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42 LISPENARD STREET MANHATTAN, NEW YORK 10013 Remedial Investigation Report NYC VCP Site Number: 14CVCP259M Prepared for: 42 Lispenard LLC C/O Funaro and Co LLP 350 Fifth Avenue, 41st Floor New York, New York 10018 Prepared by: EBC 1808 Middle Country Road Ridge, NY 11961 June 2014 Environmental Business Consultants

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Page 1: prtl-drprd-web.nyc.govprtl-drprd-web.nyc.gov/html/.../NYCBCP_Manhattan/... · REMEDIAL INVESTIGATION REPORT TABLE OF CONTENTS LIST OF ACRONYMS CERTIFICATIONS EXECUTIVE SUMMARY

 

42 LISPENARD STREET MANHATTAN, NEW YORK 10013

Remedial Investigation Report

NYC VCP Site Number: 14CVCP259M

Prepared for:

42 Lispenard LLC

C/O Funaro and Co LLP

350 Fifth Avenue, 41st Floor

New York, New York 10018

Prepared by:

EEBB CC

1808 Middle Country Road

Ridge, NY 11961

June 2014

Environmental Business Consultants

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REMEDIAL INVESTIGATION REPORT

TABLE OF CONTENTS

LIST OF ACRONYMS

CERTIFICATIONS

EXECUTIVE SUMMARY ...................................................................................................... i

REMEDIAL INVESTIGATION REPORT ............................................................................ 1

1.0 SITE BACKGROUND............................................................................................... 1

1.1 Site Location and Current Usage ...................................................................... 1

1.2 Proposed Redevelopment Plan ......................................................................... 2

1.3 Description of Surrounding Property................................................................ 2

2.0 SITE HISTORY.......................................................................................................... 3

2.1 Past Uses and Ownership.................................................................................. 3

2.2 Previous Investigations ..................................................................................... 3

2.3 Site Inspection................................................................................................... 3

2.4 Areas of Concern .............................................................................................. 4

3.0 PROJECT MANAGEMENT...................................................................................... 5

3.1 Project Organization ......................................................................................... 5

3.2 Health and Safety.............................................................................................. 5

3.3 Materials Management...................................................................................... 5

4.0 REMEDIAL INVESTIGATION ACTIVITIES......................................................... 6

4.1 Geophysical Investigation................................................................................. 6

4.2 Borings and Monitoring Wells.......................................................................... 6

4.3 Sample Collection and Chemical Analysis....................................................... 7

5.0 ENVIRONMENTAL EVALUATION..................................................................... 10

5.1 Geological and Hydrogeological Conditions.................................................. 10

5.2 Soil Chemistry ................................................................................................ 10

5.4 Prior Activity .................................................................................................. 10

5.5 Impediments to Remedial Action ................................................................... 11

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REMEDIAL INVESTIGATION REPORT

TABLE OF CONTENTS

TABLES Table 1 - Construction Details for Soil Borings Table 2 - Soil Analytical Results (VOCs) Table 3 - Soil Analytical Results (SVOCs) Table 4 - Soil Analytical Results (Pesticides/PCBs) Table 5 - Soil Analytical Results (Metals) Table 6 - Soil Gas Analytical Results (VOCs)

FIGURES Figure 1 - Site Location Map Figure 2 - Site Boundary Map Figure 3 - Redevelopment Plan Figure 4 - Surrounding Land Use Figure 5 - Site Sampling Locations Figure 6 - Soil Exceedences Map Figure 7 - Soil Vapor Detections

ATTACHMENTS Attachment A - Phase I Report Attachment B - Soil Boring Logs Attachment C - Groundwater Sampling Logs Attachment D - Soil Gas Sampling Logs Attachment E - Laboratory Reports in Digital Format

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LIST OF ACRONYMS Acronym Definition

AOC Area of Concern

CAMP Community Air Monitoring Plan

COC Contaminant of Concern

CPP Citizen Participation Plan

CSM Conceptual Site Model

DER-10 New York State Department of Environmental Conservation Technical Guide 10

FID Flame Ionization Detector

GPS Global Positioning System

HASP Health and Safety Plan

HAZWOPER Hazardous Waste Operations and Emergency Response

IRM Interim Remedial Measure

NAPL Non-aqueous Phase Liquid

NYC VCP New York City Voluntary Cleanup Program

NYC DOHMH New York City Department of Health and Mental Hygiene

NYC OER New York City Office of Environmental Remediation

NYS DOH ELAP

New York State Department of Health Environmental Laboratory Accreditation Program

OSHA Occupational Safety and Health Administration

PID Photo-ionization Detector

QEP Qualified Environmental Professional

RI Remedial Investigation

RIR Remedial Investigation Report

SCO Soil Cleanup Objective

SPEED Searchable Property Environmental Electronic Database

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

i Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

EXECUTIVE SUMMARY The Remedial Investigation Report (RIR) provides sufficient information for establishment of

remedial action objectives, evaluation of remedial action alternatives, and selection of a remedy

pursuant to RCNY§ 43-1407(f). The remedial investigation (RI) described in this document is

consistent with applicable guidance.

Site Location and Current Usage

The Site is located at 42 Lispenard Street in the Tribeca East Historic District of Lower

Manhattan, New York, and is currently identified as Block 194, Lot 24 on the New York City

Tax Map. Figure 1 shows the Site location. Lot 24 is a slightly irregular rectangular shaped lot

consisting of 29 feet of street frontage on Lispenard Street and a depth of approximately 93 feet

for a total of approximately 2,710 ft2. The Site is located on the south side of Lispenard Street

between Church Street and Broadway and is bordered by Lispenard Street to the north, a 5-story

apartment building with first floor commercial space to the west (40 Lisenpard Street), a 5-story

apartment building with first floor commercial space to the east (44 Lispenard Street), and a 5-

story apartment building with first floor commercial space to the south (40 Walker Street). A

map of the site boundary is shown on Figure 2.

The entire footprint of the Site is currently developed with a vacant 5-story commercial/office

building with a full cellar level. The building was constructed prior to 1894, and as of 2013, was

occupied by Pearl Paint Company.

Summary of Proposed Redevelopment Plan

The redevelopment plans include the interior renovation of the existing 5-story building to

construct cellar level retail space, renovate the first floor retail space and mezzanine level, and

renovate the 2nd through 5th floors to create apartments.

Layout of the renovation plans for the cellar and first floors is presented in Figure 3. The current

zoning designation is C6-2. The proposed use is consistent with existing zoning for the property.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

ii Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

Summary of Past Uses of Site and Areas of Concern

A Phase I Environmental Site Assessment Reports was completed for the Site by Alpha-Hydro

Environmental in August of 2013. The Phase I Environmental Site Assessment Report did not

reveal any Recognized Environmental Conditions. When the Phase I was completed, the building

was being utilized by Pear Paint Company. A boiler room was located in the basement (gas fired

equipment), and several one gallon plastic paint containers were stored on the basement floor

and on the 2nd floor. The building’s 2nd through 5th floors were all used for storage. The first

floor had a mezzanine level that was used for document storage, and the ground level of the first

floor was used for storage of paint, art and craft materials.

City Directory Listings included within the Phase I Report identified building occupants as Pearl

Furniture Show Room (1993), Legg Geo & Sons Flowers and Feathers (1938), Brigels Nicholas

E General Merchandise (1934), Ehrens Harry Merchandise and Joseph Harry Cotton Goods

(1927), Maltese Textile Corp (1923), and Ideals Manufacturers Supply Company (1920).

Historic Sanborn maps noted the Site as being developed with the current building prior to 1894,

and a certificate of occupancy dated 1921 noted use of the first floor as a store, and the second

through 5th floors as a factory.

Areas of Concern (AOCs) identified for the Site include potential for historic fill material, the

past use as a factory, and auto and manufacturing-related uses in the surrounding area.

Summary of the Work Performed under the Remedial Investigation

EBC performed the following scope of work within Site A in April of 2014:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,

buildings, etc.);

2. Installed three soil borings within the basement, and collected six soil samples for

chemical analysis from the soil borings to evaluate soil quality; and

3. Installed two sub-slab soil gas implants below the cellar slab and collected two sub-slab

soil gas samples for chemical analysis.

Summary of Environmental Findings

1. The elevation of the Site is approximately 14 feet.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

iii Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

2. Depth to groundwater is estimated to be approximately 14 feet below grade.

3. Depth to bedrock is at the Site is greater than 20 feet.

4. A native brown fine sand is present below the cellar slab.

5. Soil/fill samples collected during the RI showed no detectable concentrations of SVOCs

or PCBs, and no VOCs at a concentration above Unrestricted Use SCOs. The VOC

methylene chloride was detected in all six soil samples at a concentration below

Unrestricted Use SCOs. Methylene chloride is considered a common laboratory

contaminant when reported at the concentrations detected within these soil samples. The

pesticide 4,4'-DDT (5 mg/kg) was detected above its Unrestricted Use SCO, but below its

Restricted Residential Use SCO within one of the three soil samples collected from

immediately below the cellar slab and the metal manganese (1,830 mg/kg) was detected

above Unrestricted Use SCOs, but below its Restricted Residential Use SCO within one

of the three soil samples collected from 2 to 4 feet below the cellar slab.

6. Soil vapor samples collected during the RI indicated petroleum related VOCs were

present at low concentrations. Petroleum-related VOCs (BTEX) were detected at a

maximum concentration of 68.75 μg/m3. The CVOC trichloroethylene (TCE) was

detected in both of the soil gas samples at concentrations of 8.81 μg/m3 and 424 μg/m3.

Tetrachloroethylene (17.1 and 4.2 μg/m3), carbon tetrachloride, and 1,1,1-trichloethylene

(8.72 μg/m3) were detected below the monitoring level ranges established within the

NYSDOH Final Guidance on Soil Vapor Intrusion. However, the trichloroethylene

concentration exceeded the mitigation level. Overall the highest reported concentrations

were for acetone (maximum of 97.3 μg/m3), cis-1,2-dichloroethene (56.7 μg/m3), ethanol

(maximum of 45.4 μg/m3), and trichloroethylene (maximum of 424 μg/m3).

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

1

EEBB CC Environmental Business Consultants

1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

REMEDIAL INVESTIGATION REPORT 1.0 SITE BACKGROUND

42 Lispenard LLC has applied to enroll in the New York City Voluntary Cleanup Program (NYC

VCP) to investigate and remediate a 0.06-acre Site located at 42 Lispenard Street in the Tribeca

East Historic District of Lower Manhattan, New York. The current 5-story building will be

renovated to create residential apartments on floors 2 through 5, and retail space on the first floor

and cellar level. The portion of the RI work conducted on the Site was conducted on May 9,

2014. This RIR summarizes the nature and extent of contamination and provides sufficient

information for establishment of remedial action objectives, evaluation of remedial action

alternatives, and selection of a remedy that is protective of human health and the environment

consistent with the use of the property pursuant to RCNY§ 43-1407(f).

1.1 Site Location and Current Usage

The Site is located at 42 Lispenard Street in the Tribeca East Historic District of Lower

Manhattan, New York, and is currently identified as Block 194, Lot 24 on the New York City

Tax Map. Figure 1 shows the Site location. Lot 24 is a slightly irregular rectangular shaped lot

consisting of 29 feet of street frontage on Lispenard Street and a depth of approximately 93 feet

for a total of approximately 2,710 ft2. The Site is located on the south side of Lispenard Street

between Church Street and Broadway and is bordered by Lispenard Street to the north, a 5-story

apartment building with first floor commercial space to the west (40 Lisenpard Street), a 5-story

apartment building with first floor commercial space to the east (44 Lispenard Street), and a 5-

story apartment building with first floor commercial space to the south (40 Walker Street). A

map of the site boundary is shown on Figure 2.

The entire footprint of the Site is currently developed with a vacant 5-story commercial/office

building with a full cellar level. The building was constructed prior to 1894, and as of 2013, was

occupied by Pearl Paint Company.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

2 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

1.2 Proposed Redevelopment Plan

The redevelopment plans include the interior renovation of the existing 5-story building to

construct cellar level retail space, renovate the first floor retail space and mezzanine level, and

renovate the 2nd through 5th floors to create apartments.

Layout of the renovation plans for the cellar and first floors is presented in Figure 3. The current

zoning designation is C6-2. The proposed use is consistent with existing zoning for the property.

1.3 Description of Surrounding Property

The area immediately surrounding Site consists of 5 and 6 story commercial/office buildings,

some of which have been renovated to create residential units on the upper floors. Figure 4

shows the surrounding land usage of the adjacent properties listed below as well as additional

properties located up to 500 feet away from the Site. No hospitals, schools or daycare facilities

are located within a 250 ft radius of the Site.

Surrounding Property Usage

Direction Property Description

North – Opposite side of Lispenard Street

Block 210, Lot 7501 - 332 Canal Street Developed with a 6-story commercial/office building. Block 210, Lot 7 - 334 Canal Street Developed with a 5-story commercial/office building.

South – Adjacent Property

Block 194, Lot 12 - 40 Walker Street Developed with a 5-story apartment building with first floor commercial space.

East – Adjacent Property

Block 194, Lot 25 - 44 Lispenard Street Developed with a 5-story apartment building with first floor commercial space.

West – Adjacent Property

Block 194, Lot 23 - 40 Lispenard Street Developed with a 5-story apartment building with first floor commercial space.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

3 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

2.0 SITE HISTORY

2.1 Past Uses and Ownership

A Phase I Environmental Site Assessment Reports was completed for the Site by Alpha-Hydro

Environmental in August of 2013. The Phase I Environmental Site Assessment Report did not

reveal any Recognized Environmental Conditions. When the Phase I was completed, the building

was being utilized by Pear Paint Company. A boiler room was located in the basement (gas fired

equipment), and several one gallon plastic paint containers were stored on the basement floor

and on the 2nd floor. The building’s 2nd through 5th floors were all used for storage. The first

floor had a mezzanine level that was used for document storage, and the ground level of the first

floor was used for storage of paint, art and craft materials.

City Directory Listings included within the Phase I Report identified building occupants as Pearl

Furniture Show Room (1993), Legg Geo & Sons Flowers and Feathers (1938), Brigels Nicholas

E General Merchandise (1934), Ehrens Harry Merchandise and Joseph Harry Cotton Goods

(1927), Maltese Textile Corp (1923), and Ideals Manufacturers Supply Company (1920).

Historic Sanborn maps noted the Site as being developed with the current building prior to 1894,

and a certificate of occupancy dated 1921 noted use of the first floor as a store, and the second

through 5th floors as a factory.

2.2 Previous Investigations

EBC is not aware of any previous investigations conducted at the Site.

2.3 Site Inspection

Mr. Sunny Chen of EBC performed a site inspection on Friday, May 9, 2014, beginning at

approximately 7:00 am. The reconnaissance included a visual inspection of the cellar level of the

building, the sidewalk in front of the building and the exterior of adjacent properties. At the time

of the inspection, the Site was developed with a 5-story office/commercial building, which

according to signage on the building, was recently utilized by Pearl Craft Center. The cellar was

empty during the Site inspection, and no floor drains were observed. No evidence of an

aboveground or underground storage tank was observed.  

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

4 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

2.4 Areas of Concern

Areas of Concern (AOCs) identified for the Site include potential for historic fill material, the

past use as a factory, and auto and manufacturing-related uses in the surrounding area.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

5 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

3.0 PROJECT MANAGEMENT

3.1 Project Organization

The Qualified Environmental Profession (QEP) responsible for preparation of this RIR is Kevin

Brussee.

3.2 Health and Safety

All work described in this RIR was performed in full compliance with applicable laws and

regulations, including Site and OSHA worker safety requirements and HAZWOPER

requirements.

3.3 Materials Management

All material encountered during the RI was managed in accordance with applicable laws and

regulations.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

6 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

4.0 REMEDIAL INVESTIGATION ACTIVITIES

EBC performed the following scope of work within Site A in April of 2014:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,

buildings, etc.);

2. Installed three soil borings within the basement, and collected six soil samples for

chemical analysis from the soil borings to evaluate soil quality; and

3. Installed two sub-slab soil gas implants below the cellar slab and collected two sub-slab

soil gas samples for chemical analysis.

4.1 Geophysical Investigation

A geophysical investigation was not performed as a part of this assessment because the entire

footprint of the Site is developed with an office/commercial building constructed between 1894

and 1905.

4.2 Borings and Monitoring Wells

Drilling and Soil Logging

On May 9, 2014, three soil borings (SB1 through SB3) were performed in the approximate

locations shown on Figure 5. The soil borings were performed within existing test pits previously

excavated by the geotechnical company. From each of the three test pit locations, EBC collected

soil samples representing 0 to 2 feet below grade, and 2 to 4 feet below grade, by utilizing a

decontaminated stainless steel hand auger to remove soil from the sidewalls of the test pits. The

soil samples were field screened for the presence of VOCs with a photo-ionization detector (PID)

and visually inspected for evidence of contamination. No PID readings above background

concentrations were obtained from any of the soil borings.

Soil boring details are provided in Table 1. Boring logs were prepared by a Qualified

Environmental Professional and are attached in Attachment A.

Groundwater Monitoring Well Construction

EBC attempted to install a monitoring well within one of the test pits by hand augering a hole to

the groundwater interface. However, the vertical extend of the hand auger was reached (~7ft) and

no groundwater was encountered. EBC anticipates returning to the Site to make a second attempt

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

7 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

utilizing 8 additional feet of extension rods. If EBC is able to collect a groundwater sample, the

results will be forwarded to OER along with appropriate tables, figures, and summary.

Survey

Soil borings and sub-slab soil gas sampling locations were located to the nearest 0.10 foot with

respect to two or more permanent site features.

4.3 Sample Collection and Chemical Analysis

Sampling performed as part of the field investigation was conducted for all Areas of Concern

and also considered other means for bias of sampling based on professional judgment, area

history, discolored soil, stressed vegetation, drainage patterns, field instrument measurements,

odor, or other field indicators. All media including soil and soil vapor have been sampled and

evaluated in the RIR. Discrete (grab) samples have been used for final delineation of the nature

and extent of contamination and to determine the impact of contaminants on public health and

the environment. The sampling performed and presented in this RIR provides sufficient basis for

evaluation of remedial action alternatives, establishment of a qualitative human health exposure

assessment, and selection of a final remedy.

Soil Sampling

Six soil samples were collected for chemical analysis during this RI. Data on soil sample

collection for chemical analyses, including dates of collection and sample depths, is reported in

Tables 2, 3, 4 and 5. Figure 5 shows the location of samples collected during this RI.

Laboratories and analytical methods for soil samples collected during the RI are shown below.

The six soil samples were collected in pre-cleaned, laboratory supplied glassware, stored in a

cooler with ice and submitted for analysis to Phoenix Environmental Laboratories (Phoenix) of

587 East Middle Turnpike, Manchester, CT 06040, a New York State ELAP certified

environmental laboratory (ELAP Certification No. 11301). All soil samples were analyzed for

the presence of volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic

compounds (SVOCs) by EPA Method 8270, pesticides/PCBs by EPA Methods 8081/8082, and

target analyte list (TAL) metals.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

8 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

Soil Vapor Sampling

Three sub-slab soil gas implants were installed and three sub-slab soil gas samples were

collected for chemical analysis during this RI. The three sub-slab soil gas sampling locations are

shown in Figure 5. Sub-slab soil gas sample collection data is reported in Table 6, and the sub-

slab soil gas sampling logs are included in Attachment C. Methodologies used for soil vapor

assessment conform to the NYS DOH Final Guidance on Soil Vapor Intrusion, October 2006.

The three sub-slab vapor implants were installed by drilling a ½ inch hole through the slab with a

handheld drill through the building slab, and then inserting a ¼ inch polyethylene to a depth of

approximately 2 inches below the base of the concrete slab.

Prior to sampling, each sampling location was tested to ensure a proper surface seal had been

obtained. In accordance with NYSDOH guidance (NYSDOH Guidance for Evaluating Soil

Vapor Intrusion in the State of New York, February 2005), a tracer gas (helium) was used as a

quality assurance/quality control device to verify the integrity of the sampling point seal prior to

collecting the samples. Prior to testing and collecting samples, the surface immediately

surrounding the polyethylene tubing of the vapor implant was sealed using a 1 foot ft by 1 ft

square sheet of 2 mil HDPE plastic firmly adhered to a wetted layer of granular bentonite. The

seal was then tested by enriching the air space above the seal with a tracer gas (helium) while

continuously monitoring air drawn from the implant with a helium detector (Dielectric Model

MGD-2002, Multi-Gas Detector) for a minimum of 15 minutes. The tracer gas test procedure

was employed at all three soil vapor sampling locations. No surface seal leaks were observed at

any of the locations.

Following verification that the surface seal was tight, one to three volumes (i.e., the volume of

the sample probe and tube) of air was purged from the implant using a calibrated vacuum pump.

After purging, a 6-liter Summa® canister, fitted with a 2-hour flow regulator, was attached to the

surface tube of each of the three vapor implants. Prior to initiating sample collection, sample

identification, canister number, date and start time were recorded on tags attached to each

canister and in a bound field note book. Sampling then proceeded by fully opening the flow

control valve on each canister in turn. Immediately after opening the flow control valve on a

canister, the initial vacuum (inches of mercury) was recorded in the field book and on the sample

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

9 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

tag. When the vacuum level in the canister was between 5 and 8 inches of mercury (approx 2

hours), the flow controller valve was closed, and the final vacuum recorded in the field notebook

and on the sample tag.

The soil gas sample identification, date, start time, start vacuum, end time and end vacuum were

recorded on tags attached to each canister and on a sample log sheet (Attachment C). Samples

were submitted to Phoenix for laboratory analysis of VOCs EPA Method TO-15.

Chemical Analysis

Chemical analytical work presented in this RIR has been performed in the following manner:

Factor Description

Quality Assurance Officer The chemical analytical quality assurance is directed by Phoenix

Environmental Laboratories

Chemical Analytical

Laboratory

Chemical analytical laboratory(s) used in the RI is NYS ELAP

certified and was Phoenix Environmental Laboratories

Chemical Analytical

Methods

Soil analytical methods:

TAL Metals by EPA Method 6010C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Soil vapor analytical methods:

VOCs by TO-15 VOC parameters.

