Proficiency Testing - Fapas · FCAL10-SEA7 145 g 25/03/2021 211 27295 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 09/04/2021 217 27296 Cake Mix egg, egg white protein FCAL5-PRO10

Proficiency Testing

Proficiency Test List - GBP

Jan 2021 - Mar 2022

2

this page is intentionally blank

3

CONTENTS

PAGE

FOOD AND BEVERAGE CHEMISTRY 4 - 35alcohol 5 - 6allergens 6 - 7authenticity 7 - 8contaminants 8 - 12fat, fatty acids and oils 12 - 13food additives and ingredients 13 - 15mycotoxins 15 - 19nutritional and proximates 19 - 22pesticides 22 - 27quality 27 - 28veterinary drug residues 28 - 30list of potential pesticide residues 31 - 33list of potential fish species 33list of potential veterinary drug residues 34 - 35

FOOD AND BEVERAGE MICROBIOLOGY 37 - 45indicator organisms 38 - 42pathogens 42 - 45

GM FOOD 47 - 49

WATER AND ENVIRONMENTAL CHEMISTRY 51 - 79drinking water 52 - 58high salinity water 58 - 59soil 59surface water 59 - 60waste water 60 - 67approximate concentration ranges 67 - 79

WATER AND ENVIRONMENTAL MICROBIOLOGY 81 - 86indicator organisms 82 - 85parasitology 85pathogens 86unknown organisms 86

HOW TO ORDER 87

FAPAS® AGENTS 88

4

EUR

FOOD AND BEVERAGECHEMISTRYProficiency Test List - GBP

Jan 2021 - Mar 2022

5

FOOD & BEVERAGE CHEMISTRY PROFICIENCY TESTS

Quantity discounts (for materials purchased in a single order) excluding blank materials

Quantity

PurchasedDiscount Applied

21 - 45 tests 5%46 - 70 tests 10%71 or more 20%

ALCOHOL

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)

1398 Whisky

alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropan-1-ol & 2-methylbutan-1-ol + 3-methylbutan-1-ol (sum)

FCOH3-DRA10 200 ml 17/03/2021 259

1399 Wine

alcoholic strength, total SO2,

total acidity, volatile acidity and wine quality indicators

FCOH4-DRA13 220 ml 05/08/2021 267

13100 Brandy

alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropan-1-ol, 2-methylbutan-1-ol + 3-methylbutan-1-ol (sum) & ethyl carbamate

FCOH2-DRA4 200 ml 04/11/2021 267

The confidence in analytical data provided to producers can be enhanced throughusing proficiency testing. Proficiency testing (PT) provides evidence, from anindependent source, regarding the competency of the laboratory supplying theanalytical service. Important commercial and safety decisions are made on theresults of laboratory analysis, so it pays to monitor performance to ensure you canrely on these results.

Our Food Chemistry programme covers chemical analysis of real food samples for a wide range oftarget analytes including: nutritional components, additives, allergens, natural contaminants, pesticideand veterinary medicine residues, and packaging chemical migrants.

Note: The information in this price list is designed to assist you in choosing proficiency tests to meet your needs. Whilst every care has been taken in producing this information, we do not guarantee its accuracy. The Fapas® website is the definitive source of information about our proficiency tests. Orders are subject to the Fapas® terms and conditions, which are available on our website. Please check the website before placing your order.

6


13101 Whisky

alcoholic strength (real and/or apparent), ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropan-1-ol & 2-methylbutan-1-ol + 3-methylbutan-1-ol (sum)

FCOH3-DRA10 200 ml 09/03/2022 267

3115 Beveragealcohol (ethanol) Halal Compliance Check

FCOH1-DRA2 3 x 200 ml 16/08/2021 220

ALLERGENS


27285Infant Soya Formula

milk (BLG) FCAL13-INF13 2 x 20 g 07/01/2021 211

27294Infant Formula (Hydrolysed)


27286 Cooked Biscuit gluten, milk and egg FCAL7-PRO14 30 g 21/01/2021 269

27287 Chocolate peanut, peanut protein FCAL16-CON2 2 x 20 g 05/02/2021 211


milk (casein) & gluten FCAL15-INF13 2 x 20 g 18/02/2021 269

27289 Cumin gluten & sesame FCAL22-SPI8 2 x 20 g 26/02/2021 21127290 Flour lupin FCAL12-CCP28 2 x 20 g 04/03/2021 211

27291 Cooked Biscuit hazelnut, peanut FCAL9-PRO14 50 g 12/03/2021 269

27292 Canned Fishhistamine (high level >50 mg/kg)

FCAL10-SEA7 145 g 25/03/2021 211

27295 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 09/04/2021 21727296 Cake Mix egg, egg white protein FCAL5-PRO10 2 x 20 g 15/04/2021 21727297 Garlic Powder peanut, peanut protein FCAL16-SPI10 2 x 20 g 29/04/2021 21727298 Cake Mix gluten FCAL6-PRO10 2 x 20 g 07/05/2021 21727299 Chocolate hazelnut, hazelnut protein FCAL8-CON2 2 x 20 g 20/05/2021 217

27300Instant Soup Powder

celery, mustard FCAL2-PRO27 2 x 20 g 04/06/2021 217

27322Infant Breakfast Cereal

milk (casein and BLG) FCAL21-INF6 2 x 20 g 16/06/2021 277

27301 Cake Mix gluten, milk and egg FCAL7-PRO10 2 x 30 g 08/07/2021 277

27302Oat Based Foodstuff

gluten FCAL6-CCP37 2 x 20 g 21/07/2021 217

27303 Canned Fishhistamine (low level, <50 mg/kg)

FCAL11-SEA7 145 g 06/08/2021 217

27304Infant Formula (Hydrolysed)

milk (casein and BLG) FCAL21-INF20 2 x 20 g 26/08/2021 217

27305 Chocolate almond, almond protein FCAL1-CON2 2 x 20 g 02/09/2021 21727306 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 23/09/2021 21727307 Jam sulphites FCAL18-CON7 80 g 28/09/2021 21727308 Beer gluten FCAL6-DRA1 2 x 50 ml 11/10/2021 267


FCAL10-SEA7 145 g 29/10/2021 217

27310Sauce (Cooked)

Fish FCAL20-CON23 2 x 30 g 01/11/2021 277

27311 Cake Mix gluten & egg FCAL23-PRO10 2 x 30 g 19/11/2021 246

7


27312 Chocolate

contamination (presence/absence) of matrix with one or more from the following list: Almond, Hazelnut, Walnut, Cashew, Pecan nut, Brazil nut, Pistachio nut, Macadamia/Queensland nut, Peanut

FCAL3-CON2 50 g 25/11/2021 277



27314 Cooked Biscuit gluten, milk and egg FCAL7-PRO14 30 g 20/01/2022 277

27315 Chocolate peanut, peanut protein FCAL16-CON2 2 x 20 g 03/02/2022 217


milk (casein) & gluten FCAL15-INF13 2 x 20 g 17/02/2022 277

27317 Cumin gluten & sesame FCAL22-SPI8 2 x 20 g 24/02/2022 21727318 Flour lupin FCAL12-CCP28 2 x 20 g 02/03/2022 217

27319 Cooked Biscuit hazelnut, peanut FCAL9-PRO14 50 g 11/03/2022 277


FCAL10-SEA7 145 g 24/03/2022 217

27321Sausage Meat (Raw)

gluten FCAL6-MRP39 2 x 20 g 29/03/2022 217

AUTHENTICITY

Adulteration


2992 Vanilla Extract detection of adulteration FCAA1-CON31 30 g 12/01/2021 203

2991 Beefone or more from: chicken, horse, lamb or pork

FCAA4-MRP2 30 g 03/02/2021 203

2993 Chickenone or more from: beef, lamb, pork or turkey

FCAA3-MRP14 30 g 08/04/2021 209

2994 Lambone or more from: beef, chicken, goat or pork

FCAA2-MRP22 30 g 09/07/2021 209

3302 Oil Cannabidiol FCAA5-OIL20 2 x 2 ml 05/10/2021 330

2996Herb (Origanum spp.)

detection of adulteration FCAA1-VEG44 3 x 7g 11/11/2021 392

14244 Olive Oil detection of adulteration FCAA1-OIL22 3 x 50 ml 13/12/2021 392

2997 Vanilla Extract detection of adulteration FCAA1-CON31 30 g 14/01/2022 209

2998 Beefone or more from: chicken, horse, lamb or pork

FCAA4-MRP2 30 g 02/02/2022 209

Contamination


3114 Beefpork (DNA) Halal Compliance Check

FCAC1-MRP2 2 x 30 g 20/04/2021 285

8

Speciation


2995 Fishidentification of unknown fish (3 samples from a list). See list on p33

FCAS1-SEA11 3 x 10 g 11/10/2021 209

CONTAMINANTS

Environmental Contaminants


0696 Fishperfluoroalkylated substances (PFASs)

FCCE5-SEA11 50 g 05/01/2021 268

0697 Palm Oil PAHs (including PAH4 sum) FCCE2-OIL24 30 ml 25/02/2021 3800698 Shellfish PAHs (including PAH4 sum) FCCE2-SEA23 50 g 27/04/2021 391

0699 Olive Oilall 16 EU priority PAHs (including PAH4 sum)

FCCE1-OIL22 30 ml 28/05/2021 435

06100 Pork dioxins and PCBs FCCE3-MRP35 70 g 03/06/2021 39106101 Cocoa Butter PAHs (including PAH4 sum) FCCE2-FAT7 50 g 06/07/2021 39106102 Infant Formula dioxins and PCBs FCCE3-INF10 70 g 12/08/2021 391

06103Smoked Fish Product

PAHs (including PAH4 sum) FCCE2-SEA25 50 g 06/09/2021 391

06110CBD Product (Oil Based)

PAHs (including PAH4 sum) FCCE2-UMI44 10 ml 11/10/2021 391

06104 Cod Liver Oil dioxins and PCBs FCCE3-OIL10 30 ml 21/10/2021 391

06105Spice - Smoked Black Pepper

PAHs (including PAH4 sum) FCCE2-SPI26 15 g 12/11/2021 391

06106 Cod Liver Oilbrominated flame retardants (BFRs)

FCCE6-OIL10 30 ml 09/12/2021 391

06107 Fishperfluoroalkylated substances (PFASs)

FCCE5-SEA11 50 g 04/01/2022 276

06108 Palm Oil PAHs (including PAH4 sum) FCCE2-OIL24 30 ml 18/02/2022 391

06109 Milk dioxins and PCBs FCCE3-DRY13 70 g 14/03/2022 391

Overall Migration (Packaging Contaminants)


1163 Nylon Filmoverall migration into ethanol by total immersion

FCCO1-PMM136 sheets,

each 12 cm x 16 cm

14/04/2021 211

1164 Plastic Filmoverall migration into olive oil by total immersion

FCCO2-PMM16to be

confirmed20/10/2021 241

Processing Contaminants


2663 Soy Sauce3-MCPD, 1,3-DCP and 2-MCPD

FCCP2-CON15 40 g 24/02/2021 209

2664 Vegetable Oil3-MCPD esters, glycidyl esters (ester-bound glycidol) and 2-MCPD esters

FCCP1-OIL30 50 ml 14/04/2021 215

2665 Potato Crisps3-MCPD esters, glycidyl esters (ester-bound glycidol) and 2-MCPD esters

FCCP1-PRO31 50 g 06/05/2021 215

9


2666 Infant Formula3-MCPD esters, glycidyl esters (ester-bound glycidol) and 2-MCPD esters

FCCP1-INF10 50 g 09/06/2021 236

2667 Vegetable Oil3-MCPD esters, glycidyl esters (ester-bound glycidol) and 2-MCPD esters

FCCP1-OIL30 50 ml 15/09/2021 215

2668 Soy Sauce3-MCPD, 1,3-DCP and 2-MCPD

FCCP2-CON15 40 g 23/02/2022 215

30108 Coffeefuran, 2-methylfuran & 3-methylfuran

FCCP9-DRH6 100 g 18/01/2021 200

30109 Potato Crisps acrylamide FCCP3-PRO31 50 g 10/02/2021 200

30110 Infant Formulamelamine & cyanuric acid (> 5 mg/kg)

FCCP7-INF10 50 g 05/03/2021 200

30111Vegetable Crisps

acrylamide FCCP3-PRO37 50 g 07/05/2021 206

30112 Infant Food acrylamide FCCP3-INF8 50 g 04/06/2021 20630113 Animal Feed melamine & cyanuric acid FCCP5-AFE1 50 g 24/06/2021 206

30114Biscuit (Cookie)


30115French Fries (Pre-Cooked)


30116 Milk Powdermelamine & cyanuric acid (low levels, <5 mg/kg)

FCCP6-DRY14 50 g 06/10/2021 206

30117Coffee (Instant)

acrylamide FCCP3-DRH12 50 g 03/11/2021 206

30118 Crispbread acrylamide FCCP3-PRO15 50 g 02/12/2021 206

30119 Coffeefuran, 2-methylfuran & 3-methylfuran

FCCP9-DRH6 100 g 24/01/2022 206

30120 Potato Crisps acrylamide FCCP3-PRO31 50 g 17/02/2022 206

30121 Infant Formulamelamine & cyanuric acid (> 5 mg/kg)

FCCP7-INF10 50 g 04/03/2022 206

Specific Migration (Phthalates, BPA, PAA)

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)12103 Oil phthalates FCCS5-OIL20 2 x 50 ml 24/03/2021 205

121043% aq. Acetic Acid

melamine FCCS4-PMM3 50 ml 26/05/2021 211

1210550% Aqueous Ethanol

bisphenol A FCCS2-PMM4 50 ml 07/07/2021 211


formaldehyde FCCS3-PMM3 50 ml 01/09/2021 211


total primary aromatic amines FCCS6-PMM3 >300 ml 15/10/2021 211


barium, cobalt, copper, iron, lithium, manganese & zinc

FCCS1-PMM3 50 ml 24/11/2021 211

12109 Oil phthalates FCCS5-OIL20 2 x 50 ml 23/03/2022 211

10

Trace Elements


07387 Milk Powderarsenic (total), cadmium, lead & mercury (total) (all natural/low levels)

FCCM12-DRY14 50 g 06/01/2021 200

07388 Soft Drinkantimony, arsenic (total), cadmium, chromium, copper & zinc (all high levels)

FCCM3-DRN29 50 ml 20/01/2021 200

07389Canned Crab Meat

arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all natural levels)

FCCM6-SEA6 150 g 29/01/2021 200

07390 Tomato Pastecadmium, iron, lead & tin (all high levels)

FCCM21-VEG74 50 g 08/02/2021 200

07391Bivalve Molluscs (Mussels)

cadmium, lead & mercury (total) (all natural/low levels)

FCCM36-SEA29 50 g 08/02/2021 200

07392Soya Lecithin (Liquid)

aluminium, arsenic (total), cadmium, lead & mercury (total) (all natural/low levels)

FCCM42-VEG90 50 g 24/02/2021 200

07393Grapefruit Purée

cadmium, copper, iron, lead & tin (all high levels)

FCCM23-FRU51 50 g 23/03/2021 200

07394 Canned Fisharsenic (total), mercury (total) & methyl mercury (all natural levels)

FCCM17-SEA7 150 g 31/03/2021 200

07395 Rice Cakes

arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all natural/low levels)

FCCM6-PRO33 35 g 01/04/2021 206

07396 Barley Flour

aluminium, arsenic (total), cadmium, copper, lead, mercury, nickel (total) (all natural/low levels)

FCCM28-CCP4 50 g 15/04/2021 206

07397 Infant Formula

aluminium, cadmium, chromium, iodine, molybdenum, selenium, tin and nickel (all natural/low levels)

FCCM38-INF10 50 g 23/04/2021 206

07398 Canned Fisharsenic (total), cadmium & mercury (total) (all natural levels)

FCCM15-SEA7 150 g 30/04/2021 206

07399 Honeycadmium & lead (all natural/low levels)

FCCM19-HON2 50 g 05/05/2021 206

07400 Wheat Flour

aluminium, arsenic (total), cadmium, copper, iron, lead, mercury (total), nickel & zinc (all natural/low levels)

FCCM32-CCP49 50 g 26/05/2021 206

07401 Vegetable Oilarsenic (total), copper, iron & lead (all high levels)

FCCM16-OIL30 50 ml 02/06/2021 206

Note: The description 'natural/low levels' indicates naturally incurred elements at the typical ranges expected. The description 'natural levels' indicates naturally incurred elements, but some or all analytes may be at levels above the typically expected ranges.

