RE: NOVEMBER 2016 SAMPLING RESULTS SMR INDUSTRIAL ...€¦ · Signature: Date: 12/29/2016 Email: [email protected] Phone: 651-697-9737 Report form help sheet Page 1of2 SMR-SR-2016

December 29, 2016 Project No.:023-6105.017 Metropolitan Council Environmental Services Industrial Waste Division 390 Robert St. N. St. Paul, MN 55101 Attention: Ms. Ashley Corbeille RE: NOVEMBER 2016 SAMPLING RESULTS SMR INDUSTRIAL DISCHARGE PERMIT NUMBER 2289 SOUTHEAST PUMP AND TREAT SYSTEM CANADIAN PACIFIC SHOREHAM FACILITY Dear Ms. Corbeille: On behalf of Canadian Pacific, enclosed is the November 2016 Sampling Results Self-Monitoring Report for the site located at 28th & Central Avenue NE, Minneapolis MN. In accordance with the Metropolitan Council Environmental Services (MCES) Industrial Discharge Permit Number 2289, effective October 1, 2016 (MCES permit), this submittal documents the quality of water discharged from the groundwater pump and treat system owned by Canadian Pacific. Required information for the discharge is provided as follows:

• Attachment A – Sampling Results - SMR. • Attachment B – analytical data from Pace Analytical Inc. for the November 2016 monthly

sampling event. • Attachment C - Field Instrument pH Calibration Records

Analytical results from the November 2016 sampling event showed that the treated discharge water was in compliance with the MCES permit discharge limitations during this reporting period. If you have any questions or comments, please do not hesitate to contact Barbara Johnson at (651) 697-9737. Thank you for your assistance in this matter. Very truly yours, GOLDER ASSOCIATES INC.

Alan Phillips Barbara Johnson, PE Staff Geologist Associate Cc: Ms. Aimee Zack, CP Ms. Claire Mackler, Golder

Golder Associates Inc. 1751 West County Rd. B, Ste. 105

Roseville, MN USA 55113 Tel: (651) 697-9737 Fax: (651) 697-9737 www.golder.com

Golder Associates: Operations in Africa, Asia, Australasia, Europe, North America and South America

Attachment A

SAMPLING RESULTS – SELF-MONITORING REPORT

Metropolitan Council Environmental Services Industrial Waste & Pollution Prevention Section 390 North Robert Street St. Paul, Minnesota 55101-1805

For MCES Use Only

Permit No: Staff:

Received: 0 L 45 E

SAMPLING RESULTS - SMR for Standard and Special Discharge Permits Please complete Page 2 of this form for each monitoring point with sampling requirements in Attachment A of the Permit.

1. Permittee Name: Canadian Pacific Railway Permit No: 2289 ------2. Facility Address: 28th Ave NE & Central Ave NE, Minneapolis, MN 55418

3.

D

Reporting Period: Year: 20_1_6 ___ _ Choose applicable period below:

Quarterly Reporter: 0 Jan-Mar

Semi-Annual Reporter: D Jan-Jun

Annual Reporter: D Jan-Dec

D Apr-Jun

O Jul-Dec

D Jul-Sep EJ Oct-Dec

No discharge/No sampling this period. If checked, proceed to section 9 below and do not complete page 2.

4. Proper Sampling: Were all samples collected and composited according to permit requirements?

0 Yes D No If No, add explanation below:

5. Proper Analysis: Were all analyses conducted per permit requirements? [!] Yes D No If No, add explanation below:

6. Representative Discha~: Are the an~ical results representative of the wastewater discharged during this monitoring event? ~ Yes LJ No If No, add explanation below:

7. Compliance Status: Compare the analytical results with the corresponding discharge limits in your Permit. Do any analytical results exceed the corresponding discharge limit(s) in your Permit? D Yes [!] No If Yes, add explanation below:

When did you become aware of the exceedance(s)?

8. General comments regarding submission: Total suspended solids, chemical oxygen demand, are sampled quarterly while volatile organic compounds are sampled monthly. An entry of "NS" in the following sample result tables indicates that the given parameter was not analyzed during the November sampling event.

9. Certification Statement: "I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to ensure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties under law for submitting false information, including the possibility of fine and imprisonment for known violations. "

Name (print): Barbara Johnson, PE Title: Authorized Representative for Canadian Pacific

Signature: Date: 12/29/2016

Email: [email protected] Phone: 651-697-9737

Report form help sheet

Page 1of2 SMR-SR-2016

Sample Results: Submit one result sheet for each sampling day per monitoring point. Enter daily values for each sampling event from one monitoring point, in accordance with requirements in the Industrial Discharge Permit (Section 8). Daily and long-term values shall be compared to Discharge Limitations in Permit Section A.1 for compliance determinations. Attach all laboratory data sheets and supporting calculations.

Monitoring Point: SP-01 Description: Effluent discharge line

Sample Start Date & Time: 11/15/1611:25 Sample End Date & Time: _1_1_11_5_12_0_16_1_1_:2_5 _____ _

gallons

Method of collection: 0 Manual D Automatic

Discharge volume through monitoring point on sampling day: 20,550 (estimated)

Sample collected by: D Permittee E] Other, name: Golder Associates Inc.