Results of Chemical Analyses

Laboratory data for soil and sub-slab soil gas are summarized in Tables 2 through 6. Laboratory

data deliverables for all samples evaluated in this RIR are provided in digital form in Attachment

D.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

10 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

5.0 ENVIRONMENTAL EVALUATION

5.1 Geological and Hydrogeological Conditions

Stratigraphy

A native brown fine sand is present below the cellar slab.

5.2 Soil Chemistry

Data collected during the RI showed no detectable concentrations of SVOCs or PCBs, and no

VOCs at a concentration above Unrestricted Use SCOs. The VOC methylene chloride was

detected in all six soil samples at a concentration below Unrestricted Use SCOs. Methylene

chloride is considered a common laboratory contaminant when reported at the concentrations

detected within these soil samples. The pesticide 4,4'-DDT (5 mg/Kg) was detected above

Unrestricted Use SCOs but below Restricted Residential Use SCOs within one of the three soil

samples collected from immediately below the cellar slab and the metal manganese (1,830

mg/Kg) was detected above Unrestricted Use SCOs, but below Restricted Residential Use SCOs

within one of the three soil samples collected from 2 to 4 feet below the cellar slab.

5.3 Soil Vapor Chemistry

Data collected during the RI indicated petroleum related VOCs were present at low

concentrations. Petroleum-related VOCs (BTEX) were detected at a maximum concentration of

68.75 μg/m3. The CVOC trichloroethylene (TCE) was detected in both of the soil gas samples at

concentrations of 8.81 μg/m3 and 424 μg/m3. Tetrachloroethylene (17.1 and 4.2 μg/m3), and

carbon tetrachloride was detected in both soil gas samples and 1,1,1-trichloethylene (8.72 μg/m3)

was detected in one of the two soil gas samples. The PCE, carbon tetrachloride and TCA

concentrations are below the monitoring level ranges established within the NYSDOH Final

Guidance on Soil Vapor Intrusion. However, the trichloroethylene concentration exceeded the

mitigation level. Overall the highest reported concentrations were for acetone (maximum of 97.3

μg/m3), cis-1,2-dichloroethene (56.7 μg/m3), ethanol (maximum of 45.4 μg/m3), and

trichloroethylene (maximum of 424 μg/m3).

5.4 Prior Activity

Based on an evaluation of the data and information from the RIR, disposal of significant amounts

of hazardous waste is not suspected for the Site.

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42 Lispenard Street, Manhattan, NY 10013 Remedial Investigation Report

11 Environmental Business Consultants

EEBB CC 1808 Middle Country Road Ridge, NY 11961

Phone 631.504.6000 Fax 631.924.2870

5.5 Impediments to Remedial Action

There are no known impediments to remedial action at this property.

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42 Lispenard Street Remedial Investigation Report New York, NY

TABLES

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Table 142 Lispenard Street

New York, NYSoil Boring / Well Information

B1 5/9/2014 4 2 Hand Auger - -B2 5/9/2014 4 2 Hand Auger - -B3 5/9/2014 4 2 Hand Auger - -

SAMPLE ID Total Depth (ft) Diameter (in)

DTW (ft)

Screen Length (ft)Date Sampling Method

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Pearl Craft Center42 Lispenard Street, Manhattan, New York 10013

TABLE 2Soil Analytical Results

Volatile Organic Compounds

Result RL Result RL Result RL Result RL Result RL Result RL

1,1,1,2-Tetrachlorothane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1,1-Trichloroethane 680 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1,2,2-Tetrachloroethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1,2-Trichloroethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1-Dichloroethane 270 26,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1-Dichloroethene 330 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,1-Dichloropropene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2,3-Trichlorobenzene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2,3-Trichloropropane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2,4-Trichlorobenzene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2,4-Trimethylbenzene 3,600 52,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2-Dibromo-3-chloropropane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2-Dibromoethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2-Dichlorobenzene 1,100 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2-Dichloroethane 20 3,100 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,2-Dichloropropane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,3,5-Trimethylbenzene 8,400 52,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,3-Dichlorobenzene 2,400 4,900 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,3-Dichloropropane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

1,4-Dichlorobenzene 1,800 13,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

2,2-Dichloropropane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

2-Chlorotoluene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

2-Hexanone (Methyl Butyl Ketone) < 26 26 < 25 25 < 27 27 < 27 27 < 26 26 < 26 26

2-Isopropyltoluene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

4-Chlorotoluene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

4-Methyl-2-Pentanone < 26 26 < 25 25 < 27 27 < 27 27 < 26 26 < 26 26

Acetone 50 100,000 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50 < 50 50

Acrylonitrile < 10 10 < 10 10 < 11 11 < 11 11 < 10 10 < 11 11

Benzene 60 4,800 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Bromobenzene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Bromochloromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Bromodichloromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Bromoform < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Bromomethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Carbon Disulfide < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Carbon tetrachloride 760 2,400 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Chlorobenzene 1,100 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Chloroethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Chloroform 370 49,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Chloromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

cis-1,2-Dichloroethene 250 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

cis-1,3-Dichloropropene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Dibromochloromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Dibromomethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Dichlorodifluoromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Ethylbenzene 1,000 41,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Hexachlorobutadiene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Isopropylbenzene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

m&p-Xylenes 260 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Methyl Ethyl Ketone (2-Butanone) 120 100,000 < 31 31 < 30 30 < 33 33 < 32 32 < 31 31 < 32 32

Methyl t-butyl ether (MTBE) 930 100,000 < 10 10 < 10 10 < 11 11 < 11 11 < 10 10 < 11 11

Methylene chloride 50 100,000 1.4 5.1 1.2 5.1 1.6 5.5 1.9 5.3 1.5 5.2 1.7 5.3

Naphthalene 12,000 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

n-Butylbenzene 12,000 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

n-Propylbenzene 3,900 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

o-Xylene 260 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

p-Isopropyltoluene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

sec-Butylbenzene 11,000 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Styrene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

tert-Butylbenzene 5,900 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Tetrachloroethene 1,300 19,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Tetrahydrofuran (THF) < 10 10 < 10 10 < 11 11 < 11 11 < 10 10 < 11 11

Toluene 700 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

trans-1,2-Dichloroethene 190 100,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

trans-1,3-Dichloropropene < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

trabs-1,4-dichloro-2-butene < 10 10 < 10 10 < 11 11 < 11 11 < 10 10 < 11 11

Trichloroethene 470 21,000 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Trichlorofluoromethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Trichlorotrifluoroethane < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Vinyl Chloride 20 900 < 5.1 5.1 < 5.1 5.1 < 5.5 5.5 < 5.3 5.3 < 5.2 5.2 < 5.3 5.3

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

RL - Reporting Limit

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance ValueBold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

µg/Kg µg/Kg µg/Kg µg/KgCOMPOUND

NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential Soil Cleanup

Objectives* µg/Kg

(0-2')

SB1

(2-4')

µg/Kg

5/9/2014 5/9/2014

SB2

(2-4')

SB3

(0-2')(0-2') (2-4')

5/9/2014 5/9/2014 5/9/2014 5/9/2014

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Pearl Craft Center42 Lispenard Street, Manhattan, New York 10013

TABLE 3 Soil Analytical Results

Semi-Volatile Organic Compounds

Result RL Result RL Result RL Result RL Result RL Result RL1,2,4,5-Tetrachlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

1,2,4-Trichlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

1,2-Dichlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

1,2-Diphenylhydrazine < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

1,3-Dichlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

1,4-Dichlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,4,5-Trichlorophenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,4,6-Trichlorophenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,4-Dichlorophenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,4-Dimethylphenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,4-Dinitrophenol < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

2,4-Dinitrotoluene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2,6-Dinitrotoluene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2-Chloronaphthalene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2-Chlorophenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2-Methylnaphthalene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2-Methylphenol (o-cresol) 330 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

2-Nitroaniline < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

2-Nitrophenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

3&4-Methylphenol (m&p-cresol) < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

3,3'-Dichlorobenzidine < 660 660 < 670 670 < 730 730 < 690 690 < 660 660 < 690 690

3-Nitroaniline < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

4,6-Dinitro-2-methylphenol < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

4-Bromophenyl phenyl ether < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

4-Chloro-3-methylphenol < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

4-Chloroaniline < 660 660 < 670 670 < 730 730 < 690 690 < 660 660 < 690 690

4-Chlorophenyl phenyl ether < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

4-Nitroaniline < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

4-Nitrophenol < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

Acenaphthene 20,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Acenaphthylene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Acetophenone < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Aniline < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

Anthracene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benz(a)anthracene 1,000 1,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benzidine < 660 660 < 670 670 < 730 730 < 690 690 < 660 660 < 690 690

Benzo(a)pyrene 1,000 1,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benzo(b)fluoranthene 1,000 1,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benzo(ghi)perylene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benzo(k)fluoranthene 800 3,900 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Benzoic acid < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

Benzyl butyl phthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Bis(2-chloroethoxy)methane < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Bis(2-chloroethyl)ether < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Bis(2-chloroisopropyl)ether < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Bis(2-ethylhexyl)phthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Carbazole < 1700 1,700 < 1700 1,700 < 1800 1,800 < 1700 1,700 < 1600 1,600 < 1700 1,700

Chrysene 1,000 3,900 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Dibenz(a,h)anthracene 330 330 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Dibenzofuran 7,000 59,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Diethyl phthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Dimethylphthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Di-n-butylphthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Di-n-octylphthalate < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Fluoranthene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Fluorene 30,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Hexachlorobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Hexachlorobutadiene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Hexachlorocyclopentadiene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Hexachloroethane < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Indeno(1,2,3-cd)pyrene 500 500 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Isophorone < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Naphthalene 12,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Nitrobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

N-Nitrosodimethylamine < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

N-Nitrosodi-n-propylamine < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

N-Nitrosodiphenylamine < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Pentachloronitrobenzene < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Pentachlorophenol 800 6,700 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Phenanthrene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Phenol 330 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Pyrene 100,000 100,000 < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Pyridine < 230 230 < 230 230 < 260 260 < 240 240 < 230 230 < 240 240

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

RL - Reporting Limit

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance ValueBold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

COMPOUNDNYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives*

SB1

(0-2') (2-4')

µg/Kg µg/Kg

NYDEC Part 375.6 Restricted Residential

Soil Cleanup Objectives*

5/9/2014 5/9/2014

(0-2') (2-4')

SB2

µg/Kgµg/Kg µg/Kg

SB3

(0-2') (2-4')

µg/Kg

5/9/2014 5/9/2014 5/9/2014 5/9/2014

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Pearl Craft Center42 Lispenard Street, Manhattan, New York 10013

TABLE 4Soil Analytical Results

Pesticides PCBs

Result RL Result RL Result RL Result RL Result RL Result RL

4,4' -DDD 3.3 13,000 < 2.4 2.4 < 2.4 2.4 < 2.6 2.6 < 2.5 2.5 < 2.4 2.4 < 2.4 2.4

4,4' -DDE 3.3 8,900 < 2.4 2.4 < 2.4 2.4 < 2.6 2.6 < 2.5 2.5 < 2.4 2.4 < 2.4 2.4

4,4' -DDT 3.3 7,900 < 2.4 2.4 < 2.4 2.4 5 2.6 < 2.5 2.5 < 2.4 2.4 < 2.4 2.4

a-BHC 20 480 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Alachlor < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Aldrin 5 97 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

b-BHC 36 360 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Chlordane 94 4,200 < 20 20 < 20 20 < 22 22 < 20 20 < 20 20 < 20 20

d-BHC 40 100,000 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Dieldrin 5 200 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Endosulfan I 2,400 24,000 < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Endosulfan II 2,400 24,000 < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Endosulfan sulfate 2,400 24,000 < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Endrin 14 11,000 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Endrin aldehyde < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Endrin ketone < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

g-BHC 100 280 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

g-Chlordane < 3.3 3.3 < 3.3 3.3 < 3.6 3.6 < 3.4 3.4 < 3.3 3.3 < 3.4 3.4

Heptachlor 42 2,100 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Heptachlor epoxide < 1.7 1.7 < 1.6 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.7 1.7

Methoxychlor < 6.6 6.6 < 6.6 6.6 < 7.3 7.3 < 6.8 6.8 < 6.6 6.6 < 6.8 6.8

Toxaphene < 170 170 < 160 160 < 180 180 < 170 170 < 160 160 < 170 170

PCB-1016 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1221 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1232 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1242 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1248 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1254 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1260 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1262 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

PCB-1268 100 1,000 < 33 33 < 33 33 < 36 36 < 34 34 < 33 33 < 34 34

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

RL - Reporting Limit

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance ValueBold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

µg/Kg µg/Kg µg/KgCOMPOUND

NYSDEC Part 375.6 Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential Soil

Cleanup Objectives* µg/Kg

SB2

(0-2') (2-4') (0-2') (2-4')

SB1 SB3

(0-2') (2-4')µg/Kg µg/Kg

5/9/2014 5/9/2014 5/9/2014 5/9/2014 5/9/2014 5/9/2014

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Pearl Craft Center42 Lispenard Street, Manhattan, New York 10013

TABLE 5Soil Analytical Results

Metals

Result RL Result RL Result RL Result RL Result RL Result RL

Aluminum 4,550 34 3,640 32 6,330 37 3,890 35 4,400 32 2,730 35

Antimony < 1.7 1.7 1.7 1.6 < 1.8 1.8 < 1.7 1.7 < 1.6 1.6 < 1.8 1.8

Arsenic 13 16 0.9 0.7 1.3 0.6 1.4 0.7 0.7 0.7 2.3 0.6 < 0.7 0.7

Barium 350 400 42.8 0.7 180 0.6 74.4 0.7 50.8 0.7 66.2 0.6 48.1 0.7

Beryllium 7.2 72 0.29 0.27 0.27 0.26 0.46 0.29 0.28 0.28 0.27 0.26 0.18 0.28

Cadmium 2.5 4.3 < 0.34 0.34 < 0.32 0.32 < 0.37 0.37 < 0.35 0.35 < 0.32 0.32 < 0.35 0.35

Calcium 924 34 879 32 1,440 37 1,120 35 4,210 32 1,190 35

Chromium 30 180 13.3 0.34 11.2 0.32 16.6 0.37 10.8 0.35 10.2 0.32 5.93 0.35

Cobalt 4.81 0.34 3.92 0.32 5.98 0.37 3.88 0.35 5.22 0.32 2.84 0.35

Copper 50 270 8.99 0.34 7.68 0.32 8.89 0.37 5.46 0.35 13.1 0.32 8.2 0.35

Iron 9,490 34 8,250 32 13,200 37 8,600 35 11,400 32 5,900 35

Lead 63 400 5.7 0.7 3.5 0.6 5.6 0.7 11.8 0.7 16.6 0.6 7.1 0.7

Magnesium 1,900 3.4 1,510 3.2 2,250 3.7 1,720 3.5 3,480 3.2 1,770 3.5

Manganese 1,600 2,000 428 3.4 1,830 32 437 3.7 268 3.5 297 3.2 453 3.5

Mercury 0.18 0.81 < 0.07 0.07 < 0.06 0.06 < 0.08 0.08 < 0.08 0.08 0.04 0.06 < 0.06 0.06

Nickel 30 310 13.5 0.34 16.8 0.32 17.3 0.37 13.9 0.35 18.2 0.32 11.5 0.35

Potassium 1,200 7 1,190 6 2,220 7 1,310 7 1,570 6 539 7

Selenium 3.9 180 < 1.4 1.4 1.2 1.3 < 1.5 1.5 < 1.4 1.4 < 1.3 1.3 < 1.4 1.4

Silver 2 180 < 0.34 0.34 < 0.32 0.32 < 0.37 0.37 < 0.35 0.35 < 0.32 0.32 < 0.35 0.35

Sodium 155 7 96 6 157 7 95 7 159 6 110 7

Thallium < 1.4 1.4 < 1.3 1.3 < 1.5 1.5 < 1.4 1.4 < 1.3 1.3 < 1.4 1.4

Vanadium 14.3 0.3 11.1 0.3 18.8 0.4 12.1 0.3 13.4 0.3 6.4 0.4

Zinc 109 10,000 14 0.7 15.2 0.6 21.4 0.7 13.7 0.7 23.2 0.6 12.7 0.7

Notes:* - 6 NYCRR Part 375-6 Remedial Program Soil Cleanup Objectives

RL - Reporting Limit

(2-4')(2-4')

Bold/highlighted- Indicated exceedance of the NYSDEC UUSCO Guidance Value

5/9/2014 5/9/2014 5/9/2014

(0-2')mg/Kg

SB3

(0-2') (2-4')mg/Kg mg/Kgmg/Kg

SB2

(0-2')

5/9/2014mg/Kg

Bold/highlighted- Indicated exceedance of the NYSDEC RRSCO Guidance Value

5/9/2014 5/9/2014

COMPOUNDNYSDEC Part 375.6

Unrestricted Use Soil Cleanup Objectives*

NYDEC Part 375.6 Restricted Residential

Soil Cleanup Objectives*

SB1

mg/Kg

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Pearl Craft Center42 Lispenard Street, Manhattan, New York 10013

TABLE 6Soil Gas

Volatile Organic Compounds

(µg/m3) (a) Result RL Result RL

1,1,1,2-Tetrachloroethane < 1.00 1 < 1.00 1

1,1,1-Trichloroethane <2.0 - 2.8 8.72 1 < 1.00 1

1,1,2,2-Tetrachloroethane <1.5 < 1.00 1 < 1.00 1

1,1,2-Trichloroethane <1.0 < 1.00 1 < 1.00 1

1,1-Dichloroethane <1.0 5.58 1 < 1.00 1

1,1-Dichloroethene <1.0 5.82 1 < 1.00 1

1,2,4-Trichlorobenzene NA < 1.00 1 < 1.00 1

1,2,4-Trimethylbenzene <1.0 1.72 1 3.98 1

1,2-Dibromoethane <1.5 < 1.00 1 < 1.00 1

1,2-Dichlorobenzene <2.0 < 1.00 1 < 1.00 1

1,2-Dichloroethane <1.0 < 1.00 1 < 1.00 1

1,2-Dichloropropane < 1.00 1 < 1.00 1

1,2-Dichlorotetrafluoroethane < 1.00 1 < 1.00 1

1,3,5-Trimethylbenzene <1.0 < 1.00 1 4.67 1

1,3-Butadiene NA < 1.00 1 < 1.00 1

1,3-Dichlorobenzene <2.0 < 1.00 1 < 1.00 1

1,4-Dichlorobenzene NA < 1.00 1 < 1.00 1

1,4-Dioxane < 1.00 1 < 1.00 1

2-Hexanone < 1.00 1 < 1.00 1

4-Ethyltoluene NA < 1.00 1 1.42 1

4-Isopropyltoluene < 1.00 1 < 1.00 1

4-Methyl-2-pentanone 1.88 1 2.54 1

Acetone NA 97.3 1 194 1

Acrylonitrile < 1.00 1 < 1.00 1

Benzene <1.6 - 4.7 2.84 1 8.24 1

Benzyl Chloride NA < 1.00 1 2.38 1

Bromodichloromethane <5.0 < 1.00 1 < 1.00 1

Bromoform <1.0 < 1.00 1 < 1.00 1

Bromomethane <1.0 < 1.00 1 < 1.00 1

Carbon Disulfide NA 3.92 1 3.52 1

Carbon Tetrachloride <3.1 0.629 0.25 0.566 0.25

Chlorobenzene <2.0 < 1.00 1 < 1.00 1

Chloroethane NA < 1.00 1 < 1.00 1

Chloroform <2.4 6 1 4 1

Chloromethane <1.0 - 1.4 < 1.00 1 < 1.00 1

cis-1,2-Dichloroethene <1.0 56.7 1 < 1.00 1

cis-1,3-Dichloropropene NA < 1.00 1 < 1.00 1

Cyclohexane NA 1.31 1 3.03 1

Dibromochloromethane <5.0 < 1.00 1 < 1.00 1

Dichlorodifluromethane NA 1.88 1 2.37 1

Ethanol 45.4 1 41.8 1

Ethyl Acetate NA 2.45 1 4.39 1

Ethylbenzene <4.3 3.86 1 4.6 1

Heptane NA 3.36 1 19.2 1

Hexachlorobutadiene NA < 1.00 1 < 1.00 1

Hexane <1.5 4.51 1 11 1

Isopropylalcohol NA 2.6 1 4.79 1

Isopropylbenzene < 1.00 1 3.19 1

Xylene (m&p) <4.3 11.3 1 14.3 1

Methyl Ethyl Ketone 10.2 1 18.4 1

MTBE NA < 1.00 1 < 1.00 1

Methylene Chloride <3.4 2.32 1 2.53 1

n-Butylbenzene < 1.00 1 < 1.00 1

Xylene (o) <4.3 4.08 1 6.55 1

Propylene NA 2.87 1 11.8 1

sec-Butylbenzene < 1.00 1 2.36 1

Styrene <1.0 4 1 1.45 1

Tetrachloroethene 17.1 0.25 4.2 0.25

Tetrahydrofuran NA 1.15 1 2.21 1

Toluene 1.0 - 6.1 15.8 1 43.3 1

trans-1,2-Dichloroethene NA < 1.00 1 < 1.00 1

trans-1,3-Dichloropropene NA < 1.00 1 < 1.00 1

Trichloroethene <1.7 424 0.25 8.81 0.25

Trichlorofluoromethane NA 1.68 1 1.46 1

Trichlorotrifluoroethane < 1.00 1 < 1.00 1

Vinyl Chloride <1.0 < 0.25 0.25 < 0.25 0.25

BTEX 37.88 68.75

Notes:NA No guidance value or standard availableRL - Reporting Limit

(a) NYSDOH Guidance for Evaluating Soil Vapor Intrusion in the State of New York, February 2005, Summary of Background Levels for Selected Compounds (NYSDOH Database, Outdoor values)

COMPOUNDS

SG-1(µg/m3)

SG-2 (µg/m3) NYSDOH Soil Outdoor

Background Levels5/9/2014 5/9/2014

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42 Lispenard Street Remedial Investigation Report New York, NY

FIGURES

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EEBBCCEnvironm ental Business Consultants

Phone 631.504.6000Fax 631.924.2870

42 LISPENARD STREET NEW YORK, NEW YORK 10013

FIGURE 1 – SITE LOCATION MAP

SITE LOCATION

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EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

