B101

111

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

101

E2.9

0000

0095

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

05

87

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

105

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

05

10

2%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

110

E2.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

10

10

3%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

10

82

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

110

E3.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B114

107

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B114

100

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

114

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B118

123

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B118

96%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

119

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

19

91

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B119

81%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

123

E2.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

23

10

9%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

23

10

6%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB12

3 E

3.799

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B126

98%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

OU 1 001283

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

8

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B126

115

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

126

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

28+1

67

98

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

320

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

28+1

67

12

2%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t32

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB12

8+16

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B138

94%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB13

8 E

3.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B138

133

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

138

5.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

41

11

9%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B141

103

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB14

9 E

1.399

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B149

104

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B149

91%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB14

9 E

1.399

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

51

10

7%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

51

84

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

53

83

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

153

E2

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

53

11

9%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB15

3 E

3.200

0000

48ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B156

117

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

56

13

5%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB15

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B157

89%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B157

103

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

157

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

58

98

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

58

11

2%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB15

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001284

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-9

9

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

MS2

PCB1

68+1

32

82

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

300

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

168+

132

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

68+1

32

94

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

300

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

168+

132

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

69

13

2%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB16

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B169

125

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

70

12

0%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B170

135

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

170

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

77

10

6%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB17

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B177

120

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

80

11

7%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B180

130

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

180

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

83

10

6%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B183

112

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

183

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB1

87

98

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB1

87

11

4%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B200

98%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B200

106

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R2

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS2

PCB2

01

12

2%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

1 PC

B201

135

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001285

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

00

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R2 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 MS

2 PC

B206

121

% R

ecov

ery

15

8/16/0

48/2

3/04

Sedim

ent

160

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

MS1

PCB2

06

12

6%

Rec

over

y1

58/1

6/04

8/23/0

4 Se

dimen

t16

0ng

PCB

Cong

ener

s

65 -

135%

1899

7 SE

D-4

R2 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

997

SED-

4 R1

Tota

l Dete

ctable

PCB

s

14.60

0000

38ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

18

997

SED-

4 R2

Tota

l Dete

ctable

PCB

s

24.10

0000

38ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

18

998

SED-

5 R1

PCB

018

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB02

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

031

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB03

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

037

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB04

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

049

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB05

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

066

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB07

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

074

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB07

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

081

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB08

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

095

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB09

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

099

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB10

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

105

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB11

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

114

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

119

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB12

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

126

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB12

8+16

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

138

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

149

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB15

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

153

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB15

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001286

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

01

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

8 SE

D-5

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

183

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

998

SED-

5 R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

8 SE

D-5

R1 T

otal D

etecta

ble P

CBs

0

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

1899

9 SE

D-6

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB09

5 E

1.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

101

E3

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

110

E2.4

0000

0095

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

123

E3.4

0000

0095

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

OU 1 001287

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

02

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

9 SE

D-6

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB13

8

5.800

0001

91ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB14

9 E

1.399

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB15

3 E

2.700

0000

48ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

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65

- 13

5%18

999

SED-

6 R1

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183

ND

ng/dr

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58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

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1899

9 SE

D-6

R1 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%18

999

SED-

6 R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1899

9 SE

D-6

R1 T

otal D

etecta

ble P

CBs

20

ng/dr

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8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

1900

0 SE

D-7

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

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PCB

Cong

ener

s

65 -

135%

OU 1 001288

App

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x B

– R

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Page

B-1

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App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

0 SE

D-7

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

101

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

110

E2.0

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

123

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB13

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB14

9 E

1.100

0000

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB15

3 E

2.400

0000

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

183

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

000

SED-

7 R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

0 SE

D-7

R1 T

otal D

etecta

ble P

CBs

5.5

9999

9905

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

1900

1 SE

D-8

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

OU 1 001289

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

04

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

1 SE

D-8

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

101

E2.4

0000

0095

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

110

E2.0

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

123

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB13

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB14

9 E

1.600

0000

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB15

3 E

2.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

183

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB18

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB19

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 P

CB20

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

001

SED-

8 R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

1 SE

D-8

R1 T

otal D

etecta

ble P

CBs

8.6

0000

0381

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

OU 1 001290

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

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le

App

endi

x B

– R

aw D

ata

Page

B-1

05

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

2 SE

D-9

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

028

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

033

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

044

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

052

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

070

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

077

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

087

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

097

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

101

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

110

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

118

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

123

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

128+

167

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB13

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

141

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB14

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

151

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB15

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB15

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB16

8+13

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB17

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB18

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001291

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

06

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

2 SE

D-9

R1 P

CB18

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB18

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB20

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

PCB

201

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

2 SE

D-9

R1 P

CB20

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

002

SED-

9 R1

Tota

l Dete

ctable

PCB

s

0ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

19

003

SED-

10

R1 P

CB01

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB02

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB03

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB03

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB03

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB04

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB04

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB05

2 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB06

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB07

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB07

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB07

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB08

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB08

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB09

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB09

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB09

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB10

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB10

5 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB11

0 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB11

4 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB11

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB11

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB12

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB12

6 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB12

8+16

7 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB13

8 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB14

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB14

9 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB15

1 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%19

003

SED-

10

R1 P

CB15

3 ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

65

- 13

5%

OU 1 001292

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

07

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

R1

PCB

156

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

157

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

158

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

168+

132

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

169

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

170

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

177

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

180

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

183

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

187

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

189

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

194

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

200

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

201

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

PCB

206

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PCB

Cong

ener

s

65 -

135%

1900

3 SE

D-10

R1

Tota

l Dete

ctable

PCB

s

0ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPC

B Co

ngen

ers

18

993

QAQC

B1

(d1

0-Ac

enap

hthen

e)

71

% R

ecov

ery

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

52 -

125%

1899

3 QA

QC

B1 (

d10-

Phen

anthr

ene)

81%

Rec

over

y

8/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs

57 -

128%

1899

3 QA

QC

B1 (

d12-

Chrys

ene)

101

% R

ecov

ery

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

61

- 12

6%18

993

QAQC

B1

(d1

2-Pe

rylen

e)

12

8%

Rec

over

y

8/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs

53 -

122%

1899

3 QA

QC

B1 (

d8-N

aphth

alene

)

53%

Rec

over

y

8/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs

47 -

110%

1899

3 QA

QC

B1 1

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs90

-12-

050

- 12

0%18

993

QAQC

B1

1-M

ethylp

hena

nthre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs83

2-69

-970

- 13

0%18

993

QAQC

B1

2,3,

5-Tr

imeth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs22

45-3

8-7

70 -

130%

1899

3 QA

QC

B1 2

,6-Di

methy

lnaph

thalen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

581-

42-0

70 -

130%

1899

3 QA

QC

B1 2

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs91

-57-

650

- 12

0%18

993

QAQC

B1

Ace

naph

thene

ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

83-3

2-9

70 -

130%

1899

3 QA

QC

B1 A

cena

phthy

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs20

8-96

-870

- 13

0%18

993

QAQC

B1

Anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs12

0-12

-770

- 13

0%18

993

QAQC

B1

Ben

z[a]an

thrac

ene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs56

-55-

370

- 13

0%18

993

QAQC

B1

Ben

zo[a]

pyre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs50

-32-

870

- 13

0%18

993

QAQC

B1

Ben

zo[b]

fluor

anthe

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs20

5NA-

270

- 13

0%18

993

QAQC

B1

Ben

zo[e]

pyre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs19

2-97

-270

- 13

0%18

993

QAQC

B1

Ben

zo[g,

h,i]pe

rylen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

191-

24-2

70 -

130%

1899

3 QA

QC

B1 B

enzo

[k]flu

oran

thene

ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

207-

08-9

70 -

130%

1899

3 QA

QC

B1 B

iphen

yl ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

92-5

2-4

50 -

120%

1899

3 QA

QC

B1 C

hrys

ene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs21

8-01

-970

- 13

0%18

993

QAQC

B1

Dibe

nz[a,

h]anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs53

-70-

370

- 13

0%18

993

QAQC

B1

Fluo

ranth

ene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs20

6-44

-070

- 13

0%

OU 1 001293

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

08

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

3 QA

QC

B1 F

luore

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs86

-73-

770

- 13

0%18

993

QAQC

B1

Inde

no[1,

2,3-c,

d]pyre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs19

3-39

-570

- 13

0%18

993

QAQC

B1

Nap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs91

-20-

350

- 12

0%18

993

QAQC

B1

Per

ylene

ND

ng

/dry g

15

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

198-

55-0

70 -

130%

1899

3 QA

QC

B1 P

hena

nthre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs85

-01-

870

- 13

0%18

993

QAQC

B1

Pyre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 DI

Wate

r

ngPA

Hs12

9-00

-070

- 13

0%18

993

QAQC

B1

Tota

l Dete

ctable

PAH

s

0ng

/dry g

8/16/0

48/2

3/04

DI W

ater

ng

PAHs

70

- 13

0%18

994

SED-

1 R1

(d1

0-Ac

enap

hthen

e)

69

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1899

4 SE

D-1

R1 (

d10-

Phen

anthr

ene)

80%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%18

994

SED-

1 R1

(d1

2-Ch

rysen

e)

12

3%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

61

- 12

6%18

994

SED-

1 R1

(d1

2-Pe

rylen

e)

17

0%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%18

994

SED-

1 R1

(d8

-Nap

hthale

ne)

46

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1899

4 SE

D-1

R1 1

-Meth

ylnap

hthale

ne

6.1

9999

9809

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

4 SE

D-1

R1 1

-Meth

ylphe

nanth

rene

97.19

9996

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%18

994

SED-

1 R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

8.8

0000

0191

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%18

994

SED-

1 R1

2,6-

Dime

thylna

phtha

lene

12

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%18

994

SED-

1 R1

2-M

ethyln

aphth

alene

12.69

9999

81ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-57-

650

- 12

0%18

994

SED-

1 R1

Ace

naph

thene

26ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

-32-

970

- 13

0%18

994

SED-

1 R1

Ace

naph

thylen

e

6.400

0000

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

8-96

-870

- 13

0%18

994

SED-

1 R1

Anth

race

ne

11

1ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%18

994

SED-

1 R1

Ben

z[a]an

thrac

ene

19

30ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%18

994

SED-

1 R1

Ben

zo[a]

pyre

ne

33

40ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs50

-32-

870

- 13

0%18

994

SED-

1 R1

Ben

zo[b]

fluor

anthe

ne

25

60ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%18

994

SED-

1 R1

Ben

zo[e]

pyre

ne

15

70ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%18

994

SED-

1 R1

Ben

zo[g,

h,i]pe

rylen

e

2110

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

4 SE

D-1

R1 B

enzo

[k]flu

oran

thene

2450

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1899

4 SE

D-1

R1 B

iphen

yl

5.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%18

994

SED-

1 R1

Chr

ysen

e

1790

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1899

4 SE

D-1

R1 D

ibenz

[a,h]a

nthra

cene

726

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1899

4 SE

D-1

R1 F

luora

nthen

e

2530

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1899

4 SE

D-1

R1 F

luore

ne

31

.7000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1899

4 SE

D-1

R1 In

deno

[1,2,3

-c,d]p

yrene

2480

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

193-

39-5

70 -

130%

1899

4 SE

D-1

R1 N

aphth

alene

19.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%18

994

SED-

1 R1

Per

ylene

810

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1899

4 SE

D-1

R1 P

hena

nthre

ne

68

5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

994

SED-

1 R1

Pyre

ne

27

80ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%18

994

SED-

1 R1

Tota

l Dete

ctable

PAH

s

2609

8.240

23ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

70 -

130%

1899

5 SE

D-2

R1 (

d10-

Acen

aphth

ene)

65%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

52

- 12

5%18

995

SED-

2 R1

(d1

0-Ph

enan

thren

e)

75

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

57 -

128%

OU 1 001294

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

09

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

5 SE

D-2

R1 (

d12-

Chrys

ene)

107

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1899

5 SE

D-2

R1 (

d12-

Peryl

ene)

137

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

53 -

122%

1899

5 SE

D-2

R1 (

d8-N

aphth

alene

)

