Port of Vancouver | - Appendix...2016/11/12 · Table E1-1: Results of Chemical Analysis of Surficial Sediment Samples (January 2016)Vancouver Fraser Port Authority Centerm Expansion

Appendix E1Surficial Sediment Chemistry

Laboratory Results (January 2016)

Table E1-1: Results of Chemical Analysis of Surficial Sediment Samples (January 2016)

Vancouver Fraser Port AuthorityCenterm Expansion Project / South Shore Area Environmental Studies

Appendix E1

E1-1

Sample ID DUP-1 DUP-2 DUP-3 DUP-4 DUP-5 ESED1-0-10 ESED1-20-30 ESED1-40-50 ESED2-0-10 ESED2-12-22 ESED3-0-10 ESED3-13-23 ESED4-0-10 ESED4-15-30 ESED4-38-48 ESED5-0-10 ESED5-23-33 ESED6-0-10Laboratory ID / Guideline ID CCME CCME NZ2107 NZ2137 NZ4418 NZ4421 NZ5929 NZ5926 NZ5927 NZ5928 NZ5974 NZ5975 NZ5935 NZ5973 NZ5930 NZ5931 NZ5932 NZ5933 NZ5934 NZ4423

Maxxam Job # SedQG (AL) SedQG (AL) B604169 B604169 B604597 B604597 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604958 B604597Units mg/kg mg/kg (mg/kg) mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Sampling Date ISQG - Marine PEL - Marine 2016/01/19 2016/01/19 2016/01/20 2016/01/20 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/20pH (pH Units) 1.00E+34 1.00E+34 N/A 8.06 8.64 8.08 8.18 8.22 8.08 8.12 7.97 7.91 7.99 8.17 8.37 8.12 8.13 8.07 7.96 8.1 8.18

Antimony 1.00E+34 1.00E+34 0.10 5.9 0.55 <0.10 0.6 1.36 0.67 0.77 1.31 4.21 0.68 1.83 0.84 0.42 0.49 0.76 0.75 0.74 1.11 0.43Arsenic 7.24 41.6 0.50 14.6 7.91 1.62 7.06 8.62 6.51 7.04 7.76 13.9 6.6 7.8 6.45 4.8 7.22 7.29 7.68 9.63 7.45 8.45Barium 1.00E+34 1.00E+34 0.10 204 116 23.4 50 106 37.6 59.9 55.7 113 63.3 61.3 40.5 32.3 43.7 43.1 52.8 53.3 56.5 44Beryllium 1.00E+34 1.00E+34 0.40 0.51 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40Cadmium 0.7 4.2 0.050 4.5 0.945 0.09 0.991 0.984 0.887 0.694 1.39 2.56 0.721 0.879 0.609 0.467 0.722 0.798 1.21 0.923 1.42 0.552Chromium (Total) 52.3 160 1.0 58.2 23 31 32 24.4 17.1 27.2 30.4 30.3 22.2 28.9 17 14.1 18.9 16.4 20.6 26 19.8 29.6Cobalt 1.00E+34 1.00E+34 0.30 11.5 7.81 5.25 7.73 7.69 5.93 8.71 8.52 9.18 7.8 10.9 5.99 4.74 6.41 5.88 7.07 8.25 6.71 7.43Copper 18.7 108 0.50 3810 98.6 10.9 122 115 175 216 312 365 245 275 121 124 256 142 146 288 94.8 80.1Lead 30.2 112 0.10 540 44.7 1.62 31 117 27 31 77.7 149 33 49.3 25.5 19.2 46 32.8 50.2 27.1 60.4 18.2Mercury 0.13 0.7 0.050 2.42 0.121 <0.050 0.111 0.21 0.49 0.123 0.237 0.594 0.129 0.412 2.26 0.099 0.122 0.174 0.246 0.179 0.309 0.087Molybdenum 1.00E+34 1.00E+34 0.10 11.9 2.14 0.55 2.64 3.38 1.85 3.02 4.22 4.8 1.41 2.98 1.61 1.15 2.09 2.02 2.72 3.4 2.09 2.96Nickel 1.00E+34 1.00E+34 0.80 50.7 18.2 5.65 19.2 30 13.8 23.1 26.1 25.1 18.4 26.2 14.2 11.6 16 13.6 17.4 23.6 17.6 23.8Selenium 1.00E+34 1.00E+34 0.50 1.2 <0.50 <0.50 0.61 <0.50 <0.50 <0.50 0.76 0.69 <0.50 0.51 <0.50 <0.50 <0.50 <0.50 <0.50 0.53 <0.50 0.8Silver 1.00E+34 1.00E+34 0.050 5.53 0.406 <0.050 0.466 0.655 0.367 0.337 0.913 1.04 0.311 0.593 0.26 0.231 0.347 0.332 0.479 0.409 0.701 0.257Thallium 5 1.00E+34 1.00E+34 0.050 0.253 0.091 <0.050 0.134 0.099 0.15 0.108 0.165 0.17 0.141 0.14 0.144 0.091 0.112 0.149 0.149 0.171 0.109 0.097Tin 1.00E+34 1.00E+34 0.10 24 1.58 <0.10 2.57 19.4 2.1 2.55 4.54 14.1 1.67 2.4 1.72 1.32 1.68 1.83 3.74 1.54 5.11 1.44Uranium 1.00E+34 1.00E+34 0.050 2.42 1.15 0.505 1.42 1.45 1.1 1.13 1.35 1.28 0.981 1.25 0.801 0.849 1.01 0.963 1.04 1.36 0.913 1.43Vanadium 1.00E+34 1.00E+34 2.0 140 53.3 140 51.4 52.4 42.2 50.6 49.6 65.3 47.1 60 41.8 34.6 41.3 41.9 48.8 50.3 50.8 43.1Zinc 124 271 1.0 812 327 23.2 135 193 147 125 246 375 141 155 102 86.7 126 330 191 140 216 91.5

LEPHs 1.00E+34 1.00E+34 100 732 <100 125 179 <100 <100 <100 <100 <100 <100 <100HEPHs 1.00E+34 1.00E+34 100 3930 288 1500 1330 387 419 201 105 189 251 418F2 (C10-C16) 5 1.00E+34 1.00E+34 10 260 10 42 54 <10 38 11 <10 <10 15 26F3 (C16-C34) 1.00E+34 1.00E+34 10 4000 300 1200 1500 310 490 230 120 190 270 520F4 (C34-C50) 1.00E+34 1.00E+34 10 1400 240 220 500 100 150 97 56 93 140 190F4G (C34+) 1.00E+34 1.00E+34 100 17000 3100 730 16000 1600

2-Methylnaphthalene 0.0202 0.201 0.001 0.82 0.021 <0.0010 0.027 0.05 0.036 0.06 0.067 0.26 0.03 0.82 0.055 0.072 0.032 0.091 0.096 0.033 0.064 0.018Acenaphthene 0.00671 0.0889 0.0005 0.62 0.026 <0.00050 0.013 0.049 0.033 0.11 0.094 0.39 0.025 0.55 0.11 0.12 0.016 0.087 0.086 0.018 0.035 0.0062Acenaphthylene 0.00587 0.128 0.0005 0.23 0.017 0.0005 0.019 0.23 0.022 0.028 0.07 0.19 0.017 <0.027 0.024 0.014 0.03 0.047 0.066 0.031 0.03 0.0067Anthracene 0.0469 0.245 0.001 2.5 0.069 <0.0010 0.1 2.5 0.1 0.14 0.79 0.74 0.079 1.5 0.19 0.09 0.093 0.2 0.23 0.096 0.12 0.027Benzo(a)anthracene 0.0748 0.693 0.001 3.2 0.14 0.0019 0.16 3.2 0.13 0.25 1.1 1.1 0.18 1.6 0.23 0.18 0.2 0.26 0.34 0.36 0.18 0.043Benzo(a)pyrene 0.0888 0.763 0.001 2.4 0.16 0.0025 0.26 2.4 0.13 0.23 0.81 1.4 0.18 1.3 0.25 0.23 0.22 0.26 0.33 0.33 0.21 0.047Chrysene 0.108 0.846 0.001 4.6 0.17 0.002 0.27 3.1 0.16 0.32 1.3 1.4 0.23 2.1 0.27 0.22 0.29 0.38 0.43 0.53 0.23 0.059Dibenz(a,h)anthracene 0.00622 0.135 0.0005 0.39 0.025 0.0005 0.041 0.39 0.023 0.037 0.13 0.25 0.032 0.21 0.05 0.049 0.042 0.044 0.053 0.062 0.039 0.0087Fluoranthene 0.113 1.494 0.001 9 0.3 0.0025 0.29 9 0.33 0.45 3.7 2.6 0.39 2.7 0.64 0.47 0.52 0.74 1.1 0.8 0.45 0.089Fluorene 0.0212 0.144 0.001 0.68 0.032 <0.0010 0.031 0.64 0.04 0.073 0.25 0.47 0.035 0.68 0.1 0.065 0.044 0.14 0.16 0.034 0.062 0.013Naphthalene 0.0346 0.391 0.001 0.76 0.041 <0.0010 0.032 0.072 0.064 0.1 0.12 0.76 0.043 0.47 0.074 0.029 0.045 0.12 0.15 0.042 0.13 0.015Phenanthrene 0.0867 0.544 0.001 6.6 0.2 <0.0010 0.16 6.6 0.21 0.24 0.74 1.8 0.23 5.6 0.53 0.37 0.33 0.8 0.91 0.24 0.28 0.044Pyrene 0.153 1.398 0.001 8.2 0.46 0.0037 0.55 8.2 0.47 0.87 3.8 7.9 0.45 5.3 0.65 0.46 0.6 0.91 1.3 1 0.64 0.11PAHs (Total) 1.00E+34 1.00E+34 0.001 36 1.7 0.014 1.9 36 1.8 2.9 13 19 1.9 23 3.2 2.4 2.5 4.1 5.3 3.6 2.5 0.49

Aroclor 1242Aroclor 1248Aroclor 1254 0.063 0.709Aroclor 1260Total PCB 0.0215 0.189

Notes:

Metals

PetroleumHydrocarbons

Polycyclic Aromatic Hydrocarbons (PAH)

Polychlorinated Biphenyls (PCBs)

GuidelineMaximum Reported

Concentration

Reporting Limit

Red shaded cells exceed the CCME Sediment Qualtity Guideline Probable Effects Level (

Yellow shaded cells exceed the CCME Sediment Quality Guideline Interim Sediment Quality Guideline (ISQG



Appendix E1

E1-2

Sample ID Laboratory ID / Guideline ID CCME CCME

Maxxam Job # SedQG (AL) SedQG (AL)Units mg/kg mg/kg (mg/kg)

Sampling Date ISQG - Marine PEL - MarinepH (pH Units) 1.00E+34 1.00E+34 N/A

Antimony 1.00E+34 1.00E+34 0.10 5.9Arsenic 7.24 41.6 0.50 14.6Barium 1.00E+34 1.00E+34 0.10 204Beryllium 1.00E+34 1.00E+34 0.40 0.51Cadmium 0.7 4.2 0.050 4.5Chromium (Total) 52.3 160 1.0 58.2Cobalt 1.00E+34 1.00E+34 0.30 11.5Copper 18.7 108 0.50 3810Lead 30.2 112 0.10 540Mercury 0.13 0.7 0.050 2.42Molybdenum 1.00E+34 1.00E+34 0.10 11.9Nickel 1.00E+34 1.00E+34 0.80 50.7Selenium 1.00E+34 1.00E+34 0.50 1.2Silver 1.00E+34 1.00E+34 0.050 5.53Thallium 5 1.00E+34 1.00E+34 0.050 0.253Tin 1.00E+34 1.00E+34 0.10 24Uranium 1.00E+34 1.00E+34 0.050 2.42Vanadium 1.00E+34 1.00E+34 2.0 140Zinc 124 271 1.0 812

LEPHs 1.00E+34 1.00E+34 100 732HEPHs 1.00E+34 1.00E+34 100 3930F2 (C10-C16) 5 1.00E+34 1.00E+34 10 260F3 (C16-C34) 1.00E+34 1.00E+34 10 4000F4 (C34-C50) 1.00E+34 1.00E+34 10 1400F4G (C34+) 1.00E+34 1.00E+34 100 17000

2-Methylnaphthalene 0.0202 0.201 0.001 0.82Acenaphthene 0.00671 0.0889 0.0005 0.62Acenaphthylene 0.00587 0.128 0.0005 0.23Anthracene 0.0469 0.245 0.001 2.5Benzo(a)anthracene 0.0748 0.693 0.001 3.2Benzo(a)pyrene 0.0888 0.763 0.001 2.4Chrysene 0.108 0.846 0.001 4.6Dibenz(a,h)anthracene 0.00622 0.135 0.0005 0.39Fluoranthene 0.113 1.494 0.001 9Fluorene 0.0212 0.144 0.001 0.68Naphthalene 0.0346 0.391 0.001 0.76Phenanthrene 0.0867 0.544 0.001 6.6Pyrene 0.153 1.398 0.001 8.2PAHs (Total) 1.00E+34 1.00E+34 0.001 36


Notes:

Metals





Concentration

Reporting Limit



ESED6-20-38 ESED7-0-10 ESED7-20-30 ESED8-0-10 ESED8-20-30 ESED8-30-40 ESED8-40-53 ESED9-0-10 ESED9-25-35 ESED9-45-56 ESED10-0-10 ESED10-18-28 RSED1-0-10 RSED1-20-30 RSED2-0-10 RSED2-35-45NZ4422 NZ4404 NZ4405 NZ4408 NZ4409 NZ4411 NZ4410 NZ4412 NZ4413 NZ4390 NZ4406 NZ4407 NZ2105 NZ2106 NZ2121 NZ2122B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604597 B604169 B604169 B604169 B604169

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/19 2016/01/19 2016/01/19 2016/01/19

8.37 8.63 8.64 8.49 8.18 8.45 8.21 8.1 8.35 8.39 8.55 8.6 8.1 8.37 8.09 8.05

1.11 0.27 0.82 0.21 1.4 1.02 1.22 0.45 0.92 2.55 0.24 0.36 2.58 5.9 0.58 1.18.14 1.87 7.01 3.06 8.96 8 11.2 2.83 8.31 10.9 3.04 3.98 13.3 14.6 7.65 7.6108 21.6 82.2 39.4 141 147 204 27.4 65.3 97.9 24.4 27 75.3 81.5 44.6 46.6

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.400.68 0.401 0.67 0.83 3.13 2.19 1.46 1.15 1.75 4.5 0.418 0.242 1.63 3.74 0.546 0.48520.6 8.5 27.7 15.3 38.3 30 29.7 8.9 29.4 33.3 10.5 9.6 31.6 58.2 24.1 24.76.62 2.5 8.9 2.97 10.1 7.89 8.96 2.36 7.55 8.42 3.84 3.92 8.51 7.9 7.77 7.9880.8 49.6 142 54.6 123 97.3 88.3 76.5 518 133 44 37.5 3810 411 107 10375.7 15.2 52.4 65.9 185 124 141 44.3 146 262 14.5 12.5 365 540 27.3 29.9

0.159 <0.050 0.106 0.625 1.23 0.788 1.2 0.085 0.394 0.733 <0.050 0.052 0.561 2.42 0.113 0.113.06 2.11 3.06 1.25 4.73 4.79 3.8 1.31 3.71 5.05 0.61 2.71 4.01 11.9 1.93 2.4219.2 5.65 21.5 6.17 37.2 27.8 30.2 3.5 32.9 27 6.38 7.63 50.7 44.8 20.3 20.2

<0.50 <0.50 <0.50 <0.50 1.12 1.12 0.97 <0.50 0.99 0.94 <0.50 <0.50 0.73 0.83 <0.50 <0.500.452 0.08 0.556 0.144 1.55 1.27 0.831 0.165 1.21 2.42 0.098 0.081 2.58 5.53 0.374 0.7720.076 <0.050 0.11 0.076 0.156 0.125 0.134 0.083 0.108 0.199 0.089 0.062 0.143 0.166 0.111 0.09719.5 0.5 1.81 1.25 12.7 10.2 8.39 1.17 4.88 9.38 0.42 0.65 15.1 24 1.47 1.471.2 0.717 1.52 0.665 1.93 1.6 1.44 0.543 1.33 1.69 0.423 0.689 1.5 2.23 1.39 1.22

48.3 17.6 48.4 17.6 65.4 51.7 55.6 14.4 43.8 52.6 31.4 31.9 58.3 44.2 51.7 53.1145 48.7 183 117 364 207 203 164 330 751 67.9 49.1 297 812 92.5 103

<100 680 558 222 <100 141 732 <100122 2930 2620 1170 174 861 3930 730<10 230 200 73 <10 36 260 26120 3300 3000 1500 160 1000 4000 84088 1300 1100 430 100 390 1400 480

1200 17000 3500

0.18 0.0099 0.015 0.011 0.15 0.25 0.11 0.042 0.052 0.13 0.013 0.0082 0.17 0.29 0.027 0.0140.021 0.0033 0.0073 0.0062 0.061 0.06 0.041 0.0091 0.023 0.076 0.0055 0.0058 0.41 0.62 0.016 0.0120.015 0.0025 0.0057 0.0055 0.11 0.086 0.053 0.0097 0.032 0.11 0.0072 0.0097 0.052 0.095 0.017 0.0120.054 0.013 0.041 0.02 0.21 0.2 0.15 0.032 0.16 0.26 0.014 0.02 0.57 0.71 0.053 0.0370.092 0.02 0.063 0.06 0.43 0.28 0.17 0.059 0.29 0.62 0.016 0.021 0.91 1.7 0.098 0.0710.11 0.022 0.063 0.069 0.81 0.53 0.26 0.13 0.35 0.81 0.018 0.036 0.93 1.3 0.13 0.10.11 0.022 0.074 0.083 0.69 0.5 0.25 0.083 0.41 0.83 0.022 0.027 1.4 1.9 0.13 0.095

0.021 0.0041 0.011 0.016 0.16 0.07 0.051 0.024 0.066 0.15 0.0033 0.0067 0.11 0.2 0.019 0.0150.21 0.045 0.16 0.15 0.96 0.69 0.46 0.13 0.32 1.3 0.051 0.051 3.3 4.7 0.18 0.14

0.025 0.0055 0.015 0.014 0.099 0.12 0.063 0.013 0.043 0.11 0.0075 0.0089 0.39 0.45 0.022 0.0140.1 0.0081 0.02 0.011 0.15 0.21 0.17 0.058 0.078 0.15 0.034 0.031 0.25 0.37 0.04 0.025

0.14 0.023 0.078 0.11 0.64 0.44 0.26 0.072 0.19 0.69 0.032 0.034 3.2 2.4 0.12 0.0750.32 0.059 0.16 0.17 2 1.9 1 0.21 0.83 2.4 0.083 0.11 3.1 4.6 0.34 0.311.4 0.24 0.71 0.73 6.5 5.3 3 0.87 2.8 7.6 0.31 0.37 15 19 1.2 0.93



Appendix E1

E1-3








Notes:

Metals





Concentration

Reporting Limit



RSED2-60-70 RSED3-0-10 RSED3-15-25 RSED3-43-53 RSED4-0-10 RSED4-16-26 WSED1-0-10 WSED1-23-40 WSED2-0-10 WSED2-17-27 WSED3-0-10 WSED3-18-28 WSED4-0-10 WSED4-25-45 WSED4-60-70 WSED5-0-10NZ2123 NZ2126 NZ2127 NZ2128 NZ5976 NZ5977 NZ4419 NZ4420 NZ2129 NZ2130 NZ2125 NZ2124 NZ2112 NZ2113 NZ2114 NZ2110B604169 B604169 B604169 B604169 B604958 B604958 B604597 B604597 B604169 B604169 B604169 B604169 B604169 B604169 B604169 B604169

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/21 2016/01/21 2016/01/20 2016/01/20 2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/19

8.16 8.27 8.27 8.2 8.35 8.18 7.82 7.96 8.16 8.43 7.95 8.49 8.6 8.74 8.72 8.37

2.27 0.27 0.25 0.29 0.33 0.65 1.09 0.8 0.3 0.26 0.66 0.18 0.2 <0.10 <0.10 0.38.92 4.96 4.36 5.14 4.26 5.97 13.7 10.5 2.84 3.44 9.48 2.91 2.44 1.45 1.33 4.3453.6 36 56.1 58.8 44.7 112 71.8 64 26.3 36 48.4 21.8 26 22.4 23.4 33.2

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 0.51 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.401.26 0.327 0.234 0.324 0.376 0.424 2.41 1.54 0.095 0.174 0.943 0.132 0.175 0.069 0.076 0.27321.6 18.1 21 22.7 16.7 20.3 47 40.6 13.2 14.6 26.3 6.9 15.4 22.9 13.4 18.47.46 6.49 9.25 9.35 5.51 5.98 11.5 9.35 3.74 4.83 8.08 3.67 4.7 4.34 3.92 5.76129 33.9 33 30.5 68.9 78.4 162 200 16.4 28.9 92.8 16.3 25.5 11.6 10.7 49.8112 10.2 5.71 5.57 14.6 47.1 51.5 45.3 7.46 8.25 28.1 5.3 5.95 2 1.29 13.5

0.208 0.061 <0.050 <0.050 0.054 0.069 0.215 0.288 <0.050 <0.050 0.173 <0.050 <0.050 <0.050 <0.050 0.0644.55 1.36 1.02 1.26 1.44 1.98 5.61 4.44 0.57 0.77 1.73 0.59 0.5 0.53 0.46 0.7919.5 14.1 17.7 18.8 12.1 12.6 38.2 26.6 5.67 7.93 22.9 4.32 7.58 5.03 4.78 11.9

<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.2 0.68 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.501.31 0.159 0.112 0.103 0.182 0.283 0.697 0.688 0.063 0.097 0.431 <0.050 0.097 <0.050 <0.050 0.217

0.118 0.109 0.091 0.115 0.104 0.059 0.253 0.192 <0.050 0.055 0.116 <0.050 0.064 <0.050 <0.050 0.0872.25 0.53 0.23 0.24 0.93 1.58 3.81 3.35 0.39 0.36 1.66 0.15 0.25 <0.10 <0.10 0.531.57 0.861 0.867 1.11 0.841 1 2.42 2.13 1.84 0.676 1.13 0.384 0.454 0.417 0.528 0.90148.3 49.8 56.8 62.3 44.3 47.8 64.4 60.2 47.7 50 47.3 30.9 62 101 52 50.4154 52.2 53.2 52.2 72.7 108 327 194 35.8 47 119 40 36.1 22.4 22.7 56.5

<10068717

810300

0.044 <0.010 0.0025 0.0021 0.015 0.026 0.041 0.036 0.0019 0.0066 0.075 0.0067 0.0083 <0.0010 <0.0010 0.0130.036 0.0051 0.00055 0.00056 0.022 0.013 0.02 0.019 0.00096 0.0055 0.028 0.0035 0.0094 0.0011 <0.00050 0.00960.025 0.0063 0.0012 0.0011 0.0055 0.072 0.051 0.036 0.0016 0.0094 0.035 0.0045 0.0088 0.00063 <0.00050 0.00560.069 0.014 0.004 0.0041 0.056 0.32 0.18 0.12 0.0089 0.029 0.12 0.023 0.028 0.0029 <0.0010 0.030.15 0.036 0.0046 0.0034 0.16 2.2 0.36 0.18 0.02 0.04 0.27 0.049 0.06 0.0063 0.0014 0.0440.2 0.043 0.0055 0.0066 0.16 1.8 0.52 0.35 0.02 0.07 0.31 0.038 0.059 0.0075 0.0022 0.052

0.18 0.048 0.0062 0.0039 0.16 4.6 0.54 0.27 0.024 0.055 0.37 0.073 0.086 0.0079 0.0015 0.0560.031 0.0063 0.00082 0.0013 0.031 0.23 0.087 0.062 0.0029 0.012 0.052 0.0056 0.01 0.0011 0.00051 0.00870.33 0.074 0.01 0.0066 0.37 0.62 0.5 0.28 0.035 0.061 0.51 0.047 0.15 0.012 0.0022 0.1