1 Inch = 20 feet

0 10

SCALE:

20

LOT 23

ADJACENT 5-STORY

LOT 25LOT 24

APARTMENT w/1st

FLOOR COMMERCIAL

SIDEWALK

KEY:

Property Boundary

LISPENARD STREET

ADJACENT 5-STORY

APARTMENT w/1st

FLOOR COMMERCIAL

LOT 12LOT 13 LOT 11

93.5

8'

29'

5-STORY APARTMENT

BUILDING W/1st FLOOR

COMMERCIAL SPACE &

FULL CELLAR LEVEL

42 LISPENARD STREET, MANHATTAN, NYFIGURE 2

Site Boundary Map

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EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

CELLAR FLOOR PLAN

FIRST FLOOR PLAN

RETAIL SPACE

RETAIL SPACE

STORAGE UNITS

LOBBY

RETAIL MEZZANINE

RETAIL MEZZANINE

42 LISPENARD STREET, MANHATTAN, NYFIGURE 3

Redevelopment Plan

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EEBB CC ENVIRONMENTAL BUSINESSS CONSULTANTS 1808 Middle Country Road, Ridge, New York 11961 Phone: (631) 504-6000 Fax: (631) 924-2870

FIGURE 4 SURROUNDING LAND USE MAP

42 LISPENARD STREET MANHATTAN, NY 10013

Source: http://www.oasisnyc.net/map.aspx

Site

USPS

Synagogue

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EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

1 Inch = 20 feet

0 10

SCALE:

20

LOT 23

ADJACENT 5-STORY

LOT 25LOT 24

APARTMENT w/1st

FLOOR COMMERCIAL

SIDEWALK

KEY:

Groundwater Sampling Location

Soil Boring Location

Sub-Slab Sampling Location

Property Boundary

LISPENARD STREET

SB1

SB2

SB3

SG1

SG2

MW1 - Attempted

ADJACENT 5-STORY

APARTMENT w/1st

FLOOR COMMERCIAL

LOT 12LOT 13 LOT 11

42 LISPENARD STREET, MANHATTAN, NYFIGURE 5

Site Sampling Locations

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EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

1 Inch = 20 feet

0 10

SCALE:

20

LOT 23

ADJACENT 5-STORY

LOT 25LOT 24

APARTMENT w/1st

FLOOR COMMERCIAL

SIDEWALK

KEY:

Groundwater Sampling Location

Soil Boring Location

Sub-Slab Sampling Location

Property Boundary

LISPENARD STREET

SB1

SB2

SB3

SG1

SG2

MW1 - Attempted

ADJACENT 5-STORY

APARTMENT w/1st

FLOOR COMMERCIAL

LOT 12LOT 13 LOT 11

Exceedence of Restricted Residential SCO

Exceedence of Unrestricted Use SCO

SVOCs/Pesticides ppb

Metals ppm

ManganeseSB1 (2-4')

1,830

4,4'-DDTSB2 (0-2')

5

42 LISPENARD STREET, MANHATTAN, NYFIGURE 6

Soil Exceedences Map

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EEBBCCEnvironmental Business Consultants

Phone 631.504.6000Fax 631. 924 .2870

1 Inch = 20 feet

0 10

SCALE:

20

LOT 23 LOT 25LOT 24

SIDEWALK

KEY:

Groundwater Sampling Location

Soil Boring Location

Sub-Slab Sampling LocationProperty Boundary

LISPENARD STREET

SB1

SB2

SB3

SG1

SG2

MW1 - Attempted

LOT 12LOT 13 LOT 11

1,1,1-Trichloroethane 8.72

1,1-Dichloroethane 5.58

1,1-Dichloroethene 5.82

1,2,4-Trimethylbenzene 1.72

4-Methyl-2-pentanone 1.88

Acetone 97.3

Benzene 2.84

Carbon Disulfide 3.92

Carbon Tetrachloride 0.629

Chloroform 6

cis-1,2-Dichloroethene 56.7

Cyclohexane 1.31

Dichlorodifluromethane 1.88

Ethanol 45.4

Ethyl Acetate 2.45

Ethylbenzene 3.86

Heptane 3.36

Hexane 4.51

Isopropylalcohol 2.6

Xylene (m&p) 11.3

Methyl Ethyl Ketone 10.2

Methylene Chloride 2.32

Xylene (o) 4.08

Propylene 2.87

Styrene 4

Tetrachloroethene 17.1

Tetrahydrofuran 1.15

Toluene 15.8

Trichloroethene 424

Trichlorofluoromethane 1.68

1,2,4-Trimethylbenzene 3.98

1,3,5-Trimethylbenzene 4.67

4-Ethyltoluene 1.42

4-Methyl-2-pentanone 2.54

Acetone 194

Benzene 8.24

Benzyl Chloride 2.38

Carbon Disulfide 3.52

Carbon Tetrachloride 0.566

Chloroform 4

Cyclohexane 3.03

Dichlorodifluromethane 2.37

Ethanol 41.8

Ethyl Acetate 4.39

Ethylbenzene 4.6

Heptane 19.2

Hexane 11

Isopropylalcohol 4.79

Isopropylbenzene 3.19

Xylene (m&p) 14.3

Methyl Ethyl Ketone 18.4

Methylene Chloride 2.53

Xylene (o) 6.55

Propylene 11.8

sec-Butylbenzene 2.36

Styrene 1.45

Tetrachloroethene 4.2

Tetrahydrofuran 2.21

Toluene 43.3

Trichloroethene 8.81

Trichlorofluoromethane 1.46

SG1

SG2

Compound µg/m3

42 LISPENARD STREET, MANHATTAN, NYFIGURE 7

Posted Soil Gas Results

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42 Lispenard Street Remedial Investigation Report New York, NY

APPENDIX A PHASE I REPORT

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42 Lispenard Street Remedial Investigation Report New York, NY

APPENDIX B SOIL BORING LOGS

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Geologic Boring Log Details

Site Elevation Datum

Site Name: DTW Ground Elevation

CPL1401

Drilling Company:EBC Well SpecificationsDate Started:

Completion Depth:4 feet S. Chen

(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID

(in.) 6 in. (ppm)

0

to

4 * Soil Sample retained SB1(2-4).

Field Techician

0.0

0-2ft - Brown silty sand

2-4ft - Brown silty sand

* Soil Sample retained SB1(0-2).

SB1(NTS)

42 Lispenard Street, New York, NY

Groundwater depth

5/9/2014 5/9/2014

Method: Hand augerNot Encountered

Date Completed:

Address: Date

SB1 Boring LogLocation: Performed in the northeast corner of the cellar. Depth to Water

(ft. from grade.)

EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS

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Geologic Boring Log Details

Site Elevation Datum

Site Name: DTW Ground Elevation

CPL1401

Drilling Company:EBC Well SpecificationsDate Started:

Completion Depth:8 feet S. Chen

(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID

(in.) 6 in. (ppm)

0

to

4

to

8

Address: Date

SB2 Boring LogLocation: Performed on the left side of the approximate center of

the cellar.Depth to Water(ft. from grade.)

Method: Hand augerNot Encountered

Date Completed:

42 Lispenard Street, New York, NY

Groundwater depth

5/9/2014 5/9/2014Field Techician

0.0

0-2ft - Brown finesilty sand

2-4ft - Brown fine sand

* Soil Sample retained SB2(0-2).

SB2(NTS)

4-8ft - Brown coarse sand

* Soil Sample retained SB2(2-4).

EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS

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Geologic Boring Log Details

Site Elevation Datum

Site Name: DTW Ground Elevation

CPL1401

Drilling Company:EBC Well SpecificationsDate Started:

Completion Depth:4 feet S. Chen

(ft below Reco- Blow SOIL DESCRIPTIONgrade) very per PID

(in.) 6 in. (ppm)

0

to

4

Address: Date

SB3 Boring LogLocation: Performed in the southeast corner of the cellar. Depth to Water

(ft. from grade.)

Method: Hand augerNot Encountered

Date Completed:

42 Lispenard Street, New York, NY

Groundwater depth

5/9/2014 5/9/2014Field Techician

0.0

0-2ft - Brown fine silty sand

2-4ft - Brown fine sand

* Soil Sample retained SB3(0-2).

SB3(NTS)

* Soil Sample retained SB3(2-4).

EB CEB C ENVIRONMENTAL BUSINESS CONSULTANTS

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42 Lispenard Street Remedial Investigation Report New York, NY

APPENDIX C SOIL GAS SAMPLING LOGS

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42 Lispenard Street Remedial Investigation Report New York, NY

APPENDIX D

LABORATORY REPORTS IN DIGITAL FORMAT

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BG43580 - BG43588

Friday, May 16, 2014

Sample ID#s:

Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Project ID: 42 LISPENARD ST NY

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B1 (0-2)

Phoenix ID: BG43580

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.34Silver 0.34 05/15/14 LK SW6010mg/Kg0.344550Aluminum 34 05/14/14 LK SW6010mg/Kg6.80.9Arsenic 0.7 05/15/14 LK SW6010mg/Kg0.68

42.8Barium 0.7 05/15/14 LK SW6010mg/Kg0.340.29Beryllium 0.27 05/15/14 LK SW6010mg/Kg0.14924Calcium 34 05/14/14 LK SW6010mg/Kg31*

< 0.34Cadmium 0.34 05/15/14 LK SW6010mg/Kg0.144.81Cobalt 0.34 05/15/14 LK SW6010mg/Kg0.3413.3Chromium 0.34 05/15/14 LK SW6010mg/Kg0.348.99Copper 0.34 05/15/14 LK SW6010mg/kg0.349490Iron 34 05/14/14 LK SW6010mg/Kg B34

< 0.07Mercury 0.07 05/13/14 RS SW-7471mg/Kg0.041200Potassium 7 05/15/14 LK SW6010mg/Kg2.7N1900Magnesium 3.4 05/15/14 LK SW6010mg/Kg3.4428Manganese 3.4 05/14/14 LK SW6010mg/Kg3.4N155Sodium 7 05/15/14 LK SW6010mg/Kg2.9N13.5Nickel 0.34 05/15/14 LK SW6010mg/Kg0.345.7Lead 0.7 05/15/14 LK SW6010mg/Kg0.34

< 1.7Antimony 1.7 05/15/14 LK SW6010mg/Kg1.7< 1.4Selenium 1.4 05/15/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 05/15/14 LK SW6010mg/Kg1.414.3Vanadium 0.3 05/15/14 LK SW6010mg/Kg0.3414.0Zinc 0.7 05/15/14 LK SW6010mg/Kg B0.3498Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B1 (0-2)Phoenix I.D.: BG43580

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1221 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1232 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1242 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1248 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1254 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1260 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1262 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1268 33 05/13/14 AW SW 8082ug/Kg33

QA/QC Surrogates102% DCBP 05/13/14 AW 30 - 150 %%85% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDE 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDT 2.4 05/15/14 CE SW8081ug/Kg2.4NDa-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDa-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDAldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDb-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDChlordane 20 05/15/14 CE SW8081ug/Kg20NDd-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDDieldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndosulfan I 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan II 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan sulfate 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndrin aldehyde 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin ketone 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDHeptachlor 1.7 05/15/14 CE SW8081ug/Kg1.7NDHeptachlor epoxide 1.7 05/15/14 CE SW8081ug/Kg1.7NDMethoxychlor 6.6 05/15/14 CE SW8081ug/Kg6.6NDToxaphene 170 05/15/14 CE SW8081ug/Kg170

QA/QC Surrogates150% DCBP 05/15/14 CE 30 - 150 %%115% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.84ND1,1,1-Trichloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,1,2-Trichloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.50ND1,1-Dichloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.0

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B1 (0-2)Phoenix I.D.: BG43580

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1ND1,1-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg0.99ND1,2,3-Trichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,2,4-Trichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.73ND1,2-Dibromo-3-chloropropane 5.1 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dibromoethane 5.1 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.56ND1,2-Dichloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.45ND1,2-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,3,5-Trimethylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.67ND1,3-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.76ND1,3-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.54ND1,4-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.81ND2,2-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.86ND2-Chlorotoluene 5.1 05/13/14 JLI SW8260ug/Kg0.82ND2-Hexanone 26 05/13/14 JLI SW8260ug/Kg2.3ND2-Isopropyltoluene 5.1 05/13/14 JLI SW8260ug/Kg 10.70ND4-Chlorotoluene 5.1 05/13/14 JLI SW8260ug/Kg0.59ND4-Methyl-2-pentanone 26 05/13/14 JLI SW8260ug/Kg1.2NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.1NDAcrylonitrile 10 05/13/14 JLI SW8260ug/Kg2.9NDBenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDBromobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.66NDBromochloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.74NDBromodichloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.63NDBromoform 5.1 05/13/14 JLI SW8260ug/Kg0.71NDBromomethane 5.1 05/13/14 JLI SW8260ug/Kg3.9NDCarbon Disulfide 5.1 05/13/14 JLI SW8260ug/Kg0.83NDCarbon tetrachloride 5.1 05/13/14 JLI SW8260ug/Kg0.59NDChlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.76NDChloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.1 05/13/14 JLI SW8260ug/Kg0.93NDChloromethane 5.1 05/13/14 JLI SW8260ug/Kg2.7NDcis-1,2-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg0.55NDDibromochloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.57NDDibromomethane 5.1 05/13/14 JLI SW8260ug/Kg0.64NDDichlorodifluoromethane 5.1 05/13/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.93NDHexachlorobutadiene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.98NDm&p-Xylene 5.1 05/13/14 JLI SW8260ug/Kg2.0NDMethyl Ethyl Ketone 31 05/13/14 JLI SW8260ug/Kg4.4NDMethyl t-butyl ether (MTBE) 10 05/13/14 JLI SW8260ug/Kg1.41.4Methylene chloride 5.1 05/13/14 JLI SW8260ug/Kg0.84JSNDNaphthalene 5.1 05/13/14 JLI SW8260ug/Kg1.4NDn-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.93

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B1 (0-2)Phoenix I.D.: BG43580

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.92NDo-Xylene 5.1 05/13/14 JLI SW8260ug/Kg1.9NDp-Isopropyltoluene 5.1 05/13/14 JLI SW8260ug/Kg0.73NDsec-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.96NDStyrene 5.1 05/13/14 JLI SW8260ug/Kg1.5NDtert-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.82NDTetrachloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 05/13/14 JLI SW8260ug/Kg 14.6NDToluene 5.1 05/13/14 JLI SW8260ug/Kg0.81NDtrans-1,2-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 05/13/14 JLI SW8260ug/Kg9.5NDTrichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.1 05/13/14 JLI SW8260ug/Kg0.80NDVinyl chloride 5.1 05/13/14 JLI SW8260ug/Kg1.7

QA/QC Surrogates110% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%97% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%104% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg100ND1,2-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg94ND1,2-Diphenylhydrazine 230 05/13/14 KCA SW 8270ug/Kg110ND1,3-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg98ND1,4-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg98ND2,4,5-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg180ND2,4,6-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg110ND2,4-Dichlorophenol 230 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dimethylphenol 230 05/13/14 KCA SW 8270ug/Kg82ND2,4-Dinitrophenol 1700 05/13/14 KCA SW 8270ug/Kg230ND2,4-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg130ND2,6-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg100ND2-Chloronaphthalene 230 05/13/14 KCA SW 8270ug/Kg94ND2-Chlorophenol 230 05/13/14 KCA SW 8270ug/Kg94ND2-Methylnaphthalene 230 05/13/14 KCA SW 8270ug/Kg99ND2-Methylphenol (o-cresol) 230 05/13/14 KCA SW 8270ug/Kg160ND2-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg340ND2-Nitrophenol 230 05/13/14 KCA SW 8270ug/Kg210ND3&4-Methylphenol (m&p-cresol) 230 05/13/14 KCA SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 660 05/13/14 KCA SW 8270ug/Kg160ND3-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg720ND4,6-Dinitro-2-methylphenol 1700 05/13/14 KCA SW 8270ug/Kg360ND4-Bromophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg98ND4-Chloro-3-methylphenol 230 05/13/14 KCA SW 8270ug/Kg120ND4-Chloroaniline 660 05/13/14 KCA SW 8270ug/Kg150ND4-Chlorophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg110

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B1 (0-2)Phoenix I.D.: BG43580

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg110ND4-Nitrophenol 1700 05/13/14 KCA SW 8270ug/Kg150NDAcenaphthene 230 05/13/14 KCA SW 8270ug/Kg100NDAcenaphthylene 230 05/13/14 KCA SW 8270ug/Kg93NDAcetophenone 230 05/13/14 KCA SW 8270ug/Kg100NDAniline 1700 05/13/14 KCA SW 8270ug/Kg670NDAnthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenz(a)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzidine 660 05/13/14 KCA SW 8270ug/Kg200NDBenzo(a)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(b)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(ghi)perylene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(k)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzoic acid 1700 05/13/14 KCA SW 8270ug/Kg 1660NDBenzyl butyl phthalate 230 05/13/14 KCA SW 8270ug/Kg86NDBis(2-chloroethoxy)methane 230 05/13/14 KCA SW 8270ug/Kg92NDBis(2-chloroethyl)ether 230 05/13/14 KCA SW 8270ug/Kg90NDBis(2-chloroisopropyl)ether 230 05/13/14 KCA SW 8270ug/Kg 192NDBis(2-ethylhexyl)phthalate 230 05/13/14 KCA SW 8270ug/Kg96NDCarbazole 1700 05/13/14 KCA SW 8270ug/Kg250NDChrysene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenz(a,h)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenzofuran 230 05/13/14 KCA SW 8270ug/Kg97NDDiethyl phthalate 230 05/13/14 KCA SW 8270ug/Kg100NDDimethylphthalate 230 05/13/14 KCA SW 8270ug/Kg100NDDi-n-butylphthalate 230 05/13/14 KCA SW 8270ug/Kg88NDDi-n-octylphthalate 230 05/13/14 KCA SW 8270ug/Kg86NDFluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDFluorene 230 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg97NDHexachlorobutadiene 230 05/13/14 KCA SW 8270ug/Kg120NDHexachlorocyclopentadiene 230 05/13/14 KCA SW 8270ug/Kg100NDHexachloroethane 230 05/13/14 KCA SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDIsophorone 230 05/13/14 KCA SW 8270ug/Kg93NDNaphthalene 230 05/13/14 KCA SW 8270ug/Kg96NDNitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodimethylamine 230 05/13/14 KCA SW 8270ug/Kg94NDN-Nitrosodi-n-propylamine 230 05/13/14 KCA SW 8270ug/Kg110NDN-Nitrosodiphenylamine 230 05/13/14 KCA SW 8270ug/Kg130NDPentachloronitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDPentachlorophenol 230 05/13/14 KCA SW 8270ug/Kg130NDPhenanthrene 230 05/13/14 KCA SW 8270ug/Kg95NDPhenol 230 05/13/14 KCA SW 8270ug/Kg110NDPyrene 230 05/13/14 KCA SW 8270ug/Kg110NDPyridine 230 05/13/14 KCA SW 8270ug/Kg82

QA/QC Surrogates103% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%100% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B1 (0-2)Phoenix I.D.: BG43580

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

89% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%97% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%89% Phenol-d5 05/13/14 KCA 24 - 113 %%107% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B1 (2-4)

Phoenix ID: BG43581

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.32Silver 0.32 05/15/14 LK SW6010mg/Kg0.323640Aluminum 32 05/14/14 LK SW6010mg/Kg6.51.3Arsenic 0.6 05/15/14 LK SW6010mg/Kg0.65180Barium 0.6 05/15/14 LK SW6010mg/Kg0.320.27Beryllium 0.26 05/15/14 LK SW6010mg/Kg0.13879Calcium 32 05/14/14 LK SW6010mg/Kg30*

< 0.32Cadmium 0.32 05/15/14 LK SW6010mg/Kg0.133.92Cobalt 0.32 05/15/14 LK SW6010mg/Kg0.3211.2Chromium 0.32 05/15/14 LK SW6010mg/Kg0.327.68Copper 0.32 05/15/14 LK SW6010mg/kg0.328250Iron 32 05/14/14 LK SW6010mg/Kg B32

< 0.06Mercury 0.06 05/13/14 RS SW-7471mg/Kg0.041190Potassium 6 05/15/14 LK SW6010mg/Kg2.5N1510Magnesium 3.2 05/15/14 LK SW6010mg/Kg3.21830Manganese 32 05/14/14 LK SW6010mg/Kg32N96Sodium 6 05/15/14 LK SW6010mg/Kg2.8N

16.8Nickel 0.32 05/15/14 LK SW6010mg/Kg0.323.5Lead 0.6 05/15/14 LK SW6010mg/Kg0.321.7Antimony 1.6 05/15/14 LK SW6010mg/Kg1.61.2Selenium 1.3 05/15/14 LK SW6010mg/Kg1.1B

< 1.3Thallium 1.3 05/15/14 LK SW6010mg/Kg1.311.1Vanadium 0.3 05/15/14 LK SW6010mg/Kg0.3215.2Zinc 0.6 05/15/14 LK SW6010mg/Kg B0.3298Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B1 (2-4)Phoenix I.D.: BG43581

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1221 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1232 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1242 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1248 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1254 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1260 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1262 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1268 33 05/13/14 AW SW 8082ug/Kg33

QA/QC Surrogates95% DCBP 05/13/14 AW 30 - 150 %%86% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDE 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDT 2.4 05/15/14 CE SW8081ug/Kg2.4NDa-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDa-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDAldrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDb-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDChlordane 20 05/15/14 CE SW8081ug/Kg20NDd-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDDieldrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDEndosulfan I 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan II 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan sulfate 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDEndrin aldehyde 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin ketone 1.6 05/15/14 CE SW8081ug/Kg1.6NDg-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDg-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDHeptachlor 1.6 05/15/14 CE SW8081ug/Kg1.6NDHeptachlor epoxide 1.6 05/15/14 CE SW8081ug/Kg1.6NDMethoxychlor 6.6 05/15/14 CE SW8081ug/Kg6.6NDToxaphene 160 05/15/14 CE SW8081ug/Kg160