Sample composited by: 0 Permittee D Other, name: ~------------

Composite method: N_A ____________ _

Substance Analytical Result Unit Detection Limits Analysis Method Sample Method

Sample Laboratory Result Container Type Name

pH 6.4 S.U. 0-14 4500-H+ Grab-Single Other Field Measurement

Total Suspended Solids NS mg/I

Chemical Oxygen Demand NS mg/I

1, 1-Dichloroethane 0.0194 mg/I 0.00024 EPA8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

1, 1-Dichloroethene 0.0057 mg/I 0.00041 EPA8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

cis-1,2-Dichloroethene 0.0174 mg/I 0.00026 EPA8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

Tetrachloroethene 0.0389 mg/I 0.00050 EPA 8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

1, 1, 1-Trichloroethane 0.0171 mg/I 0.00050 EPA8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

Trichloroethene 0.0054 mg/I 0.00033 EPA8260 Grab - Single Vial - 40ml clear Pace Analytical Services, Inc.

mg/I

mg/I

mg/I

mg/I

mg/I

mg/I

mg/I

mg/I

Page 2 of 2 SMR-SR-2016

Attachment B

ANALYTICAL DATA FROM PACE ANALYTICAL SERVICES INC.

November 2016

#=CL#

November 18, 2016

LIMS USE: FR - ALISON ZOLLLIMS OBJECT ID: 40142093

40142093Project:Pace Project No.:

RE:

Alison ZollGolder Associates Inc.744 Broad Street25th FloorNewark, NJ 07102

023-6105-016 CP-SHOREHAM YARD

Dear Alison Zoll:Enclosed are the analytical results for sample(s) received by the laboratory on November 16, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Laurie [email protected] Manager

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC1241 Bellevue Street - Suite 9

Green Bay, WI 54302(920)469-2436

Page 1 of 16

#=CP#

CERTIFICATIONS

Pace Project No.:Project:

40142093023-6105-016 CP-SHOREHAM YARD

Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky UST Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334New York Certification #: 12064North Dakota Certification #: R-150

Virginia VELAP ID: 460263South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1Wisconsin Certification #: 405132750Wisconsin DATCP Certification #: 105-444USDA Soil Permit #: P330-16-00157Federal Fish & Wildlife Permit #: LE51774A-0




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#=SS#

SAMPLE SUMMARY


40142093023-6105-016 CP-SHOREHAM YARD

Lab ID Sample ID Matrix Date Collected Date Received

40142093001 111516-0800-200 Water 11/15/16 08:00 11/16/16 09:15

40142093002 SE EFFLUENT Water 11/15/16 11:25 11/16/16 09:15




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Page 3 of 16

#=SA#

SAMPLE ANALYTE COUNT


40142093023-6105-016 CP-SHOREHAM YARD

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

40142093001 111516-0800-200 EPA 8260 71 PASI-GHNW

40142093002 SE EFFLUENT EPA 8260 71 PASI-GHNW




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#=AR#

ANALYTICAL RESULTS


40142093023-6105-016 CP-SHOREHAM YARD

Sample: 111516-0800-200 Lab ID: 40142093001 Collected: 11/15/16 08:00 Received: 11/16/16 09:15 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Analytical Method: EPA 82608260 MSV

Acetone <3.0 ug/L 11/17/16 20:55 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 11/17/16 20:55 107-05-15.0 2.2 1Benzene <0.50 ug/L 11/17/16 20:55 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 11/17/16 20:55 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 11/17/16 20:55 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 11/17/16 20:55 75-27-41.0 0.50 1Bromoform <0.50 ug/L 11/17/16 20:55 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 11/17/16 20:55 74-83-95.0 2.4 12-Butanone (MEK) <3.0 ug/L 11/17/16 20:55 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 11/17/16 20:55 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 11/17/16 20:55 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 11/17/16 20:55 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 11/17/16 20:55 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 11/17/16 20:55 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 11/17/16 20:55 75-00-31.0 0.37 1Chloroform <2.5 ug/L 11/17/16 20:55 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 11/17/16 20:55 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 11/17/16 20:55 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 11/17/16 20:55 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 11/17/16 20:55 96-12-85.0 2.2 1Dibromochloromethane <0.50 ug/L 11/17/16 20:55 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 11/17/16 20:55 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 11/17/16 20:55 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 11/17/16 20:55 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 11/17/16 20:55 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 11/17/16 20:55 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 11/17/16 20:55 75-71-81.0 0.22 11,1-Dichloroethane <0.24 ug/L 11/17/16 20:55 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 11/17/16 20:55 107-06-21.0 0.17 11,1-Dichloroethene <0.41 ug/L 11/17/16 20:55 75-35-41.0 0.41 1cis-1,2-Dichloroethene <0.26 ug/L 11/17/16 20:55 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 11/17/16 20:55 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 11/17/16 20:55 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 11/17/16 20:55 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 11/17/16 20:55 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 11/17/16 20:55 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 11/17/16 20:55 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 11/17/16 20:55 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 11/17/16 20:55 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 11/17/16 20:55 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 11/17/16 20:55 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 11/17/16 20:55 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 11/17/16 20:55 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 11/17/16 20:55 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 11/17/16 20:55 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 11/17/16 20:55 108-10-15.0 2.1 1


without the written consent of Pace Analytical Services, LLC.Date: 11/18/2016 05:05 PM