0.038 <0.010 0.0015 0.0017 0.026 0.066 0.048 0.031 0.003 0.0071 0.046 0.0074 0.018 0.0018 <0.0010 0.0130.075 0.016 0.0051 0.0039 0.018 0.025 0.044 0.037 0.0047 0.014 0.12 0.01 0.0082 0.001 <0.0010 0.0210.21 0.035 0.0053 0.0048 0.19 0.33 0.23 0.15 0.014 0.034 0.34 0.035 0.16 0.012 <0.0010 0.0760.47 0.38 0.018 0.021 0.34 1.1 0.87 0.67 0.02 0.18 0.62 0.077 0.17 0.012 0.0023 0.131.9 0.67 0.065 0.061 1.6 11 3.5 2.2 0.16 0.52 2.9 0.38 0.77 0.066 0.01 0.57

<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02



Appendix E1

E1-4








Notes:

Metals





Concentration

Reporting Limit



WSED5-18-28 WSED6-0-10 WSED6-20-30 WSED7-0-10 WSED7-20-30 WSED7-50-60 WSED8-0-10 WSED10-0-10 WSED10-25-35 WSED10-50-60NZ2111 NZ2108 NZ2109 NZ4414 NZ4415 NZ4416 NZ4417 NZ2138 NZ2139 NZ2140B604169 B604169 B604169 B604597 B604597 B604597 B604597 B604169 B604169 B604169

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg2016/01/19 2016/01/19 2016/01/19 2016/01/20 2016/01/20 2016/01/20 2016/01/20 2016/01/19 2016/01/19 2016/01/19

8.34 8.26 8.35 8.34 8.2 8.32 8.04 8.03 8.1 8.34

0.35 0.19 0.3 0.24 0.25 0.36 0.11 0.17 0.36 0.325.07 3.33 4.63 3.31 5.86 6.05 4.06 3.42 4.84 3.7735.7 32.7 35.9 24.8 32.4 42.8 35.5 24.9 27 36.6

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.400.381 0.245 0.309 0.202 0.267 0.363 0.327 0.217 0.226 0.284

22 16.4 23.9 14.3 18.4 21.7 15.6 10.7 11 15.67.01 5.18 6.36 5.14 6.36 8.24 5.11 4.45 5 5.870.7 32.9 64.8 15.9 33.1 38.9 39.7 21.9 31.4 49.519.2 8.79 14.6 14.5 11.5 10.5 11 4.92 7.58 21.6

0.077 2 0.062 <0.050 0.05 0.142 0.06 <0.050 <0.050 0.0611.18 0.62 1.16 0.4 1.11 1.77 1.35 0.87 1.26 1.314.4 9.48 13.6 7.57 11.9 17.7 14 5.96 7.61 10.2

<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.53 <0.50 <0.50 <0.500.29 1.22 0.226 0.335 0.138 0.162 0.175 0.05 0.132 0.164

0.086 0.095 0.068 0.124 0.116 0.147 0.091 0.073 0.072 0.0550.9 0.59 0.83 0.29 0.59 0.57 0.73 0.21 0.39 0.99

0.868 0.583 0.915 0.371 0.866 1.31 0.827 1.36 0.699 0.79465.1 56.1 72.7 53.9 53.8 57.3 26 43.1 41.6 52.969.9 48.1 58.8 33.6 49.6 60.3 58.1 38.2 51 53.7

0.012 0.013 0.016 0.0071 0.011 0.006 0.0085 0.0031 0.0053 0.0220.0089 0.0078 0.014 0.0016 0.0071 0.0043 0.0047 0.0012 0.0038 0.0320.017 0.0044 0.0074 0.0023 0.0076 0.0046 0.0083 0.0013 0.0028 0.020.075 0.022 0.046 0.0076 0.043 0.011 0.022 0.0048 0.014 0.094

0.1 0.04 0.075 0.016 0.047 0.013 0.038 0.011 0.024 0.140.1 0.045 0.11 0.02 0.046 0.016 0.059 0.014 0.03 0.18

0.14 0.049 0.13 0.02 0.1 0.016 0.063 0.015 0.026 0.170.016 0.008 0.017 0.0032 0.0076 0.003 0.01 0.0024 0.0053 0.0290.17 0.1 0.11 0.028 0.057 0.035 0.12 0.021 0.048 0.29

0.016 0.01 0.024 0.0036 0.012 0.005 0.0092 0.0017 0.0067 0.0370.022 0.03 0.02 0.048 0.023 0.012 0.0074 0.0033 0.008 0.033

0.1 0.057 0.079 0.014 0.053 0.025 0.061 0.0084 0.034 0.210.22 0.11 0.16 0.041 0.083 0.052 0.11 0.029 0.068 0.46

1 0.5 0.82 0.21 0.5 0.2 0.53 0.12 0.28 1.7

<0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 <0.02<0.02 <0.02 <0.02 <0.02 <0.02 0.1<0.02 <0.02 <0.02 <0.02 <0.02 0.1

Appendix E-2

Sediment and Pore Water Chemistry Laboratory Results

Table E2: Results of Chemical Analysis of Sediment Samples (August 2016)


Appendix E2

Maxxam ID PL4792 PL4793 PL4794 PL4795 PL4796 PL4803 PL4804 PL4805 PL5047 PL5048 PL5049 PL5050 PL4954 PL5057Sampling Date 2016/08/31 10:00 2016/08/31 10:00 2016/08/31 10:00 2016/08/31 10:00 2016/08/31 10:00 2016/08/31 12:00 2016/08/31 12:00 2016/08/31 12:00 2016/09/01 17:30 2016/09/01 17:30 2016/09/01 17:30 2016/09/01 17:30 2016/08/31 18:15 2016/09/01 17:30COC Number 503355-13-01 503355-13-01 503355-13-01 503355-13-01 503355-13-01 503355-13-01 503355-13-01 503355-13-01 503355-30-01 503355-30-01 503355-30-01 503355-30-01 503355-18-01 503355-29-01

Units

Canadian Council of Ministers for the

Environment (CCME) Interim Sediment Quality

Guidelines (ISQG) for marine aquatic life

(mg/kg dw)

DAS E-05-A-0.2 DAS E-05-A-0.4 DAS E-05-A-0.6 DAS E-05-A-0.8 DAS E-05-A-1.0 DAS E-08-A-0.2 DAS E-08-A-0.4 DAS E-08-A-0.6 DAS-E-01-A-0.2 DAS-E-01-A-0.2 DAS-E-01-A-0.4 DAS-E-01-A-0.6 DAS-E-02-A-0.2 DAS-E-03-A-02 DAS-E-04-A-0.2

Physical PropertiesMoisture % - - 32 - 22 24 35 26 25 32 38 22 32 - 31Physical Properties200 mesh (>.075 mm) % - - - - - - - - - 57.6 83.5 67.4 78.5 57.4200 mesh (<.075 mm) % - - - - - - - - - 42.4 16.5 32.6 21.6 42.6Physical PropertiesSoluble (2:1) pH pH - 8.06 8.06 8.05 8.18 8.21 7.95 8.14 8.22 8.31 8.06 8.35 8.21 8.32 8Total Metals by ICPMSTotal Aluminum (Al) mg/kg 12900 12400 13200 11000 11200 12600 9540 9670 12600 15500 9210 12100 12300 14700Total Antimony (Sb) mg/kg 1.08 1.52 1.63 0.63 0.39 1.2 0.55 0.46 1.03 1.23 0.23 0.64 0.7 1.35Total Arsenic (As) mg/kg 7.24 9.18 9.42 8.15 4.99 4.72 10.2 6.82 7.24 7.33 11.3 2.75 6.17 5.85 8.43Total Barium (Ba) mg/kg 50.6 59.4 69.3 58.8 51.6 52.5 43 49.5 43.3 103 35.6 40.6 48.6 51.2Total Beryllium (Be) mg/kg <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40Total Bismuth (Bi) mg/kg 0.34 0.84 0.45 0.24 0.17 0.29 0.21 0.26 0.19 0.66 0.14 0.31 0.22 0.33Total Cadmium (Cd) mg/kg 0.7 1.09 1.59 2.03 0.759 0.417 1.17 0.716 0.816 0.756 1.18 0.304 0.536 0.737 1.26Total Calcium (Ca) mg/kg 13200 8980 7730 10800 8860 10100 6130 7940 39900 51500 6000 10800 15400 13500Total Chromium (Cr) mg/kg 52.3 25.2 24.3 24.8 15.8 18.5 27.5 19.6 18.8 21.6 29.1 9.7 20.6 18.4 27.4Total Cobalt (Co) mg/kg 8.19 8.08 7.7 6.08 7.05 8.08 6.75 7.2 7.43 9.01 5.21 7.06 6.92 8.84Total Copper (Cu) mg/kg 18.7 433 389 76.6 38.7 25.9 326 55.2 37.7 280 94.7 25.5 212 147 193Total Iron (Fe) mg/kg 23000 23100 21600 18600 18900 22500 17800 18000 23300 28100 15400 20300 19700 24300Total Lead (Pb) mg/kg 30.2 46.5 84.7 85.6 43 15.1 37.6 27.4 31.5 45.6 135 13.1 38.3 33.5 52.1Total Lithium (Li) mg/kg 14.9 16.1 14.8 12.1 12.6 15.4 12.4 13.7 16.6 19.4 12.9 13.2 12.4 16.2Total Magnesium (Mg) mg/kg 7480 7160 6880 5420 5630 7450 5210 5420 7850 9080 4500 6560 6660 8340Total Manganese (Mn) mg/kg 247 281 264 224 222 248 184 188 236 278 183 220 262 267Total Mercury (Hg) mg/kg 0.13 0.179 0.927 0.461 0.208 0.176 0.19 0.175 0.247 0.103 0.566 0.063 0.121 0.117 0.215Total Molybdenum (Mo) mg/kg 3.2 3.06 2.16 1.86 1.56 2.66 1.71 1.4 2.46 3.15 1.63 1.92 1.82 2.45Total Nickel (Ni) mg/kg 24.2 24.4 19.8 13.3 14.5 23.2 14.9 15.6 20.2 27.3 7.67 20.5 18.7 25.8Total Phosphorus (P) mg/kg 567 547 568 396 410 601 372 415 557 616 319 518 487 598Total Potassium (K) mg/kg 1850 1870 1840 1420 1600 1880 1520 1590 1740 2480 1180 1570 1530 2000Total Selenium (Se) mg/kg 0.61 0.59 <0.50 <0.50 <0.50 0.68 <0.50 <0.50 <0.50 0.58 <0.50 <0.50 <0.50 0.6Total Silver (Ag) mg/kg 0.655 0.99 0.844 0.334 0.178 0.579 0.241 0.262 0.355 0.825 0.083 0.436 0.425 0.704Total Sodium (Na) mg/kg 5760 5280 5410 3880 3640 6270 3510 3730 5360 7520 2650 4290 4240 6280Total Strontium (Sr) mg/kg 64 54.5 58.3 69.8 59.9 57.3 44.5 51 143 221 36.6 52.6 75.1 65.7Total Thallium (Tl) mg/kg 0.167 0.155 0.157 0.093 0.117 0.186 0.184 0.175 0.113 0.128 0.054 0.12 0.115 0.157Total Tin (Sn) mg/kg 2.47 5.19 6.96 6.71 1.92 3.08 3.86 2.73 17.9 34.7 2.34 1.84 2.12 2.64Total Titanium (Ti) mg/kg 672 635 729 554 680 750 608 579 685 798 570 466 540 695Total Uranium (U) mg/kg 1.52 1.05 0.928 0.745 0.824 1.36 1.42 0.795 1.15 1.33 0.673 1.17 1.14 1.31Total Vanadium (V) mg/kg 49.7 48.4 51.7 44 59.3 51.2 44.5 46 52.9 57 39.8 44.9 46.6 52.9Total Zinc (Zn) mg/kg 124 209 228 304 122 61.8 172 102 111 109 182 47.1 105 117 200Total Zirconium (Zr) mg/kg 3.72 3.37 2.19 2.9 4.4 4.78 3.17 3.2 3.29 4.87 1.76 1.07 2.04 3.27Polycyclic AromaticsNaphthalene mg/kg 0.0346 0.037 0.11 (1) 0.066 (1) 0.068 (1) 0.14 0.063 0.11 (1) 0.14 (1) 0.010 (1) 0.085 (1) 0.019 0.014 (1) 0.017 (1) 0.027 (3)2-Methylnaphthalene mg/kg 0.0202 0.025 0.061 (1) 0.066 (1) 0.039 (1) 0.028 0.039 0.050 (1) 0.072 (1) 0.011 (1) 0.070 (1) 0.0099 0.010 (1) 0.013 (1) 0.021 (3)Acenaphthylene mg/kg 0.00587 0.02 0.040 (1) 0.043 (1) 0.032 (1) 0.035 0.032 0.054 (1) 0.056 (1) 0.0088 (1) 0.050 (1) 0.0081 0.012 (1) 0.0066 (1) 0.018Acenaphthene mg/kg 0.00671 0.024 0.048 (1) 0.043 (1) 0.021 (1) 0.034 0.029 0.037 (1) 0.067 (1) 0.018 (1) 0.030 (1) 0.0033 0.0075 (1) 0.0098 (1) 0.010 (3)Fluorene mg/kg 0.0212 0.038 0.089 (1) 0.075 (1) 0.034 (1) 0.031 0.054 0.058 (1) 0.10 (1) 0.027 (1) 0.043 (1) 0.0064 0.013 (1) 0.015 (1) 0.018 (3)Phenanthrene mg/kg 0.0867 0.2 0.32 (1) 0.31 (1) 0.16 (1) 0.11 0.22 0.35 (1) 0.54 (1) 0.16 (1) 0.24 (1) 0.024 0.067 (1) 0.081 (1) 0.083 (3)Anthracene mg/kg 0.0469 0.11 0.16 (1) 0.21 (1) 0.081 (1) 0.06 0.13 0.12 (1) 0.13 (1) 0.051 (1) 0.095 (1) 0.017 0.030 (1) 0.027 (1) 0.063 (3)Fluoranthene mg/kg 0.113 0.33 0.49 (1) 0.68 (1) 0.37 (1) 0.2 0.38 0.62 (1) 0.71 (1) 0.21 (1) 0.42 (1) 0.048 0.11 (1) 0.13 (1) 0.19 (3)Pyrene mg/kg 0.153 0.42 1.2 (1) 0.84 (1) 0.66 (1) 0.21 0.55 0.70 (1) 0.80 (1) 0.24 (1) 0.89 (1) 0.089 0.16 (1) 0.15 (1) 0.29 (3)Benzo(a)anthracene mg/kg 0.0748 0.18 0.31 (1) 0.23 (1) 0.16 (1) 0.059 0.27 0.20 (1) 0.20 (1) 0.094 (1) 0.16 (1) 0.015 0.051 (1) 0.055 (1) 0.090 (3)Chrysene mg/kg 0.108 0.2 0.38 (1) 0.31 (1) 0.21 (1) 0.071 0.3 0.26 (1) 0.28 (1) 0.13 (1) 0.23 (1) 0.019 0.063 (1) 0.065 (1) 0.11 (3)Benzo(b&j)fluoranthene mg/kg 0.31 0.64 (1) 0.34 (1) 0.30 (1) 0.09 0.39 0.32 (1) 0.32 (1) 0.15 (1) 0.46 (1) 0.033 0.11 (1) 0.11 (1) 0.19 (3)Benzo(k)fluoranthene mg/kg 0.11 0.21 (1) 0.12 (1) 0.11 (1) 0.029 0.13 0.11 (1) 0.11 (1) 0.053 (1) 0.15 (1) 0.012 0.043 (1) 0.037 (1) 0.069 (3)Benzo(a)pyrene mg/kg 0.0888 0.19 0.35 (1) 0.21 (1) 0.21 (1) 0.06 0.22 0.20 (1) 0.20 (1) 0.097 (1) 0.29 (1) 0.021 0.069 (1) 0.068 (1) 0.12 (3)Indeno(1,2,3-cd)pyrene mg/kg 0.099 0.14 (1) 0.11 (1) 0.098 (1) 0.033 0.098 0.094 (1) 0.10 (1) 0.054 (1) 0.17 (1) 0.013 0.040 (1) 0.034 (1) 0.060 (3)Dibenz(a,h)anthracene mg/kg 0.0622 0.031 0.041 (1) 0.034 (1) 0.028 (1) 0.0086 0.032 0.029 (1) 0.027 (1) 0.016 (1) 0.047 (1) 0.0033 0.011 (1) 0.0095 (1) 0.018 (3)Benzo(g,h,i)perylene mg/kg 0.13 0.16 (1) 0.15 (1) 0.12 (1) 0.046 0.11 0.11 (1) 0.12 (1) 0.070 (1) 0.23 (1) 0.018 0.050 (1) 0.042 (1) 0.073 (3)Low Molecular Weight PAH`s mg/kg 0.45 0.82 0.82 0.44 0.44 0.57 0.78 1.1 0.28 0.61 0.088 0.15 0.17 0.24High Molecular Weight PAH`s mg/kg 1.3 2.8 2.3 1.6 0.61 1.7 2 2.2 0.79 2 0.2 0.46 0.48 0.82Total PAH mg/kg 1.8 3.6 3.1 2.1 1 2.3 2.8 3.3 1.1 2.7 0.28 0.62 0.65 1.1Index of Additive Cancer Risk(IAR N/A 3.9 7.7 4.6 3.9 1.2 5 4.2 4.2 2 5.5 0.42 1.4 1.4 2.4PCB'sAroclor 1016 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1221 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1232 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1242 ug/g <0.020 <0.020 0.012 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1248 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1254 ug/g 0.0633 <0.020 0.044 0.025 <0.010 <0.010 <0.010 <0.020 0.046 <0.020 <0.010 0.012 <0.020Aroclor 1260 ug/g <0.020 0.026 0.015 <0.010 <0.010 <0.010 <0.020 0.014 <0.020 <0.010 0.018 <0.020Aroclor 1262 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Aroclor 1268 ug/g <0.020 <0.020 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.010 <0.010 <0.020Total PCB ug/g 0.0215 <0.020 0.070 0.053 <0.010 <0.010 <0.010 <0.020 0.060 <0.020 <0.010 0.031 <0.020

Notes:RDL = Reportable Detection LimitN/A = Not ApplicableLab-Dup = Laboratory Initiated Duplicate

(1) Detection limits raised due to dilution as a result of sample matrix interference.(2) Detection limits raised due to dilution to bring analyte within the calibrated range.(3) Duplicate exceeds acceptance criteria due to sample matrix.(4) Detection limits raised due to dilution as a result of sample matrix interference. Duplicate exceeds acceptance criteria due to sample non homogeneity. (5) Detection limits raised due to high moisture content, sample contains => 50% moisture.(6) Qualifying ion outside of acceptance criteria. Results are tentatively identified and potentially biased high.(7) Duplicate exceeds acceptance criteria due to sample non homogeneity. (8) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.(9) Duplicate exceeds acceptance criteria for Hg. 10% of analytes failure in multielement scan is allowed.

E2‐1



Appendix E2

Maxxam IDSampling DateCOC Number

Units




(mg/kg dw)Physical PropertiesMoisture % -Physical Properties200 mesh (>.075 mm) % -200 mesh (<.075 mm) % -Physical PropertiesSoluble (2:1) pH pH -Total Metals by ICPMSTotal Aluminum (Al) mg/kgTotal Antimony (Sb) mg/kgTotal Arsenic (As) mg/kg 7.24Total Barium (Ba) mg/kgTotal Beryllium (Be) mg/kgTotal Bismuth (Bi) mg/kgTotal Cadmium (Cd) mg/kg 0.7Total Calcium (Ca) mg/kgTotal Chromium (Cr) mg/kg 52.3Total Cobalt (Co) mg/kgTotal Copper (Cu) mg/kg 18.7Total Iron (Fe) mg/kgTotal Lead (Pb) mg/kg 30.2Total Lithium (Li) mg/kgTotal Magnesium (Mg) mg/kgTotal Manganese (Mn) mg/kgTotal Mercury (Hg) mg/kg 0.13Total Molybdenum (Mo) mg/kgTotal Nickel (Ni) mg/kgTotal Phosphorus (P) mg/kgTotal Potassium (K) mg/kgTotal Selenium (Se) mg/kgTotal Silver (Ag) mg/kgTotal Sodium (Na) mg/kgTotal Strontium (Sr) mg/kgTotal Thallium (Tl) mg/kgTotal Tin (Sn) mg/kgTotal Titanium (Ti) mg/kgTotal Uranium (U) mg/kgTotal Vanadium (V) mg/kgTotal Zinc (Zn) mg/kg 124Total Zirconium (Zr) mg/kgPolycyclic AromaticsNaphthalene mg/kg 0.03462-Methylnaphthalene mg/kg 0.0202Acenaphthylene mg/kg 0.00587Acenaphthene mg/kg 0.00671Fluorene mg/kg 0.0212Phenanthrene mg/kg 0.0867Anthracene mg/kg 0.0469Fluoranthene mg/kg 0.113Pyrene mg/kg 0.153Benzo(a)anthracene mg/kg 0.0748Chrysene mg/kg 0.108Benzo(b&j)fluoranthene mg/kgBenzo(k)fluoranthene mg/kgBenzo(a)pyrene mg/kg 0.0888Indeno(1,2,3-cd)pyrene mg/kgDibenz(a,h)anthracene mg/kg 0.0622Benzo(g,h,i)perylene mg/kgLow Molecular Weight PAH`s mg/kgHigh Molecular Weight PAH`s mg/kgTotal PAH mg/kgIndex of Additive Cancer Risk(IAR N/APCB'sAroclor 1016 ug/gAroclor 1221 ug/gAroclor 1232 ug/gAroclor 1242 ug/gAroclor 1248 ug/gAroclor 1254 ug/g 0.0633Aroclor 1260 ug/gAroclor 1262 ug/gAroclor 1268 ug/gTotal PCB ug/g 0.0215


(1) Detection limits raised due to dilution as a result of sample matrix interference.(2) Detection limits raised due to dilution to bring analyte within the calibrated range.(3) Duplicate exceeds acceptance criteria due to sample matrix.(4) Detection limits raised due to dilution as a result of sample matrix interference. Duplicat(5) Detection limits raised due to high moisture content, sample contains => 50% moisture.(6) Qualifying ion outside of acceptance criteria. Results are tentatively identified and poten(7) Duplicate exceeds acceptance criteria due to sample non homogeneity. (8) Recovery or RPD for this parameter is outside control limits. The overall quality control (9) Duplicate exceeds acceptance criteria for Hg. 10% of analytes failure in multielement sc

PL4791 PL4790 PL4760 PL4757 PL4758 PL4759 PL4761 PL4737 PL4738 PL4763 PL4764 PL4779 PL4787 PL4786 PL4770 PL4785 PL4816 PL4814 PL4807 PL4818 PL48202016/08/31 10:00 2016/08/31 10:00 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:15 2016/08/30 16:45 2016/08/30 16:45 2016/08/30 16:45 2016/08/30 16:45 2016/08/30 16:45 2016/08/30 16:45 2016/08/30 16:45 2016/08/31 12:00 2016/08/31 12:00 2016/08/31 12:00 2016/08/31 13:00 2016/08/31 13:00

503355-12-01 503355-12-01 503355-10-01 503355-10-01 503355-10-01 503355-10-01 503355-10-01 503355-09-01 503355-10-01 503355-10-01 503355-10-01 503355-11-01 503355-11-01 503355-11-01 503355-11-01 503355-11-01 503355-14-01 503355-14-01 503355-14-01 503355-14-01 503355-14-01

DAS-E-05-B DAS-E-05-C DAS-E-06-A-0.2 DAS-E-06-A-0.4 DAS-E-06-A-0.6 DAS-E-06-A-0.8 DAS-E-06-A-1.0 DAS-E-06-B DAS-E-06-C DAS-E-07-A-0.2 DAS-E-07-A-0.4 DAS-E-07-A-0.6 DAS-E-07-A-0.8 DAS-E-07-A-1.0 DAS-E-07-B DAS-E-07-C DAS-E-08-A-0.8 DAS-E-08-A-10 DAS-E-08-B DAS-E-09-A-0.2 DAS-E-09-A-0.4

24 25 29 29 - 24 - 24 - 28 - 22 - 22 23 - 19 - 18 - -

52.7 52.7 - - - - - 54.4 58 - - 66.1 69.5 - - 78.9 - -47.3 47.3 - - - - - 45.6 42 - - 33.9 30.5 - - 21.1 - -

8.43 8.46 8.14 8.06 8 8.22 8.6 8.62 8.6 8.14 8.18 8.38 8.52 8.46 8.47 8.52 8.47 8.5 8.72 8.12 7.88