QA/QC Surrogates125% DCBP 05/15/14 CE 30 - 150 %%100% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.83ND1,1,1-Trichloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,1,2-Trichloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.50ND1,1-Dichloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.0

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B1 (2-4)Phoenix I.D.: BG43581

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1ND1,1-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg0.98ND1,2,3-Trichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,2,4-Trichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.73ND1,2-Dibromo-3-chloropropane 5.1 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dibromoethane 5.1 05/13/14 JLI SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.56ND1,2-Dichloroethane 5.1 05/13/14 JLI SW8260ug/Kg0.44ND1,2-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.72ND1,3,5-Trimethylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.67ND1,3-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.75ND1,3-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.54ND1,4-Dichlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.80ND2,2-Dichloropropane 5.1 05/13/14 JLI SW8260ug/Kg0.85ND2-Chlorotoluene 5.1 05/13/14 JLI SW8260ug/Kg0.81ND2-Hexanone 25 05/13/14 JLI SW8260ug/Kg2.3ND2-Isopropyltoluene 5.1 05/13/14 JLI SW8260ug/Kg 10.70ND4-Chlorotoluene 5.1 05/13/14 JLI SW8260ug/Kg0.59ND4-Methyl-2-pentanone 25 05/13/14 JLI SW8260ug/Kg1.2NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.0NDAcrylonitrile 10 05/13/14 JLI SW8260ug/Kg2.8NDBenzene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDBromobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.66NDBromochloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.74NDBromodichloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.63NDBromoform 5.1 05/13/14 JLI SW8260ug/Kg0.71NDBromomethane 5.1 05/13/14 JLI SW8260ug/Kg3.9NDCarbon Disulfide 5.1 05/13/14 JLI SW8260ug/Kg0.82NDCarbon tetrachloride 5.1 05/13/14 JLI SW8260ug/Kg0.59NDChlorobenzene 5.1 05/13/14 JLI SW8260ug/Kg0.75NDChloroethane 5.1 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.1 05/13/14 JLI SW8260ug/Kg0.92NDChloromethane 5.1 05/13/14 JLI SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg0.55NDDibromochloromethane 5.1 05/13/14 JLI SW8260ug/Kg0.57NDDibromomethane 5.1 05/13/14 JLI SW8260ug/Kg0.64NDDichlorodifluoromethane 5.1 05/13/14 JLI SW8260ug/Kg1.3NDEthylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.92NDHexachlorobutadiene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.97NDm&p-Xylene 5.1 05/13/14 JLI SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 05/13/14 JLI SW8260ug/Kg4.4NDMethyl t-butyl ether (MTBE) 10 05/13/14 JLI SW8260ug/Kg1.41.2Methylene chloride 5.1 05/13/14 JLI SW8260ug/Kg0.83JSNDNaphthalene 5.1 05/13/14 JLI SW8260ug/Kg1.4NDn-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.92

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B1 (2-4)Phoenix I.D.: BG43581

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.91NDo-Xylene 5.1 05/13/14 JLI SW8260ug/Kg1.9NDp-Isopropyltoluene 5.1 05/13/14 JLI SW8260ug/Kg0.73NDsec-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.95NDStyrene 5.1 05/13/14 JLI SW8260ug/Kg1.5NDtert-Butylbenzene 5.1 05/13/14 JLI SW8260ug/Kg0.81NDTetrachloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 05/13/14 JLI SW8260ug/Kg 14.5NDToluene 5.1 05/13/14 JLI SW8260ug/Kg0.80NDtrans-1,2-Dichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.1 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 05/13/14 JLI SW8260ug/Kg9.4NDTrichloroethene 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.1 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.1 05/13/14 JLI SW8260ug/Kg0.79NDVinyl chloride 5.1 05/13/14 JLI SW8260ug/Kg1.6

QA/QC Surrogates110% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%92% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%98% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg100ND1,2-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg94ND1,2-Diphenylhydrazine 230 05/13/14 KCA SW 8270ug/Kg110ND1,3-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg99ND1,4-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg99ND2,4,5-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg180ND2,4,6-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg110ND2,4-Dichlorophenol 230 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dimethylphenol 230 05/13/14 KCA SW 8270ug/Kg83ND2,4-Dinitrophenol 1700 05/13/14 KCA SW 8270ug/Kg230ND2,4-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg130ND2,6-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg110ND2-Chloronaphthalene 230 05/13/14 KCA SW 8270ug/Kg95ND2-Chlorophenol 230 05/13/14 KCA SW 8270ug/Kg95ND2-Methylnaphthalene 230 05/13/14 KCA SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 230 05/13/14 KCA SW 8270ug/Kg160ND2-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg340ND2-Nitrophenol 230 05/13/14 KCA SW 8270ug/Kg210ND3&4-Methylphenol (m&p-cresol) 230 05/13/14 KCA SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 670 05/13/14 KCA SW 8270ug/Kg160ND3-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg730ND4,6-Dinitro-2-methylphenol 1700 05/13/14 KCA SW 8270ug/Kg360ND4-Bromophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg98ND4-Chloro-3-methylphenol 230 05/13/14 KCA SW 8270ug/Kg120ND4-Chloroaniline 670 05/13/14 KCA SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg110

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B1 (2-4)Phoenix I.D.: BG43581

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg110ND4-Nitrophenol 1700 05/13/14 KCA SW 8270ug/Kg150NDAcenaphthene 230 05/13/14 KCA SW 8270ug/Kg100NDAcenaphthylene 230 05/13/14 KCA SW 8270ug/Kg94NDAcetophenone 230 05/13/14 KCA SW 8270ug/Kg100NDAniline 1700 05/13/14 KCA SW 8270ug/Kg670NDAnthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenz(a)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzidine 670 05/13/14 KCA SW 8270ug/Kg200NDBenzo(a)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(b)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(ghi)perylene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(k)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzoic acid 1700 05/13/14 KCA SW 8270ug/Kg 1670NDBenzyl butyl phthalate 230 05/13/14 KCA SW 8270ug/Kg86NDBis(2-chloroethoxy)methane 230 05/13/14 KCA SW 8270ug/Kg92NDBis(2-chloroethyl)ether 230 05/13/14 KCA SW 8270ug/Kg90NDBis(2-chloroisopropyl)ether 230 05/13/14 KCA SW 8270ug/Kg 193NDBis(2-ethylhexyl)phthalate 230 05/13/14 KCA SW 8270ug/Kg96NDCarbazole 1700 05/13/14 KCA SW 8270ug/Kg250NDChrysene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenz(a,h)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenzofuran 230 05/13/14 KCA SW 8270ug/Kg98NDDiethyl phthalate 230 05/13/14 KCA SW 8270ug/Kg110NDDimethylphthalate 230 05/13/14 KCA SW 8270ug/Kg100NDDi-n-butylphthalate 230 05/13/14 KCA SW 8270ug/Kg89NDDi-n-octylphthalate 230 05/13/14 KCA SW 8270ug/Kg86NDFluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDFluorene 230 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg98NDHexachlorobutadiene 230 05/13/14 KCA SW 8270ug/Kg120NDHexachlorocyclopentadiene 230 05/13/14 KCA SW 8270ug/Kg100NDHexachloroethane 230 05/13/14 KCA SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDIsophorone 230 05/13/14 KCA SW 8270ug/Kg94NDNaphthalene 230 05/13/14 KCA SW 8270ug/Kg96NDNitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodimethylamine 230 05/13/14 KCA SW 8270ug/Kg94NDN-Nitrosodi-n-propylamine 230 05/13/14 KCA SW 8270ug/Kg110NDN-Nitrosodiphenylamine 230 05/13/14 KCA SW 8270ug/Kg130NDPentachloronitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDPentachlorophenol 230 05/13/14 KCA SW 8270ug/Kg130NDPhenanthrene 230 05/13/14 KCA SW 8270ug/Kg96NDPhenol 230 05/13/14 KCA SW 8270ug/Kg110NDPyrene 230 05/13/14 KCA SW 8270ug/Kg110NDPyridine 230 05/13/14 KCA SW 8270ug/Kg82

QA/QC Surrogates80% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%86% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B1 (2-4)Phoenix I.D.: BG43581

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

65% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%80% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%68% Phenol-d5 05/13/14 KCA 24 - 113 %%103% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B2 (0-2)

Phoenix ID: BG43582

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.37Silver 0.37 05/15/14 LK SW6010mg/Kg0.376330Aluminum 37 05/14/14 LK SW6010mg/Kg7.31.4Arsenic 0.7 05/15/14 LK SW6010mg/Kg0.73

74.4Barium 0.7 05/15/14 LK SW6010mg/Kg0.370.46Beryllium 0.29 05/15/14 LK SW6010mg/Kg0.151440Calcium 37 05/14/14 LK SW6010mg/Kg34*

< 0.37Cadmium 0.37 05/15/14 LK SW6010mg/Kg0.155.98Cobalt 0.37 05/15/14 LK SW6010mg/Kg0.3716.6Chromium 0.37 05/15/14 LK SW6010mg/Kg0.378.89Copper 0.37 05/15/14 LK SW6010mg/kg0.37

13200Iron 37 05/14/14 LK SW6010mg/Kg B37< 0.08Mercury 0.08 05/13/14 RS SW-7471mg/Kg0.052220Potassium 7 05/15/14 LK SW6010mg/Kg2.9N2250Magnesium 3.7 05/15/14 LK SW6010mg/Kg3.7437Manganese 3.7 05/14/14 LK SW6010mg/Kg3.7N157Sodium 7 05/15/14 LK SW6010mg/Kg3.2N17.3Nickel 0.37 05/15/14 LK SW6010mg/Kg0.375.6Lead 0.7 05/15/14 LK SW6010mg/Kg0.37

< 1.8Antimony 1.8 05/15/14 LK SW6010mg/Kg1.8< 1.5Selenium 1.5 05/15/14 LK SW6010mg/Kg1.2< 1.5Thallium 1.5 05/15/14 LK SW6010mg/Kg1.518.8Vanadium 0.4 05/15/14 LK SW6010mg/Kg0.3721.4Zinc 0.7 05/15/14 LK SW6010mg/Kg B0.3791Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B2 (0-2)Phoenix I.D.: BG43582

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1221 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1232 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1242 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1248 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1254 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1260 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1262 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1268 36 05/13/14 AW SW 8082ug/Kg36

QA/QC Surrogates89% DCBP 05/13/14 AW 30 - 150 %%81% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.6 05/15/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 05/15/14 CE SW8081ug/Kg2.65.04,4' -DDT 2.6 05/15/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 05/15/14 CE SW8081ug/Kg3.6NDAldrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDChlordane 22 05/15/14 CE SW8081ug/Kg22NDd-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 05/15/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 05/15/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 05/15/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 05/15/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.3 05/15/14 CE SW8081ug/Kg7.3NDToxaphene 180 05/15/14 CE SW8081ug/Kg180

QA/QC Surrogates128% DCBP 05/15/14 CE 30 - 150 %%102% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.90ND1,1,1-Trichloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,1,2-Trichloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.54ND1,1-Dichloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.1

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B2 (0-2)Phoenix I.D.: BG43582

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2ND1,1-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,2,4-Trichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.79ND1,2-Dibromo-3-chloropropane 5.5 05/13/14 JLI SW8260ug/Kg1.5ND1,2-Dibromoethane 5.5 05/13/14 JLI SW8260ug/Kg1.5ND1,2-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.60ND1,2-Dichloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.48ND1,2-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,3,5-Trimethylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.73ND1,3-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.81ND1,3-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.58ND1,4-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.87ND2,2-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.92ND2-Chlorotoluene 5.5 05/13/14 JLI SW8260ug/Kg0.88ND2-Hexanone 27 05/13/14 JLI SW8260ug/Kg2.5ND2-Isopropyltoluene 5.5 05/13/14 JLI SW8260ug/Kg 10.76ND4-Chlorotoluene 5.5 05/13/14 JLI SW8260ug/Kg0.64ND4-Methyl-2-pentanone 27 05/13/14 JLI SW8260ug/Kg1.3NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.5NDAcrylonitrile 11 05/13/14 JLI SW8260ug/Kg3.1NDBenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDBromobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.71NDBromochloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.80NDBromodichloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.68NDBromoform 5.5 05/13/14 JLI SW8260ug/Kg0.77NDBromomethane 5.5 05/13/14 JLI SW8260ug/Kg4.2NDCarbon Disulfide 5.5 05/13/14 JLI SW8260ug/Kg0.89NDCarbon tetrachloride 5.5 05/13/14 JLI SW8260ug/Kg0.64NDChlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.81NDChloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.3NDChloroform 5.5 05/13/14 JLI SW8260ug/Kg1.0NDChloromethane 5.5 05/13/14 JLI SW8260ug/Kg2.9NDcis-1,2-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg0.59NDDibromochloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.62NDDibromomethane 5.5 05/13/14 JLI SW8260ug/Kg0.69NDDichlorodifluoromethane 5.5 05/13/14 JLI SW8260ug/Kg1.5NDEthylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0NDHexachlorobutadiene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDIsopropylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDm&p-Xylene 5.5 05/13/14 JLI SW8260ug/Kg2.2NDMethyl Ethyl Ketone 33 05/13/14 JLI SW8260ug/Kg4.8NDMethyl t-butyl ether (MTBE) 11 05/13/14 JLI SW8260ug/Kg1.51.6Methylene chloride 5.5 05/13/14 JLI SW8260ug/Kg0.90JSNDNaphthalene 5.5 05/13/14 JLI SW8260ug/Kg1.5NDn-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0

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B2 (0-2)Phoenix I.D.: BG43582

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.99NDo-Xylene 5.5 05/13/14 JLI SW8260ug/Kg2.1NDp-Isopropyltoluene 5.5 05/13/14 JLI SW8260ug/Kg0.79NDsec-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0NDStyrene 5.5 05/13/14 JLI SW8260ug/Kg1.6NDtert-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.88NDTetrachloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTetrahydrofuran (THF) 11 05/13/14 JLI SW8260ug/Kg 14.9NDToluene 5.5 05/13/14 JLI SW8260ug/Kg0.87NDtrans-1,2-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 11 05/13/14 JLI SW8260ug/Kg10NDTrichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorofluoromethane 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.5 05/13/14 JLI SW8260ug/Kg0.86NDVinyl chloride 5.5 05/13/14 JLI SW8260ug/Kg1.8

QA/QC Surrogates108% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%94% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%102% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 260 05/13/14 KCA SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 260 05/13/14 KCA SW 8270ug/Kg110ND1,2-Dichlorobenzene 260 05/13/14 KCA SW 8270ug/Kg100ND1,2-Diphenylhydrazine 260 05/13/14 KCA SW 8270ug/Kg120ND1,3-Dichlorobenzene 260 05/13/14 KCA SW 8270ug/Kg110ND1,4-Dichlorobenzene 260 05/13/14 KCA SW 8270ug/Kg110ND2,4,5-Trichlorophenol 260 05/13/14 KCA SW 8270ug/Kg200ND2,4,6-Trichlorophenol 260 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dichlorophenol 260 05/13/14 KCA SW 8270ug/Kg130ND2,4-Dimethylphenol 260 05/13/14 KCA SW 8270ug/Kg90ND2,4-Dinitrophenol 1800 05/13/14 KCA SW 8270ug/Kg260ND2,4-Dinitrotoluene 260 05/13/14 KCA SW 8270ug/Kg140ND2,6-Dinitrotoluene 260 05/13/14 KCA SW 8270ug/Kg120ND2-Chloronaphthalene 260 05/13/14 KCA SW 8270ug/Kg100ND2-Chlorophenol 260 05/13/14 KCA SW 8270ug/Kg100ND2-Methylnaphthalene 260 05/13/14 KCA SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 260 05/13/14 KCA SW 8270ug/Kg170ND2-Nitroaniline 1800 05/13/14 KCA SW 8270ug/Kg370ND2-Nitrophenol 260 05/13/14 KCA SW 8270ug/Kg230ND3&4-Methylphenol (m&p-cresol) 260 05/13/14 KCA SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 730 05/13/14 KCA SW 8270ug/Kg170ND3-Nitroaniline 1800 05/13/14 KCA SW 8270ug/Kg790ND4,6-Dinitro-2-methylphenol 1800 05/13/14 KCA SW 8270ug/Kg390ND4-Bromophenyl phenyl ether 260 05/13/14 KCA SW 8270ug/Kg110ND4-Chloro-3-methylphenol 260 05/13/14 KCA SW 8270ug/Kg130ND4-Chloroaniline 730 05/13/14 KCA SW 8270ug/Kg170ND4-Chlorophenyl phenyl ether 260 05/13/14 KCA SW 8270ug/Kg120

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B2 (0-2)Phoenix I.D.: BG43582

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1800 05/13/14 KCA SW 8270ug/Kg120ND4-Nitrophenol 1800 05/13/14 KCA SW 8270ug/Kg160NDAcenaphthene 260 05/13/14 KCA SW 8270ug/Kg110NDAcenaphthylene 260 05/13/14 KCA SW 8270ug/Kg100NDAcetophenone 260 05/13/14 KCA SW 8270ug/Kg110NDAniline 1800 05/13/14 KCA SW 8270ug/Kg740NDAnthracene 260 05/13/14 KCA SW 8270ug/Kg120NDBenz(a)anthracene 260 05/13/14 KCA SW 8270ug/Kg120NDBenzidine 730 05/13/14 KCA SW 8270ug/Kg210NDBenzo(a)pyrene 260 05/13/14 KCA SW 8270ug/Kg120NDBenzo(b)fluoranthene 260 05/13/14 KCA SW 8270ug/Kg120NDBenzo(ghi)perylene 260 05/13/14 KCA SW 8270ug/Kg120NDBenzo(k)fluoranthene 260 05/13/14 KCA SW 8270ug/Kg120NDBenzoic acid 1800 05/13/14 KCA SW 8270ug/Kg 1730NDBenzyl butyl phthalate 260 05/13/14 KCA SW 8270ug/Kg94NDBis(2-chloroethoxy)methane 260 05/13/14 KCA SW 8270ug/Kg100NDBis(2-chloroethyl)ether 260 05/13/14 KCA SW 8270ug/Kg99NDBis(2-chloroisopropyl)ether 260 05/13/14 KCA SW 8270ug/Kg 1100NDBis(2-ethylhexyl)phthalate 260 05/13/14 KCA SW 8270ug/Kg110NDCarbazole 1800 05/13/14 KCA SW 8270ug/Kg280NDChrysene 260 05/13/14 KCA SW 8270ug/Kg120NDDibenz(a,h)anthracene 260 05/13/14 KCA SW 8270ug/Kg120NDDibenzofuran 260 05/13/14 KCA SW 8270ug/Kg110NDDiethyl phthalate 260 05/13/14 KCA SW 8270ug/Kg120NDDimethylphthalate 260 05/13/14 KCA SW 8270ug/Kg110NDDi-n-butylphthalate 260 05/13/14 KCA SW 8270ug/Kg97NDDi-n-octylphthalate 260 05/13/14 KCA SW 8270ug/Kg94NDFluoranthene 260 05/13/14 KCA SW 8270ug/Kg120NDFluorene 260 05/13/14 KCA SW 8270ug/Kg120NDHexachlorobenzene 260 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobutadiene 260 05/13/14 KCA SW 8270ug/Kg130NDHexachlorocyclopentadiene 260 05/13/14 KCA SW 8270ug/Kg110NDHexachloroethane 260 05/13/14 KCA SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 260 05/13/14 KCA SW 8270ug/Kg120NDIsophorone 260 05/13/14 KCA SW 8270ug/Kg100NDNaphthalene 260 05/13/14 KCA SW 8270ug/Kg110NDNitrobenzene 260 05/13/14 KCA SW 8270ug/Kg130NDN-Nitrosodimethylamine 260 05/13/14 KCA SW 8270ug/Kg100NDN-Nitrosodi-n-propylamine 260 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodiphenylamine 260 05/13/14 KCA SW 8270ug/Kg140NDPentachloronitrobenzene 260 05/13/14 KCA SW 8270ug/Kg140NDPentachlorophenol 260 05/13/14 KCA SW 8270ug/Kg140NDPhenanthrene 260 05/13/14 KCA SW 8270ug/Kg100NDPhenol 260 05/13/14 KCA SW 8270ug/Kg120NDPyrene 260 05/13/14 KCA SW 8270ug/Kg130NDPyridine 260 05/13/14 KCA SW 8270ug/Kg90

QA/QC Surrogates107% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%95% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B2 (0-2)Phoenix I.D.: BG43582

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

88% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%91% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%87% Phenol-d5 05/13/14 KCA 24 - 113 %%110% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B2 (2-4)

Phoenix ID: BG43583

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.35Silver 0.35 05/15/14 LK SW6010mg/Kg0.353890Aluminum 35 05/14/14 LK SW6010mg/Kg6.90.7Arsenic 0.7 05/15/14 LK SW6010mg/Kg0.69

50.8Barium 0.7 05/15/14 LK SW6010mg/Kg0.350.28Beryllium 0.28 05/15/14 LK SW6010mg/Kg0.14B1120Calcium 35 05/14/14 LK SW6010mg/Kg32*

< 0.35Cadmium 0.35 05/15/14 LK SW6010mg/Kg0.143.88Cobalt 0.35 05/15/14 LK SW6010mg/Kg0.3510.8Chromium 0.35 05/15/14 LK SW6010mg/Kg0.355.46Copper 0.35 05/15/14 LK SW6010mg/kg0.358600Iron 35 05/14/14 LK SW6010mg/Kg B35

< 0.08Mercury 0.08 05/13/14 RS SW-7471mg/Kg0.051310Potassium 7 05/15/14 LK SW6010mg/Kg2.7N1720Magnesium 3.5 05/15/14 LK SW6010mg/Kg3.5268Manganese 3.5 05/14/14 LK SW6010mg/Kg3.5N95Sodium 7 05/15/14 LK SW6010mg/Kg3.0N

13.9Nickel 0.35 05/15/14 LK SW6010mg/Kg0.3511.8Lead 0.7 05/15/14 LK SW6010mg/Kg0.35< 1.7Antimony 1.7 05/15/14 LK SW6010mg/Kg1.7< 1.4Selenium 1.4 05/15/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 05/15/14 LK SW6010mg/Kg1.412.1Vanadium 0.3 05/15/14 LK SW6010mg/Kg0.3513.7Zinc 0.7 05/15/14 LK SW6010mg/Kg B0.3595Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B2 (2-4)Phoenix I.D.: BG43583

