Phase II Environmental Site Assessment · 2018. 5. 6. · Phase II Environmental Site Assessment 21st Street Community Center and Band Shell Building and Parking Area West of Convention

Phase II Environmental Site

Assessment

21st Street Community Center and Band Shell Building and Parking Area West of Convention Center

Miami Beach, Miami-Dade County, Florida

February, 2015 E Sciences Project Number 7-0002-023

Prepared for: City of Miami Beach Office of the City Manager City of Miami Beach 1700 Convention Center Drive, Fourth Floor Miami Beach, FL 33139

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This document is printed on recycled paper.

February 3, 2015 Ms. Thais Vieira, RA, LEED AP Senior Project Manager Office of the City Manager City of Miami Beach 1700 Convention Center Drive, Fourth Floor Miami Beach, FL 33139 Subject: Report of Phase II Environmental Site Assessment

21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Miami Beach, Miami-Dade County, Florida E Sciences Project Number 7-0002-023

Dear Ms. Vieira:

We are pleased to submit the enclosed Phase II Environmental Site Assessment (ESA) report for

the above referenced property. A summary of findings is provided in the Executive Summary.

Please read the report in its entirety for a comprehensive understanding of the items contained in

the Executive Summary.

This report is intended for the use of the City of Miami Beach only. E Sciences’ services have

been performed under mutually agreed-upon terms and conditions. If other parties wish to rely

on this report, please have them contact E Sciences so that a mutual understanding and agreement

of the terms and conditions for E Sciences’ services can be established via a Secondary Client

Agreement prior to their use of this information.

We appreciate the opportunity to perform these services for you. Please contact us at (954) 484-

8500 if you have questions regarding this information or if we can provide any other services.

Sincerely, E SCIENCES, INCORPORATED

Maria Paituvi, P.E. Nadia G. Locke, P.E., LEED AP Senior Engineer Senior Engineer Distribution: Addressee (1ec)

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Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page i of iii Miami Beach, Florida E Sciences Project Number 7-0002-023


TABLE OF CONTENTS

EXECUTIVE SUMMARY ........................................................................................................... ii

1.0 INTRODUCTION ............................................................................................................ 1

2.0 BACKGROUND INFORMATION ................................................................................ 2

3.0 STATEMENT OF OBJECTIVES .................................................................................. 3

4.0 SITE ASSESSMENT ACTIVITIES ............................................................................... 4

4.1 Incremental Soil Sampling ............................................................................................ 4 4.2 Soil Sampling Analytical Results .................................................................................. 5 4.3 Groundwater Sampling Activities ................................................................................. 7 4.3.1 Initial Groundwater Sampling Activities ....................................................................... 7 4.3.2 Additional Groundwater Sampling Activities ................................................................ 7 4.4 Groundwater Sampling Analytical Results ................................................................... 9

5.0 PHASE II ESA LIMITATIONS ................................................................................... 10

6.0 FINDINGS AND CONCLUSIONS .............................................................................. 11

7.0 REGULATORY INVOLVEMENT .............................................................................. 12

8.0 RECOMMENDATIONS ............................................................................................... 14

TABLES

1.1 Miami-Dade County Property Appraiser Information 1 4.1 Soil Analytical Scope 5 4.2 Summary of Soil Contaminant Detections 6 4.3 Initial Groundwater Analytical Scope 7 4.4 Additional Groundwater Analytical Scope 8 4.5 Monitoring Well Construction Detail 8 4.6 Summary of Groundwater Contaminant Detections 9

FIGURES 1 Location Map 2 USGS Topographic Map 3 Aerial Photograph 4A Soil Sampling Locations at Site A 4B Soil Sampling Locations at Site B 5 Groundwater Sampling Locations

APPENDICES

A Laboratory Analytical Reports and Chain of Custody Documentation B FDEP Groundwater Sampling Logs and Equipment Calibration Logs C Monitoring Well Construction and Development Logs

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Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page ii of iii Miami Beach, Florida E Sciences Project Number 7-0002-023


EXECUTIVE SUMMARY

Report of Phase II Environmental Site Assessment (ESA) 21st Street Community Center and Band Shell Building and

Parking Area West of Convention Center Miami Beach, Miami-Dade County, Florida

E Sciences Project Number 7-0002-023

E Sciences conducted a Phase II Environmental Site Assessment (ESA) to evaluate the potential

presence of impacts associated with recognized environmental conditions (REC) identified during

the Phase I ESA performed by E Sciences and documented in a report provided under separate

cover dated November 4, 2014.

The Site is comprised of two separate areas: Site A and Site B. Site A is a paved parking lot

located west of the Miami Beach Convention Center adjacent to Convention Center Drive. Site B

is located south of Dade Boulevard and north of the Convention Center. Site A includes the 21st

Street Community Center and Band Shell Building, which are used by the Miami Beach Parks

and Recreation Division as part of their Teen Club center. The remaining portions of Site B

include a paved parking lot and the SoBe Institute of the Arts. These properties provide

recreational, cultural and parking services to residents and the public. The area surrounding Site

A and Site B consists of both residential and commercial properties. Both Site A and Site B are

owned by the City of Miami Beach (the City).

Based on a review of historical documentation, Site B and the eastern portion of Site A were part

of the Miami Beach Municipal Golf Course in the 1950s. Typical chemicals applied to golf

courses during this time included arsenates, organochlorine pesticides, and Ethylene Dibromide

(EDB). Arsenate pesticides were banned by the US Environmental Protection Agency (EPA) in

the 1980s. Oganochlorine pesticides include dieldrin, dichlorodiphenyltrichloroethane (DDT),

chlordane and toxaphene. Most organochlorine pesticides were banned in the 1970s and 1980s. Many pesticides constituents accumulate and persist over time. The historic operation of a golf

course is considered to be a REC due to the likelihood of the repeated historical application of

pesticides.

Groundwater and soil sampling and analysis were conducted as part of this Phase II ESA. The

sampling activities and laboratory analysis conducted were based on the nature of the REC and

the typically associated contaminants of concern (COCs).

Soil sampling was conducted using Incremental Sampling Methodology in order to collect soil

samples representative of site conditions. Site B and the eastern portion of Site A formerly

occupied by the historic golf course were defined as separate Decision Units (DU) as part of this

Phase II ESA. Groundwater samples were collected from each site using direct push technology

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Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page iii of iii Miami Beach, Florida E Sciences Project Number 7-0002-023


and groundwater monitoring wells. The analytical scope for soil and groundwater samples

included organochlorine pesticides, organophosphate pesticides, metals, ammonia, nitrite and

nitrate.

Soil analytical results revealed the presence of arsenic concentrations above Miami-Dade

County’s Direct Exposure Residential Soil Cleanup Target Levels (SCTL) for the incremental

soil samples collected from Site A and Site B. The detected arsenic concentrations were above

the documented Barrier Islands Naturally Occurring Background Concentration published by

Miami-Dade County. Other compounds detected below regulatory standards include lead and

pesticides (4,4-DDE, Total Chlordane, and Dieldrin).

Laboratory analytical results for the groundwater samples did not reveal the presence of

groundwater contamination at Site A. Arsenic concentrations were detected above regulatory

criteria at one of the three groundwater sampling locations conducted within Site B. The arsenic

concentrations were confirmed during a confirmation sampling event. Further laboratory analysis

indicated that the presence of arsenic may be associated with dissolved metals in the

groundwater.

The City submitted a draft Phase II ESA report dated December 17, 2014 to Miami-Dade County

Regulatory and Economic Resources (RER) for review and comment. That report contained a

portion of the data contained herein.

On December 23, 2014, The city head a meeting with RER to discuss select contaminated sites

owned by the City including the subject sites. RER had conducted only a preliminary review of

the draft Phase II ESA at that time. RER requested that additional soil and groundwater testing be

conducted for both Site A and Site B and include offsite delineation of the potential impacts.

Further investigation regarding the past uses of the properties was also requested. RER noted that

additional comments and guidance would be provided upon review of the conceptual site

development plans.

The City responded to RER’s initial comments in email correspondence dated January 8, 2015.

The City indicated that offsite assessment would be conducted separately from the assessment of

the subject properties. Based on the results of additional aerial photographreview and interview

with key personnel, the City determined that the property's past uses do not suggest the need to

test additional parameters requested by RER. At this time RER has not responded to the City’s

email.

Based on the assessment information contained herein, the proposed development of the sites and

general regulatory guidance provided, we offer the following recommendations:

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Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page iv of iii Miami Beach, Florida E Sciences Project Number 7-0002-023


• Installation of an engineering control across the sites as part of the site development. At

this time we understand that the engineering control will consist of a synthetic

impermeable and colored liner followed by 12 inches of clean fill and impermeable

pavement. The proposed engineering control shall be approved by RER prior to

installation.

• Development of a Soil Management Plan and implementation during site development

after regulatory approval by RER.

• Secure a dewatering permit that includes evaluation and management of impacted

groundwater within Site B. Based on the results of the filtered samples, we anticipate

that the application of a filter process will be sufficient to treat the water to regulatory

standards for disposal purposes if treatment is necessary.

• It is anticipated that RER would require a dewatering plan for the property if dewatering

is proposed as part of site development. If dewatering is being conducted in areas that

are demonstrated not to have arsenic impacts, then the dewatering plan would

demonstrate that the dewatering activities would not exacerbate or move groundwater

impacts. If dewatering activities will be performed in an area with impacted

groundwater, then treatment of the groundwater prior to discharge or disposal of

dewatering effluent would be required.

• Restrict the use of the irrigation wells to eliminate the influence of pumping impacted

groundwater.

• Route the point of discharge of drainage structures to outside the impacted area in Site B.

We recommend that the City seek RER’s conceptual approval of a site development approach

elected by the City including the above provisions. Regulatory closure will likely require

additional assessment.

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Phase II Environmental Site Assessment February 3, 2015 21st Street Community Center and Band Shell Building and Parking Area West of Convention Center Page 1 of 15 E Sciences Project Number 7-0002-023


1.0 INTRODUCTION

The Site is comprised of two separate areas: Site A and Site B. Site A is a paved parking lot

located west of the Miami Beach Convention Center adjacent to Convention Center Drive. Site B

is adjacent south of Dade Boulevard and north of the Convention Center. Site A includes the 21st

Street Community Center and Band Shell Building, which are used by the Miami Beach Parks

and Recreation Division as part of their Teen Club center. The remaining portions of Site B

include a paved parking lot and the SoBe Institute of the Arts. These properties provide

recreational, cultural and parking services to residents and the public. The area surrounding Site

A and Site B consists of both residential and commercial properties. Both Site A and Site B are

owned by the City of Miami Beach (the City).

The western portion of Site A is comprised of six parcels. Site B and the eastern portion of Site

A are listed under the same folio number as the property developed with the Convention Center.

Portions of Site B were not linked to property information details on the Miami-Dade County

Property Appraiser website and a folio number was not identified. Table 1-1 provides

information obtained from the Miami-Dade County Property Appraiser.

TABLE 1-1 MIAMI-DADE COUNTY PROPERTY APPRAISER INFORMATION

FOLIO ADDRESS DESCRIPTION

02-3234-007-0110 1855 Meridian Avenue Western portion of Site A

02-3234-007-0100 Not provided Western portion of Site A




02-3234-007-0060 1809 Meridian Avenue Western portion of Site A

02-3234-000-0090 500 17 Street Eastern portion of Site A and Site B

A Site location map is provided in Figure 1. A United States Geological Survey (USGS)

topographic map was used to help evaluate topographic information (Figure 2) and (Figure 3)

provides aerial coverage for the Site and surrounding properties.

The City is planning to redevelop the Site into a recreational park. E Sciences was engaged by

the City to perform a Phase II Environmental Site Assessment (ESA). The purpose of the Phase

II ESA was to evaluate the potential presence of contamination associated with recognized

environmental conditions (RECs) identified during a Phase I ESA conducted in November 2014

(see Section 2.0).

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2.0 BACKGROUND INFORMATION

E Sciences, Incorporated (E Sciences) performed a Phase I ESA in general accordance with the

consensus document known as ASTM International Practice E 1527-13, a guide for conducting

ESAs. The Phase I ESA was documented in a report dated November 4, 2014. The purpose of the

Phase I ESA was to identify potential sources of environmental contamination that constitute a

recognized environmental conditions (REC), as defined by the ASTM standard. The following

findings were documented during the Phase I ESA:

• Based on a review of historical documentation, Site B and the eastern portion of Site A

were part of the Miami Beach Municipal Golf Course in the 1950s. Typical chemicals

applied to golf courses during this time included arsenates, organochlorine pesticides, and

Ethylene Dibromide (EDB). Arsenate pesticides were banned by the US Environmental

Protection Agency (EPA) in the 1980s. Oganochlorine pesticides include dieldrin,

dichlorodiphenyltrichloroethane (DDT), chlordane and toxaphene. Most organochlorine

pesticides were banned in the 1970s and 1980s. Many pesticide constituents accumulate

and persist over time. The historical operation of a golf course is considered to be a REC

due to the likely historical repeated application of pesticides such as arsenate, DDT and

EDB.

• A review of historical documentation concerning the area surrounding the Site did not

reveal indications of contaminated properties or activities within the Site vicinity that

would, in our opinion, be considered a REC in relation to the Site with the exception of

the historic golf course.

• A review of regulatory documentation concerning the Site and surrounding area did not

reveal indications of contaminated properties or activities at the Site, or within the Site

vicinity, that would be considered a REC in relation to the Site.

• The site reconnaissance did not reveal the presence of Site conditions that would be

considered a REC in relation to the Site.

E Sciences was engaged by the City to perform a Phase II ESA. The scope of the Phase II ESA was

based on historical presence of the golf course within the Site.

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3.0 STATEMENT OF OBJECTIVES

The objective of the Phase II ESA activities was to evaluate the potential presence of

contamination based on the findings of the Phase I ESA. The Phase II ESA activities at the Site

were based on the suspected location of the RECs identified during the Phase I ESA (see Section

2.0). The sampling activities and laboratory analysis conducted were based on the nature of the

RECs and the potential contaminants of concern (COCs) associated with the historical activities at

the Site and adjacent properties.

The following scope of services was completed:

• Soil evaluation using Incremental Sampling Methodology (ISM).