10600 10300 11100 10800 13100 9940 8780 10400 9560 9460 10000 9570 7560 7870 8600 8300 8290 8930 7590 12800 147000.16 0.16 1.73 2.45 1.65 0.64 0.25 0.17 0.13 2.2 0.53 0.23 0.14 0.16 0.14 0.12 0.21 0.32 0.15 3.86 1.773.33 3.99 12.4 9.95 11.1 7.18 5.31 4.08 3.35 7.3 6.05 5.77 4.82 5.08 3.76 3.2 5.24 6.09 3.94 9.09 7.4432.6 31.6 50.7 60.5 74.8 57.3 31.1 30.4 30.9 45.7 44.6 31.1 23.8 25.6 25.6 24.4 26.3 29.8 21.5 49.9 49.1

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40<0.10 <0.10 0.66 0.4 0.51 0.29 0.12 <0.10 <0.10 0.24 0.19 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.1 <0.10 0.26 0.130.342 0.332 1.37 2.05 2.2 1.17 0.473 0.348 0.297 1.36 0.927 0.313 0.262 0.277 0.293 0.279 0.346 0.379 0.274 0.793 0.57511600 8760 9870 6980 5990 5740 9770 11100 11400 10000 6540 4940 7210 14300 12400 9070 11500 13500 16100 11800 5980

19 18.5 20.7 20.4 24.3 17 17.1 18.6 16.7 17.5 16.8 19.2 16.4 16.5 16.6 14.8 17.1 16.6 15.2 23.6 24.66.64 6.82 7.38 6.99 7.91 6.58 6.36 7 6.17 6.26 6.26 7.51 6.21 6.44 6.3 5.68 6.9 6.98 5.45 8.23 9.5216.9 18.5 98.9 76.6 70.2 52.8 20.7 16.6 16.9 89.9 42.3 17.2 14.9 12.9 14 13.4 14.8 18.3 10.9 278 54.5

19500 18000 19200 18600 21300 17000 16300 18700 16600 16800 17000 17100 15100 15600 16200 14600 16900 17000 14900 22600 236003.64 4.45 51.6 69.7 82.2 40.9 12.1 3.94 3.11 41.5 31 5.7 4.09 3.7 3.49 3.07 6.38 25.2 3.28 28.1 16.812.1 13.9 11.9 14.1 16.8 13 11.7 12.6 10.7 13 14.6 13.7 10.7 11.2 11.1 9.6 11.8 11.4 8.9 14.1 18.35470 5090 5670 5540 6540 5060 4440 5110 4600 5120 5130 4900 3920 4130 4350 4070 4830 4920 4210 7340 7890209 197 220 213 248 198 171 192 190 201 203 179 148 158 171 172 167 174 155 243 273

<0.050 <0.050 0.244 0.325 0.519 0.246 0.13 <0.050 <0.050 0.176 0.183 <0.050 <0.050 <0.050 <0.050 <0.050 0.054 0.078 <0.050 0.479 0.1310.89 1.02 2.58 2.04 2.79 1.98 1.27 1.02 0.84 2 2.28 1.43 0.92 0.86 0.83 0.89 1.04 1.48 0.7 2.25 2.3412.5 14.9 18.3 19 22.6 15.7 13.7 14.4 12.5 16 14.1 16.5 11.9 12.9 13.1 11.1 12.6 12.9 10.8 20.1 19.8439 412 450 476 610 410 362 414 452 456 420 378 309 325 441 363 335 355 326 524 520

1670 1540 1450 1510 1900 1420 1280 1550 1400 1310 1360 1460 1190 1260 1330 1230 1470 1470 1180 1800 2190<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.5 <0.500.067 0.077 0.544 0.833 1.05 0.351 0.113 0.077 0.077 0.592 0.268 0.077 0.074 0.066 0.082 0.057 0.084 0.151 0.065 0.361 0.1493900 3430 4290 4350 5160 3720 2990 3570 2890 3770 3750 3130 2680 2910 3350 2870 3040 3810 2420 4790 518060.9 51.2 73.3 53.6 56.2 45.2 57.7 62.8 75 56.2 47.3 35.5 40.3 78.7 68.6 57.5 62.4 63.2 87.9 65.3 46.9

0.133 0.123 0.158 0.145 0.192 0.128 0.146 0.14 0.121 0.141 0.122 0.175 0.184 0.159 0.148 0.173 0.171 0.184 0.185 0.135 0.1340.2 0.29 3.69 5.12 7.24 5.03 1.16 0.23 0.19 2.98 2.7 0.34 0.19 0.16 0.18 0.17 0.39 0.95 0.16 2.29 1.56736 658 627 632 775 618 530 683 663 528 646 613 483 512 544 561 552 570 528 709 848

0.943 0.969 1.02 0.904 1.12 0.869 0.839 0.878 1.14 0.988 0.922 1.04 0.705 0.85 0.895 0.788 0.896 0.949 0.869 1.35 1.355.1 53.7 46.3 51.4 66.2 56 47.5 52.2 50.2 43.2 49.4 47.7 44 44.6 46 40.8 40.9 43.2 40.2 49.9 57.235 40.6 224 322 284 157 67 39 35.4 230 136 45.2 35.7 34.9 34.3 30.8 39.7 49.6 28 144 82.7

3.11 3.53 3.47 3.89 5.28 3.42 2.6 3.51 2.7 3.07 3.32 3.15 2.29 2.78 2.75 2.53 2.82 2.85 2.32 4.47 4.65

<0.0010 0.012 0.74 (1) 0.37 (1) 0.25 (1) 0.13 (1) 0.034 <0.0010 <0.0010 0.049 (1) 0.090 (1) 0.026 (1) 0.0051 <0.0010 <0.0010 <0.0010 0.0065 0.042 <0.0010 0.054 (1) 0.18<0.0010 0.0044 0.16 (1) 0.14 (1) 0.10 (1) 0.077 (1) 0.016 <0.0010 <0.0010 0.037 (1) 0.046 (1) 0.011 (1) 0.0021 <0.0010 <0.0010 <0.0010 0.0038 0.015 <0.0010 0.029 (1) 0.026<0.00050 0.0023 0.031 (1) 0.088 (1) 0.081 (1) 0.052 (1) 0.02 <0.00050 <0.00050 0.039 (1) 0.048 (1) 0.025 (1) 0.0017 <0.00050 <0.00050 <0.00050 0.0038 0.015 <0.00050 0.023 (1) 0.046<0.00050 0.0016 0.16 (1) 0.13 (1) 0.077 (1) 0.050 (1) 0.0082 <0.00050 <0.00050 0.034 (1) 0.035 (1) 0.011 (1) 0.00099 <0.00050 <0.00050 <0.00050 0.0017 0.0094 <0.00050 0.026 (1) 0.044<0.0010 0.0031 0.16 (1) 0.17 (1) 0.11 (1) 0.068 (1) 0.017 <0.0010 <0.0010 0.059 (1) 0.048 (1) 0.029 (1) 0.0017 <0.0010 <0.0010 <0.0010 0.0046 0.014 <0.0010 0.037 (1) 0.039<0.0010 0.0097 0.36 (1) 0.71 (1) 0.52 (1) 0.33 (1) 0.08 <0.0010 0.0012 0.33 (1) 0.27 (1) 0.17 (1) 0.0099 <0.0010 <0.0010 <0.0010 0.016 0.07 <0.0010 0.16 (1) 0.120.0018 0.0064 0.19 (1) 0.22 (1) 0.22 (1) 0.11 (1) 0.038 0.0022 0.0014 0.11 (1) 0.095 (1) 0.042 (1) 0.0057 0.0018 0.0019 0.0018 0.014 0.031 0.0013 0.087 (1) 0.071

<0.0010 0.014 0.59 (1) 0.88 (1) 1.0 (1) 0.51 (1) 0.14 0.0012 0.0029 0.52 (1) 0.40 (1) 0.22 (1) 0.013 <0.0010 <0.0010 <0.0010 0.026 0.13 <0.0010 0.36 (1) 0.21<0.0010 0.011 0.74 (1) 1.0 (1) 1.3 (1) 0.63 (1) 0.17 0.0017 0.0043 0.61 (1) 0.47 (1) 0.22 (1) 0.015 <0.0010 <0.0010 <0.0010 0.034 0.15 <0.0010 0.53 (1) 0.21<0.0010 0.0037 0.21 (1) 0.30 (1) 0.39 (1) 0.18 (1) 0.059 <0.0010 0.0013 0.18 (1) 0.13 (1) 0.067 (1) 0.004 <0.0010 <0.0010 <0.0010 0.016 0.036 <0.0010 0.14 (1) 0.066<0.0010 0.0044 0.27 (1) 0.39 (1) 0.50 (1) 0.24 (1) 0.077 0.0011 0.0017 0.23 (1) 0.19 (1) 0.078 (1) 0.005 <0.0010 <0.0010 <0.0010 0.028 0.049 <0.0010 0.20 (1) 0.075<0.0010 0.0054 0.32 (1) 0.43 (1) 0.58 (1) 0.29 (1) 0.081 <0.0010 <0.0010 0.27 (1) 0.23 (1) 0.085 (1) 0.0063 <0.0010 <0.0010 <0.0010 0.024 0.061 <0.0010 0.30 (1) 0.088<0.0010 0.0021 0.12 (1) 0.16 (1) 0.19 (1) 0.10 (1) 0.028 <0.0010 <0.0010 0.096 (1) 0.079 (1) 0.031 (1) 0.0022 <0.0010 <0.0010 <0.0010 0.011 0.023 <0.0010 0.093 (1) 0.035<0.0010 0.0037 0.20 (1) 0.29 (1) 0.38 (1) 0.19 (1) 0.061 <0.0010 <0.0010 0.18 (1) 0.15 (1) 0.066 (1) 0.0041 <0.0010 <0.0010 <0.0010 0.017 0.039 <0.0010 0.16 (1) 0.062<0.0020 0.0023 0.11 (1) 0.15 (1) 0.17 (1) 0.095 (1) 0.026 <0.0020 <0.0020 0.10 (1) 0.087 (1) 0.034 (1) 0.0021 <0.0020 <0.0020 <0.0020 0.0089 0.02 <0.0020 0.067 (1) 0.03<0.00050 0.00066 0.031 (1) 0.043 (1) 0.050 (1) 0.026 (1) 0.0075 <0.00050 <0.00050 0.029 (1) 0.025 (1) 0.0090 (1) 0.00062 <0.00050 <0.00050 <0.00050 0.0031 0.0056 <0.00050 0.020 (1) 0.0081<0.0020 0.0033 0.14 (1) 0.19 (1) 0.22 (1) 0.12 (1) 0.032 <0.0020 <0.0020 0.13 (1) 0.11 (1) 0.046 (1) 0.003 <0.0020 <0.0020 <0.0020 0.011 0.026 <0.0020 0.077 (1) 0.0360.0018 0.04 1.8 1.8 1.4 0.82 0.21 0.0022 0.0026 0.65 0.63 0.32 0.027 0.0018 0.0019 0.0018 0.05 0.2 0.0013 0.42 0.53

<0.0010 0.037 2 2.9 3.6 1.8 0.52 0.004 0.01 1.7 1.4 0.66 0.042 <0.0010 <0.0010 <0.0010 0.13 0.41 <0.0010 1.4 0.630.0018 0.077 3.8 4.7 4.9 2.6 0.73 0.0062 0.013 2.4 2 0.98 0.069 0.0018 0.0019 0.0018 0.18 0.6 0.0013 1.8 1.2<0.10 <0.10 4.2 5.9 7.6 3.8 1.1 <0.10 <0.10 3.6 3 1.2 <0.10 <0.10 <0.10 <0.10 0.35 0.8 <0.10 3.6 1.2

<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 0.019 0.034 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 0.014 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 0.051 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020<0.010 0.034 0.034 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 0.051 <0.020

E2‐2



Appendix E2


Units







PL4825 PL4817 PL4819 PL4843 PL5072 PL5073 PL4721 PL4920 PL4921 PL4719 PL4720 PL4722 PL4723 PL4927 PL4724 PL4887 PL49192016/08/31 13:00 2016/08/31 13:00 2016/08/31 13:00 2016/08/31 13:00 2016/09/01 17:00 2016/09/01 17:00 2016/08/30 12:45 2016/08/30 2016/08/30 2016/08/30 12:30 2016/08/30 12:30 2016/08/30 12:30 2016/08/30 12:30 2016/08/30 2016/08/30 13:15 2016/08/31 15:45 2016/08/30

503355-15-01 503355-14-01 503355-14-01 503355-15-01 503355-28-01 503355-28-01 503355-08-01 503355-36-01 503355-36-01 503355-08-01 503355-08-01 503355-08-01 503355-08-01 503355-36-01 503355-08-01 503355-16-01 503355-36-01

DAS-E-09-A-0.6 DAS-E-09-A-0.8 AS-E-09-A-0.8 Lab-D DAS-E-09-A-1.0 DAS-E-09-B DAS-E-10-G DAS-E-11-G DAS-SB-01-A-0.2 DAS-SB-01-G-ALL DAS-SB-02-G-ALL DAS-SB-03-A-0.2 DAS-SB-03-A-0.4 DAS-SB-03-A-0.6 DAS-SB-03-A-0.8 DAS-SB-03-G-ALL DAS-SB-04 DAS-SB-04-A-0.2 DAS-SB-05-G-ALL DAS-SB-06 GRAB 1DAS-SB-06 GRAB 2 DAS-SB-06-G-ALL

24 21 - 20 - 45 52 - 15 - - 42 48 43 26 - - 32 - - -

- - - - 80 37.2 19.9 - - 54.3 48.4 - 91.7 85.7 88.5 92.9 59.9 -- - - - 20 62.8 80.1 - - 45.7 51.6 - 8.33 14.3 11.5 7.15 40.1 -

8.18 8.41 - 8.46 8.53 7.94 7.8 8.3 8.6 8.25 8.33 8.21 8.17 7.96 8.45 - 8.54 8.26 - - 8.49

10800 9370 8500 8310 15000 18000 9510 10200 14700 12200 12500 14100 15800 9930 12500 10300 - - 121000.7 0.19 0.18 0.16 0.71 0.71 0.37 0.44 0.75 1.58 1.81 0.66 0.76 1.07 0.3 0.28 0.896.11 5.51 5.39 5.05 8.9 9.11 2.48 3.74 6.48 6.57 5.76 5.35 4.85 4.54 2.47 4.57 5.2232.1 27.4 23.3 21.8 53.9 59.3 45.8 46.9 56.6 81.9 112 101 80.3 52.1 46.6 38 50.8

<0.40 <0.40 <0.40 <0.40 <0.40 0.4 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40<0.10 <0.10 <0.10 <0.10 0.27 0.3 <0.10 <0.10 0.24 0.97 0.82 0.84 0.54 0.28 <0.10 0.1 0.150.38 0.307 0.28 0.232 1.09 0.979 0.11 0.257 0.58 1.41 1.58 1.72 1.47 1.04 0.362 0.283 0.5066280 7550 11500 8730 13600 14300 7690 11300 22600 129000 114000 75200 78000 56700 11400 9650 2750021.1 17.7 16.1 18 29.3 36 12.1 17.1 28.9 23.3 25.8 27 28.1 19.2 15.6 20.5 25.17.96 7.48 6.93 7.08 9.23 10.8 4.9 5.55 8.36 8.37 27.9 9.2 9.36 5.9 5.52 6.93 6.920.7 14.4 12.8 12.6 265 129 18.9 43.8 106 71.3 75.9 74.6 54.2 101 30.9 36.3 67.1

19500 17800 16900 16400 25600 29700 13500 19100 25300 27800 26700 22400 25300 19800 18000 20700 237006.18 4.05 3.78 3.82 27.6 25.5 4.01 10.5 32.5 138 255 129 63.2 1050 22.2 9.21 19.314.2 13.5 11.8 11.2 18 20.8 14.3 14.6 18.5 15.9 15.3 17.1 18.5 13.1 12.2 13.1 15.65970 5360 5040 5090 9180 11000 4140 5240 8100 8190 8070 8110 8540 6040 3710 5930 6580207 191 176 174 270 317 168 196 270 239 244 251 293 204 175 206 236

<0.050 <0.050 <0.050 <0.050 0.142 0.147 <0.050 0.052 0.175 0.826 1.02 1.23 0.772 0.562 0.055 <0.050 0.1351.2 0.8 0.61 0.68 2.14 2.41 0.97 0.91 1.8 4.39 4.54 2.85 3.04 1.74 0.8 0.57 0.7716 13.9 12.8 13.1 28.2 34.6 6.61 9.79 21.3 28.1 30.7 45.9 31.7 13.5 8.57 13.9 15.3396 376 330 339 737 845 344 483 668 519 688 607 584 495 334 568 579

1730 1620 1470 1470 2310 2750 949 1340 2040 2280 2280 2540 2690 1490 965 1470 1610<0.50 <0.50 <0.50 <0.50 0.61 0.77 <0.50 <0.50 <0.50 0.73 0.72 0.59 0.61 <0.50 <0.50 <0.50 <0.500.071 0.08 0.061 <0.050 0.522 0.43 0.053 0.085 0.453 1.35 1.31 1.08 0.955 0.594 0.101 0.139 0.2533400 2970 3030 2940 8460 9880 1980 3070 5600 10900 9130 11100 10500 6070 2010 3730 433037.5 44.7 66.8 49.9 72.3 76.9 52.5 64.4 143 748 813 502 354 353 90.4 61.9 201

0.166 0.171 0.174 0.176 0.172 0.158 <0.050 0.082 0.128 0.129 0.126 0.173 0.198 0.091 0.074 0.145 0.1160.36 0.21 0.14 0.17 1.82 1.93 0.31 0.65 3.29 10.5 18.5 10.3 6.16 6.06 0.98 0.6 1.45683 635 530 537 807 936 459 612 776 631 611 626 795 538 378 600 732

0.941 0.827 0.725 0.765 1.29 1.35 0.601 0.632 1.11 1.54 1.57 1.34 1.41 0.927 0.809 0.608 0.74750.2 44.7 40.7 39.5 55.1 60.8 42.1 57.5 63.4 45 46.2 51.2 54.9 48.5 56.9 55.2 62.350.7 40.2 36.1 35.7 144 133 34 60.8 106 172 201 239 124 133 51.6 53.2 823.48 2.85 2.33 2.35 5.1 6.18 0.64 1.45 1.87 5.3 5.8 5.18 5.94 2.69 1.78 1.93 2.8

0.0023 <0.0010 <0.0010 <0.0010 0.042 (1) 0.017 (5) 0.011 0.037 0.16 (1) 0.24 (1) 0.98 (1) 0.80 (1) 0.41 (1) 0.093 0.027 0.015 (1) 0.0310.0015 <0.0010 <0.0010 <0.0010 0.034 (1) 0.021 (5) 0.0043 0.01 0.047 (1) 0.096 (1) 0.28 (1) 0.29 (1) 0.22 (1) 0.039 0.0081 0.013 (1) 0.0120.0012 <0.00050 <0.00050 <0.00050 0.018 (1) 0.013 (5) 0.0043 0.049 0.20 (1) 0.37 (1) 0.63 (1) 0.43 (1) 0.86 (1) 0.089 0.031 0.0070 (1) 0.02

<0.00050 <0.00050 <0.00050 <0.00050 0.021 (1) 0.0098 (5) 0.0061 0.022 0.080 (1) 0.25 (1) 0.80 (1) 0.70 (1) 0.66 (1) 0.12 0.0094 0.0067 (1) 0.02<0.0010 <0.0010 <0.0010 <0.0010 0.040 (1) 0.015 (5) 0.0059 0.033 0.17 (1) 0.54 (1) 0.77 (1) 0.85 (1) 1.3 (1) 0.078 0.015 0.0092 (1) 0.0240.0033 <0.0010 <0.0010 <0.0010 0.21 (1) 0.068 (5) 0.025 0.098 0.80 (1) 2.9 (1) 2.6 (2) 2.8 (1) 5.3 (1) 0.2 0.043 0.053 (1) 0.110.0033 0.0011 <0.0010 0.0015 0.086 (1) 0.051 (5) 0.021 0.19 0.75 (1) 2.4 (1) 2.5 (2) 2.9 (1) 6.7 (1) 0.26 0.085 0.019 (1) 0.10.0073 <0.0010 <0.0010 <0.0010 0.41 (1) 0.18 (5) 0.04 0.43 0.80 (1) 3.9 (1) 15 (2) 29 (2) 45 (2) 0.3 0.078 0.10 (1) 0.240.0091 0.0011 0.0013 <0.0010 0.46 (1) 0.20 (5) 0.16 0.82 5.6 (1) 25 (2) 40 (2) 45 (2) 50 (2) 2.3 0.47 0.11 (1) 0.320.0032 <0.0010 <0.0010 <0.0010 0.21 (1) 0.078 (5) 0.019 0.41 1.8 (1) 6.2 (1) 4.3 (1) 9.2 (1) 15 (1) 0.21 0.12 0.042 (1) 0.150.0037 <0.0010 <0.0010 <0.0010 0.29 (1) 0.10 (5) 0.03 0.63 2.4 (1) 7.8 (1) 7.7 (1) 9.0 (1) 23 (2) 0.38 0.23 0.052 (1) 0.180.0065 <0.0010 <0.0010 <0.0010 0.32 (1) 0.14 (5) 0.055 0.64 3.4 (1) 8.2 (1) 9.7 (1) 9.2 (1) 14 (1) 0.96 0.3 0.043 (1) 0.250.0023 <0.0010 <0.0010 <0.0010 0.12 (1) 0.050 (5) 0.02 0.27 1.2 (1) 3.1 (1) 3.4 (1) 3.4 (1) 5.3 (1) 0.34 0.12 0.024 (1) 0.0990.0041 <0.0010 <0.0010 <0.0010 0.20 (1) 0.088 (5) 0.036 0.45 2.3 (1) 5.5 (1) 5.9 (1) 6.1 (1) 9.7 (1) 0.64 0.2 0.053 (1) 0.180.0025 <0.0020 <0.0020 <0.0020 0.091 (1) 0.050 (5) 0.014 0.17 0.90 (1) 2.2 (1) 2.1 (1) 2.5 (1) 3.8 (1) 0.28 0.071 0.026 (1) 0.082

0.00066 <0.00050 <0.00050 <0.00050 0.027 (1) 0.015 (5) 0.0041 0.055 0.30 (1) 0.74 (1) 0.68 (1) 0.85 (1) 1.3 (1) 0.084 0.023 0.0069 (1) 0.0250.0037 <0.0020 <0.0020 <0.0020 0.11 (1) 0.064 (5) 0.017 0.16 0.95 (1) 2.4 (1) 2.1 (1) 2.8 (1) 4.2 (1) 0.3 0.073 0.031 (1) 0.090.012 0.0011 <0.0010 0.0015 0.45 0.2 0.078 0.44 2.2 6.9 8.5 8.8 16 0.88 0.22 0.12 0.320.028 0.0011 0.0013 <0.0010 1.6 0.65 0.29 2.8 13 49 74 99 140 4 1.1 0.37 1.10.04 0.0022 0.0013 0.0015 2.1 0.85 0.37 3.2 15 56 83 110 160 4.8 1.4 0.49 1.4

<0.10 <0.10 <0.10 <0.10 4.2 1.8 0.66 8.7 44 110 120 130 210 11 3.8 0.75 3.4

<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.020 <0.020 <0.020 - - <0.010 <0.010 <0.010 <0.010

E2‐3



Appendix E2


Units







PL4860 PL4861 PL4862 PL4886 PL4859 PL4928 PL4929 PL5041 PL5042 PL5043 PL5044 PL5099 PL5100 PL5101 PL5106 PL5107 PL5085 PL5071 PL5081 PL50802016/08/31 15:30 2016/08/31 15:30 2016/08/31 15:30 2016/08/31 15:30 2016/08/31 15:00 2016/08/31 16:30 2016/08/31 16:45 2016/09/02 09:15 2016/09/02 09:15 2016/09/02 09:15 2016/09/02 09:15 2016/09/01 12:15 2016/09/01 12:15 2016/09/01 12:15 2016/09/01 12:15 2016/09/01 12:15 2016/09/01 12:15 2016/09/01 14:30 2016/09/01 14:30 2016/09/01 14:30

503355-16-01 503355-16-01 503355-16-01 503355-16-01 503355-16-01 503355-17-01 503355-17-01 503355-31-01 503355-31-01 503355-31-01 503355-31-01 503355-25-01 503355-25-01 503355-25-01 503355-25-01 503355-25-01 503355-26-01 503355-28-01 503355-27-01 503355-27-01