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1221 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1232 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1242 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1248 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1254 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1260 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1262 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1268 34 05/13/14 AW SW 8082ug/Kg34

QA/QC Surrogates92% DCBP 05/13/14 AW 30 - 150 %%85% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.5 05/15/14 CE SW8081ug/Kg2.5ND4,4' -DDE 2.5 05/15/14 CE SW8081ug/Kg2.5ND4,4' -DDT 2.5 05/15/14 CE SW8081ug/Kg2.5NDa-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDa-Chlordane 3.4 05/15/14 CE SW8081ug/Kg3.4NDAldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDb-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDChlordane 20 05/15/14 CE SW8081ug/Kg20NDd-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDDieldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndosulfan I 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndosulfan II 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndosulfan sulfate 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndrin aldehyde 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndrin ketone 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-Chlordane 3.4 05/15/14 CE SW8081ug/Kg3.4NDHeptachlor 1.7 05/15/14 CE SW8081ug/Kg1.7NDHeptachlor epoxide 1.7 05/15/14 CE SW8081ug/Kg1.7NDMethoxychlor 6.8 05/15/14 CE SW8081ug/Kg6.8NDToxaphene 170 05/15/14 CE SW8081ug/Kg170

QA/QC Surrogates128% DCBP 05/15/14 CE 30 - 150 %%100% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.87ND1,1,1-Trichloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,1,2-Trichloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.52ND1,1-Dichloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.1

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B2 (2-4)Phoenix I.D.: BG43583

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.2ND1,1-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,2,4-Trichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.77ND1,2-Dibromo-3-chloropropane 5.3 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dibromoethane 5.3 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.58ND1,2-Dichloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.47ND1,2-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,3,5-Trimethylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.70ND1,3-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.79ND1,3-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.56ND1,4-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.84ND2,2-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.89ND2-Chlorotoluene 5.3 05/13/14 JLI SW8260ug/Kg0.85ND2-Hexanone 27 05/13/14 JLI SW8260ug/Kg2.4ND2-Isopropyltoluene 5.3 05/13/14 JLI SW8260ug/Kg 10.73ND4-Chlorotoluene 5.3 05/13/14 JLI SW8260ug/Kg0.62ND4-Methyl-2-pentanone 27 05/13/14 JLI SW8260ug/Kg1.3NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.3NDAcrylonitrile 11 05/13/14 JLI SW8260ug/Kg3.0NDBenzene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDBromobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.69NDBromochloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.78NDBromodichloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.66NDBromoform 5.3 05/13/14 JLI SW8260ug/Kg0.74NDBromomethane 5.3 05/13/14 JLI SW8260ug/Kg4.1NDCarbon Disulfide 5.3 05/13/14 JLI SW8260ug/Kg0.86NDCarbon tetrachloride 5.3 05/13/14 JLI SW8260ug/Kg0.62NDChlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.79NDChloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.3 05/13/14 JLI SW8260ug/Kg0.97NDChloromethane 5.3 05/13/14 JLI SW8260ug/Kg2.8NDcis-1,2-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg0.57NDDibromochloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.60NDDibromomethane 5.3 05/13/14 JLI SW8260ug/Kg0.67NDDichlorodifluoromethane 5.3 05/13/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.97NDHexachlorobutadiene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.3 05/13/14 JLI SW8260ug/Kg1.0NDm&p-Xylene 5.3 05/13/14 JLI SW8260ug/Kg2.1NDMethyl Ethyl Ketone 32 05/13/14 JLI SW8260ug/Kg4.6NDMethyl t-butyl ether (MTBE) 11 05/13/14 JLI SW8260ug/Kg1.51.9Methylene chloride 5.3 05/13/14 JLI SW8260ug/Kg0.87JSNDNaphthalene 5.3 05/13/14 JLI SW8260ug/Kg1.4NDn-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.97

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B2 (2-4)Phoenix I.D.: BG43583

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.96NDo-Xylene 5.3 05/13/14 JLI SW8260ug/Kg2.0NDp-Isopropyltoluene 5.3 05/13/14 JLI SW8260ug/Kg0.77NDsec-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg1.0NDStyrene 5.3 05/13/14 JLI SW8260ug/Kg1.5NDtert-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.85NDTetrachloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 11 05/13/14 JLI SW8260ug/Kg 14.8NDToluene 5.3 05/13/14 JLI SW8260ug/Kg0.84NDtrans-1,2-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 11 05/13/14 JLI SW8260ug/Kg9.9NDTrichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.3 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.3 05/13/14 JLI SW8260ug/Kg0.83NDVinyl chloride 5.3 05/13/14 JLI SW8260ug/Kg1.7

QA/QC Surrogates111% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%97% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%101% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%102% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 05/13/14 KCA SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg97ND1,2-Diphenylhydrazine 240 05/13/14 KCA SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND1,4-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND2,4,5-Trichlorophenol 240 05/13/14 KCA SW 8270ug/Kg190ND2,4,6-Trichlorophenol 240 05/13/14 KCA SW 8270ug/Kg110ND2,4-Dichlorophenol 240 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dimethylphenol 240 05/13/14 KCA SW 8270ug/Kg85ND2,4-Dinitrophenol 1700 05/13/14 KCA SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 05/13/14 KCA SW 8270ug/Kg140ND2,6-Dinitrotoluene 240 05/13/14 KCA SW 8270ug/Kg110ND2-Chloronaphthalene 240 05/13/14 KCA SW 8270ug/Kg98ND2-Chlorophenol 240 05/13/14 KCA SW 8270ug/Kg98ND2-Methylnaphthalene 240 05/13/14 KCA SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 05/13/14 KCA SW 8270ug/Kg160ND2-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg350ND2-Nitrophenol 240 05/13/14 KCA SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 240 05/13/14 KCA SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 690 05/13/14 KCA SW 8270ug/Kg160ND3-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg750ND4,6-Dinitro-2-methylphenol 1700 05/13/14 KCA SW 8270ug/Kg370ND4-Bromophenyl phenyl ether 240 05/13/14 KCA SW 8270ug/Kg100ND4-Chloro-3-methylphenol 240 05/13/14 KCA SW 8270ug/Kg120ND4-Chloroaniline 690 05/13/14 KCA SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 05/13/14 KCA SW 8270ug/Kg120

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B2 (2-4)Phoenix I.D.: BG43583

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg110ND4-Nitrophenol 1700 05/13/14 KCA SW 8270ug/Kg160NDAcenaphthene 240 05/13/14 KCA SW 8270ug/Kg100NDAcenaphthylene 240 05/13/14 KCA SW 8270ug/Kg96NDAcetophenone 240 05/13/14 KCA SW 8270ug/Kg110NDAniline 1700 05/13/14 KCA SW 8270ug/Kg690NDAnthracene 240 05/13/14 KCA SW 8270ug/Kg110NDBenz(a)anthracene 240 05/13/14 KCA SW 8270ug/Kg120NDBenzidine 690 05/13/14 KCA SW 8270ug/Kg200NDBenzo(a)pyrene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 05/13/14 KCA SW 8270ug/Kg120NDBenzo(ghi)perylene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzoic acid 1700 05/13/14 KCA SW 8270ug/Kg 1690NDBenzyl butyl phthalate 240 05/13/14 KCA SW 8270ug/Kg89NDBis(2-chloroethoxy)methane 240 05/13/14 KCA SW 8270ug/Kg95NDBis(2-chloroethyl)ether 240 05/13/14 KCA SW 8270ug/Kg93NDBis(2-chloroisopropyl)ether 240 05/13/14 KCA SW 8270ug/Kg 196NDBis(2-ethylhexyl)phthalate 240 05/13/14 KCA SW 8270ug/Kg99NDCarbazole 1700 05/13/14 KCA SW 8270ug/Kg260NDChrysene 240 05/13/14 KCA SW 8270ug/Kg120NDDibenz(a,h)anthracene 240 05/13/14 KCA SW 8270ug/Kg110NDDibenzofuran 240 05/13/14 KCA SW 8270ug/Kg100NDDiethyl phthalate 240 05/13/14 KCA SW 8270ug/Kg110NDDimethylphthalate 240 05/13/14 KCA SW 8270ug/Kg110NDDi-n-butylphthalate 240 05/13/14 KCA SW 8270ug/Kg91NDDi-n-octylphthalate 240 05/13/14 KCA SW 8270ug/Kg89NDFluoranthene 240 05/13/14 KCA SW 8270ug/Kg110NDFluorene 240 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100NDHexachlorobutadiene 240 05/13/14 KCA SW 8270ug/Kg120NDHexachlorocyclopentadiene 240 05/13/14 KCA SW 8270ug/Kg110NDHexachloroethane 240 05/13/14 KCA SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 05/13/14 KCA SW 8270ug/Kg110NDIsophorone 240 05/13/14 KCA SW 8270ug/Kg96NDNaphthalene 240 05/13/14 KCA SW 8270ug/Kg99NDNitrobenzene 240 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 05/13/14 KCA SW 8270ug/Kg97NDN-Nitrosodi-n-propylamine 240 05/13/14 KCA SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 05/13/14 KCA SW 8270ug/Kg130NDPentachloronitrobenzene 240 05/13/14 KCA SW 8270ug/Kg130NDPentachlorophenol 240 05/13/14 KCA SW 8270ug/Kg130NDPhenanthrene 240 05/13/14 KCA SW 8270ug/Kg98NDPhenol 240 05/13/14 KCA SW 8270ug/Kg110NDPyrene 240 05/13/14 KCA SW 8270ug/Kg120NDPyridine 240 05/13/14 KCA SW 8270ug/Kg85

QA/QC Surrogates106% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%100% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B2 (2-4)Phoenix I.D.: BG43583

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

92% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%94% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%89% Phenol-d5 05/13/14 KCA 24 - 113 %%105% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B3 (0-2)

Phoenix ID: BG43584

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.32Silver 0.32 05/15/14 LK SW6010mg/Kg0.324400Aluminum 32 05/14/14 LK SW6010mg/Kg6.42.3Arsenic 0.6 05/15/14 LK SW6010mg/Kg0.64

66.2Barium 0.6 05/15/14 LK SW6010mg/Kg0.320.27Beryllium 0.26 05/15/14 LK SW6010mg/Kg0.134210Calcium 32 05/14/14 LK SW6010mg/Kg29*

< 0.32Cadmium 0.32 05/15/14 LK SW6010mg/Kg0.135.22Cobalt 0.32 05/15/14 LK SW6010mg/Kg0.3210.2Chromium 0.32 05/15/14 LK SW6010mg/Kg0.3213.1Copper 0.32 05/15/14 LK SW6010mg/kg0.32

11400Iron 32 05/14/14 LK SW6010mg/Kg B320.04Mercury 0.06 05/13/14 RS SW-7471mg/Kg0.03B1570Potassium 6 05/15/14 LK SW6010mg/Kg2.5N3480Magnesium 3.2 05/15/14 LK SW6010mg/Kg3.2297Manganese 3.2 05/14/14 LK SW6010mg/Kg3.2N159Sodium 6 05/15/14 LK SW6010mg/Kg2.7N18.2Nickel 0.32 05/15/14 LK SW6010mg/Kg0.3216.6Lead 0.6 05/15/14 LK SW6010mg/Kg0.32< 1.6Antimony 1.6 05/15/14 LK SW6010mg/Kg1.6< 1.3Selenium 1.3 05/15/14 LK SW6010mg/Kg1.1< 1.3Thallium 1.3 05/15/14 LK SW6010mg/Kg1.313.4Vanadium 0.3 05/15/14 LK SW6010mg/Kg0.3223.2Zinc 0.6 05/15/14 LK SW6010mg/Kg B0.3298Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B3 (0-2)Phoenix I.D.: BG43584

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1221 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1232 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1242 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1248 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1254 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1260 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1262 33 05/13/14 AW SW 8082ug/Kg33NDPCB-1268 33 05/13/14 AW SW 8082ug/Kg33

QA/QC Surrogates104% DCBP 05/13/14 AW 30 - 150 %%90% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDE 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDT 2.4 05/15/14 CE SW8081ug/Kg2.4NDa-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDa-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDAldrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDb-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDChlordane 20 05/15/14 CE SW8081ug/Kg20NDd-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDDieldrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDEndosulfan I 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan II 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndosulfan sulfate 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin 1.6 05/15/14 CE SW8081ug/Kg1.6NDEndrin aldehyde 3.3 05/15/14 CE SW8081ug/Kg3.3NDEndrin ketone 1.6 05/15/14 CE SW8081ug/Kg1.6NDg-BHC 1.6 05/15/14 CE SW8081ug/Kg1.6NDg-Chlordane 3.3 05/15/14 CE SW8081ug/Kg3.3NDHeptachlor 1.6 05/15/14 CE SW8081ug/Kg1.6NDHeptachlor epoxide 1.6 05/15/14 CE SW8081ug/Kg1.6NDMethoxychlor 6.6 05/15/14 CE SW8081ug/Kg6.6NDToxaphene 160 05/15/14 CE SW8081ug/Kg160

QA/QC Surrogates148% DCBP 05/15/14 CE 30 - 150 %%114% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.2 05/13/14 JLI SW8260ug/Kg0.85ND1,1,1-Trichloroethane 5.2 05/13/14 JLI SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.2 05/13/14 JLI SW8260ug/Kg0.73ND1,1,2-Trichloroethane 5.2 05/13/14 JLI SW8260ug/Kg0.51ND1,1-Dichloroethane 5.2 05/13/14 JLI SW8260ug/Kg1.0

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B3 (0-2)Phoenix I.D.: BG43584

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.2 05/13/14 JLI SW8260ug/Kg1.1ND1,1-Dichloropropene 5.2 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.2 05/13/14 JLI SW8260ug/Kg0.73ND1,2,4-Trichlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.74ND1,2-Dibromo-3-chloropropane 5.2 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dibromoethane 5.2 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg0.57ND1,2-Dichloroethane 5.2 05/13/14 JLI SW8260ug/Kg0.45ND1,2-Dichloropropane 5.2 05/13/14 JLI SW8260ug/Kg0.73ND1,3,5-Trimethylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.68ND1,3-Dichlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg0.76ND1,3-Dichloropropane 5.2 05/13/14 JLI SW8260ug/Kg0.55ND1,4-Dichlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg0.81ND2,2-Dichloropropane 5.2 05/13/14 JLI SW8260ug/Kg0.87ND2-Chlorotoluene 5.2 05/13/14 JLI SW8260ug/Kg0.82ND2-Hexanone 26 05/13/14 JLI SW8260ug/Kg2.3ND2-Isopropyltoluene 5.2 05/13/14 JLI SW8260ug/Kg 10.71ND4-Chlorotoluene 5.2 05/13/14 JLI SW8260ug/Kg0.60ND4-Methyl-2-pentanone 26 05/13/14 JLI SW8260ug/Kg1.2NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.1NDAcrylonitrile 10 05/13/14 JLI SW8260ug/Kg2.9NDBenzene 5.2 05/13/14 JLI SW8260ug/Kg1.0NDBromobenzene 5.2 05/13/14 JLI SW8260ug/Kg0.67NDBromochloromethane 5.2 05/13/14 JLI SW8260ug/Kg0.75NDBromodichloromethane 5.2 05/13/14 JLI SW8260ug/Kg0.64NDBromoform 5.2 05/13/14 JLI SW8260ug/Kg0.72NDBromomethane 5.2 05/13/14 JLI SW8260ug/Kg4.0NDCarbon Disulfide 5.2 05/13/14 JLI SW8260ug/Kg0.83NDCarbon tetrachloride 5.2 05/13/14 JLI SW8260ug/Kg0.60NDChlorobenzene 5.2 05/13/14 JLI SW8260ug/Kg0.76NDChloroethane 5.2 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.2 05/13/14 JLI SW8260ug/Kg0.94NDChloromethane 5.2 05/13/14 JLI SW8260ug/Kg2.7NDcis-1,2-Dichloroethene 5.2 05/13/14 JLI SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.2 05/13/14 JLI SW8260ug/Kg0.56NDDibromochloromethane 5.2 05/13/14 JLI SW8260ug/Kg0.58NDDibromomethane 5.2 05/13/14 JLI SW8260ug/Kg0.65NDDichlorodifluoromethane 5.2 05/13/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.94NDHexachlorobutadiene 5.2 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.99NDm&p-Xylene 5.2 05/13/14 JLI SW8260ug/Kg2.0NDMethyl Ethyl Ketone 31 05/13/14 JLI SW8260ug/Kg4.5NDMethyl t-butyl ether (MTBE) 10 05/13/14 JLI SW8260ug/Kg1.41.5Methylene chloride 5.2 05/13/14 JLI SW8260ug/Kg0.85JSNDNaphthalene 5.2 05/13/14 JLI SW8260ug/Kg1.4NDn-Butylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.94

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B3 (0-2)Phoenix I.D.: BG43584

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.93NDo-Xylene 5.2 05/13/14 JLI SW8260ug/Kg2.0NDp-Isopropyltoluene 5.2 05/13/14 JLI SW8260ug/Kg0.74NDsec-Butylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.97NDStyrene 5.2 05/13/14 JLI SW8260ug/Kg1.5NDtert-Butylbenzene 5.2 05/13/14 JLI SW8260ug/Kg0.82NDTetrachloroethene 5.2 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 05/13/14 JLI SW8260ug/Kg 14.6NDToluene 5.2 05/13/14 JLI SW8260ug/Kg0.81NDtrans-1,2-Dichloroethene 5.2 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.2 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 10 05/13/14 JLI SW8260ug/Kg9.6NDTrichloroethene 5.2 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.2 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.2 05/13/14 JLI SW8260ug/Kg0.80NDVinyl chloride 5.2 05/13/14 JLI SW8260ug/Kg1.7

QA/QC Surrogates112% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%99% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%96% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%102% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg100ND1,2-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg93ND1,2-Diphenylhydrazine 230 05/13/14 KCA SW 8270ug/Kg110ND1,3-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg98ND1,4-Dichlorobenzene 230 05/13/14 KCA SW 8270ug/Kg98ND2,4,5-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg180ND2,4,6-Trichlorophenol 230 05/13/14 KCA SW 8270ug/Kg110ND2,4-Dichlorophenol 230 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dimethylphenol 230 05/13/14 KCA SW 8270ug/Kg82ND2,4-Dinitrophenol 1600 05/13/14 KCA SW 8270ug/Kg230ND2,4-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg130ND2,6-Dinitrotoluene 230 05/13/14 KCA SW 8270ug/Kg100ND2-Chloronaphthalene 230 05/13/14 KCA SW 8270ug/Kg94ND2-Chlorophenol 230 05/13/14 KCA SW 8270ug/Kg94ND2-Methylnaphthalene 230 05/13/14 KCA SW 8270ug/Kg98ND2-Methylphenol (o-cresol) 230 05/13/14 KCA SW 8270ug/Kg160ND2-Nitroaniline 1600 05/13/14 KCA SW 8270ug/Kg330ND2-Nitrophenol 230 05/13/14 KCA SW 8270ug/Kg210ND3&4-Methylphenol (m&p-cresol) 230 05/13/14 KCA SW 8270ug/Kg 1130ND3,3'-Dichlorobenzidine 660 05/13/14 KCA SW 8270ug/Kg160ND3-Nitroaniline 1600 05/13/14 KCA SW 8270ug/Kg720ND4,6-Dinitro-2-methylphenol 1600 05/13/14 KCA SW 8270ug/Kg350ND4-Bromophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg97ND4-Chloro-3-methylphenol 230 05/13/14 KCA SW 8270ug/Kg120ND4-Chloroaniline 660 05/13/14 KCA SW 8270ug/Kg150ND4-Chlorophenyl phenyl ether 230 05/13/14 KCA SW 8270ug/Kg110

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B3 (0-2)Phoenix I.D.: BG43584

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1600 05/13/14 KCA SW 8270ug/Kg110ND4-Nitrophenol 1600 05/13/14 KCA SW 8270ug/Kg150NDAcenaphthene 230 05/13/14 KCA SW 8270ug/Kg100NDAcenaphthylene 230 05/13/14 KCA SW 8270ug/Kg92NDAcetophenone 230 05/13/14 KCA SW 8270ug/Kg100NDAniline 1600 05/13/14 KCA SW 8270ug/Kg670NDAnthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenz(a)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzidine 660 05/13/14 KCA SW 8270ug/Kg190NDBenzo(a)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(b)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(ghi)perylene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzo(k)fluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDBenzoic acid 1600 05/13/14 KCA SW 8270ug/Kg 1660NDBenzyl butyl phthalate 230 05/13/14 KCA SW 8270ug/Kg85NDBis(2-chloroethoxy)methane 230 05/13/14 KCA SW 8270ug/Kg91NDBis(2-chloroethyl)ether 230 05/13/14 KCA SW 8270ug/Kg89NDBis(2-chloroisopropyl)ether 230 05/13/14 KCA SW 8270ug/Kg 192NDBis(2-ethylhexyl)phthalate 230 05/13/14 KCA SW 8270ug/Kg95NDCarbazole 1600 05/13/14 KCA SW 8270ug/Kg250NDChrysene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenz(a,h)anthracene 230 05/13/14 KCA SW 8270ug/Kg110NDDibenzofuran 230 05/13/14 KCA SW 8270ug/Kg96NDDiethyl phthalate 230 05/13/14 KCA SW 8270ug/Kg100NDDimethylphthalate 230 05/13/14 KCA SW 8270ug/Kg100NDDi-n-butylphthalate 230 05/13/14 KCA SW 8270ug/Kg88NDDi-n-octylphthalate 230 05/13/14 KCA SW 8270ug/Kg85NDFluoranthene 230 05/13/14 KCA SW 8270ug/Kg110NDFluorene 230 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobenzene 230 05/13/14 KCA SW 8270ug/Kg96NDHexachlorobutadiene 230 05/13/14 KCA SW 8270ug/Kg120NDHexachlorocyclopentadiene 230 05/13/14 KCA SW 8270ug/Kg100NDHexachloroethane 230 05/13/14 KCA SW 8270ug/Kg99NDIndeno(1,2,3-cd)pyrene 230 05/13/14 KCA SW 8270ug/Kg110NDIsophorone 230 05/13/14 KCA SW 8270ug/Kg92NDNaphthalene 230 05/13/14 KCA SW 8270ug/Kg95NDNitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodimethylamine 230 05/13/14 KCA SW 8270ug/Kg93NDN-Nitrosodi-n-propylamine 230 05/13/14 KCA SW 8270ug/Kg110NDN-Nitrosodiphenylamine 230 05/13/14 KCA SW 8270ug/Kg130NDPentachloronitrobenzene 230 05/13/14 KCA SW 8270ug/Kg120NDPentachlorophenol 230 05/13/14 KCA SW 8270ug/Kg120NDPhenanthrene 230 05/13/14 KCA SW 8270ug/Kg94NDPhenol 230 05/13/14 KCA SW 8270ug/Kg110NDPyrene 230 05/13/14 KCA SW 8270ug/Kg110NDPyridine 230 05/13/14 KCA SW 8270ug/Kg81

