RE: PHASE II ENVIRONMENTAL SITE ASSESSMENT WAREHOUSE

13478 Chandler Road

Omaha, Nebraska 68138-3716 402.556.2171 Fax 402.556.7831

www.thielegeotech.com

G E O T E C H N I C A L M A T E R I A L E N V I R O N M E N T A L E N G I N E E R I N G

January 9, 2020

Matthew Rupert Rupert Construction 7502 Crown Point Ave Omaha, Nebraska 68134 RE: PHASE II ENVIRONMENTAL SITE ASSESSMENT WAREHOUSE PROPERTY 7502 CROWN POINT AVENUE, OMAHA NEBRASKA TG# 19631.01 Dear Mr. Rupert: This letter report summarizes the results of a Phase II Environmental Site Assessment (ESA) conducted at the above-referenced site. BACKGROUND The assessment site is a Warehouse property and is located at 7502 Crown Point Avenue. The site consists of a 7.88-acre industrial lot with a 1,500 square-foot slab-on-grade warehouse building that is currently occupied by operations of Rupert Construction. The Phase I ESA conducted by TG in November 2019 identified the following Recognized Environmental Condition. The Recognized Environmental Condition at the assessment site is the likely presence of petroleum hydrocarbons and/or hazardous substances under conditions indicative of a release. Specifically, a significant quantity of industrial debris was apparent in the storage yard and ravine at the assessment site. These operations have potential to impact the assessment site with petroleum hydrocarbons and polychlorinated biphenyls (PCBs) from oils and grease, volatile organic compounds (VOCs) from cleaning solvents, and metals contamination from weathering. In addition, the western drainage ravine has been adversely impacted by diesel fuel from a release that occurred at Sitel Corporation, located adjacent west of the assessment site. The following historical uses of the assessment site and adjoining properties were identified that occurred during a time before petroleum hydrocarbons and hazardous substances were utilized. Leaks and spills from mishandling of petroleum hydrocarbons and hazardous substances were common before regulation, creating adverse impact to soils and ground water. The identified present and historical uses of the assessment site and adjoining properties that have likely impacted the subsurface are as follows:

• The garage building has been present since at least 1997. Significant spills of petroleum hydrocarbons were apparent in the garage building. Garage service activities typically utilize and store vehicle maintenance substances and generate waste oil and solvent mixtures. These operations have potential to impact the assessment site with petroleum hydrocarbons and polychlorinated biphenyls (PCBs) from historical oils and grease, and volatile organic compounds (VOCs) from cleaning solvents. Metals

Phase II ESA January 9, 2020 TG #19631.01 Page 2 of 11

T H I E L E G E O T E C H , I N C

contamination from weathering from outdoor storage of vehicles and vehicle parts also has potential to exist.

• Sitel Corporation operated adjacent west of the assessment site. A release of approximately 1,750

gallons of diesel fuel occurred on March 31, 2014 due to faulty equipment. This spill flowed into the drainage ravine on the west side of the assessment site. An assessment conducted in 2014 found that soils in the western drainage ravine were impacted by diesel fuel from this release, which extends north into the residential subdivision. The remediation status of the release is NEBRASKA RBCA TIER I OR TIER II INVESTIGATION.

• A significant amount of construction and industrial debris were observed in the storage yard and ravine, and the soils were composed of junk fill. Stained soils were observed in numerous locations across the site and petroleum odors were noted.

FIELD ACTIVITIES Soil and groundwater sampling were completed at this site. The attached Boring Location Plan illustrates the sample locations. The soil borings were located at or adjacent to areas of environmental concern. Environmental concerns are summarized for each boring in Table 1, below. TABLE 1. ENVIRONMENTAL CONCERNS

Location Environmental Concerns Potential Hazardous Substance

EB-1 and EB-2 Shop activities and staining Petroleum, VOCs, Metals, PCBs

EB-3 through EB-9 Observed fill, debris, and staining Petroleum, VOCs, Metals, PCBs

EB-10 Sitel petroleum release area and down-gradient location from on-site fill

Petroleum, VOCs, Metals, PCBs

EB-11 and EB-12 Observed fill Petroleum, VOCs, Metals, PCBs The soil borings were advanced to depths of 15-50 feet below ground surface (bgs). Intrusive activities were conducted by standard direct push techniques with a Geoprobe® 7822DT rubber tracked machine and Geoprobe DT22 soil sampling equipment. Soil sampling was conducted at 5-foot intervals in RPVC liners during direct push sampling. A geologist described the recovered soil samples collected during this investigation. Sample descriptions included color, moisture content, consistency, sediment type, geologic origin, and notations of any visual or olfactory evidence of contamination. Recovered intervals were screened at 1-2 feet intervals with a 10.6 eV photoionization detector (PID). The field screening concentration from each interval was then recorded on the boring logs. Prior to conducting field screening, the PID was zeroed and calibrated with laboratory prepared calibration gas. The calibration gas used to calibrate the PID was a 100-ppm concentration of isobutylene. The results of field analysis are summarized in Table 2 on page 4. The boring logs are attached. Samples submitted for metals and PCB analysis were based upon visual evidence of potential contamination. Evidence of potential contamination generally included unusual discoloration, unusual odors, ash/cinders, and



other debris. The sample with the highest field screening concentration were selected for volatile organic compound (VOC) and petroleum hydrocarbon analysis. If field screening indicated no elevated concentrations, samples submitted for VOC and petroleum analyses were based upon visual and/or olfactory evidence of potential contamination. If no visual and/or olfactory cues were observed, the sample was collected from the area observed to be at or within approximately five feet of the water table. Upon completion of the soil borings, temporary monitoring wells were installed within borings EB-1, EB-4, EB-9, and EB-10. The wells in borings EB-1, EB-4, and EB-9 were set at 50 feet below ground surface (bgs) and constructed of 10 feet of one-inch nominal diameter, schedule 40, PVC screen with 0.010 slots with sufficient riser to reach the surface. The well within boring EB-10 was set at 20 feet bgs and constructed of 10-feet of one-inch nominal diameter, schedule 40, PVC screen with 0.010 slots with sufficient riser to reach the surface. A ground water sample was collected using a disposable bailer from boring EB-10. The bailer was gently lowered until groundwater was encountered. Approximately 1,000 milliliters were purged before sampling. Upon completion of sampling, well casing was pulled, and the remaining boring voids were backfilled with hydrated bentonite granules. The wells within borings EB-1, EB-4, and EB-9 were allowed to stabilize for 7 days. No ground water was encountered after this period. The well casings were pulled, and the remaining boring voids were backfilled with hydrated bentonite granules. Soil and groundwater samples were submitted for select analysis of VOCs by EPA Method 8260, total extractable hydrocarbons (TEH) by Iowa Method OA-2, RCRA metals by EPA 6010 and 7471, and PCBs by EPA Method 8082. The samples were placed into laboratory provided, new, clean, sample jars. Samples were cooled to approximately 4º C with ice in a cooler and maintained at approximately that temperature throughout delivery to the laboratory. Samples submitted for analytical testing were maintained under a sample chain-of-custody through delivery to Eurofins Laboratories (Eurofins) in Cedar Falls, Iowa. The results of laboratory analysis conducted on these samples are summarized in Tables 3 and 4, respectively, on pages 4 through 8. Laboratory reports for are attached. Standard decontamination procedures were implemented during sample collection in order to prevent cross-contamination. Cross-contamination during boring advancement was minimized by the incorporation of decontamination procedures for all probe and soil sampling equipment. All large equipment (i.e. direct push machine and probe rods) were decontaminated via a high-pressure hot water wash prior to arriving on-site, between each boring location, and before leaving the site. All smaller drilling and sampling equipment (i.e. sample tubes and fittings) were decontaminated via an Alconox wash and deionized water rinse between each sampling interval. Cross-contamination of samples was minimized with disposable, single use sampling equipment and laboratory provided and cleaned sample containers. Personnel involved in sampling wore new, disposable gloves for each phase of sampling. FINDINGS Lithology The lithology of soils identified on the site consisted of fill over Peoria Loess and Loveland Loess. Boring EB-10 consisted of colluvium over Peoria Loess The fill consisted of brown, moist, soft to hard, clay with varying amounts of concrete, brick, and glass rubble. The loess consisted of dark brown to light brown, slightly moist to wet, hard to soft silty clay, and clay. Plasticity ranges from no (silt) to high plasticity (clay). The colluvial soils consisted of light brown to brown, moist to wet, firm to soft silty clay to clay. Plasticity ranges from low (silt) to high plasticity (clay). Visual and olfactory indications of environmental impact were observed during sampling activities. Static water level was observed at 12.17 ft. bgs. within the temporary well at boring EB-10. Depth to groundwater in the upper level of the site was observed to be greater than 50 feet below ground surface.



Soil Analysis Typically, field samples slightly to moderately impacted by volatile and semi-volatile compounds exhibit field screening concentrations with an order of magnitude of 10-100 relative response units (RRUs). Maximum concentrations observed during soil field screening activities are summarized in Table 2, on page 4. TABLE 2. RESULTS OF SOIL FIELD SCREENING

Sample Location Maximum Concentration (Relative Response Units) Depth (ft bgs)

EB-1 0.1 0-1 EB-2 0.1 6-7 EB-3 0.0 N/A EB-4 0.1 35-36 EB-5 0.2 5-6 EB-6 79.3 0-1 EB-7 0.5 0-1 EB-8 0.3 0-1 EB-9 0.0 N/A

EB-10 0.0 N/A EB-11 0.0 N/A EB-12 0.0 N/A

ft bgs = feet below ground surface N/A = Not Applicable Relative Response Units (RRUs) are reported in parts per million (ppm)

TABLE 3. RESULTS OF SOIL ANALYSIS

Boring ID# (Interval)

Laboratory Method Utilized

Constituent Identified

(Above Detection Limits)

Result (mg/kg)

VCP RGs Residential-

Direct Contact (mg/kg)

VCP RGs Industrial-


EB-1 (0-1’)

PCBs (EPA 8082A) No detections N/A N/A N/A

RCRA Metals (EPA 6010C &

7471B)

Arsenic 11.3 0.46 22 Barium 210 3,900 100,000 Chromium 18.8 29,000 100,000 Lead 24.8 400 800 Mercury 0.03 5.9 350

VOCs (EPA 8260B No detections N/A N/A N/A

TEH (Iowa OA-2) Waste Oil 6,150 3,173** 3,173**

EB-2 (0-1’)

VOCs (EPA 8260B) No detections N/A N/A N/A


PCBs PCB-1254 9.06 0.24 8.9







Result (mg/kg)



VCP RGs Industrial-


EB-2 (0-1’)

(EPA 8082A)

RCRA Metals (EPA

6010C/7010/ 7471B)


EB-3 (0-1’) RCRA Metals (EPA 6010C &

7471B)


EB-3 (5-6’)


TEH (Iowa OA-2) Waste Oil 121 3,173** 3,173**

EB-4 (0-1’)


RCRA Metals (EPA 6010C &

7471B)

Barium 125 3,900 100,000

Chromium 12.3 29,000 100,000

EB-4 (35-36’)


TEH (Iowa OA-2) No detections N/A N/A N/A


7471B)

Arsenic 19.6 0.46 22 Barium 259 3,900 100,000 Chromium 20.4 29,000 100,000 Lead 478 400 800 Mercury 0.54 5.9 350

EB-5 (1-2’)



EB-6 (0-1’)

VOCs (EPA 8260B)

n-Butylbenzene 2,710 3,900* 3,900* sec-Butylbenzene 1,370 7,800* 120,000*

Ethylbenzene 137 5.8 250 Isopropylbenzene 458 490 9,900

p-Isopropyltoluene 1,000 NL NL Naphthalene 605 3.8 170

n-Propylbenzene 674 3,800* 24,000* 1,2,4-

Trimethylbenzene 4,730 76 1,800

1,3,5-Trimethylbenzene 2,290 68 1,500

Xylenes 3,110 140 2,500







Result (mg/kg)



VCP RGs Industrial-


EB-6 (0-1’) TEH (Iowa OA-2) Diesel 2,190 9,520** 9,520**

EB-6 (5-6’)


RCRA Metals EPA (6010C &

7471B)

Arsenic 6.77 0.46 22 Barium 191 3,900 100,000 Chromium 21 29,000 100,000 Lead 14.8 400 800 Mercury ND 5.9 350

EB-7 (0-1’)


TEH (Iowa OA-2) Waste Oil 45.9 3,173** 3,173**


RCRA Metals (EPA

6010C/7010/ 7471B)


EB-8 (0-1’)




7471B)

Arsenic 7.62 0.46 22 Barium 173 3,900 100,000 Chromium 19.1 29,000 100,000 Lead 31.5 400 800 Mercury ND 5.9 350

EB-9 (0-1’)



7471B)

Arsenic 13.2 0.46 22 Barium 232 3,900 100,000 Chromium 20.6 29,000 100,000 Lead 12.4 400 800 Mercury ND 5.9 350

EB-9 (1-2’)


TEH (Iowa OA-2) Waste Oil 24.0 3,173** 3,173**

EB-10 (0-1’) EB-10 (0-1’)



7471B)

Arsenic 9.52 0.46 22 Barium 249 3,900 100,000 Chromium 21.9 29,000 100,000







Result (mg/kg)



VCP RGs Industrial-


Lead 14.9 400 800 Mercury ND 5.9 350

EB-10 (12-13’)


TEH (Iowa OA-2) No detections N/A N/A N/A

EB-11 (15-16’)



EB-11 (16-17’)



7471B)


EB-12 (20-21’)



PCBs (EPA 8082A) N/A N/A N/A N/A

RCRA Metals (EPA

6010C/7010/ 7471B)


µg/kg = ppb (parts per billion) mg/kg = ppm (parts per million) Constituents in Bold exceed residential VCP remediation goals Constituents in Bold exceed industrial VCP remediation goals RGs = Remediation Goals VCP = Voluntary Cleanup Program TEH = Total Extractable Hydrocarbons N/A = Not Applicable ND = No Detections NL = Not Listed *= EPA Regional Screening levels ** NDEE RBCA RBSL guidance for contaminated surface soils



Metals Analytical testing for metals conducted on the soil samples identified concentrations(s) of metals above laboratory reporting limits within the soil samples EB-1 (0-1’), EB-2 (0-1’), EB-3 (0-1’), EB-4 (0-1’), EB-5 (0-1’), EB-6 (5-6’), EB-7 (0-1’), EB-8 (10-11’), EB-9 (0-1’), EB-10 (0-1’), EB-11 (16-17’), and EB-12 (20-21’). The constituents above laboratory detection limits were compared to Nebraska Department of Environment and Energy (NDEE) Voluntary Clean-up Program (VCP) applicable remediation goal. (RGs). The lead concentration was above the residential RG for direct contact within sample EB-5 (0-1’). Arsenic was above the residential direct contact RG at sample locations samples EB-1 (0-1’), EB-2 (0-1’), EB-3 (0-1’), EB-4 (0-1’), EB-5 (0-1’), EB-6 (5-6’), EB-7 (0-1’), EB-8 (10-11’), EB-9 (0-1’), EB-10 (0-1’), EB-11 (16-17’), and EB-12 (20-21’). Eastern Nebraska exhibits elevated background concentrations of arsenic within soils. EPA completed a study of arsenic background levels outside the Omaha Lead Superfund site within Eastern Omaha. Background concentrations ranged between 3.1 to 10.8 parts per million (ppm); with an average of 7.2 ppm. Although arsenic concentrations within the samples were slightly above the average, it is unlikely the site would be subject to an enforcement action if reported to the Nebraska Department of Environment and Energy (NDEE). PCBs Analytical testing for PCBs conducted on the soil samples identified concentration(s) of PCB-1254 above laboratory reporting limits within the soil sample EB-1 (0-1’). The result was compared to the NDEE VCP applicable remediation goal. The PCB-1254 concentration was above residential and industrial RGs for direct contact within sample EB-2 (0-1’). Petroleum Analytical testing for extractable hydrocarbons conducted on the soil samples identified concentration(s) of waste oil were above laboratory reporting limits within the soil samples EB-2 (0-1’), EB-3 (5-6’), EB-5 (1-2’), EB-7 (0-1’), EB-8 (0-1’), EB-9 (1-2’), and EB-12 (20-21’). Diesel concentrations were above laboratory reporting limits within the soil sample EB-6 (0-1’). The constituents above laboratory detection limits were compared the Nebraska Department of Environment and Energy (NDEE) Risk-Based Corrective Action Guidance exposures from contaminated surface soils. The residential and commercial Risk-Based Screening level (RBSL) for total extractable hydrocarbons as waste oil was exceeded at EB-1 (0-1’) and EB-8 (0-1’). VOCs Analytical testing for VOCs conducted on the soil samples identified concentration(s) of VOCs above laboratory reporting limits within the soil sample EB-6 (0-1’). Naphthalene, ethylbenzene, n-butylbenzene, n-propylbenzene, isopropylbenzene, n-butylbenzene, sec-butylbenzene, p-isopropyltoluene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and xylenes were above the laboratory reporting limits. The constituents above laboratory detection limits were compared to the NDEE VCP RGs. If no RGs were identified the EPA Regional Screening Levels were used. Ethylbenzene was above residential direct contact RGs. Naphthalene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and xylenes were above residential and industrial direct contact RGs.. No other COCs identified within soil samples above laboratory detection limits were identified above respective RGs.



Groundwater Analysis Analytical testing conducted on the groundwater sample collected form EB-10 identified no constituents above laboratory reporting limits. TABLE 4. RESULTS OF GROUNDWATER ANALYSIS

Well ID Laboratory Method Utilized



Result (mg/kg)



VCP RGs Industrial-


EB-10

VOCs (EPA 8260B) No Detections N/A N/A N/A

TEH (Iowa OA-2) No Detections N/A N/A N/A

µg/kg = ppb (parts per billion) mg/kg = ppm (parts per million) Constituents in Bold exceed residential VCP remediation goals RGs = Remediation Goals VCP = Voluntary Cleanup Program TEH = Total Extractable Hydrocarbons N/A = Not Applicable

CONCLUSIONS • Lead was detected within soil. One soil sample, EB-5 (0-1’), exceeded the voluntary cleanup program

(VCP) residential remediation goal (RG). • Arsenic was above the residential RG at sample locations EB-1 (0-1’), EB-2 (0-1’), EB-3 (0-1’), EB-

4 (0-1’), EB-5 (0-1’), EB-6 (5-6’), EB-7 (0-1’), EB-8 (10-11’), EB-9 (0-1’), EB-10 (0-1’), EB-11 (16-17’), and EB-12 (20-21’). Omaha has a higher background level of naturally occurring arsenic in soils. Eastern Nebraska exhibits elevated background concentrations of arsenic within soils. EPA completed a study of arsenic background levels outside the Omaha Lead Superfund site within Eastern Omaha. Background concentrations ranged between 3.1 to 10.8 parts per million (ppm); with an average of 7.2 ppm. Although arsenic concentrations within the samples were slightly above the average, it is unlikely the site would be subject to an enforcement action if reported to the Nebraska Department of Environment and Energy (NDEE).

• Waste oil was detected above the residential and industrial petroleum release risk-based screening levels (RBSLs) for exposure to contaminated surface soils in sample EB-8 (0-1’).

• PCB-1254 was detected in sample EB-1 (0-1’) and exceeded the residential and industrial RGs. • VOCs were detected in soil sample EB-6 (0-1’). Naphthalene, 1,2,4-trimethylbenzene, 1,3,5-

trimethylbenzene, and xylenes were above residential and industrial RGs. Ethylbenzene was above the residential RG.

The results of the analytical testing conducted on the groundwater samples did not identify COCs above laboratory reporting limits.