• Groundwater sampling and analysis at predetermined locations.

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4.0 SITE ASSESSMENT ACTIVITIES

Field activities were conducted by E Sciences personnel on November 20 and 21, 2014 and

January 23,24 and 29, 2015. The drilling services were provided by our subcontractor and

licensed water well driller, JAEE Environmental Services, Inc. Laboratory analyses were

conducted by state-certified Palm Beach Environmental Laboratories, Inc. (PBEL) and Accutest

Laboratories, Inc. (Accutest). Sampling activities were conducted in accordance with FDEP

Standard Operating Procedures (SOPs) as applicable. The following sections document the

activities conducted and findings associated with the Phase II ESA activities.

For the purposes of the Phase II ESA, Site A and Site B were assessed separately and a similar

sampling scope and methodology was implemented on each site.

4.1 Incremental Soil Sampling

Soil samples were collected based on the concept of Incremental Sampling Methodology (ISM).

The Interstate Technology and Regulatory Council has published an ISM documented dated

February 2012. This methodology has been used on other sites within the State with regulatory

concurrence and we understand that the Florida Department of Environmental Protection (FDEP)

is drafting a guidance document for this process. This soil sampling methodology was

implemented in order to collect a representative sample of the Site based on potential historical

onsite contamination sources.

The eastern portion of Site A and Site B were defined as separate “Decision Units” (DU) (see

Figure 4A and Figure 4B). The DU boundaries for Site A were defined based on review of the

historical aerial photographs and location of the historical golf course. Large vehicles and

equipment were parked along the eastern and western boundaries of Site A; therefore, the DU

unit for Site A was limited to the readily accessible area. Each DU was subdivided into uniform

grid cells. Based on guidance documents for ISM, a minimum of 30 cells are required within

each DU in order to obtain a representative sample of the soil quality within the DU. A total of

32 cells on Site A and 31 cells in Site B were established. A pre-determined soil mass of

approximately 45 grams was collected within each grid cell using pre-measured sampling tools

provided by the laboratory. These individual samples are referred to as increments. Each

increment was collected at a random location and random depth from zero to 12 inches below

land surface (bls) within the cell but below the existing asphalt layer. Samples were collected

from the subsurface using Direct Push Technology (DPT). Individual increments collected were

placed into bulk sample containers. One bulk sample container was designated for analysis of

volatile compounds and a second bulk sample container for semi and non-volatile compounds.

An aerial photograph of the Site depicting the DU, grid and increment sampling locations is

included in Figure 4A and Figure 4B for Site A and B respectively.

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The soil samples were collected in laboratory provided containers and shipped to PBEL under

chain of custody protocol for ISM processing and analysis. Upon receipt of the samples, PBEL

processed the samples and initiated sub-sampling activities, which included air drying and sieving

the bulk sample to remove particles larger than two millimeters. The sieved bulk sample was

then spread into a thin layer and a grid was established. A total of 30 increments of equal mass

were collected in random locations across the spread-out sample to generate the final multi-

increment sample for analysis. This process is referred to as sub-sampling. The mass collected

from each sub-sampling location depended on the analytical test. The final multi-increment

sample for each DU (DU1 and DU2) was analyzed for the following contaminants: arsenic, lead,

organochlorine pesticides and organophosphate pesticides

TABLE 4-1 SOIL ANALYTICAL SCOPE

Contaminant of Concern EPA Analytical Method

Arsenic EPA Method SW846 6020B

Lead EPA Method SW846 6020B

Organochlorine Pesticides EPA Method 8081

Organophosphate Pesticides EPA Method 8270

Duplicate sample (DUP1 for DU-1 and DUP3 for DU-2) were collected in the field using the

same sampling methodology described above. The increments for theses duplicate samples were

collected at a location different from the original samples within the same cell. A third replicate

was collected using the same increment locations as the initial sample from each DU (DUP2 for

DU-1 and DUP4 for DU-2) to evaluate the accuracy of the laboratory procedures. The replicate

samples were analyzed per the analytical scope provided in Table 4-1 above.

4.2 Soil Sampling Analytical Results

Laboratory analytical results were compared to the Miami-Dade County Soil Cleanup Target

Levels (SCTLs) defined under Chapter 24 of the Miami-Dade County Code of Ordinances.

Furthermore, analytical results for Arsenic were compared to the “Barrier Islands Naturally

Occurring Background Concentrations” documented in the Miami-Dade County Regulatory and

Economic Resources (RER) Department’s memorandum regarding Miami-Dade County

Anthropogenic Background Study dated April 3, 2014.

Analytical results revealed the presence of pesticides compounds (4,4-DDE, Dieldrin and Total

Chlordane) and lead above the laboratory method detection limits in select samples. Arsenic

concentrations were detected above the Direct Exposure Residential SCTL for the incremental

samples collected from Site A and Site B. Table 4-2 presents a summary of the soil analytical

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results for the detected analytes. Laboratory analytical reports and chain of custody

documentation are included in Appendix A.

TABLE 4-2

SUMMARY OF SOIL PARAMETER DETECTIONS

Site Sample ID gamma-

Chlordane alpha-

Chlordane 4,4-DDE Dieldrin Total

Chlordane Arsenic Lead mg/kg

Site A

DU-2 0.0009 0.0006 0.0045 0.00004 U 0.0015 5.75 25.4

DUP3 0.0011 0.0008 0.0034 0.00004 U 0.0019 5.52 25.5

DUP4 0.0004 0.0003 0.0015 0.00004 U 0.0007 5.49 35.1

Site B DU-1 0.0011 0.0006 0.0067 0.00004 U 0.0017 9.04 45.5

DUP1 0.0007 0.0004 0.0032 0.0001 0.0012 9.13 311 E

DUP2 0.003 0.0003 0.0026 0.00004 U 0.0006 10.4 42.2 Miami-Dade Direct Exposure Residential SCTL NA NA 2.9 0.06 2.8 2.1 400 Miami-Dade Direct Exposure Commercial/Industrial SCTL NA NA 15 0.3 14 12 1400 Miami-Dade Leachability based SCTL NA NA 18 0.002 9.6 *** *** Barrier Islands Naturally Occurring Background Concentration NA NA NA NA NA 5.2 NA

Notes: This table presents only the concentrations of analytes detected. Other analytes were not detected above laboratory method

detection limits and are not included in this summary table.

Analytical results presented in mg/Kg unless specified mg/Kg: milligram per kilogram

U: Indicates analyte not detected above laboratory method detection limit. BOLD Indicates contaminant above Miami-Dade SCTL E: The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is

considered an estimate (CLP E-flag). *** Leachability values may be derived using the SPLP Test to calculate the site-specific SCTLs or may be determined using TCLP in the event of oily wastes are present. NA : Not Applicable

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4.3 Groundwater Sampling Activities

Groundwater sampling activities were conducted at the Site in order to evaluate the potential

presence of groundwater impacts associated with the historical operation of the golf course. Two

sampling events were conducted. An initial sampling event was conducted on November 21,

2013. A second event was conducted on January 25 and 29, 2015 based on information and

requirements presented by Miami-Dade County Regulatory and Economic Resources (RER)

department to include additional COCs (refer to Section 7.0).

4.3.1 Initial Groundwater Sampling Activities

The initial groundwater sampling was conducted using DPT by advancing probes to

approximately two feet into the water table using a stainless steel well point and withdrawing the

point to expose four feet of stainless steel screen. The groundwater sampling locations (DP-1 on

Site B and DP-2 on Site A) are depicted on Figure 5. Groundwater sampling activities were

conducted in accordance with FDEP Standard Operating Procedures (SOPs). Field parameters

(pH, conductivity, temperature, dissolved oxygen and turbidity) were measured during purging

using a multi-sensor probe and turbidity meter. Groundwater samples were collected in

laboratory supplied containers, packaged in ice-filled coolers and shipped to PBEL under chain of

custody protocol for analysis. Groundwater sampling logs are included in Appendix B. Table 4-

3 presents a summary of the COCs and analytical methods conducted during the initial sampling

event.

TABLE 4-3 INITIAL GROUNDWATER ANALYTICAL SCOPE


Arsenic EPA Method SW846 6020B

Lead EPA Method SW846 6020B

Organochlorine Pesticides EPA Method 8081

Organophosphate Pesticides EPA Method 8270

4.3.2 Additional Groundwater Sampling Activities

Upon completion of the soil sampling and initial groundwater sampling events, a draft Phase II

ESA report dated December 17, 2014 was submitted to the City. The City submitted the draft

Phase II ESA report to RER for review and comment (See Section 7.0 for additional regulatory

involvement information). Based on this review, RER requested that the COCs for the

assessment include the following parameters:

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TABLE 4-4 ADDITIONAL GROUNDWATER ANALYTICAL SCOPE


13 RCRA Metals* EPA Method SW846 6010/6020: As, Pb, Cd, Ag, Cr, Cu, Tl, Sb, Be, Ni, Se, Zn EPA Method SW846 7470/7471: Hg

Nitrates EPA Method 353.2

Nitrites EPA Method 353.2

Ammonia EPA Method 350.1 *Arsenic (As), Lead (Pb), Cadmium (Cd), Silver (Ag), Chromium (Cr), Selenium (Se), Mercury (Hg), Beryllium (Be), Zinc (Zn), Nickel (Ni), Copper (Cu), Antimony (Sb), Thallium (Tl).

Based on the anticipated dewatering activities at both sites during the proposed development, the

City elected to install two monitoring wells at each site to evaluate the potential presence of the

additional COC identified by RER.

Two monitoring wells were installed at Site A (MW-1 and MW-2) and Site B (MW-3 and MW-4)

as depicted on Figure 5. The monitoring wells were installed using DPT on January 23, 2015 by

JAEE under E Sciences oversight. The monitoring wells were installed to a maximum depth of l5

feet bls and constructed of ten feet of pre-packed well screen and a five-foot PVC riser. The

wells were completed with a well cap and a traffic-bearing manhole. Well construction and

development logs are provided in Appendix C. Well construction details are summarized in

Table 4-5 below.

TABLE 4-5 MONITORING WELL CONSTRUCTION DETAIL

SITE MONITORING

WELL ID.

Total Depth (ft

bls)

Screen Interval (ft

bls)

Well Diameter (inches)

Installation Method

Site A MW-1 15 5-15 1.25 DPT

MW-2 15 5-15 1.25 DPT

Site B MW-3 15 5-15 1.25 DPT

MW-4 15 5-15 1.25 DPT

The newly installed monitoring wells were sampled on January 24, 2015. Groundwater sampling

activities were conducted in accordance with FDEP Standard Operating Procedures (SOPs).

Field parameters (pH, conductivity, temperature, dissolved oxygen and turbidity) were measured

during purging using a multi-sensor probe and turbidity meter. Groundwater samples were

collected in laboratory supplied containers, packaged in ice-filled coolers and shipped to Accutest

under chain of custody protocols. Groundwater sampling logs are included in Appendix B. The

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analytical scope for these samples included the COCs identified by RER and also organochlorine

pesticides based on the detection of those parameters on the ISM soil samples collected.

4.4 Groundwater Sampling Analytical Results

Laboratory analytical results were compared to the Miami-Dade County Groundwater Cleanup

Target Levels (GCTLs) defined under Chapter 24 of the Miami-Dade Code of Ordinances. Intiial

analytical results revealed the presence of arsenic and lead above the laboratory method detection

limit but below GCTLs. The other COCs were not detected above the corresponding laboratory

method detection limit. A summary of the laboratory detections is provided in Table 4-4 below.

Laboratory analytical reports and chain of custody documentation are included in Appendix A.

TABLE 4-6 SUMMARY OF GROUNDWATER CONTAMINANT DETECTIONS

Antimony Arsenic Dissolved Arsenic

Chromium Lead Nickel Silver Zinc Ammonia

ug/l mg/l

Miami-Dade GCTL 6 10 10 100 15 100 100 5000 2.8

Site Sample

ID Sampling

Date

Site B

DP-1 11/21/2014 NA 8.3 NA NA 6 NA NA NA NA

MW-3 1/24/2015* 2.2 I 21.3 1.3 U 1.0 U 1.1 U 0.40 U 0.80 I 5.9 I 1.0

1/29/2015** NA 24.6 25 NA NA NA NA NA NA

MW-4 1/24/2015 1.5 I 4.1 I NA 1.8 I 1.1 U 1.6 I 0.70 U 4.4 U 0.22

Site A

DP-2 11/21/2013 NA

0.377 U NA NA 6 NA NA NA NA

MW-1 1/24/2015 1.0 U 1.3 U NA 1.5 I 1.1 U 0.40 U 0.70 U 8.1 I 1.6

MW-2 1/24/2015 1.1 I 1.3 U NA 1.4 I 1.1 U 0.40 U 0.70 U 6.4 I 1.4

Notes:

This table presents only the concentrations of analytes detected. Other analytes were not detected above laboratory method detection limits and are not included in this summary table. *Laboratory filtered with 0.45 micron filter. **Field filtered with 1.0 micron filter.

ug/L: Micrograms per Liter mg/L: Milligrams per Liter

U: Indicates analyte not detected above laboratory method detection limit. I: Indicates analyte concentration above the maximum detection limit but below practical quantitation limit. NA = Not Analyzed for that parameter.

BOLD Indicates contaminant above Miami-Dade GCTL

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5.0 PHASE II ESA LIMITATIONS

Although this assessment has attempted to identify the potential for environmental impacts to the

Site, potential sources of contamination may have escaped detection due to:

• the limited scope of this assessment

• the inaccuracy of public records

• the presence of undetected or unreported environmental incidents

• inaccessible areas or

• deliberate concealment of detrimental information by others

It was not the purpose of this study to determine the actual degree or extent of contamination, if

any, at the Site. The sampling conducted as part of the Phase II ESA was intended to confirm the

presence of impacts based on the identified RECs. No sampling or analysis was conducted

outside the locations identified within this document.

Due to the limited nature of this Phase II ESA, there is a possibility that conditions may exist

which were not apparent at the time of report preparation and completion of the previous Phase I

ESA. It is also possible that the testing methods employed at the time of the report may later be

superseded by other methods. The description, type, and composition of what are commonly

referred to as “hazardous materials or conditions” can also change over time. E Sciences does not

accept responsibility for changes in the state of the art, nor for changes in the scope of various

lists of hazardous materials or conditions. E Sciences believes that the findings and conclusions

provided in this report are reasonable. However, no other warranties are implied or expressed.