QA/QC Surrogates104% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%98% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B3 (0-2)Phoenix I.D.: BG43584

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

91% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%92% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%87% Phenol-d5 05/13/14 KCA 24 - 113 %%110% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

B3 (2-4)

Phoenix ID: BG43585

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.35Silver 0.35 05/15/14 LK SW6010mg/Kg0.352730Aluminum 35 05/14/14 LK SW6010mg/Kg7.0< 0.7Arsenic 0.7 05/15/14 LK SW6010mg/Kg0.7048.1Barium 0.7 05/15/14 LK SW6010mg/Kg0.350.18Beryllium 0.28 05/15/14 LK SW6010mg/Kg0.14B1190Calcium 35 05/14/14 LK SW6010mg/Kg32*

< 0.35Cadmium 0.35 05/15/14 LK SW6010mg/Kg0.142.84Cobalt 0.35 05/15/14 LK SW6010mg/Kg0.355.93Chromium 0.35 05/15/14 LK SW6010mg/Kg0.358.20Copper 0.35 05/15/14 LK SW6010mg/kg0.355900Iron 35 05/14/14 LK SW6010mg/Kg B35

< 0.06Mercury 0.06 05/13/14 RS SW-7471mg/Kg0.04539Potassium 7 05/15/14 LK SW6010mg/Kg2.7N

1770Magnesium 3.5 05/15/14 LK SW6010mg/Kg3.5453Manganese 3.5 05/14/14 LK SW6010mg/Kg3.5N110Sodium 7 05/15/14 LK SW6010mg/Kg3.0N11.5Nickel 0.35 05/15/14 LK SW6010mg/Kg0.357.1Lead 0.7 05/15/14 LK SW6010mg/Kg0.35

< 1.8Antimony 1.8 05/15/14 LK SW6010mg/Kg1.8< 1.4Selenium 1.4 05/15/14 LK SW6010mg/Kg1.2< 1.4Thallium 1.4 05/15/14 LK SW6010mg/Kg1.46.4Vanadium 0.4 05/15/14 LK SW6010mg/Kg0.35

12.7Zinc 0.7 05/15/14 LK SW6010mg/Kg B0.3596Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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B3 (2-4)Phoenix I.D.: BG43585

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1221 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1232 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1242 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1248 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1254 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1260 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1262 34 05/13/14 AW SW 8082ug/Kg34NDPCB-1268 34 05/13/14 AW SW 8082ug/Kg34

QA/QC Surrogates96% DCBP 05/13/14 AW 30 - 150 %%86% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDE 2.4 05/15/14 CE SW8081ug/Kg2.4ND4,4' -DDT 2.4 05/15/14 CE SW8081ug/Kg2.4NDa-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDa-Chlordane 3.4 05/15/14 CE SW8081ug/Kg3.4NDAldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDb-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDChlordane 20 05/15/14 CE SW8081ug/Kg20NDd-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDDieldrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndosulfan I 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndosulfan II 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndosulfan sulfate 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndrin 1.7 05/15/14 CE SW8081ug/Kg1.7NDEndrin aldehyde 3.4 05/15/14 CE SW8081ug/Kg3.4NDEndrin ketone 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-BHC 1.7 05/15/14 CE SW8081ug/Kg1.7NDg-Chlordane 3.4 05/15/14 CE SW8081ug/Kg3.4NDHeptachlor 1.7 05/15/14 CE SW8081ug/Kg1.7NDHeptachlor epoxide 1.7 05/15/14 CE SW8081ug/Kg1.7NDMethoxychlor 6.8 05/15/14 CE SW8081ug/Kg6.8NDToxaphene 170 05/15/14 CE SW8081ug/Kg170

QA/QC Surrogates137% DCBP 05/15/14 CE 30 - 150 %%106% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.86ND1,1,1-Trichloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,1,2-Trichloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.52ND1,1-Dichloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.0

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B3 (2-4)Phoenix I.D.: BG43585

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,1-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,2,4-Trichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.76ND1,2-Dibromo-3-chloropropane 5.3 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dibromoethane 5.3 05/13/14 JLI SW8260ug/Kg1.4ND1,2-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.58ND1,2-Dichloroethane 5.3 05/13/14 JLI SW8260ug/Kg0.46ND1,2-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.75ND1,3,5-Trimethylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.69ND1,3-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.78ND1,3-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.56ND1,4-Dichlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.83ND2,2-Dichloropropane 5.3 05/13/14 JLI SW8260ug/Kg0.88ND2-Chlorotoluene 5.3 05/13/14 JLI SW8260ug/Kg0.84ND2-Hexanone 26 05/13/14 JLI SW8260ug/Kg2.4ND2-Isopropyltoluene 5.3 05/13/14 JLI SW8260ug/Kg 10.73ND4-Chlorotoluene 5.3 05/13/14 JLI SW8260ug/Kg0.61ND4-Methyl-2-pentanone 26 05/13/14 JLI SW8260ug/Kg1.3NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.2NDAcrylonitrile 11 05/13/14 JLI SW8260ug/Kg3.0NDBenzene 5.3 05/13/14 JLI SW8260ug/Kg1.0NDBromobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.68NDBromochloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.77NDBromodichloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.65NDBromoform 5.3 05/13/14 JLI SW8260ug/Kg0.74NDBromomethane 5.3 05/13/14 JLI SW8260ug/Kg4.1NDCarbon Disulfide 5.3 05/13/14 JLI SW8260ug/Kg0.85NDCarbon tetrachloride 5.3 05/13/14 JLI SW8260ug/Kg0.61NDChlorobenzene 5.3 05/13/14 JLI SW8260ug/Kg0.78NDChloroethane 5.3 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.3 05/13/14 JLI SW8260ug/Kg0.96NDChloromethane 5.3 05/13/14 JLI SW8260ug/Kg2.8NDcis-1,2-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg0.57NDDibromochloromethane 5.3 05/13/14 JLI SW8260ug/Kg0.59NDDibromomethane 5.3 05/13/14 JLI SW8260ug/Kg0.66NDDichlorodifluoromethane 5.3 05/13/14 JLI SW8260ug/Kg1.4NDEthylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.96NDHexachlorobutadiene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.3 05/13/14 JLI SW8260ug/Kg1.0NDm&p-Xylene 5.3 05/13/14 JLI SW8260ug/Kg2.1NDMethyl Ethyl Ketone 32 05/13/14 JLI SW8260ug/Kg4.6NDMethyl t-butyl ether (MTBE) 11 05/13/14 JLI SW8260ug/Kg1.51.7Methylene chloride 5.3 05/13/14 JLI SW8260ug/Kg0.86JSNDNaphthalene 5.3 05/13/14 JLI SW8260ug/Kg1.4NDn-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.96

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B3 (2-4)Phoenix I.D.: BG43585

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.95NDo-Xylene 5.3 05/13/14 JLI SW8260ug/Kg2.0NDp-Isopropyltoluene 5.3 05/13/14 JLI SW8260ug/Kg0.76NDsec-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.99NDStyrene 5.3 05/13/14 JLI SW8260ug/Kg1.5NDtert-Butylbenzene 5.3 05/13/14 JLI SW8260ug/Kg0.84NDTetrachloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 11 05/13/14 JLI SW8260ug/Kg 14.7NDToluene 5.3 05/13/14 JLI SW8260ug/Kg0.83NDtrans-1,2-Dichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 11 05/13/14 JLI SW8260ug/Kg9.8NDTrichloroethene 5.3 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.3 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.3 05/13/14 JLI SW8260ug/Kg0.82NDVinyl chloride 5.3 05/13/14 JLI SW8260ug/Kg1.7

QA/QC Surrogates114% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%93% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%104% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 240 05/13/14 KCA SW 8270ug/Kg120ND1,2,4-Trichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND1,2-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg97ND1,2-Diphenylhydrazine 240 05/13/14 KCA SW 8270ug/Kg110ND1,3-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND1,4-Dichlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100ND2,4,5-Trichlorophenol 240 05/13/14 KCA SW 8270ug/Kg190ND2,4,6-Trichlorophenol 240 05/13/14 KCA SW 8270ug/Kg110ND2,4-Dichlorophenol 240 05/13/14 KCA SW 8270ug/Kg120ND2,4-Dimethylphenol 240 05/13/14 KCA SW 8270ug/Kg85ND2,4-Dinitrophenol 1700 05/13/14 KCA SW 8270ug/Kg240ND2,4-Dinitrotoluene 240 05/13/14 KCA SW 8270ug/Kg140ND2,6-Dinitrotoluene 240 05/13/14 KCA SW 8270ug/Kg110ND2-Chloronaphthalene 240 05/13/14 KCA SW 8270ug/Kg97ND2-Chlorophenol 240 05/13/14 KCA SW 8270ug/Kg97ND2-Methylnaphthalene 240 05/13/14 KCA SW 8270ug/Kg100ND2-Methylphenol (o-cresol) 240 05/13/14 KCA SW 8270ug/Kg160ND2-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg350ND2-Nitrophenol 240 05/13/14 KCA SW 8270ug/Kg220ND3&4-Methylphenol (m&p-cresol) 240 05/13/14 KCA SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 690 05/13/14 KCA SW 8270ug/Kg160ND3-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg750ND4,6-Dinitro-2-methylphenol 1700 05/13/14 KCA SW 8270ug/Kg370ND4-Bromophenyl phenyl ether 240 05/13/14 KCA SW 8270ug/Kg100ND4-Chloro-3-methylphenol 240 05/13/14 KCA SW 8270ug/Kg120ND4-Chloroaniline 690 05/13/14 KCA SW 8270ug/Kg160ND4-Chlorophenyl phenyl ether 240 05/13/14 KCA SW 8270ug/Kg120

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B3 (2-4)Phoenix I.D.: BG43585

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1700 05/13/14 KCA SW 8270ug/Kg110ND4-Nitrophenol 1700 05/13/14 KCA SW 8270ug/Kg150NDAcenaphthene 240 05/13/14 KCA SW 8270ug/Kg100NDAcenaphthylene 240 05/13/14 KCA SW 8270ug/Kg96NDAcetophenone 240 05/13/14 KCA SW 8270ug/Kg110NDAniline 1700 05/13/14 KCA SW 8270ug/Kg690NDAnthracene 240 05/13/14 KCA SW 8270ug/Kg110NDBenz(a)anthracene 240 05/13/14 KCA SW 8270ug/Kg120NDBenzidine 690 05/13/14 KCA SW 8270ug/Kg200NDBenzo(a)pyrene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzo(b)fluoranthene 240 05/13/14 KCA SW 8270ug/Kg120NDBenzo(ghi)perylene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzo(k)fluoranthene 240 05/13/14 KCA SW 8270ug/Kg110NDBenzoic acid 1700 05/13/14 KCA SW 8270ug/Kg 1690NDBenzyl butyl phthalate 240 05/13/14 KCA SW 8270ug/Kg88NDBis(2-chloroethoxy)methane 240 05/13/14 KCA SW 8270ug/Kg95NDBis(2-chloroethyl)ether 240 05/13/14 KCA SW 8270ug/Kg93NDBis(2-chloroisopropyl)ether 240 05/13/14 KCA SW 8270ug/Kg 195NDBis(2-ethylhexyl)phthalate 240 05/13/14 KCA SW 8270ug/Kg99NDCarbazole 1700 05/13/14 KCA SW 8270ug/Kg260NDChrysene 240 05/13/14 KCA SW 8270ug/Kg120NDDibenz(a,h)anthracene 240 05/13/14 KCA SW 8270ug/Kg110NDDibenzofuran 240 05/13/14 KCA SW 8270ug/Kg100NDDiethyl phthalate 240 05/13/14 KCA SW 8270ug/Kg110NDDimethylphthalate 240 05/13/14 KCA SW 8270ug/Kg110NDDi-n-butylphthalate 240 05/13/14 KCA SW 8270ug/Kg91NDDi-n-octylphthalate 240 05/13/14 KCA SW 8270ug/Kg88NDFluoranthene 240 05/13/14 KCA SW 8270ug/Kg110NDFluorene 240 05/13/14 KCA SW 8270ug/Kg110NDHexachlorobenzene 240 05/13/14 KCA SW 8270ug/Kg100NDHexachlorobutadiene 240 05/13/14 KCA SW 8270ug/Kg120NDHexachlorocyclopentadiene 240 05/13/14 KCA SW 8270ug/Kg100NDHexachloroethane 240 05/13/14 KCA SW 8270ug/Kg100NDIndeno(1,2,3-cd)pyrene 240 05/13/14 KCA SW 8270ug/Kg110NDIsophorone 240 05/13/14 KCA SW 8270ug/Kg96NDNaphthalene 240 05/13/14 KCA SW 8270ug/Kg99NDNitrobenzene 240 05/13/14 KCA SW 8270ug/Kg120NDN-Nitrosodimethylamine 240 05/13/14 KCA SW 8270ug/Kg97NDN-Nitrosodi-n-propylamine 240 05/13/14 KCA SW 8270ug/Kg110NDN-Nitrosodiphenylamine 240 05/13/14 KCA SW 8270ug/Kg130NDPentachloronitrobenzene 240 05/13/14 KCA SW 8270ug/Kg130NDPentachlorophenol 240 05/13/14 KCA SW 8270ug/Kg130NDPhenanthrene 240 05/13/14 KCA SW 8270ug/Kg98NDPhenol 240 05/13/14 KCA SW 8270ug/Kg110NDPyrene 240 05/13/14 KCA SW 8270ug/Kg120NDPyridine 240 05/13/14 KCA SW 8270ug/Kg84

QA/QC Surrogates102% 2,4,6-Tribromophenol 05/13/14 KCA 19 - 122 %%95% 2-Fluorobiphenyl 05/13/14 KCA 30 - 115 %%

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B3 (2-4)Phoenix I.D.: BG43585

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

89% 2-Fluorophenol 05/13/14 KCA 25 - 121 %%91% Nitrobenzene-d5 05/13/14 KCA 23 - 120 %%84% Phenol-d5 05/13/14 KCA 24 - 113 %%108% Terphenyl-d14 05/13/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

SOIL DUPLICATE

Phoenix ID: BG43586

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

< 0.39Silver 0.39 05/15/14 LK SW6010mg/Kg0.396260Aluminum 39 05/14/14 LK SW6010mg/Kg7.71.3Arsenic 0.8 05/15/14 LK SW6010mg/Kg0.77

71.0Barium 0.8 05/15/14 LK SW6010mg/Kg0.390.46Beryllium 0.31 05/15/14 LK SW6010mg/Kg0.151500Calcium 39 05/14/14 LK SW6010mg/Kg35*0.18Cadmium 0.39 05/15/14 LK SW6010mg/Kg0.15B6.07Cobalt 0.39 05/15/14 LK SW6010mg/Kg0.3916.1Chromium 0.39 05/15/14 LK SW6010mg/Kg0.399.07Copper 0.39 05/15/14 LK SW6010mg/kg0.39

13600Iron 39 05/14/14 LK SW6010mg/Kg B39< 0.06Mercury 0.06 05/13/14 RS SW-7471mg/Kg0.042220Potassium 8 05/15/14 LK SW6010mg/Kg3.0N2220Magnesium 3.9 05/15/14 LK SW6010mg/Kg3.9459Manganese 3.9 05/14/14 LK SW6010mg/Kg3.9N152Sodium 8 05/15/14 LK SW6010mg/Kg3.3N17.1Nickel 0.39 05/15/14 LK SW6010mg/Kg0.395.8Lead 0.8 05/15/14 LK SW6010mg/Kg0.39

< 1.9Antimony 1.9 05/15/14 LK SW6010mg/Kg1.9< 1.5Selenium 1.5 05/15/14 LK SW6010mg/Kg1.3< 1.5Thallium 1.5 05/15/14 LK SW6010mg/Kg1.519.0Vanadium 0.4 05/15/14 LK SW6010mg/Kg0.3924.0Zinc 0.8 05/15/14 LK SW6010mg/Kg B0.3990Percent Solid 05/12/14 I E160.3%

CompletedSoil Extraction for PCB 05/12/14 BB/V SW3545CompletedSoil Extraction for Pesticide 05/12/14 BB SW3545CompletedSoil Extraction for SVOA 05/12/14 BJ/FV SW3545CompletedMercury Digestion 05/13/14 I/I SW7471

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SOIL DUPLICATEPhoenix I.D.: BG43586

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

CompletedTotal Metals Digest 05/12/14 CB/AG SW846 - 3050

CompletedField Extraction 05/09/14 SW5035

Polychlorinated BiphenylsNDPCB-1016 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1221 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1232 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1242 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1248 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1254 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1260 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1262 36 05/13/14 AW SW 8082ug/Kg36NDPCB-1268 36 05/13/14 AW SW 8082ug/Kg36

QA/QC Surrogates106% DCBP 05/13/14 AW 30 - 150 %%92% TCMX 05/13/14 AW 30 - 150 %%

Pesticides - SoilND4,4' -DDD 2.6 05/15/14 CE SW8081ug/Kg2.6ND4,4' -DDE 2.6 05/15/14 CE SW8081ug/Kg2.66.84,4' -DDT 2.6 05/15/14 CE SW8081ug/Kg2.6NDa-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDa-Chlordane 3.6 05/15/14 CE SW8081ug/Kg3.6NDAldrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDb-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDChlordane 22 05/15/14 CE SW8081ug/Kg22NDd-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDDieldrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDEndosulfan I 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndosulfan II 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndosulfan sulfate 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndrin 1.8 05/15/14 CE SW8081ug/Kg1.8NDEndrin aldehyde 3.6 05/15/14 CE SW8081ug/Kg3.6NDEndrin ketone 1.8 05/15/14 CE SW8081ug/Kg1.8NDg-BHC 1.8 05/15/14 CE SW8081ug/Kg1.8NDg-Chlordane 3.6 05/15/14 CE SW8081ug/Kg3.6NDHeptachlor 1.8 05/15/14 CE SW8081ug/Kg1.8NDHeptachlor epoxide 1.8 05/15/14 CE SW8081ug/Kg1.8NDMethoxychlor 7.3 05/15/14 CE SW8081ug/Kg7.3NDToxaphene 180 05/15/14 CE SW8081ug/Kg180

QA/QC Surrogates131% DCBP 05/15/14 CE 30 - 150 %%102% TCMX 05/15/14 CE 30 - 150 %%

VolatilesND1,1,1,2-Tetrachloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.90ND1,1,1-Trichloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,1,2,2-Tetrachloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,1,2-Trichloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.54ND1,1-Dichloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.1

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SOIL DUPLICATEPhoenix I.D.: BG43586

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND1,1-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2ND1,1-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,3-Trichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,2,4-Trichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1ND1,2,4-Trimethylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.79ND1,2-Dibromo-3-chloropropane 5.5 05/13/14 JLI SW8260ug/Kg1.5ND1,2-Dibromoethane 5.5 05/13/14 JLI SW8260ug/Kg1.5ND1,2-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.61ND1,2-Dichloroethane 5.5 05/13/14 JLI SW8260ug/Kg0.48ND1,2-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.78ND1,3,5-Trimethylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.73ND1,3-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.81ND1,3-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.58ND1,4-Dichlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.87ND2,2-Dichloropropane 5.5 05/13/14 JLI SW8260ug/Kg0.92ND2-Chlorotoluene 5.5 05/13/14 JLI SW8260ug/Kg0.88ND2-Hexanone 28 05/13/14 JLI SW8260ug/Kg2.5ND2-Isopropyltoluene 5.5 05/13/14 JLI SW8260ug/Kg 10.76ND4-Chlorotoluene 5.5 05/13/14 JLI SW8260ug/Kg0.64ND4-Methyl-2-pentanone 28 05/13/14 JLI SW8260ug/Kg1.3NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.5NDAcrylonitrile 11 05/13/14 JLI SW8260ug/Kg3.1NDBenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDBromobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.72NDBromochloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.80NDBromodichloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.68NDBromoform 5.5 05/13/14 JLI SW8260ug/Kg0.77NDBromomethane 5.5 05/13/14 JLI SW8260ug/Kg4.2NDCarbon Disulfide 5.5 05/13/14 JLI SW8260ug/Kg0.89NDCarbon tetrachloride 5.5 05/13/14 JLI SW8260ug/Kg0.64NDChlorobenzene 5.5 05/13/14 JLI SW8260ug/Kg0.81NDChloroethane 5.5 05/13/14 JLI SW8260ug/Kg1.3NDChloroform 5.5 05/13/14 JLI SW8260ug/Kg1.0NDChloromethane 5.5 05/13/14 JLI SW8260ug/Kg2.9NDcis-1,2-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDcis-1,3-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg0.59NDDibromochloromethane 5.5 05/13/14 JLI SW8260ug/Kg0.62NDDibromomethane 5.5 05/13/14 JLI SW8260ug/Kg0.69NDDichlorodifluoromethane 5.5 05/13/14 JLI SW8260ug/Kg1.5NDEthylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0NDHexachlorobutadiene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDIsopropylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDm&p-Xylene 5.5 05/13/14 JLI SW8260ug/Kg2.2NDMethyl Ethyl Ketone 33 05/13/14 JLI SW8260ug/Kg4.8NDMethyl t-butyl ether (MTBE) 11 05/13/14 JLI SW8260ug/Kg1.51.5Methylene chloride 5.5 05/13/14 JLI SW8260ug/Kg0.90JSNDNaphthalene 5.5 05/13/14 JLI SW8260ug/Kg1.5NDn-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0