RECOMMENDATIONS It is understood this site will remain a commercial/industrial site. If the site will remain commercial/industrial use, TG recommends surface soils with constituents exceeding industrial/commercial action levels be removed and disposed of at a permitted disposal facility. The areas of concern include EB-1, EB-2, EB-6, and EB-8. If future activities may include residential use and/or use by sensitive populations, further soil sampling and mitigation may be warranted in order to address the constituents of concern concentrations above the residential action levels. LIMITATIONS Soil and groundwater samples were collected at the discrete locations indicated on the site map and were analyzed for select parameters only. The data obtained may not be representative of other locations on the site. Also, note conditions may change over time. Consequently, Thiele Geotech, Inc. does not guarantee or warrant the environmental condition of the property. This study is not intended to meet the requirements of a "Phase I" ESA or a Risk Based Corrective Action Tier 1 Assessment. This study also did not include identification or evaluation of radon, methane gas, or sampling or testing of soil, soil vapor, and air for constituents other than those listed within this report. Our conclusions regarding the assessment site are based upon observations of existing site conditions, our interpretation of site history and site usage information and the results of a limited subsurface exploration, sample screening and chemical testing program. The results of this study must be qualified by the fact that only limited sampling and chemical testing have been conducted at the site. The concentrations of contaminants measured may change at any particular location as a function of time in response to natural conditions, chemical reactions and other events. Therefore, conclusions regarding the condition of the site do not represent a warranty that all areas within the site and beneath structures are of the same environmental quality as those sampled. Further, contamination could also exist in forms not indicated by the limited investigation conducted. If additional information becomes available regarding this site, such information should be provided to Thiele Geotech, Inc. so that our conclusions and recommendations may be reviewed and modified as necessary. This report is based on the current regulatory environment, current regulations, and guidance. Regulatory agency interpretations, future regulatory changes, and/or policy or guidance changes may affect the environmental status of the site. If you have questions, or if there is any additional information we can provide regarding the environmental condition of this site, please feel free to contact us.

Respectfully, Thiele Geotech, Inc.

Jeremy Kendle, G.I.T. Geologist



Reviewed by,

Robert T. Miller, P.G. Nebraska License G-0276

. Attachments: Site Vicinity Map Topographic Map Boring Location Plan

Boring Log Reports of Analysis/Chain of Custody Records

Site Vicinity Map

Project Warehouse Property

7502 Crown Point Ave

Job #

19631.01 Date

1/2/20

SITE

Topographic Map

(From 1984 Irvington, Nebraska Quadrangle) Project Warehouse Property

7502 Crown Point Ave

Job #

19631.01 Date

1/2/20

SITE

Thiele Geotech Inc

BORING LOCATION PLAN

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SCALE: 1 "= 60'

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PHOTO DATE:06/2O1 B

PROJECT

WAREHOUSE PROPERTY 7502 CROWN POINT AVE.

OMAHA, NE OB 19631.01 DATE: 1 7 20

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BORING LOCATION

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19631.01

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OMAHA, NE

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WAREHOUSE PROPERTY

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7502 CROWN POINT AVE.

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1/7/20

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%%UBORING LOCATION PLAN

fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

low plasticity, trace sand and gravel, hydrocarbonodor in the top 1'

low plasticity, iron oxide staining, gray mottling

low plasticity, iron oxide staining, gray mottling,silty

lean clay

lean clay

hard

firm

moist

moist

olivegray

lightbrown

lightbrown

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(0-1') 10:30PID = 0.1

(1-2')PID = 0.0

(2-3')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(7-8')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

(20-21')PID = 0.0(21-22')

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(22-23')PID = 0.0

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PAGE 1 OF 2BORING NUMBER EB-1

DRILLING DATE 12/16/19

DRILLING METHOD DT22

DRILLER Omar Ibarra

LOGGED BY Jeremy Kendle

NOTES 1'' temp. well @ 50' w/ 10' of screen

SURFACE Gravel

HOLE SIZE 2.25 inches

DRILL RIG Geoprobe 7822DT

CHECKED BY Robert Miller

GROUND ELEVATION

GROUND WATER LEVELS:

END OF DRILLING None encountered

DURING DRILLING None encountered

BORING DEPTH 50.0 feet

STATIC WATER LEVEL None encountered

CLIENT Rupert Construction

PROJECT NUMBER 19631.01

PROJECT NAME Warehouse Property

PROJECT LOCATION 7502 Crown Point Ave, Omaha NE

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JTHIELE GEOTECH INC13487 CHANDLER ROADOMAHA, NEBRASKA 68134Telephone: 402-556-2171

Peoria loess

Lovelandloess

DT22C-6

DT22C-7

DT22C-8

DT22C-9

DT22C-10

low plasticity, silty, homogenous

low plasticity, silty, iron oxide staining

moderate to high plasticity, iron oxide stainingand nodules

Bottom of borehole at 50.0 feet.

lean clay

fat clay

firm

firm

soft

hard

moist

moist

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fill

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DT22C-1

DT22C-2

DT22C-3

moderate plasticity, trace gravel, appreciableconcrete rubble

moderate plasticity, trace gravel, minor concreterubble

low plasticity, iron oxide staining, silty


fat clay

lean clay

firm

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moist

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(0-1') 12:30PID = 0.0

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(5-6')PID = 0.0

(6-7')PID = 0.1

(10-11')PID = 0.0(11-12')

PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra


NOTES Boring backfilled with bentonite

SURFACE Gravel




GROUND ELEVATION





STATIC WATER LEVEL Not measured





TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

moderate to high plasticity, trace gravel and wooddebris

low plasticity, iron oxide staining, silty, verticalroots

low plasticity, iron oxide staining, silty, verticalroots, carbon staining


fat clay

lean clay

firm

firm

moist

moist

brown

lightbrown

19

22

40

38

(0-1') 13:45PID = 0.0

(1-2')PID = 0.0

(5-6') 13:50PID = 0.0

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(12-13')PID = 0.0

(13-14')PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Gravel




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

moderate to high plasticity, trace sand, graveland brick rubble

moderate plasticity, 6'' of concrete @ 5'


fat clay

lean clay

hard

hard

moist

slightlymoist

brown

lightbrownish

gray

35

13

44

44

48

(0-1') 14:30PID = 0.0

(1-2')PID = 0.0

(2-3')PID = 0.0

(5-6')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(12-13')PID = 0.0

(13-14')PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

(20-21')PID = 0.0(21-22')

PID = 0.0

(22-23')PID = 0.0

(23-24')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20



SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


Peoria loess

Lovelandloess

DT22C-6

DT22C-7

DT22C-8

DT22C-9

DT22C-10


moderate to high plasticity, iron oxide staining,vertical root holes

moderate to high plasticity, iron oxide staining


lean clay

fat clay

lean clay

fat clay

hard

hard

slightlymoist

moist

lightbrown

gray

reddishbrown

brown

reddishbrown

60

60

34

23

47

(25-26')PID = 0.0(26-27')

PID = 0.0

(27-28')PID = 0.0

(28-29')PID = 0.0

(29-30')PID = 0.0

(30-31')PID = 0.0(31-32')

PID = 0.0

(32-33')PID = 0.0

(33-34')PID = 0.0

(34-35')PID = 0.0

(35-36') 15:15PID = 0.1(36-37')

PID = 0.0

(37-38')PID = 0.0

(40-41')PID = 0.0(41-42')

PID = 0.0

(45-46')PID = 0.0(46-47')

PID = 0.0

(47-48')PID = 0.0

(48-49')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

25

30

35

40

45

50


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

moderate to high plasticity, trace sand, gravel,and concrete rubble

moderate to high plasticity, trace brick rubble



fat clay

lean clay

hard

firm

moist

slightlymoist

brown

darkgray

brown

gray

lightbrown

23

16

26

(0-1') 8:45PID = 0.0

(1-2') 8:45PID = 0.3

(5-6')PID = 0.2

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

moderate to high plasticity, trace gravel andconcrete rubble, solvent odor

moderate to high plasticity, trace concrete rubble,slight solvent odor, black mottling

moderate to high plasticity, appreciable concreterubble, trace gravel, black mottling, wood debris

low plastcity, iron oxide staining, silty


fat clay

lean clay

fat clay

lean clay

hard

firm

hard

moist

slightlymoist

moist

slightlymoist

moist

slightlymoist

brownishgray

gray

brownishgray

lightbrown

lightbrown

35

32

32

44

49

(0-1') 9:00PID = 79.3

(1-2')PID = 4.7

(2-3')PID = 2.3

(5-6') 9:00PID = 0.3

(6-7')PID = 0.5

(7-8')PID = 0.4

(10-11')PID = 0.5(11-12')

PID = 0.2

(12-13')PID = 0.2

(15-16')PID = 0.1(16-17')

PID = 0.2

(17-18')PID = 0.1

(18-19')PID = 0.1

(20-21')PID = 0.0(21-22')

PID = 0.0

(22-23')PID = 0.0

(23-24')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20

25


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

moderate to high plasticity, trace gravel, traceconcrete and brick rubble

low plasticity, trace concrete and brick rubble

moderate to high plasticity, trace concrete andbrick rubble

6'' of concrete rubble with 1/2'' of CH

fat clay

lean clay

fat clay

hard

firm

soft

hard

slightlymoist

moist

slightlymoist

brown

grayishbrown

lightbrown

brown

darkbrown

46

24

44

48

6

(0-1') 10:00PID = 0.5

(1-2')PID = 0.0

(2-3')PID = 0.0

(3-4')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(12-13')PID = 0.0

(13-14')PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

(20-21')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20



SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


Peoria loess

DT22C-6

low plasticity, iron oxide staining


lean clayfirmmoist lightbrown

42

(25-26')PID = 0.0(26-27')

PID = 0.0

(27-28')PID = 0.0

(28-29')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

25

30


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

low plasticity, trace gravel and concrete rubble,iron oxide staining

low plasticity, trace concrete and brick rubble,trace sand

low to moderate plasticity, trace cinders, glass,and concrete

moderate to high plasticity, iron oxide staining,mottled, trace concrete rubble

moderate to high plasticity, trace concrete rubbleand wood debris, bottom 6'' concrete


lean clay

fat clay

hard

firm

hard

firm

moist brown

gray

darkbrown

brown

darkbrown

35

21

22

24

37

(0-1') 11:10PID = 0.3

(1-2')PID = 0.2

(2-3')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(10-11') 11:20PID = 0.0(11-12')

PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(20-21')PID = 0.0(21-22')

PID = 0.0

(22-23')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20

25


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

moderate to high plasticity, trace concrete rubble,wood debis

moderate to high plasticity, trace concrete rubble,wood debris, iron oxide staining, brown mottling

moderate to high plasticity, trace gravel

conrete rubble 18-19'

low plasticity, trace gravel and concrete rubble

fat clay

lean clay

firm

hard

soft

hard

soft

moist

verymoist

brown

gray

brown

32

21

26

42

16

(0-1') 12:30PID = 0.0

(1-2') 12:30PID = 0.0

(2-3')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

(20-21')PID = 0.0(21-22')

PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20



SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

Lovelandloess

DT22C-6

DT22C-7

DT22C-8

DT22C-9

DT22C-10

moderate to high plasticity, trace concrete rubble


moderate to high plasticity, iron oxide staining


fat clay

lean clay

fat clay

hard

hard

firm

soft

soft

firm

verymoist

moist

verymoist

moist

brown

lightbrown

reddishbrown

41

49

46

60

60

(25-26')PID = 0.0(26-27')

PID = 0.0

(27-28')PID = 0.0

(28-29')PID = 0.0

(30-31')PID = 0.0(31-32')

PID = 0.0

(32-33')PID = 0.0

(33-34')PID = 0.0

(35-36')PID = 0.0(36-37')

PID = 0.0

(37-38')PID = 0.0

(38-39')PID = 0.0

(40-41')PID = 0.0(41-42')

PID = 0.0

(42-43')PID = 0.0

(43-44')PID = 0.0

(44-45')PID = 0.0

(45-46')PID = 0.0(46-47')

PID = 0.0

(47-48')PID = 0.0

(48-49')PID = 0.0

(49-50')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

25

30

35

40

45

50


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Bare Ground




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


colluvium

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

low plasticity, vertical roots

low to moderate plasticity, vertical roots

low plasticity, homogenous

low plasticity, iron oxide staining, gray mottling


lean clay

fat clay

lean clay

firm

soft

soft

verymoist

moist

verymoist

wet

lightbrown

brown

lightbrown

lightbrown

29

26

33

55

(0-1') 12:40PID = 0.0

(1-2')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(12-13') 13:00PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

(19-20')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Grass




GROUND ELEVATION


END OF DRILLING 16.2 ft

DURING DRILLING 14.5 ft


STATIC WATER LEVEL 12.2 ft





TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

DT22C-1

DT22C-2

DT22C-2

DT22C-3

moderate to high plasticity, trace concrete gravel

moderate to high plasticity, trace gravel, wooddebris, horizontal roots

moderate to high plasticity, trace concrete,cinder, and galss rubble @ 11.5-12', mottled

moderate to high plasticity, minor cinders andglass, trace gravel, minor concrete rubble

Refusal at 19.0 feet.

fat clayhardslightlymoist

moist

brown

gray

brownishgray

darkbrownish

gray

27

28

47

44

(0-1')PID = 0.0

(1-2')PID = 0.0

(5-6')PID = 0.0

(6-7')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(12-13')PID = 0.0

(13-14')PID = 0.0

(15-16') 14:10PID = 0.0

(16-17') 14:10PID = 0.0

(17-18')PID = 0.0

(18-19')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Grass




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


fill

Peoria loess

DT22C-1

DT22C-2

DT22C-3

DT22C-4

DT22C-5

moderate to high plasticity, trace brick andconcrete rubble, trace sand and gravel,

low plasticity, trace concrete rubble

moderate to high plasticity, iron oxide staining,trace gravel

moderate to high plasticity, appreciable concreterubble, dark gray and brown mottling, trace

gravel

low plasticity, riable, silty, iron oxide staining,vertical roots

fat clay

lean clay

fat clay

lean clay

hard

soft

hard

moist

slightlymoist

brown

lightbrown

gray

lightbrown

31

11

24

27

44

(0-1')PID = 0.0

(1-2')PID = 0.0

(2-3')PID = 0.0

(5-6')PID = 0.0

(10-11')PID = 0.0(11-12')

PID = 0.0

(15-16')PID = 0.0(16-17')

PID = 0.0

(20-21') 14:40PID = 0.0(21-22')

PID = 0.0

(22-23')PID = 0.0

(23-24')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

0

5

10

15

20



SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

AP

HIC

LOG

CO

NS

IST

.

MO

IST

UR

E

CO

LOR

RE

CO

VE

RY

(IN





DRILLER Omar Ibarra



SURFACE Grass




GROUND ELEVATION










TG

EN

VIR

O L

OG

- G

INT

ST

D U

S L

AB

.GD

T -

1/9

/20

15:0

4 -

P:\

1963

1.0

1\B

OR

ING

LO

GS

.GP


Peoria loess

DT22C-6


lean clayfirmslightlymoist

lightbrown

60

(25-26')PID = 0.0(26-27')

PID = 0.0

(27-28')PID = 0.0

(28-29')PID = 0.0

(29-30')PID = 0.0

GE

OLO

GIC

OR

IGIN

DE

PT

H(f

t)

25

30


SA

MP

LE T

YP

EN

UM

BE

R

SAMPLE DATA

REMARKS

SO

IL T

YP

E

GR

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ANALYTICAL REPORTEurofins TestAmerica, Cedar Falls3019 Venture WayCedar Falls, IA 50613Tel: (319)277-2401

Laboratory Job ID: 310-172725-1Laboratory Sample Delivery Group: 19631.01Client Project/Site: Warehouse Property - Omaha, NE

For:Thiele Geotech Inc.13478 Chandler RoadOmaha, Nebraska 68138

Attn: Robert Miller

Authorized for release by:1/7/2020 1:49:13 PM

Angela Muehling, Project Manager II(319)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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..... ........ . LINKS ...... .... . .

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Table of Contents

Client: Thiele Geotech Inc.Project/Site: Warehouse Property - Omaha, NE

Laboratory Job ID: 310-172725-1SDG: 19631.01

Page 2 of 21Eurofins TestAmerica, Cedar Falls

1/7/2020

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

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Case NarrativeClient: Thiele Geotech Inc. Job ID: 310-172725-1Project/Site: Warehouse Property - Omaha, NE SDG: 19631.01

Job ID: 310-172725-1

Laboratory: Eurofins TestAmerica, Cedar Falls

Narrative

Job Narrative

310-172725-1

Comments

No additional comments.

Receipt

The sample was received on 12/24/2019 10:35 AM; the sample arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.7º C.

GC/MS VOA

Methods 8260C: The laboratory control sample (LCS) for analytical batch 310-265802 recovered outside control limits for the following analyte: sec-Butylbenzene. The analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data

have been reported.

Method 8260C: The continuing calibration verification (CCV) associated with batch 310-265802 recovered above the upper control limit for Xylenes, Total (22.2 %D), m,p-Xylene (22.1 %D), o-Xylene (22.3 %D), sec-Butylbenzene (28.1 %D), Bromochloromethane (21.4 %D), 1,3-Dichlorobenzene (22.8 %D), N-Propylbenzene (22.9 %D), Chlorodibromomethane (20.3 %D), tert-Butylbenzene (26.2 %D), Isopropylbenzene (23.3 %D), Tetrachloroethene 922.3 %D) and Bromobenzene (20.4 %D). The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCV 310-265802/4).

Methods 8260C: The following volatile sample was analyzed with significant headspace in the sample container(s): EB-10 (310-172725-1). Significant headspace is defined as a bubble greater than 6 mm in diameter.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Eurofins TestAmerica, Cedar FallsPage 3 of 21 1/7/2020

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Sample SummaryJob ID: 310-172725-1Client: Thiele Geotech Inc.

SDG: 19631.01Project/Site: Warehouse Property - Omaha, NE

Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID

310-172725-1 EB-10 Ground Water 12/23/19 10:30 12/24/19 10:35

Eurofins TestAmerica, Cedar Falls

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Detection SummaryJob ID: 310-172725-1Client: Thiele Geotech Inc.


Client Sample ID: EB-10 Lab Sample ID: 310-172725-1

No Detections.


This Detection Summary does not include radiochemical test results.

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Client Sample ResultsJob ID: 310-172725-1Client: Thiele Geotech Inc.