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6.0 FINDINGS AND CONCLUSIONS

The Phase II ESA was designed to evaluate the potential presence of impacts from the historic

operation of a golf course at the Site identified during the previous Phase I ESA.

Soil analytical results revealed the presence of arsenic concentrations above Miami-Dade

County’s Direct Exposure Residential Soil Cleanup Target Levels (SCTL) for the incremental

soil samples collected from Site A and Site B. The detected arsenic concentrations were above

the documented Barrier Islands Naturally Occurring Background Concentration published by

Miami-Dade County. Other compounds detected below regulatory standards include lead and

pesticides (4,4-DDE, Total Chlordane, and Dieldrin).

Groundwater samples collected from Site A did not reveal the presence of COCs above the

corresponding GCTLs. Therefore, no groundwater impacts were identified within Site A during

this limited assessment.

Groundwater samples collected from Site B revealed the presence of arsenic concentration above

the GCTL in one of the three sampling locations. The arsenic concentration detected in

groundwater samples collected from MW-3 was reported above the GCTL as confirmed by a

second sampling event conducted based on initial results. To further evaluate the presence of

arsenic, the laboratory was asked to filter the sample collected on November 21, 2015 and

analyze for dissolved arsenic. The laboratory filtered the sample using a 0.45 micron filter, and

the results that dissolved arsenic concentration for the sample was not detected above the

laboratory detection limit or the GCTL. The second sample collected at this location on January

29, 2015 was filtered on the field using a 1.0 micron filter per FDEP SOPs. Analysis of this

sample revealed a similar concentration of arsenic for the unfiltered and filtered samples, both

above the GCTL. Based on these observations, we conclude that the laboratory filtering method

and 0.45 micron filter size was more effective in removing dissolved metals from the sample

aliquot.

Based on the results documented herein, arsenic concentration are present above the GCTL

within a portion of Site B. The extent of the arsenic impacts cannot be determined based on

results available at this time.

DRAFT



7.0 REGULATORY INVOLVEMENT

The City submitted the draft Phase II ESA report dated December 17, 2014 to Miami-Dade

County RER for review and comment regarding the regulatory course of action based on the

results of the ISM soil testing and initial soil and groundwater sampling.

On December 23, 2014, a meeting was held between RER, the City, Atkins and E Sciences

representatives to discuss select contaminated sites owned by the City including the subject sites.

RER had conducted only a preliminary review of the draft Phase II ESA at that time. Items

discussed during this meeting regarding the subject site included:

• The need to develop and implement a Soil Management Plan during construction

activities;

• The background naturally occurring arsenic concentration within the island is considered

to be the applicable cleanup standard for these sites;

• The extent of impacts has not yet been delineated based on the limited scope of the Phase

II ESA;

• Potential regulatory closure approaches;

• Engineering and institutional controls;

• Delineation and excavation of arsenic impacted soil;

• Drainage and dewatering considerations might be required and would be determined

based on additional groundwater sampling and analysis;

• Acceptable engineering control alternatives were discussed (i.e. artificial turf, asphalt and

concrete parking lots, geomembranes, clean soil cover).

RER issued initial comments regarding the Phase II ESA in email correspondence dated

December 24, 2014. RER requested that additional soil and groundwater testing be conducted for

both Site A and Site B and include offsite delineation of the potential impacts. Further

investigation regarding the past uses of the properties was also requested. RER noted that

additional comments and guidance will be provided upon review of the conceptual site

development plans.

The City responded to RER’s initial comments in email correspondence dated January 8, 2015.

The City indicated that offsite assessment would be conducted separately from the assessment of

the subject properties. The City stated that based on a more extensive review of additional

historical aerial photos, the presence of building structures just north of the original Convention

Center building were observed. The City interviewed a city employee who has been with the

City for 47 years, and he confirmed that these buildings and other activities visible in this area

were associated with the Parks & Recreation Department Headquarters housed at that location.

The Department used this property to store the maintenance equipment and products associated

DRAFT



with their operations throughout the City. Based on the results of additional aerial photograph

review and interview with key personnel, the City determined that the property's past uses do not

suggest the need to test additional parameters requested by RER. At this time RER has not

responded to the City’s email.

DRAFT



8.0 RECOMMENDATIONS

Based on the findings of this Phase II ESA and general guidance provided by RER, we provide

the following recommendations regarding the proposed development of Site A and Site B:

Recommendations pertaining to existing soil impacts are as follows:

• Prepare a Soil Management Plan (SMP) for review and approval by RER prior to

site development activities. The SMP should include the following provide

procedures and precautions to be implemented for the management of contaminated soil

during construction activities. The SMP should include information associated with the

following items, at a minimum:

o Background Information;

o Soil Management Requirements such as designated storage areas, stockpile

management and tracking protocols;

o Soil Characterization and Disposal Requirements;

o Dust Control measures;

o Waste Disposal;

o Decontamination procedures;

o Notification and responsibility requirements;

o Site control measures;

o Site maps.

• At this time we understand that the City has elected to proceed with the installation of an

engineering control in order to prevent exposure and migration of the impacted soil.

Based on the 30% design site plan provided by the City for the proposed development,

specific areas of Site A and Site B will be covered with a minimum of 12 inches of fill.

• Based on information provided by RER, installing a liner of specific characteristics (color

and impermeability) below 12 inches of fill may be sufficient to achieve the required

level of protection and serve as an engineering control for the Site. It is our

understanding that this engineering control alternative will be presented to RER for

formal approval. Liner characteristics may include, but are not limited to, impermeability

and color.

• Therefore, on those areas proposed to be raised by a minimum of 12 inches of fill, an

adequate liner will be installed prior to installation of the fill layer.

• The areas not currently proposed to be covered with a minimum of 12 inches of fill will

be excavated to a depth of 12 inches in order to install the liner followed by 12 inches of

clean fill. Please note that excavated soil will be subject to the SMP provisions and shall

be treated as contaminated soil.

• Those areas proposed to be covered by impermeable pavement (such as paved pathways,

roadways, parking) will serve as an engineering control (to be approved by RER).

DRAFT



Recommendations pertaining to existing groundwater impacts are as follows:

• Groundwater sampling did not indicate the presence of COCs within Site A. Therefore

no groundwater provisions are expected to be required during development on that site.

However, RER might request that additional groundwater sampling be conducted in the

specific dewatering areas to provide assurance that no groundwater impacts are present

within those areas and no potential groundwater contamination migration or exacerbation

occurs during dewatering.

• Arsenic concentrations were detected above the GCTL for the groundwater samples

collected from MW-3 at Site B. Therefore the following general recommendations are

provided:

o Secure a dewatering permit that includes evaluation and management of

impacted groundwater within Site B. Based on the results of the filtered samples,

we anticipate that the application of a filter process will be sufficient to treat the

water to regulatory standards for disposal purposes if treatment is necessary.

o It is anticipated that RER would require a dewatering plan for the property if

dewatering is proposed as part of site development. If dewatering is being

conducted in areas that are demonstrated not to have arsenic impacts, then the

dewatering plan would demonstrate that the dewatering activities would not

exacerbate or move groundwater impacts. If dewatering activities will be

performed in an area with impacted groundwater, then treatment of the

groundwater prior to discharge or disposal of dewatering effluent would be

required.

o Restrict the use of the irrigation wells to eliminate the influence of pumping

impacted groundwater.

o Route the point of discharge of drainage structures to outside the impacted area

in Site B.

We recommend that the City seeks RER’s conceptual approval of the closure approach elected by

the City including the above provisions. The above recommendations are concerning

development of the subject properties and do not include provisions regarding the regulatory

requirements regarding site assessment. Please note that RER may not grant regulatory closure of

the site based on the absence of soil impact delineation within the property boundaries and the

requirement for offsite delineation. Please note offsite assessment and implementation of a

restrictive covenant for the properties may be required to complete the regulatory closure of the

subject sites.

DRAFT

FIGURES

DRAFT

Site A

Site B

¹

LegendProject Location

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PROJECT NUMBER:7-0002-023

Location Map 11 "=1,000 '

E Sciences, IncorporatedFL Engineering Lic. #8691224 SE 9th StreetFt. Lauderdale, Florida 33316www.esciencesinc.comPhone: 954-484-8500Fax: 954-484-5146

DATE: 12/12/2014

SCALE:DRAWNBY: TV

CHECKEDBY: MP

FIGURE21st Street Community Center and Band Shell Building and Parking

Area West of Convention Center

0 500 1,000 1,500 2,000250

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DRAFT

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SCALE:DRAWNBY: TV

CHECKEDBY: MP



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DRAFT

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DATE: 12/12/2014

SCALE:DRAWNBY: TV

CHECKEDBY: MP



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DRAFT

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DATE: 12/12/2014

SCALE:DRAWNBY: TV

CHECKEDBY: MP



0 40 80 12020

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Miami Beach, FL

DRAFT

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Soil Sampling Locationsat Site B 4B

1 "=150 '


DATE: 12/12/2014

SCALE:DRAWNBY: TV

CHECKEDBY: MP



0 50 100 150 20025

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Miami Beach, FL

DRAFT

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DRAFT

APPENDIX A

DRAFT

Enclosed is the laboratory report for your project. All results meet the requirements of the NELAC standards. Please note the following:

(1) The samples were received as stated on the chain of custody, correctly labeled and at the proper temperature unless otherwise noted. The results contained in this report relate only to the items tested or to the samples as received by the laboratory.

(2) This report may not be reproduced except in full, without the written approval of the laboratory. Any

anomalies are noted in the case narrative.

(3) Results for all solid matrices are reported in dry weight unless otherwise noted.

(4) Results for all liquid matrices are analyzed as received in the laboratory unless otherwise noted.

(5) Samples are disposed of within 30 days of their receipt by the laboratory.

(6) A statement of Qualifiers is available upon request.

(7) Certain analyses are subcontracted to outside NELAC certified laboratories and are designated on your report.

(8) Precision & Accuracy will be provided when clients require a measure of estimated uncertainty.

(9) The issuance of the final Certificate of Analysis takes precedence over any previous Preliminary Report

Preliminary Data should not be used for regular purposes. Authorized signature(s) is provided on final report only

Please contact me if you have any questions or concerns regarding this report. Sincerely,

Pamela Shore QA Officer

December 04, 2014E Sciences

0013067

Maria Paituvi

Ft Lauderdale, FL 33316

(954) 484-8500

LOG #:

Page 1 of 141550 Latham Road, Suite 2, West Palm Beach, FL 33409, phone: (561)689-6701, fax: (561)689-6702

EPA # FL01227 DOH# E86957 SFWMD# 48141 PBC # VC0000018083

DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street

(954) 484-8500 (954) 484-5146 Parking Lot and 21st Street Community Center

7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi


CERTIFICATE OF ANALYSIS

0013067

DP2-11212014Description:

Received:

Sampled:Lab ID: 0013067-01 11/21/14 12:45

11/21/14 16:00Matrix: Water Sampled By: Trent Van Allen

EPA Method 8081A

Parameter UnitsResults MDLMethod AnalystDateCAS # DF

Extraction Analysis

DatePQLQ

alpha-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-84-6 0.01110.004 0.004JEE, U

gamma-BHC (Lindane) SLug/L 11/25/14 11/26/14EPA 3510C / 8081A58-89-9 0.01110.004 0.004JEE, U

Heptachlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A76-44-8 0.01710.006 0.006JEE, U

Aldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A309-00-2 0.01110.004 0.004JEE, U

beta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-85-7 0.01310.004 0.004JEE, U

delta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-86-8 0.01210.004 0.004JEE, U

Heptachlor epoxide SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1024-57-3 0.01110.004 0.004JEE, U

Endosulfan I SLug/L 11/25/14 11/26/14EPA 3510C / 8081A959-98-8 0.01410.004 0.004JEE, U

gamma-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5566-34-7 0.06010.020 0.020JEE, U

alpha-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5103-71-9 0.06010.020 0.020JEE, U

4,4-DDE SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-55-9 0.01510.005 0.005JEE, U

Dieldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A60-57-1 0.00210.00075 0.00075JEE, U

Endrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-20-8 0.01310.004 0.004JEE, U

Endosulfan II SLug/L 11/25/14 11/26/14EPA 3510C / 8081A33213-65-9 0.01710.006 0.006JEE, U

4,4-DDD SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-54-8 0.00710.002 0.002JEE, U

4,4-DDT SLug/L 11/25/14 11/26/14EPA 3510C / 8081A50-29-3 0.01310.004 0.004JEE, U

Endrin aldehyde SLug/L 11/25/14 11/26/14EPA 3510C / 8081A7421-93-4 0.01010.003 0.003JEE, U

Endosulfan sulfate SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1031-07-8 0.00810.003 0.003JEE, U

Methoxychlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-43-5 0.01510.005 0.005JEE, U

Endrin Ketone SLug/L 11/25/14 11/26/14EPA 3510C / 8081A53494-70-5 0.01010.003 0.003JEE, U

Total Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081ANA 0.06010.020 0.020JEE, U

Toxaphene SLug/L 11/25/14 11/26/14EPA 3510C / 8081A8001-35-2 0.22510.075 0.075JEE, U

% Recovery % Recovery LimitsQ

Surrogate: Decachlorobiphenyl %2051-24-3 Limit 46-153JEE, U

Surrogate: Tetrachloro-m-xylene %877-09-8 Limit 56-153JEE, U



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-01 11/21/14 12:45


EPA Method 8141 List in Water


Extraction Analysis

DatePQLQ

Bolstar, (Sulprofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0910.03 0.03JEE, U

Crotoxphos (Ciodrin) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0810.009 0.009JEE, U

Dichlofenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 5.010.02 0.02JEE, U

Aspon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3244-90-4 0.110.04 0.04JEE, U

Azinphos, Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C86-50-0 0.110.04 0.04JEE, U

Azinphos, Ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2642-71-9 0.110.04 0.04JEE, U

Carbophenothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C786-19-6 0.110.04 0.04JEE, U

Chlorpyrifos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2921-88-2 0.110.04 0.04JEE, U