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SOIL DUPLICATEPhoenix I.D.: BG43586

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

NDn-Propylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.99NDo-Xylene 5.5 05/13/14 JLI SW8260ug/Kg2.1NDp-Isopropyltoluene 5.5 05/13/14 JLI SW8260ug/Kg0.79NDsec-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg1.0NDStyrene 5.5 05/13/14 JLI SW8260ug/Kg1.6NDtert-Butylbenzene 5.5 05/13/14 JLI SW8260ug/Kg0.88NDTetrachloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTetrahydrofuran (THF) 11 05/13/14 JLI SW8260ug/Kg 15.0NDToluene 5.5 05/13/14 JLI SW8260ug/Kg0.87NDtrans-1,2-Dichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,3-Dichloropropene 5.5 05/13/14 JLI SW8260ug/Kg1.1NDtrans-1,4-dichloro-2-butene 11 05/13/14 JLI SW8260ug/Kg10NDTrichloroethene 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorofluoromethane 5.5 05/13/14 JLI SW8260ug/Kg1.2NDTrichlorotrifluoroethane 5.5 05/13/14 JLI SW8260ug/Kg0.86NDVinyl chloride 5.5 05/13/14 JLI SW8260ug/Kg1.8

QA/QC Surrogates109% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%94% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%103% Toluene-d8 05/13/14 JLI 84 - 138 %%

SemivolatilesND1,2,4,5-Tetrachlorobenzene 260 05/14/14 KCA SW 8270ug/Kg130ND1,2,4-Trichlorobenzene 260 05/14/14 KCA SW 8270ug/Kg110ND1,2-Dichlorobenzene 260 05/14/14 KCA SW 8270ug/Kg100ND1,2-Diphenylhydrazine 260 05/14/14 KCA SW 8270ug/Kg120ND1,3-Dichlorobenzene 260 05/14/14 KCA SW 8270ug/Kg110ND1,4-Dichlorobenzene 260 05/14/14 KCA SW 8270ug/Kg110ND2,4,5-Trichlorophenol 260 05/14/14 KCA SW 8270ug/Kg200ND2,4,6-Trichlorophenol 260 05/14/14 KCA SW 8270ug/Kg120ND2,4-Dichlorophenol 260 05/14/14 KCA SW 8270ug/Kg130ND2,4-Dimethylphenol 260 05/14/14 KCA SW 8270ug/Kg90ND2,4-Dinitrophenol 1800 05/14/14 KCA SW 8270ug/Kg260ND2,4-Dinitrotoluene 260 05/14/14 KCA SW 8270ug/Kg140ND2,6-Dinitrotoluene 260 05/14/14 KCA SW 8270ug/Kg120ND2-Chloronaphthalene 260 05/14/14 KCA SW 8270ug/Kg100ND2-Chlorophenol 260 05/14/14 KCA SW 8270ug/Kg100ND2-Methylnaphthalene 260 05/14/14 KCA SW 8270ug/Kg110ND2-Methylphenol (o-cresol) 260 05/14/14 KCA SW 8270ug/Kg170ND2-Nitroaniline 1800 05/14/14 KCA SW 8270ug/Kg370ND2-Nitrophenol 260 05/14/14 KCA SW 8270ug/Kg230ND3&4-Methylphenol (m&p-cresol) 260 05/14/14 KCA SW 8270ug/Kg 1140ND3,3'-Dichlorobenzidine 730 05/14/14 KCA SW 8270ug/Kg170ND3-Nitroaniline 1800 05/14/14 KCA SW 8270ug/Kg790ND4,6-Dinitro-2-methylphenol 1800 05/14/14 KCA SW 8270ug/Kg390ND4-Bromophenyl phenyl ether 260 05/14/14 KCA SW 8270ug/Kg110ND4-Chloro-3-methylphenol 260 05/14/14 KCA SW 8270ug/Kg130ND4-Chloroaniline 730 05/14/14 KCA SW 8270ug/Kg170ND4-Chlorophenyl phenyl ether 260 05/14/14 KCA SW 8270ug/Kg120

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SOIL DUPLICATEPhoenix I.D.: BG43586

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Nitroaniline 1800 05/14/14 KCA SW 8270ug/Kg120ND4-Nitrophenol 1800 05/14/14 KCA SW 8270ug/Kg160NDAcenaphthene 260 05/14/14 KCA SW 8270ug/Kg110NDAcenaphthylene 260 05/14/14 KCA SW 8270ug/Kg100NDAcetophenone 260 05/14/14 KCA SW 8270ug/Kg110NDAniline 1800 05/14/14 KCA SW 8270ug/Kg740NDAnthracene 260 05/14/14 KCA SW 8270ug/Kg120NDBenz(a)anthracene 260 05/14/14 KCA SW 8270ug/Kg120NDBenzidine 730 05/14/14 KCA SW 8270ug/Kg210NDBenzo(a)pyrene 260 05/14/14 KCA SW 8270ug/Kg120NDBenzo(b)fluoranthene 260 05/14/14 KCA SW 8270ug/Kg120NDBenzo(ghi)perylene 260 05/14/14 KCA SW 8270ug/Kg120NDBenzo(k)fluoranthene 260 05/14/14 KCA SW 8270ug/Kg120NDBenzoic acid 1800 05/14/14 KCA SW 8270ug/Kg 1730NDBenzyl butyl phthalate 260 05/14/14 KCA SW 8270ug/Kg94NDBis(2-chloroethoxy)methane 260 05/14/14 KCA SW 8270ug/Kg100NDBis(2-chloroethyl)ether 260 05/14/14 KCA SW 8270ug/Kg98NDBis(2-chloroisopropyl)ether 260 05/14/14 KCA SW 8270ug/Kg 1100NDBis(2-ethylhexyl)phthalate 260 05/14/14 KCA SW 8270ug/Kg110NDCarbazole 1800 05/14/14 KCA SW 8270ug/Kg280NDChrysene 260 05/14/14 KCA SW 8270ug/Kg120NDDibenz(a,h)anthracene 260 05/14/14 KCA SW 8270ug/Kg120NDDibenzofuran 260 05/14/14 KCA SW 8270ug/Kg110NDDiethyl phthalate 260 05/14/14 KCA SW 8270ug/Kg120NDDimethylphthalate 260 05/14/14 KCA SW 8270ug/Kg110NDDi-n-butylphthalate 260 05/14/14 KCA SW 8270ug/Kg97NDDi-n-octylphthalate 260 05/14/14 KCA SW 8270ug/Kg94NDFluoranthene 260 05/14/14 KCA SW 8270ug/Kg120NDFluorene 260 05/14/14 KCA SW 8270ug/Kg120NDHexachlorobenzene 260 05/14/14 KCA SW 8270ug/Kg110NDHexachlorobutadiene 260 05/14/14 KCA SW 8270ug/Kg130NDHexachlorocyclopentadiene 260 05/14/14 KCA SW 8270ug/Kg110NDHexachloroethane 260 05/14/14 KCA SW 8270ug/Kg110NDIndeno(1,2,3-cd)pyrene 260 05/14/14 KCA SW 8270ug/Kg120NDIsophorone 260 05/14/14 KCA SW 8270ug/Kg100NDNaphthalene 260 05/14/14 KCA SW 8270ug/Kg110NDNitrobenzene 260 05/14/14 KCA SW 8270ug/Kg130NDN-Nitrosodimethylamine 260 05/14/14 KCA SW 8270ug/Kg100NDN-Nitrosodi-n-propylamine 260 05/14/14 KCA SW 8270ug/Kg120NDN-Nitrosodiphenylamine 260 05/14/14 KCA SW 8270ug/Kg140NDPentachloronitrobenzene 260 05/14/14 KCA SW 8270ug/Kg140NDPentachlorophenol 260 05/14/14 KCA SW 8270ug/Kg140NDPhenanthrene 260 05/14/14 KCA SW 8270ug/Kg100NDPhenol 260 05/14/14 KCA SW 8270ug/Kg120NDPyrene 260 05/14/14 KCA SW 8270ug/Kg130NDPyridine 260 05/14/14 KCA SW 8270ug/Kg90

QA/QC Surrogates116% 2,4,6-Tribromophenol 05/14/14 KCA 19 - 122 %%76% 2-Fluorobiphenyl 05/14/14 KCA 30 - 115 %%

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SOIL DUPLICATEPhoenix I.D.: BG43586

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

88% 2-Fluorophenol 05/14/14 KCA 25 - 121 %%84% Nitrobenzene-d5 05/14/14 KCA 23 - 120 %%89% Phenol-d5 05/14/14 KCA 24 - 113 %%98% Terphenyl-d14 05/14/14 KCA 18 - 137 %%

Comments:

Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine.

Please be advised that the NY unrestricted soil criteria for chromium is based on hexavalent chromium and trivalent chromium.

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.B = Present in blank, no bias suspected.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

HI TRIP BLANK

Phoenix ID: BG43587

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

100Percent Solid 1 05/09/14 E160.3%

VolatilesND1,1,1,2-Tetrachloroethane 250 05/13/14 JLI SW8260ug/Kg41ND1,1,1-Trichloroethane 250 05/13/14 JLI SW8260ug/Kg50ND1,1,2,2-Tetrachloroethane 250 05/13/14 JLI SW8260ug/Kg36ND1,1,2-Trichloroethane 250 05/13/14 JLI SW8260ug/Kg25ND1,1-Dichloroethane 250 05/13/14 JLI SW8260ug/Kg50ND1,1-Dichloroethene 250 05/13/14 JLI SW8260ug/Kg55ND1,1-Dichloropropene 250 05/13/14 JLI SW8260ug/Kg49ND1,2,3-Trichlorobenzene 250 05/13/14 JLI SW8260ug/Kg50ND1,2,3-Trichloropropane 250 05/13/14 JLI SW8260ug/Kg36ND1,2,4-Trichlorobenzene 250 05/13/14 JLI SW8260ug/Kg50ND1,2,4-Trimethylbenzene 250 05/13/14 JLI SW8260ug/Kg36ND1,2-Dibromo-3-chloropropane 250 05/13/14 JLI SW8260ug/Kg67ND1,2-Dibromoethane 250 05/13/14 JLI SW8260ug/Kg67ND1,2-Dichlorobenzene 250 05/13/14 JLI SW8260ug/Kg28ND1,2-Dichloroethane 250 05/13/14 JLI SW8260ug/Kg22ND1,2-Dichloropropane 250 05/13/14 JLI SW8260ug/Kg36ND1,3,5-Trimethylbenzene 250 05/13/14 JLI SW8260ug/Kg33ND1,3-Dichlorobenzene 250 05/13/14 JLI SW8260ug/Kg37ND1,3-Dichloropropane 250 05/13/14 JLI SW8260ug/Kg27ND1,4-Dichlorobenzene 250 05/13/14 JLI SW8260ug/Kg40ND2,2-Dichloropropane 250 05/13/14 JLI SW8260ug/Kg42ND2-Chlorotoluene 250 05/13/14 JLI SW8260ug/Kg40ND2-Hexanone 1300 05/13/14 JLI SW8260ug/Kg110ND2-Isopropyltoluene 250 05/13/14 JLI SW8260ug/Kg 135ND4-Chlorotoluene 250 05/13/14 JLI SW8260ug/Kg29

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HI TRIP BLANKPhoenix I.D.: BG43587

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Methyl-2-pentanone 1300 05/13/14 JLI SW8260ug/Kg60NDAcetone 2500 05/13/14 JLI SW8260ug/Kg250NDAcrylonitrile 500 05/13/14 JLI SW8260ug/Kg140NDBenzene 250 05/13/14 JLI SW8260ug/Kg50NDBromobenzene 250 05/13/14 JLI SW8260ug/Kg33NDBromochloromethane 250 05/13/14 JLI SW8260ug/Kg37NDBromodichloromethane 250 05/13/14 JLI SW8260ug/Kg31NDBromoform 250 05/13/14 JLI SW8260ug/Kg35NDBromomethane 250 05/13/14 JLI SW8260ug/Kg190NDCarbon Disulfide 250 05/13/14 JLI SW8260ug/Kg41NDCarbon tetrachloride 250 05/13/14 JLI SW8260ug/Kg29NDChlorobenzene 250 05/13/14 JLI SW8260ug/Kg37NDChloroethane 250 05/13/14 JLI SW8260ug/Kg59NDChloroform 250 05/13/14 JLI SW8260ug/Kg46NDChloromethane 250 05/13/14 JLI SW8260ug/Kg130NDcis-1,2-Dichloroethene 250 05/13/14 JLI SW8260ug/Kg55NDcis-1,3-Dichloropropene 250 05/13/14 JLI SW8260ug/Kg27NDDibromochloromethane 250 05/13/14 JLI SW8260ug/Kg28NDDibromomethane 250 05/13/14 JLI SW8260ug/Kg32NDDichlorodifluoromethane 250 05/13/14 JLI SW8260ug/Kg67NDEthylbenzene 250 05/13/14 JLI SW8260ug/Kg46NDHexachlorobutadiene 250 05/13/14 JLI SW8260ug/Kg53NDIsopropylbenzene 250 05/13/14 JLI SW8260ug/Kg48NDm&p-Xylene 250 05/13/14 JLI SW8260ug/Kg99NDMethyl Ethyl Ketone 1500 05/13/14 JLI SW8260ug/Kg220NDMethyl t-butyl ether (MTBE) 500 05/13/14 JLI SW8260ug/Kg6972Methylene chloride 250 05/13/14 JLI SW8260ug/Kg41JSNDNaphthalene 250 05/13/14 JLI SW8260ug/Kg67NDn-Butylbenzene 250 05/13/14 JLI SW8260ug/Kg46NDn-Propylbenzene 250 05/13/14 JLI SW8260ug/Kg45NDo-Xylene 250 05/13/14 JLI SW8260ug/Kg96NDp-Isopropyltoluene 250 05/13/14 JLI SW8260ug/Kg36NDsec-Butylbenzene 250 05/13/14 JLI SW8260ug/Kg47NDStyrene 250 05/13/14 JLI SW8260ug/Kg72NDtert-Butylbenzene 250 05/13/14 JLI SW8260ug/Kg40NDTetrachloroethene 250 05/13/14 JLI SW8260ug/Kg53NDTetrahydrofuran (THF) 500 05/13/14 JLI SW8260ug/Kg 1230NDToluene 250 05/13/14 JLI SW8260ug/Kg40NDtrans-1,2-Dichloroethene 250 05/13/14 JLI SW8260ug/Kg50NDtrans-1,3-Dichloropropene 250 05/13/14 JLI SW8260ug/Kg51NDtrans-1,4-dichloro-2-butene 500 05/13/14 JLI SW8260ug/Kg460NDTrichloroethene 250 05/13/14 JLI SW8260ug/Kg53NDTrichlorofluoromethane 250 05/13/14 JLI SW8260ug/Kg56NDTrichlorotrifluoroethane 250 05/13/14 JLI SW8260ug/Kg39NDVinyl chloride 250 05/13/14 JLI SW8260ug/Kg81

QA/QC Surrogates108% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%98% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%93% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%

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HI TRIP BLANKPhoenix I.D.: BG43587

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

103% Toluene-d8 05/13/14 JLI 84 - 138 %%

Comments:

TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%

This sample was not collected in accordance with EPA method 5035. NELAC requires the laboratory to qualify the volatile soil data as biased low.

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

Page 45 of 48 Ver 1

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

SOLIDEBC72 Hour

05/09/14SWsee "By" below

CU

Laboratory Data

LOW TRIP BLANK

Phoenix ID: BG43588

05/12/140:00

16:02

Parameter ResultRL/PQL Units Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43580

Client ID:Project ID: 42 LISPENARD ST NY

LOD/MDL

100Percent Solid 1 05/09/14 E160.3%CompletedField Extraction 05/09/14 SW5035

VolatilesND1,1,1,2-Tetrachloroethane 5.0 05/13/14 JLI SW8260ug/Kg0.82ND1,1,1-Trichloroethane 5.0 05/13/14 JLI SW8260ug/Kg1.0ND1,1,2,2-Tetrachloroethane 5.0 05/13/14 JLI SW8260ug/Kg0.71ND1,1,2-Trichloroethane 5.0 05/13/14 JLI SW8260ug/Kg0.49ND1,1-Dichloroethane 5.0 05/13/14 JLI SW8260ug/Kg0.99ND1,1-Dichloroethene 5.0 05/13/14 JLI SW8260ug/Kg1.1ND1,1-Dichloropropene 5.0 05/13/14 JLI SW8260ug/Kg0.97ND1,2,3-Trichlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg1.0ND1,2,3-Trichloropropane 5.0 05/13/14 JLI SW8260ug/Kg0.71ND1,2,4-Trichlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg1.0ND1,2,4-Trimethylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.72ND1,2-Dibromo-3-chloropropane 5.0 05/13/14 JLI SW8260ug/Kg1.3ND1,2-Dibromoethane 5.0 05/13/14 JLI SW8260ug/Kg1.3ND1,2-Dichlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg0.55ND1,2-Dichloroethane 5.0 05/13/14 JLI SW8260ug/Kg0.44ND1,2-Dichloropropane 5.0 05/13/14 JLI SW8260ug/Kg0.71ND1,3,5-Trimethylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.66ND1,3-Dichlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg0.74ND1,3-Dichloropropane 5.0 05/13/14 JLI SW8260ug/Kg0.53ND1,4-Dichlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg0.79ND2,2-Dichloropropane 5.0 05/13/14 JLI SW8260ug/Kg0.84ND2-Chlorotoluene 5.0 05/13/14 JLI SW8260ug/Kg0.80ND2-Hexanone 25 05/13/14 JLI SW8260ug/Kg2.3ND2-Isopropyltoluene 5.0 05/13/14 JLI SW8260ug/Kg 10.69

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LOW TRIP BLANKPhoenix I.D.: BG43588

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

ND4-Chlorotoluene 5.0 05/13/14 JLI SW8260ug/Kg0.58ND4-Methyl-2-pentanone 25 05/13/14 JLI SW8260ug/Kg1.2NDAcetone 50 05/13/14 JLI SW8260ug/Kg5.0NDAcrylonitrile 10 05/13/14 JLI SW8260ug/Kg2.8NDBenzene 5.0 05/13/14 JLI SW8260ug/Kg0.99NDBromobenzene 5.0 05/13/14 JLI SW8260ug/Kg0.65NDBromochloromethane 5.0 05/13/14 JLI SW8260ug/Kg0.73NDBromodichloromethane 5.0 05/13/14 JLI SW8260ug/Kg0.62NDBromoform 5.0 05/13/14 JLI SW8260ug/Kg0.70NDBromomethane 5.0 05/13/14 JLI SW8260ug/Kg3.9NDCarbon Disulfide 5.0 05/13/14 JLI SW8260ug/Kg0.81NDCarbon tetrachloride 5.0 05/13/14 JLI SW8260ug/Kg0.58NDChlorobenzene 5.0 05/13/14 JLI SW8260ug/Kg0.74NDChloroethane 5.0 05/13/14 JLI SW8260ug/Kg1.2NDChloroform 5.0 05/13/14 JLI SW8260ug/Kg0.91NDChloromethane 5.0 05/13/14 JLI SW8260ug/Kg2.6NDcis-1,2-Dichloroethene 5.0 05/13/14 JLI SW8260ug/Kg1.1NDcis-1,3-Dichloropropene 5.0 05/13/14 JLI SW8260ug/Kg0.54NDDibromochloromethane 5.0 05/13/14 JLI SW8260ug/Kg0.56NDDibromomethane 5.0 05/13/14 JLI SW8260ug/Kg0.63NDDichlorodifluoromethane 5.0 05/13/14 JLI SW8260ug/Kg1.3NDEthylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.91NDHexachlorobutadiene 5.0 05/13/14 JLI SW8260ug/Kg1.1NDIsopropylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.96NDm&p-Xylene 5.0 05/13/14 JLI SW8260ug/Kg2.0NDMethyl Ethyl Ketone 30 05/13/14 JLI SW8260ug/Kg4.3NDMethyl t-butyl ether (MTBE) 10 05/13/14 JLI SW8260ug/Kg1.41.9Methylene chloride 5.0 05/13/14 JLI SW8260ug/Kg0.82JSNDNaphthalene 5.0 05/13/14 JLI SW8260ug/Kg1.3NDn-Butylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.91NDn-Propylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.90NDo-Xylene 5.0 05/13/14 JLI SW8260ug/Kg1.9NDp-Isopropyltoluene 5.0 05/13/14 JLI SW8260ug/Kg0.72NDsec-Butylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.94NDStyrene 5.0 05/13/14 JLI SW8260ug/Kg1.4NDtert-Butylbenzene 5.0 05/13/14 JLI SW8260ug/Kg0.80NDTetrachloroethene 5.0 05/13/14 JLI SW8260ug/Kg1.1NDTetrahydrofuran (THF) 10 05/13/14 JLI SW8260ug/Kg 14.5NDToluene 5.0 05/13/14 JLI SW8260ug/Kg0.79NDtrans-1,2-Dichloroethene 5.0 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,3-Dichloropropene 5.0 05/13/14 JLI SW8260ug/Kg1.0NDtrans-1,4-dichloro-2-butene 10 05/13/14 JLI SW8260ug/Kg9.3NDTrichloroethene 5.0 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorofluoromethane 5.0 05/13/14 JLI SW8260ug/Kg1.1NDTrichlorotrifluoroethane 5.0 05/13/14 JLI SW8260ug/Kg0.78NDVinyl chloride 5.0 05/13/14 JLI SW8260ug/Kg1.6

QA/QC Surrogates106% 1,2-dichlorobenzene-d4 05/13/14 JLI 70 - 121 %%102% Bromofluorobenzene 05/13/14 JLI 59 - 113 %%

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LOW TRIP BLANKPhoenix I.D.: BG43588

Client ID:42 LISPENARD ST NYProject ID:

Parameter ResultRL/PQL Units Date/Time By Reference

LOD/MDL

95% Dibromofluoromethane 05/13/14 JLI 70 - 130 %%105% Toluene-d8 05/13/14 JLI 84 - 138 %%

Comments:

TRIP BLANK INCLUDED. %SOLIDS ASSUMED 100%

All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments.