40%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

47

- 11

0%18

995

SED-

2 R1

1-M

ethyln

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs90

-12-

050

- 12

0%18

995

SED-

2 R1

1-M

ethylp

hena

nthre

ne

8.1

9999

9809

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

832-

69-9

70 -

130%

1899

5 SE

D-2

R1 2

,3,5-

Trim

ethyln

aphth

alene

3.099

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs22

45-3

8-7

70 -

130%

1899

5 SE

D-2

R1 2

,6-Di

methy

lnaph

thalen

e

2.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%18

995

SED-

2 R1

2-M

ethyln

aphth

alene

2ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-57-

650

- 12

0%18

995

SED-

2 R1

Ace

naph

thene

1.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

-32-

970

- 13

0%18

995

SED-

2 R1

Ace

naph

thylen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

8-96

-870

- 13

0%18

995

SED-

2 R1

Anth

race

ne

4.1

9999

9809

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

120-

12-7

70 -

130%

1899

5 SE

D-2

R1 B

enz[a

]anthr

acen

e

44.29

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%18

995

SED-

2 R1

Ben

zo[a]

pyre

ne

70

.5999

9847

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1899

5 SE

D-2

R1 B

enzo

[b]flu

oran

thene

55.79

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%18

995

SED-

2 R1

Ben

zo[e]

pyre

ne

37

.2000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

192-

97-2

70 -

130%

1899

5 SE

D-2

R1 B

enzo

[g,h,i

]peryl

ene

57

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

5 SE

D-2

R1 B

enzo

[k]flu

oran

thene

54.29

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

7-08

-970

- 13

0%18

995

SED-

2 R1

Biph

enyl

E1.6

0000

0024

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

92-5

2-4

50 -

120%

1899

5 SE

D-2

R1 C

hrys

ene

41

.7000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1899

5 SE

D-2

R1 D

ibenz

[a,h]a

nthra

cene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs53

-70-

370

- 13

0%18

995

SED-

2 R1

Fluo

ranth

ene

75

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1899

5 SE

D-2

R1 F

luore

ne

2.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1899

5 SE

D-2

R1 In

deno

[1,2,3

-c,d]p

yrene

58.29

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%18

995

SED-

2 R1

Nap

hthale

ne

1.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-2

0-3

50 -

120%

1899

5 SE

D-2

R1 P

eryle

ne

20

.3999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1899

5 SE

D-2

R1 P

hena

nthre

ne

21

.2000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

85-0

1-8

70 -

130%

1899

5 SE

D-2

R1 P

yrene

102

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

129-

00-0

70 -

130%

1899

5 SE

D-2

R1 T

otal D

etecta

ble P

AHs

66

4.520

0195

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%18

996

SED-

3 R1

(d1

0-Ac

enap

hthen

e)

57

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1899

6 SE

D-3

R1 (

d10-

Phen

anthr

ene)

69%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%18

996

SED-

3 R1

(d1

2-Ch

rysen

e)

10

7%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

61

- 12

6%18

996

SED-

3 R1

(d1

2-Pe

rylen

e)

15

0%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%18

996

SED-

3 R1

(d8

-Nap

hthale

ne)

34

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1899

6 SE

D-3

R1 1

-Meth

ylnap

hthale

ne

1.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

6 SE

D-3

R1 1

-Meth

ylphe

nanth

rene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%18

996

SED-

3 R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

2.5

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%18

996

SED-

3 R1

2,6-

Dime

thylna

phtha

lene

2.9

0000

0095

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

581-

42-0

70 -

130%

1899

6 SE

D-3

R1 2

-Meth

ylnap

hthale

ne

3

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1899

6 SE

D-3

R1 A

cena

phthe

ne

1.7

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

OU 1 001295

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

10

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

6 SE

D-3

R1 A

cena

phthy

lene

1.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1899

6 SE

D-3

R1 A

nthra

cene

6.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%18

996

SED-

3 R1

Ben

z[a]an

thrac

ene

77

.4000

0153

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

56-5

5-3

70 -

130%

1899

6 SE

D-3

R1 B

enzo

[a]py

rene

152

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1899

6 SE

D-3

R1 B

enzo

[b]flu

oran

thene

128

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

205N

A-2

70 -

130%

1899

6 SE

D-3

R1 B

enzo

[e]py

rene

83ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%18

996

SED-

3 R1

Ben

zo[g,

h,i]pe

rylen

e

120

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

6 SE

D-3

R1 B

enzo

[k]flu

oran

thene

114

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1899

6 SE

D-3

R1 B

iphen

yl

3.599

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%18

996

SED-

3 R1

Chr

ysen

e

81ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs21

8-01

-970

- 13

0%18

996

SED-

3 R1

Dibe

nz[a,

h]anth

race

ne

30

.2999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1899

6 SE

D-3

R1 F

luora

nthen

e

116

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1899

6 SE

D-3

R1 F

luore

ne

2.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1899

6 SE

D-3

R1 In

deno

[1,2,3

-c,d]p

yrene

129

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

193-

39-5

70 -

130%

1899

6 SE

D-3

R1 N

aphth

alene

2.700

0000

48ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%18

996

SED-

3 R1

Per

ylene

32.59

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

8-55

-070

- 13

0%18

996

SED-

3 R1

Phe

nanth

rene

29.70

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

996

SED-

3 R1

Pyre

ne

12

3ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%18

996

SED-

3 R1

Tota

l Dete

ctable

PAH

s

1244

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%18

997

SED-

4 MS

1 (d

10-A

cena

phthe

ne)

55

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

4000

ngPA

Hs

52 -

125%

1899

7 SE

D-4

MS2

(d10

-Ace

naph

thene

)

52%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t40

00ng

PAHs

52

- 12

5%18

997

SED-

4 R1

(d1

0-Ac

enap

hthen

e)

57

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1899

7 SE

D-4

R2 (

d10-

Acen

aphth

ene)

49%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

52

- 12

5%18

997

SED-

4 MS

1 (d

10-P

hena

nthre

ne)

64

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

4000

ngPA

Hs

57 -

128%

1899

7 SE

D-4

MS2

(d10

-Phe

nanth

rene

)

61%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t40

00ng

PAHs

57

- 12

8%18

997

SED-

4 R1

(d1

0-Ph

enan

thren

e)

70

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

57 -

128%

1899

7 SE

D-4

R2 (

d10-

Phen

anthr

ene)

58%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%18

997

SED-

4 MS

1 (d

12-C

hrys

ene)

84%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t40

00ng

PAHs

61

- 12

6%18

997

SED-

4 MS

2 (d

12-C

hrys

ene)

93%

Rec

over

y

8/1

6/04

8/24/0

4 Se

dimen

t40

00ng

PAHs

61

- 12

6%18

997

SED-

4 R1

(d1

2-Ch

rysen

e)

11

3%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

61

- 12

6%18

997

SED-

4 R2

(d1

2-Ch

rysen

e)

91

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1899

7 SE

D-4

MS1

(d12

-Per

ylene

)

107

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

4000

ngPA

Hs

53 -

122%

1899

7 SE

D-4

MS2

(d12

-Per

ylene

)

117

% R

ecov

ery

8/16/0

48/2

4/04

Sedim

ent

4000

ngPA

Hs

53 -

122%

1899

7 SE

D-4

R1 (

d12-

Peryl

ene)

143

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

53 -

122%

1899

7 SE

D-4

R2 (

d12-

Peryl

ene)

112

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

53 -

122%

1899

7 SE

D-4

R1 (

d8-N

aphth

alene

)

26%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

47

- 11

0%18

997

SED-

4 R2

(d8

-Nap

hthale

ne)

27

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1899

7 SE

D-4

MS1

1-Me

thylna

phtha

lene

81

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

131

ngPA

Hs90

-12-

050

- 12

0%18

997

SED-

4 MS

2 1-

Methy

lnaph

thalen

e

73%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

1ng

PAHs

90-1

2-0

50 -

120%

OU 1 001296

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

11

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

R1 1

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

7 SE

D-4

R2 1

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

7 SE

D-4

MS1

1-Me

thylph

enan

thren

e

101

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

130

ngPA

Hs83

2-69

-970

- 13

0%18

997

SED-

4 MS

2 1-

Methy

lphen

anthr

ene

11

5%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

0ng

PAHs

832-

69-9

70 -

130%

1899

7 SE

D-4

R1 1

-Meth

ylphe

nanth

rene

2.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%18

997

SED-

4 R2

1-M

ethylp

hena

nthre

ne

3.5

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

832-

69-9

70 -

130%

1899

7 SE

D-4

MS1

2,3,5-

Trim

ethyln

aphth

alene

89%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

6ng

PAHs

2245

-38-

770

- 13

0%18

997

SED-

4 MS

2 2,3

,5-Tr

imeth

ylnap

hthale

ne

81

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

136

ngPA

Hs22

45-3

8-7

70 -

130%

1899

7 SE

D-4

R1 2

,3,5-

Trim

ethyln

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs22

45-3

8-7

70 -

130%

1899

7 SE

D-4

R2 2

,3,5-

Trim

ethyln

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs22

45-3

8-7

70 -

130%

1899

7 SE

D-4

MS1

2,6-D

imeth

ylnap

hthale

ne

91

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

132

ngPA

Hs58

1-42

-070

- 13

0%18

997

SED-

4 MS

2 2,6

-Dim

ethyln

aphth

alene

83%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

2ng

PAHs

581-

42-0

70 -

130%

1899

7 SE

D-4

R1 2

,6-Di

methy

lnaph

thalen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%18

997

SED-

4 R2

2,6-

Dime

thylna

phtha

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

581-

42-0

70 -

130%

1899

7 SE

D-4

MS1

2-Me

thylna

phtha

lene

83

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

128.3

9999

39ng

PAHs

91-5

7-6

50 -

120%

1899

7 SE

D-4

MS2

2-Me

thylna

phtha

lene

60

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

128.3

9999

39ng

PAHs

91-5

7-6

50 -

120%

1899

7 SE

D-4

R1 2

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1899

7 SE

D-4

R2 2

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1899

7 SE

D-4

MS1

Acen

aphth

ene

97

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

126

ngPA

Hs83

-32-

970

- 13

0%18

997

SED-

4 MS

2 Ac

enap

hthen

e

87%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t12

6ng

PAHs

83-3

2-9

70 -

130%

1899

7 SE

D-4

R1 A

cena

phthe

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

1899

7 SE

D-4

R2 A

cena

phthe

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

1899

7 SE

D-4

MS1

Acen

aphth

ylene

96%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

1.199

9969

ngPA

Hs20

8-96

-870

- 13

0%18

997

SED-

4 MS

2 Ac

enap

hthyle

ne

86

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

131.1

9999

69ng

PAHs

208-

96-8

70 -

130%

1899

7 SE

D-4

R1 A

cena

phthy

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1899

7 SE

D-4

R2 A

cena

phthy

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1899

7 SE

D-4

MS1

Anthr

acen

e

75%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t99

.5ng

PAHs

120-

12-7

70 -

130%

1899

7 SE

D-4

MS2

Anthr

acen

e

99%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t99

.5ng

PAHs

120-

12-7

70 -

130%

1899

7 SE

D-4

R1 A

nthra

cene

2.599

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%18

997

SED-

4 R2

Anth

race

ne

3.7

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

120-

12-7

70 -

130%

1899

7 SE

D-4

MS1

Benz

[a]an

thrac

ene

87

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

114

ngPA

Hs56

-55-

370

- 13

0%18

997

SED-

4 MS

2 Be

nz[a]

anthr

acen

e

114

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

114

ngPA

Hs56

-55-

370

- 13

0%18

997

SED-

4 R1

Ben

z[a]an

thrac

ene

24

.8999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

56-5

5-3

70 -

130%

1899

7 SE

D-4

R2 B

enz[a

]anthr

acen

e

48.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%18

997

SED-

4 MS

1 Be

nzo[a

]pyre

ne

10

6%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

9ng

PAHs

50-3

2-8

70 -

130%

1899

7 SE

D-4

MS2

Benz

o[a]py

rene

101

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

119

ngPA

Hs50

-32-

870

- 13

0%18

997

SED-

4 R1

Ben

zo[a]