Lab Sample ID: 310-172725-1Client Sample ID: EB-10Matrix: Ground WaterDate Collected: 12/23/19 10:30

Date Received: 12/24/19 10:35

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

Acetone <10.0 10.0 ug/L 12/27/19 14:57 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

0.500 ug/L 12/27/19 14:57 1Benzene <0.500

1.00 ug/L 12/27/19 14:57 1Bromobenzene <1.00

5.00 ug/L 12/27/19 14:57 1Bromochloromethane <5.00

1.00 ug/L 12/27/19 14:57 1Bromodichloromethane <1.00

5.00 ug/L 12/27/19 14:57 1Bromoform <5.00

4.00 ug/L 12/27/19 14:57 1Bromomethane <4.00

10.0 ug/L 12/27/19 14:57 12-Butanone (MEK) <10.0

1.00 ug/L 12/27/19 14:57 1n-Butylbenzene <1.00

1.00 ug/L 12/27/19 14:57 1sec-Butylbenzene <1.00 *

1.00 ug/L 12/27/19 14:57 1tert-Butylbenzene <1.00

1.00 ug/L 12/27/19 14:57 1Carbon disulfide <1.00

2.00 ug/L 12/27/19 14:57 1Carbon tetrachloride <2.00

1.00 ug/L 12/27/19 14:57 1Chlorobenzene <1.00

5.00 ug/L 12/27/19 14:57 1Chlorodibromomethane <5.00

4.00 ug/L 12/27/19 14:57 1Chloroethane <4.00

3.00 ug/L 12/27/19 14:57 1Chloroform <3.00

3.00 ug/L 12/27/19 14:57 1Chloromethane <3.00

1.00 ug/L 12/27/19 14:57 12-Chlorotoluene <1.00

1.00 ug/L 12/27/19 14:57 14-Chlorotoluene <1.00

5.00 ug/L 12/27/19 14:57 11,2-Dibromo-3-Chloropropane <5.00

1.00 ug/L 12/27/19 14:57 11,2-Dibromoethane (EDB) <1.00

1.00 ug/L 12/27/19 14:57 1Dibromomethane <1.00

1.00 ug/L 12/27/19 14:57 11,2-Dichlorobenzene <1.00



3.00 ug/L 12/27/19 14:57 1Dichlorodifluoromethane <3.00

1.00 ug/L 12/27/19 14:57 11,1-Dichloroethane <1.00

1.00 ug/L 12/27/19 14:57 11,2-Dichloroethane <1.00

2.00 ug/L 12/27/19 14:57 11,1-Dichloroethene <2.00

1.00 ug/L 12/27/19 14:57 1cis-1,2-Dichloroethene <1.00

1.00 ug/L 12/27/19 14:57 1trans-1,2-Dichloroethene <1.00

1.00 ug/L 12/27/19 14:57 11,2-Dichloropropane <1.00



1.00 ug/L 12/27/19 14:57 11,1-Dichloropropene <1.00

5.00 ug/L 12/27/19 14:57 1cis-1,3-Dichloropropene <5.00

5.00 ug/L 12/27/19 14:57 1trans-1,3-Dichloropropene <5.00

1.00 ug/L 12/27/19 14:57 1Ethylbenzene <1.00

5.00 ug/L 12/27/19 14:57 1Hexachlorobutadiene <5.00

1.00 ug/L 12/27/19 14:57 1Hexane <1.00

1.00 ug/L 12/27/19 14:57 1Isopropylbenzene <1.00

1.00 ug/L 12/27/19 14:57 1p-Isopropyltoluene <1.00

5.00 ug/L 12/27/19 14:57 1Methylene Chloride <5.00

1.00 ug/L 12/27/19 14:57 1Methyl tert-butyl ether <1.00

5.00 ug/L 12/27/19 14:57 1Naphthalene <5.00

1.00 ug/L 12/27/19 14:57 1N-Propylbenzene <1.00

1.00 ug/L 12/27/19 14:57 1Styrene <1.00

1.00 ug/L 12/27/19 14:57 11,1,1,2-Tetrachloroethane <1.00


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Lab Sample ID: 310-172725-1Client Sample ID: EB-10Matrix: Ground WaterDate Collected: 12/23/19 10:30


Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)RL MDL

1,1,2,2-Tetrachloroethane <1.00 1.00 ug/L 12/27/19 14:57 1


1.00 ug/L 12/27/19 14:57 1Tetrachloroethene <1.00

1.00 ug/L 12/27/19 14:57 1Toluene <1.00

5.00 ug/L 12/27/19 14:57 11,2,3-Trichlorobenzene <5.00

5.00 ug/L 12/30/19 19:35 11,2,4-Trichlorobenzene <5.00

1.00 ug/L 12/27/19 14:57 11,1,1-Trichloroethane <1.00

1.00 ug/L 12/27/19 14:57 11,1,2-Trichloroethane <1.00

1.00 ug/L 12/27/19 14:57 1Trichloroethene <1.00

4.00 ug/L 12/27/19 14:57 1Trichlorofluoromethane <4.00

1.00 ug/L 12/27/19 14:57 11,2,3-Trichloropropane <1.00

1.00 ug/L 12/27/19 14:57 11,2,4-Trimethylbenzene <1.00

1.00 ug/L 12/27/19 14:57 11,3,5-Trimethylbenzene <1.00

1.00 ug/L 12/27/19 14:57 1Vinyl chloride <1.00

3.00 ug/L 12/27/19 14:57 1Xylenes, Total <3.00

4-Bromofluorobenzene (Surr) 94 80 - 120 12/27/19 14:57 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 96 12/30/19 19:35 180 - 120

Dibromofluoromethane (Surr) 103 12/27/19 14:57 180 - 120

Dibromofluoromethane (Surr) 96 12/30/19 19:35 180 - 120

Toluene-d8 (Surr) 99 12/27/19 14:57 180 - 120

Toluene-d8 (Surr) 99 12/30/19 19:35 180 - 120

Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)RL MDL

Diesel <319 319 ug/L 12/30/19 10:44 01/06/20 12:50 1


319 ug/L 12/30/19 10:44 01/06/20 12:50 1Gasoline <319

319 ug/L 12/30/19 10:44 01/06/20 12:50 1Waste Oil <319

532 ug/L 12/30/19 10:44 01/06/20 12:50 1Total Extractable Hydrocarbons <532

n-Octacosane 68 32 - 148 12/30/19 10:44 01/06/20 12:50 1



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Definitions/GlossaryJob ID: 310-172725-1Client: Thiele Geotech Inc.


Qualifiers

GC/MS VOAQualifier Description

* LCS or LCSD is outside acceptance limits.

Qualifier

GlossaryThese commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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Surrogate SummaryJob ID: 310-172725-1Client: Thiele Geotech Inc.


Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Ground Water

Lab Sample ID Client Sample ID (80-120) (80-120) (80-120)

BFB DBFM TOL

94 103 99310-172725-1

Percent Surrogate Recovery (Acceptance Limits)

EB-10

96 96 99310-172725-1 EB-10

Surrogate Legend

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

TOL = Toluene-d8 (Surr)

Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Water


BFB DBFM TOL

92 105 103LCS 310-265802/6


Lab Control Sample

93 102 103LCS 310-265802/7 Lab Control Sample

102 101 98LCS 310-266165/5 Lab Control Sample

95 105 102MB 310-265802/8 Method Blank

99 94 98MB 310-266165/7 Method Blank

Surrogate Legend




Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)Prep Type: Total/NAMatrix: Ground Water

Lab Sample ID Client Sample ID (32-148)

OTCN

68310-172725-1


EB-10

Surrogate Legend

OTCN = n-Octacosane

Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)Prep Type: Total/NAMatrix: Water


OTCN

99LCS 310-266249/2-A


Lab Control Sample

71LCSD 310-266249/3-A Lab Control Sample Dup

73MB 310-266249/1-A Method Blank

Surrogate Legend

OTCN = n-Octacosane


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QC Sample ResultsJob ID: 310-172725-1Client: Thiele Geotech Inc.


Method: 8260C - Volatile Organic Compounds by GC/MS

Client Sample ID: Method BlankLab Sample ID: MB 310-265802/8Matrix: Water Prep Type: Total/NAAnalysis Batch: 265802

RL MDL

Acetone <10.0 10.0 ug/L 12/27/19 08:09 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

<0.500 0.500 ug/L 12/27/19 08:09 1Benzene

<1.00 1.00 ug/L 12/27/19 08:09 1Bromobenzene

<5.00 5.00 ug/L 12/27/19 08:09 1Bromochloromethane

<1.00 1.00 ug/L 12/27/19 08:09 1Bromodichloromethane

<5.00 5.00 ug/L 12/27/19 08:09 1Bromoform

<4.00 4.00 ug/L 12/27/19 08:09 1Bromomethane

<10.0 10.0 ug/L 12/27/19 08:09 12-Butanone (MEK)

<1.00 1.00 ug/L 12/27/19 08:09 1n-Butylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1sec-Butylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1tert-Butylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1Carbon disulfide

<2.00 2.00 ug/L 12/27/19 08:09 1Carbon tetrachloride

<1.00 1.00 ug/L 12/27/19 08:09 1Chlorobenzene

<5.00 5.00 ug/L 12/27/19 08:09 1Chlorodibromomethane

<4.00 4.00 ug/L 12/27/19 08:09 1Chloroethane

<3.00 3.00 ug/L 12/27/19 08:09 1Chloroform

<3.00 3.00 ug/L 12/27/19 08:09 1Chloromethane

<1.00 1.00 ug/L 12/27/19 08:09 12-Chlorotoluene

<1.00 1.00 ug/L 12/27/19 08:09 14-Chlorotoluene

<5.00 5.00 ug/L 12/27/19 08:09 11,2-Dibromo-3-Chloropropane

<1.00 1.00 ug/L 12/27/19 08:09 11,2-Dibromoethane (EDB)

<1.00 1.00 ug/L 12/27/19 08:09 1Dibromomethane

<1.00 1.00 ug/L 12/27/19 08:09 11,2-Dichlorobenzene



<3.00 3.00 ug/L 12/27/19 08:09 1Dichlorodifluoromethane

<1.00 1.00 ug/L 12/27/19 08:09 11,1-Dichloroethane

<1.00 1.00 ug/L 12/27/19 08:09 11,2-Dichloroethane

<2.00 2.00 ug/L 12/27/19 08:09 11,1-Dichloroethene

<1.00 1.00 ug/L 12/27/19 08:09 1cis-1,2-Dichloroethene

<1.00 1.00 ug/L 12/27/19 08:09 1trans-1,2-Dichloroethene

<1.00 1.00 ug/L 12/27/19 08:09 11,2-Dichloropropane



<1.00 1.00 ug/L 12/27/19 08:09 11,1-Dichloropropene

<5.00 5.00 ug/L 12/27/19 08:09 1cis-1,3-Dichloropropene

<5.00 5.00 ug/L 12/27/19 08:09 1trans-1,3-Dichloropropene

<1.00 1.00 ug/L 12/27/19 08:09 1Ethylbenzene

<5.00 5.00 ug/L 12/27/19 08:09 1Hexachlorobutadiene

<1.00 1.00 ug/L 12/27/19 08:09 1Hexane

<1.00 1.00 ug/L 12/27/19 08:09 1Isopropylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1p-Isopropyltoluene

<5.00 5.00 ug/L 12/27/19 08:09 1Methylene Chloride

<1.00 1.00 ug/L 12/27/19 08:09 1Methyl tert-butyl ether

<5.00 5.00 ug/L 12/27/19 08:09 1Naphthalene

<1.00 1.00 ug/L 12/27/19 08:09 1N-Propylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1Styrene


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Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)


RL MDL

1,1,1,2-Tetrachloroethane <1.00 1.00 ug/L 12/27/19 08:09 1

MB MB


<1.00 1.00 ug/L 12/27/19 08:09 11,1,2,2-Tetrachloroethane

<1.00 1.00 ug/L 12/27/19 08:09 1Tetrachloroethene

<1.00 1.00 ug/L 12/27/19 08:09 1Toluene

<5.00 5.00 ug/L 12/27/19 08:09 11,2,3-Trichlorobenzene

<1.00 1.00 ug/L 12/27/19 08:09 11,1,1-Trichloroethane

<1.00 1.00 ug/L 12/27/19 08:09 11,1,2-Trichloroethane

<1.00 1.00 ug/L 12/27/19 08:09 1Trichloroethene

<4.00 4.00 ug/L 12/27/19 08:09 1Trichlorofluoromethane

<1.00 1.00 ug/L 12/27/19 08:09 11,2,3-Trichloropropane

<1.00 1.00 ug/L 12/27/19 08:09 11,2,4-Trimethylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 11,3,5-Trimethylbenzene

<1.00 1.00 ug/L 12/27/19 08:09 1Vinyl chloride

<3.00 3.00 ug/L 12/27/19 08:09 1Xylenes, Total


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

105 12/27/19 08:09 1Dibromofluoromethane (Surr) 80 - 120

102 12/27/19 08:09 1Toluene-d8 (Surr) 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-265802/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 265802

Acetone 40.0 37.97 ug/L 95 50 - 150

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Benzene 20.0 20.87 ug/L 104 77 - 120

Bromobenzene 20.0 22.32 ug/L 112 70 - 120

Bromochloromethane 20.0 24.61 ug/L 123 73 - 132

Bromodichloromethane 20.0 21.40 ug/L 107 73 - 120

Bromoform 20.0 16.88 ug/L 84 57 - 120

2-Butanone (MEK) 40.0 39.32 ug/L 98 50 - 150

n-Butylbenzene 20.0 20.05 ug/L 100 63 - 120

sec-Butylbenzene 20.0 24.24 * ug/L 121 64 - 120

tert-Butylbenzene 20.0 23.29 ug/L 116 64 - 120

Carbon disulfide 20.0 14.65 ug/L 73 65 - 122

Carbon tetrachloride 20.0 20.65 ug/L 103 72 - 126

Chlorobenzene 20.0 22.09 ug/L 110 74 - 120

Chlorodibromomethane 20.0 21.37 ug/L 107 66 - 120

Chloroform 20.0 22.31 ug/L 112 78 - 121

2-Chlorotoluene 20.0 22.62 ug/L 113 71 - 120

4-Chlorotoluene 20.0 22.69 ug/L 113 71 - 120

1,2-Dibromo-3-Chloropropane 20.0 15.60 ug/L 78 50 - 150

1,2-Dibromoethane (EDB) 20.0 20.78 ug/L 104 71 - 125

Dibromomethane 20.0 22.64 ug/L 113 76 - 125

1,2-Dichlorobenzene 20.0 20.04 ug/L 100 66 - 120




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1,1-Dichloroethane 20.0 21.16 ug/L 106 75 - 125

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,2-Dichloroethane 20.0 21.27 ug/L 106 75 - 123

1,1-Dichloroethene 20.0 16.68 ug/L 83 75 - 124

cis-1,2-Dichloroethene 20.0 21.11 ug/L 106 77 - 120

trans-1,2-Dichloroethene 20.0 18.73 ug/L 94 75 - 122

1,2-Dichloropropane 20.0 22.71 ug/L 114 75 - 123



1,1-Dichloropropene 20.0 20.60 ug/L 103 77 - 124

cis-1,3-Dichloropropene 20.0 20.96 ug/L 105 70 - 120

trans-1,3-Dichloropropene 20.0 20.66 ug/L 103 69 - 120

Ethylbenzene 20.0 22.20 ug/L 111 73 - 120

Hexachlorobutadiene 20.0 21.05 ug/L 105 50 - 150

Hexane 20.0 20.28 ug/L 101 50 - 150

Isopropylbenzene 20.0 23.06 ug/L 115 69 - 120

p-Isopropyltoluene 20.0 21.05 ug/L 105 68 - 120

Methylene Chloride 20.0 20.50 ug/L 103 50 - 150

Methyl tert-butyl ether 20.0 19.96 ug/L 100 72 - 121

Naphthalene 20.0 11.05 ug/L 55 50 - 150

N-Propylbenzene 20.0 23.32 ug/L 117 70 - 120

Styrene 20.0 21.90 ug/L 109 70 - 120

1,1,1,2-Tetrachloroethane 20.0 20.21 ug/L 101 72 - 120

1,1,2,2-Tetrachloroethane 20.0 18.67 ug/L 93 63 - 122

Tetrachloroethene 20.0 24.48 ug/L 122 72 - 129

Toluene 20.0 23.49 ug/L 117 74 - 120

1,2,3-Trichlorobenzene 20.0 13.65 ug/L 68 50 - 150

1,1,1-Trichloroethane 20.0 20.83 ug/L 104 76 - 127

1,1,2-Trichloroethane 20.0 23.86 ug/L 119 69 - 127

Trichloroethene 20.0 20.06 ug/L 100 77 - 123

1,2,3-Trichloropropane 20.0 19.06 ug/L 95 66 - 120

1,2,4-Trimethylbenzene 20.0 21.57 ug/L 108 67 - 120

1,3,5-Trimethylbenzene 20.0 22.49 ug/L 112 68 - 120

Xylenes, Total 40.0 45.80 ug/L 115 69 - 120

4-Bromofluorobenzene (Surr) 80 - 120

Surrogate

92

LCS LCS

Qualifier Limits%Recovery

105Dibromofluoromethane (Surr) 80 - 120

103Toluene-d8 (Surr) 80 - 120


Bromomethane 20.0 11.72 ug/L 59 38 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Chloroethane 20.0 20.75 ug/L 104 69 - 129

Chloromethane 20.0 19.67 ug/L 98 50 - 150

Dichlorodifluoromethane 20.0 18.72 ug/L 94 50 - 150


Page 12 of 21 1/7/2020

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Trichlorofluoromethane 20.0 20.81 ug/L 104 68 - 146

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Vinyl chloride 20.0 19.80 ug/L 99 67 - 133


Surrogate

93

LCS LCS





RL MDL

1,2,4-Trichlorobenzene <5.00 5.00 ug/L 12/30/19 18:06 1

MB MB



MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

94 12/30/19 18:06 1Dibromofluoromethane (Surr) 80 - 120

98 12/30/19 18:06 1Toluene-d8 (Surr) 80 - 120


1,2,4-Trichlorobenzene 20.0 17.71 ug/L 89 59 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

102

LCS LCS




Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)

Client Sample ID: Method BlankLab Sample ID: MB 310-266249/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 266450 Prep Batch: 266249

RL MDL

Diesel <300 300 ug/L 12/30/19 10:44 01/06/20 08:24 1

MB MB


<300 300 ug/L 12/30/19 10:44 01/06/20 08:24 1Gasoline

<300 300 ug/L 12/30/19 10:44 01/06/20 08:24 1Waste Oil

<500 500 ug/L 12/30/19 10:44 01/06/20 08:24 1Total Extractable Hydrocarbons

n-Octacosane 73 32 - 148 01/06/20 08:24 1

MB MB

Surrogate

12/30/19 10:44

Dil FacPrepared AnalyzedQualifier Limits%Recovery


Page 13 of 21 1/7/2020

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Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-266249/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 266450 Prep Batch: 266249

Diesel 2000 1635 ug/L 82 17 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

n-Octacosane 32 - 148

Surrogate

99

LCS LCS


Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 310-266249/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 266450 Prep Batch: 266249

Diesel 2000 1248 ug/L 62 17 - 120 27 35

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

71

LCSD LCSD



Page 14 of 21 1/7/2020

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QC Association SummaryJob ID: 310-172725-1Client: Thiele Geotech Inc.


GC/MS VOA

Analysis Batch: 265802

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Ground Water 8260C310-172725-1 EB-10 Total/NA

Water 8260CMB 310-265802/8 Method Blank Total/NA

Water 8260CLCS 310-265802/6 Lab Control Sample Total/NA





Water 8260CMB 310-266165/7 Method Blank Total/NA


GC Semi VOA

Prep Batch: 266249



Water 3510CMB 310-266249/1-A Method Blank Total/NA

Water 3510CLCS 310-266249/2-A Lab Control Sample Total/NA

Water 3510CLCSD 310-266249/3-A Lab Control Sample Dup Total/NA



Ground Water OA-2 266249310-172725-1 EB-10 Total/NA

Water OA-2 266249MB 310-266249/1-A Method Blank Total/NA

Water OA-2 266249LCS 310-266249/2-A Lab Control Sample Total/NA

Water OA-2 266249LCSD 310-266249/3-A Lab Control Sample Dup Total/NA


Page 15 of 21 1/7/2020

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Lab ChronicleClient: Thiele Geotech Inc. Job ID: 310-172725-1Project/Site: Warehouse Property - Omaha, NE SDG: 19631.01

Client Sample ID: EB-10 Lab Sample ID: 310-172725-1Matrix: Ground WaterDate Collected: 12/23/19 10:30


Analysis 8260C 12/27/19 14:57 SJN1 265802 TAL CF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 266165 12/30/19 19:35 SJN TAL CFTotal/NA

Prep 3510C 266249 12/30/19 10:44 NRH TAL CFTotal/NA

Analysis OA-2 1 266450 01/06/20 12:50 JTA TAL CFTotal/NA

Laboratory References:

TAL CF = Eurofins TestAmerica, Cedar Falls, 3019 Venture Way, Cedar Falls, IA 50613, TEL (319)277-2401


Page 16 of 21 1/7/2020

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Accreditation/Certification SummaryClient: Thiele Geotech Inc. Job ID: 310-172725-1Project/Site: Warehouse Property - Omaha, NE SDG: 19631.01

Laboratory: Eurofins TestAmerica, Cedar FallsThe accreditations/certifications listed below are applicable to this report.