Green Bay, WI 54302(920)469-2436

Page 5 of 16

#=AR#

ANALYTICAL RESULTS


40142093023-6105-016 CP-SHOREHAM YARD

Sample: 111516-0800-200 Lab ID: 40142093001 Collected: 11/15/16 08:00 Received: 11/16/16 09:15 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 11/17/16 20:55 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 11/17/16 20:55 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 11/17/16 20:55 103-65-11.0 0.50 1Styrene <0.50 ug/L 11/17/16 20:55 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 11/17/16 20:55 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 11/17/16 20:55 79-34-51.0 0.25 1Tetrachloroethene <0.50 ug/L 11/17/16 20:55 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 11/17/16 20:55 109-99-95.0 2.0 1Toluene <0.50 ug/L 11/17/16 20:55 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 11/17/16 20:55 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 11/17/16 20:55 120-82-15.0 2.2 11,1,1-Trichloroethane <0.50 ug/L 11/17/16 20:55 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 11/17/16 20:55 79-00-51.0 0.20 1Trichloroethene <0.33 ug/L 11/17/16 20:55 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 11/17/16 20:55 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 11/17/16 20:55 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 11/17/16 20:55 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 11/17/16 20:55 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 11/17/16 20:55 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 11/17/16 20:55 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 11/17/16 20:55 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 11/17/16 20:55 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 93 % 11/17/16 20:55 460-00-470-130 1Dibromofluoromethane (S) 109 % 11/17/16 20:55 1868-53-770-130 1Toluene-d8 (S) 97 % 11/17/16 20:55 2037-26-570-130 1




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#=AR#

ANALYTICAL RESULTS


40142093023-6105-016 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40142093002 Collected: 11/15/16 11:25 Received: 11/16/16 09:15 Matrix: Water



Acetone <3.0 ug/L 11/17/16 21:17 67-64-120.0 3.0 1Allyl chloride <2.2 ug/L 11/17/16 21:17 107-05-15.0 2.2 1Benzene <0.50 ug/L 11/17/16 21:17 71-43-21.0 0.50 1Bromobenzene <0.23 ug/L 11/17/16 21:17 108-86-11.0 0.23 1Bromochloromethane <0.34 ug/L 11/17/16 21:17 74-97-51.0 0.34 1Bromodichloromethane <0.50 ug/L 11/17/16 21:17 75-27-41.0 0.50 1Bromoform <0.50 ug/L 11/17/16 21:17 75-25-21.0 0.50 1Bromomethane <2.4 ug/L 11/17/16 21:17 74-83-95.0 2.4 12-Butanone (MEK) <3.0 ug/L 11/17/16 21:17 78-93-320.0 3.0 1n-Butylbenzene <0.50 ug/L 11/17/16 21:17 104-51-81.0 0.50 1sec-Butylbenzene <2.2 ug/L 11/17/16 21:17 135-98-85.0 2.2 1tert-Butylbenzene <0.18 ug/L 11/17/16 21:17 98-06-61.0 0.18 1Carbon tetrachloride <0.50 ug/L 11/17/16 21:17 56-23-51.0 0.50 1Chlorobenzene <0.50 ug/L 11/17/16 21:17 108-90-71.0 0.50 1Chloroethane <0.37 ug/L 11/17/16 21:17 75-00-31.0 0.37 1Chloroform <2.5 ug/L 11/17/16 21:17 67-66-35.0 2.5 1Chloromethane <0.50 ug/L 11/17/16 21:17 74-87-31.0 0.50 12-Chlorotoluene <0.50 ug/L 11/17/16 21:17 95-49-81.0 0.50 14-Chlorotoluene <0.21 ug/L 11/17/16 21:17 106-43-41.0 0.21 11,2-Dibromo-3-chloropropane <2.2 ug/L 11/17/16 21:17 96-12-85.0 2.2 1Dibromochloromethane <0.50 ug/L 11/17/16 21:17 124-48-11.0 0.50 11,2-Dibromoethane (EDB) <0.18 ug/L 11/17/16 21:17 106-93-41.0 0.18 1Dibromomethane <0.43 ug/L 11/17/16 21:17 74-95-31.0 0.43 11,2-Dichlorobenzene <0.50 ug/L 11/17/16 21:17 95-50-11.0 0.50 11,3-Dichlorobenzene <0.50 ug/L 11/17/16 21:17 541-73-11.0 0.50 11,4-Dichlorobenzene <0.50 ug/L 11/17/16 21:17 106-46-71.0 0.50 1Dichlorodifluoromethane <0.22 ug/L 11/17/16 21:17 75-71-81.0 0.22 11,1-Dichloroethane 19.4 ug/L 11/17/16 21:17 75-34-31.0 0.24 11,2-Dichloroethane <0.17 ug/L 11/17/16 21:17 107-06-21.0 0.17 11,1-Dichloroethene 5.7 ug/L 11/17/16 21:17 75-35-41.0 0.41 1cis-1,2-Dichloroethene 17.4 ug/L 11/17/16 21:17 156-59-21.0 0.26 1trans-1,2-Dichloroethene <0.26 ug/L 11/17/16 21:17 156-60-51.0 0.26 1Dichlorofluoromethane <0.21 ug/L 11/17/16 21:17 75-43-41.0 0.21 11,2-Dichloropropane <0.23 ug/L 11/17/16 21:17 78-87-51.0 0.23 11,3-Dichloropropane <0.50 ug/L 11/17/16 21:17 142-28-91.0 0.50 12,2-Dichloropropane <0.48 ug/L 11/17/16 21:17 594-20-71.0 0.48 11,1-Dichloropropene <0.44 ug/L 11/17/16 21:17 563-58-61.0 0.44 1cis-1,3-Dichloropropene <0.50 ug/L 11/17/16 21:17 10061-01-51.0 0.50 1trans-1,3-Dichloropropene <0.23 ug/L 11/17/16 21:17 10061-02-61.0 0.23 1Diethyl ether (Ethyl ether) <2.2 ug/L 11/17/16 21:17 60-29-75.0 2.2 1Ethylbenzene <0.50 ug/L 11/17/16 21:17 100-41-41.0 0.50 1Hexachloro-1,3-butadiene <2.1 ug/L 11/17/16 21:17 87-68-35.0 2.1 1Isopropylbenzene (Cumene) <0.14 ug/L 11/17/16 21:17 98-82-81.0 0.14 1p-Isopropyltoluene <0.50 ug/L 11/17/16 21:17 99-87-61.0 0.50 1Methylene Chloride <0.23 ug/L 11/17/16 21:17 75-09-21.0 0.23 14-Methyl-2-pentanone (MIBK) <2.1 ug/L 11/17/16 21:17 108-10-15.0 2.1 1