DAS-SB-07-G1 DAS-SB-07-G2 DAS-SB-07-G3 DAS-SB-07-G-ALL DAS-SB-08-A0.2 DAS-SB-08-G-ALL DAS-SB-09-G-ALL DAS-W-01-A-0.2 DAS-W-01-A-0.6 DAS-W-01-A-1.0 DAS-W-01-B DAS-W-02-A-0.2 DAS-W-02-A-0.2-1 DAS-W-02-A-0.2-2 DAS-W-02-A-0.2-3 DAS-W-02-A-0.6 DAS-W-02-A-1.0 DAS-W-02-B DAS-W-03-A-0.2 DAS-W-03-A-0.6 DAS-W-03-A-1.0

24 - 26 - 37 - 26 28 30 26 25 29 30 30 33 26 31 28 32 30

- - - 86.6 - 83.3 87.4 67.6 60.5 70.3 74.2 74.8 - - - 54.7 70.1 55.1 76.4 60.5 60.7- - - 13.4 - 16.7 12.7 32.4 39.5 29.8 25.8 25.2 - - - 45.3 29.9 44.9 23.6 39.5 39.3

8.39 8.54 8.39 8.5 8.04 8.25 8.38 8.1 8.09 8.2 8.33 8.1 8.07 8.14 7.8 8.17 8.18 8.17 7.96 8.14

11100 10000 11000 10200 17400 11900 12700 12100 13200 11400 10800 11500 12000 11400 15600 11500 14700 11400 14700 146000.6 0.43 0.57 0.96 2.19 0.63 0.57 0.35 0.67 0.22 0.2 0.46 0.37 0.34 0.87 0.21 0.34 0.32 0.69 0.285.05 3.51 4.08 3.65 8.28 4.52 4.94 5.04 7.95 5.53 5.16 5.29 5.62 5.26 8.72 4.99 7.63 5.13 8.07 5.948.1 37.4 54.1 49.2 75 46.5 69.8 41.8 52.2 34.3 30.3 45.4 42.1 40.1 59.9 33.7 40.6 39.1 52.2 41.6

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.400.13 <0.10 0.14 <0.10 0.32 0.13 0.14 0.13 0.19 <0.10 <0.10 0.14 0.14 0.13 0.28 <0.10 0.1 0.14 0.27 <0.10

0.387 0.342 0.355 0.344 0.876 0.472 0.637 0.436 0.612 0.349 0.324 0.456 0.469 0.445 0.956 0.392 0.463 0.399 0.755 0.49912400 11000 15100 11800 11500 9870 11400 9130 9360 8410 8250 8560 7900 8920 8310 7900 10600 9160 7430 823021.1 19.4 21.3 18.9 29.6 23.4 25.2 20.7 23.6 19.3 20.5 21.6 22.5 21.4 26 21.2 25.5 20.6 25.2 24.56.84 5.47 6.45 6.05 9.96 7 7.06 7.53 8.25 7.85 7.84 7.11 7.09 7.03 8.88 7.74 10.2 6.65 8.66 8.658.7 39.7 56.1 49.5 134 63 64.7 46 52.3 19.3 18.5 51.6 54.8 56.1 91 17.8 24.5 51.2 50.3 22.8

21900 20100 20900 19800 28900 21900 24500 22000 23600 20600 20600 22300 22400 22200 24900 21300 25400 21900 24800 2360016.7 12.1 17.1 15.7 67.1 21.1 17.6 11.5 39.6 5.63 4.13 21.5 19.5 16.2 47 4.17 5.75 13.3 29.2 5.515.9 13.7 15.1 14.1 20.1 15.3 17.4 14.2 17.5 16.4 15 14.4 15.1 13.9 19.6 16.3 21.3 13.9 19.5 20.26260 4970 6130 5430 9130 6690 6970 6380 6910 6250 6110 6360 6480 6100 8250 6310 8310 6030 7780 7420227 203 218 197 293 236 245 223 233 204 197 217 223 213 253 205 255 209 254 242

0.089 0.057 0.144 0.066 0.239 0.09 0.098 0.067 0.252 <0.050 <0.050 0.099 0.086 0.085 0.551 <0.050 <0.050 0.082 0.456 <0.0500.95 0.55 0.66 0.52 2.34 0.82 0.72 0.74 2.05 1.26 0.98 0.95 0.85 0.82 3.23 1.57 1.73 0.86 2.84 1.4814.6 9.48 13.8 11.6 24.6 15.4 16.6 16.4 18.7 16.2 14.8 15.6 17 16 22.8 16.1 23.3 15.4 22.2 20.1591 455 547 485 638 601 646 509 482 404 394 540 587 510 547 380 483 512 526 436

1460 1210 1590 1360 2320 1590 1750 1770 1960 1830 1820 1620 1680 1550 2360 1830 2450 1550 2270 2220<0.50 <0.50 <0.50 <0.50 0.5 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.53 <0.50 <0.50 <0.50 <0.50 <0.500.205 0.136 0.3 0.62 0.842 0.232 0.281 0.187 0.426 0.078 0.052 0.25 0.241 0.267 0.648 0.061 0.107 0.16 0.742 0.1113800 2860 3490 3130 6860 4320 4270 4110 4260 4190 3880 4790 4420 3680 6960 3760 5420 4020 5710 466078.2 72.1 107 77.1 78.4 59.9 79.5 54.8 62.1 48 45.9 53.5 49.8 49.9 62.3 46.8 57.5 52.9 57.1 50.9

0.109 0.09 0.087 0.094 0.148 0.109 0.105 0.131 0.147 0.148 0.163 0.125 0.135 0.135 0.159 0.143 0.141 0.133 0.153 0.1431.16 1.05 1.03 0.9 6.03 1.26 1.4 1.14 1.88 0.31 0.23 1.37 1.16 1.13 4.1 0.24 0.29 0.84 3.01 0.33655 568 664 599 819 666 760 716 754 698 697 675 703 719 872 762 888 705 868 883

0.642 0.682 0.598 0.59 1.3 0.739 0.703 0.828 1.31 1.11 0.919 0.735 0.781 0.742 1.74 0.914 1.5 0.697 1.46 1.2559.6 55.6 56.3 54.1 66.1 58.9 62.9 58.9 63.1 55.2 54.3 61.7 59.4 60.9 61.4 57.6 62.7 60.2 61.3 59.473.5 73.1 72.8 90 143 76.7 93 63.8 90 46.3 42.4 80.8 76.3 67.5 113 44.3 57.2 71 89.6 54.42.39 1.63 2.39 1.84 4.97 2.59 2.89 3.11 4.15 3.26 3.15 2.98 3.01 2.9 5.2 3.45 6.32 2.94 5.31 4.51

0.052 (1) 0.019 (1) 0.3 0.036 (1) 0.28 (1) 0.056 (1) 0.035 (1) 0.009 0.032 (1) 0.0087 <0.0010 0.014 (1) 0.013 (1) 0.023 (4) 0.066 (1) <0.0010 <0.0010 0.038 (4) 0.071 (1) 0.00110.026 (1) 0.0076 (1) 0.1 0.016 (1) 0.079 (1) 0.022 (1) 0.015 (1) 0.006 0.012 (1) 0.0019 <0.0010 0.0076 (1) 0.0077 (1) 0.013 (1) 0.023 (1) <0.0010 <0.0010 0.039 (4) 0.031 (1) 0.0016

0.0096 (1) 0.0049 (1) 0.031 0.0093 (1) 0.091 (1) 0.011 (1) 0.0089 (1) 0.0053 0.020 (1) 0.0028 <0.00050 0.0095 (1) 0.012 (1) 0.011 (4) 0.034 (1) <0.00050 <0.00050 0.0093 (1) 0.019 (1) 0.000710.032 (1) 0.014 (1) 0.063 0.020 (1) 0.10 (1) 0.029 (1) 0.0096 (1) 0.0043 0.041 (1) 0.0011 <0.00050 0.0079 (1) 0.0078 (1) 0.0066 (4) 0.018 (1) <0.00050 <0.00050 0.0083 (4) 0.028 (1) <0.000500.061 (1) 0.014 (1) 0.065 0.024 (1) 0.14 (1) 0.040 (1) 0.017 (1) 0.0053 0.036 (1) 0.0015 <0.0010 0.012 (1) 0.014 (1) 0.013 (4) 0.024 (1) <0.0010 <0.0010 0.012 (4) 0.028 (1) <0.00100.17 (1) 0.052 (1) 0.22 0.11 (1) 0.46 (1) 0.24 (1) 0.087 (1) 0.022 0.29 (1) 0.0082 <0.0010 0.055 (1) 0.098 (1) 0.071 (4) 0.13 (1) <0.0010 <0.0010 0.063 (4) 0.10 (1) 0.00270.22 (1) 0.022 (1) 0.19 0.050 (1) 0.36 (1) 0.084 (1) 0.049 (1) 0.02 0.077 (1) 0.0051 0.0017 0.026 (1) 0.037 (1) 0.035 (4) 0.051 (1) 0.0019 0.0019 0.030 (4) 0.036 (1) 0.00270.23 (1) 0.11 (1) 0.32 0.19 (1) 0.65 (1) 0.38 (1) 0.18 (1) 0.044 0.44 (1) 0.012 <0.0010 0.092 (1) 0.18 (1) 0.16 (4) 0.19 (1) <0.0010 <0.0010 0.12 (4) 0.18 (1) 0.00830.35 (1) 0.17 (1) 0.52 0.27 (1) 4.3 (1) 0.57 (1) 0.25 (1) 0.054 0.50 (1) 0.012 <0.0010 0.13 (1) 0.22 (1) 0.22 (4) 0.26 (1) <0.0010 <0.0010 0.15 (4) 0.28 (1) 0.00840.099 (1) 0.046 (1) 0.24 0.095 (1) 0.59 (1) 0.16 (1) 0.075 (1) 0.026 0.17 (1) 0.0042 <0.0010 0.040 (1) 0.076 (1) 0.073 (4) 0.068 (1) <0.0010 <0.0010 0.059 (4) 0.066 (1) 0.0030.17 (1) 0.056 (1) 0.37 0.12 (1) 1.1 (1) 0.20 (1) 0.10 (1) 0.035 0.20 (1) 0.0044 <0.0010 0.051 (1) 0.095 (1) 0.094 (4) 0.084 (1) <0.0010 <0.0010 0.081 (4) 0.082 (1) 0.00360.17 (1) 0.084 (1) 0.34 0.15 (1) 1.9 (1) 0.28 (1) 0.14 (1) 0.061 0.27 (1) 0.0058 <0.0010 0.087 (1) 0.12 (1) 0.11 (4) 0.14 (1) <0.0010 <0.0010 0.14 (1) 0.16 (1) 0.00460.057 (1) 0.030 (1) 0.14 0.050 (1) 0.73 (1) 0.095 (1) 0.048 (1) 0.021 0.10 (1) 0.0023 <0.0010 0.033 (1) 0.042 (1) 0.036 (4) 0.049 (1) <0.0010 <0.0010 0.041 (1) 0.052 (1) 0.00160.11 (1) 0.053 (1) 0.24 0.096 (1) 1.2 (1) 0.18 (1) 0.095 (1) 0.039 0.22 (1) 0.0043 <0.0010 0.058 (1) 0.088 (1) 0.082 (4) 0.096 (1) <0.0010 <0.0010 0.084 (1) 0.10 (1) 0.00290.050 (1) 0.023 (1) 0.098 0.040 (1) 0.49 (1) 0.081 (1) 0.044 (1) 0.02 0.13 (1) 0.0023 <0.0020 0.034 (1) 0.047 (1) 0.039 (4) 0.062 (1) <0.0020 <0.0020 0.037 (1) 0.058 (1) <0.00200.014 (1) 0.0069 (1) 0.031 0.012 (1) 0.16 (1) 0.023 (1) 0.013 (1) 0.006 0.031 (1) <0.00050 <0.00050 0.010 (1) 0.014 (1) 0.011 (4) 0.016 (1) <0.00050 <0.00050 0.011 (4) 0.015 (1) <0.000500.061 (1) 0.025 (1) 0.11 0.048 (1) 0.52 (1) 0.094 (1) 0.052 (1) 0.023 0.18 (1) 0.0032 <0.0020 0.044 (1) 0.060 (1) 0.049 (4) 0.088 (1) <0.0020 <0.0020 0.041 (1) 0.077 (1) 0.0027

0.57 0.13 0.97 0.26 1.5 0.48 0.22 0.072 0.51 0.029 0.0017 0.13 0.19 0.17 0.34 0.0019 0.0019 0.2 0.32 0.00880.97 0.44 1.7 0.79 7.9 1.5 0.71 0.2 1.6 0.037 <0.0010 0.38 0.67 0.63 0.71 <0.0010 <0.0010 0.51 0.73 0.0261.5 0.58 2.7 1.1 9.4 2 0.93 0.28 2.1 0.067 0.0017 0.51 0.86 0.8 1.1 0.0019 0.0019 0.71 1 0.0352.2 1.1 4.7 1.9 23 3.5 1.8 0.75 3.8 <0.10 <0.10 1.1 1.6 1.5 1.8 <0.10 <0.10 1.6 1.9 <0.10

<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 0.019 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.0100.024 <0.010 0.049 <0.010 0.032 <0.010 <0.010 0.11 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010

<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.0100.024 <0.010 0.068 <0.010 0.032 <0.010 <0.010 0.11 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.010

E2‐4



Appendix E2


Units







PL5082 PL4667 PL4669 PL4670 PL4668 PL4693 PL4694 PL4692 PL4712 PL4666 PL4956 PL5074 PL5078 PL5054 PL5056 PL5053 PL5017 PL5028 PL49982016/09/01 14:30 2016/08/29 16:30 2016/08/29 16:30 2016/08/29 16:30 2016/08/29 16:30 2016/08/29 18:05 2016/08/29 18:05 2016/08/29 18:05 2016/08/29 18:05 2016/08/29 14:30 2016/09/02 13:00 2016/09/01 17:15 2016/09/01 17:15 2016/09/01 17:15 2016/09/01 17:15 2016/09/01 17:15 2016/09/02 12:00 2016/09/02 12:00 2016/09/02 12:00

503355-27-01 503355-02-01 503355-02-01 503355-02-01 503355-02-01 503355-04-01 503355-04-01 503355-04-01 503355-05-01 503355-01-01 503355-35-01 503355-28-01 503355-28-01 503355-29-01 503355-29-01 503355-29-01 503355-32-01 503355-32-01 503355-33-01

DAS-W-03-B DAS-W-03-B Lab-Du DAS-W-04-A-0.2 DAS-W-04-A-0.6 DAS-W-04-A-1.0 DAS-W-04-B DAS-W-04-B Lab-Du DAS-W-05-A-0.2 DAS-W-05-A-0.6 DAS-W-05-A-1.0 DAS-W-05-B DAS-W-06-A-0.2 DAS-W-07-A-0.2 DAS-W-08-A-0.2 DAS-W-08-A-0.6 DAS-W-08-A-1.0 DAS-W-08-B DAS-W-08-C DAS-W-09-A-0.2 DAS-W-09-A-0.6 DAS-W-09-A-1.0

27 - - 29 29 36 - - 28 45 - 30 26 28 28 25 - 29 31

73.2 81.3 76.1 59.4 67.4 57.4 94.3 57.1 63.8 46.3 53.9 62.3 28.1 31.6 46 71.6 77.6 58.8 67.326.9 18.7 23.9 40.6 32.6 42.6 5.7 42.9 36.2 53.7 46.1 37.7 71.9 68.4 54 28.4 22.4 41.2 32.7

8.22 8.32 8.39 8.39 8.35 8.14 8.67 8.35 8.33 8.22 8.03 8.24 8.32 8.39 8.26 8.42 8.14 8.02 8.18

12200 9780 10500 12600 11500 12400 8400 12900 12400 14400 14700 13200 17900 17700 14200 11500 12300 13800 122000.21 0.25 0.26 0.28 0.23 0.43 <0.10 0.44 0.23 0.5 0.49 0.25 0.39 0.36 0.42 0.23 0.27 0.41 0.285.21 4.24 4.14 5.76 5.7 6.17 1.43 6.2 5.86 7.23 6.41 5.16 5.68 5.85 6.37 5.55 5.83 7.78 5.7733.7 33.2 35.5 37.6 34.2 41.6 21.8 43.8 37.8 46.9 48.8 42.6 77.2 67.8 45.7 32.6 34.3 46.9 37.5

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40<0.10 0.11 <0.10 <0.10 <0.10 0.19 <0.10 0.16 <0.10 0.21 0.18 0.11 0.1 <0.10 0.17 <0.10 0.14 0.18 <0.100.314 0.313 0.345 0.424 0.449 0.465 0.13 0.599 0.448 0.561 0.558 0.355 0.374 0.371 0.572 0.379 0.389 0.621 0.4068080 9180 12600 7070 6700 7920 22000 6490 7080 9480 11200 9730 10200 10800 12900 9940 13600 8920 813021 21.2 21 23 20.9 25.2 21.7 24.2 23 26.4 26 21.6 26.5 25.3 24.1 19.5 20.5 23.5 20.4

8.06 6.11 6.71 8.37 7.83 7.43 4.95 8.09 8.23 8.12 8.24 8.17 12.5 10.9 8.71 7.72 8.33 8.87 8.0617.5 46.4 29.4 22.4 20.2 79.9 13 32 21.5 91.5 86.3 38.9 40.9 34.5 39 17.4 26.1 45.9 19.8

21600 19300 19200 21100 20400 20200 20900 21300 21300 21800 23800 22700 26800 26500 23700 20600 22200 23700 220004.03 12.9 9.14 4.95 4.47 19.9 2.31 17.8 4.77 20.9 23.7 9.12 5.75 5.73 16.7 4.29 6.87 18.8 5.9818 14.4 16.5 19.9 19 16.2 14.2 20.2 19.7 17.9 17.6 14.8 15.4 18 17.6 16.4 16.6 18.7 18.2

6530 4650 5070 6320 5680 6160 3620 6310 6220 6790 7850 7330 10600 9610 7370 6250 6470 7410 6610211 192 195 227 208 235 164 233 226 251 249 268 404 347 248 202 220 235 215

<0.050 0.06 0.12 <0.050 <0.050 0.092 <0.050 0.123 <0.050 0.109 0.106 <0.050 <0.050 <0.050 0.102 <0.050 <0.050 0.145 <0.0501.1 0.67 1.5 1.12 1.42 1.35 0.64 1.54 1.24 1.35 1.35 0.81 1.15 1.45 1.68 1.3 0.9 2.44 1.3515.9 14 13.7 19.1 17.7 21 6.97 20.6 18.6 23.1 22.1 18 24.8 21 19.7 16.1 16.5 20.5 17367 455 402 412 382 611 338 446 413 676 718 581 643 581 502 381 458 473 406

1890 1160 1430 1900 1740 1620 883 1900 1870 1860 2030 2040 3110 3040 2160 1870 1810 2020 1950<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.500.07 0.181 0.164 0.09 0.08 0.339 <0.050 0.295 0.101 0.386 0.375 0.147 0.091 0.131 0.269 0.069 1.63 0.274 0.094080 2860 3320 4260 3840 5530 1980 3960 3940 6280 5930 4530 4860 5450 4440 3850 4200 4760 429046 57.5 72.1 47 46.5 54 123 47.6 46.6 66.3 69.9 61.9 62.3 67.2 77.8 51.7 70.4 57.5 47.7

0.144 0.109 0.09 0.142 0.144 0.108 <0.050 0.132 0.14 0.14 0.116 0.112 0.108 0.114 0.14 0.177 0.146 0.149 0.1580.24 0.61 0.58 0.25 0.22 1.19 0.17 1.05 0.24 1.25 1.19 0.52 0.37 0.43 1.06 0.28 0.35 1.61 0.4781 619 668 846 753 738 631 841 830 805 830 807 1200 1210 820 740 734 786 752

0.856 0.577 0.938 1.21 1.11 0.999 0.612 1.31 1.38 1.04 1.08 0.901 1.05 1.31 1.46 1.15 1.01 1.76 1.2756.2 67.7 64 58.9 56.1 56.3 92.1 59.5 58.6 53 56.9 59 67.5 70.3 60.6 54.2 58.2 59 56.445.2 58.9 50.3 52.4 46.3 83.6 28.2 80.7 51 93.6 88.8 62.1 67.8 67.1 66 44.7 49 80.2 48.63.46 2.09 2.57 4.14 4.26 3.88 0.74 4.44 4.48 4.01 4.27 3.05 4.27 5.02 4.45 3.2 3.51 4.61 3.84

<0.0010 0.015 (1) 0.01 <0.0010 <0.0010 0.021 (1) <0.0010 0.015 <0.0010 0.028 0.027 0.006 0.0031 0.0024 0.019 0.0037 0.0065 (1) 0.076 0.019<0.0010 0.0097 (1) 0.004 0.0011 <0.0010 0.018 (1) <0.0010 0.0068 <0.0010 0.025 0.021 0.0057 0.0019 0.0017 0.0083 <0.0010 <0.0050 (1) 0.024 0.0043<0.00050 0.0052 (1) 0.005 <0.00050 <0.00050 0.012 (1) 0.0012 0.009 <0.00050 0.018 0.017 0.0036 0.00054 0.00083 0.01 0.00093 0.0032 (1) 0.088 0.007<0.00050 0.0096 (1) 0.0042 <0.00050 <0.00050 0.010 (1) <0.00050 0.0037 <0.00050 0.013 0.0096 0.0031 <0.00050 0.00097 0.005 <0.00050 <0.0025 (1) 0.016 0.0032<0.0010 0.012 (1) 0.0058 <0.0010 <0.0010 0.020 (1) <0.0010 0.0059 <0.0010 0.022 0.044 0.005 <0.0010 0.0011 0.0097 <0.0010 <0.0050 (1) 0.036 0.0043<0.0010 0.068 (1) 0.026 <0.0010 <0.0010 0.095 (1) 0.0037 0.025 <0.0010 0.099 0.12 0.031 0.0028 0.0054 0.034 0.0021 0.028 (1) 0.19 0.0190.0015 0.031 (1) 0.015 0.0021 0.0017 0.036 (1) 0.0022 0.019 0.0017 0.067 0.092 0.018 0.0019 0.0035 0.026 0.0024 0.011 (1) 0.16 0.013

<0.0010 0.091 (1) 0.047 <0.0010 <0.0010 0.16 (1) 0.0067 0.047 <0.0010 0.2 0.17 0.046 0.002 0.0089 0.053 <0.0010 0.032 (1) 0.68 0.026<0.0010 0.11 (1) 0.05 0.0013 <0.0010 0.20 (1) 0.0076 0.083 <0.0010 0.28 0.22 0.06 0.0068 0.018 0.082 0.0012 0.059 (1) 0.93 0.033<0.0010 0.046 (1) 0.02 <0.0010 <0.0010 0.071 (1) 0.0042 0.017 <0.0010 0.11 0.085 0.022 <0.0010 0.0032 0.02 <0.0010 0.045 (1) 0.48 0.0084<0.0010 0.075 (1) 0.022 <0.0010 <0.0010 0.096 (1) 0.0045 0.024 <0.0010 0.14 0.12 0.026 0.0015 0.0054 0.027 <0.0010 0.095 (1) 0.54 0.011<0.0010 0.087 (1) 0.032 <0.0010 <0.0010 0.14 (1) 0.0066 0.045 <0.0010 0.21 0.16 0.033 0.0015 0.0062 0.048 <0.0010 0.038 (1) 0.76 0.014<0.0010 0.033 (1) 0.012 <0.0010 <0.0010 0.054 (1) 0.0028 0.016 <0.0010 0.074 0.054 0.012 <0.0010 0.0019 0.018 <0.0010 0.011 (1) 0.32 0.0052<0.0010 0.060 (1) 0.022 <0.0010 <0.0010 0.086 (1) 0.0048 0.03 <0.0010 0.14 0.099 0.023 0.0011 0.0039 0.031 <0.0010 0.033 (1) 0.7 0.011<0.0020 0.028 (1) 0.012 <0.0020 <0.0020 0.046 (1) 0.0026 0.019 <0.0020 0.07 0.055 0.012 <0.0020 <0.0020 0.02 <0.0020 0.011 (1) 0.35 0.0055<0.00050 0.0083 (1) 0.0034 <0.00050 <0.00050 0.013 (1) 0.00073 0.0052 <0.00050 0.02 0.015 0.0034 <0.00050 0.00055 0.0051 <0.00050 0.0082 (1) 0.095 0.0015<0.0020 0.034 (1) 0.015 <0.0020 <0.0020 0.060 (1) 0.0028 0.027 <0.0020 0.084 0.066 0.015 <0.0020 0.0029 0.027 <0.0020 0.019 (1) 0.39 0.00770.0015 0.15 0.07 0.0033 0.0017 0.21 0.0071 0.083 0.0017 0.27 0.33 0.073 0.01 0.016 0.11 0.0091 0.049 0.59 0.07