Chlorpyrifos Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C5598-13-0 0.0810.03 0.03JEE, U

Coumaphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-72-4 0.410.1 0.1JEE, U

Demeton O & S SLug/L 11/25/14 11/25/14EPA 3510C / 8270C8065-48-3 0.210.05 0.05JEE, U

Diazinon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C333-41-5 0.110.04 0.04JEE, U

Dichlorvos (DDVP) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C62-73-7 0.0410.01 0.01JEE, U

Dicrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C141-66-2 0.0410.02 0.02JEE, U

Dimethoate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C60-51-5 0.0510.02 0.02JEE, U

Dioxathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C78-34-2 0.0910.03 0.03JEE, U

Disulfoton SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-04-4 0.210.08 0.08JEE, U

EPN SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2104-64-5 0.0910.03 0.03JEE, U

Ethion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C563-12-2 0.0810.02 0.02JEE, U

Ethoprop SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13194-48-4 0.0910.03 0.03JEE, U

Famphur SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-85-7 0.0810.03 0.03JEE, U

Fenitrothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C122-14-5 0.0410.02 0.02JEE, U

Fensulfothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C115-90-2 0.0210.005 0.005JEE, U

Fenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C55-38-9 0.0910.03 0.03JEE, U

Fonophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C944-22-9 0.0510.02 0.02JEE, U

Leptophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C21609-90-5 0.210.06 0.06JEE, U

Malathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C121-75-5 0.110.03 0.03JEE, U

Merphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C150-50-5 0.210.08 0.08JEE, U

Mevinphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C7786-34-7 0.0710.02 0.02JEE, U

Monocrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C6923-22-4 0.0210.007 0.007JEE, U

Naled SLug/L 11/25/14 11/25/14EPA 3510C / 8270C300-76-5 0.0310.01 0.01JEE, U

Parathion-ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-38-2 0.310.1 0.1JEE, U

Parathion-methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-00-0 0.0210.008 0.008JEE, U

Phorate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-02-2 0.0610.02 0.02JEE, U

Phosphamidon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13171-21-6 0.0510.02 0.02JEE, U

Ronnel SLug/L 11/25/14 11/25/14EPA 3510C / 8270C299-84-3 0.110.04 0.04JEE, U



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-01 11/21/14 12:45




Extraction Analysis

DatePQLQ

Stirophos (Tetrachlorvinphos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C22248-79-9 0.0510.02 0.02JEE, U

Sulfotepp SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3689-24-5 0.0810.03 0.03JEE, U

Terbufos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13071-79-9 0.0610.02 0.02JEE, U

Thionazin (Zinophos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C297-97-2 0.0710.02 0.02JEE, U

Tokuthion (Prothiofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C34643-46-4 0.0410.01 0.01JEE, U

Trichloronate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C327-98-0 0.210.06 0.06JEE, U


Surrogate: Nitrobenzene-d5 %NA Limit 47-131JEE, U

Surrogate: 2-Fluorobiphenyl %321-60-8 Limit 51-134JEE, U

Surrogate: p-Terphenyl-d14 %NA Limit 59-135JEE, U

Metals by EPA 6000/7000 Series Methods


Extraction Analysis

DatePQLQ

Arsenic DDmg/L 11/25/14 11/25/14EPA 6020B7440-38-2 0.00510.000377 0.000377U

Lead DDmg/L 11/25/14 11/25/14EPA 6020B7439-92-1 0.00510.006 0.00001



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067

DU2-11212014Description:

Received:

Sampled:Lab ID: 0013067-02 11/21/14 14:00

11/21/14 16:00Matrix: Soil Sampled By: Trent Van Allen

EPA Method 8081A


Extraction Analysis

DatePQLQ

alpha-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-84-6 0.110.03 0.03U

gamma-BHC (Lindane) DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A58-89-9 0.110.04 0.04U

Heptachlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A76-44-8 0.110.04 0.04U

Aldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A309-00-2 0.110.03 0.03U

beta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-85-7 0.110.05 0.05U

delta-BHC DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A319-86-8 0.110.04 0.04U

Heptachlor epoxide DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1024-57-3 0.110.04 0.04U

Endosulfan I DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A959-98-8 0.110.03 0.03U

gamma-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5566-34-7 0.110.9 0.04

alpha-Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A5103-71-9 0.110.6 0.04

4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.114.5 0.04

Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.04 0.04U

Endrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-20-8 0.110.01 0.01U

Endosulfan II DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A33213-65-9 0.110.05 0.05U

4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U

Endrin aldehyde DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A7421-93-4 0.110.04 0.04U

Endosulfan sulfate DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A1031-07-8 0.110.04 0.04U

Methoxychlor DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-43-5 0.110.1 0.1U

Endrin Ketone DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A53494-70-5 0.110.03 0.03U

Total Chlordane DDug/kg 11/26/14 11/26/14EPA 3545 / 8081ANA 0.111.5 0.1

Toxaphene DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A8001-35-2 0.110.1 0.1U


Surrogate: Decachlorobiphenyl 132 %2051-24-3 Limit 41-170

Surrogate: Tetrachloro-m-xylene 108 %877-09-8 Limit 40-175



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-02 11/21/14 14:00


EPA Method 8141 List in Soil


Extraction Analysis

DatePQLQ

Bolstar, (Sulprofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0075410.00251 0.00251JEE, U

Crotoxphos (Ciodrin) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0018110.000602 0.000602JEE, U

Dichlofenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C 0.0068910.00230 0.00230JEE, U

Aspon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3244-90-4 0.0073110.00244 0.00244JEE, U

Azinphos, Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C86-50-0 0.0105010.00350 0.00350JEE, U

Azinphos, Ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2642-71-9 0.0087110.00290 0.00290JEE, U

Carbophenothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C786-19-6 0.0097810.00326 0.00326JEE, U

Chlorpyrifos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2921-88-2 0.0043010.00143 0.00143JEE, U

Chlorpyrifos Methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C5598-13-0 0.0063910.00213 0.00213JEE, U

Coumaphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-72-4 0.0192010.00641 0.00641JEE, U

Demeton O & S SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C8065-48-3 0.0159010.00530 0.00530JEE, U

Diazinon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C333-41-5 0.0043310.00144 0.00144JEE, U

Dichlorvos (DDVP) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C62-73-7 0.0055810.00186 0.00186JEE, U

Dicrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C141-66-2 0.00095610.000319 0.000319JEE, U

Dimethoate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C60-51-5 0.0024510.000816 0.000816JEE, U

Dioxathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C78-34-2 0.0070010.00233 0.00233JEE, U

Disulfoton SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-04-4 0.0178010.00592 0.00592JEE, U

EPN SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C2104-64-5 0.0079610.00266 0.00266JEE, U

Ethion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C563-12-2 0.0072510.00242 0.00242JEE, U

Ethoprop SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13194-48-4 0.0063810.00213 0.00213JEE, U

Famphur SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C52-85-7 0.0076510.00255 0.00255JEE, U

Fenitrothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C122-14-5 0.0044910.00150 0.00150JEE, U

Fensulfothion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C115-90-2 0.0017710.00059 0.00059JEE, U

Fenthion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C55-38-9 0.0068010.00227 0.00227JEE, U

Fonophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C944-22-9 0.0035310.00118 0.00118JEE, U

Leptophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C21609-90-5 0.0124010.00413 0.00413JEE, U

Malathion SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C121-75-5 0.0059410.00198 0.00198JEE, U

Merphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C150-50-5 0.0227010.00758 0.00758JEE, U

Mevinphos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C7786-34-7 0.0027510.000916 0.000916JEE, U

Monocrotophos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C6923-22-4 0.00095310.000318 0.000318JEE, U

Naled SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C300-76-5 0.0023110.000769 0.000769JEE, U

Parathion-ethyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C56-38-2 0.0290010.00967 0.00967JEE, U

Parathion-methyl SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-00-0 0.0056710.00189 0.00189JEE, U

Phorate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C298-02-2 0.0081010.00270 0.00270JEE, U

Phosphamidon SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13171-21-6 0.0014610.000487 0.000487JEE, U

Ronnel SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C299-84-3 0.0074710.00249 0.00249JEE, U



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-02 11/21/14 14:00




Extraction Analysis

DatePQLQ

Stirophos (Tetrachlorvinphos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C22248-79-9 0.0036710.00122 0.00122JEE, U

Sulfotepp SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C3689-24-5 0.0081910.00273 0.00273JEE, U

Terbufos SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C13071-79-9 0.0069010.00230 0.00230JEE, U

Thionazin (Zinophos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C297-97-2 0.0066210.00220 0.00220JEE, U

Tokuthion (Prothiofos) SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C34643-46-4 0.00025318.40E-5 8.40E-5JEE, U

Trichloronate SLmg/kg 11/28/14 11/29/14EPA 3545 / 8270C327-98-0 0.0092010.00307 0.00307JEE, U







Extraction Analysis

DatePQLQ

Arsenic PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7440-38-2 0.20015.75 0.003

Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.200125.4 0.007

Percent Dry Weight


Extraction Analysis

DatePQLQ

% Solids AT% 11/23/14 11/26/14CalculationNA 1.01100 1.0



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067

DUP3-11212014Description:

Received:

Sampled:Lab ID: 0013067-03 11/21/14 00:00


EPA Method 8081A


Extraction Analysis

DatePQLQ











4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.113.4 0.04




4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U












DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-03 11/21/14 00:00




Extraction Analysis

DatePQLQ







































DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-03 11/21/14 00:00




Extraction Analysis

DatePQLQ













Extraction Analysis

DatePQLQ



Percent Dry Weight


Extraction Analysis

DatePQLQ




DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-04 11/21/14 00:00


EPA Method 8081A


Extraction Analysis

DatePQLQ











4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.111.5 0.04




4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U












DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-04 11/21/14 00:00




Extraction Analysis

DatePQLQ







































DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21619

12/4/2014 9:24:08AM

Maria Paituvi



0013067


Received:

Sampled:Lab ID: 0013067-04 11/21/14 00:00




Extraction Analysis

DatePQLQ













Extraction Analysis

DatePQLQ



Percent Dry Weight


Extraction Analysis

DatePQLQ




DRAFT

Notes and Definitions

Analyte included in the analysis, but not detectedU

Analysis performed by Florida Environmental Cert#E86006JEE



DRAFT

Enclosed is the laboratory report for your project. All results meet the requirements of the NELAC standards. Please note the following:

(1) The samples were received as stated on the chain of custody, correctly labeled and at the proper temperature unless otherwise noted. The results contained in this report relate only to the items tested or to the samples as received by the laboratory.

(2) This report may not be reproduced except in full, without the written approval of the laboratory. Any

anomalies are noted in the case narrative.

(3) Results for all solid matrices are reported in dry weight unless otherwise noted.

(4) Results for all liquid matrices are analyzed as received in the laboratory unless otherwise noted.

(5) Samples are disposed of within 30 days of their receipt by the laboratory.

(6) A statement of Qualifiers is available upon request.

(7) Certain analyses are subcontracted to outside NELAC certified laboratories and are designated on your report.

(8) Precision & Accuracy will be provided when clients require a measure of estimated uncertainty.

(9) The issuance of the final Certificate of Analysis takes precedence over any previous Preliminary Report

Preliminary Data should not be used for regular purposes. Authorized signature(s) is provided on final report only

Please contact me if you have any questions or concerns regarding this report. Sincerely,

Pamela Shore QA Officer

December 04, 2014E Sciences

0013068

Maria Paituvi


(954) 484-8500

LOG #:



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-01 11/20/14 13:45


EPA Method 8081A


Extraction Analysis

DatePQLQ

alpha-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-84-6 0.01110.004 0.004JEE, U

gamma-BHC (Lindane) SLug/L 11/25/14 11/26/14EPA 3510C / 8081A58-89-9 0.01110.004 0.004JEE, U

Heptachlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A76-44-8 0.01710.006 0.006JEE, U

Aldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A309-00-2 0.01110.004 0.004JEE, U

beta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-85-7 0.01310.004 0.004JEE, U

delta-BHC SLug/L 11/25/14 11/26/14EPA 3510C / 8081A319-86-8 0.01210.004 0.004JEE, U

Heptachlor epoxide SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1024-57-3 0.01110.004 0.004JEE, U

Endosulfan I SLug/L 11/25/14 11/26/14EPA 3510C / 8081A959-98-8 0.01410.004 0.004JEE, U

gamma-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5566-34-7 0.06010.020 0.020JEE, U

alpha-Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081A5103-71-9 0.06010.020 0.020JEE, U

4,4-DDE SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-55-9 0.01510.005 0.005JEE, U

Dieldrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A60-57-1 0.00210.00075 0.00075JEE, U

Endrin SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-20-8 0.01310.004 0.004JEE, U

Endosulfan II SLug/L 11/25/14 11/26/14EPA 3510C / 8081A33213-65-9 0.01710.006 0.006JEE, U

4,4-DDD SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-54-8 0.00710.002 0.002JEE, U

4,4-DDT SLug/L 11/25/14 11/26/14EPA 3510C / 8081A50-29-3 0.01310.004 0.004JEE, U

Endrin aldehyde SLug/L 11/25/14 11/26/14EPA 3510C / 8081A7421-93-4 0.01010.003 0.003JEE, U

Endosulfan sulfate SLug/L 11/25/14 11/26/14EPA 3510C / 8081A1031-07-8 0.00810.003 0.003JEE, U

Methoxychlor SLug/L 11/25/14 11/26/14EPA 3510C / 8081A72-43-5 0.01510.005 0.005JEE, U

Endrin Ketone SLug/L 11/25/14 11/26/14EPA 3510C / 8081A53494-70-5 0.01010.003 0.003JEE, U

Total Chlordane SLug/L 11/25/14 11/26/14EPA 3510C / 8081ANA 0.06010.020 0.020JEE, U

Toxaphene SLug/L 11/25/14 11/26/14EPA 3510C / 8081A8001-35-2 0.22510.075 0.075JEE, U


Surrogate: Decachlorobiphenyl %2051-24-3 Limit 46-153JEE, U

Surrogate: Tetrachloro-m-xylene %877-09-8 Limit 56-153JEE, U



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-01 11/20/14 13:45




Extraction Analysis

DatePQLQ

Bolstar, (Sulprofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.110.004 0.004JEE, U