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#=AR#

ANALYTICAL RESULTS


40142093023-6105-016 CP-SHOREHAM YARD

Sample: SE EFFLUENT Lab ID: 40142093002 Collected: 11/15/16 11:25 Received: 11/16/16 09:15 Matrix: Water



Methyl-tert-butyl ether <0.17 ug/L 11/17/16 21:17 1634-04-41.0 0.17 1Naphthalene <2.5 ug/L 11/17/16 21:17 91-20-35.0 2.5 1n-Propylbenzene <0.50 ug/L 11/17/16 21:17 103-65-11.0 0.50 1Styrene <0.50 ug/L 11/17/16 21:17 100-42-51.0 0.50 11,1,1,2-Tetrachloroethane <0.18 ug/L 11/17/16 21:17 630-20-61.0 0.18 11,1,2,2-Tetrachloroethane <0.25 ug/L 11/17/16 21:17 79-34-51.0 0.25 1Tetrachloroethene 38.9 ug/L 11/17/16 21:17 127-18-41.0 0.50 1Tetrahydrofuran <2.0 ug/L 11/17/16 21:17 109-99-95.0 2.0 1Toluene <0.50 ug/L 11/17/16 21:17 108-88-31.0 0.50 11,2,3-Trichlorobenzene <2.1 ug/L 11/17/16 21:17 87-61-65.0 2.1 11,2,4-Trichlorobenzene <2.2 ug/L 11/17/16 21:17 120-82-15.0 2.2 11,1,1-Trichloroethane 17.1 ug/L 11/17/16 21:17 71-55-61.0 0.50 11,1,2-Trichloroethane <0.20 ug/L 11/17/16 21:17 79-00-51.0 0.20 1Trichloroethene 5.4 ug/L 11/17/16 21:17 79-01-61.0 0.33 1Trichlorofluoromethane <0.18 ug/L 11/17/16 21:17 75-69-41.0 0.18 11,2,3-Trichloropropane <0.50 ug/L 11/17/16 21:17 96-18-41.0 0.50 11,1,2-Trichlorotrifluoroethane <0.81 ug/L 11/17/16 21:17 76-13-15.0 0.81 11,2,4-Trimethylbenzene <0.50 ug/L 11/17/16 21:17 95-63-61.0 0.50 11,3,5-Trimethylbenzene <0.50 ug/L 11/17/16 21:17 108-67-81.0 0.50 1Vinyl chloride <0.18 ug/L 11/17/16 21:17 75-01-41.0 0.18 1m&p-Xylene <1.0 ug/L 11/17/16 21:17 179601-23-12.0 1.0 1o-Xylene <0.50 ug/L 11/17/16 21:17 95-47-61.0 0.50 1Surrogates4-Bromofluorobenzene (S) 93 % 11/17/16 21:17 460-00-470-130 1Dibromofluoromethane (S) 110 % 11/17/16 21:17 1868-53-770-130 1Toluene-d8 (S) 97 % 11/17/16 21:17 2037-26-570-130 1




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#=QC#

QUALITY CONTROL DATA


40142093023-6105-016 CP-SHOREHAM YARD

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

241643EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 40142093001, 40142093002

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1432616Associated Lab Samples: 40142093001, 40142093002

Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L <0.18 1.0 11/17/16 14:340.181,1,1-Trichloroethane ug/L <0.50 1.0 11/17/16 14:340.501,1,2,2-Tetrachloroethane ug/L <0.25 1.0 11/17/16 14:340.251,1,2-Trichloroethane ug/L <0.20 1.0 11/17/16 14:340.201,1,2-Trichlorotrifluoroethane ug/L <0.81 5.0 11/17/16 14:340.811,1-Dichloroethane ug/L <0.24 1.0 11/17/16 14:340.241,1-Dichloroethene ug/L <0.41 1.0 11/17/16 14:340.411,1-Dichloropropene ug/L <0.44 1.0 11/17/16 14:340.441,2,3-Trichlorobenzene ug/L <2.1 5.0 11/17/16 14:342.11,2,3-Trichloropropane ug/L <0.50 1.0 11/17/16 14:340.501,2,4-Trichlorobenzene ug/L <2.2 5.0 11/17/16 14:342.21,2,4-Trimethylbenzene ug/L <0.50 1.0 11/17/16 14:340.501,2-Dibromo-3-chloropropane ug/L <2.2 5.0 11/17/16 14:342.21,2-Dibromoethane (EDB) ug/L <0.18 1.0 11/17/16 14:340.181,2-Dichlorobenzene ug/L <0.50 1.0 11/17/16 14:340.501,2-Dichloroethane ug/L <0.17 1.0 11/17/16 14:340.171,2-Dichloropropane ug/L <0.23 1.0 11/17/16 14:340.231,3,5-Trimethylbenzene ug/L <0.50 1.0 11/17/16 14:340.501,3-Dichlorobenzene ug/L <0.50 1.0 11/17/16 14:340.501,3-Dichloropropane ug/L <0.50 1.0 11/17/16 14:340.501,4-Dichlorobenzene ug/L <0.50 1.0 11/17/16 14:340.502,2-Dichloropropane ug/L <0.48 1.0 11/17/16 14:340.482-Butanone (MEK) ug/L <3.0 20.0 11/17/16 14:343.02-Chlorotoluene ug/L <0.50 1.0 11/17/16 14:340.504-Chlorotoluene ug/L <0.21 1.0 11/17/16 14:340.214-Methyl-2-pentanone (MIBK) ug/L <2.1 5.0 11/17/16 14:342.1Acetone ug/L <3.0 20.0 11/17/16 14:343.0Allyl chloride ug/L <2.2 5.0 11/17/16 14:342.2Benzene ug/L <0.50 1.0 11/17/16 14:340.50Bromobenzene ug/L <0.23 1.0 11/17/16 14:340.23Bromochloromethane ug/L <0.34 1.0 11/17/16 14:340.34Bromodichloromethane ug/L <0.50 1.0 11/17/16 14:340.50Bromoform ug/L <0.50 1.0 11/17/16 14:340.50Bromomethane ug/L <2.4 5.0 11/17/16 14:342.4Carbon tetrachloride ug/L <0.50 1.0 11/17/16 14:340.50Chlorobenzene ug/L <0.50 1.0 11/17/16 14:340.50Chloroethane ug/L <0.37 1.0 11/17/16 14:340.37Chloroform ug/L <2.5 5.0 11/17/16 14:342.5Chloromethane ug/L <0.50 1.0 11/17/16 14:340.50cis-1,2-Dichloroethene ug/L <0.26 1.0 11/17/16 14:340.26cis-1,3-Dichloropropene ug/L <0.50 1.0 11/17/16 14:340.50




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#=QC#



40142093023-6105-016 CP-SHOREHAM YARD


Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1432616Associated Lab Samples: 40142093001, 40142093002

Matrix: Water

AnalyzedMDL

Dibromochloromethane ug/L <0.50 1.0 11/17/16 14:340.50Dibromomethane ug/L <0.43 1.0 11/17/16 14:340.43Dichlorodifluoromethane ug/L <0.22 1.0 11/17/16 14:340.22Dichlorofluoromethane ug/L <0.21 1.0 11/17/16 14:340.21Diethyl ether (Ethyl ether) ug/L <2.2 5.0 11/17/16 14:342.2Ethylbenzene ug/L <0.50 1.0 11/17/16 14:340.50Hexachloro-1,3-butadiene ug/L <2.1 5.0 11/17/16 14:342.1Isopropylbenzene (Cumene) ug/L <0.14 1.0 11/17/16 14:340.14m&p-Xylene ug/L <1.0 2.0 11/17/16 14:341.0Methyl-tert-butyl ether ug/L <0.17 1.0 11/17/16 14:340.17Methylene Chloride ug/L <0.23 1.0 11/17/16 14:340.23n-Butylbenzene ug/L <0.50 1.0 11/17/16 14:340.50n-Propylbenzene ug/L <0.50 1.0 11/17/16 14:340.50Naphthalene ug/L <2.5 5.0 11/17/16 14:342.5o-Xylene ug/L <0.50 1.0 11/17/16 14:340.50p-Isopropyltoluene ug/L <0.50 1.0 11/17/16 14:340.50sec-Butylbenzene ug/L <2.2 5.0 11/17/16 14:342.2Styrene ug/L <0.50 1.0 11/17/16 14:340.50tert-Butylbenzene ug/L <0.18 1.0 11/17/16 14:340.18Tetrachloroethene ug/L <0.50 1.0 11/17/16 14:340.50Tetrahydrofuran ug/L <2.0 5.0 11/17/16 14:342.0Toluene ug/L <0.50 1.0 11/17/16 14:340.50trans-1,2-Dichloroethene ug/L <0.26 1.0 11/17/16 14:340.26trans-1,3-Dichloropropene ug/L <0.23 1.0 11/17/16 14:340.23Trichloroethene ug/L <0.33 1.0 11/17/16 14:340.33Trichlorofluoromethane ug/L <0.18 1.0 11/17/16 14:340.18Vinyl chloride ug/L <0.18 1.0 11/17/16 14:340.184-Bromofluorobenzene (S) % 95 70-130 11/17/16 14:34Dibromofluoromethane (S) % 109 70-130 11/17/16 14:34Toluene-d8 (S) % 98 70-130 11/17/16 14:34

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1432617LABORATORY CONTROL SAMPLE:LCSSpike