<0.0010 0.39 0.16 0.0013 <0.0010 0.62 0.028 0.21 <0.0010 0.89 0.7 0.18 0.011 0.04 0.22 0.0012 0.27 3.4 0.0920.0015 0.54 0.23 0.0046 0.0017 0.83 0.036 0.29 0.0017 1.2 1 0.25 0.022 0.055 0.33 0.01 0.32 4 0.16<0.10 1.1 0.42 <0.10 <0.10 1.8 <0.10 0.55 <0.10 2.7 2 0.44 <0.10 <0.10 0.6 <0.10 0.62 11 0.19

<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 0.027 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.020 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 0.027 <0.020 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.020 <0.010

E2‐5



Appendix E2


Units







PL5001 PL5000 PL5112 PL5113 PL5114 PL5143 PL5116 PL5144 PL5111 PL4675 PL4676 PL4677 PL4691 PL4789 PL5014 PL5015 PL4665 PL46642016/09/02 12:00 2016/09/02 12:00 2016/09/01 11:45 2016/09/01 11:45 2016/09/01 11:45 2016/09/01 11:45 2016/09/01 11:45 2016/09/01 11:45 2016/09/01 11:45 2016/08/29 17:00 2016/08/29 17:00 2016/08/29 17:00 2016/08/29 17:00 2016/08/29 14:30 2016/09/02 09:30 2016/09/02 09:30 2016/08/29 14:00 2016/08/29 13:00

503355-33-01 503355-33-01 503355-24-01 503355-24-01 503355-24-01 503355-23-01 503355-24-01 503355-23-01 503355-24-01 503355-03-01 503355-03-01 503355-03-01 503355-04-01 503355-12-01 503355-32-01 503355-32-01 503355-01-01 503355-01-01

DAS-W-09-B DAS-W-09-C DAS-W-10-A-0.2 DAS-W-10-A-0.2-1 DAS-W-10-A-0.2-2 DAS-W-10-A-0.2-3 DAS-W-10-A-0.6AS-W-10-A-0.6 Lab-D DAS-W-10-A-1.0 DAS-W-10-B DAS-W-10-C DAS-W-11-A-0.2 DAS-W-11-A-0.6 DAS-W-11-A-1.0 DAS-W-11-B DAS-W-11-C DAS-W-12-GRAB DAS-W-13-A-0.2 DAS-W-13-A-0.6 DAS-W-14-A-0.2 DAS-W-15-A-0.2

27 23 - 22 22 22 31 29 27 32 - 23 - 29 - 38 39 30 - 25

69.5 38.6 87.5 - - - 53.9 62.6 70.8 52 79.4 89.9 55.3 66.9 68.4 61.4 46.3 37.8 68.1 74.130.5 61.4 12.5 - - - 46.1 37.5 29.2 48 20.6 10.1 44.7 33.1 31.6 38.6 53.7 62.2 31.9 25.9

8.39 8.13 - 8.35 8.21 8.2 8 8.12 8.17 8.16 8.27 8.57 8.1 8.29 - 8.02 7.96 7.77 8.34 8.49

11900 18400 9650 9300 9220 14500 13100 11400 15300 9290 8750 13600 11700 11100 15000 17200 11200 110000.22 0.45 0.23 0.23 0.26 0.45 0.25 0.18 0.31 0.27 0.22 0.53 0.21 0.54 0.51 1.46 0.45 0.346.23 8.2 4.98 3.76 3.62 7.14 6.07 4.95 7.77 3.85 2.9 7.23 6.07 6.68 7.21 9.19 5.43 4.3734.1 50.9 28.7 27.8 29.2 55.8 40 32.5 41.8 34.1 27.7 57 34.9 42.1 49.8 63.4 40 35.4

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40<0.10 0.12 <0.10 <0.10 0.12 0.2 <0.10 <0.10 <0.10 0.11 <0.10 0.16 <0.10 0.17 0.18 0.61 0.14 0.120.411 0.594 0.297 0.253 0.286 0.551 0.411 0.374 0.498 0.354 0.206 0.642 0.382 0.608 0.61 1.41 0.431 0.3419080 11400 6640 6370 6060 10600 8530 7890 12900 6960 15300 7270 7420 8360 9550 11000 9340 1130020.6 29.8 20.4 21.4 22.5 35.9 25.3 40.4 26.3 20.4 21.5 24.6 21.9 21.7 25.8 30.7 23 22.58.63 11.9 6.13 5.93 6.01 9.03 8.55 8.18 10.3 5.99 5.32 8.88 8.07 7.23 8.76 10.2 6.91 7.1818.5 33.2 33.3 37.2 33.8 50.5 21.4 17.5 25.3 42 28.2 39.2 20.3 71.4 88.8 207 70.1 55.2

21900 29500 22400 21700 21700 24400 22700 21800 26400 19100 20600 22600 20700 19900 24900 27600 20600 191004.39 7.22 9.04 8.97 8.78 23.1 5 4.05 5.81 9.3 6.42 70.2 4.69 17.8 20.8 81.7 16.2 13.717.7 27.2 13 11.9 13.8 19.3 20.1 17.3 21.2 13.3 15.5 19.9 19.4 15.4 18.4 20 15.8 16.26650 10400 5040 4800 4970 7770 7340 6320 8600 4580 4060 6730 5900 6230 8330 9060 5670 5320211 317 192 187 194 251 230 206 264 195 170 267 213 229 272 293 222 199

<0.050 <0.050 <0.050 <0.050 0.053 0.155 <0.050 <0.050 <0.050 <0.050 <0.050 0.132 <0.050 0.09 0.126 0.25 0.072 0.0551.27 2.93 0.55 1.65 0.5 2.64 1.55 1.12 1.6 0.6 0.68 2.49 1.24 1.25 1.66 4.39 0.85 0.7417.2 28.8 12.1 10.9 11.2 22.2 17.9 17.2 23.6 12.3 9.21 22.2 17.8 19 23.1 30.8 17.3 16.7387 552 448 428 421 526 420 386 479 462 384 476 406 638 700 654 623 619

1960 3000 1240 1210 1270 2190 2160 1820 2480 1200 1060 2010 1740 1590 2170 2410 1480 1250<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.62 <0.50 <0.500.064 0.132 0.128 0.135 0.259 0.368 0.078 0.071 0.108 0.195 0.107 0.312 0.099 0.268 0.392 1.62 0.28 0.2294410 7000 3010 2710 2870 5350 5350 3780 5420 3160 2250 4640 3980 5230 6820 6480 4110 302050.7 66.8 43.9 40.1 38.5 82.7 51.8 44.7 77.6 43.5 86.1 58.2 50.5 51.8 61 70.1 61 64.6

0.165 0.14 0.057 0.102 0.102 0.089 0.134 0.143 0.142 0.097 0.059 0.14 0.14 0.126 0.141 0.153 0.111 0.0870.22 0.34 0.51 0.49 0.53 2.59 0.28 0.23 0.29 0.57 0.34 1.81 0.22 1.12 1.37 3.44 0.95 0.65739 1070 638 596 646 824 846 709 901 671 624 813 777 686 877 885 678 5781.04 1.95 0.528 0.513 0.525 1.48 1.34 0.955 1.68 0.571 0.613 1.49 1.16 0.982 1.18 1.71 0.875 0.72756.2 70.6 72.1 71.7 71.3 61.7 58.8 56.1 63.6 62.4 85.4 58.8 56.4 51.2 58.3 64.9 63 62.646.3 69.7 48.6 48.4 48.8 73.9 50.2 43.5 56.1 59.6 39 76 47 81.3 95.7 179 73.3 62.84.41 8.46 1.94 1.9 1.91 4.81 4.54 3.72 6.76 2.34 1.22 4.63 4.13 4.04 4.74 6.31 2.75 1.87

<0.0010 <0.0010 0.0073 0.0045 0.011 (1) 0.050 (1) 0.011 <0.0010 <0.0010 0.017 (1) 0.024 0.022 <0.0010 0.020 (1) 0.020 (1) 0.044 (1) 0.021 (1) 0.0094<0.0010 0.0013 0.0055 0.0037 0.0056 (1) 0.017 (1) 0.0061 <0.0010 <0.0010 0.012 (1) 0.018 0.011 <0.0010 0.017 (1) 0.015 (1) 0.030 (1) 0.014 (1) 0.0076<0.00050 <0.00050 0.0043 0.0031 0.0028 (1) 0.020 (1) 0.0054 <0.00050 <0.00050 0.0047 (1) 0.0098 0.011 <0.00050 0.0076 (1) 0.014 (1) 0.038 (1) 0.0087 (1) 0.012<0.00050 <0.00050 0.0082 0.0028 0.0042 (1) 0.014 (1) 0.0034 <0.00050 <0.00050 0.0059 (1) 0.014 0.0049 <0.00050 0.011 (1) 0.022 (1) 0.032 (1) 0.011 (1) 0.0045<0.0010 <0.0010 0.011 0.0046 0.0051 (1) 0.018 (1) 0.0067 <0.0010 <0.0010 0.0075 (1) 0.027 0.0081 <0.0010 0.015 (1) 0.027 (1) 0.045 (1) 0.013 (1) 0.012<0.0010 0.0019 0.052 0.032 0.022 (1) 0.096 (1) 0.03 <0.0010 0.0012 0.041 (1) 0.09 0.041 <0.0010 0.078 (1) 0.12 (1) 0.27 (1) 0.063 (1) 0.0550.0023 0.002 0.033 0.018 0.010 (1) 0.034 (1) 0.023 0.0017 0.0021 0.016 (1) 0.055 0.032 0.0021 0.033 (1) 0.053 (1) 0.13 (1) 0.029 (1) 0.043

<0.0010 <0.0010 0.073 0.061 0.044 (1) 0.16 (1) 0.053 <0.0010 <0.0010 0.13 (1) 0.086 0.11 <0.0010 0.18 (1) 0.19 (1) 0.55 (1) 0.13 (1) 0.15<0.0010 <0.0010 0.076 0.058 0.054 (1) 0.22 (1) 0.073 <0.0010 <0.0010 0.14 (1) 0.15 0.12 <0.0010 0.23 (1) 0.28 (1) 0.86 (1) 0.16 (1) 0.15<0.0010 <0.0010 0.03 0.021 0.019 (1) 0.060 (1) 0.024 <0.0010 <0.0010 0.045 (1) 0.052 0.042 <0.0010 0.080 (1) 0.092 (1) 0.25 (1) 0.055 (1) 0.095<0.0010 0.0013 0.039 0.026 0.028 (1) 0.071 (1) 0.036 <0.0010 0.001 0.062 (1) 0.096 0.046 <0.0010 0.11 (1) 0.12 (1) 0.31 (1) 0.078 (1) 0.15<0.0010 <0.0010 0.055 0.034 0.039 (1) 0.10 (1) 0.043 <0.0010 <0.0010 0.083 (1) 0.11 0.071 <0.0010 0.15 (1) 0.18 (1) 0.46 (1) 0.12 (1) 0.14<0.0010 <0.0010 0.021 0.012 0.014 (1) 0.035 (1) 0.016 <0.0010 <0.0010 0.027 (1) 0.046 0.028 <0.0010 0.047 (1) 0.058 (1) 0.17 (1) 0.037 (1) 0.054<0.0010 <0.0010 0.036 0.021 0.022 (1) 0.074 (1) 0.027 <0.0010 <0.0010 0.050 (1) 0.074 0.05 <0.0010 0.091 (1) 0.11 (1) 0.32 (1) 0.073 (1) 0.089<0.0020 <0.0020 0.02 0.012 0.012 (1) 0.040 (1) 0.016 <0.0020 <0.0020 0.025 (1) 0.033 0.027 <0.0020 0.039 (1) 0.060 (1) 0.17 (1) 0.033 (1) 0.04<0.00050 <0.00050 0.0056 0.0032 0.0033 (1) 0.010 (1) 0.0044 <0.00050 <0.00050 0.0071 (1) 0.01 0.008 <0.00050 0.011 (1) 0.017 (1) 0.050 (1) 0.0096 (1) 0.012<0.0020 <0.0020 0.023 0.014 0.014 (1) 0.052 (1) 0.02 <0.0020 <0.0020 0.031 (1) 0.043 0.035 <0.0020 0.045 (1) 0.074 (1) 0.21 (1) 0.041 (1) 0.0470.0023 0.0052 0.12 0.069 0.061 0.25 0.085 0.0017 0.0032 0.1 0.24 0.13 0.0021 0.18 0.27 0.59 0.16 0.14

<0.0010 0.0013 0.26 0.19 0.17 0.59 0.22 <0.0010 0.001 0.44 0.47 0.37 <0.0010 0.69 0.81 2.4 0.5 0.650.0023 0.0065 0.38 0.26 0.23 0.84 0.3 0.0017 0.0042 0.54 0.71 0.5 0.0021 0.88 1.1 2.9 0.66 0.8<0.10 <0.10 0.72 0.45 0.48 1.4 0.56 <0.10 <0.10 1 1.4 0.96 <0.10 1.8 2.3 6.1 1.4 1.9

<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 0.026 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 0.029 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.010<0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.020 <0.020 <0.010 <0.020 <0.010 <0.020 0.055 <0.010 <0.010

E2‐6



Appendix E2


Units







PL4931 PL4946 PL4947 PL4932 PL4945 PL4957 PL4958 PL4961 PL4918 PL5140 PL5138 PL5139 PL5141 PL4845 PL5133 PL5135 PL5136 PL5132 PL48462016/08/31 17:30 2016/08/31 17:30 2016/08/31 17:30 2016/08/31 17:30 2016/08/31 17:30 2016/09/02 13:30 2016/09/02 13:30 2016/09/02 13:30 2016/09/02 13:30 2016/09/01 11:30 2016/09/01 11:30 2016/09/01 11:30 2016/09/01 11:30 2016/08/31 2016/09/01 09:30 2016/09/01 09:30 2016/09/01 09:30 2016/09/01 09:30 2016/08/31

503355-17-01 503355-18-01 503355-18-01 503355-17-01 503355-18-01 503355-35-01 503355-35-01 503355-35-01 503355-36-01 503355-22-01 503355-22-01 503355-22-01 503355-23-01 503355-15-01 503355-21-01 503355-22-01 503355-22-01 503355-21-01 503355-15-01

DAS-W-16-A-0.2 DAS-W-16-A-0.6AS-W-16-A-0.6 Lab-D DAS-W-16-A-1.0 DAS-W-16-B DAS-W-16-C DAS-W-17-A-0.2 DAS-W-17-A-0.6 DAS-W-17-A-1.0 DAS-W-17-B DAS-W-18-A-0.2 DAS-W-18-A-0.6 DAS-W-18-A-1.0 DAS-W-18-B DAS-W-19 G1 DAS-W-19-A-0.2 DAS-W-19-A-0.6 DAS-W-19-A-1.0 DAS-W-19-B DAS-W-19-B Lab-Du DAS-W-19-G2

26 24 24 28 - 26 - - - 20 21 27 27 - 28 31 27 22 34

76.7 27.2 24.4 31.9 49.7 78.3 71.2 68.1 75.5 89.3 82.2 69 66.1 - 71.1 61.9 73.6 80.3 -23.4 72.8 75.6 68.1 50.3 21.8 28.8 31.9 24.5 10.7 17.8 31.1 33.9 - 28.9 38.1 26.4 19.7 -

8.34 8.43 8.42 8.51 8.42 8.32 8.32 8.24 8.46 8.08 8.28 8.27 8.29 8.21 8.14 8.04 8.33 8.29 8.14

11000 13100 14500 15600 13900 10200 12500 13700 10600 8850 10300 11800 12300 12000 10700 13700 10600 8970 115000.22 0.23 0.28 0.3 0.37 0.25 0.59 0.25 0.19 0.3 0.32 0.27 0.2 0.29 0.26 0.68 0.26 0.18 0.314.88 5.11 4.95 5.33 6.65 4.7 6.04 6.04 5.22 4.56 3.56 4.53 5.55 4.43 5.08 7.69 5.54 4.8 5.536.4 41.6 50.1 56.8 44.1 32.7 43.6 38 32.1 24.4 29.5 37.1 35.6 39.3 42.2 60 30.1 25.4 39.9

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40<0.10 <0.10 <0.10 0.1 0.13 <0.10 0.16 <0.10 <0.10 <0.10 <0.10 0.1 <0.10 0.1 0.11 0.29 <0.10 <0.10 0.13

0.3 0.464 0.465 0.44 0.596 0.322 0.498 0.37 0.346 0.279 0.298 0.35 0.325 0.332 0.383 0.707 0.327 0.265 0.33610400 15000 14700 14800 13900 10000 9180 7480 9160 10000 13200 13100 8160 10200 11300 9140 9540 18100 1240023.9 22.5 25.4 26.1 26.2 16.7 20.1 22.7 21.6 20 20.3 20.9 41.2 21.4 23.3 28.6 20.4 21 21.57.47 8.13 9.1 10.1 9.37 6.28 7.44 8.54 7.73 5.57 5.85 7.43 8.2 7.72 6.9 8.39 7.7 7.27 7.7929.8 22.5 27.1 31.6 30.3 32.6 51.5 20.4 16.6 31.7 49.2 24.5 20 34.1 41.9 73.4 20.7 13.3 43.8

21600 22300 24000 25000 24900 18700 21700 22900 20800 18800 22200 21000 22400 20600 21300 23200 19600 18100 2080021.4 4.62 5.15 6.02 12.9 8.54 20.8 5.66 3.81 6.43 11.9 9.85 4.51 7.76 9.56 34.1 8.83 3.54 11.813.4 13.9 15.3 17.2 18.8 12.3 16.2 18.6 16.3 11 13.9 17.5 18.4 14 13.6 17 14.3 12.8 14.26080 6860 7830 8740 7790 5310 6220 6930 6020 4690 4970 5840 6740 6750 5700 7050 5930 5200 7070226 259 287 316 258 198 215 229 206 193 194 205 219 245 207 228 189 175 230

<0.050 <0.050 <0.050 <0.050 0.073 <0.050 0.541 (9) 0.055 <0.050 <0.050 <0.050 0.061 <0.050 0.058 <0.050 0.2 <0.050 <0.050 0.10.65 1.15 1.23 1.36 1.98 0.65 1.76 1.53 0.94 0.69 1.24 1.48 1.11 0.75 0.77 2.32 1.24 0.92 0.9614.8 16.1 18.2 20.1 21.6 12.8 15.9 17.8 15.4 9.58 10.3 15 18.2 15.5 14.1 21.2 15.1 13.9 18.8477 576 585 567 491 437 437 425 348 398 393 407 416 527 486 510 366 354 543

1630 2070 2370 2610 2270 1430 1720 2000 1750 1140 1350 1680 1920 1780 1560 1960 1790 1600 1800<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.500.105 0.079 0.111 0.129 0.19 0.117 0.292 0.076 0.059 0.116 0.147 0.179 0.074 0.12 0.143 0.486 0.08 0.056 0.143700 4490 4680 5160 5060 3900 3950 4350 3530 2630 3310 3650 3190 4160 3200 4660 4240 3430 480054.5 86 87.7 87.8 75.8 54.3 61.5 47.5 48.3 45 66.3 79.3 46.4 57.8 60.8 68.4 53.4 86.7 70.6

0.131 0.124 0.113 0.111 0.096 0.122 0.137 0.158 0.159 0.091 0.083 0.113 0.139 0.11 0.137 0.152 0.165 0.164 0.1690.46 0.29 0.33 0.38 0.94 0.48 1.42 0.36 0.23 0.44 0.66 0.6 0.25 0.46 0.58 4.32 0.3 0.18 3.42752 923 1040 1040 835 655 776 873 729 587 712 687 760 754 651 788 648 572 643

0.711 1.36 1.33 1.35 1.49 0.617 1.16 1.32 0.862 0.531 0.848 1.09 1.01 0.873 1.53 1.37 0.939 0.902 0.81259.4 62.2 63.6 65.6 64.4 50.1 62.8 60.1 53.6 51.3 76.9 60.4 58.5 52.9 57.1 59.5 49.1 44.8 47.349.7 43.6 51.9 58.4 64.2 49.5 77.6 48.5 41.6 43 48 50.7 47 54.8 57 93.5 42.3 36.6 62.82.56 4.36 4.68 4.88 5.58 2 3.34 3.81 3.41 1.81 2.38 3.15 3.78 2.75 2.65 4.29 3 2.71 2.21

<0.0050 (1) 0.0017 0.0021 0.0025 0.018 (1) 0.020 (1) 0.037 0.0063 <0.0010 0.0065 0.011 (7) 0.02 <0.0010 0.010 (1) 0.0029 0.086 (1) 0.004 <0.0010 0.013<0.0050 (1) <0.0010 0.0016 0.0018 <0.0050 (1) 0.0086 (1) 0.015 0.0032 <0.0010 0.0065 0.0067 0.0079 <0.0010 0.0096 (1) 0.0018 0.023 (1) 0.0023 <0.0010 0.00850.0046 (1) 0.00065 0.00092 0.00097 0.0046 (1) 0.0026 (1) 0.019 0.0036 <0.00050 0.0021 0.0073 0.0078 <0.00050 0.0037 (1) 0.0011 0.038 (1) 0.0028 <0.00050 0.00640.0026 (1) <0.00050 <0.00050 0.0015 <0.0025 (1) 0.023 (1) 0.026 0.0019 <0.00050 0.0015 0.014 0.0025 <0.00050 0.0034 (1) <0.00050 0.014 (1) 0.0011 <0.00050 0.0038

<0.0050 (1) <0.0010 <0.0010 0.0021 <0.0050 (1) 0.0072 (1) 0.025 0.0021 <0.0010 0.0034 0.012 0.004 <0.0010 0.0064 (1) <0.0010 0.024 (1) 0.0012 <0.0010 0.00840.018 (1) 0.0029 0.0033 0.014 0.019 (1) 0.025 (1) 0.13 0.0085 0.0011 0.012 0.065 0.023 0.0016 0.027 (1) 0.0021 0.15 (1) 0.0056 0.0026 0.0410.011 (1) 0.0041 0.0038 0.0073 0.0073 (1) 0.011 (1) 0.062 0.0058 0.002 0.009 0.033 0.014 0.0022 0.010 (1) 0.0023 0.052 (1) 0.0061 0.0021 0.030.045 (1) 0.0031 0.0037 0.024 0.031 (1) 0.069 (1) 0.22 0.013 <0.0010 0.027 0.10 (7) 0.034 0.0011 0.058 (1) 0.0025 0.26 (1) 0.011 0.0021 0.0660.052 (1) 0.01 0.0086 0.033 0.092 (1) 0.095 (1) 0.27 0.013 <0.0010 0.039 0.2 0.052 0.0012 0.070 (1) 0.0025 0.36 (1) 0.015 0.0027 0.070.021 (1) <0.0010 0.0015 0.0091 0.011 (1) 0.054 (1) 0.081 0.0054 <0.0010 0.012 0.048 0.01 <0.0010 0.023 (1) <0.0010 0.11 (1) 0.0041 <0.0010 0.0390.026 (1) 0.0017 0.0023 0.011 0.015 (1) 0.070 (1) 0.1 0.0063 <0.0010 0.014 0.057 0.013 <0.0010 0.032 (1) 0.0015 0.14 (1) 0.0052 0.0013 0.0610.039 (1) 0.0029 0.0037 0.014 0.024 (1) 0.12 (1) 0.14 0.0081 <0.0010 0.023 0.083 0.024 <0.0010 0.045 (1) 0.0012 0.29 (1) 0.0098 <0.0010 0.060.014 (1) <0.0010 0.0011 0.0051 0.0075 (1) 0.045 (1) 0.051 0.0029 <0.0010 0.0084 0.033 0.0078 <0.0010 0.014 (1) <0.0010 0.088 (1) 0.0039 <0.0010 0.0210.026 (1) 0.0013 0.002 0.0097 0.015 (1) 0.11 (1) 0.099 0.0057 <0.0010 0.013 0.059 0.014 <0.0010 0.027 (1) 0.0014 0.22 (1) 0.0063 <0.0010 0.0380.014 (1) <0.0020 <0.0020 0.0046 <0.010 (1) 0.057 (1) 0.054 0.003 <0.0020 0.0074 0.029 0.0078 <0.0020 0.014 (1) <0.0020 0.093 (1) 0.0037 <0.0020 0.019