Crotoxphos (Ciodrin) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0310.009 0.009JEE, U

Dichlofenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 0.0810.02 0.02JEE, U

Guthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C 5.01JEE, U

Aspon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3244-90-4 0.110.04 0.04JEE, U

Azinphos, Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C86-50-0 0.110.04 0.04JEE, U

Azinphos, Ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2642-71-9 0.110.04 0.04JEE, U

Carbophenothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C786-19-6 0.110.04 0.04JEE, U

Chlorpyrifos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2921-88-2 0.110.04 0.04JEE, U

Chlorpyrifos Methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C5598-13-0 0.0810.03 0.03JEE, U

Coumaphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-72-4 0.410.1 0.1JEE, U

Demeton O & S SLug/L 11/25/14 11/25/14EPA 3510C / 8270C8065-48-3 0.210.05 0.05JEE, U

Diazinon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C333-41-5 0.110.04 0.04JEE, U

Dichlorvos (DDVP) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C62-73-7 0.0410.01 0.01JEE, U

Dicrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C141-66-2 0.0410.02 0.02JEE, U

Dimethoate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C60-51-5 0.0510.02 0.02JEE, U

Dioxathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C78-34-2 0.0910.03 0.03JEE, U

Disulfoton SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-04-4 0.210.08 0.08JEE, U

EPN SLug/L 11/25/14 11/25/14EPA 3510C / 8270C2104-64-5 0.0910.03 0.03JEE, U

Ethion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C563-12-2 0.0810.02 0.02JEE, U

Ethoprop SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13194-48-4 0.0910.03 0.03JEE, U

Famphur SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-85-7 0.0810.03 0.03JEE, U

Fenitrothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C122-14-5 0.0410.02 0.02JEE, U

Fensulfothion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C115-90-2 0.0210.005 0.005JEE, U

Fenthion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C55-38-9 0.0910.03 0.03JEE, U

Fonophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C944-22-9 0.0510.02 0.02JEE, U

Leptophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C21609-90-5 0.210.06 0.06JEE, U

Malathion SLug/L 11/25/14 11/25/14EPA 3510C / 8270C121-75-5 0.110.03 0.03JEE, U

Merphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C150-50-5 0.210.08 0.08JEE, U

Mevinphos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C7786-34-7 0.0710.02 0.02JEE, U

Monocrotophos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C6923-22-4 0.0210.007 0.007JEE, U

Naled SLug/L 11/25/14 11/25/14EPA 3510C / 8270C300-76-5 0.0310.01 0.01JEE, U

Parathion-ethyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C56-38-2 0.310.1 0.1JEE, U

Parathion-methyl SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-00-0 0.0210.008 0.008JEE, U

Phorate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C298-02-2 0.0610.02 0.02JEE, U

Phosphamidon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13171-21-6 0.0510.02 0.02JEE, U



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-01 11/20/14 13:45




Extraction Analysis

DatePQLQ

Ronnel SLug/L 11/25/14 11/25/14EPA 3510C / 8270C299-84-3 0.110.04 0.04JEE, U

Stirophos (Tetrachlorvinphos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C22248-79-9 0.0510.02 0.02JEE, U

Sulfotepp SLug/L 11/25/14 11/25/14EPA 3510C / 8270C3689-24-5 0.0810.03 0.03JEE, U

TEPP (Tetraethyl Pyrophosphate) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C107-49-3 5.01JEE, U

Terbufos SLug/L 11/25/14 11/25/14EPA 3510C / 8270C13071-79-9 0.0610.02 0.02JEE, U

Thionazin (Zinophos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C297-97-2 0.0710.02 0.02JEE, U

Tokuthion (Prothiofos) SLug/L 11/25/14 11/25/14EPA 3510C / 8270C34643-46-4 0.0410.01 0.01JEE, U

Trichlorfon SLug/L 11/25/14 11/25/14EPA 3510C / 8270C52-68-6 5.01JEE, U

Trichloronate SLug/L 11/25/14 11/25/14EPA 3510C / 8270C327-98-0 0.210.06 0.06JEE, U







Extraction Analysis

DatePQLQ

Arsenic DDmg/L 11/25/14 11/25/14EPA 6020B7440-38-2 0.00510.0083 0.000377

Lead DDmg/L 11/25/14 11/25/14EPA 6020B7439-92-1 0.00510.006 0.00001



DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-02 11/20/14 15:00


EPA Method 8081A


Extraction Analysis

DatePQLQ











4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.116.7 0.04




4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U












DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-02 11/20/14 15:00




Extraction Analysis

DatePQLQ







































DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-02 11/20/14 15:00




Extraction Analysis

DatePQLQ













Extraction Analysis

DatePQLQ



Percent Dry Weight


Extraction Analysis

DatePQLQ




DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-03 11/20/14 00:00


EPA Method 8081A


Extraction Analysis

DatePQLQ











4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.113.2 0.04

Dieldrin DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A60-57-1 0.110.1 0.04



4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U












DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-03 11/20/14 00:00




Extraction Analysis

DatePQLQ







































DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-03 11/20/14 00:00




Extraction Analysis

DatePQLQ













Extraction Analysis

DatePQLQ


Lead PLSmg/kg dry 12/02/14 12/03/14EPA 6020B7439-92-1 0.2001311 0.007E

Percent Dry Weight


Extraction Analysis

DatePQLQ




DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-04 11/20/14 00:00


EPA Method 8081A


Extraction Analysis

DatePQLQ











4,4-DDE DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-55-9 0.112.6 0.04




4,4-DDD DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A72-54-8 0.110.07 0.07U

4,4-DDT DDug/kg 11/26/14 11/26/14EPA 3545 / 8081A50-29-3 0.110.03 0.03U












DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-04 11/20/14 00:00




Extraction Analysis

DatePQLQ







































DRAFT

LOG #:

PROJECT:

PROJECT #:

REPORTED:

COC#:

ATTN:

FAX: PHONE:

E Sciences

224 SE 9th Street


7-0002-023

21623

12/4/2014 9:38:04AM

Maria Paituvi



0013068


Received:

Sampled:Lab ID: 0013068-04 11/20/14 00:00




Extraction Analysis

DatePQLQ













Extraction Analysis

DatePQLQ



Percent Dry Weight


Extraction Analysis

DatePQLQ




DRAFT

Notes and Definitions

Analyte included in the analysis, but not detectedU

Analysis performed by Florida Environmental Cert#E86006JEE

The concentration indicated for this analyte is an estimated value above the calibration range of the instrument.. This

value is considered an estimate (CLP E-flag).

E



DRAFT

DRAFT

DRAFT

02/02/15

Technical Report for

E Sciences, Inc

Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

7-0002-025

Accutest Job Number: FA21662

Sampling Date: 01/24/15

Report to:

E Sciences, Inc224 SE 9th StFt Lauderdale, FL [email protected]

ATTN: Maria Paituvi

Total number of pages in report:

Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)

DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),

AK, AR, GA, KY, MA, NV, OK, UT, WA

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.

Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Program

and/or state specific certification programs as applicable.

Client Service contact: Andrea Colby 407-425-6700

Norm FarmerTechnical Director

Southeast

02/02/15

e-Hardcopy 2.0Automated Report

51

Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.

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Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 3Section 2: Summary of Hits .................................................................................................... 4Section 3: Sample Results ........................................................................................................ 5

3.1: FA21662-1: MW1-01242015 ....................................................................................... 63.2: FA21662-2: MW2-01242015 ....................................................................................... 93.3: FA21662-3: MW3-01242015 ....................................................................................... 123.4: FA21662-3F: MW3-01242015 ..................................................................................... 153.5: FA21662-4: MW4-01242015 ....................................................................................... 16

Section 4: Misc. Forms ............................................................................................................ 194.1: Chain of Custody ........................................................................................................... 20

Section 5: GC Semi-volatiles - QC Data Summaries ............................................................ 255.1: Method Blank Summary ................................................................................................ 265.2: Blank Spike Summary ................................................................................................... 275.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 29

Section 6: Metals Analysis - QC Data Summaries ................................................................ 306.1: Prep QC MP28493: Hg .................................................................................................. 316.2: Prep QC MP28495: Sb,As,Be,Cd,Cr,Cu,Pb,Ni,Se,Ag,Tl,Zn ........................................ 366.3: Prep QC MP28507: As .................................................................................................. 42

Section 7: General Chemistry - QC Data Summaries .......................................................... 487.1: Method Blank and Spike Results Summary .................................................................. 497.2: Matrix Spike Results Summary ..................................................................................... 507.3: Matrix Spike Duplicate Results Summary .................................................................... 51

12

34

56

7

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Accutest Laboratories

Sample Summary

E Sciences, IncJob No: FA21662

Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLProject No: 7-0002-025

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

FA21662-1 01/24/15 10:00 TV 01/26/15 AQ Ground Water MW1-01242015



FA21662-3F 01/24/15 11:10 TV 01/26/15 AQ Groundwater Filtered MW3-01242015


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Summary of Hits Page 1 of 1 Job Number: FA21662Account: E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLCollected: 01/24/15

Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method

FA21662-1 MW1-01242015

Chromium 1.5 I 10 1.0 ug/l SW846 6010CZinc 8.1 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.6 0.10 0.030 mg/l EPA 350.1

FA21662-2 MW2-01242015

Antimony 1.1 I 6.0 1.0 ug/l SW846 6010CChromium 1.4 I 10 1.0 ug/l SW846 6010CZinc 6.4 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.4 0.10 0.030 mg/l EPA 350.1

FA21662-3 MW3-01242015

Antimony 2.2 I 6.0 1.0 ug/l SW846 6010CArsenic 21.3 10 1.3 ug/l SW846 6010CSilver 0.80 I 10 0.70 ug/l SW846 6010CZinc 5.9 I 20 4.4 ug/l SW846 6010CNitrogen, Ammonia 1.0 0.10 0.030 mg/l EPA 350.1

FA21662-3F MW3-01242015

No hits reported in this sample.

FA21662-4 MW4-01242015

Antimony 1.5 I 6.0 1.0 ug/l SW846 6010CArsenic 4.1 I 10 1.3 ug/l SW846 6010CChromium 1.8 I 10 1.0 ug/l SW846 6010CNickel 1.6 I 40 0.40 ug/l SW846 6010CNitrogen, Ammonia 0.22 0.10 0.030 mg/l EPA 350.1

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Sample Results

Report of Analysis

Southeast

Section 3

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Report of Analysis Page 1 of 1

Client Sample ID: MW1-01242015 Lab Sample ID: FA21662-1 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 TT370659.D 1 01/29/15 EM 01/27/15 OP54722 GTT1590Run #2

Initial Volume Final VolumeRun #1 250 ml 5.0 mlRun #2

Pesticide PPL List

CAS No. Compound Result PQL MDL Units Q

309-00-2 Aldrin 0.0064 U 0.040 0.0064 ug/l319-84-6 alpha-BHC 0.0040 U 0.040 0.0040 ug/l319-85-7 beta-BHC 0.011 U 0.040 0.011 ug/l319-86-8 delta-BHC 0.0079 U 0.040 0.0079 ug/l58-89-9 gamma-BHC (Lindane) 0.0042 U 0.040 0.0042 ug/l12789-03-6 Chlordane 0.17 U 0.40 0.17 ug/l60-57-1 Dieldrin 0.0067 U 0.040 0.0067 ug/l72-54-8 4,4'-DDD 0.010 U 0.080 0.010 ug/l72-55-9 4,4'-DDE 0.015 U 0.080 0.015 ug/l50-29-3 4,4'-DDT 0.010 U 0.080 0.010 ug/l72-20-8 Endrin 0.0070 U 0.080 0.0070 ug/l1031-07-8 Endosulfan sulfate 0.0066 U 0.080 0.0066 ug/l7421-93-4 Endrin aldehyde 0.0065 U 0.080 0.0065 ug/l959-98-8 Endosulfan-I 0.0066 U 0.040 0.0066 ug/l33213-65-9 Endosulfan-II 0.0080 U 0.040 0.0080 ug/l76-44-8 Heptachlor 0.0062 U 0.040 0.0062 ug/l1024-57-3 Heptachlor epoxide 0.0072 U 0.040 0.0072 ug/l72-43-5 Methoxychlor 0.010 U 0.080 0.010 ug/l8001-35-2 Toxaphene 1.2 U 2.0 1.2 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

877-09-8 Tetrachloro-m-xylene 87% 42-127%2051-24-3 Decachlorobiphenyl 76% 27-127%

U = Not detected MDL = Method Detection Limit I = Result >= MDL but < PQL J = Estimated valuePQL = Practical Quantitation Limit V = Indicates analyte found in associated method blankL = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

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Client Sample ID: MW1-01242015 Lab Sample ID: FA21662-1 Date Sampled: 01/24/15 Matrix: AQ - Ground Water Date Received: 01/26/15

Percent Solids: n/a Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

Total Metals Analysis

Analyte Result PQL MDL Units DF Prep Analyzed By Method Prep Method

Antimony 1.0 U 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Arsenic 1.3 U 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Beryllium 0.20 U 4.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Cadmium 0.20 U 5.0 0.20 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Chromium 1.5 I 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Copper 1.0 U 25 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Lead 1.1 U 5.0 1.1 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Mercury 0.030 U 0.50 0.030 ug/l 1 01/27/15 01/27/15 JL SW846 7470A 1 SW846 7470A 3

Nickel 0.40 U 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Selenium 2.9 U 10 2.9 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Silver 0.70 U 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Thallium 1.4 U 10 1.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

Zinc 8.1 I 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4

(1) Instrument QC Batch: MA12180(2) Instrument QC Batch: MA12182(3) Prep QC Batch: MP28493(4) Prep QC Batch: MP28495

PQL = Practical Quantitation Limit U = Indicates a result < MDLMDL = Method Detection Limit I = Indicates a result >= MDL but < PQL

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General Chemistry

Analyte Result PQL MDL Units DF Analyzed By Method

Nitrogen, Ammonia 1.6 0.10 0.030 mg/l 1 01/28/15 11:21 DM EPA 350.1

Nitrogen, Nitrate a 2.5 U 5.0 2.5 mg/l 50 01/26/15 09:51 JA EPA 300/SW846 9056A

Nitrogen, Nitrite a 2.5 U 5.0 2.5 mg/l 50 01/26/15 09:51 JA EPA 300/SW846 9056A

(a) Dilution required due to matrix interference.