1,1,1-Trichloroethane ug/L 53.050 106 70-1311,1,2,2-Tetrachloroethane ug/L 47.450 95 67-1301,1,2-Trichloroethane ug/L 49.350 99 70-1301,1,2-Trichlorotrifluoroethane ug/L 54.650 109 50-1501,1-Dichloroethane ug/L 52.050 104 70-1331,1-Dichloroethene ug/L 48.550 97 70-1301,2,4-Trichlorobenzene ug/L 48.450 97 70-1301,2-Dibromo-3-chloropropane ug/L 45.950 92 50-1501,2-Dibromoethane (EDB) ug/L 50.750 101 70-1301,2-Dichlorobenzene ug/L 49.750 99 70-130




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#=QC#



40142093023-6105-016 CP-SHOREHAM YARD


Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1432617LABORATORY CONTROL SAMPLE:LCSSpike

1,2-Dichloroethane ug/L 53.850 108 70-1301,2-Dichloropropane ug/L 49.050 98 70-1301,3-Dichlorobenzene ug/L 49.450 99 70-1301,4-Dichlorobenzene ug/L 48.750 97 70-130Benzene ug/L 53.850 108 60-135Bromodichloromethane ug/L 50.750 101 70-130Bromoform ug/L 43.950 88 70-130Bromomethane ug/L 42.650 85 33-130Carbon tetrachloride ug/L 55.250 110 70-138Chlorobenzene ug/L 49.650 99 70-130Chloroethane ug/L 51.750 103 51-130Chloroform ug/L 53.650 107 70-130Chloromethane ug/L 45.550 91 25-132cis-1,2-Dichloroethene ug/L 52.750 105 69-130cis-1,3-Dichloropropene ug/L 45.250 90 70-130Dibromochloromethane ug/L 50.850 102 70-130Dichlorodifluoromethane ug/L 25.250 50 23-130Ethylbenzene ug/L 52.350 105 70-136Isopropylbenzene (Cumene) ug/L 53.350 107 70-140m&p-Xylene ug/L 105100 105 70-138Methyl-tert-butyl ether ug/L 54.850 110 66-138Methylene Chloride ug/L 51.650 103 70-130o-Xylene ug/L 53.650 107 70-134Styrene ug/L 50.150 100 70-133Tetrachloroethene ug/L 48.250 96 70-138Toluene ug/L 50.350 101 70-130trans-1,2-Dichloroethene ug/L 51.650 103 70-131trans-1,3-Dichloropropene ug/L 44.050 88 69-130Trichloroethene ug/L 50.350 101 70-130Trichlorofluoromethane ug/L 51.550 103 50-150Vinyl chloride ug/L 47.450 95 49-1304-Bromofluorobenzene (S) % 99 70-130Dibromofluoromethane (S) % 110 70-130Toluene-d8 (S) % 98 70-130

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1432699MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40142158023

1432700

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1-Trichloroethane ug/L 50 99 70-134105 6 2050<0.50 49.3 52.51,1,2,2-Tetrachloroethane ug/L 50 96 67-130100 4 2050<0.25 47.9 50.01,1,2-Trichloroethane ug/L 50 98 70-130103 4 2050<0.20 49.2 51.51,1,2-Trichlorotrifluoroethane ug/L 50 108 50-150117 8 2050<0.81 54.0 58.51,1-Dichloroethane ug/L 50 96 70-134102 7 2050<0.24 47.9 51.21,1-Dichloroethene ug/L 50 95 68-136101 6 2050<0.41 47.3 50.4




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#=QC#



40142093023-6105-016 CP-SHOREHAM YARD


Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1432699MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40142158023

1432700

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L 50 101 62-139105 4 2050<2.2 50.6 52.61,2-Dibromo-3-chloropropane

ug/L 50 94 50-15098 3 2050<2.2 47.2 48.8

1,2-Dibromoethane (EDB) ug/L 50 101 70-130106 4 2050<0.18 50.7 52.91,2-Dichlorobenzene ug/L 50 99 70-130104 5 2050<0.50 49.5 51.81,2-Dichloroethane ug/L 50 99 70-130106 6 2050<0.17 49.7 52.81,2-Dichloropropane ug/L 50 97 70-130100 2 2050<0.23 48.7 49.81,3-Dichlorobenzene ug/L 50 99 70-131102 3 2050<0.50 49.4 51.11,4-Dichlorobenzene ug/L 50 98 70-130101 3 2050<0.50 48.8 50.5Benzene ug/L 50 99 57-138105 6 2050<0.50 49.5 52.6Bromodichloromethane ug/L 50 101 70-130104 3 2050<0.50 50.4 52.1Bromoform ug/L 50 88 70-13091 4 2050<0.50 43.8 45.4Bromomethane ug/L 50 96 33-130109 13 2750<2.4 48.0 54.5Carbon tetrachloride ug/L 50 104 70-138112 8 2050<0.50 52.1 56.2Chlorobenzene ug/L 50 99 70-130102 3 2050<0.50 49.5 51.1Chloroethane ug/L 50 102 51-130109 7 2050<0.37 50.9 54.7Chloroform ug/L 50 98 70-130105 7 2050<2.5 49.0 52.6Chloromethane ug/L 50 105 25-132113 7 2050<0.50 52.4 56.3cis-1,2-Dichloroethene ug/L 50 97 61-140104 7 2050<0.26 48.5 52.0cis-1,3-Dichloropropene ug/L 50 92 70-13095 3 2050<0.50 46.0 47.5Dibromochloromethane ug/L 50 102 70-130104 3 2050<0.50 50.8 52.2Dichlorodifluoromethane ug/L 50 89 23-13094 6 2050<0.22 44.5 47.2Ethylbenzene ug/L 50 104 70-138108 4 2050<0.50 51.8 53.9Isopropylbenzene (Cumene) ug/L 50 105 70-152110 4 2050<0.14 52.7 54.9m&p-Xylene ug/L 100 104 70-140108 4 20100<1.0 104 108Methyl-tert-butyl ether ug/L 50 102 66-139110 7 2050<0.17 51.1 54.9Methylene Chloride ug/L 50 95 70-130102 7 2050<0.23 47.6 50.8o-Xylene ug/L 50 105 70-134110 4 2050<0.50 52.7 55.1Styrene ug/L 50 99 70-138102 4 2050<0.50 49.3 51.2Tetrachloroethene ug/L 50 98 70-148102 4 2050<0.50 49.2 51.0Toluene ug/L 50 100 70-130103 3 2050<0.50 50.0 51.6trans-1,2-Dichloroethene ug/L 50 97 70-133104 6 2050<0.26 48.5 51.8trans-1,3-Dichloropropene ug/L 50 90 69-13093 4 2050<0.23 44.8 46.7Trichloroethene ug/L 50 101 70-131104 3 2050<0.33 50.6 52.2Trichlorofluoromethane ug/L 50 103 50-150110 7 2050<0.18 51.4 55.2Vinyl chloride ug/L 50 106 49-133113 7 2050<0.18 52.8 56.54-Bromofluorobenzene (S) % 99 70-13099Dibromofluoromethane (S) % 103 70-130106Toluene-d8 (S) % 98 70-13098