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level LOD=Limit of Detection MDL=Method Detection Limit

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Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 1 of 1

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GBG43580 - EBCCriteria: NY: 375, 375RRS, 375RS

RLCriteria

State: NY

MN-SM Manganese 16001830 32 mg/KgBG43581 NY / 375-6.8 Metals / Unrestricted Use Soil 1600

$PESTSMDPR 4,4' -DDT 3.35.0 2.6 ug/KgBG43582 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$PESTSMDPR 4,4' -DDT 3.36.8 2.6 ug/KgBG43586 NY / 375-6.8 PCBs/Pesticides / Unrestricted Use Soil 3.3

$8260-SMDPR Vinyl chloride 210ND 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Residential 210$8260-SMDPR Vinyl chloride 20ND 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20$8260-SMDPR trans-1,2-Dichloroethene 190ND 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 190$8260-SMDPR Methylene chloride 5072 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR Methyl Ethyl Ketone 120ND 1500 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 120$8260-SMDPR Benzene 60ND 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 60$8260-SMDPR Acetone 50ND 2500 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 50$8260-SMDPR 1,2-Dichloroethane 20ND 250 ug/KgBG43587 NY / 375-6.8 Volatiles / Unrestricted Use Soil 20

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

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NY Temperature NarrationMay 16, 2014

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GBG43580

The samples in this delivery group were received at 4°C.(Note acceptance criteria is above freezing up to 6°C)

Page 1 of 1

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BG43589 - BG43590

Friday, May 16, 2014

Sample ID#s:

Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Project ID: 42 LISPENARD ST NY

Sincerely yours,

Laboratory DirectorPhyllis Shiller

If you have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext. 200.

NELAC - #NY11301CT Lab Registration #PH-0618MA Lab Registration #MA-CT-007ME Lab Registration #CT-007NH Lab Registration #213693-A,B

NJ Lab Registration #CT-003NY Lab Registration #11301PA Lab Registration #68-03530RI Lab Registration #63VT Lab Registration #VT11301

This laboratory is in compliance with the NELAC requirements of procedures used except where indicated.

This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory.

A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original.

587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040Telephone (860) 645-1102 Fax (860) 645-0823

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

AIREBC72 Hour

05/09/14SWsee "By" below

SUNNY

Laboratory Data

SS-1

Phoenix ID: BG43589

05/12/1413:0416:02

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43589

Client ID:Project ID: 42 LISPENARD ST NY

ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 05/13/14 KCA TO15ND 11.001.601,1,1-Trichloroethane 0.183 05/13/14 KCA TO158.72 1.00ND1,1,2,2-Tetrachloroethane 0.146 05/13/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 05/13/14 KCA TO15ND 1.001.381,1-Dichloroethane 0.247 05/13/14 KCA TO155.58 1.001.471,1-Dichloroethene 0.252 05/13/14 KCA TO155.82 1.00ND1,2,4-Trichlorobenzene 0.135 05/13/14 KCA TO15ND 1.00

0.3501,2,4-Trimethylbenzene 0.204 05/13/14 KCA TO151.72 1.00ND1,2-Dibromoethane(EDB) 0.130 05/13/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 05/13/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 05/13/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 05/13/14 KCA TO15ND 1.00ND1,3,5-Trimethylbenzene 0.204 05/13/14 KCA TO15ND 1.00ND1,3-Butadiene 0.452 05/13/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 05/13/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 05/13/14 KCA TO15ND 11.00ND4-Ethyltoluene 0.204 05/13/14 KCA TO15ND 11.00ND4-Isopropyltoluene 0.182 05/13/14 KCA TO15ND 11.00

0.4604-Methyl-2-pentanone(MIBK) 0.244 05/13/14 KCA TO151.88 1.0041.0Acetone 0.421 05/13/14 KCA TO1597.3 1.00NDAcrylonitrile 0.461 05/13/14 KCA TO15ND 1.00

0.890Benzene 0.313 05/13/14 KCA TO152.84 1.00NDBenzyl chloride 0.193 05/13/14 KCA TO15ND 1.00

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SS-1Phoenix I.D.: BG43589

Client ID:42 LISPENARD ST NYProject ID:

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

ug/m3RL

NDBromodichloromethane 0.149 05/13/14 KCA TO15ND 1.00NDBromoform 0.097 05/13/14 KCA TO15ND 1.00NDBromomethane 0.258 05/13/14 KCA TO15ND 1.001.26Carbon Disulfide 0.321 05/13/14 KCA TO153.92 1.000.100Carbon Tetrachloride 0.040 05/13/14 KCA TO150.629 0.25NDChlorobenzene 0.217 05/13/14 KCA TO15ND 1.00NDChloroethane 0.379 05/13/14 KCA TO15ND 1.001.23Chloroform 0.205 05/13/14 KCA TO156.00 1.00NDChloromethane 0.484 05/13/14 KCA TO15ND 1.0014.3Cis-1,2-Dichloroethene 0.252 05/13/14 KCA TO1556.7 1.00NDcis-1,3-Dichloropropene 0.220 05/13/14 KCA TO15ND 1.00

0.380Cyclohexane 0.291 05/13/14 KCA TO151.31 1.00NDDibromochloromethane 0.117 05/13/14 KCA TO15ND 1.00

0.380Dichlorodifluoromethane 0.202 05/13/14 KCA TO151.88 1.0024.1Ethanol 0.531 05/13/14 KCA TO1545.4 11.000.680Ethyl acetate 0.278 05/13/14 KCA TO152.45 11.000.890Ethylbenzene 0.230 05/13/14 KCA TO153.86 1.000.820Heptane 0.244 05/13/14 KCA TO153.36 1.00NDHexachlorobutadiene 0.094 05/13/14 KCA TO15ND 1.001.28Hexane 0.284 05/13/14 KCA TO154.51 1.001.06Isopropylalcohol 0.407 05/13/14 KCA TO152.60 1.00NDIsopropylbenzene 0.204 05/13/14 KCA TO15ND 1.002.60m,p-Xylene 0.230 05/13/14 KCA TO1511.3 1.003.48Methyl Ethyl Ketone 0.339 05/13/14 KCA TO1510.2 1.00NDMethyl tert-butyl ether(MTBE) 0.278 05/13/14 KCA TO15ND 1.00

0.670Methylene Chloride 0.288 05/13/14 KCA TO152.32 1.00NDn-Butylbenzene 0.182 05/13/14 KCA TO15ND 11.00

0.940o-Xylene 0.230 05/13/14 KCA TO154.08 1.001.67Propylene 0.581 05/13/14 KCA TO152.87 11.00NDsec-Butylbenzene 0.182 05/13/14 KCA TO15ND 11.00

0.940Styrene 0.235 05/13/14 KCA TO154.00 1.002.53Tetrachloroethene 0.037 05/13/14 KCA TO1517.1 0.250.390Tetrahydrofuran 0.339 05/13/14 KCA TO151.15 11.004.20Toluene 0.266 05/13/14 KCA TO1515.8 1.00NDTrans-1,2-Dichloroethene 0.252 05/13/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 05/13/14 KCA TO15ND 1.0079.0Trichloroethene 0.047 05/13/14 KCA TO15424 0.250.300Trichlorofluoromethane 0.178 05/13/14 KCA TO151.68 1.00NDTrichlorotrifluoroethane 0.130 05/13/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 05/13/14 KCA TO15ND 0.25

QA/QC Surrogates105% Bromofluorobenzene % 05/13/14 KCA TO15105 %

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SS-1Phoenix I.D.: BG43589

Client ID:42 LISPENARD ST NYProject ID:

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

ug/m3RL

Comments:

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level

Page 3 of 6 Ver 1

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Sample Information Custody InformationMatrix:Location Code:Rush Request:P.O.#:

Collected by:Received by:Analyzed by:

AIREBC72 Hour

05/09/14SWsee "By" below

SUNNY

Laboratory Data

SS-2

Phoenix ID: BG43590

05/12/1413:0516:02

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

FOR: Attn: Mr. Charles B. Sosik, P.G.Environmental Business Consultants1808 Middle Country RdRidge NY 11961-2406

Analysis ReportMay 16, 2014

Date Time

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG ID: GBG43589

Client ID:Project ID: 42 LISPENARD ST NY

ug/m3RL

Volatiles (TO15)ND1,1,1,2-Tetrachloroethane 0.146 05/13/14 KCA TO15ND 11.00ND1,1,1-Trichloroethane 0.183 05/13/14 KCA TO15ND 1.00ND1,1,2,2-Tetrachloroethane 0.146 05/13/14 KCA TO15ND 1.00ND1,1,2-Trichloroethane 0.183 05/13/14 KCA TO15ND 1.00ND1,1-Dichloroethane 0.247 05/13/14 KCA TO15ND 1.00ND1,1-Dichloroethene 0.252 05/13/14 KCA TO15ND 1.00ND1,2,4-Trichlorobenzene 0.135 05/13/14 KCA TO15ND 1.00

0.8101,2,4-Trimethylbenzene 0.204 05/13/14 KCA TO153.98 1.00ND1,2-Dibromoethane(EDB) 0.130 05/13/14 KCA TO15ND 1.00ND1,2-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,2-Dichloroethane 0.247 05/13/14 KCA TO15ND 1.00ND1,2-dichloropropane 0.216 05/13/14 KCA TO15ND 1.00ND1,2-Dichlorotetrafluoroethane 0.143 05/13/14 KCA TO15ND 1.00

0.9501,3,5-Trimethylbenzene 0.204 05/13/14 KCA TO154.67 1.00ND1,3-Butadiene 0.452 05/13/14 KCA TO15ND 1.00ND1,3-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,4-Dichlorobenzene 0.166 05/13/14 KCA TO15ND 1.00ND1,4-Dioxane 0.278 05/13/14 KCA TO15ND 1.00ND2-Hexanone(MBK) 0.244 05/13/14 KCA TO15ND 11.00

0.2904-Ethyltoluene 0.204 05/13/14 KCA TO151.42 11.00ND4-Isopropyltoluene 0.182 05/13/14 KCA TO15ND 11.00

0.6204-Methyl-2-pentanone(MIBK) 0.244 05/13/14 KCA TO152.54 1.0081.8Acetone 0.421 05/13/14 KCA TO15194 1.00NDAcrylonitrile 0.461 05/13/14 KCA TO15ND 1.002.58Benzene 0.313 05/13/14 KCA TO158.24 1.000.460Benzyl chloride 0.193 05/13/14 KCA TO152.38 1.00

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SS-2Phoenix I.D.: BG43590

Client ID:42 LISPENARD ST NYProject ID:

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

ug/m3RL

NDBromodichloromethane 0.149 05/13/14 KCA TO15ND 1.00NDBromoform 0.097 05/13/14 KCA TO15ND 1.00NDBromomethane 0.258 05/13/14 KCA TO15ND 1.001.13Carbon Disulfide 0.321 05/13/14 KCA TO153.52 1.000.090Carbon Tetrachloride 0.040 05/13/14 KCA TO150.566 0.25NDChlorobenzene 0.217 05/13/14 KCA TO15ND 1.00NDChloroethane 0.379 05/13/14 KCA TO15ND 1.00

0.820Chloroform 0.205 05/13/14 KCA TO154.00 1.00NDChloromethane 0.484 05/13/14 KCA TO15ND 1.00NDCis-1,2-Dichloroethene 0.252 05/13/14 KCA TO15ND 1.00NDcis-1,3-Dichloropropene 0.220 05/13/14 KCA TO15ND 1.00

0.880Cyclohexane 0.291 05/13/14 KCA TO153.03 1.00NDDibromochloromethane 0.117 05/13/14 KCA TO15ND 1.00

0.480Dichlorodifluoromethane 0.202 05/13/14 KCA TO152.37 1.0022.2Ethanol 0.531 05/13/14 KCA TO1541.8 11.001.22Ethyl acetate 0.278 05/13/14 KCA TO154.39 11.001.06Ethylbenzene 0.230 05/13/14 KCA TO154.60 1.004.69Heptane 0.244 05/13/14 KCA TO1519.2 1.00NDHexachlorobutadiene 0.094 05/13/14 KCA TO15ND 1.003.13Hexane 0.284 05/13/14 KCA TO1511.0 1.001.95Isopropylalcohol 0.407 05/13/14 KCA TO154.79 1.000.650Isopropylbenzene 0.204 05/13/14 KCA TO153.19 1.003.29m,p-Xylene 0.230 05/13/14 KCA TO1514.3 1.006.26Methyl Ethyl Ketone 0.339 05/13/14 KCA TO1518.4 1.00NDMethyl tert-butyl ether(MTBE) 0.278 05/13/14 KCA TO15ND 1.00

0.730Methylene Chloride 0.288 05/13/14 KCA TO152.53 1.00NDn-Butylbenzene 0.182 05/13/14 KCA TO15ND 11.001.51o-Xylene 0.230 05/13/14 KCA TO156.55 1.006.89Propylene 0.581 05/13/14 KCA TO1511.8 11.000.430sec-Butylbenzene 0.182 05/13/14 KCA TO152.36 11.000.340Styrene 0.235 05/13/14 KCA TO151.45 1.000.620Tetrachloroethene 0.037 05/13/14 KCA TO154.20 0.250.750Tetrahydrofuran 0.339 05/13/14 KCA TO152.21 11.0011.5Toluene 0.266 05/13/14 KCA TO1543.3 1.00NDTrans-1,2-Dichloroethene 0.252 05/13/14 KCA TO15ND 1.00NDtrans-1,3-Dichloropropene 0.220 05/13/14 KCA TO15ND 1.001.64Trichloroethene 0.047 05/13/14 KCA TO158.81 0.250.260Trichlorofluoromethane 0.178 05/13/14 KCA TO151.46 1.00NDTrichlorotrifluoroethane 0.130 05/13/14 KCA TO15ND 1.00NDVinyl Chloride 0.098 05/13/14 KCA TO15ND 0.25

QA/QC SurrogatesInterference% Bromofluorobenzene % 05/13/14 KCA TO15Interference %

Page 5 of 6 Ver 1

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SS-2Phoenix I.D.: BG43590

Client ID:42 LISPENARD ST NYProject ID:

Parameterppbv

ResultppbvRL

ug/m3Result Date/Time By Reference

ug/m3RL

Comments:

Phyllis Shiller, Laboratory DirectorMay 16, 2014

1 = This parameter is not certified by NY NELAC for this matrix. NY NELAC does not offer certification for all parameters at this time.

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.This report must not be reproduced except in full as defined by the attached chain of custody.

Reviewed and Released by: Bobbi Aloisa, Vice President

RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quanitation) ND=Not Detected BRL=Below Reporting Level

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QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

QA/QC ReportMay 16, 2014

587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823

Environmental Laboratories, Inc.

SDG I.D.: GBG43589

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

QA/QC Batch 274353, QC Sample No: BG43589 (BG43589, BG43590)

VolatilesND ND1,1,1,2-Tetrachloroethane ND NC104 ND ND 70 - 130 20ND

1.60 1.601,1,1-Trichloroethane ND 0.0110 8.72 8.72 70 - 130 20ND

ND ND1,1,2,2-Tetrachloroethane ND NC87 ND ND 70 - 130 20ND

ND ND1,1,2-Trichloroethane ND NC96 ND ND 70 - 130 20ND

1.38 1.331,1-Dichloroethane ND 3.799 5.58 5.38 70 - 130 20ND

1.47 1.431,1-Dichloroethene ND 2.894 5.82 5.67 70 - 130 20ND

ND ND1,2,4-Trichlorobenzene ND NC109 ND ND 70 - 130 20ND

0.350 0.3401,2,4-Trimethylbenzene ND 2.989 1.72 1.67 70 - 130 20ND

ND ND1,2-Dibromoethane(EDB) ND NC99 ND ND 70 - 130 20ND

ND ND1,2-Dichlorobenzene ND NC95 ND ND 70 - 130 20ND

ND ND1,2-Dichloroethane ND NC102 ND ND 70 - 130 20ND

ND ND1,2-dichloropropane ND NC95 ND ND 70 - 130 20ND

ND ND1,2-Dichlorotetrafluoroethane ND NC109 ND ND 70 - 130 20ND

ND ND1,3,5-Trimethylbenzene ND NC88 ND ND 70 - 130 20ND

ND ND1,3-Butadiene ND NC97 ND ND 70 - 130 20ND

ND ND1,3-Dichlorobenzene ND NC93 ND ND 70 - 130 20ND

ND ND1,4-Dichlorobenzene ND NC99 ND ND 70 - 130 20ND

ND ND1,4-Dioxane ND NC98 ND ND 70 - 130 20ND

ND ND2-Hexanone(MBK) ND NC97 ND ND 70 - 130 20ND

ND ND4-Ethyltoluene ND NC91 ND ND 70 - 130 20ND

ND ND4-Isopropyltoluene ND NC88 ND ND 70 - 130 20ND

0.460 0.4404-Methyl-2-pentanone(MIBK) ND 4.494 1.88 1.80 70 - 130 20ND

41.0 38.1Acetone ND 7.394 97.3 90.4 70 - 130 20ND

ND NDAcrylonitrile ND NC105 ND ND 70 - 130 20ND

0.890 0.880Benzene ND 1.1108 2.84 2.81 70 - 130 20ND

ND NDBenzyl chloride ND NC128 ND ND 70 - 130 20ND

ND NDBromodichloromethane ND NC98 ND ND 70 - 130 20ND

ND NDBromoform ND NC107 ND ND 70 - 130 20ND

ND NDBromomethane ND NC96 ND ND 70 - 130 20ND

1.26 1.20Carbon Disulfide ND 4.9101 3.92 3.73 70 - 130 20ND

0.100 0.100Carbon Tetrachloride ND 0.0114 0.629 0.629 70 - 130 20ND

ND NDChlorobenzene ND NC87 ND ND 70 - 130 20ND

ND NDChloroethane ND NC95 ND ND 70 - 130 20ND

1.23 1.23Chloroform ND 0.098 6.00 6.00 70 - 130 20ND

ND NDChloromethane ND NC95 ND ND 70 - 130 20ND

14.3 14.3Cis-1,2-Dichloroethene ND 0.0100 56.7 56.7 70 - 130 20ND

ND NDcis-1,3-Dichloropropene ND NC104 ND ND 70 - 130 20ND

0.380 0.390Cyclohexane ND 2.6104 1.31 1.34 70 - 130 20ND

ND NDDibromochloromethane ND NC106 ND ND 70 - 130 20ND

0.380 0.520Dichlorodifluoromethane ND 31.1102 1.88 2.57 70 - 130 20ND

24.1 22.7Ethanol ND 6.091 45.4 42.7 70 - 130 20ND

Page 1 of 2

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QA/QC Data

ParameterBlankppbv

SampleResultppbv

SampleDupppbv

DUPRPD

SDG I.D.: GBG43589

LCS%

SampleResultug/m3

SampleDup

ug/m3

%Rec

Limits

%RPD

LimitsBlankug/m3

0.680 0.690Ethyl acetate ND 1.5122 2.45 2.48 70 - 130 20ND

0.890 0.870Ethylbenzene ND 2.395 3.86 3.78 70 - 130 20ND

0.820 0.860Heptane ND 4.886 3.36 3.52 70 - 130 20ND

ND NDHexachlorobutadiene ND NC75 ND ND 70 - 130 20ND

1.28 1.04Hexane ND 20.7104 4.51 3.66 70 - 130 20ND

1.06 1.00Isopropylalcohol ND 5.8100 2.60 2.46 70 - 130 20ND

ND NDIsopropylbenzene ND NC91 ND ND 70 - 130 20ND

2.60 2.56m,p-Xylene ND 1.692 11.3 11.1 70 - 130 20ND

3.48 3.32Methyl Ethyl Ketone ND 4.7105 10.2 9.78 70 - 130 20ND

ND NDMethyl tert-butyl ether(MTBE) ND NC109 ND ND 70 - 130 20ND

0.670 0.680Methylene Chloride ND 1.584 2.32 2.36 70 - 130 20ND

ND NDn-Butylbenzene ND NC94 ND ND 70 - 130 20ND

0.940 0.960o-Xylene ND 2.189 4.08 4.16 70 - 130 20ND

1.67 1.45Propylene ND 14.1110 2.87 2.49 70 - 130 20ND

ND NDsec-Butylbenzene ND NC86 ND ND 70 - 130 20ND

0.940 0.920Styrene ND 2.2100 4.00 3.92 70 - 130 20ND

2.53 2.60Tetrachloroethene ND 2.799 17.1 17.6 70 - 130 20ND

0.390 0.390Tetrahydrofuran ND 0.0116 1.15 1.15 70 - 130 20ND

4.20 4.27Toluene ND 1.796 15.8 16.1 70 - 130 20ND

ND NDTrans-1,2-Dichloroethene ND NC99 ND ND 70 - 130 20ND

ND NDtrans-1,3-Dichloropropene ND NC111 ND ND 70 - 130 20ND

76.5 76.8Trichloroethene ND 0.492 411 412 70 - 130 20ND

0.300 0.280Trichlorofluoromethane ND 6.995 1.68 1.57 70 - 130 20ND

ND NDTrichlorotrifluoroethane ND NC90 ND ND 70 - 130 20ND

ND NDVinyl Chloride ND NC94 ND ND 70 - 130 20ND

105 99% Bromofluorobenzene 101 5.996 105 99 70 - 130 20101

MS - Matrix SpikePhyllis Shiller, Laboratory Director

If there are any questions regarding this data, please call Phoenix Client Services at extension 200.

May 16, 2014MS Dup - Matrix Spike Duplicate

RPD - Relative Percent DifferenceLCS - Laboratory Control Sample

LCSD - Laboratory Control Sample Duplicate

NC - No CriteriaIntf - Interference

Page 2 of 2

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Sample Criteria Exceedences ReportFriday, May 16, 2014 Page 1 of 1

Acode Phoenix Analyte CriteriaResult RLSampNoAnalysis

UnitsCriteria

GBG43589 - EBCCriteria: None

RLCriteria

State: NY

#Error*** No Data to Display ***

Phoenix Laboratories does not assume responsibility for the data contained in this report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance.

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