11


07402Vegetable Purée (Root Vegetables)

cadmium, lead, arsenic (total) and mercury (total) (all natural/low levels)

FCCM39-VEG103

50 g 14/06/2021 206

07403 Cocoa Powder

aluminium, arsenic (total), cadmium, copper, iron, lead, manganese, nickel & zinc (all natural levels)

FCCM33-DRH5 50 g 23/06/2021 206

07404 Chilli Powderarsenic (total), cadmium & lead (all high levels)

FCCM10-SPI6 50 g 01/07/2021 206

07405Powdered Brown Rice

arsenic (total), arsenic (inorganic), cadmium, iron, lead & mercury (total), nickel & zinc (all natural/low levels)

FCCM34-CCP41 50 g 14/07/2021 206

07406 Offal (Liver)arsenic (total), cadmium, lead & mercury (total) (all high levels)

FCCM13-MRP27 50 g 28/07/2021 206

07407 Winecadmium, copper, iron, lead & pH

FCCM40-DRA13 50 ml 04/08/2021 206

07408Baby Food (Vegetable Based)

arsenic (total), cadmium & lead (all low levels)

FCCM31-INF19 50 g 09/08/2021 206

07409Herb (mixed, dried)

cadmium, lead & nickel (all natural/low levels)

FCCM35-VEG89 30 g 11/08/2021 206


FCCM12-DRY14 50 g 25/08/2021 206

07411 Canned Fisharsenic (total), cadmium, mercury (total) (all natural levels)

FCCM15-SEA7 150 g 03/09/2021 206

07412 Squidcadmium, lead & mercury (total) (all natural / low levels)

FCCM36-SEA27 50 g 06/09/2021 206

07413Infant Cereal (Rice Based)

arsenic (total), arsenic (inorganic), cadmium, chromium, lead, mercury (total) & selenium (all natural/low levels)

FCCM22-INF18 50 g 16/09/2021 206

07414 Fruit Juicearsenic (inorganic) (natural/low level), cadmium, iron, lead & tin (all high levels)

FCCM5-DRN17 50 ml 28/09/2021 206

07415 Seaweed

arsenic (total), arsenic (inorganic), cadmium, iodine, lead, mercury (total) & nickel (all natural levels)

FCCM37-VEG64 25 g 01/10/2021 206

07416Mushroom Powder

arsenic (total), cadmium, lead, mercury (total), nickel (all natural/low levels)

FCCM30-VEG51 30 g 08/10/2021 206

07417 Soya Flouraluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels)

FCCM1-VEG68 50 g 20/10/2021 206

07418Vegetable Purée

cadmium, lead, nickel & tin (all high levels)

FCCM24-VEG79 50 g 01/11/2021 206

07419 Powdered Ricearsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all high levels)

FCCM7-CCP42 50 g 10/11/2021 206

12


07420Animal Feed (Cereal Based)

arsenic (total), cadmium, lead, mercury (total), nickel (all natural/low levels)

FCCM30-AFE1 50 g 25/11/2021 206

07421Nutritional Food Supplement

arsenic (total), cadmium, chromium, lead & mercury (total) (all natural/low levels)

FCCM27-SUP2 50 g 01/12/2021 206


FCCM12-DRY14 50 g 05/01/2022 206

07423 Soft Drinkantimony, arsenic (total), cadmium, chromium, copper & zinc (all high levels)

FCCM3-DRN29 50 ml 19/01/2022 206

07424Bivalve Molluscs (Mussels)

cadmium, lead & mercury (total) (all natural / low levels)

FCCM36-SEA29 50 g 24/01/2022 206

07425Canned Crab Meat

arsenic (total), arsenic (inorganic), cadmium, lead & mercury (total) (all natural/low levels)

FCCM6-SEA6 150 g 28/01/2022 206

07426 Tomato Pastecadmium, iron, lead & tin (all high levels)

FCCM21-VEG74 50 g 08/02/2022 206

07427Soya Lecithin (Liquid)

aluminium, arsenic (total), cadmium, lead & mercury (total) (all natural/low levels)

FCCM42-VEG90 50 ml 23/02/2022 206

07428Animal Feed (Vegetable Based)

arsenic (total), cadmium, lead, mercury (total), nickel (all high levels)

FCCM43-AFE23 50 g 10/03/2022 206

07429Grapefruit Purée

cadmium, copper, iron, lead & tin (all high levels)

FCCM23-FRU51 50 g 22/03/2022 206

07430 Canned Fisharsenic (total), cadmium, mercury (total) & methyl mercury (all natural levels)

FCCM41-SEA7 150 g 31/03/2022 206


arsenic (total), cadmium, lead & mercury (total)

FCCM14-UMI44 7 g 29/10/2021 206

FAT, FATTY ACIDS & OILS


14229 Vegetable Oilsaturates, mono-unsaturates & poly-unsaturates

FCFO3-OIL30 30 ml 17/02/2021 196


total fat, saturates, mono-unsaturates, poly-unsaturates, trans fatty acids (& possibly individual fatty acids: linoleic acid, a-linolenic acid (ALA), ARA, DHA & EPA)

FCFO13-INF10 50 g 22/04/2021 202

14233Mixed Fat Spread

total fat, saturates, mono-unsaturates, poly-unsaturates & total trans fatty acids

FCFO8-FAT12 50 g 11/05/2021 202

14235 Vegetable Oilsaturates, mono-unsaturates & poly-unsaturates & limited fatty acid profile

FCFO4-OIL30 30 ml 30/06/2021 202

13



Total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, total omega-3, total omega-6 & total omega-9 series fatty acids, (& possibly individual omega-3, omega-6 & omega-9 fatty acids)

FCFO10-FAT12 50 g 16/08/2021 202

14239 Fish Oil

Total omega-3, total omega-6 & total omega-9 series fatty acids, (& possibly individual omega-3, omega-6 & omega-9 fatty acids)

FCFO1-OIL13 30 ml 22/09/2021 202


total fat, saturates, mono-unsaturates & poly-unsaturates, total trans fatty acids & butyric acid

FCFO7-PRO2 50 g 05/10/2021 202

14241Infant Breakfast Cereal

total fat, saturates, mono-unsaturates, poly-unsaturates (& possibly individual fatty acids: linoleic acid, a-linolenic acid (ALA), ARA, DHA & EPA)

FCFO9-INF6 50 g 21/10/2021 202


total fat, butyric acid, cholesterol & selected plant sterols

FCFO14-FAT12 50 g 30/11/2021 202


fatty acid profile (inc. butyric acid) & cholesterol

FCFO12-PRO2 50 g 11/01/2022 202

14247 Vegetable Oilsaturates, mono-unsaturates & poly-unsaturates

FCFO3-OIL30 30 ml 16/02/2022 202

FOOD ADDITIVES & INGREDIENTS

03164 Cola Drinkbenzoic acid, caffeine, acesulfame-K & saccharin

FCFA2-DRN12 150 ml 15/01/2021 195

03165 Soft Drinksweeteners: acesulfame-K, aspartame, cyclamate & saccharin

FCFA26-DRN29 150 ml 17/03/2021 205

03166Coffee (Ground)

caffeine FCFA28-DRH10 2 x 30 g 12/05/2021 204

03167 Soft Drinkbrix, pH, citric acid, sorbic acid, cyclamate, saccharin & benzoic acid

FCFA7-DRN29 150 ml 16/07/2021 204

03168 Soft Drink

colours, a selection from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine

FCFA20-DRN29 150 ml 04/08/2021 204

03169 Cola Drink

caffeine, benzoic acid, total sugars & phosphoric acid (as P2O5)

FCFA13-DRN12 150 ml 14/10/2021 204

14


03170 Tonic Waterbenzoic acid, quinine, acesulfame-K & aspartame

FCFA3-DRN32 150 ml 03/11/2021 204

03171 Cola Drinkbenzoic acid, caffeine, acesulfame-K & saccharin

FCFA2-DRN12 150 ml 21/01/2022 204

03172 Soft Drinksweeteners: acesulfame-K, aspartame, cyclamate & saccharin

FCFA26-DRN29 150 ml 17/03/2022 204

15150 Meatnitrate as NaNO3 & nitrite as

NaNO2FCFA18-MRP23 25 g 13/01/2021 198

15151 Milk Powdernitrate as NaNO3 & nitrite as

NaNO2FCFA18-DRY14 40 g 26/02/2021 198


NaNO2FCFA18-MRP23 25 g 13/05/2021 204

15153Cabbage Purée

nitrate FCFA17-VEG32 70 g 08/06/2021 204

15154 Lettuce Purée nitrate FCFA17-VEG49 70 g 09/08/2021 204


NaNO2FCFA18-MRP23 25 g 10/09/2021 204

15156Rocket (Rucola) Purée

nitrate FCFA17-VEG60 70 g 26/10/2021 204

15157 Spinach Purée nitrate FCFA17-VEG70 70 g 23/11/2021 204


NaNO2FCFA18-MRP23 25 g 12/01/2022 204

15159 Milk Powdernitrate as NaNO3 & nitrite as

NaNO2FCFA18-DRY14 40 g 24/02/2022 204

20179 Tomato Saucebrix, pH, total acidity, sodium, chloride & benzoic acid

FCFA8-CON21 150 g 06/01/2021 198

20180 Meat sulphur dioxide FCFA22-MRP23 100 g 01/03/2021 19820181 Prawns sulphur dioxide FCFA22-SEA20 100 g 12/04/2021 204

20182 Jambrix, pH, benzoic acid, citric acid & sorbic acid

FCFA4-CON7 70 g 29/04/2021 204

20183Chocolate Cake Mix

caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose)

FCFA14-PRO13 50 g 23/06/2021 204

20184Dried Apricot (Water/Fruit Slurry)

sulphur dioxide FCFA22-FRU37 100 g 12/07/2021 204

20185

Sugar Confectionery (Boiled Sweets)


FCFA20-CON17 50 g 15/07/2021 204

20186 Oilantioxidants: total BHA (E320), total BHT (E321) & propyl gallate (E310)

FCFA1-OIL20 50 ml 24/09/2021 204

20187 Meat sulphur dioxide FCFA22-MRP23 100 g 04/10/2021 204

15


20188Hot Pepper Sauce

non-permitted colours (illegal dyes) high level, a selection from the following list: Butter Yellow, Orange II, Para Red, Rhodamine B, Sudan (I, II, III, IV), Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red

FCFA19-CON5 50 ml 11/11/2021 204

20189Dried Apple (Water/Fruit Slurry)

sulphur dioxide FCFA22-FRU36 100 g 22/11/2021 204

20191 Tomato Saucebrix, pH, total acidity, sodium, chloride & benzoic acid

FCFA8-CON21 150 g 05/01/2022 204

20192 Meat sulphur dioxide FCFA22-MRP23 100 g 01/03/2022 204

20193Sweets (gum-based)


FCFA20-CON32 50 g 30/03/2022 204

MYCOTOXINS

Aflatoxins

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)04403 Maize aflatoxins B & G &/or total FCMA2-CCP30 55 g 07/01/2021 196

04404Pistachio (Water/Nut Slurry)

aflatoxins B & G &/or total FCMA2-NUT14 100 g 18/01/2021 196

04406 Milk Powder aflatoxin M1 FCMA1-DRY14 55 g 17/02/2021 196

04408Peanut (Water/Nut Slurry)



aflatoxins B & G &/or total FCMA2-AFE2 55 g 01/04/2021 202

04413Almond (Water/Nut Slurry)


04414 Maize aflatoxins B & G &/or total FCMA2-CCP30 55 g 19/05/2021 202






aflatoxins B & G &/or total FCMA2-AFE2 55 g 14/10/2021 202

04428 Rice aflatoxins B & G &/or total FCMA2-CCP43 55 g 18/11/2021 202

16


04429Peanut Butter (Water/Nut Butter Slurry)

aflatoxins B & G &/or total FCMA2-CON12 100 g 23/11/2021 202

04431 Maize aflatoxins B & G &/or total FCMA2-CCP30 55 g 06/01/2022 202

04432Pistachio (Water/Nut Slurry)





Ergot Alkaloids


22180 Rye Flour

ergot alkaloids: contamination of matrix with two or more from ergometrine, ergotamine, ergosine, ergocristine, ergocryptine & ergocornine & their related-inines

FCME1-CCP47 55 g 10/03/2021 415

22184 Baby Food


FCME1-INF1 30 g 18/08/2021 427

22190 Rye Flour


FCME1-CCP47 55 g 09/03/2022 427

Fusarium Toxins


22178Breakfast Cereal

deoxynivalenol (DON) & zearalenone (ZON)

FCMF1-CCP13 55 g 08/01/2021 256

22179 Cerealtropane alkaloids: atropine & scopolamine

FCMF6-CCP15 30 g 10/02/2021 256

22181 Dried Pasta

deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins

FCMF2-PRO17 75 g 19/05/2021 264

22182 Maize FlourFB1 & FB2 and total fumonisins

(as a sum of FB1 & FB2)FCMF3-CCP32 55 g 18/06/2021 197

22183 Maize Flour

trichothecenes: nivalenol, DON, 3 Ac DON, 15 Ac DON, T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins

FCMF5-CCP32 100 g 21/07/2021 480

17


22185 Animal Feed

deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins

FCMF2-AFE1 75 g 23/09/2021 306

22186Baby Food (Multigrain)

tropane alkaloids: atropine & scopolamine

FCMF6-INF17 30 g 07/10/2021 264


deoxynivalenol (DON) & zearalenone (ZON)

FCMF1-CCP13 55 g 07/01/2022 264

22189 Cerealtropane alkaloids: atropine & scopolamine

FCMF6-CCP15 30 g 23/02/2022 264

Multi-Mycotoxins


04405 Maizeaflatoxin B1 &/or total, DON,

ZON & OTAFCMM1-CCP30 100 g 04/02/2021 340

04407Spice (Black Pepper)

aflatoxins B & G &/or total & OTA

FCMM4-SPI1 75 g 04/03/2021 262

04409 Oat Flouraflatoxin B & G &/or total, OTA, T-2 & HT-2 toxins, sum of T-2 & HT-2 toxins & sterigmatocystin

FCMM11-CCP38 55 g 25/03/2021 340

04411 Maize

aflatoxin B1, DON, ZON, OTA,

FB1 & FB2 & total fumonisins

(as a sum of FB1 & FB2), T-2 &

HT-2 toxins & as sum of T-2 & HT-2 toxins

FCMM3-CCP30 100 g 07/04/2021 490

04412 Infant Food

contamination of matrix with two or more from the following list: aflatoxins B & G &/or total, OTA, ZON, DON, FB1 & FB2 &

total fumonisins (as a sum of FB1 & FB2) & T-2 & HT-2 toxins

& as sum of T-2 & HT-2 toxins

FCMM6-INF8 150 g 22/04/2021 350

04416 Paprikaaflatoxins B & G &/or total & OTA

FCMM4-SPI14 75 g 17/06/2021 270

04417Hazelnut (Water/Nut Slurry)


FCMM4-NUT6 100 g 29/06/2021 202

04418 Maize

aflatoxin B1, DON, ZON, OTA,

FB1 & FB2 & total fumonisins

(as a sum of FB1 & FB2), T-2 &

HT-2 toxins & as sum of T-2 &

HT-2 toxins

FCMM3-CCP30 100 g 22/07/2021 490

04419Dried Figs (Water/Fruit Slurry)


FCMM4-FRU38 150 g 03/08/2021 270

04420Sesame Paste (Tahini)


FCMM4-NUT17 100 g 17/08/2021 270

04421 Chilli Powderaflatoxins B & G &/or total & OTA

FCMM4-SPI6 75 g 09/09/2021 270

18


04424 Infant Foodaflatoxins B & G &/or total & OTA

FCMM4-INF8 55 g 07/10/2021 270

04426 Maize aflatoxin B1, DON, ZON & OTA FCMM2-CCP30 150 g 27/10/2021 350

04427 Gingeraflatoxins B & G &/or total & OTA

FCMM4-SPI23 75 g 04/11/2021 270


contamination of matrix with two or more from the following list: aflatoxin B1, OTA, ZON,

DON, FB1 & FB2 & total

fumonisins (as a sum of FB1 &

FB2)

FCMM5-AFE2 150 g 03/12/2021 350

04433 Maizeaflatoxin B1 &/or total, DON,

ZON & OTAFCMM1-CCP30 100 g 03/02/2022 350

04435Spice - Black Pepper


FCMM4-SPI1 75 g 03/03/2022 270

04437 Oat Flouraflatoxin B & G &/or total, OTA, T-2 & HT-2 toxins, sum of T-2 & HT-2 toxins & sterigmatocystin

FCMM11-CCP38 55 g 23/03/2022 350

17210 Flour OTA & citrinin FCMM8-CCP28 100 g 25/02/2021 19617221 Flour OTA & citrinin FCMM8-CCP28 75 g 02/03/2022 202

22187 Wheat Flour

deoxynivalenol (DON), zearalenone (ZON), T-2 & HT-2 toxins, sum of T-2 & HT-2 toxins & aflatoxin B & G &/or total

FCMM10-CCP49 75 g 10/11/2021 350

Ochratoxin A (OTA)

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)17209 Wheat Flour OTA FCMO1-CCP49 55 g 27/01/2021 19617211 Offal (Liver) OTA FCMO1-MRP27 75 g 22/03/2021 196

17212Dried Vine Fruit (Water/ Fruit Slurry)

OTA FCMO1-FRU43 100 g 06/04/2021 202

17213 Barley Flour OTA FCMO1-CCP4 55 g 20/05/2021 20217214 Coffee (Green) OTA FCMO1-DRH9 55 g 01/07/2021 20217215 Wine OTA FCMO1-DRA13 55 ml 12/08/2021 20217216 Maize Flour OTA FCMO1-CCP32 55 g 02/09/2021 20217217 Instant Coffee OTA FCMO1-DRH18 55 g 15/10/2021 20217218 Animal Feed OTA FCMO1-AFE1 55 g 05/11/2021 202

17219Roasted Coffee

OTA FCMO1-DRH21 55 g 24/11/2021 202

17220 Wheat Flour OTA FCMO1-CCP49 55 g 26/01/2022 20217222 Grape Juice OTA FCMO1-DRN19 55 ml 22/03/2022 202

19

Patulin


1675Apple Juice (Clear)

patulin FCMP1-DRN2 50 ml 26/01/2021 196

1676 Apple Purée patulin FCMP1-FRU2 60 g 04/05/2021 202

1677Apple Juice (Cloudy)


1678Apple Juice (Clear)