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#=QL#

QUALIFIERS


40142093023-6105-016 CP-SHOREHAM YARD

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Green BayPASI-G




Green Bay, WI 54302(920)469-2436

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#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE


40142093023-6105-016 CP-SHOREHAM YARD

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

40142093001 241643111516-0800-200 EPA 826040142093002 241643SE EFFLUENT EPA 8260




Green Bay, WI 54302(920)469-2436

Page 14 of 16

Pag

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6UPPERMIDWESTREGI~~~ ·' oi MN: 612-607-1700 WI:~ ~

(Please PilntClearlYJ.

I ::ompany Name: IGoiJer lss~•"'etkS I :.ranch/Location: I JV\ fo, Lei, v I e- {

1 NJ 18Ana/yticaJ 41 cJll 'f ®1L.f2.0C/3

c N OF c STODY. le--_Q_u_ote_#=~1------>hone:

>roject Contact: IAfi5Atl'l 2..o ti 17 'J-6 "( )-{ q LL

www.pecelab.s.oom

Mail To Contact:

Project Number: (JL~ -6(0)-0l' A=None B=HCL C=H2S04 D=HN03 E=DI Water I *Preservation Cod!s F=Methanol

J=Olher Project Name: C P- S 1'.t> re "1ciwi Yqrd H=Sodium Bisulfate Solution !=Sodium Thiosulfate

Project State: ;ill tJ Sampled By (Print): I l~·fo Y} '\:> h : I { J ttJ

Sampled By (Sign): Al- fr.. 'i?ll hf J

FILTERED? (YES/NO)

PRESERVATION (CODE)*

PO #: 1 Regulatory Program:

Data Package Options MS/MSD Matrix Codes (billable) O On your sample A= Air w =water 0 EPA Level Ill . B =Biota ow= Drinking Water

(billable) C = Charcoal GW =Ground Water

0 EPA Level IV O NOT needed on ~: ~~11 sw =Surface water

your sample 51 = Slud e COLLECTION

PACE LAB# CLIENT FIELD ID MATRIX DATE I TtlllE

6bl TllSl 6-0fOd- 2..80 11/trft' I Moo I w CD2 .SE efff \.\l"'l'lt- •t1r/l6 I H 2..) I w

R1,1sh Turnaround Time Requested~ Prelims

f'llllli ~

(Rush TAT subject to approval/surcharge) 5 Date Needed:

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DatefTime:

1111r:;111 r DatefTime:

Transmit Prelim Rush Results by (complete what you want): r':4z:£ //-1 )-{ (,,,

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G=NaOH Mail To Company:

Mail To Address:

Invoice To Contact:

Invoice To Company:

Invoice To Address:

Invoice To Phone:

CLIENT COMMENTS

Emall#1: \

Email #2: ( vlf 'iJ\ .J Telephone:

Dale/Time:

1U\fnlll11 ~

(\°t, ~ri:~ it t/aL A AJ. R ived By:

Fax:

Samples on HOLD are subject to

special pricing and release of llablllty

C019a(27 Jun2006)

'Relinquished By: Datemme: Received By: Date/Time:

LAB COMMENTS Profile#

(lab Use Only)

-i..-4 OmLv!?

~-;;< -:-4 n or\l "B 'b&} tA\lij\llP

PACE Project No.

l/oJ 4 2-093 oc

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Page 16 of 16

~eAnalytica( Sample Condition Upon Receipt Pace Analytical Services, Inc.