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Pesticide PPL List






9 of 51FA21662

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Antimony 1.1 I 6.0 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4















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General Chemistry



Nitrogen, Nitrate a 5.0 U 10 5.0 mg/l 100 01/26/15 10:08 JA EPA 300/SW846 9056A

Nitrogen, Nitrite a 5.0 U 10 5.0 mg/l 100 01/26/15 10:08 JA EPA 300/SW846 9056A



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Pesticide PPL List






12 of 51FA21662

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Arsenic 21.3 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4



Chromium 1.0 U 10 1.0 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4






Silver 0.80 I 10 0.70 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4





13 of 51FA21662

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General Chemistry



Nitrogen, Nitrate a 10 U 20 10 mg/l 200 01/26/15 10:25 JA EPA 300/SW846 9056A

Nitrogen, Nitrite a 10 U 20 10 mg/l 200 01/26/15 10:25 JA EPA 300/SW846 9056A



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Client Sample ID: MW3-01242015 Lab Sample ID: FA21662-3F Date Sampled: 01/24/15 Matrix: AQ - Groundwater Filtered Date Received: 01/26/15


Dissolved Metals Analysis



(1) Instrument QC Batch: MA12191(2) Prep QC Batch: MP28507


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Pesticide PPL List






16 of 51FA21662

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Arsenic 4.1 I 10 1.3 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4







Nickel 1.6 I 40 0.40 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4




Zinc 4.4 U 20 4.4 ug/l 1 01/27/15 01/27/15 LM SW846 6010C 2 SW846 3010A 4



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General Chemistry



Nitrogen, Nitrate a 2.5 U 5.0 2.5 mg/l 50 01/26/15 10:42 JA EPA 300/SW846 9056A

Nitrogen, Nitrite a 2.5 U 5.0 2.5 mg/l 50 01/26/15 10:42 JA EPA 300/SW846 9056A



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Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Chain of Custody

Southeast

Section 4

19 of 51FA21662

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FA21662: Chain of CustodyPage 1 of 5

20 of 51FA21662

44.1

DRAFT


21 of 51FA21662

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Job Change Order: FA21662_1/26/2015

Requested Date: 1/26/2015 Received Date: 1/26/2015

Account Name: E Sciences, Inc Due Date: 1/29/2015

Project Parking Lot & Community Center; 1700 Deliverable: COMMB

CSR: AC TAT (Days): 3

Sample #: Change: Please change TAT to 3 day, due 1/29/15. FA21662-all

Above Changes Per: Maria Paituvi Date: 1/26/2015

To Client: This Change Order is confirmation of the revisions, previously discussed with the Accutest Client Service

Page 1 of 1


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Job Change Order: FA21662_1/28/2015

Requested Date: 1/28/2015 Received Date: 1/26/2015

Account Name: E Sciences, Inc Due Date: 1/29/2015

Project Parking Lot & Community Center; 1700 Deliverable: COMMB

CSR: AC TAT (Days): 3

Sample #: Change: Please lab filter an unpreserved aliquot and FA21662-3 analyze for dissolved arsenic.

MW3-01242015

Above Changes Per: Maria Paituvi Date: 1/28/2015

To Client: This Change Order is confirmation of the revisions, previously discussed with the Accutest Client Service

Page 1 of 1


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GC Semi-volatiles

QC Data Summaries


• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries

Southeast

Section 5

25 of 51FA21662

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Method Blank Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-MB TT370630.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589

The QC reported here applies to the following samples: Method: SW846 8081B

FA21662-1, FA21662-2, FA21662-3, FA21662-4

CAS No. Compound Result RL MDL Units Q

309-00-2 Aldrin ND 0.040 0.0064 ug/l319-84-6 alpha-BHC ND 0.040 0.0040 ug/l319-85-7 beta-BHC ND 0.040 0.011 ug/l319-86-8 delta-BHC ND 0.040 0.0079 ug/l58-89-9 gamma-BHC (Lindane) ND 0.040 0.0042 ug/l12789-03-6 Chlordane ND 0.40 0.17 ug/l60-57-1 Dieldrin ND 0.040 0.0067 ug/l72-54-8 4,4'-DDD ND 0.080 0.010 ug/l72-55-9 4,4'-DDE ND 0.080 0.015 ug/l50-29-3 4,4'-DDT ND 0.080 0.010 ug/l72-20-8 Endrin ND 0.080 0.0070 ug/l1031-07-8 Endosulfan sulfate ND 0.080 0.0066 ug/l7421-93-4 Endrin aldehyde ND 0.080 0.0065 ug/l959-98-8 Endosulfan-I ND 0.040 0.0066 ug/l33213-65-9 Endosulfan-II ND 0.040 0.0080 ug/l76-44-8 Heptachlor ND 0.040 0.0062 ug/l1024-57-3 Heptachlor epoxide ND 0.040 0.0072 ug/l72-43-5 Methoxychlor ND 0.080 0.010 ug/l8001-35-2 Toxaphene ND 2.0 1.2 ug/l

CAS No. Surrogate Recoveries Limits


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Blank Spike Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-BS TT370628.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589


FA21662-1, FA21662-2, FA21662-3, FA21662-4

Spike BSP BSPCAS No. Compound ug/l ug/l % Limits

309-00-2 Aldrin 1 1.0 100 61-126319-84-6 alpha-BHC 1 1.0 100 66-129319-85-7 beta-BHC 1 1.0 100 66-132319-86-8 delta-BHC 1 1.0 100 41-14258-89-9 gamma-BHC (Lindane) 1 1.1 110 68-13260-57-1 Dieldrin 1 1.1 110 66-13872-54-8 4,4'-DDD 1 1.0 100 63-13872-55-9 4,4'-DDE 1 0.92 92 59-13350-29-3 4,4'-DDT 1 0.96 96 55-14572-20-8 Endrin 1 1.1 110 71-1471031-07-8 Endosulfan sulfate 1 0.97 97 64-1287421-93-4 Endrin aldehyde 1 0.82 82 60-130959-98-8 Endosulfan-I 1 1.1 110 66-13333213-65-9 Endosulfan-II 1 0.93 93 65-13376-44-8 Heptachlor 1 0.98 98 63-1301024-57-3 Heptachlor epoxide 1 1.1 110 67-12972-43-5 Methoxychlor 1 0.87 87 60-136

CAS No. Surrogate Recoveries BSP Limits


* = Outside of Control Limits.

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Blank Spike Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-BS2 TT370629.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589


FA21662-1, FA21662-2, FA21662-3, FA21662-4

Spike BSP BSPCAS No. Compound ug/l ug/l % Limits

12789-03-6 Chlordane 5 6.8 136 62-1418001-35-2 Toxaphene 10 14.9 149 57-151

CAS No. Surrogate Recoveries BSP Limits



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DRAFT

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA21662Account: ESFLFL E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchOP54722-MS TT370640.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589OP54722-MSD TT370641.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589FA21662-4 TT370637.D 1 01/28/15 EM 01/27/15 OP54722 GTT1589


FA21662-1, FA21662-2, FA21662-3, FA21662-4

FA21662-4 Spike MS MS Spike MSD MSD LimitsCAS No. Compound ug/l Q ug/l ug/l % ug/l ug/l % RPD Rec/RPD

309-00-2 Aldrin 0.038 U 1.92 2.4 125 1.92 2.0 104 18 61-126/21319-84-6 alpha-BHC 0.038 U 1.92 2.2 114 1.92 1.9 99 15 66-129/23319-85-7 beta-BHC 0.038 U 1.92 2.3 120 1.92 1.9 99 19 66-132/23319-86-8 delta-BHC 0.038 U 1.92 2.3 120 1.92 2.0 104 14 41-142/2758-89-9 gamma-BHC (Lindane) 0.038 U 1.92 2.3 120 1.92 2.0 104 14 68-132/2260-57-1 Dieldrin 0.038 U 1.92 2.5 130 1.92 2.2 114 13 66-138/2272-54-8 4,4'-DDD 0.077 U 1.92 2.4 125 1.92 2.1 109 13 63-138/2472-55-9 4,4'-DDE 0.077 U 1.92 2.0 104 1.92 1.8 94 11 59-133/2350-29-3 4,4'-DDT 0.077 U 1.92 2.1 109 1.92 1.9 99 10 55-145/2772-20-8 Endrin 0.077 U 1.92 2.5 130 1.92 2.3 120 8 71-147/231031-07-8 Endosulfan sulfate 0.077 U 1.92 2.2 114 1.92 2.0 104 10 64-128/267421-93-4 Endrin aldehyde 0.077 U 1.92 1.8 94 1.92 1.7 88 6 60-130/22959-98-8 Endosulfan-I 0.038 U 1.92 2.5 130 1.92 2.2 114 13 66-133/2133213-65-9 Endosulfan-II 0.038 U 1.92 2.1 109 1.92 1.9 99 10 65-133/2276-44-8 Heptachlor 0.038 U 1.92 2.3 120 1.92 1.9 99 19 63-130/231024-57-3 Heptachlor epoxide 0.038 U 1.92 2.5 130* 1.92 2.1 109 17 67-129/2372-43-5 Methoxychlor 0.077 U 1.92 1.8 94 1.92 1.7 88 6 60-136/25

CAS No. Surrogate Recoveries MS MSD FA21662-4 Limits

877-09-8 Tetrachloro-m-xylene 91% 80% 109% 42-127%2051-24-3 Decachlorobiphenyl 85% 81% 94% 27-127%


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Metals Analysis

QC Data Summaries


• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries

Southeast

Section 6

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BLANK RESULTS SUMMARY Part 2 - Method Blanks

Login Number: FA21662 Account: ESFLFL - E Sciences, Inc

Project: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

QC Batch ID: MP28493 Methods: SW846 7470A Matrix Type: AQUEOUS Units: ug/l

Prep Date: 01/27/15

MB Metal RL IDL MDL raw final

Mercury 0.50 .03 .03 -0.0074 <0.50

Associated samples MP28493: FA21662-1, FA21662-2, FA21662-3, FA21662-4

Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 1

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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY




Prep Date: 01/27/15 01/27/15

FA21662-1 QC FA21662-1 Spikelot QC Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits

Mercury 0.0 0.0 NC 0-20 0.0 3.1 3 103.3 80-120


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

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Prep Date: 01/27/15

FA21662-1 Spikelot MSD QC Metal Original MSD HGFLWS1 % Rec RPD Limit

Mercury 0.0 3.1 3 103.3 0.0 20



_________________________________________________________________________________________________________

Page 2

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SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY




Prep Date: 01/27/15

BSP Spikelot QC Metal Result HGFLWS1 % Rec Limits

Mercury 3.1 3 103.3 80-120



_________________________________________________________________________________________________________

Page 1

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SERIAL DILUTION RESULTS SUMMARY




Prep Date: 01/27/15

FA21662-1 QC Metal Original SDL 1:5 %DIF Limits

Mercury 0.00 0.00 NC 0-10



_________________________________________________________________________________________________________

Page 1

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QC Batch ID: MP28495 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/l

Prep Date: 01/27/15


Aluminum 200 15 14

Antimony 6.0 2 1 0.30 <6.0

Arsenic 10 2 1.3 -0.90 <10

Barium 200 1 1

Beryllium 4.0 .5 .2 -0.10 <4.0

Cadmium 5.0 .5 .2 -0.30 <5.0

Calcium 1000 50 50

Chromium 10 1 1 0.20 <10

Cobalt 50 .5 .2

Copper 25 1 1 -0.40 <25

Iron 300 17 17

Lead 5.0 1.1 1.1 0.20 <5.0

Magnesium 5000 50 35

Manganese 15 .5 1

Molybdenum 50 .5 .3

Nickel 40 .5 .4 -0.20 <40

Potassium 10000 200 200

Selenium 10 2.3 2.9 -0.30 <10

Silver 10 .65 .7 -0.20 <10

Sodium 10000 500 500

Strontium 10 .4 .5

Thallium 10 1.5 1.4 -1.2 <10

Tin 50 .7 1

Titanium 10 .9 1

Vanadium 50 .5 .6

Zinc 20 3 4.4 0.0 <20



_________________________________________________________________________________________________________

Page 1

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Prep Date: 01/27/15 01/27/15

FA21662-4 QC FA21662-4 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits

Aluminum

Antimony 0.0 2.9 200.0(a) 0-20 0.0 549 500 109.8 80-120

Arsenic 4.1 2.5 48.5 (a) 0-20 4.1 2260 2000 112.8 80-120

Barium

Beryllium 0.0 0.0 NC 0-20 0.0 53.2 50 106.4 80-120

Cadmium 0.0 0.0 NC 0-20 0.0 49.7 50 99.4 80-120

Calcium

Chromium 1.8 0.0 200.0(a) 0-20 1.8 213 200 105.6 80-120

Cobalt

Copper 0.0 0.0 NC 0-20 0.0 281 250 112.4 80-120

Iron

Lead 0.0 0.0 NC 0-20 0.0 504 500 100.8 80-120

Magnesium

Manganese

Molybdenum

Nickel 1.6 1.5 6.5 0-20 1.6 501 500 99.9 80-120

Potassium

Selenium 0.0 0.0 NC 0-20 0.0 2240 2000 112.0 80-120

Silver 0.0 0.0 NC 0-20 0.0 56.7 50 113.4 80-120

Sodium

Strontium

Thallium 0.0 0.0 NC 0-20 0.0 1900 2000 95.0 80-120

Tin

Titanium

Vanadium

Zinc 4.2 3.9 7.4 0-20 4.2 509 500 101.0 80-120


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) RPD acceptable due to low duplicate and sample concentrations.