NUTRITIONAL & PROXIMATES

Nutritional Components


01141 Canned Meatmoisture, ash, total fat, nitrogen, sodium & chloride

FCNC15-MRP12 150 g 14/01/2021 192

01142Canned Meat Meal

moisture, ash, total fat, nitrogen, sodium & chloride

FCNC15-MRP13 150 g 18/03/2021 192

01145 Canned Meatmoisture, ash, total fat, nitrogen & hydroxyproline

FCNC11-MRP12 150 g 14/05/2021 205


FCNC15-MRP12 150 g 09/07/2021 205


total fat, saturated fatty acids, protein, total sugars & salt

FCNC25-MRP13 150 g 27/08/2021 205

01148 Canned Meatmoisture, ash, total fat, nitrogen & hydroxyproline

FCNC11-MRP12 150 g 30/09/2021 205


moisture, ash, total fat, nitrogen, sodium, chloride & total sugars

FCNC16-MRP13 150 g 19/11/2021 205


FCNC15-MRP12 150 g 13/01/2022 205



FCNC15-MRP13 150 g 17/03/2022 205

0879 Apple Juicebrix, pH, total acidity, sugars, calcium, magnesium, phosphorus, sodium

FCNC27-DRN1 250 ml 28/01/2021 198

0880Pineapple Juice

ash, brix, pH, total acidity, fructose, sucrose, glucose, total sugars, calcium, magnesium, potassium & sodium

FCNC1-DRN27 250 ml 12/05/2021 204

0881 Orange Juice

nutritional elements brix, pH, citric acid, fructose, sucrose, glucose, total sugars, calcium, magnesium, phosphorus, sodium & potassium

FCNC31-DRN26 250 ml 18/08/2021 216

0882Banana Smoothie

brix, pH, total acidity, fructose, sucrose, glucose, total sugars, calcium, magnesium, potassium & sodium

FCNC34-DRN40 250 ml 27/10/2021 204

20


0883 Apple Juice

brix, pH, total acidity, fructose, sucrose, glucose, total sugars, calcium, magnesium, phosphorus, sodium

FCNC27-DRN1 250 ml 27/01/2022 204

10175 Dairy Rationmoisture, ash, total oil, protein, crude fibre, iron, magnesium, manganese & selenium

FCNC20-AFE7 225 g 19/03/2021 365

10176 Pig Rationmoisture, ash, total oil, protein, crude fibre, aNDF, vitamin E & zinc

FCNC19-AFE14 150 g 02/06/2021 225

10177 Soybean mealmoisture, ash, protein & crude fibre

FCNC7-AFE20 150 g 24/09/2021 208

10178Pet Dog Food (Dry)

moisture, ash, protein, total oil, crude fibre, starch & total sugars

FCNC9-PFO7 150 g 28/10/2021 225

10179 Poultry Rationmoisture, ash, total oil, protein, crude fibre, starch, total sugars, calcium & phosphorus

FCNC21-AFE16 225 g 03/12/2021 376

10181 Dairy Rationmoisture, ash, total oil, protein, crude fibre, iron, magnesium, manganese & selenium

FCNC20-AFE7 225 g 18/03/2022 376

20190Sweets (Gum-based)

fructose, glucose & sucrose FCNC38-CON32 50 g 10/12/2021 204

2491 Wheat Flourmoisture at 130°C, ash, nitrogen & total dietary fibre by AOAC

FCNC4-CCP49 150 g 12/02/2021 192

2492 Porridge Oatsmoisture at 130°C, ash, total fat, nitrogen & total dietary fibre by AOAC

FCNC5-CCP40 150 g 23/04/2021 198

2493 Cerealmoisture at 130°C, ash, nitrogen & total dietary fibre by AOAC

FCNC4-CCP15 150 g 02/07/2021 198

2494 Breadcrumbsmoisture, ash, nitrogen, starch, sodium & total dietary fibre by AOAC

FCNC6-PRO9 150 g 09/09/2021 198

2495Baby Food (Cereal Based)

moisture, ash, total fat, nitrogen, dietary fibre, starch, sodium & chloride

FCNC39-INF21 150 g 28/10/2021 198


moisture, ash, total fat, nitrogen & total dietary fibre by AOAC

FCNC13-PRO2 150 g 12/11/2021 198

2497 Wheat Flourmoisture at 130°C, ash, nitrogen & total dietary fibre by AOAC

FCNC4-CCP49 150 g 11/02/2022 198

25192Cheese & Pasta Meal


FCNC15-PRO12 100 g 14/01/2021 192

25193 Buttermoisture, total fat, non-fat solids, pH & chloride

FCNC24-DRY6 200 g 23/02/2021 192

25195Corn/Maize based Snack Food


FCNC15-PRO39 50 g 24/03/2021 192

21


25198 Fish Pastemoisture, ash, total fat, nitrogen, sodium & chloride

FCNC15-SEA15 150 g 09/04/2021 205

25199Condensed Milk

moisture, ash, total fat, nitrogen & total sugars

FCNC14-DRY9 150 ml 13/05/2021 218

25200Milkshake Powder

fructose, galactose, glucose, lactose, maltose & sucrose

FCNC3-DRY15 50 g 11/06/2021 198

25201 Cheesemoisture, ash, total fat, nitrogen, sodium, chloride & starch

FCNC37-DRY7 150 g 29/06/2021 198

25202 Chocolatemoisture, total fat, nitrogen, butyric acid, lactose & sucrose

FCNC23-CON2 150 g 12/07/2021 198

25203 Infant Formulamoisture, ash, total fat, nitrogen, pH, titratable acidity, lactose, sodium & chloride

FCNC29-INF10 50 g 19/08/2021 198

25205 Milk Powdermoisture, ash, total fat, nitrogen, titratable acidity, lactose & pH

FCNC17-DRY14 50 g 29/10/2021 198


pH, titratable acidity, total sugars, monosodium glutamate, magnesium, potassium

FCNC30-PRO39 50 g 05/11/2021 198

25207Cheese & Pasta Meal


FCNC15-PRO12 100 g 13/01/2022 205

25208 Yoghurtash, total fat, nitrogen, pH, titratable acidity, & total sugars

FCNC40-DRY19 150 g 08/02/2022 198

25209 Buttermoisture, total fat, non-fat solids, pH & chloride

FCNC24-DRY6 200 g 22/02/2022 198



FCNC15-PRO39 50 g 16/03/2022 198

3203Processed Food (Ready to Eat Meal)

nutritional components, elements, allergens & contaminants

FCXS1-PRO41 300 g 02/11/2021 459

Nutritional Elements


10174 Premixcalcium, magnesium, manganese, phosphorus, sodium & zinc

FCNE5-AFE17 150 g 28/01/2021 202

10180 Premixcalcium, magnesium, manganese, phosphorus, sodium & zinc

FCNE5-AFE17 150 g 27/01/2022 208


calcium, copper, iodine, iron, magnesium, manganese, phosphorus, potassium, selenium, sodium & zinc

FCNE1-INF10 50 g 11/03/2021 202


calcium, iron, magnesium, phosphorus, potassium, sodium & zinc

FCNE4-CCP13 50 g 07/07/2021 208

22


18104Coconut Powder

calcium, copper, iron, manganese, magnesium, molybdenum, phosphorus, potassium, selenium, sodium & zinc

FCNE9-NUT28 50 g 03/09/2021 208

18105 Milk Powder

calcium, copper, iodine, iron, manganese, magnesium, molybdenum, phosphorus, potassium, selenium, sodium & zinc

FCNE8-DRY14 50 g 17/11/2021 208


calcium, copper, iodine, iron, magnesium, manganese, phosphorus, potassium, selenium, sodium & zinc

FCNE1-INF10 50 g 10/03/2022 208

Vitamins



vitamins B1, B2 (total), B6, B12,

total niacin & folic acidFCNV9-CCP13 100 g 03/02/2021 212

21124Powdered Baby Food

vitamins A, B1, B2, B6, B12, C, E,

folic acid & total niacinFCNV10-INF15 140 g 08/04/2021 249

21125 Infant Formula vitamins A, B12, C, D3, E & K1 FCNV5-INF10 100 g 27/05/2021 225

21126 Fruit Purée vitamin C FCNV2-FRU47 100 g 21/06/2021 208

21127Liquid Vitamin Supplement

vitamins B1, B2 (total), B6 & D3 FCNV11-SUP4 40 ml 01/09/2021 225


vitamins B1, B2 (total), B6, B12,

total niacin & folic acidFCNV9-CCP13 100 g 10/02/2022 225

PESTICIDES (for list of possible residues see pages 31 to 33)

Combined Multi-residue and Single-residue Methods


09136 Basmati Rice

pesticide residues [multi-residue methods] including bromide [single-residue methods]

FCPM15-CCP51 50 g 27/01/2021 199

09136bBlank Basmati Rice

BLANK BLPM2-CCP52 50 g 27/01/2021 63

09141Soya Beans (Dried)

pesticide residues [multi-residue methods] including glyphosate & AMPA [single-residue methods]

FCPX6-VEG67 90 g 10/09/2021 205

09141bBlank Soya Beans (Dried)

BLANK BLPM2-VEG104 90 g 10/09/2021 65

Blank matrix samples are available to purchase with many of the proficiency test materials. Every effort has been made to ensure these do not contain the target analytes. Other analytes may be present.

23


09144 Basmati Rice

pesticide residues [multi-residue methods] including bromide [single-residue methods]

FCPX2-CCP51 50 g 26/01/2022 205

09144bBlank Basmati Rice

BLANK BLPM2-CCP52 50 g 26/01/2022 65

19313Cucumber Purée

pesticide residues [multi-residue methods] including chlormequat/mepiquat [single-residue methods]

FCPX4-VEG38 90 g 07/06/2021 205

19313bBlank Cucumber Purée

BLANK BLPM2-VEG13 90 g 07/06/2021 65

19324Salad Leaf Purée

biocides (quaternary ammonium compounds) [multi-residue methods] including (per)chlorates [single-residue methods]

FCPX1-VEG62 90 g 19/10/2021 205

19324bBlank Salad Leaf Purée

BLANK BLPM6-VEG24 90 g 19/10/2021 65

19327 Green Tea

pesticide residues (tea matrix) [multi-residue] including perchlorate (single residue method)

FCPX5-DRH14 50 g 02/12/2021 205

19327bBlank Green Tea

BLANK BLPM3-DRH1 50 g 02/12/2021 65

19330Herb (Parsley) Purée

biocides (quaternary ammonium compounds) [multi-residue methods] including (per)chlorates [single-residue methods]

FCPX1-VEG45 90 g 21/02/2022 205

19330bBlank Herb (Parsley) Purée

BLANK BLPM6-VEG15 90 g 21/02/2022 65

19332 Tea (Herbal)

pesticide residues (tea matrix) [multi-residue methods] including perchlorate [single-residue methods]

FCPX5-DRH23 50 g 03/03/2022 205

19332bBlank Tea (Herbal)

BLANK BLPM3-DRH26 50 g 03/03/2022 65

Multi Residue Methods


05149 Infant Formulapesticide residues (fat soluble, inc. EU 'red list' - low level and perchlorate)

FCPM10-INF10 50 g 13/01/2021 210

05149bBlank Infant Formula

BLANK BLPM10-INF5 50 g 13/01/2021 63

05150Chicken (Hens) Eggs

pesticide residues (fat soluble and recommended monitoring)

FCPM11-EGG2 50 g 01/03/2021 210

05150bBlank Chicken (Hens) Eggs

BLANK BLPM11-EGG1 50 g 01/03/2021 63

24


05151 Oily Fish pesticide residues (fat soluble) FCPM9-SEA18 50 g 25/05/2021 216

05151b Blank Oily Fish BLANK BLPM9-SEA3 50 g 25/05/2021 65

05152 Infant Formulapesticide residues (specified residues) [fat soluble]

FCPM20-INF10 50 g 09/06/2021 216


BLANK BLPM20-INF5 50 g 09/06/2021 65

05153 Milk Powder pesticide residues (fat soluble) FCPM9-DRY14 50 g 29/07/2021 216

05153bBlank Milk Powder

BLANK BLPM9-DRY2 50 g 29/07/2021 65

05154Animal Fat (Pork)

pesticide residues (fat soluble) FCPM9-FAT2 50 g 07/09/2021 216

05154bBlank Animal Fat (Pork)

BLANK BLPM9-FAT3 50 g 07/09/2021 65

05155Olive Oil (Virgin)

pesticide residues (multi-residue)

FCPM2-OIL34 50 g 13/10/2021 216

05155bBlank Olive Oil (Virgin)

BLANK BLPM2-OIL36 50 g 13/10/2021 65

05156 Prawnsbiocides (quaternary ammonium compounds)

FCPM7-SEA20 50 g 23/11/2021 216

05156b Blank Prawns BLANK BLPM7-SEA4 50 g 23/11/2021 65

05157 Infant Formulapesticide residues (fat soluble, inc. EU 'red list' - low level, and perchlorate)

FCPM10-INF10 50 g 12/01/2022 216


BLANK BLPM10-INF5 50 g 12/01/2022 65



FCPM2-UMI44 10 g 02/02/2022 216

05158bBlank CBD Product (Oil Based)

BLANK BLPM2-UMI45 10 g 02/02/2022 65


pesticide residues (fat soluble & recommended monitoring)

FCPM11-EGG2 50 g 01/03/2022 216


BLANK BLPM11-EGG1 50 g 01/03/2022 65

09137 Wheat Flourpesticide residues (multi-residue)

FCPM2-CCP49 50 g 11/02/2021 199

09137bBlank Wheat Flour

BLANK BLPM2-CCP11 50 g 11/02/2021 63

19309 Lime Puréepesticide residues (multi-residue)

FCPM2-FRU53 90 g 13/04/2021 205

09139Brown Rice (Powdered)


FCPM2-CCP14 50 g 10/06/2021 205

09139bBlank Brown Rice

BLANK BLPM2-CCP5 50 g 10/06/2021 65


FCPM2-CCP49 50 g 11/08/2021 205


BLANK BLPM2-CCP11 50 g 11/08/2021 65

09142 Animal Feedpesticide residues (multi-residue)

FCPM2-AFE1 50 g 06/10/2021 205

09142bBlank Animal Feed

BLANK BLPM2-AFE4 50 g 06/10/2021 65

25



FCPM2-CCP49 50 g 10/02/2022 205


BLANK BLPM2-CCP11 50 g 10/02/2022 65

19304 Honeypesticide residues (honey matrix) [multi-residue]

FCPM8-HON2 90 g 11/01/2021 199

19304b Blank Honey BLANK BLPM8-HON1 90 g 11/01/2021 63

19305Spice (Turmeric)


FCPM2-SPI21 50 g 11/01/2021 199

19305bBlank Spice (Turmeric)

BLANK BLPM2-SPI25 50 g 11/01/2021 63

19306 Melon Puréepesticide residues (specified residues) [multi-residue]

FCPM22-FRU56 90 g 16/02/2021 199

19306bBlank Melon Purée

BLANK BLPM22-FRU20 90 g 16/02/2021 63

19307 Apple Puréepesticide residues (multi-residue)

FCPM2-FRU2 90 g 08/03/2021 199

19307bBlank Apple Purée

BLANK BLPM2-FRU5 90 g 08/03/2021 63

19309bBlank Lime Purée

BLANK BLPM2-FRU17 90 g 13/04/2021 65

19310Yard Long Bean Purée


FCPM2-VEG106 90 g 13/04/2021 205

19310bBlank Yard Long Bean Purée

BLANK BLPM2-VEG105 90 g 13/04/2021 65

19311 Tomato Puréepesticide residues (multi-residue)

FCPM2-VEG76 90 g 10/05/2021 205

19311bBlank Tomato Purée

BLANK BLPM2-VEG29 90 g 10/05/2021 65

19312Chilli Pepper Purée


FCPM2-SPI22 90 g 10/05/2021 205

19312bBlank Chilli Pepper Purée

BLANK BLPM2-SPI24 90 g 10/05/2021 65

19314 Lettuce Puréepesticide residues (multi-residue)

FCPM2-VEG49 90 g 07/06/2021 205

19314bBlank Lettuce Purée

BLANK BLPM2-VEG18 90 g 07/06/2021 65

19315 Celery Puréepesticide residues (multi-residue)

FCPM2-VEG81 90 g 20/07/2021 205

19315bBlank Celery Purée

BLANK BLPM2-VEG84 90 g 20/07/2021 65

19316 Broccoli Puréepesticide residues (multi-residue)

FCPM2-VEG30 90 g 20/07/2021 205

19316bBlank Broccoli Purée

BLANK BLPM2-VEG7 90 g 20/07/2021 65

19317Strawberry Purée


FCPM2-FRU67 90 g 24/08/2021 205

19317bBlank Strawberry Purée

BLANK BLPM2-FRU30 90 g 24/08/2021 65

19318 Potato Puréepesticide residues (multi-residue)

FCPM2-VEG59 90 g 24/08/2021 205

19318bBlank Potato Purée

BLANK BLPM2-VEG23 90 g 24/08/2021 65

26


19319Herb (Coriander) Purée


FCPM2-VEG35 90 g 13/09/2021 205

19319bBlank Herb (Coriander) Purée

BLANK BLPM2-VEG11 90 g 13/09/2021 65

19321 Mango Puréepesticide residues (multi-residue)

FCPM2-FRU55 90 g 21/09/2021 205

19321bBlank Mango Purée

BLANK BLPM2-FRU19 90 g 21/09/2021 65

19323Grape (Table) Purée


FCPM2-FRU48 90 g 19/10/2021 205

19323bBlank Grape (Table) Purée

BLANK BLPM2-FRU14 90 ml 19/10/2021 65

19325 Peach Puréepesticide residues (multi-residue)

FCPM2-FRU59 90 g 08/11/2021 205

19325bBlank Peach Purée

BLANK BLPM2-FRU23 90 g 08/11/2021 65

19326 Honeypesticide residues (honey matrix) [multi-residue]

FCPM8-HON2 90 g 08/11/2021 205

19326b Blank Honey BLANK BLPM8-HON1 90 g 08/11/2021 65

19328Spice (Black Pepper)