Authority Program Identification Number Expiration Date

Oregon IA100001NELAP 09-29-20


Page 17 of 21 1/7/2020

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[----------

Method SummaryJob ID: 310-172725-1Client: Thiele Geotech Inc.


Method Method Description LaboratoryProtocol

SW8468260C Volatile Organic Compounds by GC/MS TAL CF

Iowa DNROA-2 Iowa - Extractable Petroleum Hydrocarbons (GC) TAL CF

SW8463510C Liquid-Liquid Extraction (Separatory Funnel) TAL CF

SW8465030B Purge and Trap TAL CF

Protocol References:

Iowa DNR = Iowa Department of Natural Resources

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.




Page 18 of 21 1/7/2020

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Page 19 of 21 1/7/2020

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:;; eurofins Environment Testing TestAmerica

310-172725 Chain of Custody

Cooler/Sample Receipt and Temperature Log Form Client Information

' I

Client: ~" \ e_\~ ~ "0 \-e.c,,h City/State:

I CITY

I CS> i/V'--~"'- (A,__ : ST;J (_,, j Project:

Receipt Information . . D t fT' R . d ! DATE '/ C, a e ,me ece1ve :

1 I~/ ILL/ I l TIME < I

1 I u J Received By: e><---

. , '

Delivery Type: □ UPS ~x D FedEx Ground □ US Mail D Spee-Dee

D Lab Courier D Lab Field Services D Client Drop-off D Other:

Condition of Cooler/Containers -Sample(s) received in Cooler? 1:JYes □ No If yes: Cooler ID:

Multiple Coolers? □ Yes ,flNo If yes: Cooler# __ of __

Cooler Custody Seals Present? .[].-¥es □ No If yes: Cooler custody seals intact? flYes □ No

Sample Custody Seals Present? □ Yes .e:JNo If yes: Sample custody seals intact?□ Yes □ No

Trip Blank Present? □ Yes rJNo If yes: Which VOA samples are in cooler? !

Temoerature Record

Coolant: ...E:]Wetice D Blue ice D Dry ice D Other: □ NONE

Thermometer ID: c? j Correction Factor (°C): }-Cl / I • Temp Blank Temserature - If no temp blan!c, or temp blank temperature above criteria, proceed to Sample Container Temperature

Uncorrected Temp (0 C): l. VLJ; j Corrected Temp (°C): 'l_ . , • Sample Container Temoerature

CONTAINER 1 CONTAINER 2 Container(s) used:

Uncorrected Temp (0 C):

Corrected Temp (0 C):

Exceptions Noted -. ~ ·-J.

1) If temperature exceeds criteria, was sample(s) received same day of sampling? □ Yes □ No a) If yes: Is there evidence that the chilling process began? □ Yes □ No

2) If temperature is <0°C, are there obvious signs that the integrity of sample containers is compromised? (e.g ., bulging septa, broken/cracked bottles, frozen solid?) □ Yes □ No

NOTE: If ves, contact PM before oroceedina. If no, proceed with login Additional Comments ·:

. Document: CF-LG-Wl-002 Revision: 25 Date: 06/17/2019 Eurofins TestAmerica, Cedar Falls

General temperature criteria is Oto 6°C Bacteria temperature criteria is Oto 1o·c

Page 20 of 21

1/7/2020

123456789101112131415

Cedar Falls 704 Enterprise Drive

Cedar Falls, IA 50613

phone 319.277.2401 fax 319.277 .2425

Client Contact

Thiele Geotech, Inc.

13478 Chandler Road

Omaha, NE 68138

402.556.2171

402.556.7831

Project Name: Warehouse Property

7502 Crown Poinl Ave , Omaha, NE

PO#

Sample Identification

EB-10

Chain of Custody Record

Project Manager: Robert Miller Site Contact: Jeremy Kendle

Tel/Fax: Lab Contact:

Analysis Turnaround Time

Calendar ( C) or Work Days (W) ~

TATifdifferentfromBetow ~ ~ D

2weeks ~ :;;:

I week S .. D <

~

D 2 days u u ~ .. 0 m < D I day i5.. > u ;:: E

"' .. .. :i: ...

(I) c:, N r-.,, [.:I

'° 00 oi!! ;,. N 0

Sample Sample Sample ~ N 00 .. "' # of ~ < < < =!

Date Time Type Matrix Cont. i.: .. .. c:,

0 '-l '-l '° 12/23/20 19 10:30 Grab GW 5

X X

Test America THE LEADER IN ENVIRONMENTAL TESTING

TestAmerica Laboratories, Inc.

Date: 12123 / 19 COC No:

Carrier: _I_ of _I_ COCs

Job No. 19631.01

SDG No.

Sample Specific Notes:

Prcservation&sed: 1; I~; HCI; ) ; I-12SO4; 4; HNO3; S;NaOH; 6; Other

Possible Hazard lde11tificatio11 Jfu Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)

D Non-Hazard D F/a111111able D Skin Irritant Poison B D Unknown D Return To Client ~posal By Lab D Archive For Months

Special Instructions/QC Requirements & Comments:

~ ./~

Relinquishezy~ 7k ,/_ Ftfr· Daterrirnefl,t T ~eANJ;tf !Yl1uffi/jh Com_p~: ,, 0

l:J1)()/;9 /05§' c.(t. (7eo~e~L J]. :10 t Tffr ~-Relinquishp·: (

, Company: Dateffirne: Rel!'eived b)j C Company: Dateffime:

Reli nquished by: Company: Daterrime: Received by: Company: Daterfime:

Login Sample Receipt Checklist

Client: Thiele Geotech Inc. Job Number: 310-172725-1

SDG Number: 19631.01

Login Number: 172725

Question Answer Comment

Creator: Lickness, Corina A

List Source: Eurofins TestAmerica, Cedar Falls

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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ANALYTICAL REPORTEurofins TestAmerica, Cedar Falls3019 Venture WayCedar Falls, IA 50613Tel: (319)277-2401

Laboratory Job ID: 310-172445-1Laboratory Sample Delivery Group: 19631.01Client Project/Site: Warehouse Property

For:Thiele Geotech Inc.13478 Chandler RoadOmaha, Nebraska 68138

Attn: Robert Miller

Authorized for release by:1/8/2020 3:45:49 PM

Angela Muehling, Project Manager II(319)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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..... ........ . LINKS ...... .... . .

Review your project results through

TotdAccess • ? Have a Question.

~

k The Ex ert

Visit us at: www.testamericainc.com

_;~ eu rofi ns Environment Testing TestAmerica

■

https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/services-we-offer/ask-the-expert

http://www.testamericainc.com

mailto:[email protected]

Table of Contents

Client: Thiele Geotech Inc.Project/Site: Warehouse Property

Laboratory Job ID: 310-172445-1SDG: 19631.01

Page 2 of 81Eurofins TestAmerica, Cedar Falls

1/8/2020

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 64

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

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Case NarrativeClient: Thiele Geotech Inc. Job ID: 310-172445-1Project/Site: Warehouse Property SDG: 19631.01

Job ID: 310-172445-1

Laboratory: Eurofins TestAmerica, Cedar Falls

Narrative

Job Narrative

310-172445-1

Comments

No additional comments.

Receipt

The samples were received on 12/19/2019 10:05 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 5.7º C.

GC/MS VOA

Method 8260D: The continuing calibration verification (CCV) associated with batch 310-266187 recovered above the upper control limit for Carbon tetrachloride(21.0%D). The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have

been reported. The following sample is impacted: (CCV 310-266187/3).

Method 8260D: The continuing calibration verification (CCV) associated with batch 310-266187 recovered above the upper control limit for Chloroethane(33.3%D) and Trichlorofluoromethane(23.7%D). The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCV 310-266187/4).


GC Semi VOA Method OA-2: Surrogate recovery for the following samples were outside control limits: EB-1 (0-1) (310-172445-1), EB-2 (0-1) (310-172445-2), EB-8 (0-1) (310-172445-12), (310-172445-B-1-F MS) and (310-172445-B-1-G MSD). Evidence of matrix interference is

present; therefore, re-extraction and/or re-analysis was not performed.


Metals

Methods 6010C: The following samples were diluted due to the presence of an interferent: EB-1 (0-1) (310-172445-1), EB-2 (0-1) (310-172445-2), EB-3 (0-1) (310-172445-3), EB-4 (0-1) (310-172445-5), EB-5 (0-1) (310-172445-7), EB-9 (0-1) (310-172445-14), EB-10 (0-1) (310-172445-16) and EB-12 (20-21) (310-172445-20). Elevated reporting limits (RLs) are provided.


General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.


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Sample SummaryJob ID: 310-172445-1Client: Thiele Geotech Inc.

SDG: 19631.01Project/Site: Warehouse Property

Lab Sample ID Client Sample ID ReceivedCollectedMatrix Asset ID

310-172445-1 EB-1 (0-1) Soil 12/16/19 10:30 12/19/19 10:05

310-172445-2 EB-2 (0-1) Soil 12/16/19 12:30 12/19/19 10:05

310-172445-3 EB-3 (0-1) Soil 12/16/19 13:45 12/19/19 10:05

310-172445-4 EB-3 (5-6) Soil 12/16/19 13:50 12/19/19 10:05

310-172445-5 EB-4 (0-1) Soil 12/16/19 14:30 12/19/19 10:05

310-172445-6 EB-4 (35-36) Soil 12/16/19 15:15 12/19/19 10:05

310-172445-7 EB-5 (0-1) Soil 12/17/19 08:45 12/19/19 10:05

310-172445-8 EB-5 (1-2) Soil 12/17/19 08:45 12/19/19 10:05

310-172445-9 EB-6 (0-1) Soil 12/17/19 09:00 12/19/19 10:05

310-172445-10 EB-6 (5-6) Soil 12/17/19 09:00 12/19/19 10:05

310-172445-11 EB-7 (0-1) Soil 12/17/19 10:00 12/19/19 10:05

310-172445-12 EB-8 (0-1) Soil 12/17/19 11:10 12/19/19 10:05

310-172445-13 EB-8 (10-11) Soil 12/17/19 11:20 12/19/19 10:05

310-172445-14 EB-9 (0-1) Soil 12/17/19 12:30 12/19/19 10:05

310-172445-15 EB-9 (1-2) Soil 12/17/19 12:30 12/19/19 10:05

310-172445-16 EB-10 (0-1) Soil 12/18/19 12:40 12/19/19 10:05

310-172445-17 EB-10 (12-13) Soil 12/18/19 13:00 12/19/19 10:05

310-172445-18 EB-11 (15-16) Soil 12/17/19 14:10 12/19/19 10:05

310-172445-19 EB-11 (16-17) Soil 12/17/19 14:10 12/19/19 10:05

310-172445-20 EB-12 (20-21) Soil 12/17/19 14:40 12/19/19 10:05


Page 4 of 81 1/8/2020

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Client Sample ID: EB-1 (0-1) Lab Sample ID: 310-172445-1

Waste Oil

RL

38.9 mg/Kg

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA46150 OA-2

☼Arsenic 10.3 mg/Kg Total/NA311.3 6010C

☼Barium 2.57 mg/Kg Total/NA3210 F1 F2 6010C

☼Chromium 2.57 mg/Kg Total/NA318.8 6010C

☼Lead 12.8 mg/Kg Total/NA324.8 6010C

☼Mercury 0.0211 mg/Kg Total/NA10.0331 7471B


☼PCB-1254

RL

3.00 mg/Kg


Total/NA509.06 8082A

Waste Oil 9.52 mg/Kg Total/NA11250 OA-2


☼Barium 1.91 mg/Kg Total/NA2215 6010C





☼Arsenic

RL

7.82 mg/Kg


Total/NA212.0 6010C






Waste Oil

RL

9.54 mg/Kg


Total/NA1121 OA-2


☼Barium

RL

5.96 mg/Kg


Total/NA7125 6010C



No Detections.


☼Arsenic

RL

7.12 mg/Kg


Total/NA219.6 6010C



☼Lead 8.90 mg/Kg Total/NA2478 6010C



Waste Oil

RL

9.77 mg/Kg


Total/NA1283 OA-2



Page 5 of 81 1/8/2020

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-----------

-----------

-----------

[-----------

[-----------[

-----------

[-----------




☼Ethylbenzene

RL

136 ug/Kg


Total/NA1137 8260D

☼Isopropylbenzene 136 ug/Kg Total/NA1458 8260D

☼Naphthalene 341 ug/Kg Total/NA1605 8260D

☼n-Butylbenzene 136 ug/Kg Total/NA12710 F1 8260D

☼n-Propylbenzene 136 ug/Kg Total/NA1674 8260D

☼p-Isopropyltoluene 136 ug/Kg Total/NA11000 F1 8260D

☼sec-Butylbenzene 136 ug/Kg Total/NA11370 F1 8260D

☼1,2,4-Trimethylbenzene 136 ug/Kg Total/NA14730 F1 8260D

☼1,3,5-Trimethylbenzene 136 ug/Kg Total/NA12290 F1 8260D

☼Xylenes, Total 204 ug/Kg Total/NA13110 F1 8260D

Diesel 9.76 mg/Kg Total/NA12190 OA-2


☼Arsenic

RL

3.65 mg/Kg


Total/NA16.77 6010C





Waste Oil

RL

9.65 mg/Kg


Total/NA145.9 OA-2







Waste Oil

RL

96.6 mg/Kg


Total/NA1016100 OA-2


☼Arsenic

RL

3.29 mg/Kg


Total/NA17.62 6010C





☼Arsenic

RL

7.51 mg/Kg


Total/NA213.2 6010C







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------------

------------

------------

[------------

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Waste Oil

RL

9.52 mg/Kg


Total/NA124.0 OA-2


☼Arsenic

RL

7.64 mg/Kg


Total/NA29.52 6010C






No Detections.


Waste Oil

RL

9.89 mg/Kg


Total/NA1168 OA-2


☼Arsenic

RL

3.92 mg/Kg


Total/NA113.7 6010C






Waste Oil

RL

9.59 mg/Kg


Total/NA1158 OA-2








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[-------------

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[

[-------------

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Lab Sample ID: 310-172445-1Client Sample ID: EB-1 (0-1)Matrix: SoilDate Collected: 12/16/19 10:30

Percent Solids: 84.4Date Received: 12/19/19 10:05

Method: 8260D - Volatile Organic Compounds by GC/MSRL MDL

Acetone <130 F1 130 ug/Kg ☼ 12/20/19 05:43 12/20/19 08:51 1


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Benzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Bromobenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Bromochloromethane <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Bromodichloromethane <13.0

25.9 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Bromoform <25.9

51.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Bromomethane <51.8

130 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼2-Butanone (MEK) <130

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Carbon disulfide <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Carbon tetrachloride <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Chlorobenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Chlorodibromomethane <13.0

51.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Chloroethane <51.8

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Chloroform <13.0

51.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Chloromethane <51.8

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼2-Chlorotoluene <13.0


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼cis-1,2-Dichloroethene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼cis-1,3-Dichloropropene <13.0

130 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2-Dibromo-3-chloropropane <130

130 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2-Dibromoethane (EDB) <130

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Dibromomethane <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2-Dichlorobenzene <13.0



38.9 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Dichlorodifluoromethane <38.9

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,1-Dichloroethane <13.0


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,1-Dichloroethene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2-Dichloropropane <13.0



13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,1-Dichloropropene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Ethylbenzene <13.0

64.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Hexachlorobutadiene <64.8

64.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Hexane <64.8

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Isopropylbenzene <13.0

130 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Methylene chloride <130

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Methyl tert-butyl ether <13.0

64.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Naphthalene <64.8

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼n-Butylbenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼n-Propylbenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼p-Isopropyltoluene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼sec-Butylbenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Styrene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼tert-Butylbenzene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,1,1,2-Tetrachloroethane <13.0


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Tetrachloroethene <13.0


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Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)RL MDL

Toluene <13.0 13.0 ug/Kg ☼ 12/20/19 05:43 12/20/19 08:51 1


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼trans-1,2-Dichloroethene <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼trans-1,3-Dichloropropene <13.0

64.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2,3-Trichlorobenzene <64.8


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,1,1-Trichloroethane <13.0


13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Trichloroethene <13.0

51.8 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Trichlorofluoromethane <51.8

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2,3-Trichloropropane <13.0

13.0 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼1,2,4-Trimethylbenzene <13.0


38.9 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Vinyl chloride <38.9

38.9 ug/Kg 12/20/19 05:43 12/20/19 08:51 1☼Xylenes, Total <38.9

4-Bromofluorobenzene (Surr) 93 80 - 120 12/20/19 05:43 12/20/19 08:51 1


Dibromofluoromethane (Surr) 101 12/20/19 05:43 12/20/19 08:51 180 - 120

Toluene-d8 (Surr) 100 12/20/19 05:43 12/20/19 08:51 180 - 120

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 <0.0575 0.0575 mg/Kg ☼ 12/20/19 12:30 12/23/19 14:23 1


0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1221 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1232 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1242 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1248 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1254 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1260 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:23 1☼PCB-1268 <0.0575

DCB Decachlorobiphenyl (Surr) 64 10 - 110 12/20/19 12:30 12/23/19 14:23 1


Tetrachloro-m-xylene 64 12/20/19 12:30 12/23/19 14:23 110 - 110


Diesel <9.74 F1 9.74 mg/Kg 12/27/19 10:21 12/30/19 18:22 1


9.74 mg/Kg 12/27/19 10:21 12/30/19 18:22 1Gasoline <9.74

38.9 mg/Kg 12/27/19 10:21 01/07/20 12:37 4Waste Oil 6150

14.6 mg/Kg 12/27/19 10:21 12/30/19 18:22 1Total Extractable Hydrocarbons <14.6

n-Octacosane 2 X 10 - 123 12/27/19 10:21 12/30/19 18:22 1


Method: 6010C - Metals (ICP)RL MDL

Arsenic 11.3 10.3 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:03 3


2.57 mg/Kg 12/23/19 09:46 12/30/19 13:03 3☼Barium 210 F1 F2

2.57 mg/Kg 12/23/19 09:46 12/30/19 13:03 3☼Cadmium <2.57

2.57 mg/Kg 12/23/19 09:46 12/30/19 13:03 3☼Chromium 18.8


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Method: 6010C - Metals (ICP) (Continued)RL MDL

Lead 24.8 12.8 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:03 3


12.8 mg/Kg 12/23/19 09:46 12/30/19 13:03 3☼Selenium <12.8

2.57 mg/Kg 12/23/19 09:46 12/30/19 13:03 3☼Silver <2.57

Method: 7471B - Mercury (CVAA)RL MDL

Mercury 0.0331 0.0211 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:43 1



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Acetone <130 130 ug/Kg ☼ 12/20/19 05:43 12/20/19 09:15 1


13.0 ug/Kg 12/20/19 05:43 12/20/19 09:15 1☼Benzene <13.0




26.0 ug/Kg 12/20/19 05:43 12/20/19 09:15 1☼Bromoform <26.0








13.0 ug/Kg 12/20/19 05:43 12/20/19 09:15 1☼Chloroform <13.0






















65.0 ug/Kg 12/20/19 05:43 12/20/19 09:15 1☼Hexane <65.0









13.0 ug/Kg 12/20/19 05:43 12/20/19 09:15 1☼Styrene <13.0






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Toluene <13.0 13.0 ug/Kg ☼ 12/20/19 05:43 12/20/19 09:15 1


