pyre

ne

36

.7999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1899

7 SE

D-4

R2 B

enzo

[a]py

rene

76.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1899

7 SE

D-4

MS1

Benz

o[b]flu

oran

thene

84%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

1ng

PAHs

205N

A-2

70 -

130%

OU 1 001297

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

12

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

MS2

Benz

o[b]flu

oran

thene

116

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

131

ngPA

Hs20

5NA-

270

- 13

0%18

997

SED-

4 R1

Ben

zo[b]

fluor

anthe

ne

32

.4000

0153

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

205N

A-2

70 -

130%

1899

7 SE

D-4

R2 B

enzo

[b]flu

oran

thene

61.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%18

997

SED-

4 MS

1 Be

nzo[e

]pyre

ne

87

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

131

ngPA

Hs19

2-97

-270

- 13

0%18

997

SED-

4 MS

2 Be

nzo[e

]pyre

ne

11

6%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

1ng

PAHs

192-

97-2

70 -

130%

1899

7 SE

D-4

R1 B

enzo

[e]py

rene

22.39

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%18

997

SED-

4 R2

Ben

zo[e]

pyre

ne

38

.2000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

192-

97-2

70 -

130%

1899

7 SE

D-4

MS1

Benz

o[g,h,

i]per

ylene

100

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

117

ngPA

Hs19

1-24

-270

- 13

0%18

997

SED-

4 MS

2 Be

nzo[g

,h,i]p

eryle

ne

10

9%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

7ng

PAHs

191-

24-2

70 -

130%

1899

7 SE

D-4

R1 B

enzo

[g,h,i

]peryl

ene

32

.2000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

7 SE

D-4

R2 B

enzo

[g,h,i

]peryl

ene

53

.4000

0153

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

7 SE

D-4

MS1

Benz

o[k]flu

oran

thene

117

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

131

ngPA

Hs20

7-08

-970

- 13

0%18

997

SED-

4 MS

2 Be

nzo[k

]fluor

anthe

ne

12

2%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

1ng

PAHs

207-

08-9

70 -

130%

1899

7 SE

D-4

R1 B

enzo

[k]flu

oran

thene

31.29

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

7-08

-970

- 13

0%18

997

SED-

4 R2

Ben

zo[k]

fluor

anthe

ne

55

.7999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1899

7 SE

D-4

MS1

Biph

enyl

84

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

132

ngPA

Hs92

-52-

450

- 12

0%18

997

SED-

4 MS

2 Bi

phen

yl

74%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

2ng

PAHs

92-5

2-4

50 -

120%

1899

7 SE

D-4

R1 B

iphen

yl ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%18

997

SED-

4 R2

Biph

enyl

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

92-5

2-4

50 -

120%

1899

7 SE

D-4

MS1

Chrys

ene

92

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

132

ngPA

Hs21

8-01

-970

- 13

0%18

997

SED-

4 MS

2 Ch

rysen

e

72%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

2ng

PAHs

218-

01-9

70 -

130%

1899

7 SE

D-4

R1 C

hrys

ene

22

.7000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1899

7 SE

D-4

R2 C

hrys

ene

47

.7000

0076

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1899

7 SE

D-4

R1 D

ibenz

[a,h]a

nthra

cene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs53

-70-

370

- 13

0%18

997

SED-

4 R2

Dibe

nz[a,

h]anth

race

ne

15

.6000

0038

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1899

7 SE

D-4

R1 F

luora

nthen

e

33.40

0001

53ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

6-44

-070

- 13

0%18

997

SED-

4 R2

Fluo

ranth

ene

83

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1899

7 SE

D-4

MS1

Fluor

ene

11

1%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

7ng

PAHs

86-7

3-7

70 -

130%

1899

7 SE

D-4

MS2

Fluor

ene

11

0%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

7ng

PAHs

86-7

3-7

70 -

130%

1899

7 SE

D-4

R1 F

luore

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1899

7 SE

D-4

R2 F

luore

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1899

7 SE

D-4

MS1

Inden

o[1,2,

3-c,d

]pyre

ne

11

3%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

7ng

PAHs

193-

39-5

70 -

130%

1899

7 SE

D-4

MS2

Inden

o[1,2,

3-c,d

]pyre

ne

10

4%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t11

7ng

PAHs

193-

39-5

70 -

130%

1899

7 SE

D-4

R1 In

deno

[1,2,3

-c,d]p

yrene

36.70

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%18

997

SED-

4 R2

Inde

no[1,

2,3-c,

d]pyre

ne

60

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

193-

39-5

70 -

130%

1899

7 SE

D-4

MS1

Naph

thalen

e

75%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

2ng

PAHs

91-2

0-3

50 -

120%

1899

7 SE

D-4

MS2

Naph

thalen

e

70%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t13

2ng

PAHs

91-2

0-3

50 -

120%

1899

7 SE

D-4

R1 N

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%18

997

SED-

4 R2

Nap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-2

0-3

50 -

120%

OU 1 001298

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

13

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

7 SE

D-4

MS1

Peryl

ene

13

0%

Rec

over

y1

58/1

6/04

8/24/0

4 Se

dimen

t99

.4000

0153

ngPA

Hs19

8-55

-070

- 13

0%18

997

SED-

4 MS

2 Pe

rylen

e

125

% R

ecov

ery

15

8/16/0

48/2

4/04

Sedim

ent

99.40

0001

53ng

PAHs

198-

55-0

70 -

130%

1899

7 SE

D-4

R1 P

eryle

ne

9.8

9999

9619

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1899

7 SE

D-4

R2 P

eryle

ne

16

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

8-55

-070

- 13

0%18

997

SED-

4 R1

Phe

nanth

rene

5.199

9998

09ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

997

SED-

4 R2

Phe

nanth

rene

29.70

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

997

SED-

4 R1

Pyre

ne

36

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

129-

00-0

70 -

130%

1899

7 SE

D-4

R2 P

yrene

75.90

0001

53ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%18

997

SED-

4 R1

Tota

l Dete

ctable

PAH

s

329

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%18

997

SED-

4 R2

Tota

l Dete

ctable

PAH

s

669

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%18

998

SED-

5 R1

(d1

0-Ac

enap

hthen

e)

38

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1899

8 SE

D-5

R1 (

d10-

Phen

anthr

ene)

43%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%18

998

SED-

5 R1

(d1

2-Ch

rysen

e)

66

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1899

8 SE

D-5

R1 (

d12-

Peryl

ene)

91%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%18

998

SED-

5 R1

(d8

-Nap

hthale

ne)

22

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1899

8 SE

D-5

R1 1

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

8 SE

D-5

R1 1

-Meth

ylphe

nanth

rene

2ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%18

998

SED-

5 R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%18

998

SED-

5 R1

2,6-

Dime

thylna

phtha

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

581-

42-0

70 -

130%

1899

8 SE

D-5

R1 2

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1899

8 SE

D-5

R1 A

cena

phthe

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

1899

8 SE

D-5

R1 A

cena

phthy

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1899

8 SE

D-5

R1 A

nthra

cene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%18

998

SED-

5 R1

Ben

z[a]an

thrac

ene

10

.8999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

56-5

5-3

70 -

130%

1899

8 SE

D-5

R1 B

enzo

[a]py

rene

23.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1899

8 SE

D-5

R1 B

enzo

[b]flu

oran

thene

17.60

0000

38ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%18

998

SED-

5 R1

Ben

zo[e]

pyre

ne

10

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%18

998

SED-

5 R1

Ben

zo[g,

h,i]pe

rylen

e

15.80

0000

19ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

1-24

-270

- 13

0%18

998

SED-

5 R1

Ben

zo[k]

fluor

anthe

ne

19

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1899

8 SE

D-5

R1 B

iphen

yl ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%18

998

SED-

5 R1

Chr

ysen

e

11.39

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs21

8-01

-970

- 13

0%18

998

SED-

5 R1

Dibe

nz[a,

h]anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1899

8 SE

D-5

R1 F

luora

nthen

e

14.89

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

6-44

-070

- 13

0%18

998

SED-

5 R1

Fluo

rene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs86

-73-

770

- 13

0%18

998

SED-

5 R1

Inde

no[1,

2,3-c,

d]pyre

ne

17

.6000

0038

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

193-

39-5

70 -

130%

1899

8 SE

D-5

R1 N

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%18

998

SED-

5 R1

Per

ylene

5.199

9998

09ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

8-55

-070

- 13

0%18

998

SED-

5 R1

Phe

nanth

rene

3.900

0000

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

998

SED-

5 R1

Pyre

ne

17

.3999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

129-

00-0

70 -

130%

OU 1 001299

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

14

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

8 SE

D-5

R1 T

otal D

etecta

ble P

AHs

16

9.699

9969

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%18

999

SED-

6 R1

(d1

0-Ac

enap

hthen

e)

31

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1899

9 SE

D-6

R1 (

d10-

Phen

anthr

ene)

40%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%18

999

SED-

6 R1

(d1

2-Ch

rysen

e)

65

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1899

9 SE

D-6

R1 (

d12-

Peryl

ene)

90%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%18

999

SED-

6 R1

(d8

-Nap

hthale

ne)

20

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1899

9 SE

D-6

R1 1

-Meth

ylnap

hthale

ne

8.3

9999

9619

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1899

9 SE

D-6

R1 1

-Meth

ylphe

nanth

rene

90.30

0003

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%18

999

SED-

6 R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

16

.8999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%18

999

SED-

6 R1

2,6-

Dime

thylna

phtha

lene

13

.1000

0038

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

581-

42-0

70 -

130%

1899

9 SE

D-6

R1 2

-Meth

ylnap

hthale

ne

9.8

0000

0191

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1899

9 SE

D-6

R1 A

cena

phthe

ne

3.7

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

1899

9 SE

D-6

R1 A

cena

phthy

lene

23

.2999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1899

9 SE

D-6

R1 A

nthra

cene

27.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%18

999

SED-

6 R1

Ben

z[a]an

thrac

ene

30

8ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%18

999

SED-

6 R1

Ben

zo[a]

pyre

ne

45

0ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs50

-32-

870

- 13

0%18

999

SED-

6 R1

Ben

zo[b]

fluor

anthe

ne

27

9ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%18

999

SED-

6 R1

Ben

zo[e]

pyre

ne

25

5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%18

999

SED-

6 R1

Ben

zo[g,

h,i]pe

rylen

e

321

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1899

9 SE

D-6

R1 B

enzo

[k]flu

oran

thene

275

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1899

9 SE

D-6

R1 B

iphen

yl

7.099

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%18

999

SED-

6 R1

Chr

ysen

e

301

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1899

9 SE

D-6

R1 D

ibenz

[a,h]a

nthra

cene

72.69

9996

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs53

-70-

370

- 13

0%18

999

SED-

6 R1

Fluo

ranth

ene

58

1ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

6-44

-070

- 13

0%18

999

SED-

6 R1

Fluo

rene

22ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs86

-73-

770

- 13

0%18

999

SED-

6 R1

Inde

no[1,

2,3-c,

d]pyre

ne

32

6ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%18

999

SED-

6 R1

Nap

hthale

ne

8.1

9999

9809

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-2

0-3

50 -

120%

1899

9 SE

D-6

R1 P

eryle

ne

70

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1899

9 SE

D-6

R1 P

hena

nthre

ne

61

6ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%18

999

SED-

6 R1

Pyre

ne

92

6ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%18

999

SED-

6 R1

Tota

l Dete

ctable

PAH

s

5010

.7001

95ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

70 -

130%

1900

0 SE

D-7

R1 (

d10-

Acen

aphth

ene)

49%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

52

- 12

5%19

000

SED-

7 R1

(d1

0-Ph

enan

thren

e)

67

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

57 -

128%

1900

0 SE

D-7

R1 (

d12-

Chrys

ene)

100

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1900

0 SE

D-7

R1 (

d12-

Peryl

ene)

137

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

53 -

122%

1900

0 SE

D-7

R1 (

d8-N

aphth

alene

)