0.0043 (1) <0.00050 <0.00050 0.0014 <0.0025 (1) 0.017 (1) 0.015 0.00083 <0.00050 0.0018 0.0092 (7) 0.0022 <0.00050 0.0037 (1) <0.00050 0.033 (1) 0.00096 <0.00050 0.00580.018 (1) <0.0020 <0.0020 0.0061 <0.010 (1) 0.062 (1) 0.07 0.0044 <0.0020 0.0091 0.034 0.012 <0.0020 0.018 (1) <0.0020 0.16 (1) 0.0052 <0.0020 0.024

0.036 0.0093 0.012 0.03 0.048 0.098 0.31 0.031 0.0031 0.041 0.15 0.079 0.0038 0.071 0.01 0.39 0.023 0.0046 0.110.17 0.017 0.018 0.088 0.16 0.41 0.79 0.044 <0.0010 0.11 0.47 0.13 0.0023 0.21 0.0079 1.1 0.042 0.0061 0.280.21 0.026 0.03 0.12 0.21 0.51 1.1 0.076 0.0031 0.15 0.62 0.2 0.0061 0.28 0.018 1.5 0.065 0.011 0.390.5 <0.10 <0.10 0.19 0.28 1.7 1.8 0.11 <0.10 0.29 1.1 0.28 <0.10 0.55 <0.10 3.6 0.12 <0.10 0.79

<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020

E2‐7



Appendix E2


Units







PL4966 PL4967 PL4968 PL4955 PL4969 PL5086 PL5087 PL5088 PL5079 PL4844 PL4847 PL5119 PL5120 PL5121 PL5123 PL51242016/09/02 12:30 2016/09/02 12:30 2016/09/02 12:30 2016/09/02 12:30 2016/09/02 12:30 2016/09/01 13:15 2016/09/01 13:15 2016/09/01 13:15 2016/09/01 13:15 2016/08/31 2016/08/29 2016/09/01 10:00 2016/09/01 10:00 2016/09/01 10:00 2016/09/01 10:00 2016/09/01 10:00

503355-34-01 503355-34-01 503355-34-01 503355-35-01 503355-34-01 503355-26-01 503355-26-01 503355-26-01 503355-27-01 503355-15-01 503355-15-01 503355-20-01 503355-20-01 503355-20-01 503355-21-01 503355-21-01

DAS-W-20-A-0.2 DAS-W-20-A-0.6 DAS-W-20-A-1.0 DAS-W-20-B DAS-W-20-C DAS-W-21-A-0.2 DAS-W-21-A-0.6 DAS-W-21-A-1.0 DAS-W-21-B DAS-W-22 G1 DAS-W-22 G1 DAS-W-22 G2 DAS-W-22-A-0.2 DAS-W-22-A-0.6 DAS-W-22-A-1.0 DAS-W-22-B DAS-W-22-C

23 - - 29 - 20 29 28 27 28 17 29 28 26 30 24

64.5 46.4 43 42.8 56.5 95.2 69.9 61.1 72.8 - - 63.8 37.7 22.2 56.1 78.435.5 53.6 57.1 57.2 43.5 4.76 30.2 38.9 27.3 - - 36.3 62.3 77.8 43.9 21.6

8.26 8.34 8.24 8.41 8.39 8.49 8.25 8.22 8.3 8.16 8.51 8.12 8.2 8.32 8.38 8.35

11000 15300 17400 16900 14300 8260 12800 13100 12400 9140 10600 12300 15200 13300 13100 96600.34 0.35 0.44 0.36 0.41 0.12 0.79 0.26 0.2 0.23 2.4 0.33 0.33 0.25 0.49 0.25.45 6.64 8.87 6.9 5.29 5.25 5.83 6.41 4.89 5.24 5.5 5.29 6.1 5.46 6.43 5.1737.2 41.3 48.8 47.3 47.2 21.5 49.5 38.2 35.1 43.4 42.9 41.8 48.4 45.5 48.7 26

<0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.40 <0.400.16 <0.10 0.13 0.11 0.13 <0.10 0.21 <0.10 <0.10 <0.10 0.22 0.11 0.1 <0.10 0.2 <0.10

0.401 0.536 0.587 0.554 0.544 0.163 0.713 0.435 0.392 0.301 0.573 0.35 0.516 0.36 0.565 0.2867560 13400 12400 11700 10500 12300 15900 8260 9470 10500 39700 10800 13700 7790 10000 1040017.8 24.5 28.9 26.9 23.6 17.5 25.5 23 22 20.6 21.7 21.6 31.5 22.6 29.1 21.56.64 9.63 11.5 10.4 8.56 5.25 7.44 8.44 8 6.84 6.18 8.1 9.86 7.84 8.96 7.4450.6 25 30.2 27.9 58.2 16.1 41 23.3 17.9 32.5 65.2 41.2 28.6 24.5 43.5 14.1

19600 25500 28600 27000 24000 21200 24600 22500 22200 20100 24300 21900 25200 21500 22300 1890041.1 5.89 6.73 6.59 16.8 5.28 34.8 5.16 4.08 8.25 40.5 9.68 6.64 4.51 19.2 3.7413.7 18.7 24.7 21.8 17.8 11.5 17.3 20 17.9 12.8 14.2 14.3 18.1 14.1 16.3 13.55700 7870 9660 8980 7290 4350 6540 6900 6310 5220 5930 7090 8230 6800 7120 5420198 256 307 289 260 183 225 232 218 199 218 242 278 260 236 183

0.084 <0.050 <0.050 <0.050 0.068 <0.050 0.184 <0.050 <0.050 0.074 0.195 <0.050 <0.050 <0.050 0.118 <0.0500.85 1.67 2.09 1.6 1.67 0.55 1.99 1.36 1.13 0.56 1 0.78 1.47 1.4 1.46 0.9215 21.6 27.2 23.6 19.7 6.36 18.1 18.5 16.5 13.2 13.8 17.5 22.2 17.7 20 13.8509 486 535 533 513 373 454 411 391 484 554 575 536 550 495 327

1570 2420 2790 2680 2110 941 1750 2080 1930 1380 1510 1920 2420 2160 2020 1670<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.500.246 0.09 0.14 0.134 0.185 <0.050 0.55 0.089 0.051 0.133 0.377 0.145 0.123 0.116 0.29 0.0575040 5120 5760 5280 4060 2290 4530 4500 3390 3650 4720 4940 4960 4090 4080 314047.7 71.5 67.7 66.4 61 61 90.2 49.4 51.9 59.9 255 63.4 71.9 50.9 60.1 51.3

0.134 0.159 0.131 0.129 0.108 0.061 0.102 0.135 0.143 0.146 0.102 0.121 0.136 0.119 0.14 0.1660.99 0.28 0.39 0.38 0.86 0.33 4.43 0.25 0.27 0.5 2.52 0.61 0.47 0.34 1.44 0.19676 894 1020 989 827 555 808 825 801 562 576 731 917 901 759 596

0.713 1.6 1.9 1.58 1.2 0.374 1.19 1.16 3.4 0.533 0.76 0.865 1.59 1.35 1.35 0.75351.6 62.7 71.1 66.1 64.8 74.5 77.3 57.5 59.2 51.4 55.7 55.5 63.1 58.5 55.1 47.362.9 54.7 65.4 61.7 74.9 31 87.7 51.7 44.8 50.4 97.4 63.7 58.3 50 74.5 37.82.88 5.64 7.43 6.16 4.45 0.94 3.4 4.36 3.99 2 2.29 2.86 5.78 3.86 3.94 2.63

0.012 (1) 0.0017 <0.0010 0.0018 0.035 (1) 0.0019 0.052 (1) <0.0010 <0.0010 <0.0050 (1) 0.029 (1) 0.0079 0.002 0.0074 0.035 <0.00100.0068 (1) <0.0010 0.0012 0.0015 0.023 (1) 0.0018 0.019 (1) 0.0014 <0.0010 <0.0050 (1) 0.011 (1) 0.0069 0.0014 0.0023 0.013 <0.00100.0083 (1) 0.0013 <0.00050 0.0017 0.013 (1) 0.00088 0.018 (1) <0.00050 <0.00050 0.0042 (1) 0.018 (1) 0.0038 0.0011 0.0015 0.018 <0.000500.0068 (1) <0.00050 <0.00050 <0.00050 0.013 (1) 0.00088 0.0098 (1) <0.00050 <0.00050 0.0040 (1) 0.015 (1) 0.0023 <0.00050 <0.00050 0.0098 <0.000500.0091 (1) <0.0010 <0.0010 0.0013 0.022 (1) 0.0014 0.016 (1) <0.0010 <0.0010 0.0057 (1) 0.028 (1) 0.0038 <0.0010 <0.0010 0.014 <0.00100.056 (1) 0.0036 0.0016 0.0037 0.11 (1) 0.0064 0.082 (1) 0.0017 (6) <0.0010 0.025 (1) 0.12 (1) 0.019 0.0029 0.0054 0.062 <0.00100.024 (1) 0.0042 0.0023 0.0046 0.067 (1) 0.004 0.032 (1) 0.0037 0.0017 0.017 (1) 0.096 (1) 0.013 0.0048 0.0038 0.042 0.0020.10 (1) 0.0073 <0.0010 0.0069 0.13 (1) 0.0093 0.14 (1) 0.0014 <0.0010 0.059 (1) 0.24 (1) 0.047 0.0049 0.0051 0.11 <0.00100.13 (1) 0.013 0.002 0.025 0.29 (1) 0.011 0.21 (1) 0.0018 <0.0010 0.068 (1) 0.42 (1) 0.051 0.01 0.016 0.17 <0.00100.041 (1) 0.0044 <0.0010 0.0021 0.091 (1) 0.0034 0.052 (1) <0.0010 <0.0010 0.023 (1) 0.22 (1) 0.019 0.002 0.008 0.038 <0.00100.055 (1) 0.0061 0.0012 0.0035 0.15 (1) 0.0043 0.065 (1) 0.0011 <0.0010 0.029 (1) 0.28 (1) 0.024 0.0029 0.0054 0.047 <0.00100.085 (1) 0.0058 <0.0010 0.0056 0.14 (1) 0.0076 0.11 (1) <0.0010 <0.0010 0.046 (1) 0.33 (1) 0.032 0.005 0.014 0.079 <0.00100.027 (1) 0.0021 <0.0010 0.0017 0.049 (1) 0.0025 0.037 (1) <0.0010 <0.0010 0.014 (1) 0.12 (1) 0.013 0.0015 0.0047 0.029 <0.00100.052 (1) 0.0037 <0.0010 0.003 0.089 (1) 0.0046 0.076 (1) <0.0010 <0.0010 0.029 (1) 0.22 (1) 0.021 0.0029 0.009 0.055 <0.00100.031 (1) <0.0020 <0.0020 0.0021 0.046 (1) 0.0023 0.040 (1) <0.0020 <0.0020 0.017 (1) 0.085 (1) 0.012 <0.0020 0.0031 0.033 <0.0020

0.0082 (1) <0.00050 <0.00050 0.00056 0.013 (1) 0.00063 0.010 (1) <0.00050 <0.00050 0.0046 (1) 0.027 (1) 0.0033 <0.00050 0.0007 0.0093 <0.000500.039 (1) 0.0026 <0.0020 0.0039 0.054 (1) 0.0029 0.054 (1) <0.0020 <0.0020 0.022 (1) 0.095 (1) 0.016 0.0027 0.0042 0.046 <0.0020

0.12 0.011 0.0051 0.015 0.29 0.017 0.23 0.0068 0.0017 0.056 0.31 0.056 0.012 0.02 0.19 0.0020.39 0.034 0.0032 0.041 0.76 0.033 0.55 0.0043 <0.0010 0.21 1.4 0.17 0.023 0.044 0.43 <0.00100.51 0.045 0.0083 0.056 1 0.051 0.78 0.011 0.0017 0.27 1.7 0.22 0.035 0.064 0.62 0.002

1 <0.10 <0.10 <0.10 1.9 <0.10 1.4 <0.10 <0.10 0.57 4.4 0.43 <0.10 0.18 1 <0.10

<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010<0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 <0.020 <0.010 <0.010 <0.010 <0.010 <0.010

E2‐8

Appendix E3Pore Water Chemistry Laboratory Results

Table E3-1: Results of Pore Water Chemical Analysis

Vancouver Fraser Port AuthorityCenterm Expansion Project / South Shore Access Project Environmental Studies

Appendix E3

E3-1

Sample ID Guideline Guideline DUP-1 DUP-2 ESED2-0.5 ESED2-1.0 ESED3-0.5 ESED3-1.0 ESED3-0.5B ESED3-1.0B ESED6-0.5 ESED6-1.0 ESED7-0.5 ESED7-1.0 ESED8-0.5 ESED8-1.0 ESED9-0.5 ESED9-10 ESED9-0.5B ESED9-1.0B ESED10-0.5Laboratory ID / Guideline ID CCME BC AWQG OD0216 OD0217 NZ6041 NZ6038 NZ6035 NZ6042 NZ6036 NZ6037 OD0242 OD0243 NZ4443 NZ4384 OD0244 OD0245 NZ4439 NZ4440 NZ6039 NZ6040 NZ4388

Maxxam Job # Aquatic Life - Marine Marine B611527 B611527 B604958 B604958 B604958 B604958 B604958 B604958 B611527 B611527 B604597 B604597 B611527 B611527 B604597 B604597 B604958 B604958 B604597Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L

Sampling Date 2016/02/16 2016/02/16 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/01/21 2016/02/16 2016/02/16 2016/01/20 2016/01/20 2016/02/16 2016/02/16 2016/01/20 2016/01/20 2016/01/21 2016/01/21 2016/01/20Aluminum (Dissolved) 13,16 1.00E+34 1.00E+34 10 45 10 12 <10 <10 <10 <10 11 11 13 12 <10Antimony (Dissolved) 1.00E+34 1.00E+34 0.5 7.13 1.39 <0.50 1.79 <0.50 0.84 1.13 <0.50 <0.50 <0.50 <0.50 1.41Arsenic (Dissolved) 12.5 12.5 0.5 10.8 9.47 0.93 3.39 1.02 3.45 7.28 1.04 1.72 0.55 2.41 2.13Barium (Dissolved) 1.00E+34 1.00E+34 1 619 18 21.1 21.9 32.4 23.3 29.3 16.6 75.3 167 303 82.6Beryllium (Dissolved) 1.00E+34 1.00E+34 1 0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Boron (Dissolved) 6,14 1.00E+34 1200 50 3530 2480 3120 2950 3170 3280 2900 2830 2590 3020 3290 2070Cadmium (Dissolved) 7,14 0.12 0.12 0.05 0.078 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050Calcium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 378 258 344 313 321 316 328 326 289 271 273 163Chromium (Dissolved) 1.00E+34 1.00E+34 0.5 1.23 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.85 0.6 <0.50 <0.50Cobalt (Dissolved) 1.00E+34 1.00E+34 0.1 0.72 0.52 0.11 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10Copper (Dissolved) 7,8,13,14,15 1.00E+34 3 0.5 1.63 1.63 1.49 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50Iron (Dissolved) 8 1.00E+34 350 2 746 9.1 20.6 <2.0 13.3 17 17.5 746 5.2 9.1 <2.0 8.9Lead (Dissolved) 7,13 1.00E+34 140 0.1 0.58 0.33 <0.10 <0.10 0.17 <0.10 0.16 <0.10 <0.10 <0.10 <0.10 <0.10Lithium (Dissolved) 12 1.00E+34 1.00E+34 20 154 99 142 120 129 127 137 138 103 114 110 75Magnesium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 1140 835 1030 956 1030 961 1040 989 961 945 885 506Manganese (Dissolved) 8 1.00E+34 1.00E+34 0.5 381 61.5 4.18 19 98.4 381 46.5 41.2 <0.50 0.93 <0.50 4.03Mercury (Dissolved) 0.016 0.02 0.3 0 <0.30 <0.30 <0.30 <0.30 <0.30Molybdenum (Dissolved) 9 1.00E+34 1.00E+34 1 13.1 6.7 <1.0 9.8 2.4 5.5 9.9 5.6 2.3 1.6 3.3 13.1Nickel (Dissolved) 7,13 1.00E+34 1.00E+34 0.2 3.75 3.75 1.49 0.65 0.82 1.33 0.71 0.46 0.64 0.5 0.48 <0.20Selenium (Dissolved) 10 1.00E+34 2 0.5 2.46 0.78 0.84 <0.50 <0.50 <0.50 0.58 0.79 0.9 1.41 <0.50 <0.50Silver (Dissolved) 7 7.5 3 0.05 0 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050Sodium (Dissolved) (mg/L) 8 1.00E+34 1E+34 1 9040 6790 8320 7760 8400 7740 8290 8060 7740 7940 7480 4190Thallium (Dissolved) 1.00E+34 1E+34 0.1 0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10Titanium (Dissolved) 1.00E+34 1E+34 10 0 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10Uranium (Dissolved) 1.00E+34 1E+34 0.05 5.1 3.76 0.64 5.1 1.11 2.65 2.05 1.42 1.33 0.763 4.5 2.78Vanadium (Dissolved) 1.00E+34 1E+34 10 14 14 <10 <10 <10 <10 <10 <10 <10 <10 <10 11Zinc (Dissolved) 7,8,11 1.00E+34 10 1 7.2 1.9 <1.0 2.6 1.4 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 1.6Acenaphthene 1.00E+34 6 0.05 6.4 0.6 1.2 <0.050 0.26 0.1 <0.050 <0.10 0.075 0.42 6.4 1.1 2.6 <0.050Acridine 1.00E+34 1E+34 0.05 1.8 0.24 0.46 <0.050 <0.050 <0.050 <0.050 <0.10 <0.050 0.34 1.8 0.45 0.96 <0.050Anthracene 1.00E+34 1E+34 0.01 19 2.4 2.4 0.068 0.6 0.18 0.039 0.31 0.51 1.4 19 2.5 5.9 <0.010Benzo(a)anthracene 1.00E+34 1E+34 0.01 43 5.5 4.9 0.19 0.63 0.4 0.082 0.85 0.45 3.2 43 4 15 <0.010Benzo(a)pyrene (a) 1.00E+34 0.01 0.009 51 6.4 5.8 0.3 0.77 0.72 0.17 1.3 0.53 6.5 51 4.7 18 0.012Chrysene (b) 1.00E+34 0.1 0.05 60 6.7 6.6 0.23 0.72 0.58 0.11 1.1 0.56 3.5 60 5 19 <0.050Fluoranthene 1.00E+34 1E+34 0.02 100 12 13 0.39 0.99 0.62 0.17 1.8 1.7 7 100 6.3 34 0.021Fluorene 1.00E+34 12 0.05 8.7 0.88 1.3 <0.050 0.41 0.089 <0.050 0.12 0.13 0.47 8.7 1.2 3.4 <0.050Naphthalene 1.4 1 0.1 8.8 <0.40 0.92 <0.10 0.88 <0.10 <0.10 <0.20 <0.10 0.44 8.8 0.82 1.8 <0.10Phenanthrene 1.00E+34 1E+34 0.05 48 6.6 8.7 0.19 1.5 0.51 0.073 0.81 0.77 4.1 48 6.7 25 <0.050Pyrene 1.00E+34 1E+34 0.02 140 13 17 0.46 1.4 1.1 0.6 2.8 1.5 12 140 14 56 0.025Quinoline 1.00E+34 1E+34 0.24 0 <0.96 <0.96 <0.24 <0.24 <0.24 <0.24 <0.48 <0.24 <0.48 <4.8 <0.48 <1.2 <0.24

Notes:

Maximum Reported

Concentration

Reporting Limit

a Concentrations of benzo(a)pyrene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values censored at the solubility limit of 3.8 µ g/L at 25 C b Concentrations of chrysene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values censored at the solubility limit of 1.9 µ g/L at 25 C

Reporting limit exceeds applicable guideline.

Value Exceeds CCME Water Quality Guidelines for Protection of Marine Aquatic Life

Value Exceeds BC Ambient Water Quality Guidelines for Protection of Marine Aquatic Life

Red Shaded

Yellow Shaded

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Appendix E3

E3-2

Sample ID Guideline GuidelineLaboratory ID / Guideline ID CCME BC AWQG

Maxxam Job # Aquatic Life - Marine MarineUnits ug/L ug/L ug/L

Sampling Date Aluminum (Dissolved) 13,16 1.00E+34 1.00E+34 10 45Antimony (Dissolved) 1.00E+34 1.00E+34 0.5 7.13Arsenic (Dissolved) 12.5 12.5 0.5 10.8Barium (Dissolved) 1.00E+34 1.00E+34 1 619Beryllium (Dissolved) 1.00E+34 1.00E+34 1 0Boron (Dissolved) 6,14 1.00E+34 1200 50 3530Cadmium (Dissolved) 7,14 0.12 0.12 0.05 0.078Calcium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 378Chromium (Dissolved) 1.00E+34 1.00E+34 0.5 1.23Cobalt (Dissolved) 1.00E+34 1.00E+34 0.1 0.72Copper (Dissolved) 7,8,13,14,15 1.00E+34 3 0.5 1.63Iron (Dissolved) 8 1.00E+34 350 2 746Lead (Dissolved) 7,13 1.00E+34 140 0.1 0.58Lithium (Dissolved) 12 1.00E+34 1.00E+34 20 154Magnesium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 1140Manganese (Dissolved) 8 1.00E+34 1.00E+34 0.5 381Mercury (Dissolved) 0.016 0.02 0.3 0Molybdenum (Dissolved) 9 1.00E+34 1.00E+34 1 13.1Nickel (Dissolved) 7,13 1.00E+34 1.00E+34 0.2 3.75Selenium (Dissolved) 10 1.00E+34 2 0.5 2.46Silver (Dissolved) 7 7.5 3 0.05 0Sodium (Dissolved) (mg/L) 8 1.00E+34 1E+34 1 9040Thallium (Dissolved) 1.00E+34 1E+34 0.1 0Titanium (Dissolved) 1.00E+34 1E+34 10 0Uranium (Dissolved) 1.00E+34 1E+34 0.05 5.1Vanadium (Dissolved) 1.00E+34 1E+34 10 14Zinc (Dissolved) 7,8,11 1.00E+34 10 1 7.2Acenaphthene 1.00E+34 6 0.05 6.4Acridine 1.00E+34 1E+34 0.05 1.8Anthracene 1.00E+34 1E+34 0.01 19Benzo(a)anthracene 1.00E+34 1E+34 0.01 43Benzo(a)pyrene (a) 1.00E+34 0.01 0.009 51Chrysene (b) 1.00E+34 0.1 0.05 60Fluoranthene 1.00E+34 1E+34 0.02 100Fluorene 1.00E+34 12 0.05 8.7Naphthalene 1.4 1 0.1 8.8Phenanthrene 1.00E+34 1E+34 0.05 48Pyrene 1.00E+34 1E+34 0.02 140Quinoline 1.00E+34 1E+34 0.24 0

Notes:

Maximum Reported

Concentration

Reporting Limit





Red Shaded

Yellow Shaded

Blue Shaded

ESED10-1.0 PWEB-1 PWEB-2 RSED1-0.5 RSED1-1.0 RSED2-0.5 RSED2-1.0 RSED3-0.5 RSED3-1.0 RSED4-0.5 RSED4-1.0 WSED1-0.5 WSED1-1.0 WSED2-0.5 WSED2-1.0 WSED3-0.5 WSED3-1.0 WSED4-0.5 WSED4-1.0 WSED5-0.5NZ4389 NZ4438 NZ6034 OD0236 OD0237 NZ2080 NZ2095 NZ2086 NZ2097 NZ6043 NZ5978 OD0240 OD0241 OD0238 OD0239 OD0234 OD0235 OD0232 OD0233 OD0230B604597 B604597 B604958 B611527 B611527 B604169 B604169 B604169 B604169 B604958 B604958 B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527

ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L2016/01/20 2016/01/20 2016/01/21 2016/02/16 2016/02/16 2016/01/19 2016/01/19 2016/01/19 2016/01/19 2016/01/21 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16