Toluene-d8 (Surr) 99 12/20/19 05:43 12/20/19 09:15 180 - 120


PCB-1016 <0.0600 0.0600 mg/Kg ☼ 12/30/19 13:05 01/05/20 21:26 1


0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1221 <0.0600

0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1232 <0.0600

0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1242 <0.0600

0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1248 <0.0600

3.00 mg/Kg 12/30/19 13:05 01/07/20 13:10 50☼PCB-1254 9.06

0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1260 <0.0600

0.0600 mg/Kg 12/30/19 13:05 01/05/20 21:26 1☼PCB-1268 <0.0600





Diesel <9.52 9.52 mg/Kg 12/27/19 10:21 01/06/20 16:20 1


9.52 mg/Kg 12/27/19 10:21 01/06/20 16:20 1Gasoline <9.52

9.52 mg/Kg 12/27/19 10:21 01/06/20 16:20 1Waste Oil 1250


n-Octacosane 5 X 10 - 123 12/27/19 10:21 01/06/20 16:20 1



Arsenic 11.8 7.62 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:08 2


1.91 mg/Kg 12/23/19 09:46 12/30/19 13:08 2☼Barium 215

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:08 2☼Cadmium <1.91

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:08 2☼Chromium 20.8


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Lead 27.0 9.53 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:08 2


9.53 mg/Kg 12/23/19 09:46 12/30/19 13:08 2☼Selenium <9.53

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:08 2☼Silver <1.91


Mercury 0.0591 0.0244 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:45 1



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Arsenic 12.0 7.82 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:10 2


1.95 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Barium 266

1.95 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Cadmium <1.95

1.95 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Chromium 23.3

9.77 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Lead 22.4

9.77 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Selenium <9.77

1.95 mg/Kg 12/23/19 09:46 12/30/19 13:10 2☼Silver <1.95


Mercury 0.0324 0.0222 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:47 1



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Acetone <145 145 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:04 1


14.5 ug/Kg 12/20/19 05:43 12/20/19 10:04 1☼Benzene <14.5




28.9 ug/Kg 12/20/19 05:43 12/20/19 10:04 1☼Bromoform <28.9








14.5 ug/Kg 12/20/19 05:43 12/20/19 10:04 1☼Chloroform <14.5






















72.3 ug/Kg 12/20/19 05:43 12/20/19 10:04 1☼Hexane <72.3









14.5 ug/Kg 12/20/19 05:43 12/20/19 10:04 1☼Styrene <14.5






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Toluene <14.5 14.5 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:04 1


















Toluene-d8 (Surr) 98 12/20/19 05:43 12/20/19 10:04 180 - 120


Diesel <9.54 9.54 mg/Kg 12/27/19 10:21 01/06/20 16:35 1


9.54 mg/Kg 12/27/19 10:21 01/06/20 16:35 1Gasoline <9.54

9.54 mg/Kg 12/27/19 10:21 01/06/20 16:35 1Waste Oil 121


n-Octacosane 66 10 - 123 12/27/19 10:21 01/06/20 16:35 1



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PCB-1016 <0.0551 0.0551 mg/Kg ☼ 12/20/19 12:30 12/23/19 14:33 1


0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1221 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1232 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1242 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1248 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1254 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1260 <0.0551

0.0551 mg/Kg 12/20/19 12:30 12/23/19 14:33 1☼PCB-1268 <0.0551





Arsenic <23.9 23.9 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:12 7


5.96 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Barium 125

5.96 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Cadmium <5.96

5.96 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Chromium 12.3

29.8 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Lead <29.8

29.8 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Selenium <29.8

5.96 mg/Kg 12/23/19 09:46 12/30/19 13:12 7☼Silver <5.96


Mercury <0.0212 0.0212 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:49 1



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Acetone <130 130 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:29 1


13.0 ug/Kg 12/20/19 05:43 12/20/19 10:29 1☼Benzene <13.0




26.0 ug/Kg 12/20/19 05:43 12/20/19 10:29 1☼Bromoform <26.0








13.0 ug/Kg 12/20/19 05:43 12/20/19 10:29 1☼Chloroform <13.0






















65.0 ug/Kg 12/20/19 05:43 12/20/19 10:29 1☼Hexane <65.0









13.0 ug/Kg 12/20/19 05:43 12/20/19 10:29 1☼Styrene <13.0






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Toluene <13.0 13.0 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:29 1


















Toluene-d8 (Surr) 98 12/20/19 05:43 12/20/19 10:29 180 - 120


Diesel <9.66 9.66 mg/Kg 12/27/19 10:21 01/06/20 14:35 1


9.66 mg/Kg 12/27/19 10:21 01/06/20 14:35 1Gasoline <9.66

9.66 mg/Kg 12/27/19 10:21 01/06/20 14:35 1Waste Oil <9.66


n-Octacosane 63 10 - 123 12/27/19 10:21 01/06/20 14:35 1



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Arsenic 19.6 7.12 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:17 2


1.78 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Barium 259

1.78 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Cadmium <1.78

1.78 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Chromium 20.4

8.90 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Lead 478

8.90 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Selenium <8.90

1.78 mg/Kg 12/23/19 09:46 12/30/19 13:17 2☼Silver <1.78


Mercury 0.544 0.0237 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:52 1



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Acetone <146 146 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:54 1


14.6 ug/Kg 12/20/19 05:43 12/20/19 10:54 1☼Benzene <14.6




29.3 ug/Kg 12/20/19 05:43 12/20/19 10:54 1☼Bromoform <29.3








14.6 ug/Kg 12/20/19 05:43 12/20/19 10:54 1☼Chloroform <14.6






















73.2 ug/Kg 12/20/19 05:43 12/20/19 10:54 1☼Hexane <73.2









14.6 ug/Kg 12/20/19 05:43 12/20/19 10:54 1☼Styrene <14.6






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Toluene <14.6 14.6 ug/Kg ☼ 12/20/19 05:43 12/20/19 10:54 1


















Toluene-d8 (Surr) 99 12/20/19 05:43 12/20/19 10:54 180 - 120


Diesel <9.77 9.77 mg/Kg 12/27/19 10:21 01/06/20 16:56 1


9.77 mg/Kg 12/27/19 10:21 01/06/20 16:56 1Gasoline <9.77

9.77 mg/Kg 12/27/19 10:21 01/06/20 16:56 1Waste Oil 283


n-Octacosane 69 10 - 123 12/27/19 10:21 01/06/20 16:56 1



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Acetone <682 682 ug/Kg ☼ 12/30/19 05:26 12/30/19 16:12 1


136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Benzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Bromobenzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Bromochloromethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Bromodichloromethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Bromoform <136

682 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Bromomethane <682


136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Carbon disulfide <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Carbon tetrachloride <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Chlorobenzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Chlorodibromomethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Chloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Chloroform <136

341 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Chloromethane <341

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼2-Chlorotoluene <136 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼4-Chlorotoluene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼cis-1,2-Dichloroethene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼cis-1,3-Dichloropropene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2-Dibromo-3-chloropropane <136 F2


136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Dibromomethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2-Dichlorobenzene <136



136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Dichlorodifluoromethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1-Dichloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2-Dichloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1-Dichloroethene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2-Dichloropropane <136



136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1-Dichloropropene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Ethylbenzene 137

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Hexachlorobutadiene <136 F2

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Hexane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Isopropylbenzene 458


136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Methyl tert-butyl ether <136

341 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Naphthalene 605

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼n-Butylbenzene 2710 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼n-Propylbenzene 674

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼p-Isopropyltoluene 1000 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼sec-Butylbenzene 1370 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Styrene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼tert-Butylbenzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1,1,2-Tetrachloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1,2,2-Tetrachloroethane <136 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Tetrachloroethene <136


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Toluene <136 136 ug/Kg ☼ 12/30/19 05:26 12/30/19 16:12 1


136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼trans-1,2-Dichloroethene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼trans-1,3-Dichloropropene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2,3-Trichlorobenzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2,4-Trichlorobenzene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1,1-Trichloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,1,2-Trichloroethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Trichloroethene <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Trichlorofluoromethane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2,3-Trichloropropane <136

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,2,4-Trimethylbenzene 4730 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼1,3,5-Trimethylbenzene 2290 F1

136 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Vinyl chloride <136

204 ug/Kg 12/30/19 05:26 12/30/19 16:12 1☼Xylenes, Total 3110 F1




Toluene-d8 (Surr) 97 12/30/19 05:26 12/30/19 16:12 180 - 120


Diesel 2190 9.76 mg/Kg 12/27/19 10:21 12/30/19 19:36 1


9.76 mg/Kg 12/27/19 10:21 12/30/19 19:36 1Gasoline <9.76

9.76 mg/Kg 12/27/19 10:21 12/30/19 19:36 1Waste Oil <9.76


n-Octacosane 70 10 - 123 12/27/19 10:21 12/30/19 19:36 1



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PCB-1016 <0.0575 0.0575 mg/Kg ☼ 12/20/19 12:30 12/23/19 14:44 1


0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1221 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1232 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1242 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1248 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1254 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1260 <0.0575

0.0575 mg/Kg 12/20/19 12:30 12/23/19 14:44 1☼PCB-1268 <0.0575





Arsenic 6.77 3.65 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:19 1


0.912 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Barium 191

0.912 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Cadmium <0.912

0.912 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Chromium 21.0

4.56 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Lead 14.8

4.56 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Selenium <4.56

0.912 mg/Kg 12/23/19 09:46 12/30/19 13:19 1☼Silver <0.912


Mercury <0.0220 0.0220 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:56 1



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Acetone <117 117 ug/Kg ☼ 12/20/19 05:43 12/20/19 12:36 1


11.7 ug/Kg 12/20/19 05:43 12/20/19 12:36 1☼Benzene <11.7




23.5 ug/Kg 12/20/19 05:43 12/20/19 12:36 1☼Bromoform <23.5








11.7 ug/Kg 12/20/19 05:43 12/20/19 12:36 1☼Chloroform <11.7






















58.7 ug/Kg 12/20/19 05:43 12/20/19 12:36 1☼Hexane <58.7









11.7 ug/Kg 12/20/19 05:43 12/20/19 12:36 1☼Styrene <11.7






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Toluene <11.7 11.7 ug/Kg ☼ 12/20/19 05:43 12/20/19 12:36 1


















Toluene-d8 (Surr) 97 12/20/19 05:43 12/20/19 12:36 180 - 120


PCB-1016 <0.0577 0.0577 mg/Kg ☼ 12/20/19 12:30 12/23/19 14:55 1


0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1221 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1232 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1242 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1248 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1254 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1260 <0.0577

0.0577 mg/Kg 12/20/19 12:30 12/23/19 14:55 1☼PCB-1268 <0.0577





Diesel <9.65 9.65 mg/Kg 12/27/19 10:21 01/06/20 14:50 1


9.65 mg/Kg 12/27/19 10:21 01/06/20 14:50 1Gasoline <9.65

9.65 mg/Kg 12/27/19 10:21 01/06/20 14:50 1Waste Oil 45.9


n-Octacosane 59 10 - 123 12/27/19 10:21 01/06/20 14:50 1



Arsenic 9.19 3.94 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:21 1


0.986 mg/Kg 12/23/19 09:46 12/30/19 13:21 1☼Barium 240

0.986 mg/Kg 12/23/19 09:46 12/30/19 13:21 1☼Cadmium <0.986

0.986 mg/Kg 12/23/19 09:46 12/30/19 13:21 1☼Chromium 20.9


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Lead 25.8 4.93 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:21 1


4.93 mg/Kg 12/23/19 09:46 12/30/19 13:21 1☼Selenium <4.93

0.986 mg/Kg 12/23/19 09:46 12/30/19 13:21 1☼Silver <0.986


Mercury 0.0541 0.0203 mg/Kg ☼ 12/20/19 12:11 12/23/19 13:58 1



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Acetone <134 134 ug/Kg ☼ 12/20/19 05:43 12/20/19 14:40 1


13.4 ug/Kg 12/20/19 05:43 12/20/19 14:40 1☼Benzene <13.4




26.7 ug/Kg 12/20/19 05:43 12/20/19 14:40 1☼Bromoform <26.7








13.4 ug/Kg 12/20/19 05:43 12/20/19 14:40 1☼Chloroform <13.4






















66.8 ug/Kg 12/20/19 05:43 12/20/19 14:40 1☼Hexane <66.8









13.4 ug/Kg 12/20/19 05:43 12/20/19 14:40 1☼Styrene <13.4






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Toluene <13.4 13.4 ug/Kg ☼ 12/20/19 05:43 12/20/19 14:40 1


















Toluene-d8 (Surr) 96 12/20/19 05:43 12/20/19 14:40 180 - 120


Diesel <9.66 9.66 mg/Kg 12/27/19 10:21 12/30/19 20:06 1


9.66 mg/Kg 12/27/19 10:21 12/30/19 20:06 1Gasoline <9.66

96.6 mg/Kg 12/27/19 10:21 01/06/20 17:55 10Waste Oil 16100


n-Octacosane 8 X 10 - 123 12/27/19 10:21 12/30/19 20:06 1



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Arsenic 7.62 3.29 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:22 1


0.822 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Barium 173

0.822 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Cadmium <0.822

0.822 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Chromium 19.1

4.11 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Lead 31.5

4.11 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Selenium <4.11

0.822 mg/Kg 12/23/19 09:46 12/30/19 13:22 1☼Silver <0.822


Mercury <0.0194 0.0194 mg/Kg ☼ 12/20/19 12:11 12/23/19 14:00 1



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PCB-1016 <0.0613 0.0613 mg/Kg ☼ 12/20/19 12:30 12/23/19 15:06 1


0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1221 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1232 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1242 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1248 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1254 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1260 <0.0613

0.0613 mg/Kg 12/20/19 12:30 12/23/19 15:06 1☼PCB-1268 <0.0613





Arsenic 13.2 7.51 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:24 2


1.88 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Barium 232

1.88 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Cadmium <1.88

1.88 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Chromium 20.6

9.38 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Lead 12.4

9.38 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Selenium <9.38

1.88 mg/Kg 12/23/19 09:46 12/30/19 13:24 2☼Silver <1.88


Mercury 0.0348 0.0228 mg/Kg ☼ 12/20/19 12:11 12/23/19 14:06 1



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Acetone <146 146 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:01 1


14.6 ug/Kg 12/20/19 05:43 12/20/19 13:01 1☼Benzene <14.6




29.1 ug/Kg 12/20/19 05:43 12/20/19 13:01 1☼Bromoform <29.1








14.6 ug/Kg 12/20/19 05:43 12/20/19 13:01 1☼Chloroform <14.6






















72.8 ug/Kg 12/20/19 05:43 12/20/19 13:01 1☼Hexane <72.8









14.6 ug/Kg 12/20/19 05:43 12/20/19 13:01 1☼Styrene <14.6






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Toluene <14.6 14.6 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:01 1


















Toluene-d8 (Surr) 98 12/20/19 05:43 12/20/19 13:01 180 - 120


Diesel <9.52 9.52 mg/Kg 12/27/19 10:21 01/06/20 15:05 1


9.52 mg/Kg 12/27/19 10:21 01/06/20 15:05 1Gasoline <9.52

9.52 mg/Kg 12/27/19 10:21 01/06/20 15:05 1Waste Oil 24.0


n-Octacosane 66 10 - 123 12/27/19 10:21 01/06/20 15:05 1



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PCB-1016 <0.0638 0.0638 mg/Kg ☼ 12/20/19 12:30 12/23/19 15:16 1


0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1221 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1232 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1242 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1248 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1254 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1260 <0.0638

0.0638 mg/Kg 12/20/19 12:30 12/23/19 15:16 1☼PCB-1268 <0.0638





Arsenic 9.52 7.64 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:28 2


1.91 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Barium 249

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Cadmium <1.91

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Chromium 21.9

9.55 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Lead 14.9

9.55 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Selenium <9.55

1.91 mg/Kg 12/23/19 09:46 12/30/19 13:28 2☼Silver <1.91


Mercury 0.0284 0.0253 mg/Kg ☼ 12/20/19 12:11 12/23/19 14:08 1



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Acetone <142 142 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:26 1


14.2 ug/Kg 12/20/19 05:43 12/20/19 13:26 1☼Benzene <14.2




28.5 ug/Kg 12/20/19 05:43 12/20/19 13:26 1☼Bromoform <28.5








14.2 ug/Kg 12/20/19 05:43 12/20/19 13:26 1☼Chloroform <14.2






















71.2 ug/Kg 12/20/19 05:43 12/20/19 13:26 1☼Hexane <71.2









14.2 ug/Kg 12/20/19 05:43 12/20/19 13:26 1☼Styrene <14.2






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Toluene <14.2 14.2 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:26 1


















Toluene-d8 (Surr) 98 12/20/19 05:43 12/20/19 13:26 180 - 120


Diesel <9.57 9.57 mg/Kg 12/30/19 12:59 01/06/20 09:41 1


9.57 mg/Kg 12/30/19 12:59 01/06/20 09:41 1Gasoline <9.57

9.57 mg/Kg 12/30/19 12:59 01/06/20 09:41 1Waste Oil <9.57


n-Octacosane 49 10 - 123 12/30/19 12:59 01/06/20 09:41 1



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Acetone <128 128 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:51 1


12.8 ug/Kg 12/20/19 05:43 12/20/19 13:51 1☼Benzene <12.8




25.7 ug/Kg 12/20/19 05:43 12/20/19 13:51 1☼Bromoform <25.7








12.8 ug/Kg 12/20/19 05:43 12/20/19 13:51 1☼Chloroform <12.8






















64.1 ug/Kg 12/20/19 05:43 12/20/19 13:51 1☼Hexane <64.1









12.8 ug/Kg 12/20/19 05:43 12/20/19 13:51 1☼Styrene <12.8






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Toluene <12.8 12.8 ug/Kg ☼ 12/20/19 05:43 12/20/19 13:51 1


















Toluene-d8 (Surr) 97 12/20/19 05:43 12/20/19 13:51 180 - 120


Diesel <9.89 9.89 mg/Kg 12/27/19 10:21 12/30/19 20:35 1


9.89 mg/Kg 12/27/19 10:21 12/30/19 20:35 1Gasoline <9.89

9.89 mg/Kg 12/27/19 10:21 12/30/19 20:35 1Waste Oil 168


n-Octacosane 81 10 - 123 12/27/19 10:21 12/30/19 20:35 1



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PCB-1016 <0.0528 0.0528 mg/Kg ☼ 12/20/19 12:30 12/23/19 15:27 1


0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1221 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1232 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1242 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1248 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1254 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1260 <0.0528

0.0528 mg/Kg 12/20/19 12:30 12/23/19 15:27 1☼PCB-1268 <0.0528





Arsenic 13.7 3.92 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:29 1


0.980 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Barium 130

0.980 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Cadmium <0.980

0.980 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Chromium 15.9

4.90 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Lead 10.4

4.90 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Selenium <4.90

0.980 mg/Kg 12/23/19 09:46 12/30/19 13:29 1☼Silver <0.980


Mercury 0.0256 0.0201 mg/Kg ☼ 12/20/19 12:11 12/23/19 14:11 1



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Acetone <131 131 ug/Kg ☼ 12/20/19 05:43 12/20/19 14:15 1


13.1 ug/Kg 12/20/19 05:43 12/20/19 14:15 1☼Benzene <13.1




26.1 ug/Kg 12/20/19 05:43 12/20/19 14:15 1☼Bromoform <26.1








13.1 ug/Kg 12/20/19 05:43 12/20/19 14:15 1☼Chloroform <13.1






















65.3 ug/Kg 12/20/19 05:43 12/20/19 14:15 1☼Hexane <65.3









13.1 ug/Kg 12/20/19 05:43 12/20/19 14:15 1☼Styrene <13.1






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Toluene <13.1 13.1 ug/Kg ☼ 12/20/19 05:43 12/20/19 14:15 1


















Toluene-d8 (Surr) 94 12/20/19 05:43 12/20/19 14:15 180 - 120


PCB-1016 <0.0617 0.0617 mg/Kg ☼ 12/20/19 12:30 12/23/19 15:38 1


0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1221 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1232 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1242 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1248 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1254 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1260 <0.0617

0.0617 mg/Kg 12/20/19 12:30 12/23/19 15:38 1☼PCB-1268 <0.0617





Diesel <9.59 9.59 mg/Kg 12/27/19 10:21 12/30/19 20:50 1


9.59 mg/Kg 12/27/19 10:21 12/30/19 20:50 1Gasoline <9.59

9.59 mg/Kg 12/27/19 10:21 12/30/19 20:50 1Waste Oil 158


n-Octacosane 61 10 - 123 12/27/19 10:21 12/30/19 20:50 1



Arsenic 9.25 7.14 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:35 2


1.79 mg/Kg 12/23/19 09:46 12/30/19 13:35 2☼Barium 289

1.79 mg/Kg 12/23/19 09:46 12/30/19 13:35 2☼Cadmium <1.79

1.79 mg/Kg 12/23/19 09:46 12/30/19 13:35 2☼Chromium 21.3


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Lead 37.0 8.93 mg/Kg ☼ 12/23/19 09:46 12/30/19 13:35 2


8.93 mg/Kg 12/23/19 09:46 12/30/19 13:35 2☼Selenium <8.93

1.79 mg/Kg 12/23/19 09:46 12/30/19 13:35 2☼Silver <1.79


Mercury 0.476 0.0237 mg/Kg ☼ 12/20/19 12:11 12/23/19 14:13 1



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Definitions/GlossaryJob ID: 310-172445-1Client: Thiele Geotech Inc.