26%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

47

- 11

0%19

000

SED-

7 R1

1-M

ethyln

aphth

alene

1.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs90

-12-

050

- 12

0%19

000

SED-

7 R1

1-M

ethylp

hena

nthre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

832-

69-9

70 -

130%

1900

0 SE

D-7

R1 2

,3,5-

Trim

ethyln

aphth

alene

2.599

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs22

45-3

8-7

70 -

130%

OU 1 001300

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

15

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

0 SE

D-7

R1 2

,6-Di

methy

lnaph

thalen

e

2.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%19

000

SED-

7 R1

2-M

ethyln

aphth

alene

2.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-57-

650

- 12

0%19

000

SED-

7 R1

Ace

naph

thene

1.399

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

-32-

970

- 13

0%19

000

SED-

7 R1

Ace

naph

thylen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

8-96

-870

- 13

0%19

000

SED-

7 R1

Anth

race

ne

4.1

9999

9809

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

120-

12-7

70 -

130%

1900

0 SE

D-7

R1 B

enz[a

]anthr

acen

e

43.09

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%19

000

SED-

7 R1

Ben

zo[a]

pyre

ne

80

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs50

-32-

870

- 13

0%19

000

SED-

7 R1

Ben

zo[b]

fluor

anthe

ne

68

.4000

0153

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

205N

A-2

70 -

130%

1900

0 SE

D-7

R1 B

enzo

[e]py

rene

44.59

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%19

000

SED-

7 R1

Ben

zo[g,

h,i]pe

rylen

e

61.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

1-24

-270

- 13

0%19

000

SED-

7 R1

Ben

zo[k]

fluor

anthe

ne

59

.5999

9847

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1900

0 SE

D-7

R1 B

iphen

yl

1.899

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%19

000

SED-

7 R1

Chr

ysen

e

45.90

0001

53ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs21

8-01

-970

- 13

0%19

000

SED-

7 R1

Dibe

nz[a,

h]anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1900

0 SE

D-7

R1 F

luora

nthen

e

70.30

0003

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

6-44

-070

- 13

0%19

000

SED-

7 R1

Fluo

rene

2.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs86

-73-

770

- 13

0%19

000

SED-

7 R1

Inde

no[1,

2,3-c,

d]pyre

ne

56

.5ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%19

000

SED-

7 R1

Nap

hthale

ne

2

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-2

0-3

50 -

120%

1900

0 SE

D-7

R1 P

eryle

ne

19

.7999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1900

0 SE

D-7

R1 P

hena

nthre

ne

14

.3999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

85-0

1-8

70 -

130%

1900

0 SE

D-7

R1 P

yrene

71.59

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%19

000

SED-

7 R1

Tota

l Dete

ctable

PAH

s

656.4

0002

44ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

70 -

130%

1900

1 SE

D-8

R1 (

d10-

Acen

aphth

ene)

55%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

52

- 12

5%19

001

SED-

8 R1

(d1

0-Ph

enan

thren

e)

65

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

57 -

128%

1900

1 SE

D-8

R1 (

d12-

Chrys

ene)

89%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

61

- 12

6%19

001

SED-

8 R1

(d1

2-Pe

rylen

e)

12

1%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%19

001

SED-

8 R1

(d8

-Nap

hthale

ne)

33

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

47 -

110%

1900

1 SE

D-8

R1 1

-Meth

ylnap

hthale

ne

1.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1900

1 SE

D-8

R1 1

-Meth

ylphe

nanth

rene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

2-69

-970

- 13

0%19

001

SED-

8 R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%19

001

SED-

8 R1

2,6-

Dime

thylna

phtha

lene

3.2

0000

0048

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

581-

42-0

70 -

130%

1900

1 SE

D-8

R1 2

-Meth

ylnap

hthale

ne

3.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1900

1 SE

D-8

R1 A

cena

phthe

ne

1.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

83-3

2-9

70 -

130%

1900

1 SE

D-8

R1 A

cena

phthy

lene

1.2

9999

9952

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1900

1 SE

D-8

R1 A

nthra

cene

6ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

0-12

-770

- 13

0%19

001

SED-

8 R1

Ben

z[a]an

thrac

ene

62

.4000

0153

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

56-5

5-3

70 -

130%

1900

1 SE

D-8

R1 B

enzo

[a]py

rene

129

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1900

1 SE

D-8

R1 B

enzo

[b]flu

oran

thene

115

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

205N

A-2

70 -

130%

1900

1 SE

D-8

R1 B

enzo

[e]py

rene

74.09

9998

47ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

2-97

-270

- 13

0%

OU 1 001301

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

16

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

1 SE

D-8

R1 B

enzo

[g,h,i

]peryl

ene

11

9ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

1-24

-270

- 13

0%19

001

SED-

8 R1

Ben

zo[k]

fluor

anthe

ne

98

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

207-

08-9

70 -

130%

1900

1 SE

D-8

R1 B

iphen

yl

1.899

9999

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%19

001

SED-

8 R1

Chr

ysen

e

71ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs21

8-01

-970

- 13

0%19

001

SED-

8 R1

Dibe

nz[a,

h]anth

race

ne

30

.3999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1900

1 SE

D-8

R1 F

luora

nthen

e

102

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1900

1 SE

D-8

R1 F

luore

ne

2.0

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1900

1 SE

D-8

R1 In

deno

[1,2,3

-c,d]p

yrene

119

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

193-

39-5

70 -

130%

1900

1 SE

D-8

R1 N

aphth

alene

2.799

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%19

001

SED-

8 R1

Per

ylene

29.79

9999

24ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

8-55

-070

- 13

0%19

001

SED-

8 R1

Phe

nanth

rene

24.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

85-0

1-8

70 -

130%

1900

1 SE

D-8

R1 P

yrene

111

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

129-

00-0

70 -

130%

1900

1 SE

D-8

R1 T

otal D

etecta

ble P

AHs

11

08.80

0049

ng/dr

y g

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

70

- 13

0%19

002

SED-

9 R1

(d1

0-Ac

enap

hthen

e)

28

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1900

2 SE

D-9

R1 (

d10-

Phen

anthr

ene)

44%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

57

- 12

8%19

002

SED-

9 R1

(d1

2-Ch

rysen

e)

81

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1900

2 SE

D-9

R1 (

d12-

Peryl

ene)

107

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

53 -

122%

1900

2 SE

D-9

R1 (

d8-N

aphth

alene

)

12%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

47

- 11

0%19

002

SED-

9 R1

1-M

ethyln

aphth

alene

1.299

9999

52ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs90

-12-

050

- 12

0%19

002

SED-

9 R1

1-M

ethylp

hena

nthre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

832-

69-9

70 -

130%

1900

2 SE

D-9

R1 2

,3,5-

Trim

ethyln

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs22

45-3

8-7

70 -

130%

1900

2 SE

D-9

R1 2

,6-Di

methy

lnaph

thalen

e

2.400

0000

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%19

002

SED-

9 R1

2-M

ethyln

aphth

alene

2.099

9999

05ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-57-

650

- 12

0%19

002

SED-

9 R1

Ace

naph

thene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

-32-

970

- 13

0%19

002

SED-

9 R1

Ace

naph

thylen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

8-96

-870

- 13

0%19

002

SED-

9 R1

Anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

120-

12-7

70 -

130%

1900

2 SE

D-9

R1 B

enz[a

]anthr

acen

e

10.69

9999

81ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs56

-55-

370

- 13

0%19

002

SED-

9 R1

Ben

zo[a]

pyre

ne

16

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1900

2 SE

D-9

R1 B

enzo

[b]flu

oran

thene

21.20

0000

76ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

5NA-

270

- 13

0%19

002

SED-

9 R1

Ben

zo[e]

pyre

ne

14

.8000

0019

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

192-

97-2

70 -

130%

1900

2 SE

D-9

R1 B

enzo

[g,h,i

]peryl

ene

20

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

191-

24-2

70 -

130%

1900

2 SE

D-9

R1 B

enzo

[k]flu

oran

thene

15.89

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

7-08

-970

- 13

0%19

002

SED-

9 R1

Biph

enyl

2.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

92-5

2-4

50 -

120%

1900

2 SE

D-9

R1 C

hrys

ene

11

.8999

9962

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1900

2 SE

D-9

R1 D

ibenz

[a,h]a

nthra

cene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs53

-70-

370

- 13

0%19

002

SED-

9 R1

Fluo

ranth

ene

19

.2999

9924

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1900

2 SE

D-9

R1 F

luore

ne

1

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

86-7

3-7

70 -

130%

1900

2 SE

D-9

R1 In

deno

[1,2,3

-c,d]p

yrene

16.89

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%19

002

SED-

9 R1

Nap

hthale

ne

1.6

0000

0024

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-2

0-3

50 -

120%

OU 1 001302

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

17

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

2 SE

D-9

R1 P

eryle

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1900

2 SE

D-9

R1 P

hena

nthre

ne

6.5

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

85-0

1-8

70 -

130%

1900

2 SE

D-9

R1 P

yrene

19.89

9999

62ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs12

9-00

-070

- 13

0%19

002

SED-

9 R1

Tota

l Dete

ctable

PAH

s

184.1

0000

61ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

70 -

130%

1900

3 SE

D-10

R1

(d1

0-Ac

enap

hthen

e)

55

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

52 -

125%

1900

3 SE

D-10

R1

(d1

0-Ph

enan

thren

e)

65

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

57 -

128%

1900

3 SE

D-10

R1

(d1

2-Ch

rysen

e)

86

% R

ecov

ery

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

61 -

126%

1900

3 SE

D-10

R1

(d1

2-Pe

rylen

e)

10

6%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53

- 12

2%19

003

SED-

10

R1 (

d8-N

aphth

alene

)

26%

Rec

over

y

8/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

47

- 11

0%19

003

SED-

10

R1 1

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

90-1

2-0

50 -

120%

1900

3 SE

D-10

R1

1-M

ethylp

hena

nthre

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

832-

69-9

70 -

130%

1900

3 SE

D-10

R1

2,3,

5-Tr

imeth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

2245

-38-

770

- 13

0%19

003

SED-

10

R1 2

,6-Di

methy

lnaph

thalen

e ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs58

1-42

-070

- 13

0%19

003

SED-

10

R1 2

-Meth

ylnap

hthale

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

91-5

7-6

50 -

120%

1900

3 SE

D-10

R1

Ace

naph

thene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs83

-32-

970

- 13

0%19

003

SED-

10

R1 A

cena

phthy

lene

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

208-

96-8

70 -

130%

1900

3 SE

D-10

R1

Anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

120-

12-7

70 -

130%

1900

3 SE

D-10

R1

Ben

z[a]an

thrac

ene

5.3

0000

0191

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

56-5

5-3

70 -

130%

1900

3 SE

D-10

R1

Ben

zo[a]

pyre

ne

8.1

0000

0381

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

50-3

2-8

70 -

130%

1900

3 SE

D-10

R1

Ben

zo[b]

fluor

anthe

ne

7

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

205N

A-2

70 -

130%

1900

3 SE

D-10

R1

Ben

zo[e]

pyre

ne

5.0

9999

9905

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

192-

97-2

70 -

130%

1900

3 SE

D-10

R1

Ben

zo[g,

h,i]pe

rylen

e

6.400

0000

95ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

1-24

-270

- 13

0%19

003

SED-

10

R1 B

enzo

[k]flu

oran

thene

8.300

0001

91ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs20

7-08

-970

- 13

0%19

003

SED-

10

R1 B

iphen

yl ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs92

-52-

450

- 12

0%19

003

SED-

10

R1 C

hrys

ene

5.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

218-

01-9

70 -

130%

1900

3 SE

D-10

R1

Dibe

nz[a,

h]anth

race

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

53-7

0-3

70 -

130%

1900

3 SE

D-10

R1

Fluo

ranth

ene

7

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

206-

44-0

70 -

130%

1900

3 SE

D-10

R1

Fluo

rene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs86

-73-

770

- 13

0%19

003

SED-

10

R1 In

deno

[1,2,3

-c,d]p

yrene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs19

3-39

-570

- 13

0%19

003

SED-

10

R1 N

aphth

alene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs91

-20-

350

- 12

0%19

003

SED-

10

R1 P

eryle

ne

ND

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

198-

55-0

70 -

130%

1900

3 SE

D-10

R1

Phe

nanth

rene

ND

ng

/dry g

15

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs85

-01-

870

- 13

0%19

003

SED-

10

R1 P

yrene

11.5

ng/dr

y g1

58/1

6/04

8/23/0

4 Se

dimen

t ng

PAHs

129-

00-0

70 -

130%

1900

3 SE

D-10

R1

Tota

l Dete

ctable

PAH

s

64.19

9996

95ng

/dry g

8/16/0

48/2

3/04

Sedim

ent

ngPA

Hs

70 -

130%

1899

3 QA

QC

B1 A

luminu

m (A

l) ND

mg

/dry k

g1

57/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Anti

mony

(Sb)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

40 -

160%

1899

3 QA

QC

B1 A

rsenic

(As)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

65

- 13

5%18

993

QAQC

B1

Bar

ium (B

a)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Ber

yllium

(Be)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

70 -

130%

OU 1 001303

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

18

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

3 QA

QC

B1 C

admi

um (C

d)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

60

- 14

0%18

993

QAQC

B1

Chr

omium

(Cr)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Cob

alt (C

o)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Cop

per (

Cu)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Iron

(Fe)