<10 <10 <10 10 45 <10 11 13 <10 <10 <10 10 11<0.50 7.13 1.06 0.51 <0.50 <0.50 <0.50 1.1 <0.50 <0.50 <0.50 <0.50 <0.50<0.50 4.71 3.59 1.21 2.68 1.34 1.96 0.81 1.27 1 <0.50 <0.50 1.67<1.0 575 619 31 18.3 14.6 11.2 17.9 17.3 14.5 13.9 15.1 15.6<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<50 2530 2510 3530 3140 2610 2650 2850 2920 2940 3000 2900 3030

<0.050 <0.050 <0.050 <0.050 <0.050 <0.050 0.065 <0.050 <0.050 <0.050 <0.050 <0.050 0.078<1.0 286 208 317 332 290 306 339 338 331 332 328 346

<0.50 0.83 1.23 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50<0.10 0.5 0.72 0.39 <0.10 0.16 0.11 0.28 0.25 0.17 <0.10 <0.10 0.23<0.50 1.1 1.12 <0.50 <0.50 0.51 0.87 <0.50 0.97 0.94 0.91 0.91 1.23

3.6 33.1 33 2.3 26.9 441 <2.0 89.7 32.6 218 13.3 79.4 4.8<0.10 <0.10 <0.10 0.58 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10<20 98 92 135 151 126 144 133 137 134 132 141 148<1.0 878 904 998 1020 871 961 942 1010 1020 980 1040 1050

<0.50 2.75 30.7 50.7 39.2 52.1 4.93 63 36.7 30.8 39.4 47.4 28.7<0.30 <0.30<1.0 <1.0 <1.0 7.1 6.6 5.4 7.2 10.9 8.1 6.4 9.2 8.9 9.2

<0.20 1 2.47 1.01 3.62 2.38 1.44 1.69 1.2 0.91 0.51 1 1.42<0.50 2.46 1.96 <0.50 <0.50 0.57 <0.50 <0.50 0.74 0.74 0.57 0.51 0.86

<0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.05011.2 7040 7670 8190 8140 7080 7810 7780 8120 8150 7930 8310 8290

<0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10

<0.050 0.309 0.12 1.49 0.933 0.635 1.95 1.8 2.37 1.41 0.837 0.106 2.32<10 <10 <10 13 <10 <10 <10 <10 <10 <10 <10 <10 <107.2 <1.0 <1.0 1.8 <1.0 2.2 3.7 <1.0 3.9 <1.0 <1.0 <1.0 2.1

<0.050 <0.050 <0.050 0.35 3.1 0.97 0.31 <0.10 <0.10 0.094 <0.050 0.065 0.55 0.33 0.11 <0.050 <0.050 <0.050 <0.050 0.25<0.050 <0.050 <0.050 0.36 1.2 0.32 0.12 <0.10 <0.10 <0.050 <0.050 0.16 0.24 0.19 0.079 <0.050 <0.050 <0.050 <0.050 0.11<0.010 <0.010 <0.010 1.2 8.5 2.8 1.2 <0.020 0.059 0.2 0.037 0.76 2.7 1.5 0.9 0.021 <0.010 0.032 <0.010 0.69<0.010 <0.010 <0.010 3.2 19 4.8 2.2 0.02 0.035 0.51 0.12 1.5 4.5 2.3 1.9 0.025 <0.010 0.07 0.013 1.2<0.0090 <0.0090 <0.0090 4.7 18 6.9 3.7 0.035 0.071 0.85 0.16 3.5 8.3 4.3 2.6 0.042 <0.0090 0.088 0.017 1.6<0.050 <0.050 <0.050 4.4 22 6 3.1 <0.10 0.22 0.53 0.16 2.9 7.2 3.8 2.6 <0.050 <0.050 0.073 <0.050 1.5<0.020 <0.020 <0.020 5.2 55 9.4 4.3 0.06 0.093 1.2 0.32 2.2 6.7 3.6 4.1 0.075 <0.020 0.15 0.037 2.6<0.050 <0.050 <0.050 0.47 3.6 1.2 0.32 <0.10 <0.10 0.068 <0.050 0.14 1 0.46 0.26 <0.050 <0.050 <0.050 <0.050 0.34<0.10 <0.10 <0.10 <0.50 1.7 0.58 0.12 <0.20 0.22 <0.10 <0.10 <0.10 0.4 0.29 <0.10 <0.10 <0.10 <0.10 <0.10 0.25

<0.050 <0.050 <0.050 3.3 21 7 2.2 <0.10 0.1 0.64 0.12 0.82 5.9 2.4 1.8 <0.050 <0.050 0.068 <0.050 1.60.021 <0.020 <0.020 28 56 12 6.2 0.1 0.53 1.3 0.41 4.8 10 10 3.5 0.22 0.024 0.16 0.046 2.8<0.24 <0.24 <0.24 <1.2 <1.2 <0.48 <0.24 <0.48 <0.48 <0.24 <0.24 <0.24 <0.24 <0.48 <0.24 <0.24 <0.24 <0.24 <0.24 <0.48



Appendix E3

E3-3

Sample ID Guideline GuidelineLaboratory ID / Guideline ID CCME BC AWQG

Maxxam Job # Aquatic Life - Marine MarineUnits ug/L ug/L ug/L

Sampling Date Aluminum (Dissolved) 13,16 1.00E+34 1.00E+34 10 45Antimony (Dissolved) 1.00E+34 1.00E+34 0.5 7.13Arsenic (Dissolved) 12.5 12.5 0.5 10.8Barium (Dissolved) 1.00E+34 1.00E+34 1 619Beryllium (Dissolved) 1.00E+34 1.00E+34 1 0Boron (Dissolved) 6,14 1.00E+34 1200 50 3530Cadmium (Dissolved) 7,14 0.12 0.12 0.05 0.078Calcium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 378Chromium (Dissolved) 1.00E+34 1.00E+34 0.5 1.23Cobalt (Dissolved) 1.00E+34 1.00E+34 0.1 0.72Copper (Dissolved) 7,8,13,14,15 1.00E+34 3 0.5 1.63Iron (Dissolved) 8 1.00E+34 350 2 746Lead (Dissolved) 7,13 1.00E+34 140 0.1 0.58Lithium (Dissolved) 12 1.00E+34 1.00E+34 20 154Magnesium (Dissolved) (mg/L) 1.00E+34 1.00E+34 1 1140Manganese (Dissolved) 8 1.00E+34 1.00E+34 0.5 381Mercury (Dissolved) 0.016 0.02 0.3 0Molybdenum (Dissolved) 9 1.00E+34 1.00E+34 1 13.1Nickel (Dissolved) 7,13 1.00E+34 1.00E+34 0.2 3.75Selenium (Dissolved) 10 1.00E+34 2 0.5 2.46Silver (Dissolved) 7 7.5 3 0.05 0Sodium (Dissolved) (mg/L) 8 1.00E+34 1E+34 1 9040Thallium (Dissolved) 1.00E+34 1E+34 0.1 0Titanium (Dissolved) 1.00E+34 1E+34 10 0Uranium (Dissolved) 1.00E+34 1E+34 0.05 5.1Vanadium (Dissolved) 1.00E+34 1E+34 10 14Zinc (Dissolved) 7,8,11 1.00E+34 10 1 7.2Acenaphthene 1.00E+34 6 0.05 6.4Acridine 1.00E+34 1E+34 0.05 1.8Anthracene 1.00E+34 1E+34 0.01 19Benzo(a)anthracene 1.00E+34 1E+34 0.01 43Benzo(a)pyrene (a) 1.00E+34 0.01 0.009 51Chrysene (b) 1.00E+34 0.1 0.05 60Fluoranthene 1.00E+34 1E+34 0.02 100Fluorene 1.00E+34 12 0.05 8.7Naphthalene 1.4 1 0.1 8.8Phenanthrene 1.00E+34 1E+34 0.05 48Pyrene 1.00E+34 1E+34 0.02 140Quinoline 1.00E+34 1E+34 0.24 0

Notes:

Maximum Reported

Concentration

Reporting Limit





Red Shaded

Yellow Shaded

Blue Shaded

WSED5-1.0 WSED6-0.5 WSED6-1.0 WSED7-0.5 WSED7-1.0 WSED8-0.5 WSED8-1.0 WSED9-0.5 WSED9-1.0 WSED10-0.5 WSED10-1.0OD0231 OD0212 OD0213 OD0208 OD0209 OD0210 OD0211 OD0214 OD0215 OD0228 OD0229B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527 B611527

ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16 2016/02/16

10 <10 11 13 11 10 10 16 16 17 11<0.50 <0.50 2.26 0.92 1.38 <0.50 <0.50 <0.50 <0.50 <0.50 <0.502.17 1.91 9.69 7.66 10.8 4.46 1.03 <0.50 <0.50 1.51 1.6910.7 11.4 15.3 18.7 17.3 28 22.1 58.1 72.5 14.9 22.8<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.02200 3040 2760 2860 2320 3310 3230 3060 2940 3220 2730

<0.050 0.054 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050237 326 302 339 259 351 354 373 327 378 334

<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.500.41 0.4 0.2 0.33 0.4 <0.10 <0.10 <0.10 <0.10 0.13 0.181.19 1.24 1.13 0.55 1.04 0.96 1.06 1.31 1.43 1.04 1.297.4 4.7 6.9 7.5 10.7 16.3 17.5 41 34.7 10 15.1

<0.10 0.15 0.24 0.27 0.3 <0.10 <0.10 <0.10 <0.10 0.12 0.19101 145 121 132 94 124 154 102 75 149 122728 1000 919 1050 819 1080 1110 1120 1060 1140 100051.6 57.7 53.3 47.8 58.7 9.51 2.21 3.3 3.4 31.2 24.5

7.7 8.3 13 10.2 6.9 1.4 <1.0 <1.0 <1.0 7.7 2.72.83 1.12 1.8 2.83 3.1 0.55 1.82 0.66 0.89 0.96 0.820.6 0.67 0.71 <0.50 <0.50 1.7 1.43 0.75 1.85 <0.50 0.72

<0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 <0.0505880 8100 7410 8300 6690 8600 8780 8970 8540 9040 8050<0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <101.56 2.02 3.62 2.2 4.02 1.3 0.838 0.314 0.138 1.37 0.75<10 <10 <10 <10 14 <10 <10 <10 <10 <10 <10<1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.071 <0.050 <0.050 0.12 0.13 <0.050 <0.050 <0.050 0.093

<0.050 <0.050 <0.050 <0.10 0.1 <0.050 <0.050 <0.050 0.0920.37 <0.010 <0.010 0.36 0.31 <0.010 <0.010 0.045 1.10.84 <0.010 0.024 0.71 0.64 <0.010 <0.010 0.074 1.51.2 0.012 0.031 1 0.9 <0.0090 <0.0090 0.16 2.80.99 <0.050 <0.050 0.97 1.2 <0.050 <0.050 0.086 1.41.1 0.022 0.052 1.7 3.8 <0.020 <0.020 0.16 2.10.12 <0.050 <0.050 0.17 0.15 <0.050 <0.050 <0.050 0.16

<0.10 <0.10 <0.10 <0.20 <0.20 <0.10 <0.10 <0.10 <0.100.75 <0.050 <0.050 0.85 0.56 <0.050 <0.050 0.068 0.81.4 0.039 0.074 1.9 4.9 <0.020 <0.020 0.22 4

<0.24 <0.24 <0.24 <0.48 <0.48 <0.24 <0.24 <0.24 <0.24

Appendix E4Water Column Chemistry

Vancouver Fraser Port Authority Centerm Expansion Project / South Shore Area Environmental Studies

Appendix E4: Marine Water Column Sampling Plan

Appx_2016-11-03_Appendix E4 Water Column-60476505.Docx E4-1

Appendix E4 Marine Water Column Sampling Plan

Marine water samples were collected from 10 locations in the Marine Water and Sediment Quality Study Area on July 14, 2016, to characterize the existing water quality around the Centerm facility (see Figure E4-1 for water sampling locations). Prior to collecting each sample, measurements were taken of physical parameters (e.g., dissolved oxygen, total dissolved solids, temperature, salinity, etc.) to determine whether there was a physical difference in surface water and subsurface water.

At each of the 10 locations, samples were collected using a Teflon-lined Niskin bottle, at three depths:

• near-surface 1 meter below surface; • mid-column midway between the surface and bottom; and, • near-bottom approximately 1 meter above bottom.

Samples were submitted to Maxxam Analytical for analysis of metals (total and dissolved), PAHs, physical properties including total suspended solids, and microbiological parameters.

The field protocol involved the following:

1. Position sampling vessel at proposed stations suing the coordinates and locations shown in Figure E4-1. 2. Record, stations ID, Date, Time, and Water Depth 3. Run the YSI for full depth, recording the profile. 4. Identify whether a thermocline or halocline exists. 5. Record Secchi depth 6. At each station water samples will be collected from three depths intervals, 05 m below surface; mid-column,

and 0,5 m above mudline. For each depth interval conduct the following: a. Arm and rinse Niskin Bottle b. Lower Niskin bottle to desired depth c. Retrieve Niskin Bottle d. Record time of sample retrieval e. Using the pour spout on the bottom, fill each of the required bottles as defined in Table E4-1. f. Fill bottles to be filtered first, so that hydrostatic head forces water through filter cartridges. g. Samples must be kept on ice. h. Discard any excess water i. Rinse Niskin Bottle with DI water

7. Once all samples for each of the three depth intervals has been collected transit to the next sampling location.

Sample containers were organized in such a way that individual samples are held together in a large ziplock bag. Sample bottles for each sample location (i.e., SW-01) were packaged into a dedicated cooler. Pre-labeled bottles were used to aid organization and efficiency while in the field.

Vancouver Fraser Port Authority Centerm Expansion Project / South Shore Area Environmental Studies

Appendix E4: Marine Water Column Sampling Plan

Appx_2016-11-03_Appendix E4 Water Column-60476505.Docx E4-2

Chain of Custody forms were filled out electronically. All samples were delivered on ice in good condition on the day of collection to:

Maxxam Analytics 4606 Canada Way, Burnaby, BC V5G 1K5 Ph: (604) 734-7276 Fax: (604) 731-2386, Toll Free: (800) 665-8566

Table E4-1. Requested Analytes, Required Sample Volumes and Containers, Preservatives, and Hold Times

Parameter Bottles/Sample Collection/Preservation Hold Time NH4, TOC, COD 120 ml Plastic preserved with H2SO4 28 Days Alkalinity, Br, Cl, F, NO2, NO3, SO4, PO4 250 ml Plastic 3 days DOC 120 ml Plastic field filtered with H2SO4 28 days Total Metals 120 ml plastic unfiltered 180 days Dissolved Metals 120 ml Plastic field filtered 180 days PAH 2 x 100 ml Amber glass with Sodium Bisulphate 14 days Fecal, Enteroccus 1 x 250 ml Microbiology bottle with Sodium Thiosulphate 30 hours TSS 1 litre Plastic 7 days BOD 1 litre Plastic 3 days Turbidity 120 ml Plastic 3 days

Note: For multi-parameter samples, the parameters with the shortest hold times (indicated in bold) dictate the hold time for the sample.

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Appendix E5Statistical Analysis of Surficial Sediment

(January 2016) and Pore Water

Vancouver Fraser Port Authority Centerm Expansion Project / South Shore Access Project Environmental Studies

Appendix E5, Statistical Analysis of Marine Sediment and Pore Water

E5-1

Appendix E5 Statistical Analysis of Marine Sediment and Pore Water

This appendix outlines the workflow process for computation of summary statistics, including 95% Upper Confidence Limits of the mean (UCL95) for environmental concentration data with and without non-detect (ND). The UCL95 represents the upper bound of a statistical interval, for a hypothesized population, in which one would expect 95% of all future averages to be below the upper bound. As such, it represents the majority of expected typical concentrations on which to make inferences about the contaminant population of interest (i.e., either sediment or pore water concentrations).Summary statistics were computed using the US Environmental Protection Agency's (USEPA’s) statistical platform ProUCL Version 5.0. This workflow was developed based on a review of relevant literature and guidance delivered by Dr. Dennis Helsel (Helsel 2012b).

E5.1 Methodology

E5.1.1 Uncensored Data Sets

Calculating an upper confidence limit on environmental data that does not have ND values is largely influenced by the number of observations (n) and the skewness of the data. For data sets where the number of observations is less than twenty (n<20) bootstrap re-sampling techniques are unlikely to capture the breadth of the sample population shape and are likely to return inaccurate estimates of the UCL. Under these circumstances, either a normal or gamma distribution is assumed based on the strongest goodness of fit statistic provided by ProUCL (i.e., larger R-squared value). ProUCL does not include suitable methods for computation of 95% UCLs based on lognormal distributions, so non-normal (i.e., skewed) distributions are assumed to resemble a gamma distribution. Based on the selected distribution, the 95% Student’s-t UCL or 95% Adjusted Gamma UCL was carried forward for normal and gamma distributions, respectively.

For data sets without ND values and a sample size of n≥20, bootstrap re-sampling techniques are the best way to compute a UCL95 from skewed data (Helsel 2012b). The Bias Corrected Accelerated (BCA) Bootstrap intervals are recommended for general use, especially for non-parametric problems (Efron and Tibshirani 1994). The BCA bootstrap technique adjusts for skewness and provides a confidence limit of the mean that should exceed the true population mean in 95% of cases (i.e., 95% coverage). Under these circumstances the 95% BCA Bootstrap UCL was used.

E5.1.2 Censored Data Sets

In the past, regulatory guidance in environmental sciences supported the use of substitution methods for handing data below reportable limits of detection (ND values); however, substitution methods have been shown to result in poor estimates and incorrect statistical tests (Helsel 2012a). Substitution methods do not provide adequate coverage for UCLs computed on censored data, even when censoring levels are as low as 10% (Singh et al. 2006). Based on this study, the USEPA has stated that, “it is strongly recommended to avoid the use of the DL/2 method….even when the percentage of NDs if as low as 5-10%” (USEPA 2012). Accordingly, AECOM did not use substitution methods in this statistical analysis.



E5-2

Two recommended non-substitution methods for handling NDs are (1) the Kaplan-Meier procedure (KM) and (2) Robust Regression on Order Statistics (ROS).

• Kaplan-Meier: The KM procedure is a nonparametric method not requiring transformations or assumptions of distribution and is the standard in medical and industrial statistics for estimating a mean of censored data (Klein and Moeschberger 2003). KM was determined to be the most reliable method for computing the UCL95 of concentration data (Singh et al. 2006). The KM method was not developed for use where a single censoring value (i.e., one reportable detection limit) exists in the population. In this case, the KM estimates of the mean will be equal to the mean based on DL substitution. AECOM has used KM methods for data sets with multiple detections limits.

• Robust Regression on Order Statistics (ROS): The ROS procedure is the most suitable method for data sets with a single detection limit (Helsel 2005). ROS uses regression on a probability plot to estimate distributional parameters, usually in log units. Individual estimates are then predicted from the line and retransformed back into original units. No transformation of the estimated summary statistics occurs. The imputed values are then used collectively with the detected data to compute summary statistics. This is the preferred method for data sets with a single censoring level.

Calculation of summary statistics, including 95% UCLs, for data sets with NDs is based on both the number of censoring levels as described above and the percentage of the data set being censored. For data sets where less than 40% of the observations are censored, the BCA method is used. BCA intervals are recommended for general use for data sets where the degree of censoring is low (less than 40%); however, the method breaks down when the degree of censoring is high (greater than or equal to 40%) (Singh et al. 2006). Under these circumstances the median value, which is used to make the adjustment for skewness, is difficult/impossible to determine (Singh et al. 2006). Therefore, AECOM elected to use BCA Bootstrap UCL95 for data sets where the degree of censoring is low (less than 40%), and UCL95 Bootstrap where 40% or more of the observations are NDs.

E5.2 Statistical Analysis of Sediment and Pore Water Concentration Data

E5.2.1 Sediment

Sediments collected from the vicinity of Centerm were submitted for analysis of total metals and polycyclic aromatic hydrocarbons (PAHs). Select samples (refer to Appendix E-1) were also analyzed for either total petroleum hydrocarbons or polychlorinated biphenyls (PCBs).

E5.2.1.1 Metals

Table E5-1 to Table E5-3 present concentration data for metals from RSED, ESED, and WSED sample locations, respectively.

Table E5-1: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated Metals

Measured in Sediments Collected from the RSED Sample Locations

Contaminant ISQG PEL n % ND Max. Mean SD CV Skewness UCL95

Arsenic 7.24 41.6 11 0% 14.6 7.697 3.472 0.451 1.128 10.29 Cadmium 0.7 4.2 11 0% 3.74 0.936 1.03 1.100 2.364 1.758



E5-3

Contaminant ISQG PEL n % ND Max. Mean SD CV Skewness UCL95 Chromium (Total) 52.3 160 11 0% 58.2 25.64 11.48 0.448 2.686 32.9

Copper 18.7 108 11 0% 3810 445.8 1121 2.515 3.265 1458 Lead 30.2 112 11 0% 540 109.3 176.7 1.617 2.016 315.4 Mercury 0.13 0.7 11 18% 2.42 0.34 0.707 2.079 - 0.978 Zinc 124 271 11 0% 812 193.1 226.4 1.172 2.403 376.8 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL).

Table E5-2: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated Metals Measured in Sediments Collected from the ESED Sample Locations


Arsenic 7.24 41.6 27 0% 13.9 7.204 2.706 0.376 0.0317 8.0 Cadmium 0.7 4.2 27 0% 4.5 1.194 0.946 0.792 2.142 1.5 Chromium (Total) 52.3 160 27 0% 38.3 22.4 8.179 0.365 -0.15 25

Copper 18.7 108 27 0% 518 162.9 113.5 0.697 1.468 205 Lead 30.2 112 27 0% 262 70.44 61.84 0.878 1.539 94.3 Mercury 0.13 0.7 27 7% 2.26 0.411 0.496 1.207 - 0.61 Zinc 124 271 27 0% 751 196.1 142.6 0.727 2.471 259 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL).

Table E5-3: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated Metals Measured in Sediments Collected from the WSED Sample Locations


Arsenic 7.24 41.6 22 0% 13.7 4.793 3.069 0.640 1.557 6.0 Cadmium 0.7 4.2 22 0% 2.41 0.445 0.565 1.270 2.572 0.7 Chromium (Total) 52.3 160 22 0% 47 20.51 9.883 0.482 1.281 24 Copper 18.7 108 22 0% 200 52.08 50.51 0.970 1.85 74 Lead 30.2 112 22 0% 51.5 14.79 13.45 0.909 1.595 20 Mercury 0.13 0.7 22 45% 2 0.155 0.419 2.703 - 0.33 Zinc 124 271 22 0% 327 71.82 69.97 0.974 2.777 111 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL).

E5.2.1.2 PAHs

Table E5-4 to Table E5-6 present concentration data for PAHs from RSED, ESED, and WSED sample locations, respectively.