Qualifiers

GC/MS VOAQualifier Description

4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not

applicable.

Qualifier

F1 MS and/or MSD Recovery is outside acceptance limits.

F2 MS/MSD RPD exceeds control limits

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

GC Semi VOAQualifier Description


Qualifier

X Surrogate is outside control limits

MetalsQualifier Description


Qualifier

F2 MS/MSD RPD exceeds control limits

GlossaryThese commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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Method: 8260D - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Soil


BFB DBFM TOL

93 101 100310-172445-1


EB-1 (0-1)

99 98 103310-172445-1 MS EB-1 (0-1)

98 96 100310-172445-1 MSD EB-1 (0-1)

94 102 99310-172445-2 EB-2 (0-1)

94 102 98310-172445-4 EB-3 (5-6)

93 102 98310-172445-6 EB-4 (35-36)

96 101 99310-172445-8 EB-5 (1-2)

96 116 97310-172445-9 EB-6 (0-1)

97 120 97310-172445-9 MS EB-6 (0-1)

91 114 94310-172445-9 MSD EB-6 (0-1)

93 104 97310-172445-11 EB-7 (0-1)

96 102 96310-172445-12 EB-8 (0-1)

90 102 98310-172445-15 EB-9 (1-2)

92 103 98310-172445-17 EB-10 (12-13)

93 100 97310-172445-18 EB-11 (15-16)

90 101 94310-172445-20 EB-12 (20-21)

Surrogate Legend




Method: 8260D - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid


BFB DBFM TOL

100 97 100LCS 310-265360/2-A


Lab Control Sample

104 120 92LCS 310-266150/2-A Lab Control Sample

95 102 99MB 310-265360/1-A Method Blank

104 119 99MB 310-266150/1-A Method Blank

Surrogate Legend




Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Soil

Lab Sample ID Client Sample ID (10-110) (10-110)

DCB1 TCX1

64 64310-172445-1


EB-1 (0-1)

65 73310-172445-2 EB-2 (0-1)

46 50310-172445-5 EB-4 (0-1)

77 82310-172445-10 EB-6 (5-6)

72 76310-172445-11 EB-7 (0-1)

75 61310-172445-14 EB-9 (0-1)

64 58310-172445-16 EB-10 (0-1)


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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)Prep Type: Total/NAMatrix: Soil


DCB1 TCX1

44 47310-172445-19


EB-11 (16-17)

71 70310-172445-20 EB-12 (20-21)

Surrogate Legend

DCB = DCB Decachlorobiphenyl (Surr)

TCX = Tetrachloro-m-xylene

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid


DCB1 TCX1

70 64LCS 310-265491/2-A


Lab Control Sample

82 73LCS 310-266266/2-A Lab Control Sample

62 58MB 310-265491/1-A Method Blank

101 100MB 310-266266/1-A Method Blank

Surrogate Legend

DCB = DCB Decachlorobiphenyl (Surr)

TCX = Tetrachloro-m-xylene

Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)Prep Type: Total/NAMatrix: Soil


OTCN

2 X310-172445-1


EB-1 (0-1)

10310-172445-1 MS EB-1 (0-1)

7 X310-172445-1 MSD EB-1 (0-1)

5 X310-172445-2 EB-2 (0-1)

66310-172445-4 EB-3 (5-6)

63310-172445-6 EB-4 (35-36)

69310-172445-8 EB-5 (1-2)

70310-172445-9 EB-6 (0-1)

59310-172445-11 EB-7 (0-1)

8 X310-172445-12 EB-8 (0-1)

66310-172445-15 EB-9 (1-2)

49310-172445-17 EB-10 (12-13)

81310-172445-18 EB-11 (15-16)

61310-172445-20 EB-12 (20-21)

Surrogate Legend

OTCN = n-Octacosane

Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)Prep Type: Total/NAMatrix: Solid


OTCN

84LCS 310-266074/2-A


Lab Control Sample


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Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC) (Continued)Prep Type: Total/NAMatrix: Solid


OTCN

74LCS 310-266264/2-A


Lab Control Sample



Surrogate Legend

OTCN = n-Octacosane


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Method: 8260D - Volatile Organic Compounds by GC/MS

Client Sample ID: Method BlankLab Sample ID: MB 310-265360/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 265370 Prep Batch: 265360

RL MDL

Acetone <86.8 86.8 ug/Kg 12/20/19 05:43 12/20/19 08:01 1

MB MB


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Benzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Bromobenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Bromochloromethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Bromodichloromethane

<17.4 17.4 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Bromoform

<34.7 34.7 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Bromomethane

<86.8 86.8 ug/Kg 12/20/19 05:43 12/20/19 08:01 12-Butanone (MEK)

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Carbon disulfide

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Carbon tetrachloride

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Chlorobenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Chlorodibromomethane

<34.7 34.7 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Chloroethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Chloroform

<34.7 34.7 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Chloromethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 12-Chlorotoluene


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1cis-1,2-Dichloroethene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1cis-1,3-Dichloropropene

<86.8 86.8 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2-Dibromo-3-chloropropane

<86.8 86.8 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2-Dibromoethane (EDB)

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Dibromomethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2-Dichlorobenzene



<26.0 26.0 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Dichlorodifluoromethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,1-Dichloroethane


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,1-Dichloroethene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2-Dichloropropane



<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,1-Dichloropropene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Ethylbenzene

<43.4 43.4 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Hexachlorobutadiene

<43.4 43.4 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Hexane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Isopropylbenzene

<86.8 86.8 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Methylene chloride

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Methyl tert-butyl ether

<43.4 43.4 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Naphthalene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1n-Butylbenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1n-Propylbenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1p-Isopropyltoluene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1sec-Butylbenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Styrene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1tert-Butylbenzene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,1,1,2-Tetrachloroethane



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Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)


RL MDL

Tetrachloroethene <8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1

MB MB


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Toluene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1trans-1,2-Dichloroethene

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1trans-1,3-Dichloropropene

<43.4 43.4 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2,3-Trichlorobenzene


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,1,1-Trichloroethane


<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Trichloroethene

<34.7 34.7 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Trichlorofluoromethane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2,3-Trichloropropane

<8.68 8.68 ug/Kg 12/20/19 05:43 12/20/19 08:01 11,2,4-Trimethylbenzene


<26.0 26.0 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Vinyl chloride

<26.0 26.0 ug/Kg 12/20/19 05:43 12/20/19 08:01 1Xylenes, Total


MB MB

Surrogate

12/20/19 05:43


102 12/20/19 05:43 12/20/19 08:01 1Dibromofluoromethane (Surr) 80 - 120

99 12/20/19 05:43 12/20/19 08:01 1Toluene-d8 (Surr) 80 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 310-265360/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 265370 Prep Batch: 265360

Acetone 178 184.6 ug/Kg 104 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzene 89.0 95.04 ug/Kg 107 72 - 145

Bromobenzene 89.0 88.94 ug/Kg 100 74 - 121

Bromochloromethane 89.0 91.39 ug/Kg 103 76 - 147

Bromodichloromethane 89.0 92.40 ug/Kg 104 80 - 122

Bromoform 89.0 85.56 ug/Kg 96 80 - 127

2-Butanone (MEK) 178 204.8 ug/Kg 115 50 - 150

Carbon disulfide 89.0 88.22 ug/Kg 99 65 - 146

Carbon tetrachloride 89.0 87.62 ug/Kg 98 75 - 150

Chlorobenzene 89.0 91.32 ug/Kg 103 76 - 120

Chlorodibromomethane 89.0 88.83 ug/Kg 100 80 - 125

Chloroform 89.0 89.65 ug/Kg 101 71 - 143

2-Chlorotoluene 89.0 92.84 ug/Kg 104 71 - 120

4-Chlorotoluene 89.0 87.20 ug/Kg 98 67 - 121

cis-1,2-Dichloroethene 89.0 89.98 ug/Kg 101 72 - 146

cis-1,3-Dichloropropene 89.0 92.25 ug/Kg 104 78 - 124

1,2-Dibromo-3-chloropropane 89.0 97.98 J ug/Kg 110 50 - 150

1,2-Dibromoethane (EDB) 89.0 89.09 J ug/Kg 100 80 - 123

Dibromomethane 89.0 91.20 ug/Kg 102 76 - 146

1,2-Dichlorobenzene 89.0 92.73 ug/Kg 104 67 - 120




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1,1-Dichloroethane 89.0 94.40 ug/Kg 106 74 - 144

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,2-Dichloroethane 89.0 91.67 ug/Kg 103 76 - 142

1,1-Dichloroethene 89.0 87.49 ug/Kg 98 67 - 150

1,2-Dichloropropane 89.0 98.35 ug/Kg 110 75 - 143



1,1-Dichloropropene 89.0 95.80 ug/Kg 108 71 - 145

Ethylbenzene 89.0 95.88 ug/Kg 108 73 - 120

Hexachlorobutadiene 89.0 83.37 ug/Kg 94 50 - 150

Hexane 89.0 78.55 ug/Kg 88 50 - 150

Isopropylbenzene 89.0 89.67 ug/Kg 101 72 - 123

Methylene chloride 89.0 93.45 J ug/Kg 105 50 - 150

Methyl tert-butyl ether 89.0 90.04 ug/Kg 101 78 - 145

m,p-Xylene 89.0 92.78 ug/Kg 104 70 - 120

Naphthalene 89.0 95.45 ug/Kg 107 50 - 150

n-Butylbenzene 89.0 89.38 ug/Kg 100 57 - 121

n-Propylbenzene 89.0 95.75 ug/Kg 108 68 - 121

o-Xylene 89.0 93.98 ug/Kg 106 72 - 121

p-Isopropyltoluene 89.0 93.62 ug/Kg 105 63 - 121

sec-Butylbenzene 89.0 96.64 ug/Kg 109 65 - 121

Styrene 89.0 88.27 ug/Kg 99 73 - 123

tert-Butylbenzene 89.0 96.31 ug/Kg 108 69 - 122

1,1,1,2-Tetrachloroethane 89.0 89.54 ug/Kg 101 80 - 123

1,1,2,2-Tetrachloroethane 89.0 95.97 ug/Kg 108 79 - 126

Tetrachloroethene 89.0 87.15 ug/Kg 98 72 - 120

Toluene 89.0 92.99 ug/Kg 104 75 - 120

trans-1,2-Dichloroethene 89.0 89.99 ug/Kg 101 71 - 145

trans-1,3-Dichloropropene 89.0 89.18 ug/Kg 100 79 - 124

1,2,3-Trichlorobenzene 89.0 92.12 ug/Kg 103 50 - 150

1,2,4-Trichlorobenzene 89.0 91.42 ug/Kg 103 53 - 126

1,1,1-Trichloroethane 89.0 93.35 ug/Kg 105 73 - 150

1,1,2-Trichloroethane 89.0 91.57 ug/Kg 103 80 - 124

Trichloroethene 89.0 91.58 ug/Kg 103 71 - 145

1,2,3-Trichloropropane 89.0 92.29 ug/Kg 104 80 - 121

1,2,4-Trimethylbenzene 89.0 92.87 ug/Kg 104 61 - 120

1,3,5-Trimethylbenzene 89.0 92.25 ug/Kg 104 64 - 121

Xylenes, Total 178 186.8 ug/Kg 105 72 - 120


Surrogate

100

LCS LCS





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Client Sample ID: EB-1 (0-1)Lab Sample ID: 310-172445-1 MSMatrix: Soil Prep Type: Total/NAAnalysis Batch: 265370 Prep Batch: 265360

Acetone <130 F1 205 728.7 F1 ug/Kg 313 48 - 150☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Benzene <13.0 103 85.23 ug/Kg 83 52 - 145☼

Bromobenzene <13.0 103 41.27 ug/Kg 40 10 - 135☼

Bromochloromethane <13.0 103 91.00 ug/Kg 89 56 - 147☼

Bromodichloromethane <13.0 103 79.03 ug/Kg 77 48 - 127☼

Bromoform <25.9 103 53.30 ug/Kg 52 22 - 137☼

2-Butanone (MEK) <130 205 223.4 ug/Kg 99 23 - 150☼

Carbon disulfide <13.0 103 73.03 ug/Kg 70 30 - 147☼

Carbon tetrachloride <13.0 103 64.03 ug/Kg 62 41 - 150☼

Chlorobenzene <13.0 103 53.81 ug/Kg 52 21 - 132☼

Chlorodibromomethane <13.0 103 67.16 ug/Kg 66 35 - 134☼

Chloroform <13.0 103 85.68 ug/Kg 82 53 - 143☼

2-Chlorotoluene <13.0 103 37.75 ug/Kg 37 10 - 130☼

4-Chlorotoluene <13.0 103 34.73 ug/Kg 32 10 - 128☼

cis-1,2-Dichloroethene <13.0 103 86.10 ug/Kg 84 55 - 146☼

cis-1,3-Dichloropropene <13.0 103 76.50 ug/Kg 75 34 - 132☼

1,2-Dibromo-3-chloropropane <130 103 <128 ug/Kg 50 14 - 150☼

1,2-Dibromoethane (EDB) <130 103 <128 ug/Kg 73 35 - 134☼

Dibromomethane <13.0 103 86.40 ug/Kg 84 49 - 147☼

1,2-Dichlorobenzene <13.0 103 29.51 ug/Kg 28 10 - 127☼



1,1-Dichloroethane <13.0 103 95.76 ug/Kg 93 62 - 146☼

1,2-Dichloroethane <13.0 103 92.37 ug/Kg 90 56 - 142☼

1,1-Dichloroethene <13.0 103 79.40 ug/Kg 76 51 - 150☼

1,2-Dichloropropane <13.0 103 89.86 ug/Kg 88 55 - 143☼



1,1-Dichloropropene <13.0 103 73.14 ug/Kg 70 41 - 149☼

Ethylbenzene <13.0 103 54.12 ug/Kg 53 22 - 133☼

Hexachlorobutadiene <64.8 103 <64.1 ug/Kg 12 10 - 150☼

Hexane <64.8 103 <64.1 ug/Kg 43 10 - 150☼

Isopropylbenzene <13.0 103 42.28 ug/Kg 39 18 - 133☼

Methylene chloride <130 103 <128 ug/Kg 77 41 - 150☼

Methyl tert-butyl ether <13.0 103 99.61 ug/Kg 97 67 - 146☼

m,p-Xylene <13.0 103 50.61 ug/Kg 49 15 - 137☼

Naphthalene <64.8 103 <64.1 ug/Kg 19 10 - 150☼

n-Butylbenzene <13.0 103 24.30 ug/Kg 21 10 - 121☼

n-Propylbenzene <13.0 103 38.99 ug/Kg 37 10 - 129☼

o-Xylene <13.0 103 49.87 ug/Kg 48 18 - 135☼

p-Isopropyltoluene <13.0 103 29.61 ug/Kg 28 10 - 123☼

sec-Butylbenzene <13.0 103 32.78 ug/Kg 31 10 - 127☼

Styrene <13.0 103 45.91 ug/Kg 42 12 - 134☼

tert-Butylbenzene <13.0 103 37.20 ug/Kg 35 11 - 132☼

1,1,1,2-Tetrachloroethane <13.0 103 56.73 ug/Kg 55 35 - 132☼

1,1,2,2-Tetrachloroethane <13.0 103 60.30 ug/Kg 59 29 - 135☼

Tetrachloroethene <13.0 103 50.48 ug/Kg 48 28 - 124☼

Toluene <13.0 103 68.48 ug/Kg 65 37 - 126☼


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trans-1,2-Dichloroethene <13.0 103 84.44 ug/Kg 81 50 - 145☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

trans-1,3-Dichloropropene <13.0 103 69.79 ug/Kg 68 28 - 134☼

1,2,3-Trichlorobenzene <64.8 103 <64.1 ug/Kg 12 10 - 150☼

1,2,4-Trichlorobenzene <64.8 103 <64.1 ug/Kg 11 10 - 126☼

1,1,1-Trichloroethane <13.0 103 76.80 ug/Kg 75 55 - 150☼

1,1,2-Trichloroethane <13.0 103 81.54 ug/Kg 80 48 - 129☼

Trichloroethene <13.0 103 72.20 ug/Kg 69 43 - 147☼

1,2,3-Trichloropropane <13.0 103 68.78 ug/Kg 67 35 - 129☼

1,2,4-Trimethylbenzene <13.0 103 34.84 ug/Kg 34 10 - 135☼

1,3,5-Trimethylbenzene <13.0 103 36.82 ug/Kg 35 10 - 130☼

Xylenes, Total <38.9 205 100.5 ug/Kg 49 18 - 136☼


Surrogate

99

MS MS




Client Sample ID: EB-1 (0-1)Lab Sample ID: 310-172445-1 MSDMatrix: Soil Prep Type: Total/NAAnalysis Batch: 265370 Prep Batch: 265360

Acetone <130 F1 205 671.5 F1 ug/Kg 286 48 - 150 8 34☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Benzene <13.0 102 93.60 ug/Kg 91 52 - 145 9 32☼