ND

mg

/dry k

g1

57/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Lea

d (Pb

) ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 M

anga

nese

(Mn)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 M

ercu

ry (H

g)

ND

mg/dr

y kg

0.005

0.01

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 M

olybd

enum

(Mo)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 N

ickel

(Ni)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Sele

nium

(Se)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

40 -

160%

1899

3 QA

QC

B1 S

ilver

(Ag)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 S

tronti

um (S

r) ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 T

halliu

m (T

l) ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

3 QA

QC

B1 T

in (S

n)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

60

- 14

0%18

993

QAQC

B1

Tita

nium

(Ti)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Van

adium

(V)

ND

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 DI

Wate

r

µgTr

ace M

etals

75

- 12

5%18

993

QAQC

B1

Zinc

(Zn)

ND

mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

DI W

ater

µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 A

luminu

m (A

l)

3590

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 A

ntimo

ny (S

b)

6.7

6999

9981

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

4 SE

D-1

R1 A

rsenic

(As)

14

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1899

4 SE

D-1

R1 B

arium

(Ba)

313

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 B

eryll

ium (B

e)

0.7

5999

999

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

70 -

130%

1899

4 SE

D-1

R1 C

admi

um (C

d)

4.5

7999

9924

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1899

4 SE

D-1

R1 C

hrom

ium (C

r)

81mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

994

SED-

1 R1

Cob

alt (C

o)

17

.3999

9962

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 C

oppe

r (Cu

)

272

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 Ir

on (F

e)

53

500

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

994

SED-

1 R1

Lea

d (Pb

)

292

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 M

anga

nese

(Mn)

486

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 M

ercu

ry (H

g)

0.6

3999

9986

mg/dr

y kg

0.005

0.01

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

994

SED-

1 R1

Moly

bden

um (M

o)

15

.3000

0019

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 N

ickel

(Ni)

42

.5999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 S

eleniu

m (S

e)

2.0

9999

9905

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

4 SE

D-1

R1 S

ilver

(Ag)

1.850

0000

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

994

SED-

1 R1

Stro

ntium

(Sr)

92

.8000

0305

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 T

halliu

m (T

l)

0.519

9999

81mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

994

SED-

1 R1

Tin

(Sn)

24.70

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

994

SED-

1 R1

Tita

nium

(Ti)

28

30mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%

OU 1 001304

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

19

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

4 SE

D-1

R1 V

anad

ium (V

)

138

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

4 SE

D-1

R1 Z

inc (Z

n)

10

20mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Alum

inum

(Al)

Offsc

ale

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Anti

mony

(Sb)

0.370

0000

05mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

995

SED-

2 R1

Arse

nic (A

s)

5.460

0000

38mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

65

- 13

5%18

995

SED-

2 R1

Bar

ium (B

a)

10

3mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Ber

yllium

(Be)

0.370

0000

05mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%18

995

SED-

2 R1

Cad

mium

(Cd)

0.319

9999

93mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

995

SED-

2 R1

Chr

omium

(Cr)

27

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 C

obalt

(Co)

7.980

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Cop

per (

Cu)

37

.7999

9924

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 Ir

on (F

e)

28

200

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Lea

d (Pb

)

24.39

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Man

gane

se (M

n)

26

7mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Mer

cury

(Hg)

0.239

9999

95mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 M

olybd

enum

(Mo)

1.549

9999

52mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Nick

el (N

i)

11.5

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 S

eleniu

m (S

e)

0.5

6999

9993

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

5 SE

D-2

R1 S

ilver

(Ag)

0.400

0000

06mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Stro

ntium

(Sr)

11

0mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Tha

llium

(Tl)

0.3

1000

0002

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 T

in (S

n)

3.0

3999

9962

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1899

5 SE

D-2

R1 T

itaniu

m (T

i)

1540

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

5 SE

D-2

R1 V

anad

ium (V

)

60.29

9999

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

995

SED-

2 R1

Zinc

(Zn)

99mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Alum

inum

(Al)

Offsc

ale

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Anti

mony

(Sb)

1.940

0000

57mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

996

SED-

3 R1

Arse

nic (A

s)

7.090

0001

53mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

65

- 13

5%18

996

SED-

3 R1

Bar

ium (B

a)

15

1mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Ber

yllium

(Be)

0.439

9999

98mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%18

996

SED-

3 R1

Cad

mium

(Cd)

1.350

0000

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

996

SED-

3 R1

Chr

omium

(Cr)

54

.4000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 C

obalt

(Co)

10.39

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Cop

per (

Cu)

12

6mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Iron

(Fe)

3320

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 L

ead (

Pb)

11

0mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Man

gane

se (M

n)

26

8mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Mer

cury

(Hg)

0.310

0000

02mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 M

olybd

enum

(Mo)

3.140

0001

05mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%

OU 1 001305

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

20

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

6 SE

D-3

R1 N

ickel

(Ni)

20

.6000

0038

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 S

eleniu

m (S

e)

0.9

5999

9979

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

6 SE

D-3

R1 S

ilver

(Ag)

0.860

0000

14mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Stro

ntium

(Sr)

53

.9000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 T

halliu

m (T

l)

0.300

0000

12mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Tin

(Sn)

9.880

0001

14mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

996

SED-

3 R1

Tita

nium

(Ti)

17

00mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

996

SED-

3 R1

Van

adium

(V)

81

.4000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

6 SE

D-3

R1 Z

inc (Z

n)

35

8mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Alum

inum

(Al)

Offsc

ale

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Anti

mony

(Sb)

6.760

0002

29mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

997

SED-

4 R1

Arse

nic (A

s)

4.880

0001

14mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

65

- 13

5%18

997

SED-

4 R1

Bar

ium (B

a)

10

6mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Ber

yllium

(Be)

0.409

9999

96mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%18

997

SED-

4 R1

Cad

mium

(Cd)

0.319

9999

93mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

997

SED-

4 R1

Chr

omium

(Cr)

28

.7999

9924

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 C

obalt

(Co)

8.810

0004

2mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Cop

per (

Cu)

33

.0999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 Ir

on (F

e)

27

600

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Lea

d (Pb

)

2720

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 M

anga

nese

(Mn)

212

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 M

ercu

ry (H

g)

0.0

9000

0004

mg/dr

y kg

0.005

0.01

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Moly

bden

um (M

o)

2.3

9000

0105

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 N

ickel

(Ni)

11

.8999

9962

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 S

eleniu

m (S

e)

0.5

8999

9974

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

7 SE

D-4

R1 S

ilver

(Ag)

0.439

9999

98mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Stro

ntium

(Sr)

38

.5999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 T

halliu

m (T

l)

0.349

9999

94mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Tin

(Sn)

10.80

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

997

SED-

4 R1

Tita

nium

(Ti)

15

00mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

997

SED-

4 R1

Van

adium

(V)

62

.9000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

7 SE

D-4

R1 Z

inc (Z

n)

15

1mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Alum

inum

(Al)

Offsc

ale

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Anti

mony

(Sb)

0.389

9999

86mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

998

SED-

5 R1

Arse

nic (A

s)

18.29

9999

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

65

- 13

5%18

998

SED-

5 R1

Bar

ium (B

a)

14

2mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Ber

yllium

(Be)

0.689

9999

98mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%18

998

SED-

5 R1

Cad

mium

(Cd)

0.280

0000

01mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

998

SED-

5 R1

Chr

omium

(Cr)

60

.5999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

OU 1 001306

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

21

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1899

8 SE

D-5

R1 C

obalt

(Co)

13.80

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Cop

per (

Cu)

40

.2000

0076

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

8 SE

D-5

R1 Ir

on (F

e)

41

400

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Lea

d (Pb

)

19.70

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Man

gane

se (M

n)

35

9mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Mer

cury

(Hg)

0.109

9999

99mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

8 SE

D-5

R1 M

olybd

enum

(Mo)

3.130

0001

14mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Nick

el (N

i)

19.89

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Sele

nium

(Se)

1.179

9999

48mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

998

SED-

5 R1

Silv

er (A

g)

0.5

5000

0012

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

8 SE

D-5

R1 S

tronti

um (S

r)

54.5

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

8 SE

D-5

R1 T

halliu

m (T

l)

0.479

9999

89mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Tin

(Sn)

2.930

0000

67mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

998

SED-

5 R1

Tita

nium

(Ti)

24

30mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Van

adium

(V)

11

9mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

998

SED-

5 R1

Zinc

(Zn)

107

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 A

luminu

m (A

l) Of

fscale

mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 A

ntimo

ny (S

b)

1.1

3999

9986

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1899

9 SE

D-6

R1 A

rsenic

(As)

4.1

1000

0134

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1899

9 SE

D-6

R1 B

arium

(Ba)

124

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 B

eryll

ium (B

e)

0.2

5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%18

999

SED-

6 R1

Cad

mium

(Cd)

0.730

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%18

999

SED-

6 R1

Chr

omium

(Cr)

29

.3999

9962

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 C

obalt

(Co)

5.309

9999

43mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Cop

per (

Cu)

57

.5999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 Ir

on (F

e)

16

900

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Lea

d (Pb

)

50mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Man

gane

se (M

n)

15

7mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Mer

cury

(Hg)

0.540

0000

21mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 M

olybd

enum

(Mo)

1.529

9999

71mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Nick

el (N

i)

14.80

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Sele

nium

(Se)

0.529

9999

71mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%18

999

SED-

6 R1

Silv

er (A

g)

0.5

5000

0012

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 S

tronti

um (S

r)

52.09

9998

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Tha

llium

(Tl)

0.1

8000

0007

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 T

in (S

n)

4.4

8999

9771

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1899

9 SE

D-6

R1 T

itaniu

m (T

i)

923

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1899

9 SE

D-6

R1 V

anad

ium (V

)

40.20

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%18

999

SED-

6 R1

Zinc

(Zn)

253

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

OU 1 001307

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

22

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

0 SE

D-7

R1 A

luminu

m (A

l) Of

fscale

mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 A

ntimo

ny (S

b)

0.6

4999

9976

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1900

0 SE

D-7

R1 A

rsenic

(As)

4.8

6999

9886

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1900

0 SE

D-7

R1 B

arium

(Ba)

101

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 B

eryll

ium (B

e)

0.3

4999

9994

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

70 -

130%

1900

0 SE

D-7

R1 C

admi

um (C

d)

0.6

3999

9986

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

0 SE

D-7

R1 C

hrom

ium (C

r)

28.20

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Cob

alt (C

o)

7.7

5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Cop

per (

Cu)

56

.2999

9924

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 Ir

on (F

e)

25

600

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Lea

d (Pb

)

36.09

9998

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Man

gane

se (M

n)

21

7mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Mer

cury

(Hg)

0.119

9999

97mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 M

olybd

enum

(Mo)

1.950

0000

48mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Nick

el (N

i)

10.89

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Sele

nium

(Se)

0.680

0000

07mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%19

000

SED-

7 R1

Silv

er (A

g)

0.5

8999

9974

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 S

tronti

um (S

r)