FCPM2-SPI1 50 g 17/01/2022 205

19328bBlank Spice (Black Pepper)

BLANK BLPM2-SPI2 50 g 17/01/2022 65

19329Pumpkin Purée

pesticide residues (specified residues) [multi-residue]

FCPM22-VEG102

90 g 17/01/2022 205

19329bBlank Pumpkin Purée

BLANK BLPM22-VEG101 90 g 17/01/2022 65

19331 Apple Puréepesticide residues (multi-residue)

FCPM2-FRU2 90 g 21/02/2022 205

19331bBlank Apple Purée

BLANK BLPM2-FRU5 90 g 21/02/2022 65

Single Residue Methods


09138 Oatschlormequat, mepiquat, glyphosate & AMPA

FCMS2-CCP39 100 g 28/04/2021 205

09138bBlank Oat Flour

BLANK BLMS5-CCP67 100 g 28/04/2021 65

09143 Wheat Flourchlormequat, mepiquat, glyphosate & AMPA

FCMS2-CCP49 100 g 18/11/2021 205


BLANK BLMS5-CCP11 100 g 18/11/2021 65

19308 Pear Purée dithiocarbamates FCMS3-FRU60 90 g 22/03/2021 267

19308bBlank Pear Purée

BLANK BLMS3-FRU24 90 g 22/03/2021 82

19320 Lettuce Purée dithiocarbamates FCMS3-VEG49 90 g 13/09/2021 275

19320bBlank Lettuce Purée

BLANK BLMS3-VEG18 90 g 13/09/2021 84

27


19322 Tomato Puréesingle residue monitoring (see page 30 for potential residues)

FCMS5-VEG76 100 g 04/10/2021 350

19322bBlank Tomato Purée

BLANK BLPM1-VEG29 100 g 04/10/2021 84

19333 Grape Purée dithiocarbamates FCMS3-FRU49 90 g 21/03/2022 275

19333bBlank Grape Purée

BLANK BLMS3-FRU15 90 g 21/03/2022 84

QUALITY

Honey


2848 Honeymoisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF), diastase & free acid

FCQH3-HON2 100 g 09/03/2021 196

2849 Honeymoisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase

FCQH2-HON2 100 g 22/06/2021 202

2850 Honey

fructose, glucose, sucrose, hydroxymethylfurfural (HMF), diastase, electrical conductivity, lead (Pb) & pH

FCQH1-HON2 100 g 02/11/2021 202

2851 Honeymoisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF), diastase & free acid

FCQH3-HON2 100 g 08/03/2022 202

Meat & Fish Indices


01144 Salami Water Activity FCQW1-MRP3815 g

(4 slices)04/05/2021 205

01152 Canned Meattotal volatile basic nitrogen (TVB-N)

FCQT1-MRP12 150 g 31/03/2022 205

25194 Canned Fishtotal volatile basic nitrogen (TVB-N)

FCQT1-SEA7 150 g 05/03/2021 192


FCQT1-SEA7 150 g 08/09/2021 205


FCQT1-SEA7 150 g 04/03/2022 205

Olive Oil and Vegetable Oil


14228 Olive Oilperoxide value, acidity, anisidine value & iodine value

FCQO1-OIL22 100 ml 12/01/2021 196

14230 Olive Oilperoxide value, acidity, K232 &

K270FCQO2-OIL22 100 ml 30/03/2021 196

14234 Vegetable Oilperoxide value (lower level), acidity (lower level), anisidine value & iodine value

FCQO1-OIL30 50 ml 14/06/2021 202


FCQO1-OIL22 100 ml 13/07/2021 202

28



K270FCQO2-OIL22 100 ml 14/09/2021 202

14242 Vegetable Oilperoxide value (lower level), acidity (lower level), anisidine value & iodine value

FCQO1-OIL30 50 ml 09/11/2021 202


FCQO1-OIL22 100 ml 04/01/2022 202


K270FCQO2-OIL22 100 ml 29/03/2022 202

VETERINARY DRUG RESIDUES (for list of possible residues please see pages 34-35)


02418 Fish Musclemalachite green, leucomalachite green & total malachite green

FCVD11-SEA13 20 g 04/01/2021 258

02418bBlank Fish Muscle

BLANK BLVD11-SEA2 20 g 04/01/2021 78

02419 Fish Muscle sulfonamides FCVD20-SEA13 20 g 04/01/2021 258


BLANK BLVD20-SEA2 20 g 04/01/2021 78

02420 Honey tetracyclines & macrolides FCVD27-HON2 40 g 19/01/2021 258

02420b Blank Honey BLANK BLVD27-HON1 40 g 19/01/2021 78

02421 Honey nitrofuran metabolites FCVD12-HON2 20 g 19/01/2021 258

02422Chicken Muscle

quinolones & fluoroquinolones FCVD15-MRP17 20 g 01/02/2021 258

02422bBlank Chicken Muscle

BLANK BLVD15-MRP50 20 g 01/02/2021 78

02423 Bovine Liver glucocorticoids FCVD9-MRP7 20 g 01/02/2021 25802424 Prawns tetracyclines FCVD22-SEA20 20 g 15/02/2021 25802424b Blank Prawns BLANK BLVD22-SEA4 20 g 15/02/2021 78

02425 Bovine Liversulfonamides & trimethoprim & macrolides

FCVD29-MRP7 20 g 15/02/2021 258

02425bBlank Bovine Liver

BLANK BLVD29-MRP51 20 g 15/02/2021 78

02426 Bovine Serum specified hormones FCVD31-MRP52 2 x 25 ml 08/03/2021 295

02426bBlank Bovine Serum

BLANK BLVD31-MRP53 2 x 25 ml 08/03/2021 78

02427 Honeychloramphenicol, florfenicol, thiamphenicol & total phenicols

FCVD5-HON2 20 g 12/04/2021 266

02427b Blank Honey BLANK BLVD5-HON1 20 g 12/04/2021 8002428 Fish Muscle quinolones & fluoroquinolones FCVD15-SEA13 20 g 26/04/2021 266


BLANK BLVD15-SEA2 20 g 26/04/2021 80

02429Chicken Muscle

nitrofuran metabolites FCVD12-MRP17 20 g 26/04/2021 266


BLANK BLVD12-MRP50 20 g 26/04/2021 80

Blank matrix samples are available to purchase with many of the proficiency test materials. Every effort has been made to ensure these do not contain the target analytes. Other analytes may be present. Where possible, naturally incurred residues are used.

29


02430Chicken Muscle

tetracyclines FCVD26-MRP17 40 g 17/05/2021 266


BLANK BLVD22-MRP50 20 g 17/05/2021 80

02431 Fish Muscle avermectins FCVD1-SEA13 20 g 17/05/2021 266


BLANK BLVD1-SEA2 20 g 17/05/2021 80

02432 Pig Liver Beta-agonists FCVD17-MRP30 20 g 01/06/2021 266

02432b Blank Pig Liver BLANK BLVD17-MRP56 20 g 01/06/2021 80

02433 Fish Muscle illegal dyes (veterinary drugs) FCVD10-SEA13 20 g 01/06/2021 266


BLANK BLVD10-SEA2 20 g 01/06/2021 80

02434 Bovine Urine synthetic hormones FCVD21-MRP9 25 ml 21/06/2021 266

02434bBlank Bovine Urine

BLANK BLVD21-MRP46 25 ml 21/06/2021 80

02435 Bovine Liver tetracyclines & aminoglycosides FCVD26-MRP7 40 g 05/07/2021 266


BLANK BLVD26-MRP51 40 g 05/07/2021 80

02436 Fish Musclechloramphenicol, florfenicol, thiamphenicol & total phenicols

FCVD5-SEA13 20 g 05/07/2021 266


BLANK BLVD5-SEA2 20 g 05/07/2021 80

02437 Honey sulfonamides FCVD20-HON2 20 g 19/07/2021 26602437b Blank Honey BLANK BLVD20-HON1 20 g 19/07/2021 8002438 Fish Muscle nitrofuran metabolites FCVD12-SEA13 20 g 19/07/2021 266


BLANK BLVD12-SEA2 20 g 19/07/2021 80

02439 Chicken Liver coccidiostats FCVD7-MRP16 20 g 02/08/2021 266

02439bBlank Chicken Liver

BLANK BLVD7-MRP54 20 g 02/08/2021 80

02440Chicken Muscle

nitroimidazoles FCVD13-MRP17 20 g 02/08/2021 266


BLANK BLVD13-MRP50 20 g 02/08/2021 80

02441 Honey quinolones & fluoroquinolones FCVD15-HON2 20 g 17/08/2021 26602441b Blank Honey BLANK BLVD15-HON1 20 g 17/08/2021 8002442 Sheep Muscle avermectins & anthelmintics FCVD2-MRP42 40 g 31/08/2021 266

02442bBlank Sheep Muscle

BLANK BLVD23-MRP57 40 g 31/08/2021 80

02443 Pig Muscle tranquilizers FCVD32-MRP32 20 g 31/08/2021 266

02443bBlank Pig Muscle

BLANK BLVD24-MRP48 20 g 31/08/2021 80

02444 Bovine Milkchloramphenicol, florfenicol, thiamphenicol & total phenicols

FCVD5-DRY4 25 ml 27/09/2021 266

02444bBlank Bovine Milk

BLANK BLVD5-DRY20 25 ml 27/09/2021 80

02445 Bovine MilkBeta-lactams (penicillins & cephalosporins)

FCVD18-DRY4 25 ml 27/09/2021 266

02445bBlank Bovine Milk

BLANK BLVD18-DRY20 25 ml 27/09/2021 80

30


02446 Poultry Feedcoccidiostats & chloramphenicol (contaminant levels)

FCVD8-AFE15 40 g 01/10/2021 266

02447 Prawns nitrofuran metabolites FCVD12-SEA20 20 g 18/10/2021 26602447b Blank Prawns BLANK BLVD12-SEA4 20 g 18/10/2021 8002448 Fish Muscle tetracyclines FCVD22-SEA13 20 g 18/10/2021 266


BLANK BLVD22-SEA2 20 g 18/10/2021 80

02449 Prawnschloramphenicol, florfenicol, thiamphenicol & total phenicols

FCVD5-SEA20 20 g 15/11/2021 266

02449b Blank Prawns BLANK BLVD5-SEA4 20 g 15/11/2021 80

02450 Bovine Musclenon-steroidal anti-inflammatory drugs (NSAIDs)

FCVD24-MRP8 25 g 15/11/2021 266

02450bBlank Bovine Muscle

BLANK BLVD25-MRP49 25 g 15/11/2021 80

02451 Corned Beef Beta-agonists FCVD17-MRP18 20 g 22/11/2021 266

02452 Honeynitroimidazoles & aminoglycosides

FCVD14-HON2 40 g 06/12/2021 266

02452b Blank Honey BLANK BLVD14-HON1 40 g 06/12/2021 80

02453 Bovine UrineNatural Hormones and Thyrostats

FCVD33-MRP9 25 ml 06/12/2021 266

02454 Fish Musclemalachite green, leucomalachite green & total malachite green

FCVD11-SEA13 20 g 10/01/2022 266


BLANK BLVD11-SEA2 20 g 10/01/2022 80

02455 Fish Muscle sulfonamides FCVD20-SEA13 20 g 10/01/2022 266


BLANK BLVD20-SEA2 20 g 10/01/2022 80

02456 Honey tetracyclines & macrolides FCVD27-HON2 40 g 18/01/2022 26602456b Blank Honey BLANK BLVD27-HON1 40 g 18/01/2022 8002457 Honey nitrofuran metabolites FCVD12-HON2 20 g 18/01/2022 26602457b Blank Honey BLANK BLVD12-HON1 20 g 18/01/2022 80


quinolones & fluoroquinolones FCVD15-EGG2 20 g 31/01/2022 266


BLANK BLVD15-EGG1 20 g 31/01/2022 80

02459 Bovine Muscle glucocorticoids FCVD9-MRP8 20 g 31/01/2022 266

02459bBlank Bovine Muscle

BLANK BLVD28-MRP49 20 g 31/01/2022 80

02460 Prawns tetracyclines FCVD22-SEA20 20 g 14/02/2022 26602460b Blank Prawns BLANK BLVD22-SEA4 20 g 14/02/2022 80

02461 Bovine Liversulfonamides & trimethoprim & macrolides

FCVD29-MRP7 40 g 14/02/2022 266


BLANK BLVD29-MRP51 20 g 14/02/2022 80

02462 Bovine Serum specified hormones FCVD31-MRP52 2 x 25 ml 07/03/2022 304

02462bBlank Bovine Serum

BLANK BLVD31-MRP53 2 x 25 ml 07/03/2022 80

31

Potential pesticide residues

multi-residue2,4-D (free acid only), 2-phenylphenol (ortho-phenylphenol), 6-benzylaminopurine, abamectin (sum of avermectin B1a and B1b only), acephate, acetamiprid, acetochlor, aclonifen, acrinathrin, aldicarb, aldicarb-sulfone (aldoxycarb), aldicarb-sulfoxide, aldrin, allethrin, ametoctradin, amidosulfuron, atrazine, azinphos-ethyl, azinphos-methyl, azoxystrobin, benalaxyl, bendiocarb, benthiavalicarb-isopropyl, bifenthrin (sum of isomers), biphenyl, bitertanol, boscalid, bromophos-ethyl, bromopropylate, bromuconazole (sum of diastereoisomers), bupirimate, buprofezin, cadusafos, carbaryl, carbendazim, carbofuran, carbofuran (3-hydroxy), carboxin, chlorantraniliprole (rynaxypyr), chlordane (cis), chlordane (oxy), chlordane (trans), chlorfenapyr, chlorfenvinphos (sum of E and Z isomers), chloridazon, chlorobenzilate, chlorothalonil, chlorpropham, chlorpyrifos (ethyl), chlorpyrifos-methyl, chlorthaldimethyl, clofentezine, clothianidin, coumaphos, cyazofamid, cyflufenamid, cyfluthrin (sum of constituent isomers), cyhalothrin-lambda (includes cyhalothrin-gamma) (sum of R,S and S,R isomers), cymoxanil, cypermethrin (sum of constituent isomers), cyproconazole, cyprodinil, cyromazine, DDD-pp (TDE), DDE-pp, DDT-op, DDT-pp, deltamethrin, demeton-S-methyl, demeton-S-methyl-sulfone, demeton-S-methyl-sulfoxide (oxydemeton-methyl), diafenthiuron, diazinon, dichlorvos, dicloran, dicofol (sum of p,p' and o,p' isomers), dicrotophos, dieldrin, diethofencarb, difenoconazole, diflubenzuron, dimethoate, dimethomorph (sum of isomers), dimoxystrobin, diniconazole, dinotefuran, diphenylamine, disulfoton, disulfoton-sulfone, disulfoton-sulfoxide, diuron, dodine, Emamectin (as emamectin benzoate B1a, expressed as emamectin), endosulfan I (alpha), endosulfan II (beta), endosulfan-sulfate, endrin, EPN, epoxiconazole, ethiofencarb, ethiofencarb-sulfone, ethiofencarb-sulfoxide, ethion, ethirimol, ethoprophos, etofenprox, etoxazole, etrimfos, famoxadone, fenamidone, fenamiphos, fenamiphos-sulfone, fenamiphos-sulfoxide, fenarimol, fenazaquin, fenbuconazole, fenbutatin oxide, fenhexamid, fenitrothion, fenoxycarb, fenpropathrin, fenpropidin (sum of fenpropidin and its salts, expressed as fenpropidin), fenpropimorph (sum of isomers), fenpyroximate, fensulfothion, fensulfothion-oxon, fensulfothion-oxon-sulfone, fensulfothion-sulfone, fenthion (parent compound only), fenthion-sulfone, fenthion-sulfoxide, fenvalerate (sum of constituent isomers in any ratio including esfenvalerate), fipronil (parent compound only), fipronil-desulfinyl,fipronil-sulfone, flonicamid, fluazifop (free acid), fluazinam, flubendiamide, flucythrinate, fludioxonil, flufenacet (parent compound only), flufenoxuron, fluopicolide, fluopyram, fluoxastrobin (sum of fluoxastrobin and its Z-isomer), fluquinconazole, flusilazole, flutolanil, flutriafol, fluvalinate (tau), fluxapyroxad, fonofos, fosthiazate, furathiocarb, haloxyfop (free acid), HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), heptachlor,

heptachlor-epoxide (cis), heptachlor-epoxide (trans), heptenophos, hexaconazole, hexythiazox, imazalil, imidacloprid, indoxacarb (sum of indoxacarb and its R enantiomer), iprodione, iprovalicarb, isocarbofos, isofenphos (ethyl), isofenphos-methyl, isoprocarb, isoprothiolane, isoproturon, kresoxim-methyl, lenacil, linuron, ufenuron, malaoxon, malathion, mandipropamid, mecarbam, mepanipyrim, metaflumizone (sum of E and Z isomers), metalaxyl (sum of constituent isomers including metalaxyl-M), metamitron, metconazole, methacrifos, methamidophos, methidathion, methiocarb, methiocarb-sulfone, methiocarb-sulfoxide, methomyl, methoxychlor, methoxyfenozide, metolachlor (sum of constituent isomers including S-metolachlor), metrafenone, metribuzin, mevinphos (sum of E and Z isomers), molinate, monocrotophos, monolinuron, myclobutanil, nitrofen, novaluron, omethoate, oxadiazon, oxadixyl, oxamyl, oxyfluorfen, paclobutrazol, parathion (-ethyl),parathion-methyl, penconazole, pencycuron, pendimethalin, penflufen, pentachloroaniline, penthiopyrad, permethrin (sum of isomers), phenthoate, phorate, phorate-sulfone, phorate-sulfoxide, phosalone, phosmet, phosphamidon, phoxim, phthalimide, picoxystrobin, piperonyl butoxide, pirimicarb, pirimicarb (desmethyl), pirimiphos-ethyl,pirimiphos-methyl, prochloraz (parent compound only), procymidone, profenofos, promecarb, prometryn, propamocarb, propargite, propetamphos, propiconazole, propoxur, propyzamide, proquinazid, prosulfocarb, prothioconazole-desthio (sum of isomers), prothiofos, pymetrozine, pyraclostrobin, pyrazophos, pyrethrin (sum), pyridaben, pyridalyl, pyridaphenthion, pyrimethanil, pyriproxyfen, quassia, quinalphos, quinoxyfen, quintozene, spinetoram, spinosad (sum of spinosyn A and D), spirodiclofen, spiromesifen, spirotetramat (parent compound only), spirotetramat-enol (expressed as spirotetramat), spiroxamine, tebuconazole, tebufenozide, tebufenpyrad, tecnazene, teflubenzuron, tefluthrin, terbufos, terbufos-sulfone, terbufos-sulfoxide, terbuthylazine, tetrachlorvinphos, tetraconazole, tetradifon, tetramethrin (sum of constituent isomers), TFNA, TFNG, thiabendazole, thiacloprid, thiamethoxam, thiodicarb, thiophanate-methyl, THPI, tolclofos-methyl, tolfenpyrad, tolylfluanid, triadimefon, triadimenol, triallate, triazophos, tricyclazole, trifloxystrobin, triflumuron, trifluralin, triticonazole, vinclozolin, zoxamide

multi-residue: honey matrix acetamiprid, amitraz (parent compound only), clothianidin, coumaphos, dinotefuran, DMF (N-2,4-dimethylformamide) DMPF (N-2,4-dimethylphenylformamide), fluvalinate (tau), imidacloprid, methamidophos, nitenpyram, thiacloprid, thiamethoxam