_________________________________________________________________________________________________________

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Prep Date: 01/27/15

FA21662-4 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit

Aluminum

Antimony 0.0 540 500 108.0 1.7 20

Arsenic 4.1 2230 2000 111.3 1.3 20

Barium

Beryllium 0.0 53.1 50 106.2 0.2 20

Cadmium 0.0 49.4 50 98.8 0.6 20

Calcium

Chromium 1.8 213 200 105.6 0.0 20

Cobalt

Copper 0.0 277 250 110.8 1.4 20

Iron

Lead 0.0 503 500 100.6 0.2 20

Magnesium

Manganese

Molybdenum

Nickel 1.6 499 500 99.5 0.4 20

Potassium

Selenium 0.0 2210 2000 110.5 1.3 20

Silver 0.0 57.0 50 114.0 0.5 20

Sodium

Strontium

Thallium 0.0 1900 2000 95.0 0.0 20

Tin

Titanium

Vanadium

Zinc 4.2 508 500 100.8 0.2 20



_________________________________________________________________________________________________________

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Prep Date: 01/27/15

BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits

Aluminum

Antimony 511 500 102.2 80-120

Arsenic 2050 2000 102.5 80-120

Barium

Beryllium 53.7 50 107.4 80-120

Cadmium 51.5 50 103.0 80-120

Calcium

Chromium 215 200 107.5 80-120

Cobalt

Copper 267 250 106.8 80-120

Iron

Lead 498 500 99.6 80-120

Magnesium

Manganese

Molybdenum

Nickel 531 500 106.2 80-120

Potassium

Selenium 2040 2000 102.0 80-120

Silver 49.4 50 98.8 80-120

Sodium

Strontium

Thallium 1990 2000 99.5 80-120

Tin

Titanium

Vanadium

Zinc 512 500 102.4 80-120



_________________________________________________________________________________________________________

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Prep Date: 01/27/15


Aluminum

Antimony 0.00 0.00 NC 0-10

Arsenic 4.10 0.00 100.0(a) 0-10

Barium

Beryllium 0.00 0.00 NC 0-10

Cadmium 0.00 0.00 NC 0-10

Calcium

Chromium 1.80 0.00 100.0(a) 0-10

Cobalt

Copper 0.00 0.00 NC 0-10

Iron

Lead 0.00 0.00 NC 0-10

Magnesium

Manganese

Molybdenum

Nickel 1.60 0.00 100.0(a) 0-10

Potassium

Selenium 0.00 0.00 NC 0-10

Silver 0.00 0.00 NC 0-10

Sodium

Strontium

Thallium 0.00 0.00 NC 0-10

Tin

Titanium

Vanadium

Zinc 4.20 0.00 100.0(a) 0-10


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

_________________________________________________________________________________________________________

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POST DIGESTATE SPIKE SUMMARY




Prep Date: 01/27/15

Sample Final FA21662-4 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits

Aluminum

Antimony 9.8 10 115.6 0.2 5 100 115.6 80-120

Arsenic 9.8 10 4.1 4.018 121.4 0.2 5 100 117.4 80-120

Barium

Beryllium 9.8 10 53.9 0.2 2.5 50 107.8 80-120

Cadmium 9.8 10 52.6 0.2 2.5 50 105.2 80-120

Calcium

Chromium 9.8 10 1.8 1.764 57 0.2 2.5 50 110.5 80-120

Cobalt

Copper 9.8 10 116.2 0.2 5 100 116.2 80-120

Iron

Lead 9.8 10 50.7 0.2 2.5 50 101.4 80-120

Magnesium

Manganese

Molybdenum

Nickel 9.8 10 1.6 1.568 106.2 0.2 5 100 104.6 80-120

Potassium

Selenium 9.8 10 113 0.2 5 100 113.0 80-120

Silver 9.8 10 61.2 0.2 2.5 50 122.4*(a 80-120

Sodium

Strontium

Thallium 9.8 10 94.4 0.2 5 100 94.4 80-120

Tin

Titanium

Vanadium

Zinc 9.8 10 4.2 4.116 267.8 0.2 12.5 250 105.5 80-120


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested(a) Spike recovery indicates matrix interference and/or outside control limits due to high level in

sample relative to spike amount.

_________________________________________________________________________________________________________

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Prep Date: 01/30/15 01/30/15

MB MB Metal RL IDL MDL raw final raw final

Aluminum 200 14 14

Antimony 6.0 1 1

Arsenic 10 1.3 1.3 -0.80 <10 -0.90 <10

Barium 200 1 1

Beryllium 4.0 .2 .2

Cadmium 5.0 .2 .2

Calcium 1000 50 50

Chromium 10 1 1

Cobalt 50 .2 .2

Copper 25 1 1

Iron 300 17 17

Lead 5.0 1 1.1


Manganese 15 .5 1

Molybdenum 50 .3 .3

Nickel 40 .4 .4

Potassium 10000 200 200

Selenium 10 2.4 2.9

Silver 10 .7 .7

Sodium 10000 500 500

Strontium 10 .5 .5

Thallium 10 1.1 1.4

Tin 50 .9 1

Titanium 10 .5 1

Vanadium 50 .5 .6

Zinc 20 3 4.4

Associated samples MP28507: FA21662-3F


_________________________________________________________________________________________________________

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Prep Date: 01/30/15 01/30/15

FA21734-1 QC FA21734-1 Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits

Aluminum

Antimony

Arsenic 0.0 0.0 NC 0-20 0.0 2110 2000 105.5 80-120

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron anr

Lead anr

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

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Prep Date: 01/30/15

FA21734-1 Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit

Aluminum

Antimony

Arsenic 0.0 2100 2000 105.0 0.5 20

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron anr

Lead anr

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 2

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Prep Date: 01/30/15


Aluminum

Antimony

Arsenic 2080 2000 104.0 80-120

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron anr

Lead anr

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

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Prep Date: 01/30/15


Aluminum

Antimony

Arsenic 0.00 0.00 NC 0-10

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron anr

Lead anr

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

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Prep Date: 01/30/15

Sample Final FA21734-1 PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits

Aluminum

Antimony

Arsenic 9.8 10 104.7 0.2 5 100 104.7 80-120

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 1

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General Chemistry

QC Data Summaries


• Method Blank and Blank Spike Summaries• Duplicate Summaries• Matrix Spike Summaries

Southeast

Section 7

48 of 51FA21662

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METHOD BLANK AND SPIKE RESULTS SUMMARY GENERAL CHEMISTRY



MB Spike BSP BSP QC Analyte Batch ID RL Result Units Amount Result %Recov Limits

Nitrogen, Ammonia GP25398/GN64997 0.10 0.0 mg/l 2.5 2.51 100.4 90-110% Nitrogen, Nitrate GP25385/GN64952 0.10 0.0 mg/l 2.5 2.36 94.4 90-110% Nitrogen, Nitrite GP25385/GN64952 0.10 0.0 mg/l 2.5 2.38 95.2 90-110%

Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits

__________________________________________________________________________________________________________________________

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MATRIX SPIKE RESULTS SUMMARY GENERAL CHEMISTRY



QC Original Spike MS QC Analyte Batch ID Sample Units Result Amount Result %Rec Limits

Nitrogen, Ammonia GP25398/GN64997 FA21603-1 mg/l 0.030 U 2.5 2.4 96.0 90-110% Nitrogen, Nitrate GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.3 132.0N(a) 90-110% Nitrogen, Nitrite GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.7 148.0N(a) 90-110%

Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(a) Spike recovery indicates possible matrix interference.

__________________________________________________________________________________________________________________________

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MATRIX SPIKE DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY



QC Original Spike MSD QC Analyte Batch ID Sample Units Result Amount Result RPD Limit

Nitrogen, Ammonia GP25398/GN64997 FA21603-1 mg/l 0.030 U 2.5 2.4 0.0 20% Nitrogen, Nitrate GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.1 6.2 20% Nitrogen, Nitrite GP25385/GN64952 FA21662-1 mg/l 2.5 U 2.5 3.2 14.5 20%

Associated Samples: Batch GP25385: FA21662-1, FA21662-2, FA21662-3, FA21662-4Batch GP25398: FA21662-1, FA21662-2, FA21662-3, FA21662-4(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits

__________________________________________________________________________________________________________________________

Page 1

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02/02/15

Technical Report for

E Sciences, Inc

Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FL

7-0002-023

Accutest Job Number: FA21783

Sampling Date: 01/29/15

Report to:

E Sciences, Inc224 SE 9th StFt Lauderdale, FL [email protected]

ATTN: Maria Paituvi

Total number of pages in report:

Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)

DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),

AK, AR, GA, KY, MA, NV, OK, UT, WA

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.

Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Program

and/or state specific certification programs as applicable.

Client Service contact: Andrea Colby 407-425-6700

Norm FarmerTechnical Director

Southeast

02/02/15

e-Hardcopy 2.0Automated Report

18

Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.

1 of 18FA21783

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Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 3Section 2: Summary of Hits .................................................................................................... 4Section 3: Sample Results ........................................................................................................ 5

3.1: FA21783-1: MW3-01292015 ....................................................................................... 63.2: FA21783-1F: MW3-01292015 ..................................................................................... 7

Section 4: Misc. Forms ............................................................................................................ 84.1: Chain of Custody ........................................................................................................... 9

Section 5: Metals Analysis - QC Data Summaries ................................................................ 125.1: Prep QC MP28511: As ................................................................................................... 13

12

34

5

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Sample Summary

E Sciences, IncJob No: FA21783

Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLProject No: 7-0002-023

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID


FA21783-1F 01/29/15 08:30 TV 01/30/15 AQ Groundwater Filtered MW3-01292015

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Summary of Hits Page 1 of 1 Job Number: FA21783Account: E Sciences, IncProject: Parking Lot & Community Center; 1700 Convention Center Dr, Miami Bch, FLCollected: 01/29/15

Lab Sample ID Client Sample ID Result/Analyte Qual PQL MDL Units Method

FA21783-1 MW3-01292015

Arsenic 24.6 10 1.3 ug/l SW846 6010C

FA21783-1F MW3-01292015

Arsenic 25.0 10 1.3 ug/l SW846 6010C

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Sample Results

Report of Analysis

Southeast

Section 3

5 of 18FA21783

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DRAFT










6 of 18FA21783

33.1

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Client Sample ID: MW3-01292015 Lab Sample ID: FA21783-1F Date Sampled: 01/29/15 Matrix: AQ - Groundwater Filtered Date Received: 01/30/15


Dissolved Metals Analysis





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Misc. Forms

Custody Documents and Other Forms


• Chain of Custody

Southeast

Section 4

8 of 18FA21783

4

DRAFT


9 of 18FA21783

44.1

DRAFT


10 of 18FA21783

44.1

DRAFT


11 of 18FA21783

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Metals Analysis

QC Data Summaries


• Method Blank Summaries• Matrix Spike and Duplicate Summaries• Blank Spike and Lab Control Sample Summaries• Serial Dilution Summaries

Southeast

Section 5

12 of 18FA21783

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Prep Date: 01/30/15


Aluminum 200 14 14

Antimony 6.0 1 1

Arsenic 10 1.3 1.3 -0.70 <10

Barium 200 1 1

Beryllium 4.0 .2 .2

Cadmium 5.0 .2 .2

Calcium 1000 50 50

Chromium 10 1 1

Cobalt 50 .2 .2

Copper 25 1 1

Iron 300 17 17

Lead 5.0 1 1.1


Manganese 15 .5 1

Molybdenum 50 .3 .3

Nickel 40 .4 .4

Potassium 10000 200 200

Selenium 10 2.4 2.9

Silver 10 .7 .7

Sodium 10000 500 500

Strontium 10 .5 .5

Thallium 10 1.1 1.4

Tin 50 .9 1

Titanium 10 .5 1

Vanadium 50 .5 .6

Zinc 20 3 4.4

Associated samples MP28511: FA21783-1, FA21783-1F


_________________________________________________________________________________________________________

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Prep Date: 01/30/15 01/30/15

FA21752-5F QC FA21752-5F Spikelot QC Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits

Aluminum

Antimony

Arsenic 7.2 6.7 7.2 0-20 7.2 1930 2000 96.1 80-120

Barium

Beryllium anr

Cadmium anr

Calcium

Chromium

Cobalt

Copper anr

Iron anr

Lead anr

Magnesium

Manganese anr

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium anr

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

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Prep Date: 01/30/15

FA21752-5F Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit

Aluminum

Antimony

Arsenic 7.2 1980 2000 98.6 2.6 20

Barium

Beryllium anr

Cadmium anr

Calcium

Chromium

Cobalt

Copper anr

Iron anr

Lead anr

Magnesium

Manganese anr

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium anr

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 2

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Prep Date: 01/30/15


Aluminum

Antimony

Arsenic 1940 2000 97.0 80-120

Barium

Beryllium anr

Cadmium anr

Calcium

Chromium

Cobalt

Copper anr

Iron anr

Lead anr

Magnesium

Manganese anr

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium anr

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



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16 of 18FA21783

55.1.3

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Prep Date: 01/30/15

FA21752-5F QC Metal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic 7.20 8.40 16.7 (a) 0-10

Barium

Beryllium anr

Cadmium anr

Calcium

Chromium

Cobalt

Copper anr

Iron anr

Lead anr

Magnesium

Manganese anr

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium anr

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

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Page 1

17 of 18FA21783

55.1.4

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Prep Date: 01/30/15

Sample Final FA21752-5F PS Spike Spike Spike QC Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits

Aluminum

Antimony

Arsenic 9.8 10 7.2 7.056 108.5 0.2 5 100 101.4 80-120

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested

_________________________________________________________________________________________________________

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18 of 18FA21783

55.1.5

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APPENDIX B

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APPENDIX C

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Florida Department of Environmental Protection - Division of Waste Management- Bureau of Petroleum Storage Systems

WELL CONSTRUCTION AND DEVELOPMENT LOG

\\''ELL CONSTRUCTION DATA

wMcr~1 Site~e: FDEP Facility I.D. Number: !Well Ins~Jate(s): ~A.k< Nf L.C'I,. 1/ZJ l.o'5

Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:

~ On-Site D Right-of-Way DSI Shallow (Water-Table) Monitoring DP-r 0 Off-Site Private Property 0 Intermediate or Deep Monitoring 0 Above Grade D Rush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: ............................................................................................... If AG, list feet of riser above land surface:

Borehole Depth 1WellDepth ~~orehole Diameter · l~anhole Diameter Well Pad Size:

(feet): ' ') (feet): \5 (inches): 3, 2. ~ (inches): t)' \ feet by _..1_ feet -Riser Diameter and Material: Riser/Screen 0 Rush-Threaded Riser Length: .....l...._ feet