43.29

9999

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Tha

llium

(Tl)

0.2

8000

0001

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 T

in (S

n)

3.7

7999

9971

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

0 SE

D-7

R1 T

itaniu

m (T

i)

1550

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

0 SE

D-7

R1 V

anad

ium (V

)

62.59

9998

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

000

SED-

7 R1

Zinc

(Zn)

169

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 A

luminu

m (A

l) Of

fscale

mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 A

ntimo

ny (S

b)

0.7

2000

0029

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1900

1 SE

D-8

R1 A

rsenic

(As)

5.3

6999

9886

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1900

1 SE

D-8

R1 B

arium

(Ba)

109

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 B

eryll

ium (B

e)

0.4

0999

9996

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

70 -

130%

1900

1 SE

D-8

R1 C

admi

um (C

d)

0.8

8999

9986

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

1 SE

D-8

R1 C

hrom

ium (C

r)

32.79

9999

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Cob

alt (C

o)

8.4

8999

9771

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 C

oppe

r (Cu

)

74.19

9996

95mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Iron

(Fe)

2850

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 L

ead (

Pb)

49

.0999

9847

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 M

anga

nese

(Mn)

238

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 M

ercu

ry (H

g)

0.1

2999

9995

mg/dr

y kg

0.005

0.01

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Moly

bden

um (M

o)

2.1

9000

0057

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 N

ickel

(Ni)

12

.1000

0038

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 S

eleniu

m (S

e)

0.7

9000

0021

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

OU 1 001308

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

23

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

1 SE

D-8

R1 S

ilver

(Ag)

0.730

0000

19mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Stro

ntium

(Sr)

58

.2000

0076

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

1 SE

D-8

R1 T

halliu

m (T

l)

0.280

0000

01mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Tin

(Sn)

4.809

9999

43mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%19

001

SED-

8 R1

Tita

nium

(Ti)

15

00mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Van

adium

(V)

74

.5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

001

SED-

8 R1

Zinc

(Zn)

207

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 A

luminu

m (A

l) Of

fscale

mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 A

ntimo

ny (S

b)

0.8

8999

9986

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1900

2 SE

D-9

R1 A

rsenic

(As)

7.9

2999

9828

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1900

2 SE

D-9

R1 B

arium

(Ba)

142

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 B

eryll

ium (B

e)

0.6

7000

0017

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

70 -

130%

1900

2 SE

D-9

R1 C

admi

um (C

d)

0.8

3999

9974

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

2 SE

D-9

R1 C

hrom

ium (C

r)

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

002

SED-

9 R1

Cob

alt (C

o)

13

.3000

0019

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 C

oppe

r (Cu

)

98.19

9996

95mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

002

SED-

9 R1

Iron

(Fe)

4350

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 L

ead (

Pb)

46

.4000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 M

anga

nese

(Mn)

321

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 M

ercu

ry (H

g)

0.1

4000

0001

mg/dr

y kg

0.005

0.01

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

002

SED-

9 R1

Moly

bden

um (M

o)

4.3

8999

9866

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 N

ickel

(Ni)

19

.5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

002

SED-

9 R1

Sele

nium

(Se)

1.350

0000

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%19

002

SED-

9 R1

Silv

er (A

g)

1.1

2000

0005

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 S

tronti

um (S

r)

76.59

9998

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

002

SED-

9 R1

Tha

llium

(Tl)

0.4

3999

9998

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 T

in (S

n)

7.1

3999

9866

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

2 SE

D-9

R1 T

itaniu

m (T

i)

2180

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 V

anad

ium (V

)

107

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

2 SE

D-9

R1 Z

inc (Z

n)

25

5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 A

luminu

m (A

l) Of

fscale

mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Alum

inum

(Al)

Offsc

ale

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 A

ntimo

ny (S

b)

0.3

7999

9995

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1900

3 SE

D-10

R2

Anti

mony

(Sb)

0.379

9999

95mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%19

003

SED-

10

MS1

Antim

ony (

Sb)

10

7%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

40 -

160%

1900

3 SE

D-10

MS

2 An

timon

y (Sb

)

109

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

40

- 16

0%19

003

SED-

10

R1 A

rsenic

(As)

4.0

9000

0153

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

65 -

135%

1900

3 SE

D-10

R2

Arse

nic (A

s)

4.039

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

65

- 13

5%19

003

SED-

10

MS1

Arse

nic (A

s)

91%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

65 -

135%

OU 1 001309

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

24

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

MS

2 Ar

senic

(As)

93

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

65

- 13

5%19

003

SED-

10

R1 B

arium

(Ba)

81.69

9996

95mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 B

arium

(Ba)

92.40

0001

53mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Bariu

m (B

a)

10

9%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

2 Ba

rium

(Ba)

111

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 B

eryll

ium (B

e)

0.2

7000

0011

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

70 -

130%

1900

3 SE

D-10

R2

Ber

yllium

(Be)

0.280

0000

01mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

70

- 13

0%19

003

SED-

10

MS1

Beryl

lium

(Be)

83%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

70 -

130%

1900

3 SE

D-10

MS

2 Be

rylliu

m (B

e)

84

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

70

- 13

0%19

003

SED-

10

R1 C

admi

um (C

d)

0.4

6999

9999

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

3 SE

D-10

R2

Cad

mium

(Cd)

0.5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%19

003

SED-

10

MS1

Cadm

ium (C

d)

97

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

60

- 14

0%19

003

SED-

10

MS2

Cadm

ium (C

d)

98

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

60

- 14

0%19

003

SED-

10

R1 C

hrom

ium (C

r)

23.79

9999

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 C

hrom

ium (C

r)

24.39

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Chro

mium

(Cr)

97

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Chro

mium

(Cr)

99

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 C

obalt

(Co)

6.440

0000

57mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 C

obalt

(Co)

6.340

0001

53mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Coba

lt (Co

)

94%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

2 Co

balt (

Co)

98

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 C

oppe

r (Cu

)

41.70

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 C

oppe

r (Cu

)

41.09

9998

47mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Copp

er (C

u)

89

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Copp

er (C

u)

91

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 Ir

on (F

e)

22

200

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 Ir

on (F

e)

21

900

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 L

ead (

Pb)

14

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Lea

d (Pb

)

14.39

9999

62mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Lead

(Pb)

94%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

2 Le

ad (P

b)

98

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 M

anga

nese

(Mn)

180

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Man

gane

se (M

n)

17

5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Mang

anes

e (Mn

)

95%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

2 Ma

ngan

ese (

Mn)

10

7%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Mer

cury

(Hg)

0.050

0000

01mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Mer

cury

(Hg)

0.050

0000

01mg

/dry k

g0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Me

rcury

(Hg)

84%

Rec

over

y0.0

050.0

17/2

9/04

7/30/0

4 Se

dimen

t0.0

5000

0001

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Mercu

ry (H

g)

86

% R

ecov

ery

0.005

0.01

7/29/0

47/3

0/04

Sedim

ent

0.050

0000

01µg

Trac

e Meta

ls

75 -

125%

OU 1 001310

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

25

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

R1

Moly

bden

um (M

o)

3.9

2000

0076

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Moly

bden

um (M

o)

3.9

0000

0095

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Mo

lybde

num

(Mo)

110

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Molyb

denu

m (M

o)

11

3%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Nick

el (N

i)

8.420

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 N

ickel

(Ni)

8.3

6999

9886

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Ni

ckel

(Ni)

91

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Nick

el (N

i)

94%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Sele

nium

(Se)

0.600

0000

24mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

40

- 16

0%19

003

SED-

10

R2 S

eleniu

m (S

e)

0.5

5000

0012

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

40 -

160%

1900

3 SE

D-10

MS

1 Se

lenium

(Se)

89%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

40 -

160%

1900

3 SE

D-10

MS

2 Se

lenium

(Se)

89%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

40 -

160%

1900

3 SE

D-10

R1

Silv

er (A

g)

0.5

6000

0002

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Silv

er (A

g)

0.5

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Si

lver (

Ag)

97

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Silve

r (Ag

)

99%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Stro

ntium

(Sr)

43

.7000

0076

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R2

Stro

ntium

(Sr)

38

.2000

0076

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 St

ronti

um (S

r)

104

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Stro

ntium

(Sr)

10

7%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Tha

llium

(Tl)

0.2

5mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 T

halliu

m (T

l)

0.25

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Th

allium

(Tl)

95

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Thall

ium (T

l)

96%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

R1

Tin

(Sn)

2.529

9999

71mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

60

- 14

0%19

003

SED-

10

R2 T

in (S

n)

2.4

6000

0038

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

60 -

140%

1900

3 SE

D-10

MS

1 Tin

(Sn)

113

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

60

- 14

0%19

003

SED-

10

MS2

Tin (S

n)

11

6%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

60 -

140%

1900

3 SE

D-10

R1

Tita

nium

(Ti)

13

40mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 T

itaniu

m (T

i)

1290

mg/dr

y kg

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

1 Tit

anium

(Ti)

96

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS2

Titan

ium (T

i)

116

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 V

anad

ium (V

)

54.70

0000

76mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 V

anad

ium (V

)

53.40

0001

53mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Vana

dium

(V)

10

2%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

3 SE

D-10

MS

2 Va

nadiu

m (V

)

104

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R1 Z

inc (Z

n)

10

3mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

R2 Z

inc (Z

n)

10

4mg

/dry k

g0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75

- 12

5%19

003

SED-

10

MS1

Zinc (

Zn)

76

% R

ecov

ery

0.025

0.050

0000

017/2

9/04

7/30/0

4 Se

dimen

t2

µgTr

ace M

etals

75

- 12

5%

OU 1 001311

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

26

App

endi

x B

: Ta

ble

8.

Sedi

men

t Che

mis

try R

esul

ts fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Sample ID

Client Sample ID

Replicate Number

Parameter

Qualifier

Result

Units

MDL

RL

DateProcessed

DateAnalyzed

Matrix

True Value

Units

Group

CAS No

Acceptance Range

Comment

1900

3 SE

D-10

MS

2 Zin

c (Zn

)

78%

Rec

over

y0.0

250.0

5000

0001

7/29/0

47/3

0/04

Sedim

ent

2µg

Trac

e Meta

ls

75 -

125%

1900

0SE

D-7

R1Al

uminu

m (A

l) 26

530

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1899

9SE

D-6

R1Al

uminu

m (A

l) 16

610

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1899

8SE

D-5

R1Al

uminu

m (A

l) 56

860

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1900

3SE

D-10

R1Al

uminu

m (A

l) 20

270

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1899

3QA

QCB1

Alum

inum

(Al)

NDmg

/dry k

g1

57/2

9/04

7/30/0

4 DI

Wate

rµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

994

SED-

1R1

Alum

inum

(Al)

4648

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis19

003

SED-

10R2

Alum

inum

(Al)

2307

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

995

SED-

2R1

Alum

inum

(Al)

2850

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

997

SED-

4R1

Alum

inum

(Al)

3258

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis19

002

SED-

9R1

Alum

inum

(Al)

4925

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis19

001

SED-

8R1

Alum

inum

(Al)

2922

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

996

SED-

3R1

Alum

inum

(Al)

3152

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

997

SED-

4R1

Iron (

Fe)

2926

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis19

000

SED-

7R1

Iron (

Fe)

2608

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

995

SED-

2R1

Iron (

Fe)

2715

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

994

SED-

1R1

Iron (

Fe)

4402

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

996

SED-

3R1

Iron (

Fe)

3418

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

999

SED-

6R1

Iron (

Fe)

1609

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

998

SED-

5R1

Iron (

Fe)

4554

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis19

003

SED-

10R1

Iron (

Fe)

1982

0mg

/dry k

g1

57/2

9/04

7/30/0

4 Se

dimen

tµg

Trac

e Meta

ls 75

- 12

5%Re

analy

sis18

993

QAQC

B1Iro

n (Fe

) ND

mg/dr

y kg

15

7/29/0

47/3

0/04

DI W

ater

µgTr

ace M

etals

75 -

125%

Rean

alysis

1900

3SE

D-10

R2Iro

n (Fe

) 22

250

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1900

2SE

D-9

R1Iro

n (Fe

) 40

740

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

1900

1SE

D-8

R1Iro

n (Fe

) 26

710

mg/dr

y kg

15

7/29/0

47/3

0/04

Sedim

ent

µgTr

ace M

etals

75 -

125%

Rean

alysis

B1 =

QAQ

C sa

mple

DI

Wate

r = D

eioniz

ed W

ater

E =

Estim

ated

MDL =

Meth

od D

etecti

on Li

mit

MEC

= ME

C An

alytic

al Sy

stems

, Inc.

mg/dr

y kg =

milli

gram

s per

dry k

ilogr

am

mm =

milli

meter

MS

= M

atrix

Spike

ND =

Non

detec

t ng

= na

nogr

ams

ng/dr

y g =

nano

gram

s per

dry g

ram

QAQC

= Q

uality

Ass

uran

ce / Q

uality

Con

trol

R1 =

Rep

licate

1 R2

= R

eplic

ate 2

RL =

Rep

ortin

g Lim

it Se

d-# =

samp

ling l

ocati

on nu

mber

ug

= m

icrog

rams

ug

/dry g

= m

icrog

rams

per d

ry gr

am

OU 1 001312

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

27

App

endi

x B

: Ta

ble

9.