32

multi-residue: tea matrix 2-phenylphenol (ortho-phenylphenol), abamectin (sum of avermectin B1a and B1b only), acetamiprid, anthraquinone, bifenthrin (sum of isomers), boscalid, buprofezin, carbaryl, carbendazim, chlorfenapyr, chlorfenvinphos (sum of E and Z isomers), chlorothalonil, chlorpyrifos (ethyl), cyhalothrin-lambda (includes cyhalothrin-gamma) (sum of R,S and S,R isomers), cypermethrin (sum of constituent isomers), DDD-pp (TDE), DDE-pp, DDT-op, DDT-pp, deltamethrin, diazinon, dicofol (sum of p,p' and o,p' isomers), dimethoate, dinotefuran, diuron, endosulfan I (alpha), endosulfan II (beta),endosulfan-sulfate, ethion, fenazaquin, fenitrothion, fenpropathrin, fenpropimorph (sum of isomers), fenvalerate (sum of constituent isomers in any ratio including esfenvalerate), fipronil-sulfone, flubendiamide, HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), imidacloprid, linuron, malathion, methomyl, monocrotophos, oxadixyl, permethrin (sum of isomers), phenthoate, phosalone, picoxystrobin, pirimiphos-methyl, procymidone, propargite, propiconazole, pyridaben, pyrimethanil, quinalphos, tebuconazole, terbuthylazine, tolfenpyrad, triazophos, trifloxystrobin

specified residues acetamiprid, aldrin, azoxystrobin, bifenthrin (sum of isomers), chlorpyrifos (ethyl), chlorpyrifos-methyl, cypermethrin, (sum of constituent isomers), DDE-pp, deltamethrin, dichlorvos, dieldrin, dimethoate, endosulfan I (alpha), endosulfan II (beta), endosulfan-sulfate, endrin, ethion, fenpropathrin, fenthion-sulfone, HCH-A (alpha hexachlorocyclohexane), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), malathion, parathion-methyl, permethrin (sum of isomers), triazophos

recommended monitoring abamectin (sum of avermectin B1a and B1b only) amitraz (parent compound only), bifenthrin, cypermethrin (sum of constituent isomers), diazinon,

dichlorvos, DMF (N-2,4-dimethylformamide), DMPF (N-2,4-dimethylphenylformamide), etoxazole, fipronil (parent compound only), fipronil-desulfinyl, fipronil-sulfone, flufenoxuron, pyridaben, pyriproxyfen, thiamethoxam

single residues monitoring2,4-DB, AMPA, bromide, chlormequat (sum of chlormequat and its salts, expressed as chlormequat chloride), dithiocarbamates, ethephon, ETU, fenbutatin oxide, glyphosate, haloxyfop (free acid), maleic hydrazide, mepiquat (sum of mepiquat and its salts, expressed as mepiquat chloride) MPPA, phosphoric acid, PTU, quizalofop (free acid)

Fat solubleabamectin (sum of avermectin B1a and B1b only), acephate, aldicarb,aldicarb-sulfone (aldoxycarb),

aldicarb-sulfoxide, aldrin, allethrin, azamethiphos, azinphos-ethyl, azinphos-methyl, bendiocarb, bifenthrin (sum of isomers), bixafen, boscalid, bromophos-ethyl, cadusafos, carbaryl, carbendazim, carbofuran, carbofuran (3-hydroxy), chlordane (cis), chlordane (oxy), chlordane (trans), chlorfenvinphos (sum of E and Z isomers), chlorobenzilate, chlorpropham, chlorpyrifos (ethyl), chlorpyrifos-methyl, coumaphos, cyfluthrin (sum of constituent isomers), cyhalothrin-lambda (includes cyhalothrin-gamma) (sum of R,S and S,R isomers), cypermethrin (sum of constituent isomers), cyproconazole, cyromazine, DDD-pp (TDE), DDE-pp, DDT-op,DDT-pp, deltamethrin, diazinon, dieldrin, diflubenzuron, dimethoate, endosulfan I (alpha), endosulfan II (beta),endosulfan-sulfate, endrin, epoxiconazole, ethoprophos, etofenprox, etoxazole, famoxadone, fenitrothion, fenoxycarb, fenpropathrin, fenpropidin (sum of fenpropidin and its salts, expressed as fenpropidin), fenpropimorph (sum of isomers), fensulfothion-sulfone, fenthion (parent compound only), fenthion-sulfoxide, fenvalerate (sum of constituent isomers in any ratio including esfenvalerate), fipronil (parent compound only), fipronil-desulfinyl, fipronil-sulfone, fluazifop (free acid), flufenoxuron, flumethrin, fluquinconazole, flusilazole, fluvalinate (tau), haloxyfop (free acid), HCB (hexachlorobenzene), HCH-A (alpha hexachlorocyclohexane), HCH-B (beta hexachlorocyclohexane), HCH-D (delta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), heptachlor, heptachlor-epoxide (cis), heptachlor-epoxide (trans), indoxacarb (sum of indoxacarb and its R enantiomer), lufenuron, malathion, metaflumizone (sum of E and Z isomers),metazachlor,methacrifos,methamidophos,methidathion,methiocarb,methiocarb-sulfone,methiocarb-sulfoxide, methomyl, methoxychlor, nitrofen, omethoate, oxamyl, parathion (-ethyl), parathion-methyl, PCB 101, PCB 118, PCB 138, PCB 153, PCB 180, PCB 28, PCB 52, pendimethalin, permethrin (sum of isomers), phosmet, phoxim, pirimicarb, pirimicarb (desmethyl), pirimiphos-methyl, prochloraz (parent compound only), profenofos, propetamphos, propoxur, prothioconazole-desthio (sum of isomers), pyrazophos, pyridaben, pyriproxyfen, quintozene, spinosad (sum of spinosyn A and D), tebuconazole, tecnazene, teflubenzuron, tefluthrin, tetrachlorvinphos, tetraconazole, thiacloprid, thiamethoxam, thiodicarb, triazophos, trifluralin, vinclozolin

EU red listaldrin, cadusafos, chlorpropham, demeton-S-methyl, demeton-S-methyl-sulfone, demeton-S-methyl-sulfoxide (oxydemeton-methyl), dieldrin, dimethoate, diphenylamine, disulfoton, disulfoton-sulfone, disulfoton-sulfoxide, endrin, ethoprophos, fensulfothion fensulfothion-oxon, fensulfothion-oxon-sulfone, fensulfothion-sulfone, fentin (as triphenyltin cation), fipronil (parent compound only), fipronil desulfinyl, fipronil sulphone, haloxyfop (free acid), HCB (hexachlorobenzene), heptachlor, nitrofen, omethoate, terbufos, terbufos-sulfone, terbufos-sulfoxide,

33

Potential Fish Species

Quaternary Ammonium CompoundsBAC 10 (Benzyldimethyldecylammonium Chloride),BAC 12 (Benzyldimethyldodecylammonium Chloride), BAC 14 (Benzyldimethyltetradecylammonium Chloride), BAC 16 (Benzyldimethylhexadecylammonium Chloride), DDAC (Didecyldimethylammonium Chloride)

disinfection by-products BAC 10 (Benzyldimethyldecylammonium Chloride),BAC 12 (Benzyldimethyldodecylammonium Chloride), BAC 14 (Benzyldimethyltetradecylammonium Chloride), BAC 16 (Benzyldimethylhexadecylammonium Chloride), DDAC (Didecyldimethylammonium Chloride), chlorate, perchlorate

specified residues (infant formula)DDD-pp, (TDE), DDE-pp, HCB (hexachlorobenzene), HCH-B (beta hexachlorocyclohexane), HCH-G (gamma hexachlorocyclohexane / lindane), PCB 52, PCB 138

fish speciationGadus macrocephalus (Tilesius 1810), Gadus morhua (Linnaeus 1758), Hippoglossus hippoglossus (Linnaeus 1758), Limanda limanda (Linnaeus 1758), Melanogrammus aeglefinus (Linnaeus 1758), Merlangius merlangus (Linnaeus 1758), Merluccius merluccius (Linnaeus 1758), Pangasius hypophthalmus (Sauvage 1878), Pleuronectes platessa (Linnaeus 1758), Pollachius virens (Linnaeus 1758), Gadus chalcogrammus (Pallas 1814) (previously Theragra chalcogramma)

34

Potential veterinary drug residues

aminoglycosidesapramycin, dihydrostreptomycin, gentamicin, kanamycin, neomycin, paromomycin, spectinomycin, streptomycin, total aminoglycosides

anthelmintics5-hydroxythiabendazole, albendazole, albendazole-2-amino-sulfone, albendazole-sulfone, albendazole-sulfoxide, aminoflubendazole, aminomebendazole (mebendazole amine), amino-oxibendazole, cambendazole, clorsulon, closantel, coumaphos, derquantel, febantel, fenbendazole, flubendazole, hydroxyflubendazole, hydroxymebendazole, ketotriclabendazole, levamisole, mebendazole, monepantel, monepantel-sulfone, morantel, niclosamide, nitroxinil (nitroxynil), oxfendazole, oxfendazole-sulfone, oxibendazole, oxyclozanide, rafoxanide, thiabendazole, total albendazole-sulfone, total benzimidazoles, total flubendazole, total mebendazole, total oxfendazole-sulfone (sum of extractable residues which may be oxidized to oxfendazole sulfone), total thiabendazole, total triclabendazole, triclabendazole, triclabendazole-sulfone, triclabendazole-sulfoxide

avermectinsabamectin (avermectin B1a only), doramectin, emamectin, eprinomectin, ivermectin, moxidectin, total avermectins

b-agonistsbrombuterol, bromchlorbuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol, clenproperol, hydroxyclenbuterol, hydroxymethylclenbuterol,isoxsuprine, mabuterol, mapenterol, ractopamine, ritodrine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol, total β-agonists

b-lactamsamoxicillin, ampicillin, benzyl penicillin (penicillin G), cefalexin, cefalonium, cefapirin, cefazolin, cefoperazone, cefquinome, cloxacillin, desacetylcefapirin, dicloxacillin, nafcillin, oxacillin, penicillin V

coccidiostatsclopidol, decoquinate, diclazuril, DNC (nicarbazin component), halofuginone, lasalocid, maduramycin, monensin, narasin, robenidine, salinomycin, semduramycin, toltrazuril-sulfpne, total coccidiostats

glucocorticoidsbetamethasone, dexamethasone, prednisolone, total glucocorticoids

gestagens, altrenogest, chlormadinone, medroxyprogesterone, megestrol, melengestrol, total gestagens

illegal dyes (veterinary drugs)

brilliant green, crystal violet, leucomalachite

green,malachite green, total malachite green, leucocrystal violet, total crystal violet, total veterinary dyes

nitrofuran metabolitesAHD (bound), AHD (total), AMOZ (bound), AMOZ (total), AOZ (bound), AOZ (total), SEM (bound), SEM (total), total nitrofuran metabolites

nitroimidazoles2-hydroxy dimetridazole (HMMNI), 2-hydroxy

ipronidazole, 2-hydroxy metronidazole, dimetridazole, ipronidazole, metronidazole, ronidazole, total nitroimidazoles

macrolides 3-O-acetyltylosin, erythromycin, gamithromycin, josamycin, lincomycin, oleandamycin, pirlimycin, rifampicin, spiramycin, tildipirosin, tilmicosin, total macrolides, total tylosin, tulathromycin, tylosin A, tylosin B, tylvalosin (aivlosin), virginiamycin

natural hormones 17alpha-19-nortestosterone, 17beta-oestradiol (estradiol), 17beta-testosterone, beta-boldenone, boldenone, methyltestosterone, total natural hormones

non-steroidal anti-inflammatory drugs (NSAIDs)

5-hydroxyflunixin, carprofen, diclofenac, flunixin,ibuprofen, ketoprofen, meloxicam, naproxen, niflumic acid, oxyphenylbutazone, phenylbutazone, tolfenamic

acid, total NSAIDs, vedaprofen

phenicolschloramphenicol, florfenicol, florfenicol-amine, thiamphenicol

quinolones & fluoroquinolonesciprofloxacin, danofloxacin, difloxacin, enrofloxacin,

flumequine, marbofloxacin, nalidixic acid, norfloxacin,

oxolinic acid, sarafloxacin, total quinolones

sulfonamidesdapsone, sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanidine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulfanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole, total sulfonamides

35

synthetic hormonesalpha-trenbolone, beta-trenbolone, cis-diethylstilbestrol (DES), dienestrol, ethinylestradiol, hexoestrol, methylboldenone, methyltestosterone, stanozolol, taleranol (beta-zearalanol), total diethylstilbestrol (DES), total synthetic hormones, trans-diethylstilbestrol (DES), zearalenone (ZON), zeranol (alpha-zearalanol)

tetracyclines4-epi-chlortetracycline, 4-epi-oxytetracycline, 4-epi-tetracycline, chlortetracycline, doxycycline, oxytetracycline, tetracycline, total chlortetracycline (parent + epimer), total oxytetracycline (parent + epimer), total tetracycline (parent + epimer), total tetracyclines (all)

thyrostats6-methyl-2-thiouracil (methylthiouracil), dimethylthiouracil, ethylthiouracil, mercaptobenzimidazole, methimazole (tapazole), phenylthiouracil, propylthiouracil, thiouracil, total

thyrostats

tranquilizersacepromazine, azaperol, azaperone, carazolol, chlorpromazine, haloperidol, propionylpromazine, total tranquilizers, xylazine

36


37

EUR

FOOD AND BEVERAGEMICROBIOLOGYProficiency Test List - GBP

Jan 2021 - Mar 2022

38

FOOD AND BEVERAGE MICROBIOLOGY PROFICIENCY TESTS

Quantity discounts (for materials purchased in a single order)

Quantity Purchased Discount Applied11 - 25 tests 10%26 or more 25%

INDICATOR ORGANISMS

Beef


M260e14 BeefCoagulase Positive Staphylococci (Enumeration)

FMOE14-MRP2equivalent to

10 g25/01/2021 130

M261e13 BeefBacillus cereus and

Aerobic Plate Count (Enumeration)


10 g22/02/2021 130

M262e05 BeefEnterobacteriaceae and Aerobic Plate Count (Enumeration)


10 g29/03/2021 130

M262e06 Beef

Clostridium spp., Sulphite

Reducing Clostridia, Clostridium Perfringens

(Enumeration)


10 g29/03/2021 130

M263e10 BeefEscherichia coli (Enumeration)

by MPN methodFMOE10-MRP2

equivalent to 10 g

19/04/2021 134

M263e19 Beef Enterococci (Enumeration) FMOE19-MRP2equivalent to

10 g19/04/2021 134

M264e10 Beef Escherichia coli (Enumeration) FMOE10-MRP2equivalent to

10 g24/05/2021 134

Foods which exceed specifications for total bacterial and fungal load, or which arecontaminated with a pathogen, pose a risk to both public health and brandreputation. Modern food processing often involves complicated global supplychains and ample opportunity for foods to be contaminated in their journey to ourtables. Even in a carefully controlled environment contamination can occur, andlaboratory analysis is a key safety measure to ensure the process and controls areworking as they should.

Our Food and Beverage Microbiology tests provide a flexible programme of 11 distributions a year, with varying levels of target organisms and background flora, giving a more realistic challenge than some proficiency programmes.