1241 Bellevue Street, Suite 9 Green Bay, WI 54302

I

«:uent Name: C:l16 \c\ e .c Project#:

Courier: r Fed Ex r UPS """ Client r Pace,J5ther: /). JUCf!l;) Tracking #: {2../ 2.,3 !?2Q - '2-Custody Seal on Cooler/Box Present: f7 yes - no Seals intact: T yes r no

Custody Seal on Samples Present: r yes J7' no Seals intact: r yes - no

W0#:40142093 II II If II II lllf 11111111 40142093

Packing Material: p' Bubble Wrap 17" Bubble Bags r None r Other

Thermometer Used -?e- Ss:;> Type of Ice: e Blue Dry None r /Samples on ice, cooling process has begun

CoolerTemperatu,. """'" )1 /Co~ 2 Biological Tissue Is Froze"' ryes Temp Blank Present: ryes no rno Person examining contents:

Temp should be above freezing to 6°C for all sample except Biota. Date: lt/j!Jt/l l~ Frozen Biota Samples should be received :> 0°C. Comments: Initials:

Chain of Custody Present: J?'.fves ONo ON/A 1.

Chain of Custody Filled Out: jlfYes 0No ON/A 2.

Chain of Custody Relinquished: \21'Yes ONo ON/A 3.

Sampler Name & Signature on COC: Elves ONo ON/A 4.

Samples Arrived within Hold Time: ¢'es ONo ON/A 5.

- VOA Samples frozen upon receipt 0Yes 0No DatefTime:

Short Hold Time Analysis (<72hr): 0Yes .l2f No ON/A 6.

Rush Turn Around Time Requested: OYesA'.'.SNo ON/A 7.

Sufficient Volume: rzfves ONo ON/A 8.

Correct Containers Used: ,l2!'ves 0No ON/A 9 .

-Pace Containers Used: .el'ves 0No ON/A

-Pace IR Containers Used: OYes ONo _,eiNIA

Containers Intact: 0Yes ONo ON/A 10.

Filtered volume received for Dissolved tests 0Yes 0No ~IA 11.

Sample Labels match COC: ~es 0No ON/A 12.

-Includes date/time/ID/Analysis Matrix: 11 '\ All containers needing preservation have been checked. (Non-Compliance noted in 13.) 0Yes 0No flN!A 13.

r HN03 r H2S04 rNaOH r NaOH +ZnAct

- ----- --- ----- -- --- -- - ---- -- --- ---- --All containers needing preservation are found to be in compliance with EPA recommendation. 0Yes ONo ~/A (~_9~:..!::!~ :>_2.:_ ~qf:!+Znf-_9~9.:, ~!!,2':' ~12) ____ ._ _________ exceptions: OA coliform, TOC, TOX, TOH, Ji' Initial when 'lab Std #ID of ILJaret O&G, WIDROW, Phenolics, OTHER: Yes 0No completed preservative Time:

Headspace in VOA Vials ( >6mm}: 0Yes J2l'No ON/A 14.

Trip Blank Present: <fli!it?Jt!IU/1,P)/ 15. 00 \ tA IN_-' .l.Jit ..mJd t:D 1,a-e, T /::5 l?~(I_ n I J .A I

<Yb l'~ ,A.jMJ, Trip Blank Custody Seals Present µ{es 0No ON/A

Pace Trip Blank Lot# (if purchased}: ?, 1 L. il.A- vi II lei itc Client Notification/ Resolution: If checked, see attached form for additional comments ·u

Project Manager Review: Date: __ 1~ .... \...,11e..,\11o11·'i\J.a..-----

F-GB-C-031-Rev.03 (9Apri12015) SCURFonn

Attachment C

FIELD INSTRUMENT pH CALIBRATION RECORDS

Page _1_of_1_

Field Instrument pH Calibration Records INSTRUMENT (MAKE/MODEL NO.) Sper Scientific/850051 INSTRUMENT NO.

STANDARD INFORMATION

Project Number: 0236105017 Project Name: CP-Shoreham Yard

Standard Vendor: Field Environmental Instruments

Prepared Date: NA Where Prepared: NA

Purchase Date: 10/16/2016 Expiration Date: Varies Grade: N/A Units: Standard Units

Standard 4.00 @25 0C Lot # F133-18 Exp Date 5/18/18

Standard 7.00 @25 0C Lot # F172-18 Exp Date 6/29/18

DATE

(mm/dd/yy) TIME

(hr:min) TEMP DEG C

STD VALUE

INSTRUMENT RESPONSE % DEV PASS/

FAIL CALIBRATED

(YES, NO) SAMPLER INITIALS

10/17/16 1310 23.0 4.0 4.0 0 Pass Yes AP

10/17/16 1315 23.0 7.0 7.0 0 Pass Yes AP

10/31/16 1335 19.0 7.0 7.0 0 Pass Yes AP

10/31/16 1343 19.0 4.0 4.0 0 Pass Yes AP

11/15/16 1130 19.0 4.0 4.0 0 Pass Yes AP

11/15/16 1135 18.5 7.0 7.0 0 Pass Yes AP

Acceptable calibration check is if the meter reads within +/- 0.2 pH units of the value of appropriate calibration standard.

\\MIN1-V-FS1\Projects\Golder Projects\023 PROJECTS\023-6105 Shoreham Yard File Review\East Side Southeast P&T System\MCES Special Discharge Reports\2016\November Sample Results\Final\pH_Calibration Form.doc

Golder Associates REV-2-03/07

Documents

RE: NOVEMBER 2016 SAMPLING RESULTS SMR INDUSTRIAL ...€¦ · Signature: Date: 12/29/2016 Email: [email protected] Phone: 651-697-9737 Report form help sheet Page 1of2 SMR-SR-2016