E5-4

Table E5-4: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated PAHs Measured in Sediments Collected from the RSED Sample Locations

Contaminant ISQG PEL n n >LOD

% ND Max. Min. Mean SD CV UCL95

2-Methylnaphthalene 0.0202 0.201 11 10 9% 0.29 0.0021 0.0612 0.0909 1.485 0.118 Acenaphthene 0.00671 0.0889 11 11 0% 0.62 0.00055 0.106 0.208 1.962 0.417 Acenaphthylene 0.00587 0.128 11 11 0% 0.095 0.0011 0.0276 0.0315 1.141 0.0682 Anthracene 0.0469 0.245 11 11 0% 0.71 0.004 0.173 0.249 1.439 0.513 Benzo(a)anthracene 0.0748 0.693 11 11 0% 2.2 0.0034 0.498 0.769 1.544 1.695 Benzo(a)pyrene 0.0888 0.763 11 11 0% 1.8 0.0055 0.44 0.616 1.4 1.337 Chrysene 0.108 0.846 11 11 0% 4.6 0.0039 0.79 1.413 1.789 2.898 Dibenz(a,h)anthracene 0.00622 0.135 11 11 0% 0.23 0.00082 0.0609 0.0821 1.348 0.177 Fluoranthene 0.113 1.494 11 11 0% 4.7 0.0066 0.912 1.569 1.72 3.083 Fluorene 0.0212 0.144 11 10 9% 0.45 0.0015 0.104 0.162 1.558 0.202 Naphthalene 0.0346 0.391 11 11 0% 0.37 0.0039 0.079 0.119 1.506 0.208 Phenanthrene 0.0867 0.544 11 11 0% 3.2 0.0048 0.615 1.099 1.787 2.175 Pyrene 0.153 1.398 11 11 0% 4.6 0.018 1.013 1.47 1.451 2.821 PAHs (Total) 2.5* 11 11 0% 19 0.061 4.83 6.799 1.408 14.86 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL) * Disposal at Sea Regulations Lower Level Value for Total PAHs Table E5-5: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated PAHs

Measured in Sediments Collected from the ESED Sample Locations


% ND

Max. Min. Mean SD CV UCL95

2-Methylnaphthalene 0.0202 0.201 27 27 0% 0.82 0.0082 0.102 0.159 1.559 0.179 Acenaphthene 0.00671 0.0889 27 27 0% 0.55 0.0033 0.0759 0.121 1.594 0.131 Acenaphthylene 0.00587 0.128 27 26 4% 0.23 0.0025 0.0482 0.0563 1.168 0.0691 Anthracene 0.0469 0.245 27 27 0% 2.5 0.013 0.299 0.543 1.816 0.557 Benzo(a)anthracene 0.0748 0.693 27 27 0% 3.2 0.016 0.425 0.671 1.579 0.716 Benzo(a)pyrene 0.0888 0.763 27 27 0% 2.4 0.018 0.427 0.539 1.262 0.66 Chrysene 0.108 0.846 27 27 0% 3.1 0.022 0.523 0.708 1.354 0.842 Dibenz(a,h)anthracene 0.00622 0.135 27 27 0% 0.39 0.0033 0.0742 0.0895 1.206 0.11 Fluoranthene 0.113 1.494 27 27 0% 9 0.045 1.056 1.82 1.723 2.097 Fluorene 0.0212 0.144 27 27 0% 0.68 0.0055 0.123 0.182 1.48 0.196 Naphthalene 0.0346 0.391 27 27 0% 0.76 0.0081 0.121 0.158 1.306 0.193 Phenanthrene 0.0867 0.544 27 27 0% 6.6 0.023 0.801 1.58 1.973 1.521 Pyrene 0.153 1.398 27 27 0% 8.2 0.059 1.552 2.224 1.433 2.512 PAHs (Total) 2.5* 27 27 27 36 0.24 5.612 8.217 1.464 9.003 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL). * Disposal at Sea Regulations Lower Level Value for Total PAHs



E5-5

Table E5-6: Summary Statistics of Environmental Concentration Data (mg/kg) for Regulated PAHs Measured in Sediments Collected from the WSED Sample Locations


% ND

Max. Min. Mean SD CV UCL95

2-Methylnaphthalene 0.0202 0.201 22 19 14% 0.075 0.0019 0.0168 0.0174 1.036 0.0238 Acenaphthene 0.00671 0.0889 22 20 9% 0.032 0.00096 0.00977 0.0089 0.911 0.0123 Acenaphthylene 0.00587 0.128 22 21 5% 0.051 0.0005 0.0118 0.0135 1.144 0.0172 Anthracene 0.0469 0.245 22 20 9% 0.18 0.0029 0.0491 0.0489 0.996 0.065 Benzo(a)anthracene 0.0748 0.693 22 22 0% 0.36 0.0014 0.0771 0.0929 1.205 0.118 Benzo(a)pyrene 0.0888 0.763 22 22 0% 0.52 0.0022 0.105 0.136 1.295 0.166 Chrysene 0.108 0.846 22 22 0% 0.54 0.0015 0.113 0.137 1.212 0.178 Dibenz(a,h)anthracene 0.00622 0.135 22 22 0% 0.087 0.0005 0.0175 0.023 1.314 0.0275 Fluoranthene 0.113 1.494 22 22 0% 0.51 0.0022 0.135 0.149 1.104 0.203 Fluorene 0.0212 0.144 22 20 9% 0.048 0.0017 0.0166 0.0147 0.886 0.0211 Naphthalene 0.0346 0.391 22 20 9% 0.12 0.001 0.0249 0.026 1.044 0.0356 Phenanthrene 0.0867 0.544 22 20 9% 0.34 0.0084 0.0926 0.0891 0.962 0.122 Pyrene 0.153 1.398 22 22 0% 0.87 0.0023 0.211 0.251 1.19 0.321 PAHs (Total) 2.5* 22 22 0% 3.5 0.01 0.857 0.972 1.134 1.285 Bold Italic = Concentration greater than CCME Interim Sediment Quality Guideline (ISQG). Black = Concentration greater than CCME Probable Effects Level (PEL). * Disposal at Sea Regulations Lower Level Value for Total PAHs

E5.2.1.3 PCBs

Concentrations of total PCBs were below limits of detection in all samples, with the exceptions of WSED10-50-60, which had a reported concentration of total PCB of 0.1 mg/kg. No statistical summary has been prepared.

E5.2.1.4 Key Observations

Key observations for the eastern (i.e., Ballantyne Pier), western, and near-field reference samples are as follows:

Eastern Pier Expansion Area (ESed sample stations) – Ballantyne Pier

• Metals (Table E5-2) • Arsenic, cadmium, copper, lead, mercury, and zinc exceeded the CCME ISQGs in at least one sample. • Maximum measured concentrations exceeded the CCME PEL for cadmium, copper, lead, mercury,

and zinc. • The maximum copper concentration (518 mg/kg) was observed in sample ESed9-25-35, collected from

25 cm to 35 cm below grade, and exceeded the PEL by a factor of 5. • Typical concentrations (i.e., mean and UCLM95) for arsenic, cadmium, copper, lead, mercury, and zinc

exceeded the ISQG. • Typical concentrations (mean and UCLM95) for cadmium, lead, mercury, and zinc exceeded the ISQG,

but were below the PEL. • The typical copper concentration (UCLM95) exceeded the CCME PEL.



E5-6

• Polycyclic Aromatic Hydrocarbons (Table E5-5) • All PAHs reported concentrations in excess of the CCME ISQG. • Maximum concentrations of 7 of the 13 PAHs for which a CCME SQG exist exceeded the PEL. • Typical concentrations (UCLM95) of the PAHs acenaphthene, anthracene, benzo(a)anthracene,

fluoranthene, fluorene, phenanthrene, and pyrene exceeded the CCME PEL.

Western Pier Expansion Area (WSed sample stations)

• Metals (Table E5-3) • Arsenic, cadmium, copper, lead, mercury, and zinc concentrations exceeded the CCME ISQGs in at

least one sample. • Maximum concentrations of copper (200 mg/kg), mercury (2 mg/kg), and zinc (327 mg/kg) exceeded

the CCME PEL. • Typical concentrations (UCLM95) of copper and mercury exceeded the CCME ISQG, but were below

the PEL. • Polycyclic Aromatic Hydrocarbons (Table E5-6)

• All regulated PAHs exceeded the ISQG in at least one sample. • Typical concentrations (UCLM95) exceeded the CCME ISQG for 2-methylnaphthalene, acenaphthene,

acenaphthylene, anthracene, benzo(a)anthracene, benzo(a)pyrene, chrysene, dibenz(a,h)anthracene, fluoranthene, naphthalene, phenanthrene, and pyrene.

• No PAH concentrations exceeded the PEL.

Near-field Reference Stations (RSed sample stations)

• Metals (Table E5-1) • Maximum concentrations of arsenic, cadmium, copper, lead, mercury, and zinc exceeded the CCME

ISQG. • The maximum measured concentration of copper from RSed1-0-1 ([Cu] = 3810 mg/kg) was the highest

concentration measured in any sediment and exceeded the CCME ISQG by two orders of magnitude. • Typical concentrations (i.e., the UCLM95) of copper, lead, mercury, and zinc typical of near-field

reference sediments exceeded the CCME ISQG and PEL. • Polycyclic Aromatic Hydrocarbons (Table E5-4)

• All regulated PAHs exceeded CCME ISQG in at least one near-field reference sample. Of the 13 federally regulated PAHs, 11 were measured at concentrations in excess of the PEL in at least one near-field reference sample.

Maximum PAH concentrations were measured in sample RSed1, located near CRAB Park and Main Street dock, and may, in part, reflect urban runoff from a combined storm/sanitary overflow located in this area.

E5.2.2 Interstitial Pore Water

E5.2.2.1 Metals

Concentrations of all metals for which a guideline exists were below CCME Water Quality Guidelines for the Protection of Marine Aquatic Life. Concentrations of metals in interstitial waters were also screened against the British Columbia Approved Water Quality Guidelines for Protection of Marine Aquatic Life (BC WQG). Three metals (boron, iron, and selenium) were measured at concentrations that exceed the BC WQG in at least a single sample (Table E5-7).



E5-7

Interstitial pore water concentrations from the eastern and western pier expansion areas were compared to determine whether concentrations of metals in interstitial pore water represents two separate and distinct populations or a single data set. The eastern and western data were graphically examined using a combination of kernel density plots and quantile-quantile plots. Figure E5-1 provides an example of the density plot and Q-Q plot for selenium concentrations measured in pore water collected from ESED and WSED sampling locations. Density plots and Q-Q plots for concentrations of metals in pore water support the combination of the data set into a single population. The plots identify the presence of potential outliers in the data; however, in general the distribution of the measured concentrations is similar between groups. As such, AECOM elected to group the metals data into a single population. This provides a greater number of samples from which to calculate statistical intervals such as the UCLM95.



E5-8

Note: The density plot and Q-Q plot indicate a similar distribution of pore water concentration data Figure E5-1: Kernel Density Plot (left) and Quantile-Quantile Plot of Log Normalized Data (right) of Dissolved Selenium Concentration

(µg/L) Measured in Pore Water Samples Collected from the Vicinity of the Eastern Pier (ESED) and Western Pier (WSED)



E5-9

Table E5-7: Calculated Descriptive Statistics of Dissolved Metals Concentration (µg/L) Measured in

Interstitial Pore Water Collected from the Vicinity of the CENTERM Terminal Expansion Areas (East and West Combined)

Contaminant Guideline n % ND Max. Min. Mean SD CV UCL95

Arsenic 12.5a 29 14% 10.8 0.55 2.986 2.788 0.934 3.676 Boron 1200b 29 0% 3310 2070 2890 311.2 0.108 2973 Cadmium 0.12a 29 90% 0.078 0.054 0.0657 0.013 0.198 0.0306 Copper 3b 29 38% 1.43 0.51 1.032 0.43 0.417 0.942 Iron 350b 29 10% 746 4.7 72.87 157.6 2.163 137.7 Mercury 0.016a 7 100% <0.3 <0.3 NA NA NA NA Lead 140b 29 72% 0.3 0.12 0.2 0.0752 0.376 0.123 Selenium 2b 29 38% 1.85 0.51 0.894 0.451 0.504 0.824 Silver 7.5a 29 100% <0.050 <0.050 NA NA NA NA Zinc 10b 29 69% 3.9 1.1 2.256 0.98 0.434 1.379 a CCME Water Quality Guidelines for the Protection of Marine Aquatic Life (µg/L) b BC Ambient Water Quality Guidelines for Marine Aquatic Life (µg/L)

E5.2.2.2 PAHs

Analytical data for select PAHs were observed to be unreliable, owing to a high proportion of fine suspended sediment entrained in the pore water sampling procedure. The result being concentration data that are biased high. Evidence of this is present in the reported dissolved PAH concentrations of benzo(a)pyrene and chrysene that greatly exceed their respective solubility limits (3.8 µg/L and 1.9 µg/L, respectively at 25°C) in 14 samples. In order to account for this, AECOM substituted all concentrations which were reported in excess of the solubility limits at the respective solubility limit (i.e., concentrations of benzo(a)pyrene reported to be above 3.8 µg/L were substituted with a value of 3.8 µg/L).

This is deemed to be an appropriate strategy for dealing with these high-biased values since the true value is known to have a maximum equal to the solubility limit. Furthermore, censoring the data set at the solubility limit at 25°C maintains conservatism of the assessment, as environmentally relevant temperatures are much lower than 25°C. The solubility at environmentally relevant temperatures would likely be reduced by a factor of 3 to 4.1

Concentrations of PAHs measured in interstitial pore waters were observed to show a marked variation between the western and eastern ends of the Centerm pier expansion areas. As such, summary statistics (censored to remove unreliable results in excess of solubility limits) were generated for sampling locations in the vicinity of the Ballantyne Pier (Table E5-8) and the Western Pier (Table E5-9) separately.

1 The solubility of PAHs in water is enhanced three- to four-fold by a rise in temperature from 5°C to 30°C. (Neff 1979).



E5-10

Table E5-8: Descriptive Statistics of Measured Concentrations (µg/L) of PAHs in Interstitial Pore Water from Sampling Locations in the Vicinity of Ballantyne Pier (ESED)

Contaminant BC AWQG

n %<LOD Max. Min. Mean SD CV UCL95

Acenaphthene 6 14 36% 6.4 0.075 1.417 1.734 1.224 1.864 Acridine 1E+34 14 57% 1.8 0.24 0.708 0.506 0.715 0.701 Anthracene 1E+34 14 14% 19 0.039 2.942 5.017 1.705 6.394 Benzo(a)anthracene 1E+34 14 14% 43 0.082 6.517 11.5 1.765 14.33 Benzo(a)pyrene 0.01 14 7% 3.8a 0.012 2.046 1.738 0.849 2.676 Chrysene 0.1 14 14% 1.9b 0.11 1.225 0.812 0.663 1.401 Fluoranthene 1E+34 14 7% 100 0.021 13.69 26.75 1.954 30.94 Fluorene 12 14 29% 8.7 0.089 1.67 2.344 1.404 2.879 Naphthalene 1 14 57% 8.8 0.44 2.277 2.299 1.010 2.39 Phenanthrene 1E+34 14 14% 48 0.073 8.579 13.46 1.569 16.07 Pyrene 1E+34 14 0% 140 0.021 18.56 37.95 2.045 59.46 Notes: Bold exceeds BC Ambient Water Quality Guidelines for Marine Aquatic Life a Concentrations of benzo(a)pyrene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values

censored at the solubility limit of 3.8 µg/L at 25°C. b Concentrations of chrysene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values

censored at the solubility limit of 1.9 µg/L at 25°C. Solubility limits sourced from Ambient Water Quality Criteria for Polycyclic Aromatic Hydrocarbons (PAHs), BC Ministry of Environment, Lands

and Parks. 1993. Online access at http://www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/index.html#TopOfPage

Table E5-9: Descriptive Statistics of Measured Concentrations (µg/L) of PAHs in Interstitial Pore Water from Sampling Locations in the Vicinity of the Western Pier Expansion Area (WSED)

Contaminant BC AWQG

n %<LOD Max. Min. Mean SD CV UCL95

Acenaphthene 6 18 50% 0.55 0.065 0.191 0.14 0.733 0.163 Acridine 1E+34 18 61% 0.24 0.079 0.139 0.0665 0.478 0.129 Anthracene 1E+34 18 33% 2.7 0.021 0.732 0.714 0.975 0.864 Benzo(a)anthracene 1E+34 18 22% 4.5 0.013 1.093 1.18 1.080 1.47 Benzo(a)pyrene 0.01 18 17% 3.8a 0.012 1.437 1.45 1.009 1.831 Chrysene 0.1 18 39% 1.9b 0.073 1.256 0.81 0.645 1.114 Fluoranthene 1E+34 18 17% 6.7 0.022 1.893 1.946 1.028 2.459 Fluorene 12 18 50% 1 0.12 0.311 0.243 0.781 0.27 Naphthalene 1 18 83% 0.4 0.25 0.313 0.103 0.329 0.4 Phenanthrene 1E+34 18 39% 5.9 0.068 1.42 1.444 1.017 1.745 Pyrene 1E+34 18 11% 10 0.024 2.755 3.261 1.184 3.949 Notes: BC AWQG = BC Ambient Water Quality Guidelines for Marine Aquatic Life



E5-11

a Concentrations of benzo(a)pyrene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values censored at the solubility limit of 3.8 µg/L at 25°C.

b Concentrations of chrysene reported in excess of solubility limits due to high suspended solids in collected samples. Erroneous values censored at the solubility limit of 1.9 µg/L at 25°C.

Solubility limits sourced from Ambient Water Quality Criteria for Polycyclic Aromatic Hydrocarbons (PAHs), BC Ministry of Environment, Lands and Parks. 1993. Online access at http://www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/index.html#TopOfPage

E5.2.2.3 Key Observations

Key observations from the combined eastern (i.e., Ballantyne Pier) and western pore water data are as follows:

• Metals (Table E5-7) • The majority of metal analytes were below CCME concentrations. Isolated exceedances, all less than

three-fold, were noted for iron, boron, and selenium. • Concentrations of dissolved iron exceed the BC WQG in 2 of the 29 samples. Typical concentrations

(mean = 73 µg/L and UCLM95 = 138 µg/L) measured in pore water from the project footprint were below applicable standards.

• Concentrations of dissolved boron ranged from 2,070 µg/L to 3,310 µg/L. These concentrations are above the BC WQG for protection of marine aquatic life, but are below the average concentrations of boron in sea water (average seawater = 4,500 µg/L (Canadian Council of Ministers of the Environment (CCME) 2009]). Boron is therefore not considered as a substance of interest with respect to pore water expulsion.

• Dissolved selenium (2.6 µg/L) marginally exceeded the BC WQG of 2.0 µg/L in one sample. • Polycyclic Aromatic Hydrocarbons (Table E5-8and Table E5-9)

• Concentrations of acenaphthene, benzo(a)pyrene, chrysene, and naphthalene measured in pore water samples exceeded the BC Ambient WQG for the protection of marine aquatic life.

• Maximum concentrations of PAHs measured in pore water were observed in the eastern vicinity of the Project, at the Ballantyne Pier.

• Turbid pore water caused PAH data to be biased high and this principal is likely applicable to all PAHs due to their varying affinity to partition into organic compartments such as the carbon moiety of sediment particles. Where pore water was very turbid (e.g., sediment sample ESed-8), benz(a)pyrene and chrysene reported above their solubility limits. This exceedance of solubility limit was observed in 14 instances. To resolve these occurrences and provide a more meaningful and statistical interpretation, it was conservatively assumed that benzo(a)pyrene and chrysene were present at their solubility limit.

• Comparison of the eastern UCL95 values for benzo(a)pyrene and chrysene (268 µg/L and 1.4 µg/L, respectively) suggests regulatory exceedance factors of approximately 267- and 14-fold, respectively. These are upwardly-biased values and likely to be at least two- to three times lower (i.e., approximately 90-fold and 5-fold, respectively) at the benthic in situ temperature of approximately 5°C. (Note: The solubility of PAHs in water is enhanced three- to four-fold by a rise in temperature from 5°C to 30°C. (www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/pahs-02.htm#TopOfPage).

http://www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/index.html#TopOfPage

http://www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/pahs-02.htm#TopOfPage



E5-12

E5.3 References

Efron, B. and R.J. Tibshirani. 1994. An Introduction to the Bootstrap. Boca Raton, FL: CRC Press.

Helsel, D. 2012a. Course presented January 19th 2012 to the Society of Contaminated Sites Approved Professionals of British Columbia titled Environmental Statistics Using ProUCL.

Helsel, D. 2012b. Course presented November 29th 2012 titled Practical Statistics for Contaminated Site Studies through GeoEnviroLogic Professional Development.

Helsel, D.R. 2005. Nondetects and data analysis: Statistics for censored environmental data. Hoboken (NJ). John Wiley & Sons, 250p.

Klein and Moeschberger. 2003. “Summing Nondetects: Incorporating Low-Level contaminants in Risk Assessment.” Integrated Environmental Assessment and Management. Vol.6, No. 3, pp. 361-366.

Neff, J.M. 1979. Polycyclic Aromatic Hydrocarbons in the Aquatic Environment: Sources, Fates and Biological Effects. Applied Science Publishers Ltd., Essex, England. 262 p. as cited by BC MoE: http://www.env.gov.bc.ca/wat/wq/BCguidelines/pahs/index.html.

Singh, A., R. Maichle, and S. Lee. 2006. On the Computation of a 95% Upper Confidence Limit of the Unknown Population Mean Based Upon Data Sets with Below Detection Limit Observations. EPA/600/R-06/022, March 2006. Available at: http://www.epa.gov/osp/hstl/tsc/softwaredocs.htm.

USEPA. 2012. ProUCL Version 4.1 User Guide (Draft). EPA/600/r-07/041. US Environmental Protection Agency, Office of Research and Development, Washington, DC. Available at http:// http://www.epa.gov/osp/hstl/tsc/ProUCL_v4.1_user.pdf.

Appendix E6Statistical Analysis of Supplemental

Deep Sediment (August 2016)

Table E6-1: Summary of Sediment Chemistry Data and Statistics


Appendix E6

E6-1

Parameter As Cd Crtotal Cu Pb Hg Zn PAHtotal PCBtotal

CCME ISQG 7.24 0.70 52.3 18.7 30.2 0.13 124 --- 0.022CCME PEL 41.6 4.2 160 108 112 0.70 271 --- 0.19N 47 47 47 47 47 47 47 47 47%>ISQG 13 11 0 96 15 21 2 N/A 6%<DL 0 0 0 0 0 38 0 0 93Mean 5.56 0.46 23 51 17.7 0.16 68 0.71 0.064SD 1.51 0.22 4 30 14.5 0.12 25 0.75 0.017Minimum 1.43 0.13 17 13 2.31 0.05 28 0.02 0.027Maximum 9.19 1.41 36 207 82 0.55 179 4.0 0.1195%UCLM 5.94 0.52 24 60 21.9 0.14 76 0.92 0.014N 16 16 16 16 16 16 16 16 16%>ISQG 6 0 0 94 6 6 0 N/A 0%<DL 0 0 0 0 0 75 0 0 100Mean 5.94 0.44 23 25 10.7 0.09 55 0.12 N/ASD 1.00 0.10 3 6.1 16.2 0.04 11 0.14 N/AMinimum 4.53 0.33 19 18 4.2 0.06 42 0.002 N/AMaximum 8.87 0.64 29 39 70 0.13 81 0.5 N/A95%UCLM 6.44 0.49 25 28 17.1 0.05 61 0.23 N/AN 22 22 22 22 22 22 22 22 22%>ISQG 14 0 0 59 0 0 0 N/A 0%<DL 0 0 0 0 0 82 0 0 100Mean 5.95 0.43 25 25 6.9 0.09 53 0.11 N/ASD 0.98 0.10 6 11 4.8 0.03 12 0.25 N/AMinimum 4.80 0.26 20 13 3.5 0.07 37 0.002 N/AMaximum 8.20 0.60 41 58 19.2 0.12 75 1 N/A95%UCLM 6.34 0.47 28 30 9.1 0.05 57 0.24 N/AN 33 33 33 33 33 33 33 33 29%>ISQG 45 58 0 79 52 61 45 27 21%<DL 0 0 0 0 0 18 0 N/A 79Mean 7.28 0.88 21 110 35.6 0.24 131 1.68 0.046SD 2.24 0.54 5.2 119 29.5 0.20 83 1.39 0.017Minimum 2.75 0.26 9.7 13 3.7 0.05 35 0.001 <DLMaximum 12.4 2.20 36 433 135 0.93 322 4.9 0.07095%UCLM 7.94 1.05 22 147 46 0.28 155 2.08 0.041N 8 8 8 8 8 8 8 8 7%>ISQG 0 0 0 0 0 0 0 N/A 0%<DL 0 0 0 0 0 100 0 0 100Mean 3.84 0.30 17 15 3.6 N/A 35 0.013 N/ASD 0.59 0.04 1.6 2.6 0.5 N/A 4.0 0.026 N/AMinimum 3.20 0.23 15 11 3.1 N/A 28 0.001 N/AMaximum 5.05 0.35 19 18 4.4 N/A 41 0.077 N/A95%UCLM 4.38 0.34 19 18 4.0 N/A 39 0.061 N/AN 15 15 15 15 15 15 15 15 15%>ISQG 1 3 0 15 4.0 6 3 N/A 3%<DL 0 0 0 0 0 13 0 0 80Mean 4.67 0.53 21 63 97 0.20 88 6.72 0.041SD 1.55 0.34 4.7 31 265 0.22 37 14 0.017Minimum 2.47 0.11 12 19 4.0 0.05 34 0.37 0.024Maximum 8.28 1.41 30 134 1050 0.83 172 56 0.06895%UCLM 5.57 0.74 24 82 240 0.31 110 15.2 0.068

Values exceed CCME ISQGValues exceed CCME PEL

Site Depth

West

East

0-0.6m

0.6-1.0m

>1.0m

0-1.0m

>1.0m

0-0.2mSeabus

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Port of Vancouver | - Appendix...2016/11/12 · Table E1-1: Results of Chemical Analysis of Surficial Sediment Samples (January 2016)Vancouver Fraser Port Authority Centerm Expansion