39


M264e15 BeefYeasts and Moulds (sum of) (Enumeration)


10 g24/05/2021 134

M264e18 Beef Coliforms (Enumeration) FMOE18-MRP2equivalent to

10 g24/05/2021 134



10 g28/06/2021 134

M267e01 BeefLactic acid bacteria (Enumeration)


10 g23/08/2021 134

M267e06 Beef



(Enumeration)


10 g23/08/2021 134

M270e04 BeefEnterobacteriaceae, Coliforms and Escherichia coli

(Enumeration)


10 g29/11/2021 134

M271e10 Beef Escherichia coli (Enumeration) FMOE10-MRP2equivalent to

10 g07/02/2022 134



10 g07/02/2022 134

M272e13 BeefBacillus cereus and



10 g28/02/2022 134

M273e05 BeefEnterobacteriaceae and Aerobic Plate Count (Enumeration)


10 g28/03/2022 134

M273e06 Beef



(Enumeration)


10 g28/03/2022 134

Chicken


M270e09 ChickenAerobic Plate Count (Enumeration)


10 g29/11/2021 134

Cooked Rice


M260e12 Cooked Rice Bacillus cereus (Enumeration) FMOE12-CCP22equivalent to

10 g25/01/2021 130


10 g23/08/2021 134


10 g07/02/2022 134

Fish


M268e24 Fish

Aerobic Plate Count, Enterobacteriaceae, Coliforms and Escherichia coli

(Enumeration)

FMOE24-SEA11equivalent to

10 g20/09/2021 134

40

Flour


M261e15 FlourYeasts and Moulds (sum of) (Enumeration)

FMOE15-CCP28equivalent to

10 g22/02/2021 130



10 g29/11/2021 134



10 g28/02/2022 134

Fruit Juice


M261e22 Fruit Juice

Thermophilic acidophilic bacteria (TAB) (Enumeration) and Guaiacol Producing TAB (Detection)

FMOE20-DRN17equivalent to

10 ml22/02/2021 130

M262e15 Fruit Juice Moulds (Enumeration) FM0E25-DRN17equivalent to

10 ml29/03/2021 130

M267e23 Fruit JuiceAerobic Plate Count and Lactic acid bacteria (Enumeration)


10 ml23/08/2021 134

M268e15 Fruit Juice Yeasts (Enumeration) FMOE16-DRN17equivalent to

10 ml20/09/2021 134

M272e22 Fruit Juice

Thermophilic acidophilic bacteria (TAB) (Enumeration) and Guaiacol Producing TAB (Detection)


10 ml28/02/2022 134

M273e15 Fruit Juice Moulds (Enumeration) FMOE25-DRN17equivalent to

10 ml28/03/2022 134

Infant Formula


M268e06 Infant Formula



(Enumeration)

FMOE6-INF10equivalent to

10 g20/09/2021 134

Milk Powder


M260e06 Milk Powder



(Enumeration)

FMOE06-DRY14equivalent to

10 g25/01/2021 130

M261e18 Milk Powder Coliforms (Enumeration) FMOE18-DRY14equivalent to

10 g22/02/2021 130

M262e09 Milk PowderAerobic Plate Count (Enumeration)


10 g29/03/2021 130

M263e03 Milk PowderEnterobacteriaceae (Enumeration)


10 g19/04/2021 134

M263e13 Milk PowderBacillus cereus and



10 g19/04/2021 134

41


M263e14 Milk PowderCoagulase Positive Staphylococci (Enumeration)


10 g19/04/2021 134

M264e06 Milk Powder



(Enumeration)


10 g24/05/2021 134

M268e10 Milk Powder Escherichia coli (Enumeration) FMOE10-DRY14equivalent to

10 g20/09/2021 134

M269e14 Milk PowderCoagulase Positive Staphylococci (Enumeration)


10 g25/10/2021 134

M269e24 Milk Powder


(Enumeration)


10 g25/10/2021 134

M271e06 Milk Powder



(Enumeration)


10 g07/02/2022 134



10 g07/02/2022 134

M272e18 Milk Powder Coliforms (Enumeration) FMOE18-DRY14equivalent to

10 g28/02/2022 134



10 g28/03/2022 134

Ready To Eat (RTE) Meal


M265e24Ready To Eat (RTE) Meal


(Enumeration)

FMOE24-PRO40equivalent to

10 g28/06/2021 134

Salad


M271e03 SaladEnterobacteriaceae (Enumeration)

FMOE3-VEG61equivalent to

10 g07/02/2022 134

Spice


M269e27 SpiceBacillus spp. and Moulds

(Enumeration)FMOE27-SPI17

equivalent to 10 g

25/10/2021 134

Swab (cotton / sponge)


M261e09 Swab (Cotton)Aerobic Plate Count (Enumeration)

FMOE9-UNF12 1 swab 22/02/2021 130

M266e26Swab (Sponge)

Aerobic Plate Count, Enterobacteriaceae, Coagulase Positive Staphylococci and Escherichia coli

(Enumeration)

FMOE26-UNF12 1 swab 26/07/2021 134

42


M272e09 Swab (Cotton)Aerobic Plate Count (Enumeration)

FMOE9-UNF12 1 swab 28/02/2022 134

PATHOGENS

Animal Feed


M264d072 Animal Feed Salmonella spp. (Detection) FMOD7-AFE1equivalent to

2 x 25 g24/05/2021 134

Beef


M260d02 BeefListeria monocytogenes /

Listeria spp. (Detection)FMOD2-MRP2

equivalent to 2 x 25 g

25/01/2021 130

M264d11 BeefEscherichia coli O157:H7

(Detection)FMOD11-MRP2


24/05/2021 134

M269d071 Beef Salmonella spp. (Detection) FMOD7-MRP2equivalent to

2 x 25 g25/10/2021 134

M269d11 BeefEscherichia coli O157:H7



25/10/2021 134

M271d02 BeefListeria monocytogenes /



07/02/2022 134

Cheese


M267d11 CheeseEscherichia coli O157:H7

(Detection)FMOD11-DRY7


23/08/2021 134

Chicken


M260d071 Chicken Salmonella spp. (Detection) FMOD7-MRP14equivalent to

2 x 25 g25/01/2021 130

M262e02 ChickenListeria monocytogenes

(Enumeration)FMOE2-MRP14

equivalent to 10 g

29/03/2021 130

M263d17 ChickenCampylobacter spp.



19/04/2021 134

M264d02 ChickenListeria monocytogenes /

Listeria spp . (Detection)FMOD2-MRP14


24/05/2021 134


2 x 25 g23/08/2021 134



equivalent to 10 g

20/09/2021 134

M269d17 ChickenCampylobacter spp.



25/10/2021 134

M270d02 ChickenListeria monocytogenes /

Listeria spp . (Detection)FMOD2-MRP14


29/11/2021 134

M270e17 ChickenCampylobacter spp.


equivalent to 10 g

29/11/2021 134


2 x 25 g07/02/2022 134



equivalent to 10 g

28/03/2022 134

43

Chocolate


M260d072 Chocolate Salmonella spp. (Detection) FMOD7-CON2equivalent to

2 x 25 g25/01/2021 130

M271d072 Chocolate Salmonella spp. (Detection) FMOD7-CON2equivalent to

2 x 25 g07/02/2022 134

Chocolate powder


M268d07Chocolate Powder

Salmonella spp. (Detection) FMOD7-CON3equivalent to

2 x 25 g20/09/2021 134

Dried Egg


M262d071 Dried Egg Salmonella spp. (Detection) FMOD7-EGG3equivalent to

2 x 25 g29/03/2021 130

M273d071 Dried Egg Salmonella spp. (Detection) FMOD7-EGG3equivalent to

2 x 25 g28/03/2022 134

Dry Cured Meat


M265d02Dry Cured Meat

Listeria monocytogenes /



28/06/2021 134

Fish


M261d21 FishVibrio parahaemolyticus

(Detection)FMOD21-SEA11


22/02/2021 130




20/09/2021 134




28/02/2022 134

Flour


M268d11 FlourEscherichia coli O157:H7

(Detection)FMOD11-CCP28


20/09/2021 134

Ground Pepper


M270d071 Ground Pepper Salmonella spp. (Detection) FMOD7-SPI11equivalent to

2 x 25 g29/11/2021 134

Herbs


M265d072 Herbs Salmonella spp. (Detection) FMOD7-VEG47equivalent to

2 x 25 g28/06/2021 134

44

Infant Formula


M261d20 Infant FormulaCronobacter (Enterobacter )

sakazakii (Detection)FMOD20-INF10


22/02/2021 130

M269d072 Infant Formula Salmonella spp. (Detection) FMOD7-INF10equivalent to

2 x 25 g25/10/2021 134

M272d20 Infant FormulaCronobacter (Enterobacter )

sakazakii (Detection)FMOD20-INF10


28/02/2022 134

Milk Powder


M262d02 Milk PowderListeria monocytogenes /

Listeria spp. (Detection)FMOD2-DRY14


29/03/2021 130

M262d072 Milk Powder Salmonella spp. (Detection) FMOD7-DRY14equivalent to

2 x 25 g29/03/2021 130

M265d17 Milk PowderCampylobacter spp.



28/06/2021 134


2 x 25 g23/08/2021 134

M273d02 Milk PowderListeria monocytogenes /

Listeria spp. (Detection)FMOD2-DRY14


28/03/2022 134


2 x 25 g28/03/2022 134

Mixed Vegetables


M267d02Mixed Vegetables


Listeria spp. (Detection)FMOD2-VEG88


23/08/2021 134

Peanut (Ground)


M270d072Peanut (Ground)

Salmonella spp. (Detection) FMOD7-NUT12equivalent to

2 x 25 g29/11/2021 134

Pork


M265d071 Pork Salmonella spp. (Detection) FMOD7-MRP35equivalent to

2 x 25 g28/06/2021 134

Ready to Eat (RTE) Meal


M269d02Ready To Eat (RTE) Meal


Listeria spp. (Detection)FMOD2-PRO40


25/10/2021 134

Salad


M262d11 SaladEscherichia coli O157:H7

(Detection)FMOD11-VEG61


29/03/2021 130

M264d071 Salad Salmonella spp. (Detection) FMOD7-VEG61equivalent to

2 x 25 g24/05/2021 134

45


M273d11 SaladEscherichia coli O157:H7



28/03/2022 134

Smoked Fish


M267e02 Smoked FishListeria monocytogenes

(Enumeration)FMOE2-SEA28

equivalent to 10 g

23/08/2021 134

M268d02 Smoked FishListeria monocytogenes /

Listeria spp. (Detection)FMOD2-SEA28


20/09/2021 134

Soft Cheese


M263d02 Soft CheeseListeria monocytogenes



19/04/2021 134

Sprouting Seeds and Lettuce


M263d07Sprouting Seeds and Lettuce

Salmonella spp. (Detection) FMOD7-VEG71equivalent to

2 x 25 g19/04/2021 134

M270d11Sprouting Seeds and Lettuce

Escherichia coli O157:H7



29/11/2021 134

Swab (Sponge)


M261d02Swab (Sponge)


Listeria spp. (Detection)FMOD2-UNF11

2 x sponge swab

22/02/2021 130


Salmonella spp. (Detection) FMOD7-UNF112 x sponge

swab22/02/2021 130




2 x sponge swab

26/07/2021 134



swab26/07/2021 134



(Detection)FMOD11-UNF11

2 x sponge swab

26/07/2021 134




2 x sponge swab

28/02/2022 134



swab28/02/2022 134

46


47

EUR

GM FOODProficiency Test List - GBP

Jan 2021 - Mar 2022

48

GENETICALLY MODIFIED FOOD PROFICIENCY TESTS

ANIMAL FEED


GeMMP38Animal Feed (Cereal Based)

Maize & Soya FGM3-AFE1 5 g 19/03/2021 320

GeMMP40Animal Feed (Cereal Based)

Maize & Soya FGM3-AFE1 5 g 18/03/2022 330

BAKED PRODUCT

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)GeMMP39 Baked Product Maize & Soya FGM3-PRO1 5 g 10/06/2021 330

MAIZE FLOUR


GeMMU91100% Maize Flour

Maize FGM2-CCP2 5 g 08/04/2021 330


Maize FGM2-CCP2 5 g 13/08/2021 330


Maize FGM2-CCP2 5 g 10/12/2021 330

MIXED FLOURS

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)GeMMU90 Mixed Flours Maize & Soya FGM3-CCP35 5 g 12/02/2021 320GeMMU93 Mixed Flours Maize & Soya FGM3-CCP35 5 g 02/07/2021 330GeMMU98 Mixed Flours Maize & Soya FGM3-CCP35 5 g 11/02/2022 330

Nearly 35 years after the first product trials, GM foods and crops remain a topic of much discussion. Some territories embrace the technology widely, some restrict the use and cultivation of GM crops and others continue to ban their use in agriculture.

Currently there are over 30 approved GM crop plants, from apples to wheat, being used in the agriculture of 24 countries in 2017. This represents nearly 190 million hectares planted by 17 million farmers. It is estimated that the cultivation of GM crops has prevented 671 million kg of pesticide active ingredients being used in the environment in the period 1996-2016. (ISAA Report 2017).


49

MIXED FLOURS & PROCESSED MATRIX


GeMMC06

Mixed Flours & Processed Matrix (Baked Product)

Maize & Soya FGM3-CCP53 2 x 5 g 08/01/2021 445

GeMMC07Mixed Flours & Processed Matrix

Soya FGM5-CCP53 2 x 5 g 08/10/2021 458

GeMMC08

Mixed Flours & Processed Matrix (Baked Product)

Maize & Soya FGM3-CCP53 2 x 5 g 07/01/2022 458

SOYA FLOUR


GeMMU89100% Soya Flour

Soya FGM5-CCP3 5 g 15/01/2021 320


Soya FGM5-CCP3 5 g 14/05/2021 330


Soya FGM5-CCP3 5 g 14/01/2022 330

TOBACCO

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)GeMST08 Tobacco p35S & tNOS FGM4-TOB3 3 x 5 g 18/06/2021 330

WHEAT FLOUR


GeMMU95 Wheat FlourContamination test (maize, soya & rice)

FGM1-CCP49 3 x 5 g 05/11/2021 330

50


51

WATER AND ENVIRONMENTALCHEMISTRYProficiency Test List - GBP

Jan 2021 - Mar 2022

52

WATER & ENVIRONMENTAL CHEMISTRY PROFICIENCY TESTS


Quantity Purchased Discount AppliedFor product codes starting DWC11 - 25 tests 10%26 or more 25%

For product codes starting WW21 - 34 tests 10%35 - 44 tests 15%45 or more tests 25%

DRINKING WATER

Acid Herbicides


DWC0911 Drinking Water Acid Herbicides FWAH1-DRW11 litre +

spiking conc.27/04/2021 221

DWC0912 Drinking Water Acid Herbicides FWAH1-DRW11 litre +


BTEX


DWC1120 Drinking Water BTEX FWBT1-DRW11 litre +






For typical analyte ranges, please see pages 17 - 29

Modern analytical techniques are allowing us to detect chemicals in water at everdecreasing concentrations, and this is changing our understanding of the pollutantsthat may be present in the environment, which can consequently be an issue for our drinking water. Regular monitoring of these diverse water types is required bygovernmental regulation to ensure the safety of the water we drink and theenvironment we live in.

Our extensive programme covers a wide range of water types including, drinking, waste, high salinity,and surface waters, and is complemented by schemes for emergency chemical contamination, tasteand odour chemical identification, and soil chemistry.


53






Chlorine


DWC1219Drinking Water (Standard Concentrate)

Chlorine FWCH1-DRW1 3 ml 16/03/2021 84


Chlorine FWCH1-DRW1

3 ml

18/05/2021 87




Chlorine FWCH1-DRW1

3 ml

16/11/2021 87



Contamination Incident (Emergency Scheme)


EMY42 Drinking Water Contamination incident FWEM1-DRW13 x 1 litre + 250 ml + blanks

06/05/2021 695

EMY43 Drinking Water Contamination incident FWEM1-DRW1

3 x 1 litre + 250 ml + blanks

30/09/2021 695

Fluorosurfactants (PFOS & PFOA)




FWFL1-DRW1 spiking conc. 16/02/2021 126







Haloacetic Acids


DWC1709Drinking Water (Ultra Pure Water)

Haloacetic Acids FWHA1-DRW11 litre +



Haloacetic Acids FWHA1-DRW1 1 litre + spiking conc.

09/11/2021 221

54

Hexavalent Chromium



Hexavalent Chromium FWHC1-DRW1 20 ml 16/03/2021 95


Hexavalent Chromium FWHC1-DRW1

20 ml

18/05/2021 98




Hexavalent Chromium FWHC1-DRW1

20 ml

16/11/2021 98



Inorganic Disinfection By-products


DWC0519Drinking Water (Standard Solution)


FWID1-DRW1 125 ml 16/03/2021 143



FWID1-DRW1

125 ml

18/05/2021 147



FWID1-DRW1 125 ml 27/07/2021 147



FWID1-DRW1 125 ml 16/11/2021 147



FWID1-DRW1 125 ml 15/03/2022 147

Major Inorganic Components


DWC0129 Drinking Water Major Inorganic Components FWIC1-DRW11 litre +










Note: If you purchase the major inorganic components sample and the corresponding routine component sample in the same round,(such as DWC0129 and DWC0229) you will receive only ONE litre of water and ONE spiking concentrate.

55








Non-Routine Metals



Non-Routine Metals FWNM1-DRW11 x 60 ml,

1 x 500 ml + spiking conc.

16/03/2021 209




18/05/2021 215




27/07/2021 215




16/11/2021 215




15/03/2022 215

OC Pesticides


DWC1020 Drinking Water OC Pesticides FWOC1-DRW11 litre +










OP Pesticides


DWC0820 Drinking Water OP Pesticides FWOP1-DRW11 litre +






Note: If you purchase the major inorganic components sample and the corresponding routine component sample in the same round,(such as DWC0129 and DWC0229) you will receive only ONE litre of water and ONE spiking concentrate.