Sedi

men

t Che

mis

try –

Bat

ch In

form

atio

n fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Project ID

Project Description

Client Sample ID

Batch ID

DateSampled

Time Collected

DateReceived

Client Name

Project Officer

Instrument

Analyst

Group

Method

2411

2

QAQC

24

112-

1100

9

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

QA

QC

2411

2-11

009

ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

QA

QC

2411

2-11

009

ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

QA

QC

2411

2-11

009

ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

QA

QC

2411

2-10

062

ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2

QAQC

24

112-

1006

2

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

1 24

112-

1100

9 7/2

1/200

413

:23

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

1 24

112-

1100

9 7/2

1/200

413

:23

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Chlor

inated

Pes

ticide

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-1

2411

2-11

009

7/21/2

004

13:23

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

1 24

112-

1100

9 7/2

1/200

413

:23

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PAHs

EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-1

2411

2-10

062

7/21/2

004

13:23

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-1

2411

2-10

062

7/21/2

004

13:23

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-10

24

112-

1100

9 7/2

1/200

409

:18

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

10

2411

2-11

009

7/21/2

004

09:18

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

10

2411

2-11

009

7/21/2

004

09:18

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

10

2411

2-11

009

7/21/2

004

09:18

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

10

2411

2-10

062

7/21/2

004

09:18

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-10

24

112-

1006

2 7/2

1/200

409

:18

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

2 24

112-

1100

9 7/2

1/200

412

:44

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

2 24

112-

1100

9 7/2

1/200

412

:44

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Chlor

inated

Pes

ticide

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-2

2411

2-11

009

7/21/2

004

12:44

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

2 24

112-

1100

9 7/2

1/200

412

:44

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PAHs

EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-2

2411

2-10

062

7/21/2

004

12:44

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-2

2411

2-10

062

7/21/2

004

12:44

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-3

2411

2-11

009

7/21/2

004

13:53

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ar

oclor

PCB

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-3

2411

2-11

009

7/21/2

004

13:53

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

3 24

112-

1100

9 7/2

1/200

413

:53

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PCB

Cong

ener

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-3

2411

2-11

009

7/21/2

004

13:53

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

3 24

112-

1006

2 7/2

1/200

413

:53

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

3 24

112-

1006

2 7/2

1/200

413

:53

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

4 24

112-

1100

9 7/2

1/200

414

:38

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

4 24

112-

1100

9 7/2

1/200

414

:38

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Chlor

inated

Pes

ticide

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-4

2411

2-11

009

7/21/2

004

14:38

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

4 24

112-

1100

9 7/2

1/200

414

:38

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PAHs

EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-4

2411

2-10

062

7/21/2

004

14:38

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-4

2411

2-10

062

7/21/2

004

14:38

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-5

2411

2-11

009

7/22/2

004

13:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ar

oclor

PCB

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-5

2411

2-11

009

7/22/2

004

13:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

5 24

112-

1100

9 7/2

2/200

413

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PCB

Cong

ener

s EP

A 82

70C

OU 1 001313

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

28

App

endi

x B

: Ta

ble

9.

Sedi

men

t Che

mis

try –

Bat

ch In

form

atio

n fo

r the

Par

adis

e M

arsh

Con

tam

inan

ts In

vest

igat

ion,

San

Die

go, C

A.*

(c

ontin

ued

from

pre

viou

s pag

e)

Project ID

Project Description

Client Sample ID

Batch ID

DateSampled

Time Collected

DateReceived

Client Name

Project Officer

Instrument

Analyst

Group

Method

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-5

2411

2-11

009

7/22/2

004

13:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

5 24

112-

1006

2 7/2

2/200

413

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

5 24

112-

1006

2 7/2

2/200

413

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

6 24

112-

1100

9 7/2

2/200

412

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

6 24

112-

1100

9 7/2

2/200

412

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Chlor

inated

Pes

ticide

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-6

2411

2-11

009

7/22/2

004

12:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

6 24

112-

1100

9 7/2

2/200

412

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PAHs

EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-6

2411

2-10

062

7/22/2

004

12:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-6

2411

2-10

062

7/22/2

004

12:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-7

2411

2-11

009

7/22/2

004

11:42

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ar

oclor

PCB

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-7

2411

2-11

009

7/22/2

004

11:42

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

7 24

112-

1100

9 7/2

2/200

411

:42

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PCB

Cong

ener

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-7

2411

2-11

009

7/22/2

004

11:42

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

7 24

112-

1006

2 7/2

2/200

411

:42

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

7 24

112-

1006

2 7/2

2/200

411

:42

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

8 24

112-

1100

9 7/2

2/200

410

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Aroc

lor P

CBs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

8 24

112-

1100

9 7/2

2/200

410

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

Chlor

inated

Pes

ticide

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-8

2411

2-11

009

7/22/2

004

10:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PC

B Co

ngen

ers

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

8 24

112-

1100

9 7/2

2/200

410

:30

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PAHs

EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-8

2411

2-10

062

7/22/2

004

10:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-8

2411

2-10

062

7/22/2

004

10:30

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

ICPM

S #1

HP

4500

P.

Her

shelm

an

Trac

e Meta

ls EP

A 60

20

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-9

2411

2-11

009

7/22/2

004

09:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ar

oclor

PCB

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-9

2411

2-11

009

7/22/2

004

09:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

Ch

lorina

ted P

estic

ides

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

9 24

112-

1100

9 7/2

2/200

409

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s GC

/MS

#3 A

gilen

t 689

0/597

3S.

Bote

ro

PCB

Cong

ener

s EP

A 82

70C

2411

2 SC

CWRP

/USF

WS-

Para

dise M

arsh

SE

D-9

2411

2-11

009

7/22/2

004

09:35

7/2

7/200

4ME

C An

alytic

al Su

sie W

atts

GC/M

S #3

Agil

ent 6

890/5

973

S. B

otero

PA

Hs

EPA

8270

C 24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

9 24

112-

1006

2 7/2

2/200

409

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

24

112

SCCW

RP/U

SFW

S-Pa

radis

e Mar

sh

SED-

9 24

112-

1006

2 7/2

2/200

409

:35

7/27/2

004

MEC

Analy

tical

Susie

Watt

s IC

PMS

#1 H

P 45

00

P. H

ersh

elman

Tr

ace M

etals

EPA

6020

EP

A =

Envir

onme

ntal P

rotec

tion A

genc

y GC

/MS

= Ga

s chr

omato

grap

hy-m

ass s

pectr

omete

r IC

PMC

= In

strum

ental

Plas

ma M

ass S

pectr

ometr

y

MEC

= ME

C An

alytic

al Sy

stems

, Inc.

QAQC

= Q

uality

Ass

uran

ce / Q

uality

Con

trol

SCCW

RP =

Sou

thern

Cali

fornia

Coa

stal W

ater R

esea

rch P

rojec

t

Sed-

# = sa

mplin

g loc

ation

numb

er

USFW

S =

Unite

d Stat

es F

ish an

d Wild

life S

ervic

e

OU 1 001314

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

29

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location

Discrete Sample Depth (M)