PVt., Connections: ·~

L)" lN(M .. D Other (describe) from 0 feet to .~ feet

Screen Diameter and Material: Screen Slot Size: Screen Length: J.2..._ feet

L~ ti\lct\ .. f~tPAL~ ~-C I C '!r.l\..1:-\ from ...s:_ feet to ~feet 1st Surface Casing Material: 1st Surface Casing I.D. (inches): 1st Surface Casing Length: feet --also check: D Permanent 0Temporary from 0 feet to feet

2nd Surface Casing Material: 2nd Surface Casing I.D. (inches): 2nd Surface Casing Length: feet --also check: D Permanent 0Temporary from 0 feet to feet

3rd Surface Casing Material: 3"' Surface Casing I.D. (inches): 3"' Surface Casing Length: -- feet

also check: D Permanent 0Temporary from 0 feet to feet

Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: •o feet

~13c) SAI\l.O [jJ ves 0No from .5_ feet to r-s feet

Filter Pack Seal Material and Filter Pack Seal Length: -!:1..- feet Size: 3'0Jc:/S -~i~\"' 0_ from ' feet to _s__ feet

Surface Seal Material: Surface Seal Length: ~feet

6~oor /PuP-.l~w{) ( C:·M(r~l from 0 feet to \ feet

WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): U Surge/Pump ~ Pump D Compressed Air

i {"1..3/"Zv( r:; D Other (describe)

Development Pump Type (check): Iii Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):

0 Submersible 0 Other (describe) ~'-( I Pumping Rate (gallons per minute): I Maximum Drawdown of Groundwater During Well Purged Dry (check one):

0 :r: (.,..ft'\ Development (feet):~ 0 \ Oves ¥J No

Pumping Condition (check one): Total Development Water Development Duration Development Water Drummed

[iJ Continuous D Intermittent Removed (gallons): \o (minutes): ~() (check one): IZJ Yes 0No

Water Appearance (color and odor) At Start of Development: Water Appearance (color and odor) At End of Development:

~J t,\zr rr.- , NCJ 1\, c Lcr::~~r;},_ ( ~~1>\=.,

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Florida Department of Environmental Protection- Division of Waste Management- Bureau of Petroleum Storage Systems


WELL CONSTRUCTION DATA

WMtber: SiteNA e: FDEP Facility I.D. Number: 1Well Install Date(s):

,lid- 2 !tt~ \.( ;r"' lt Lv-r VZ1/LDL'( Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:

~ On-Site D Right-of-Way ~ Shallow (Water-Table) Monitoring OPT 0 Off-Site Private Property 0 Intermediate or Deep Monitoring 0 Above Grade D Rush-to-Grade 0 Remediation or other (describe)

Surface Casing Install Method: ............................................................................................... If .\G, list feet of riser above land surfuce:

Borehole Depth IWellDepth ~~orehole Diameter ~~anhole Diameter Well Pad Size:

(feet): 1 ~- (feet): ~~ (inches): ], 2- ~ (inches): 0 ' _L_ feet by I feet

Riser Diameter and Material: Riser/Screen D Flush-Threaded Riser Length: _s_feet

j I ) liiiU\ ~v c.. Connections: D other (describe) . from _a_ feet to ...S::... feet

Screen Diameter and Material: Screen Slot Size: Screen Length: _.Lfeet

l , ~ ::T/\1{.~ ~£-PAl-l-. Q,D\w l NL"' from ~ feet to ..l...( feet

181 Surface Casing Material: 1 '1 Surface Casing I.D. (inches): 1st Surface Casing Length: feet --also check: 0 Permanent 0Temporary from 0 feet to feet

znd Surface Casing Material: zncl Surface Casing l.D. (inches): . znc! surface Casing Length: --feet

also check: D Permanent 0Temporary from 0 feet to feet

3rd Surface Casing Material: 3rd Surface Casing I.D. (inches): 3rd Surface Casing Length: --feet

also check: 0 Permanent 0Temporary from 0 feet to feet

Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: &O feet --'?.ofJo 5At.JO [i ves 0No from __t::_ feet to _!..S_ feet

Filter Pack Seal Material and Filter Pack Seal Length: ___j_ feet Size: ~/0.{_ 5f\N~

..... from l feet to 0 feet

Surface Seal Material: Surface Seal Length: _ ?._feet

br>. o:.n J fvr~ ... :t't-Ai'l'O Lf:Mr; 1\JI from G feet to ..L..._ feet

WELL DEVELOPMENT DATA Well Development Date: Well Development Method (check one): U Surge/Pump ljl Pump 0 Compressed Air

·, /t..-:s ; w5 0 other (desaibe)

Development Pump Type (check): ~ Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):

0 Submersible 0 Other (describe) rtb y ' Purnpin~Jite (gallons per minute): ~Maximum Drawdown of Groundwater During Well Purged Dry (check one):

Q, &AU..uN~ Development (feet): :;!J 0' DYes ~ No

Pumpin~ndition (check one): Total Development Water Development Duration Development Water Drummed

~ Continuous 0 Intermittent Removed (gallons): ~ (minutes): \ 4 (check one): fiLves 0No

Water Appearance (color and odor) At Start of Development: Water Appearance7 lor and odor) At End of Development:

'vJ ~~--~"1£ I ~J ~Ji'J n.- (\.-~-An... 'N Cf-.f [ I

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Florida Department of Environmental Protection- Division of Waste Management - Bureau of Petroleum Storage Systems


~7: : : :: : : : : ::: ::::: : :: :::: ::7 ::: :: :: :::: ::: :: ::: :: ::: ::: ::: :: ::: : : : :: :: ::: ::: :: : : :: :::~t.t.:~9~~r~v<:r:•P.~:j)~~~::: ::: :: :: : : :: :::: : :: ::: ::::: : ::: :::: : ::: : :::: ::: ::: : :::: ::: ::~ : :: ::: ::JJT?: fifeii' ~~~b~:· ~ tSite ~~~ ~~ . . (. FDEP Facility J.D. Number: I Well Install D~te(s): Mll\i-5 121 )1 ~--,n.~,, oMMurv:nt f.IV7~ ~ '/? 3 jz.oij;

Well Location and Type {check appropriate boxes): Well Purpose: 0 Perched Monitoring Well Install Method:

ltl On-Site 0 Right-of-Way [il Shallow (Water-Table) Monitoring Di>--r 0 Off-Site Private Property · 0 Intermediate or Deep Monitoring 0 Above Grade 0 Rush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: w~ooooooooooouooouuooouoooooooooouooooo•onoo ooouuoooooooooooo o o o oo ooOooo ouooo oo ooooooo

If AG, list feet of riser above land surface:

·Borehole Depth !Well Depth I Borehole Diameter ~~anhole Diameter Well Pad Size:

(feet): r .... (feet): n ~ (inches):~,(.~ (inches): 1.:\ _!_feet by ! feet ~

Riser Diameter and Material: Riser/Screen 0 Flush-Threaded Riser Length: -~feet

1/~ D\Jr Connections: 0 Other (describe) from 6 feet to c; feet "1 .tJ.(t-\

Screen Diameter and Material: Screen Slot Size: Screen Length: _!SL feet

1.;- 'If\1(.\1 ~f~f\ t\4.... from ....:L feet to I ( feet

1st Surface Casing Material: 1"1 Surface Casing l.D. (inches): 1"1 Surface Casing Length: feet --also check: 0 Pennanent 0Temporary from 0 feet to feet -2'00 Surface Casing Material: 2nd Surface Casing l.D. (inches): 2JWJ Surface Casing Length: feet --also check: 0Permanent 0Temporary from 0 feet to feet -3nl Surface Casing Material: 3nl Surface Casing I.D. (inches): 3nl Surface Casing Length: - feet

also check: 0 Permanent 0Temporary from 0 feet to feet

Filter Pack Material and Size: Prepacked Filter Around Screen (check one): Filter Pack Length: If.~ feet

'-~l$oS~ . ll9 Yes 0No from _s:_ feet to t. '' feet

Filter Pack Seal Material and Filter Pack Seal Length: ....!::L_ feet

Size: 3D { t,~":. SAr"fD from ~ feet to ~ feet

Surface Seal Material: Surface Seal Length: _ \_feet

i G,.r-cu-r. / PortTI..fte () (f{Y)~N1' . from _Q_ feet to \ feet - - - '

Development Pump Type (check): []. Centrifugal 0 Peristaltic Depth to Groundwater (before developing in feet): d., t.l \ 0 Submersible 0 other (describe) , v \

Pumpin~ ~te (gallons per m!nute): !Maximum Drawdown of Groundwater During Well Purged Dry (check one): ,!"'' ( n.. 1\ ""' '- Development (feet): ,J. " \ 0 Yes 'Cl No .,_) 1 11'1\ I.,UI•./ N U i,fll.J

Development Duration Development Water Drummed Pumpingcondition (check one): Total Development Water

[jJ Continuous 0 Intermittent Removed (gallons): I{) (minutes): LO (check one): f!] Yes 0No

..

Water Appearance (color and odor) At Start of Development: Water Appearance (color and odor) At End of Development:

-~~W~H~~~~~L~~~c-~k~~ -------------~& __ c_~~A-~~/~~~o~~f~~ ------------~ •: :: ;::77::: :;: ;: ;:; :::; :; ::: ;: ;:;:;:;:: :: :: ::: W:Ef.ili :C.ffJ~TRU:CTI0~..£1RUEVELOP~!T::RE~S: ::: ::: :; :: :: :::~::: :: ;::: : :::: :: ::: ::: ::: :: ::;: : :::::

L0d\'~ll~l\,l~ 7._\~1 s1~t.ti.'1' C:>H\i'V\'J~--~,, Ur\l')~fl L:)'1 t vJtS1 .Sa.oc.

·---------------------------------------------------------·------------- ------·----------

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Florida Department of Environmental Protection- Division of Waste Management- Bureau of Petroleum Storage Systems


Well Location and Type (check appropriate boxes): Well Purpose: 0 Perched Monitoring Well In~ll Method:

[jJ On-Site 0 Right-of-Way [11 Shallow (Water-Table) Monitoring 0 Off-Site Private Property · 0 Intermediate or Deep Monitoring

0 Above Grade 0 Flush-to-Grade 0 Remediation or Other (describe) Surface Casing Install Method: •••••oooouooonoouuuuooooooouoouooooooouoounoooouuouonouoooooooooouooooooonoooo

·If AG,list feet of riser above land surface:

Borehole Depth rWell Depth !Borehole Diameter !Manhole Diameter

!<inches): :]. 'l"f !Cinches): ~ (feet): ) ') (feet): ( <; Riser Diameter and Material:

I , ) "J.II\Ji..'i_ - pJ L Riser/Screen 0 Flush-Threaded Connections: 0 Other (describe)

Screen Diameter and Material: Screen Slot Size:

\, ~ 'lr'\l<..~~~t. ~ ... ~jlkfd-JJ 111 Surface Casing Material: 1"1 Surface Casing l.D. (inches):

also check: 0 Permanent 0 Temporary

2nd Surface Casing Material: 2nd Surface Casing I.D. (inches):


3rc1 Surface Casing Material: 3nl Surface Casing I.D. (inches):


Filter Pack Material and Size: Prepacked Filter Around Screen (check one):

' '"to /so 5AI'J-D . . l!l ves 0 No

Filter Pack Seal Material and

Size: so;~S' St>~N'b Surface Seal Material:

Well Pad Size:

I feet by ' feet

Riser Length: ....::i._ feet ...;

from _Q__ feet to ~feet

Screen Length: '·~ feet

from ~

111 Surface Casing Length:

from 0

2nd Surface Casing Length:

from 0

3rci Surface Casing Length:

from 0

Filter Pack Length:

from S' Filter Pack Seal Length:

from J

feet to \ ( feet

feet --feet to feet

feet --feet to feet

feet --feet to feet

\~ feet

feet to I 5 feet

....:L feet feet to ~ feet

Surface Seal Length: _ \_ feet

from ___:u_ feet to \ feet I 4 PPLn f Port 1Lt\c~ l f.f\1\fJV 7 ~-~~ ~.. ~ ....... _ i!W ~-~

~----.... --·--·"'""'!'~'!""'":'~'-~~~~~~~~\'!·~''!'~~~'!"·:·~.~-. !'" .. "!"'. !'" .. -.' ~-. ~-.... :-~ ... ·. -. . - . -.. -.-.. .-........ ~·.-. . -.-.. - .. -.-.. -.-. . -.~--. - . -. - . -.. - .. --. _.,_,...__......._....11!1 :::;:;:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::~~~:~E.W.~Q~~:i)~J:'~::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: ~~;I Development Dat;--,-· wcii~~mmt M;th~d(,check one): D Surge/Pump [jj Pu;p 0 Compressed-Air

. 1/21 /Zo•) 0 Other (describe)

Developnfent Pump Type (check): ftl Centrifugal D Peristaltic Depth to Groundwater (before developing in feet):

0 Submersible 0 Other (describe) ~~ \ Pumpl.nf te (gallons per minute): !Maximum Drawdown of Groundwater During Well Purged Dry (check one):

I - \ ... (). Development (feet): . t;J O Oves rn No

Pumpi~ Condition (check one): Total Development Water Development Duration Development Water Drummed

[ll.Continuous 0 Intermittent Removed (gallons): )6 (minutes): 7._0 (check one): ~ Yes 0No

Water Appearance (color and odor) At Ste,.0,1Development: .

IJ j,_'\'-; ~-'" • -;i~1 G ...... tJ: ,· WH'J-'"'ik../fJor~ Water Appearance (color and odor) At End of Development:

Ct...l AR. /IV or~£ ~o---~

:::: ::: ::; :;: ::::;:::;: :::::::::: ::: :: ::::::::: ;:;: :::W.EL'L~£2eU.cTI~.N:OR:UEVELOP.MENT::REM.AJU{s::::::::::::::::::::;::777:77::::::::;:::

iAxr1lzQr'\l; "1,(6 '1 ~~ R..f.Jt.~l (o!VItV'JLJJ~·l.·N Lf-r.rlf:/'1 Lo·-;, ti1J'-l S"ioP'

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