56






Perchlorate



Perchlorate FWPE1-DRW1 2 ml 16/03/2021 89





Polycyclic Aromatic Hydrocarbons (PAHs)


DWC0720 Drinking WaterPolycyclic Aromatic Hydrocarbons

FWPC1-DRW11 litre +



FWPC1-DRW11 litre +



FWPC1-DRW11 litre +



FWPC1-DRW11 litre +



FWPC1-DRW11 litre +


Routine Components


DWC0229 Drinking Water Routine Components FWRC1-DRW11 litre +
















See note on page 54 for purchases of routine components and major inorganic components in the same round.

57

Routine Metals

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)DWC0329 Drinking Water Routine Metals FWRM1-DRW1 500 ml 26/01/2021 143DWC0330 Drinking Water Routine Metals FWRM1-DRW1 500 ml 16/03/2021 143DWC0331 Drinking Water Routine Metals FWRM1-DRW1 500 ml 18/05/2021 147DWC0332 Drinking Water Routine Metals FWRM1-DRW1 500 ml 27/07/2021 147DWC0333 Drinking Water Routine Metals FWRM1-DRW1 500 ml 28/09/2021 147DWC0334 Drinking Water Routine Metals FWRM1-DRW1 500 ml 16/11/2021 147DWC0335 Drinking Water Routine Metals FWRM1-DRW1 500 ml 25/01/2022 147DWC0336 Drinking Water Routine Metals FWRM1-DRW1 500 ml 15/03/2022 147

Taste & Odour Chemical Identification (NOT for organoleptic testing)


TOCHEM10 Drinking WaterTaste & Odour Chemical Identification

FWTO1-DRW12 x 1 litre +

blank15/07/2021 530

Total Cyanide



Total Cyanide FWTC1-DRW1 3 ml 16/03/2021 84









Triazines and Urea Herbicides


DWC1510 Drinking Water Triazines and Urea Herbicides FWTU1-DRW11 litre +






58

Trihalomethanes / Chlorinated Solvents




FWTR1-DRW11 litre +




FWTR1-DRW11 litre +




FWTR1-DRW11 litre +




FWTR1-DRW11 litre +




FWTR1-DRW11 litre +


Uranium



Uranium FWUR1-DRW1 60 ml 27/07/2021 87


Uranium FWUR1-DRW1 60 ml 16/11/2021 87

HIGH SALINITY WATER

Complex Nutrients


HS0112High Salinity Water

Complex Nutrients FWCN1-HSW1 500 ml 08/06/2021 173


Complex Nutrients FWCN1-HSW1 500 ml 30/11/2021 173

Minerals



Minerals FWMI1-HSW1 500 ml 08/06/2021 205


Minerals FWMI1-HSW1 500 ml 30/11/2021 205

Simple Nutrients



Simple Nutrients FWSN1-HSW1 500 ml 08/06/2021 173


Simple Nutrients FWSN1-HSW1 500 ml 30/11/2021 173

59

Trace Metals 3



Trace Metals 3 FWTM3-HSW1 500 ml 08/06/2021 173



Trace Metals 4






SOIL

Trace Metals 5

Item Code Matrix Analytes Product Code Approx. Size Start Date Fee (GBP)SL0108 Soil Trace Metals 5 FWTM5-SOI1 6 g 07/10/2021 174

SURFACE WATER

Major Inorganic Compounds


SW0111 Surface Water Major Inorganic Components FWIC1-SUW11 litre +






Metals


SW0311 Surface Water Metals FWME1-SUW1500 ml +

Standard Sol02/02/2021 178





Routine Components


SW0211 Surface Water Routine Components FWRC1-SUW11 litre +






See note above for purchases of routine components and major inorganic components in the same round.

Note: If you purchase the major inorganic components sample and the corresponding routine component sample in the same round,(such as SW0111 and SW0211) you will receive only ONE litre of water and ONE spiking concentrate.

60

Toxic Metals


SW0411 Surface Water Toxic Metals FWTX1-SUW1500 ml +






WASTE WATER

Anions


WW0928Waste Water (Standard Concentrate)

Anions FWAN1-EWW1 20 ml 09/02/2021 69













Dissolved Oxygen



Dissolved Oxygen FWDO1-EWW1 2 ml 09/02/2021 87









61






Hexavalent Chromium



Hexavalent Chromium FWHC1-EWW1 20 ml 09/02/2021 72













Minerals



Minerals FWMI1-EWW1 2 x 20 ml 09/02/2021 66













62

Nutrients



Nutrients FWNU1-EWW1 4 x 60 ml 09/02/2021 94













Oil & Grease



Oil & Grease FWOG1-EWW1 2 ml 09/02/2021 60













63

Oxygen Demand



Oxygen Demand FWDE1-EWW1 20 ml 09/02/2021 77













pH & Electrical Conductivity


WW0428Waste Water (Standard Solution)

pH & Electrical Conductivity FWPH1-EWW1 2 x 125 ml 09/02/2021 81













64

Phthalates



Phthalates (Environmental) FWPT1-EWW1 2 ml 15/06/2021 99


Phthalates (Environmental) FWPT1-EWW1 2 ml 07/12/2021 99

Residues



Residues FWRE1-EWW1 500 ml 09/02/2021 87













Settleable Solids


WW1328Waste Water (requires dilution)

Settleable Solids FWSS1-EWW1 25 g 09/02/2021 94









65






Total Cyanide



Total Cyanide FWTC1-EWW1 2 ml 09/02/2021 77













Total Sulphide



Total Sulphide FWTS1-EWW1 20 ml 09/02/2021 94













66

Trace Metals 1



Trace Metals 1 FWTM1-EWW1 20 ml 09/02/2021 108













Trace Metals 2
















67

VOCs



VOC FWVO1-EWW1 2 ml 09/02/2021 96


VOC FWVO1-EWW1 2 ml 21/04/2021 99


VOC FWVO1-EWW1 2 ml 15/06/2021 99


VOC FWVO1-EWW1 2 ml 10/08/2021 99


VOC FWVO1-EWW1 2 ml 12/10/2021 99


VOC FWVO1-EWW1 2 ml 07/12/2021 99


VOC FWVO1-EWW1 2 ml 09/02/2022 99

WATER & ENVIRONMENTAL CHEMISTRY PROFICIENCY TESTS - APPROXIMATE CONCENTRATION RANGES

DRINKING WATER

Acid Herbicides (group 9)

MatrixApprox.

RangeUnits

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l

Product Code Analytes

FWAH1-DRW1 Drinking Water

MCPA

MCPB2,4-Ddichlorpropdicamba,2,4-DBbentazonemecoproppropyzamideioxynilbromoxyniltriclopyrclopyralidfluroxypyr2,3,6-TBA2,4,5-Tdichlobenilbromacilmetazachlorpropachlorbenazolinmetaldehyde

68

BTEX (group 11)

MatrixApprox.

RangeUnits

0.1 - 1.5 mg/l

0.2 - 4.0 mg/l

0.2 - 4.0 mg/l

0.2 - 4.0 mg/l

0.2 - 4.0 mg/l

0.2 - 4.0 mg/l

0.2 - 4.0 mg/l

0.2 - 8.0 mg/l0.5 - 12.0 mg/l

Chlorine (group 12)

MatrixApprox.

RangeUnits

0.5 - 3.0 mg/l

0.5 - 3.0 mg/l

Emergency contamination incident (no group)

MatrixApprox.

RangeUnits

Drinking Water not set not set

Fluorosurfactants (PFOS & PFOA, group 19)

MatrixApprox.

RangeUnits

0.2 - 5.0 mg/l

0.2 - 10.0 mg/l

Haloacetic Acids (group 17)

MatrixApprox.

RangeUnits

5.0 - 50.0 mg/l5.0 - 50.0 mg/l5.0 - 50.0 mg/l5.0 - 50.0 mg/l5.0 - 50.0 mg/l

Hexavalent Chromium (group 18)

MatrixApprox.

RangeUnits

Standard concentrate 5.0 - 50.0 mg/l


toluene

ethylbenzene

styrene

o-xylene

m-xylene

p-xylene

total xylene


FWBT1-DRW1 Drinking Water

benzene

m+p xylene

FWHA1-DRW1 Drinking Water

monochloroacetic acid (MCA)dichloroacetic acid (DCA)trichloroacetic acid (TCA)monobromoacetic acid (MBA)dibromoacetic acid (DBA)

FWFL1-DRW1 Standard concentrate

FWCH1-DRW1 Standard concentratechlorine (total)

chlorine (free)


FWEM1-DRW1 not set - blind sample



FWHC1-DRW1 hexavalent chromium

perfluorooctane sulfonic acid

perfluorooctanoic acid PFOA


69

Inorganic Disinfection By-products (group 5)

MatrixApprox.

RangeUnits

5.0 - 200 mg/l

1.0 - 20.0 mg/l

1.0 - 100 mg/l

1.0 - 1000 mg/l

Major Inorganic Components (group 1)

MatrixApprox.

RangeUnits

5.0 - 50.0 mg/l0.3 - 3.0 mg/l6.0 - 50.0 mg/l10.0 - 150 mg/l1.0 - 15.0 mg/l

30.0 - 300 mg/l

30.0 - 130 mg/l100 - 3000 mg/l150 - 1800 mg/l8.0 - 100 mg/l

Non-Routine Metals (group 4)

MatrixApprox.

RangeUnits

0.1 - 2.0 mg/l

100 - 1000 mg/l

200 - 1500 mg/l

1.0 - 15.0 mg/l

1.0 - 15.0 mg/l

0.5 - 7.5 mg/l

1.0 - 20.0 mg/l

50.0 - 500 mg/l

10.0 - 100 mg/l

3.0 - 30.0 mg/l

3.0 - 30.0 mg/l

3.0 - 30.0 mg/l

3.0 - 100 mg/l

3.0 - 10.0 mg/l



FWID1-DRW1Standard Solution in ultra pure

water

bromide

bromate

chlorite

chlorate


FWIC1-DRW1 Drinking Water

sodiumpotassiumchloridecalciummagnesium

alkalinity HCO3

total hardness Catotal phosphorus Pfluoridesulphate

FWNM1-DRW1 Drinking Water

mercury

barium

boron

arsenic

selenium

antimony

silver

strontium

lithium

cobalt

vanadium

molybdenum

tin

beryllium

70

OC Pesticides (group 10)

MatrixApprox.

RangeUnits

0.01 - 0.15 mg/l0.006 – 0.05 mg/l0.006 – 0.05 mg/l0.01 - 0.15 mg/l0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.006 - 0.04 mg/l

0.006 - 0.04 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

OP Pesticides (group 8)

MatrixApprox.

RangeUnits

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

Perchlorates (group 20)

MatrixApprox.

RangeUnits

Standard concentrate 4.0 - 20.0 mg/l


FWOC1-DRW1 Drinking Water

endrindieldrinaldrinp,p’ DDTo,p’-DDT

p,p’-DDE

o,p’-DDE

p,p’-DDD

o,p-DDD (TDE)

hexachlorocyclohexane (alpha)

hexachlorocyclohexane (beta)

hexachlorocyclohexane (delta)

mevinphos

chlorofenvinphos

chlorpyrifos

heptachlor epoxide (total)

pentachlorobenzene

pendimethalin

lindane (gamma HCH)

trifluralin

alpha endosulphan

beta endosulphan

hexachlorobenzene

heptachlor


FWOP1-DRW1 Drinking Water

alachlor

azinphos-ethyl

azinphos-methyl

dichlorvos

fenitrothion

malathion

diazinon

fenthion

parathion-ethyl

parathion-methyl

cypermethrin

propetamphos


FWPE1-DRW1 perchlorate

71

Polycyclic Aromatic Hydrocarbons (PAHs group 7)

MatrixApprox.

RangeUnits

0.005 – 0.05 mg/l

0.01 – 0.10 mg/l

0.003 – 0.05 mg/l

0.003 – 0.05 mg/l

0.005 – 0.05 mg/l

0.002 – 0.02 mg/l

0.01 – 0.07 mg/l

0.01 – 0.07 mg/l

Routine Components (group 2)

MatrixApprox.

RangeUnits

0.02 - 0.60 mg/l

2.0 - 60.0 mg/l

0.1 - 0.60 mg/l

0.2 - 5.0 mg/l

0.2 - 5.0 mg/l

0.2 - 20.0 HAZEN

10.0 - 1500 mg/l

6.0 - 10.0 pH units

0.05 - 4.0 NTU

100 - 600 mS/cm

Routine Metals (group 3)

Matrix Approx. Units0.5 - 7.0 mg/l0.5 - 20.0 mg/l20.0 - 400 mg/l10.0 - 75.0 mg/l20.0 - 300 mg/l50.0 - 2000 mg/l50.0 - 500 mg/l5.0 - 30.0 mg/l5.0 - 50.0 mg/l

Taste & Odour Chemical Identification (no group)

Matrix Approx. UnitsDrinking Water not set not set

Total Cyanide (group 16)

MatrixApprox.

RangeUnits

Standard Concentrate 0.01 - 0.10 mg/l



FWPC1-DRW1 Drinking Water

anthracene

fluoranthene

benzo (b) fluoranthene

benzo (k) fluoranthene

naphthalene

benzo (a) pyrene

benzo (ghi) perylene

indeno (1,2,3-cd) pyrene


FWRC1-DRW1 Drinking Water

nitrite NO2

nitrate NO3

ammonium NH4

TOC

PI

colour (filtered)

SR phosphate

pH

turbidity

conductivity @ 20°C

leadironmanganesealuminiumcopperzinc

chromium


FWRM1-DRW1 Drinking Water

cadmium

nickel

FWTC1-DRW1 total cyanide

FWTO1-DRW1 not set - blind sample


72

Triazines and Urea Herbicides (group 15)

MatrixApprox.

RangeUnits

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

0.01 - 0.15 mg/l

Trihalomethanes / Chlorinated Solvents (group 6)

MatrixApprox.

RangeUnits

2.0 - 100 mg/l

2.0 - 40.0 mg/l

2.0 - 50.0 mg/l

2.0 - 50.0 mg/l

2.0 - 50.0 mg/l

0.5 - 10.0 mg/l

0.5 - 10.0 mg/l

0.5 - 4.0 mg/l

0.5 - 4.0 mg/l

0.1 - 2.0 mg/l

0.1 - 2.0 mg/l

0.1 - 2.0 mg/l

0.01 - 0.15 mg/l

0.1 - 2.0 mg/l

Uranium (group 21)

Matrix Approx. UnitsStandard solution 10.0 - 100 mg/l


isoproturon

diuron

linuron

ametryn

monuron

methabenzthiazuron

diflufenican

metamitron

simazine

atrazine

chlortoluron

propazine

cyanazine

trietazine

prometryn

terbutryn

1,1,1-trichloroethane


carbetamide

pirimicarb


FWTR1-DRW1 Drinking Water

chloroform

dichloromethane

bromodichloromethane

dibromochloromethane

bromoform

trichloroethene

tetrachloroethene

carbon tetrachloride

1,2-dichloroethane

1,2,3-trichlorobenzene



hexachlorobutadiene

FWTU1-DRW1 Drinking Water

FWUR1-DRW1 uranium

73

HIGH SALINITY WATER

Complex Nutrients (group 1)

MatrixApprox.

RangeUnits

1.5 - 35.0 mg/l

1.5 - 35.0 mg/l0.5 -10.0 mg/l

Minerals (group 3)

MatrixApprox.

RangeUnits

25.0 - 110 mg/l

2.0 - 40.0 mg/l

4.0 - 40.0 mg/l

10.0 - 100,000 mg/l

0.0 - 100 mS/cm

8.7 - 275 mg/l

5.0 - 10.0 pH units

Simple Nutrients (group 2)

MatrixApprox.

RangeUnits

0.65 - 19.0 mg/l

0.25 - 40.0 mg/l

0.25 - 40.0 mg/l

0.40 - 4.0 mg/l

0.50 -5.50 mg/l

Trace Metals 3 (group 4)

MatrixApprox.

RangeUnits

0.0 - 10,000 mg/l

0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l0.0 - 10,000 mg/l


FWCN1-HSW1 High Salinity WaterKjeldahl nitrogen (total) (TKN)nitrogen (total)

phosphorus (total)


FWMI1-HSW1 High Salinity Water

calcium

magnesium

potassium

alkalinity as CaCO3

conductivity (25ºC)

hardness (total) as CaCO3

pH


FWSN1-HSW1 High Salinity Water

ammonia as N

nitrate as N

nitrate+nitrite as N

nitrite as N

orthophosphate as P


FWTM3-HSW1 High Salinity Water

Aluminium

ArsenicBerylliumCadmiumChromiumCobaltCopperIronLeadManganeseMercuryNickelSelenium

74


MatrixApprox.

RangeUnits

95.0 - 900 mg/l

100 - 2500 mg/l800 - 2000 mg/l60.0 - 600 mg/l26.0 - 600 mg/l30.0 - 300 mg/l60.0 - 900 mg/l

1000 - 5000 mg/l80.0 - 300 mg/l

WASTE WATER

Anions (group 9)

MatrixApprox.

RangeUnits

1.0 - 10.0 mg/l

0.3 - 4.0 mg/l

VOC

MatrixApprox.

RangeUnits

8.0 - 120 mg/l8.0 - 100 mg/l9.0 - 125 mg/l8.0 - 115 mg/l9.0 - 100 mg/l15.0 - 100 mg/l8.0 - 190 mg/l7.0 - 100 mg/l8.0 - 100 mg/l8.0 - 100 mg/l8.0 - 300 mg/l8.0 - 300 mg/l20.0 - 300 mg/l

Dissolved Oxygen (group 14)

MatrixApprox.