Bromobenzene <13.0 102 50.14 ug/Kg 48 10 - 135 19 38☼

Bromochloromethane <13.0 102 94.91 ug/Kg 93 56 - 147 4 32☼

Bromodichloromethane <13.0 102 87.72 ug/Kg 86 48 - 127 10 33☼

Bromoform <25.9 102 62.50 ug/Kg 61 22 - 137 16 36☼

2-Butanone (MEK) <130 205 206.6 ug/Kg 91 23 - 150 8 40☼

Carbon disulfide <13.0 102 77.46 ug/Kg 74 30 - 147 6 36☼

Carbon tetrachloride <13.0 102 74.33 ug/Kg 73 41 - 150 15 34☼

Chlorobenzene <13.0 102 63.38 ug/Kg 62 21 - 132 16 36☼

Chlorodibromomethane <13.0 102 76.75 ug/Kg 75 35 - 134 13 33☼

Chloroform <13.0 102 93.20 ug/Kg 90 53 - 143 8 33☼

2-Chlorotoluene <13.0 102 45.88 ug/Kg 45 10 - 130 19 40☼

4-Chlorotoluene <13.0 102 41.61 ug/Kg 39 10 - 128 18 40☼

cis-1,2-Dichloroethene <13.0 102 93.28 ug/Kg 91 55 - 146 8 33☼

cis-1,3-Dichloropropene <13.0 102 84.56 ug/Kg 83 34 - 132 10 35☼

1,2-Dibromo-3-chloropropane <130 102 <128 ug/Kg 59 14 - 150 16 39☼

1,2-Dibromoethane (EDB) <130 102 <128 ug/Kg 79 35 - 134 8 40☼

Dibromomethane <13.0 102 90.96 ug/Kg 89 49 - 147 5 32☼

1,2-Dichlorobenzene <13.0 102 37.15 ug/Kg 35 10 - 127 23 40☼



1,1-Dichloroethane <13.0 102 101.0 ug/Kg 99 62 - 146 5 34☼

1,2-Dichloroethane <13.0 102 97.32 ug/Kg 95 56 - 142 5 32☼

1,1-Dichloroethene <13.0 102 87.23 ug/Kg 84 51 - 150 9 31☼

1,2-Dichloropropane <13.0 102 97.39 ug/Kg 95 55 - 143 8 31☼


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Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


1,1-Dichloropropene <13.0 102 83.55 ug/Kg 81 41 - 149 13 32☼

Ethylbenzene <13.0 102 63.82 ug/Kg 62 22 - 133 16 38☼

Hexachlorobutadiene <64.8 102 <64.0 ug/Kg 16 10 - 150 30 40☼

Hexane <64.8 102 <64.0 ug/Kg 48 10 - 150 10 40☼

Isopropylbenzene <13.0 102 50.63 ug/Kg 47 18 - 133 18 37☼

Methylene chloride <130 102 <128 ug/Kg 80 41 - 150 4 38☼

Methyl tert-butyl ether <13.0 102 101.4 ug/Kg 99 67 - 146 2 34☼

m,p-Xylene <13.0 102 59.70 ug/Kg 58 15 - 137 16 40☼

Naphthalene <64.8 102 <64.0 ug/Kg 24 10 - 150 24 40☼

n-Butylbenzene <13.0 102 30.98 ug/Kg 28 10 - 121 24 40☼

n-Propylbenzene <13.0 102 46.68 ug/Kg 45 10 - 129 18 40☼

o-Xylene <13.0 102 58.80 ug/Kg 57 18 - 135 16 37☼

p-Isopropyltoluene <13.0 102 37.04 ug/Kg 35 10 - 123 22 40☼

sec-Butylbenzene <13.0 102 41.61 ug/Kg 40 10 - 127 24 40☼

Styrene <13.0 102 53.47 ug/Kg 50 12 - 134 15 40☼

tert-Butylbenzene <13.0 102 47.23 ug/Kg 45 11 - 132 24 40☼

1,1,1,2-Tetrachloroethane <13.0 102 68.05 ug/Kg 67 35 - 132 18 35☼

1,1,2,2-Tetrachloroethane <13.0 102 70.78 ug/Kg 69 29 - 135 16 34☼

Tetrachloroethene <13.0 102 60.17 ug/Kg 58 28 - 124 18 34☼

Toluene <13.0 102 80.12 ug/Kg 77 37 - 126 16 33☼

trans-1,2-Dichloroethene <13.0 102 89.37 ug/Kg 86 50 - 145 6 35☼

trans-1,3-Dichloropropene <13.0 102 76.92 ug/Kg 75 28 - 134 10 35☼

1,2,3-Trichlorobenzene <64.8 102 <64.0 ug/Kg 15 10 - 150 26 40☼

1,2,4-Trichlorobenzene <64.8 102 <64.0 ug/Kg 16 10 - 126 27 40☼

1,1,1-Trichloroethane <13.0 102 88.30 ug/Kg 86 55 - 150 14 32☼

1,1,2-Trichloroethane <13.0 102 88.34 ug/Kg 86 48 - 129 8 33☼

Trichloroethene <13.0 102 80.55 ug/Kg 78 43 - 147 11 35☼

1,2,3-Trichloropropane <13.0 102 75.31 ug/Kg 74 35 - 129 9 35☼

1,2,4-Trimethylbenzene <13.0 102 42.92 ug/Kg 42 10 - 135 21 40☼

1,3,5-Trimethylbenzene <13.0 102 44.62 ug/Kg 43 10 - 130 19 40☼

Xylenes, Total <38.9 205 118.5 ug/Kg 58 18 - 136 16 40☼


Surrogate

98

MSD MSD





RL MDL

Acetone <482 482 ug/Kg 12/30/19 05:26 12/30/19 08:32 1

MB MB


<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Benzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Bromobenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Bromochloromethane


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RL MDL

Bromodichloromethane <96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1

MB MB


<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Bromoform

<482 482 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Bromomethane

<241 241 ug/Kg 12/30/19 05:26 12/30/19 08:32 12-Butanone (MEK)

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Carbon disulfide

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Carbon tetrachloride

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Chlorobenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Chlorodibromomethane

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Chloroethane

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Chloroform

<241 241 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Chloromethane



<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1cis-1,2-Dichloroethene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1cis-1,3-Dichloropropene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 11,2-Dibromo-3-chloropropane

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 11,2-Dibromoethane (EDB)

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Dibromomethane




<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Dichlorodifluoromethane



<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 11,1-Dichloroethene




<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 11,1-Dichloropropene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Ethylbenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Hexachlorobutadiene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Hexane

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Isopropylbenzene

<241 241 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Methylene chloride

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Methyl tert-butyl ether

<241 241 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Naphthalene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1n-Butylbenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1n-Propylbenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1p-Isopropyltoluene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1sec-Butylbenzene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Styrene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1tert-Butylbenzene



<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Tetrachloroethene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Toluene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1trans-1,2-Dichloroethene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1trans-1,3-Dichloropropene



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RL MDL

1,2,4-Trichlorobenzene <96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1

MB MB




<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Trichloroethene

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Trichlorofluoromethane

<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 11,2,3-Trichloropropane



<96.4 96.4 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Vinyl chloride

<145 145 ug/Kg 12/30/19 05:26 12/30/19 08:32 1Xylenes, Total


MB MB

Surrogate

12/30/19 05:26


119 12/30/19 05:26 12/30/19 08:32 1Dibromofluoromethane (Surr) 80 - 120

99 12/30/19 05:26 12/30/19 08:32 1Toluene-d8 (Surr) 80 - 120


Acetone 1870 1708 ug/Kg 91 42 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzene 934 990.6 ug/Kg 106 75 - 147

Bromobenzene 934 924.9 ug/Kg 99 77 - 132

Bromochloromethane 934 1034 ug/Kg 111 72 - 150

Bromodichloromethane 934 947.4 ug/Kg 101 74 - 144

Bromoform 934 922.0 ug/Kg 99 74 - 124

2-Butanone (MEK) 1870 2088 ug/Kg 112 50 - 150

Carbon disulfide 934 829.2 ug/Kg 89 71 - 135

Carbon tetrachloride 934 1013 ug/Kg 108 70 - 144

Chlorobenzene 934 900.5 ug/Kg 96 78 - 132

Chlorodibromomethane 934 947.5 ug/Kg 101 77 - 132

Chloroform 934 1034 ug/Kg 111 69 - 148

2-Chlorotoluene 934 879.6 ug/Kg 94 72 - 132

4-Chlorotoluene 934 869.1 ug/Kg 93 74 - 130

cis-1,2-Dichloroethene 934 985.7 ug/Kg 106 74 - 148

cis-1,3-Dichloropropene 934 978.3 ug/Kg 105 78 - 138

1,2-Dibromo-3-chloropropane 934 903.0 ug/Kg 97 50 - 150

1,2-Dibromoethane (EDB) 934 871.3 ug/Kg 93 80 - 134

Dibromomethane 934 952.2 ug/Kg 102 76 - 148

1,2-Dichlorobenzene 934 906.3 ug/Kg 97 76 - 127



1,1-Dichloroethane 934 978.7 ug/Kg 105 74 - 150

1,2-Dichloroethane 934 1001 ug/Kg 107 74 - 148

1,1-Dichloroethene 934 956.6 ug/Kg 102 74 - 139

1,2-Dichloropropane 934 970.8 ug/Kg 104 74 - 150

1,3-Dichloropropane 934 904.3 ug/Kg 97 80 - 136


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2,2-Dichloropropane 934 1192 ug/Kg 128 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1-Dichloropropene 934 1020 ug/Kg 109 73 - 144

Ethylbenzene 934 910.9 ug/Kg 98 78 - 131

Hexachlorobutadiene 934 1083 ug/Kg 116 50 - 150

Hexane 934 935.1 ug/Kg 100 50 - 150

Isopropylbenzene 934 880.9 ug/Kg 94 77 - 130

Methylene chloride 934 987.9 ug/Kg 106 50 - 150

Methyl tert-butyl ether 934 1018 ug/Kg 109 79 - 146

m,p-Xylene 934 945.1 ug/Kg 101 75 - 131

Naphthalene 934 961.4 ug/Kg 103 50 - 150

n-Butylbenzene 934 921.7 ug/Kg 99 73 - 131

n-Propylbenzene 934 900.9 ug/Kg 96 77 - 132

o-Xylene 934 909.9 ug/Kg 97 76 - 134

p-Isopropyltoluene 934 930.5 ug/Kg 100 73 - 128

sec-Butylbenzene 934 888.5 ug/Kg 95 72 - 129

Styrene 934 908.7 ug/Kg 97 75 - 138

tert-Butylbenzene 934 893.3 ug/Kg 96 73 - 128

1,1,1,2-Tetrachloroethane 934 964.2 ug/Kg 103 78 - 133

1,1,2,2-Tetrachloroethane 934 957.7 ug/Kg 103 78 - 141

Tetrachloroethene 934 935.3 ug/Kg 100 77 - 127

Toluene 934 901.0 ug/Kg 96 77 - 134

trans-1,2-Dichloroethene 934 1010 ug/Kg 108 76 - 139

trans-1,3-Dichloropropene 934 946.3 ug/Kg 101 77 - 138

1,2,3-Trichlorobenzene 934 1061 ug/Kg 114 50 - 150

1,2,4-Trichlorobenzene 934 1067 ug/Kg 114 65 - 133

1,1,1-Trichloroethane 934 1038 ug/Kg 111 74 - 144

1,1,2-Trichloroethane 934 862.9 ug/Kg 92 80 - 137

Trichloroethene 934 967.8 ug/Kg 104 75 - 142

1,2,3-Trichloropropane 934 807.1 ug/Kg 86 77 - 141

1,2,4-Trimethylbenzene 934 892.2 ug/Kg 96 71 - 134

1,3,5-Trimethylbenzene 934 910.6 ug/Kg 98 72 - 132

Xylenes, Total 1870 1855 ug/Kg 99 76 - 132


Surrogate

104

LCS LCS





Acetone <682 2390 2080 ug/Kg 87 42 - 150☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Benzene <136 1190 1160 ug/Kg 97 54 - 150☼

Bromobenzene <136 1190 1069 ug/Kg 90 56 - 136☼

Bromochloromethane <136 1190 1188 ug/Kg 100 57 - 150☼

Bromodichloromethane <136 1190 1071 ug/Kg 90 56 - 149☼


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Bromoform <136 1190 1015 ug/Kg 85 52 - 128☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

2-Butanone (MEK) <341 2390 2314 ug/Kg 97 50 - 150☼

Carbon disulfide <136 1190 897.9 ug/Kg 75 48 - 138☼

Carbon tetrachloride <136 1190 1131 ug/Kg 95 53 - 147☼

Chlorobenzene <136 1190 1020 ug/Kg 86 59 - 134☼

Chlorodibromomethane <136 1190 1094 ug/Kg 92 56 - 136☼

Chloroform <136 1190 1182 ug/Kg 99 49 - 150☼

2-Chlorotoluene <136 F1 1190 1992 F1 ug/Kg 167 50 - 137☼

4-Chlorotoluene <136 1190 1351 ug/Kg 113 44 - 149☼

cis-1,2-Dichloroethene <136 1190 1172 ug/Kg 98 53 - 150☼

cis-1,3-Dichloropropene <136 1190 1046 ug/Kg 88 58 - 138☼

1,2-Dibromo-3-chloropropane <136 F2 1190 463.6 ug/Kg 39 38 - 150☼

1,2-Dibromoethane (EDB) <136 1190 1078 ug/Kg 90 62 - 139☼

Dibromomethane <136 1190 1183 ug/Kg 99 57 - 150☼

1,2-Dichlorobenzene <136 1190 924.2 ug/Kg 77 53 - 131☼



1,1-Dichloroethane <136 1190 1139 ug/Kg 96 54 - 150☼

1,2-Dichloroethane <136 1190 1154 ug/Kg 97 54 - 150☼

1,1-Dichloroethene <136 1190 1059 ug/Kg 89 53 - 142☼

1,2-Dichloropropane <136 1190 1109 ug/Kg 93 57 - 150☼



1,1-Dichloropropene <136 1190 1111 ug/Kg 93 54 - 148☼

Ethylbenzene 137 1190 1290 ug/Kg 97 48 - 142☼

Hexachlorobutadiene <136 F2 1190 837.2 ug/Kg 70 12 - 150☼

Hexane <136 1190 1216 ug/Kg 102 10 - 150☼

Isopropylbenzene 458 1190 1947 ug/Kg 125 44 - 147☼

Methylene chloride <341 1190 1131 ug/Kg 95 50 - 150☼

Methyl tert-butyl ether <136 1190 1154 ug/Kg 97 60 - 150☼

m,p-Xylene 1310 F1 1190 3628 F1 ug/Kg 195 40 - 143☼

Naphthalene 605 1190 2153 ug/Kg 130 24 - 150☼

n-Butylbenzene 2710 F1 1190 6217 F1 ug/Kg 294 33 - 150☼

n-Propylbenzene 674 1190 2277 ug/Kg 134 44 - 147☼

o-Xylene 1800 F1 1190 4470 F1 ug/Kg 224 36 - 150☼

p-Isopropyltoluene 1000 F1 1190 2950 F1 ug/Kg 163 23 - 150☼

sec-Butylbenzene 1370 F1 1190 3610 F1 ug/Kg 188 26 - 150☼

Styrene <136 1190 1185 ug/Kg 99 47 - 150☼

tert-Butylbenzene <136 1190 1068 ug/Kg 90 39 - 148☼

1,1,1,2-Tetrachloroethane <136 1190 981.4 ug/Kg 82 59 - 136☼

1,1,2,2-Tetrachloroethane <136 F1 1190 2556 F1 ug/Kg 214 48 - 150☼

Tetrachloroethene <136 1190 1137 ug/Kg 95 50 - 136☼

Toluene <136 1190 1242 ug/Kg 97 50 - 144☼

trans-1,2-Dichloroethene <136 1190 1161 ug/Kg 97 55 - 144☼

trans-1,3-Dichloropropene <136 1190 1044 ug/Kg 88 58 - 138☼

1,2,3-Trichlorobenzene <136 1190 1334 ug/Kg 112 33 - 150☼

1,2,4-Trichlorobenzene <136 1190 1275 ug/Kg 107 45 - 133☼

1,1,1-Trichloroethane <136 1190 1152 ug/Kg 97 54 - 150☼

1,1,2-Trichloroethane <136 1190 1186 ug/Kg 99 60 - 146☼


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Trichloroethene <136 1190 1102 ug/Kg 92 52 - 150☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,2,3-Trichloropropane <136 1190 1085 ug/Kg 91 60 - 146☼

1,2,4-Trimethylbenzene 4730 F1 1190 9405 F1 ug/Kg 392 40 - 143☼

1,3,5-Trimethylbenzene 2290 F1 1190 5218 F1 ug/Kg 245 48 - 136☼

Xylenes, Total 3110 F1 2390 8098 F1 ug/Kg 209 40 - 150☼


Surrogate

97

MS MS





Acetone <682 2330 2229 ug/Kg 96 42 - 150 7 40☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Benzene <136 1170 1262 ug/Kg 108 54 - 150 8 23☼

Bromobenzene <136 1170 1207 ug/Kg 104 56 - 136 12 20☼

Bromochloromethane <136 1170 1375 ug/Kg 118 57 - 150 15 21☼

Bromodichloromethane <136 1170 1239 ug/Kg 106 56 - 149 15 20☼

Bromoform <136 1170 1124 ug/Kg 96 52 - 128 10 36☼

2-Butanone (MEK) <341 2330 2388 ug/Kg 102 50 - 150 3 19☼

Carbon disulfide <136 1170 966.0 ug/Kg 83 48 - 138 7 21☼

Carbon tetrachloride <136 1170 1234 ug/Kg 106 53 - 147 9 19☼

Chlorobenzene <136 1170 1160 ug/Kg 100 59 - 134 13 20☼

Chlorodibromomethane <136 1170 1179 ug/Kg 101 56 - 136 8 21☼

Chloroform <136 1170 1279 ug/Kg 110 49 - 150 8 20☼

2-Chlorotoluene <136 F1 1170 2135 F1 ug/Kg 183 50 - 137 7 24☼

4-Chlorotoluene <136 1170 1360 ug/Kg 117 44 - 149 1 22☼

cis-1,2-Dichloroethene <136 1170 1286 ug/Kg 110 53 - 150 9 21☼

cis-1,3-Dichloropropene <136 1170 1153 ug/Kg 99 58 - 138 10 20☼

1,2-Dibromo-3-chloropropane <136 F2 1170 1121 F2 ug/Kg 96 38 - 150 83 40☼

1,2-Dibromoethane (EDB) <136 1170 1103 ug/Kg 95 62 - 139 2 20☼

Dibromomethane <136 1170 1308 ug/Kg 112 57 - 150 10 21☼

1,2-Dichlorobenzene <136 1170 1102 ug/Kg 95 53 - 131 18 22☼



1,1-Dichloroethane <136 1170 1218 ug/Kg 105 54 - 150 7 19☼

1,2-Dichloroethane <136 1170 1267 ug/Kg 109 54 - 150 9 20☼

1,1-Dichloroethene <136 1170 1096 ug/Kg 94 53 - 142 3 24☼

1,2-Dichloropropane <136 1170 1346 ug/Kg 115 57 - 150 19 21☼



1,1-Dichloropropene <136 1170 1322 ug/Kg 113 54 - 148 17 20☼

Ethylbenzene 137 1170 1357 ug/Kg 105 48 - 142 5 29☼

Hexachlorobutadiene <136 F2 1170 1544 F2 ug/Kg 132 12 - 150 59 40☼

Hexane <136 1170 1284 ug/Kg 110 10 - 150 5 40☼


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Isopropylbenzene 458 1170 1825 ug/Kg 117 44 - 147 6 23☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Methylene chloride <341 1170 1248 ug/Kg 107 50 - 150 10 22☼