Sample Date

Preparation Batch ID

Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis

Field Duplicate Lab Duplicate

Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Gr

avel2

mNo

ne

0Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Gr

avel2

mNo

ne

0Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Gr

avel2

mNo

ne

0Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Gr

avel2

mNo

ne

0Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Grav

el2m

None

0

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.38

9235

239

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.40

1523

262

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.42

1774

651

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.38

0124

834

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.48

4033

841

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ku

rtosis

No

ne

-0.39

7520

2Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Kurto

sis

None

-0

.4400

9983

4Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Kurto

sis

None

-0

.4509

7314

2Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Kurto

sis

None

-0

.5383

3054

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Kurto

sis

None

-0

.3548

8977

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

an

None

4.1

7344

9144

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

an

None

4.1

1936

76Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.078

8480

54Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.413

6561

79Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.798

7347

29Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

OU 1 001315

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

30

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

3.998

5565

31Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.260

4365

8Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.430

7379

89Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mean

No

ne

4.486

5334

48Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

an

None

3.9

2673

8217

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

4.9

2831

5265

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.0

8078

5869

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

4.9

7530

299

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.2

4557

5866

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.8

4197

1144

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

4.8

8129

0939

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.2

5426

8626

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.3

9894

8691

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Me

dian

None

5.6

9878

6422

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Media

n No

ne

4.694

1283

89Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.495

5282

26Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.234

7280

34Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.719

9945

12Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.728

1492

19Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

5.759

8985

39Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.255

2233

98Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.260

6433

29Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

3.492

5047

16Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Mode

No

ne

5.764

5589

51Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Mo

de

None

3.0

2311

828

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i-0.5

None

0

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

OU 1 001316

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

31

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-0

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i-0.5

None

0

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.0

None

0

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0.025

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.5

None

0

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.5

None

0

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i00.5

None

0.0

22Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

OU 1 001317

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

32

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0.018

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi00

.5 No

ne

0.015

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0.1

03Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.0 No

ne

0.118

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0.4

95Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.0 No

ne

0.041

5Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.0 No

ne

0.042

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.0 No

ne

0.443

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0.0

505

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0.3

05Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.0

None

0.3

115

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

0.9

295

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

1.2

1Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.5 No

ne

1.841

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

0.4

21Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.5 No

ne

0.379

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

1.9

315

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

0.7

435

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

0.5

09Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi01

.5 No

ne

1.119

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i01.5

None

1.7

885

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.0

None

3.4

675

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.0

None

4.6

45Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

4.375

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

OU 1 001318

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

33

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

2.108

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.0

None

1.5

04Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

5.170

5Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

3.571

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

2.463

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.0

None

2.9

215

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.0 No

ne

6.006

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.5

None

7.9

52Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

9.510

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

7.615

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

6.169

5Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

3.718

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

9.015

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.5

None

8.3

385

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.5

None

6.5

17Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi02

.5 No

ne

5.332

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i02.5

None

10

.3285

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

10

.403

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

10

.714

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

9.7

315

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

9.8

385

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

5.9

55Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.0 No

ne

10.49

8Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.0 No

ne

10.13

9Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.0 No

ne

9.120

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.0 No

ne

6.745

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

OU 1 001319

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

34

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.0

None

10

.843

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.5

None

10

.3495

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.5

None

9.0

43Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.5 No

ne

9.842

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.5 No

ne

10.51

75Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.5 No

ne

7.417

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.5 No

ne

9.497

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.5

None

9.0

405

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.5

None

9.2

155

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i03.5

None

7.2

725

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi03

.5 No

ne

9.548

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

9.3

285

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

7.2

315

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

8.6

81Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.0 No

ne

9.096

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

7.8

145

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

7.9

455

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

7.5

305

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

8.2

155

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

7.3

68Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.0

None

8.1

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

8.677

5Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

6.383

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

7.719

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.5

None

7.9

85Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

8.137

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

OU 1 001320

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

35

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

7.069

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.5

None

6.9

155

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.5

None

7.6

785

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i04.5

None

7.5

825

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi04

.5 No

ne

7.321

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.0

None

8.6

645

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.0

None

6.3

85Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.0 No

ne

7.541

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.0

None

7.7

015

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.0

None

8.7

25Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.0 No

ne

7.000

5Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.0 No

ne

7.123

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.0 No

ne

7.847

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.0 No

ne

8.025

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.0

None

7.1

44Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

8.658

5Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

6.594

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

7.702

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.5

None

7.6

36Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

9.161

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i05.5

None

7.1

68Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

7.515

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

8.182

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

8.404

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi05

.5 No

ne

7.109

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.0

None

8.0

145

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

OU 1 001321

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

36

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.0 No

ne

6.581

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.0 No

ne

7.585

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.0

None

7.3

065

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.0

None

8.9

55Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.0 No

ne

7.067

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.0

None

7.5

75Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.0 No

ne

8.164

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.0 No

ne

8.390

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.0

None

6.8

315

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

7.0

82Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.5 No

ne

6.641

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

7.2

54Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.5 No

ne

7.03

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

8.6

14Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.5 No

ne

6.883

5Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi06

.5 No

ne

7.52

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

8.0

185

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

8.3

51Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i06.5

None

6.5

155

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i07.0

None

5.2

4Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

5.964

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

5.833

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

5.979

5Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

7.219

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i07.0

None

5.7

45Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

6.402

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

OU 1 001322

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

37

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

6.712

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.0 No

ne

7.211

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i07.0

None

5.2

94Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

3.635

5Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

5.038

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

4.326

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

4.853

5Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

5.739

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

4.432

5Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

5.052

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

5.175

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

5.805

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi07

.5 No

ne

3.944

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.0 No

ne

2.264

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

3.6

88Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.0 No

ne

2.823

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.0 No

ne

3.507

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

4.0

825

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

2.9

985

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

3.5

305

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

3.5

2Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.0 No

ne

4.123

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.0

None

2.6

01Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

1.728

5Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

3.129

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.5

None

2.1

94Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

OU 1 001323

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

38

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

3.009

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.5

None

3.5

185

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i08.5

None

2.3

95Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

2.935

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

2.869

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

3.495

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi08

.5 No

ne

2.048

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.0 No

ne

1.022

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.0

None

1.9

32Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.0 No

ne

1.275

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.0

None

1.8

93Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.0 No

ne

2.254

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.0

None

1.4

11Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.0 No

ne

1.781

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.0 No

ne

1.721

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.0

None

2.1

53Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.0

None

1.1

985

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

0.5

945

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

1.0

845

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

0.7

07Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.5 No

ne

1.076

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

1.3

175

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

0.7

73Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.5 No

ne

0.972

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi09

.5 No

ne

0.939

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

1.1

775

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

OU 1 001324

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

39

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i09.5

None

0.6

66Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi-1

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i-1.0

None

0

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

0.6

635

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

1.2

65Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.0 No

ne

0.797

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

1.2

17Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.0 No

ne

1.549

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

0.8

58Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.0 No

ne

1.073

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

1.0

535

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

1.3

41Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.0

None

0.7

445

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.5

None

0.6

87Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

1.413

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

0.833

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.5

None

1.2

89Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

1.788

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

OU 1 001325

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

40

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

0.88

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.5

None

1.1

19Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

1.117

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i10.5

None

1.4

455

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi10

.5 No

ne

0.775

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.0 No

ne

0.453

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.0

None

1.0

135

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.0

None

0.6

105

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.0

None

0.9

285

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.0

None

1.4

385

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.0

None

0.6

13Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.0 No

ne

0.783

5Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.0 No

ne

0.751

5Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.0 No

ne

1.005

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.0 No

ne

0.577

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.082

5Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.413

5Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.190

5Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.397

5Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.643

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.184

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.5

None

0.2

885

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.5

None

0.2

09Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi11

.5 No

ne

0.406

5Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i11.5

None

0.2

38Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.294

NANA

NA

AB

C

OU 1 001326

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

41

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

2 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.295

NANA

NA

AB

C

Sed-

3 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.296

NANA

NA

AB

C

Sed-

4 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.297

NANA

NA

AB

C

Sed-

5 0

7/21/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0.024

5Ph

i No

ne1

1 SW

P070

4.298

NANA

NA

AB

C

Sed-

6 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.299

NANA

NA

AB

C

Sed-

7 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.300

NANA

NA

AB

C

Sed-

8 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.301

NANA

NA

AB

C

Sed-

9 0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Phi12

.0 No

ne

0Ph

i No

ne1

1 SW

P070

4.302

NANA

NA

AB

C

Sed-

10

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Ph

i12.0

None

0

Phi

None

1 1

SWP0

704.3

03NA

NA

NA

ABC

Se

d-1

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.55

6570

456

Phi

None

1 1

SWP0

704.2

94NA

NA

NA

ABC

Se

d-2

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.50

5157

267

Phi

None

1 1

SWP0

704.2

95NA

NA

NA

ABC

Se

d-3

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.54

4458

892

Phi

None

1 1

SWP0

704.2

96NA

NA

NA

ABC

Se

d-4

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.54

9274

996

Phi

None

1 1

SWP0

704.2

97NA

NA

NA

ABC

Se

d-5

0 7/2

1/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.68

3145

119

Phi

None

1 1

SWP0

704.2

98NA

NA

NA

ABC

Se

d-6

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.50

2778

049

Phi

None

1 1

SWP0

704.2

99NA

NA

NA

ABC

Se

d-7

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.50

3770

564

Phi

None

1 1

SWP0

704.3

00NA

NA

NA

ABC

Se

d-8

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.53

4132

866

Phi

None

1 1

SWP0

704.3

01NA

NA

NA

ABC

Se

d-9

0 7/2

2/200

4 1

2 PS

EP86

8/3/

2004

SEDI

MENT

Resu

lt Sk

ewne

ssNo

ne

-2.58

8983

374

Phi

None

1 1

SWP0

704.3

02NA

NA

NA

ABC

Se

d-10

0

7/22/2

004

1 2

PSEP

86 8

/3/20

04SE

DIME

NTRe

sult

Skew

ness

None

-2

.5162

0738

5Ph

i No

ne1

1 SW

P070

4.303

NANA

NA

AB

C

Sed-

1 0

7/21/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

5.194

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

2 0

7/21/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

1.178

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

3 0

7/21/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

2.763

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

4 0

7/21/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

1.398

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

OU 1 001327

App

endi

ces

*lis

t of a

cron

yms f

ound

at e

nd o

f tab

le

App

endi

x B

– R

aw D

ata

Page

B-1

42

App

endi

x B

: Ta

ble

10.

Gra

in S

ize

and

Tota

l Org

anic

Car

bon

Res

ults

for t

he P

arad

ise

Mar

sh C

onta

min

ants

Inve

stig

atio

n, S

an D

iego

, CA

.*

(con

tinue

d fr

om p

revi

ous p

age)

Sampling Location


Sample Date


Analysis Batch ID

Analysis Method

Analysis Date

Matrix

Sample Type

Parameter Code

Qualifier

Result

Units

Measurement Basis


Lab Sample ID

TrueValue

MDL

RL

Lab Code

Comments

Sed-

4 0

7/21/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

DUP

TOC

None

1.3

61Pe

rcent

DW

1 2

NA

0.017

0.366

SCCW

RP

Sed-

5 0

7/22/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

2.192

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

6 0

7/22/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

2.426

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

7 0

7/22/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

1.82

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

8 0

7/22/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

2.091

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

9 0

7/22/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

RESU

LTTO

C No

ne

2.483

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

Sed-

10

0 7/2

1/200

4 13

AUG0

4SC

CWRP

18AU

G04

SCCW

RPCH

N 8/1

8/200

4SED

IMEN

TRE

SULT

TOC

None

1.1

42Pe

rcent

DW

1 1

NA

0.017

0.366

SCCW

RP

PACS

-1

NA8/1

3/200

4 13

AUG0

4SC

CWRP

18AU

G04

SCCW

RPCH

N 8/1

8/200

4SED

IMEN

TSR

M TO

C No

ne

3.542

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

SRM

run b

efore

sa

mples

PACS

-1

NA8/1

3/200

4 13

AUG0

4SC

CWRP

18AU

G04

SCCW

RPCH

N 8/1

8/200

4SED

IMEN

TSR

M TO

C No

ne

3.546

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

SRM

run a

fter

samp

les

Cyclo

hexa

none

NA

8/13/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

LCM

TOC

None

52

.081

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

LCM-

1 run

be

fore s

ample

s

Cyclo

hexa

none

NA

8/13/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

LCM

TOC

None

51

.967

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

LCM-

1 run

after

sa

mples

Aceta

nilide

NA

8/13/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

LCM

TOC

None

71

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

LCM-

2 run

be

fore s

ample

s

Aceta

nilide

NA

8/13/2

004

13AU

G04

SCCW

RP18

AUG0

4SC

CWRP

CHN

8/18/2

004S

EDIM

ENT

LCM

TOC

None

71

.132

Perce

nt DW

1

1

NA0.0

170.3

66SC

CWRP

LCM-

2 run

after

sa

mples

AB

C =

Aqua

tic B

ioass

ay an

d Con

sultin

g CH

N =

Carb

on H

ydro

gen N

itroge

n Sam

pler

Dup =

Dup

licate

DW

= D

istille

d Wate

r LC

M =

Labo

rator

y Con

trol M

ateria

l NA

= N

ot Ap

plica

ble

PSEP

= P

uget

Soun

d Estu

ary P

rogr

am M

ethod

SC

CWRP

= S

outhe

rn C

alifor

nia W

ater R

esea

rch P

rojec

t Se

d-# =

Sed

imen

t Sam

pling

Loca

tion

SRM

= St

anda

rd R

efere

nce M

ateria

l TO

C =

Total

Org

anic

Carb

on

OU 1 001328

Appendices

Appendix C – Raw Data Page C-143

Appendix C. List of Indicator Species and their Classifications used for Relative Benthic Index Analysis for the Paradise Marsh Contaminants Investigation, San Diego, CA.

Taxon Species Classification Source Polychaetes Capitella capitata Complex disturbed ABCDG Polychaetes Oligochaeta disturbed ACDG Polychaetes Streblospio benedicti disturbed BC Polychaetes Mediomastus sp disturbed E Molluscs Theora lubrica disturbed E Molluscs Chione fluctifraga disturbed F Molluscs Crepidula dorsata disturbed F Molluscs Cryptomya californica disturbed F Polychaetes Marphysa sanguinea disturbed F Polychaetes Marphysa sp disturbed F Polychaetes Marphysa sp B disturbed F Crustaceans Pyromaia tuberculata disturbed F Polychaetes Chaetozone sp disturbed FG Polychaetes Cirratulidae disturbed FG Polychaetes Prionospio heterobranchia disturbed FG Crustaceans Ampithoe sp disturbed F Crustaceans Grandidierella japonica disturbed ABC Molluscs Macoma sp undisturbed A Molluscs Tellina sp undisturbed AD Crustaceans Gammaridea undisturbed E Polychaetes Cirriformia sp undisturbed F Polychaetes Drilonereis sp undisturbed F Polychaetes Exogone verugera undisturbed F Crustaceans Leptochelia dubia undisturbed F Minor Phyla Phoronida undisturbed F Polychaetes Polydora nuchalis undisturbed F Polychaetes Syllis (Typosyllis) sp undisturbed F Note: A “disturbed” species classification denotes a species that is likely to occur in a relatively disturbed benthic habitat. An “undisturbed” classification denotes a species that is likely to occur in a relatively undisturbed benthic habitat.

SourcesA – from page 32 (Jacobi et al. 1998) B – from page C-13 (Ranasinghe et al. 2003) C – from page 3-6 (Anderson et al. 2004) D – from page 60 (Anderson et al. 1998) E – from table 4.2 (SFEI. 1999) E – from Chapter 4 (SFEI. 1999) F – from Table 2 (Smith et al. 2001) G – from page 32 (ICES 2004)

OU 1 001329

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Paradise Marsh Contaminants Investigation - U.S. Fish and … · 2017-08-30 · Paradise Marsh Refuge Cleanup Project ... in our analysis of the Bight 1998 data from San Diego Bay)