RangeUnits

Standard Concentrate 1.0 - 100 mg/l

Hexavalent Chromium (group 7)

MatrixApprox.

RangeUnits



FWTM4-HSW1 High Salinity Water

Antimony

BariumBoronMolybdenumSilver

benzene

FWDO1-EWW1dissolved oxygen & dissolved oxygen (Winkler)


FWHC1-EWW1 hexavalent chromium [Cr(VI)]

StrontiumThalliumTinTitanium


FWAN1-EWW1 Standard Concentratebromide

fluoride


1,2-dichlorobenzene1,3-dichlorobenzene1,4-dichlorobenzeneethylbenzenemethyl tert-butyl ether (mtbe)naphthalene

1,2,4-trimethylbenzene1,3,5-trimethylbenzenem+p-xylene

toluene

o-xylenetotal xylene


FWVO1-EWW1 Standard Concentrate

75

Minerals (group 8)

MatrixApprox.

RangeUnits

10.0 - 120 mg/l

3.5 - 110 mg/l

17.0 - 675 mg/l

2.0 - 40.0 mg/l

4.0 - 40.0 mg/l

6.0 - 100 mg/l

Nutrients (routine components group 3)

MatrixApprox.

RangeUnits

0.5 - 50.0 mg/l0.2 - 10.0 mg/l0.2 - 20.0 mg/l10.0 - 500 mg/l1.0 - 100 mg/l10.0 - 500 mg/l0.2 - 5.0 mg/l2.0 - 50.0 mg/l2.0 - 50.0 mg/l

Oil & Grease (group 10)

MatrixApprox.

RangeUnits


Oxygen Demand (group 1)

MatrixApprox.

RangeUnits

6.0 - 250 mg/l

6.0 - 250 mg/l

6.0 - 250 mg/l

pH & Electrical Conductivity (group 4)

MatrixApprox.

RangeUnits

1.0 - 13.0 pH units

200 - 2000 mS/cm

sodium

total phosphorus (as P)kjeldahl nitrogen (as N)total nitrogen (as N)


orthophosphate (as P)sulphate (as SO4)


FWMI1-EWW1 Standard Concentrate

alkalinity (as CaCO3)

calcium

total hardness (as CaCO3)

magnesium

potassium

FWPH1-EWW1 Standard SolutionpH

electrical conductivity @25°C

FWOG1-EWW1

oil & grease suitable for EPA 1664, SM 5520B and other gravimetric methods (not suitable for IR methods)


FWNU1-EWW1 Standard Concentrate

nitrate (as N)nitrite (as N)ammonia (as N)chloride


FWDE1-EWW1 Standard Concentrate

BOD 5-day

COD

TOC


76

Phthalates (Environmental group 16)

MatrixApprox.

RangeUnits

8.0 - 50.0 mg/l

8.0 - 50.0 mg/l

8.0 - 50.0 mg/l

8.0 - 50.0 mg/l

8.0 - 50.0 mg/l

8.0 - 50.0 mg/l

Residues (group 2)

MatrixApprox.

RangeUnits

23.0 - 675 mg/l

23.0 - 675 mg/l

23.0 - 675 mg/l

Settleable Solids (group 13)

MatrixApprox.

RangeUnits

Standard Concentrate 5.0 - 100 ml/l

Total Cyanide (group 11)

MatrixApprox.

RangeUnits

Standard Concentrate 0.1 - 1.0 mg/l

Total Sulphide (group 12)

MatrixApprox.

RangeUnits

Standard Concentrate 1.0 - 10.0 mg/lFWTS1-EWW1 total sulphide


FWPT1-EWW1 Standard Concentrate

bis (2-ethylhexyl) phthalate

butyl benzyl phthalate

di-n-butyl phthalate

diethyl phthalate

dimethyl phthalate

di-n-octyl phthalate


FWRE1-EWW1 Standard Solution

dissolved solids @ 180°C

suspended solids

total solids


FWSS1-EWW1settleable solids (volumetric test using Imhoff Cone)


FWTC1-EWW1 total cyanide


77


MatrixApprox.

RangeUnits

200 - 4000 mg/l

70.0 - 900 mg/l

8.0 - 900 mg/l

8.0 - 750 mg/l

17.0 - 1000 mg/l

28.0 - 1000 mg/l

40.0 - 900 mg/l

200 - 4000 mg/l

70.0 - 3000 mg/l

70.0 - 4000 mg/l

2.0 - 30.0 mg/l

80.0 - 3000 mg/l

90.0 - 2000 mg/l

55.0 - 2000 mg/l

100 - 2000 mg/l


MatrixApprox.

RangeUnits

95.0 - 900 mg/l

100 - 2500 mg/l

800 - 2000 mg/l

60.0 - 600 mg/l

26.0 - 600 mg/l

30.0 - 300 mg/l

60.0 - 900 mg/l

SOIL

Trace Metals 5 (no group)

MatrixApprox.

RangeUnits

1.0 - 400 mg/kg10.0 - 2000 mg/kg10.0 - 500 mg/kg1.0 - 500 mg/kg

30.0 - 2500 mg/kg1.0 - 200 mg/kg2.0 - 200 mg/kg10.0 - 200 mg/kg0.1 - 200 mg/kg



FWTM1-EWW1 Standard Concentrate

aluminium

arsenic

beryllium

cadmium

chromium (total)

cobalt

copper

iron

lead

manganese

mercury

nickel

selenium

vanadium

zinc


FWTM2-EWW1 Standard Concentrate

antimony

barium

boron

molybdenum

silver

strontium

thallium

FWTM5-SOI1 Soil

cadmiumleadchromiumarsenicbariumnickelcopperzincmercury

78

SURFACE WATER

Major Inorganic Components (group 1)

MatrixApprox.

RangeUnits

5.0 - 50.0 mg/l0.3 - 3.0 mg/l6.0 - 50.0 mg/l10.0 - 150 mg/l1.0 - 15.0 mg/l30.0 - 300 mg/l30.0 - 130 mg/l100 - 3000 mg/l150 - 1800 mg/l5.0 - 100 mg/l

Routine Components (group 2)

MatrixApprox.

RangeUnits

0.02 - 0.60 mg/l2.0 - 60.0 mg/l0.1 - 0.6 mg/l0.2 - 5.0 mg/l0.2 - 5.0 mg/l0.2 - 30.0 HAZEN1.0 - 1500 mg/l6.0 - 10.0 pH units

0.05 - 10.0 NTU100 - 600 mS/cm

Metals (group 3)

MatrixApprox.

RangeUnits

15.0 - 400 mg/l10.0 - 70.0 mg/l20.0 - 700 mg/l10.0 - 500 mg/l20.0 - 700 mg/l2.0 - 15.0 mg/l10.0 - 700 mg/l25.0 - 1500 mg/l10.0 - 1000 mg/l10.0 - 100 mg/l


FWIC1-SUW1 Surface Water

sodiumpotassiumchloridecalciummagnesium

conductivity @ 20°C

alkalinity as HCO3

total hardness as Catotal phosphorus Pfluoridesulphate

nitrite NO2

nitrate NO3

ammonium NH4

strontiumlithium


FWME1-SUW1 Surface Water

ironmanganese


zincsilverbariumboron

copperaluminium

FWRC1-SUW1 Surface Water

SR phosphatepH

TOCPIcolour (filtered)

turbidity

79

Toxic Metals (group 4)

MatrixApprox.

RangeUnits

0.2 - 7.0 mg/l1.0 -25.0 mg/l3.0 - 30.0 mg/l1.0 - 15.0 mg/l1.0 - 15.0 mg/l0.5 - 7.0 mg/l0.1 - 2.0 mg/l2.0 - 30.0 mg/l2.0 - 30.0 mg/l3.0 - 60.0 mg/l2.0 - 30.0 mg/l1.0 - 100 mg/l1.0 - 10.0 mg/l


FWTX1-SUW1 Surface Water

cadmiumleadnickelseleniumarsenicantimony

beryllium

mercurycobaltvanadiumchromiummolybdenumtin

80


81

EUR

WATER AND ENVIRONMENTALMICROBIOLOGYProficiency Test List - GBP

Jan 2021 - Mar 2022

82

WATER AND ENVIRONMENTAL MICROBIOLOGY PROFICIENCY TESTS


Quantity Purchased Distribution PriceAll PTs in the same distribution 235 GBP

242 (from April 2021)

Quantity Purchased Discount AppliedParasitology - 6 or more 10%

INDICATOR ORGANISMS

Bathing Water


BWM0108 Bathing WaterEscherichia coli and

EnterococciFWM10-RWB1

lyophilised sample

19/05/2021 92

BWM0109 Bathing WaterEscherichia coli and

EnterococciFWM10-RWB1

lyophilised sample

22/09/2021 92

Drinking Water


DWM0150 Drinking WaterTotal coliforms and Escherichia coli

FWM01-DRW1lyophilised

sample20/01/2021 89



sample03/03/2021 89



sample07/04/2021 92



sample05/05/2021 92



sample16/06/2021 92



sample14/07/2021 92



sample08/09/2021 92

Modern water distribution systems in developed countries provide clean water tovast populations, so regular monitoring of water for microbiological safety is highlyregulated. A failure in the system could lead to a significant public health risk, ifsuch a widespread and essential commodity were to become contaminated with apathogenic organism.

The Fapas® programme covers all the common indicator organisms for drinking water, as well asLegionella spp. in environmental (cooling) waters and common water parasites (Cryptosporidium andGiardia). The programme also covers tests for swimming pool and spa waters and tests for outdoorbathing waters, whether they are swimming lakes or beach bathing.


83




sample13/10/2021 92



sample17/11/2021 92



sample08/12/2021 92



sample19/01/2022 92



sample16/03/2022 92

DWM0250 Drinking WaterColony Counts (22ºC/72h) and Colony Counts (37ºC/48h)


sample20/01/2021 89



sample03/03/2021 89



sample07/04/2021 92



sample05/05/2021 92



sample16/06/2021 92



sample14/07/2021 92



sample08/09/2021 92



sample13/10/2021 92



sample17/11/2021 92



sample08/12/2021 92



sample19/01/2022 92



sample16/03/2022 92

DWM0350 Drinking Water

Enterococci, Pseudomonas aeruginosa ,

Clostridium perfringens ,

Clostridium spp.,

Sulphite Reducing Clostridia


sample20/01/2021 89




Clostridium spp.,



sample03/03/2021 89




Clostridium spp.,



sample07/04/2021 92

84





Clostridium spp.,



sample05/05/2021 92




Clostridium spp.,



sample16/06/2021 92




Clostridium spp.,



sample14/07/2021 92




Clostridium spp.,



sample08/09/2021 92




Clostridium spp.,



sample13/10/2021 92




Clostridium spp.,



sample17/11/2021 92




Clostridium spp.,



sample08/12/2021 92




Clostridium spp.,



sample19/01/2022 92




Clostridium spp.,



sample16/03/2022 92

Swimming Pool and Spa Water


SPM0108Swimming Pool and Spa Water

Total coliforms and Escherichia coli

FWM01-RWS1lyophilised

sample28/07/2021 92


Total coliforms and Escherichia coli


sample01/12/2021 92

85



Total Viable Count (TVC) at 37°C for 24h


sample28/07/2021 92


Total Viable Count (TVC) at 37°C for 24h


sample01/12/2021 92


Pseudomonas aeruginosa ,

Coagulase Positive Staphylococci, Total Staphylococci


sample28/07/2021 92


Pseudomonas aeruginosa ,

Coagulase Positive Staphylococci, Total Staphylococci


sample01/12/2021 92

PARASITOLOGY

Drinking Water


DWP0129 Drinking Water

Cryptosporidium oocysts

and/or Giardia cysts

Count ONLY

FWPA1-DRW1 1 ml 19/01/2021 125




Count ONLY

FWPA1-DRW1 1 ml 02/03/2021 125




Count ONLY

FWPA1-DRW1 1 ml 04/05/2021 129




Count ONLY

FWPA1-DRW1 1 ml 07/09/2021 129




Count ONLY

FWPA1-DRW1 1 ml 18/01/2022 129

DWP0229 Drinking WaterCryptosporidium oocysts and/or

Giardia cysts RecoveryFWPA2-DRW1 1 ml 19/01/2021 125















86

PATHOGENS

Bathing Water


BWM0208 Bathing Water Salmonella spp. (Detection) FMOD7-RWB1lyophilised

sample19/05/2021 92

BWM0209 Bathing Water Salmonella spp. (Detection) FMOD7-RWB1lyophilised

sample22/09/2021 92

BWM0304 Bathing WaterCampylobacter spp.

(Detection)FMOD17-RWB1

lyophilised sample

19/05/2021 92

BWM0305 Bathing WaterCampylobacter spp.


lyophilised sample

22/09/2021 92

BWM0404 Bathing WaterEscherichia coli O157:H7


lyophilised sample

19/05/2021 92

Swimming Pool and Spa Water




(Detection)FMOD11-RWS1

lyophilised sample

01/12/2021 92

Water (Environmental)


LG0113 Water Legionella spp. FWM05-WAW1lyophilised

sample05/05/2021 133


sample08/09/2021 133


sample17/11/2021 133


sample16/03/2022 133

UNKNOWN ORGANISMS

Drinking Water


DWM0419 Drinking Water Organism Identification FWM04-DRW1lyophilised

sample03/03/2021 89


sample05/05/2021 92


sample08/09/2021 92


sample17/11/2021 92


sample16/03/2022 92

87

How to Order

To order with Fapas® you will need an account. If you already have an account, simply go towww.fapas.com and login with your username and password by clicking on ‘My Account’ (top right of thepage). If you have forgotten your password, you can reset it in ‘My Account’. If you have not orderedyourself, but your company has ordered from Fapas® previously, simply email us at [email protected] andwe will set up your account for you. If your company has not ordered from us before, click on the ‘register’button on the page. For further information please visit www.fapas.com and choose ‘How to Order’ fromthe top menu.

88

Fapas® has a network of agents to help you locally. Please contact your nearest office:

Argentina

Phone: +5411-4701-6262

[email protected]

Indonesia

Phone: +62 811824811

[email protected]

Russia

Phone: +7 495 707 28 68

[email protected]

Armenia

Phone: +7 495 707 28 68

[email protected]

Israel

Phone: +972572400503

[email protected]

South Africa

Phone: +27 11 691 6500

[email protected]

Austria

Phone: +49 40 49294 2930

[email protected]

Italy

Phone: + 39 02 89540225

[email protected]

Spain

Phone: +34 91.504.66.02

[email protected]

Australia

Phone: +61 (0)3 9416 0093

[email protected]

Japan

Phone: +81 3 5627 8150

[email protected]

Switzerland

Phone: +49 40 49294 2930

[email protected]

Azerbaijan

Phone: +7 495 707 28 68

[email protected]

Kazakhstan

Phone: +7 495 707 28 68

[email protected]

Taiwan

Phone: +886228484509

[email protected]

Belgium

Phone: +32 2 736 62 18

[email protected]

Korea

Phone: +81 2529 2282

[email protected]

Tajikistan

Phone: +7 495 707 28 68

[email protected]

Belarus

Phone: +7 495 707 28 68

[email protected]

Kyrgyzstan

Phone: +7 495 707 28 68

[email protected]

Thailand

Phone: +6628817404

[email protected]

China (Shanghai)

Phone: + 86 13311603693

[email protected]

Latvia

Phone: +7 495 707 28 68

[email protected]

Turkey

Phone: + 90 232 464 8006

[email protected]

China (Beijing)

Phone: +86-10-88026887

[email protected]

Lithuania

Phone: +7 495 707 28 68

[email protected]

Turkmenistan

Phone: +7 495 707 28 68

[email protected]

Egypt

Phone: +202 0114 15 215 26

[email protected]

Malaysia

Phone: +603-5122 5108

[email protected]

Ukraine

Phone: +7 495 707 28 68

[email protected]

Estonia

Phone: +7 495 707 28 68

[email protected]

Moldova

Phone: +7 495 707 28 68

[email protected]

United Arab Emirates

Phone: +971-4-2852211

[email protected]

France

Phone: +33 478643200

[email protected]

Pakistan

Phone: +92 42 3733 9116

[email protected]

United States of America

Phone: +18507278107

[email protected]

Georgia

Phone: +7 495 707 28 68

[email protected]

Philippines

Phone: +6324410430

[email protected]

Uzbekistan

Phone: +7 495 707 28 68

[email protected]

Germany

Phone: +49 40 49294 2930

[email protected]

Poland

Phone: +48 61 868 6272

[email protected]

Vietnam

Phone: +84 8 3726 0440

[email protected]

Greece

Phone: +30-210-2934745

[email protected]

Portugal

Phone: +351 22 996 20 69

[email protected]

89

Notes:

PROFICIENCY TESTING

www.fapas.com

[email protected]

Fera Science Ltd York Biotech Campus

Sand Hutton, York, YO41 1LZ United Kingdom

company/fera-science

FeraScienceLTD

labtube.tv/channel/ferascienceltd

thescientistschannel.com/fera-science-uk

www.fera.co.uk

+44 (0)1904 462100

Fera Science Ltd is a company registered in England and Wales with Company Number 9413107. VAT Registered number GB618184140. Products and services availability may change at any time without prior notice given and all content are for illustration purposes only. ©2020 Fera Science Limited. Confidential and proprietary information.

http://www.fapas.com/

mailto:[email protected]

http://www.fera.co.uk/

Documents

Proficiency Testing - Fapas · FCAL10-SEA7 145 g 25/03/2021 211 27295 Wheat Flour soya, soya protein FCAL17-CCP49 2 x 20 g 09/04/2021 217 27296 Cake Mix egg, egg white protein FCAL5-PRO10