Methyl tert-butyl ether <136 1170 1296 ug/Kg 111 60 - 150 12 19☼

m,p-Xylene 1310 F1 1170 3031 F1 ug/Kg 148 40 - 143 18 35☼

Naphthalene 605 1170 2021 ug/Kg 121 24 - 150 6 37☼

n-Butylbenzene 2710 F1 1170 5128 F1 ug/Kg 207 33 - 150 19 40☼

n-Propylbenzene 674 1170 2208 ug/Kg 132 44 - 147 3 35☼

o-Xylene 1800 F1 1170 3478 ug/Kg 144 36 - 150 25 30☼

p-Isopropyltoluene 1000 F1 1170 2713 ug/Kg 147 23 - 150 8 25☼

sec-Butylbenzene 1370 F1 1170 3042 ug/Kg 144 26 - 150 17 26☼

Styrene <136 1170 1241 ug/Kg 107 47 - 150 5 21☼

tert-Butylbenzene <136 1170 1248 ug/Kg 107 39 - 148 16 26☼

1,1,1,2-Tetrachloroethane <136 1170 1124 ug/Kg 96 59 - 136 14 21☼

1,1,2,2-Tetrachloroethane <136 F1 1170 2665 F1 ug/Kg 229 48 - 150 4 22☼

Tetrachloroethene <136 1170 1216 ug/Kg 104 50 - 136 7 23☼

Toluene <136 1170 1268 ug/Kg 101 50 - 144 2 30☼

trans-1,2-Dichloroethene <136 1170 1260 ug/Kg 108 55 - 144 8 21☼

trans-1,3-Dichloropropene <136 1170 1186 ug/Kg 102 58 - 138 13 20☼

1,2,3-Trichlorobenzene <136 1170 1644 ug/Kg 141 33 - 150 21 28☼

1,2,4-Trichlorobenzene <136 1170 1473 ug/Kg 126 45 - 133 14 30☼

1,1,1-Trichloroethane <136 1170 1294 ug/Kg 111 54 - 150 12 20☼

1,1,2-Trichloroethane <136 1170 1288 ug/Kg 111 60 - 146 8 21☼

Trichloroethene <136 1170 1219 ug/Kg 105 52 - 150 10 20☼

1,2,3-Trichloropropane <136 1170 1203 ug/Kg 103 60 - 146 10 22☼

1,2,4-Trimethylbenzene 4730 F1 1170 7892 4 ug/Kg 271 40 - 143 17 35☼

1,3,5-Trimethylbenzene 2290 F1 1170 4146 F1 ug/Kg 159 48 - 136 23 28☼

Xylenes, Total 3110 F1 2330 6509 ug/Kg 146 40 - 150 22 33☼


Surrogate

91

MSD MSD




Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography


RL MDL

PCB-1016 <0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1

MB MB


<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1221

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1232

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1242

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1248

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1254

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1260

<0.0482 0.0482 mg/Kg 12/20/19 12:30 12/23/19 13:18 1PCB-1268


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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)


DCB Decachlorobiphenyl (Surr) 62 10 - 110 12/23/19 13:18 1

MB MB

Surrogate

12/20/19 12:30


58 12/20/19 12:30 12/23/19 13:18 1Tetrachloro-m-xylene 10 - 110


PCB-1016 0.317 0.2016 mg/Kg 64 30 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

PCB-1260 0.317 0.2331 mg/Kg 74 24 - 110

DCB Decachlorobiphenyl (Surr) 10 - 110

Surrogate

70

LCS LCS


64Tetrachloro-m-xylene 10 - 110


RL MDL

PCB-1016 <0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1

MB MB


<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1221

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1232

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1242

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1248

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1254

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1260

<0.0481 0.0481 mg/Kg 12/30/19 13:05 01/05/20 20:32 1PCB-1268

DCB Decachlorobiphenyl (Surr) 101 10 - 110 01/05/20 20:32 1

MB MB

Surrogate

12/30/19 13:05


100 12/30/19 13:05 01/05/20 20:32 1Tetrachloro-m-xylene 10 - 110


PCB-1016 0.316 0.2342 mg/Kg 74 30 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

PCB-1260 0.316 0.2757 mg/Kg 87 24 - 110

DCB Decachlorobiphenyl (Surr) 10 - 110

Surrogate

82

LCS LCS


73Tetrachloro-m-xylene 10 - 110


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Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC)


RL MDL

Diesel <9.58 9.58 mg/Kg 12/27/19 10:21 12/30/19 17:24 1

MB MB


<9.58 9.58 mg/Kg 12/27/19 10:21 12/30/19 17:24 1Gasoline

<9.58 9.58 mg/Kg 12/27/19 10:21 12/30/19 17:24 1Waste Oil

<14.4 14.4 mg/Kg 12/27/19 10:21 12/30/19 17:24 1Total Extractable Hydrocarbons

n-Octacosane 81 10 - 123 12/30/19 17:24 1

MB MB

Surrogate

12/27/19 10:21



Diesel 130 101.8 mg/Kg 78 18 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

84

LCS LCS



Diesel <19.5 F1 131 3672 F1 mg/Kg 2810 18 - 135

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

10

MS MS



Diesel <19.5 F1 131 3292 F1 mg/Kg 2512 18 - 135 11 40

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

n-Octacosane X 10 - 123

Surrogate

7

MSD MSD



RL MDL

Diesel <9.52 9.52 mg/Kg 12/30/19 12:59 01/06/20 09:11 1

MB MB


<9.52 9.52 mg/Kg 12/30/19 12:59 01/06/20 09:11 1Gasoline

<9.52 9.52 mg/Kg 12/30/19 12:59 01/06/20 09:11 1Waste Oil

<14.3 14.3 mg/Kg 12/30/19 12:59 01/06/20 09:11 1Total Extractable Hydrocarbons


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Method: OA-2 - Iowa - Extractable Petroleum Hydrocarbons (GC) (Continued)


n-Octacosane 73 10 - 123 01/06/20 09:11 1

MB MB

Surrogate

12/30/19 12:59



Diesel 127 84.72 mg/Kg 67 18 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

74

LCS LCS


Method: 6010C - Metals (ICP)


RL MDL

Arsenic <2.88 2.88 mg/Kg 12/23/19 09:46 12/30/19 12:58 1

MB MB


<0.719 0.719 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Barium

<0.719 0.719 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Cadmium

<0.719 0.719 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Chromium

<3.59 3.59 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Lead

<3.59 3.59 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Selenium

<0.719 0.719 mg/Kg 12/23/19 09:46 12/30/19 12:58 1Silver


Arsenic 155 162.3 mg/Kg 105 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 77.3 74.57 mg/Kg 96 80 - 120

Cadmium 77.3 74.05 mg/Kg 96 80 - 120

Chromium 77.3 71.98 mg/Kg 93 80 - 120

Lead 155 150.7 mg/Kg 97 80 - 120

Selenium 309 297.0 mg/Kg 96 80 - 120

Silver 77.3 75.67 mg/Kg 98 80 - 120


Arsenic 11.3 194 212.6 mg/Kg 104 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 210 F1 F2 96.8 272.0 F1 mg/Kg 64 75 - 125☼

Cadmium <2.57 96.8 94.37 mg/Kg 98 75 - 125☼

Chromium 18.8 96.8 104.4 mg/Kg 88 75 - 125☼


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Method: 6010C - Metals (ICP) (Continued)


Lead 24.8 194 199.9 mg/Kg 90 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Selenium <12.8 387 379.1 mg/Kg 98 75 - 125☼

Silver <2.57 96.8 95.55 mg/Kg 99 75 - 125☼


Arsenic 11.3 180 205.6 mg/Kg 108 75 - 125 3 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 210 F1 F2 90.1 346.8 F1 F2 mg/Kg 152 75 - 125 24 20☼

Cadmium <2.57 90.1 86.35 mg/Kg 96 75 - 125 9 20☼

Chromium 18.8 90.1 105.2 mg/Kg 96 75 - 125 1 20☼

Lead 24.8 180 195.7 mg/Kg 95 75 - 125 2 20☼

Selenium <12.8 361 352.7 mg/Kg 98 75 - 125 7 20☼

Silver <2.57 90.1 93.08 mg/Kg 103 75 - 125 3 20☼

Client Sample ID: EB-9 (0-1)Lab Sample ID: 310-172445-14 DUMatrix: Soil Prep Type: Total/NAAnalysis Batch: 266336 Prep Batch: 265445

Arsenic 13.2 10.85 mg/Kg 19 20☼

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Barium 232 230.7 mg/Kg 0.7 20☼

Cadmium <1.88 <1.88 mg/Kg NC 20☼

Chromium 20.6 21.63 mg/Kg 5 20☼

Lead 12.4 13.58 mg/Kg 9 20☼

Selenium <9.38 <9.42 mg/Kg NC 20☼

Silver <1.88 <1.88 mg/Kg NC 20☼

Method: 7471B - Mercury (CVAA)


RL MDL

Mercury <0.0178 0.0178 mg/Kg 12/20/19 12:11 12/23/19 13:23 1

MB MB



Mercury 0.152 0.1490 mg/Kg 98 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


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GC/MS VOA

Prep Batch: 265360


Soil 5035310-172445-1 EB-1 (0-1) Total/NA

Soil 5035310-172445-2 EB-2 (0-1) Total/NA

Soil 5035310-172445-4 EB-3 (5-6) Total/NA

Soil 5035310-172445-6 EB-4 (35-36) Total/NA

Soil 5035310-172445-8 EB-5 (1-2) Total/NA

Soil 5035310-172445-11 EB-7 (0-1) Total/NA

Soil 5035310-172445-12 EB-8 (0-1) Total/NA

Soil 5035310-172445-15 EB-9 (1-2) Total/NA

Soil 5035310-172445-17 EB-10 (12-13) Total/NA

Soil 5035310-172445-18 EB-11 (15-16) Total/NA

Soil 5035310-172445-20 EB-12 (20-21) Total/NA

Solid 5035MB 310-265360/1-A Method Blank Total/NA

Solid 5035LCS 310-265360/2-A Lab Control Sample Total/NA

Soil 5035310-172445-1 MS EB-1 (0-1) Total/NA

Soil 5035310-172445-1 MSD EB-1 (0-1) Total/NA



Soil 8260D 265360310-172445-1 EB-1 (0-1) Total/NA

Soil 8260D 265360310-172445-2 EB-2 (0-1) Total/NA

Soil 8260D 265360310-172445-4 EB-3 (5-6) Total/NA

Soil 8260D 265360310-172445-6 EB-4 (35-36) Total/NA

Soil 8260D 265360310-172445-8 EB-5 (1-2) Total/NA

Soil 8260D 265360310-172445-11 EB-7 (0-1) Total/NA

Soil 8260D 265360310-172445-12 EB-8 (0-1) Total/NA

Soil 8260D 265360310-172445-15 EB-9 (1-2) Total/NA

Soil 8260D 265360310-172445-17 EB-10 (12-13) Total/NA

Soil 8260D 265360310-172445-18 EB-11 (15-16) Total/NA

Soil 8260D 265360310-172445-20 EB-12 (20-21) Total/NA

Solid 8260D 265360MB 310-265360/1-A Method Blank Total/NA

Solid 8260D 265360LCS 310-265360/2-A Lab Control Sample Total/NA

Soil 8260D 265360310-172445-1 MS EB-1 (0-1) Total/NA

Soil 8260D 265360310-172445-1 MSD EB-1 (0-1) Total/NA

Prep Batch: 266150


Soil 5035310-172445-9 EB-6 (0-1) Total/NA







Soil 8260D 266150310-172445-9 EB-6 (0-1) Total/NA

Solid 8260D 266150MB 310-266150/1-A Method Blank Total/NA

Solid 8260D 266150LCS 310-266150/2-A Lab Control Sample Total/NA

Soil 8260D 266150310-172445-9 MS EB-6 (0-1) Total/NA

Soil 8260D 266150310-172445-9 MSD EB-6 (0-1) Total/NA


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GC Semi VOA

Prep Batch: 265491


Soil 3546310-172445-1 EB-1 (0-1) Total/NA

Soil 3546310-172445-5 EB-4 (0-1) Total/NA

Soil 3546310-172445-10 EB-6 (5-6) Total/NA

Soil 3546310-172445-11 EB-7 (0-1) Total/NA

Soil 3546310-172445-14 EB-9 (0-1) Total/NA

Soil 3546310-172445-16 EB-10 (0-1) Total/NA

Soil 3546310-172445-19 EB-11 (16-17) Total/NA

Soil 3546310-172445-20 EB-12 (20-21) Total/NA





Soil 8082A 265491310-172445-1 EB-1 (0-1) Total/NA

Soil 8082A 265491310-172445-5 EB-4 (0-1) Total/NA

Soil 8082A 265491310-172445-10 EB-6 (5-6) Total/NA

Soil 8082A 265491310-172445-11 EB-7 (0-1) Total/NA

Soil 8082A 265491310-172445-14 EB-9 (0-1) Total/NA

Soil 8082A 265491310-172445-16 EB-10 (0-1) Total/NA

Soil 8082A 265491310-172445-19 EB-11 (16-17) Total/NA

Soil 8082A 265491310-172445-20 EB-12 (20-21) Total/NA

Solid 8082A 265491MB 310-265491/1-A Method Blank Total/NA

Solid 8082A 265491LCS 310-265491/2-A Lab Control Sample Total/NA

Prep Batch: 266074


Soil 3546310-172445-1 EB-1 (0-1) Total/NA

Soil 3546310-172445-2 EB-2 (0-1) Total/NA

Soil 3546310-172445-4 EB-3 (5-6) Total/NA

Soil 3546310-172445-6 EB-4 (35-36) Total/NA

Soil 3546310-172445-8 EB-5 (1-2) Total/NA

Soil 3546310-172445-9 EB-6 (0-1) Total/NA

Soil 3546310-172445-11 EB-7 (0-1) Total/NA

Soil 3546310-172445-12 EB-8 (0-1) Total/NA

Soil 3546310-172445-15 EB-9 (1-2) Total/NA

Soil 3546310-172445-18 EB-11 (15-16) Total/NA

Soil 3546310-172445-20 EB-12 (20-21) Total/NA







Soil OA-2 266074310-172445-1 EB-1 (0-1) Total/NA





Solid OA-2 266074MB 310-266074/1-A Method Blank Total/NA

Solid OA-2 266074LCS 310-266074/2-A Lab Control Sample Total/NA


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GC Semi VOA

Prep Batch: 266264


Soil 3546310-172445-17 EB-10 (12-13) Total/NA



Prep Batch: 266266


Soil 3546310-172445-2 EB-2 (0-1) Total/NA





Soil 8082A 266266310-172445-2 EB-2 (0-1) Total/NA

Solid 8082A 266266MB 310-266266/1-A Method Blank Total/NA

Solid 8082A 266266LCS 310-266266/2-A Lab Control Sample Total/NA




Solid OA-2 266264MB 310-266264/1-A Method Blank Total/NA

Solid OA-2 266264LCS 310-266264/2-A Lab Control Sample Total/NA










Soil OA-2 266074310-172445-1 MS EB-1 (0-1) Total/NA

Soil OA-2 266074310-172445-1 MSD EB-1 (0-1) Total/NA






Soil 8082A 266266310-172445-2 EB-2 (0-1) Total/NA

Metals

Prep Batch: 265445


Soil 3050B310-172445-1 EB-1 (0-1) Total/NA

Soil 3050B310-172445-2 EB-2 (0-1) Total/NA

Soil 3050B310-172445-3 EB-3 (0-1) Total/NA

Soil 3050B310-172445-5 EB-4 (0-1) Total/NA

Soil 3050B310-172445-7 EB-5 (0-1) Total/NA


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l I l I

[------

[-------



Metals (Continued)

Prep Batch: 265445 (Continued)


Soil 3050B310-172445-10 EB-6 (5-6) Total/NA

Soil 3050B310-172445-11 EB-7 (0-1) Total/NA

Soil 3050B310-172445-13 EB-8 (10-11) Total/NA

Soil 3050B310-172445-14 EB-9 (0-1) Total/NA

Soil 3050B310-172445-16 EB-10 (0-1) Total/NA

Soil 3050B310-172445-19 EB-11 (16-17) Total/NA

Soil 3050B310-172445-20 EB-12 (20-21) Total/NA

Solid 3050BMB 310-265445/1-A Method Blank Total/NA

Solid 3050BLCS 310-265445/2-A Lab Control Sample Total/NA

Soil 3050B310-172445-1 MS EB-1 (0-1) Total/NA

Soil 3050B310-172445-1 MSD EB-1 (0-1) Total/NA

Soil 3050B310-172445-14 DU EB-9 (0-1) Total/NA

Prep Batch: 265487


Soil 7471B310-172445-1 EB-1 (0-1) Total/NA

Soil 7471B310-172445-2 EB-2 (0-1) Total/NA

Soil 7471B310-172445-3 EB-3 (0-1) Total/NA

Soil 7471B310-172445-5 EB-4 (0-1) Total/NA

Soil 7471B310-172445-7 EB-5 (0-1) Total/NA

Soil 7471B310-172445-10 EB-6 (5-6) Total/NA

Soil 7471B310-172445-11 EB-7 (0-1) Total/NA

Soil 7471B310-172445-13 EB-8 (10-11) Total/NA

Soil 7471B310-172445-14 EB-9 (0-1) Total/NA

Soil 7471B310-172445-16 EB-10 (0-1) Total/NA

Soil 7471B310-172445-19 EB-11 (16-17) Total/NA

Soil 7471B310-172445-20 EB-12 (20-21) Total/NA

Solid 7471BMB 310-265487/1-A Method Blank Total/NA

Solid 7471BLCS 310-265487/2-A Lab Control Sample Total/NA



Soil 7471B 265487310-172445-1 EB-1 (0-1) Total/NA

Soil 7471B 265487310-172445-2 EB-2 (0-1) Total/NA

Soil 7471B 265487310-172445-3 EB-3 (0-1) Total/NA

Soil 7471B 265487310-172445-5 EB-4 (0-1) Total/NA

Soil 7471B 265487310-172445-7 EB-5 (0-1) Total/NA

Soil 7471B 265487310-172445-10 EB-6 (5-6) Total/NA

Soil 7471B 265487310-172445-11 EB-7 (0-1) Total/NA

Soil 7471B 265487310-172445-13 EB-8 (10-11) Total/NA

Soil 7471B 265487310-172445-14 EB-9 (0-1) Total/NA

Soil 7471B 265487310-172445-16 EB-10 (0-1) Total/NA

Soil 7471B 265487310-172445-19 EB-11 (16-17) Total/NA

Soil 7471B 265487310-172445-20 EB-12 (20-21) Total/NA

Solid 7471B 265487MB 310-265487/1-A Method Blank Total/NA

Solid 7471B 265487LCS 310-265487/2-A Lab Control Sample Total/NA



Soil 6010C 265445310-172445-1 EB-1 (0-1) Total/NA

Soil 6010C 265445310-172445-2 EB-2 (0-1) Total/NA


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Metals (Continued)

Analysis Batch: 266336 (Continued)


Soil 6010C 265445310-172445-3 EB-3 (0-1) Total/NA

Soil 6010C 265445310-172445-5 EB-4 (0-1) Total/NA

Soil 6010C 265445310-172445-7 EB-5 (0-1) Total/NA

Soil 6010C 265445310-172445-10 EB-6 (5-6) Total/NA

Soil 6010C 265445310-172445-11 EB-7 (0-1) Total/NA

Soil 6010C 265445310-172445-13 EB-8 (10-11) Total/NA

Soil 6010C 265445310-172445-14 EB-9 (0-1) Total/NA

Soil 6010C 265445310-172445-16 EB-10 (0-1) Total/NA

Soil 6010C 265445310-172445-19 EB-11 (16-17) Total/NA

Soil 6010C 265445310-172445-20 EB-12 (20-21) Total/NA

Solid 6010C 265445MB 310-265445/1-A Method Blank Total/NA

Solid 6010C 265445LCS 310-265445/2-A Lab Control Sample Total/NA

Soil 6010C 265445310-172445-1 MS EB-1 (0-1) Total/NA

Soil 6010C 265445310-172445-1 MSD EB-1 (0-1) Total/NA

Soil 6010C 265445310-172445-14 DU EB-9 (0-1) Total/NA


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Lab ChronicleClient: Thiele Geotech Inc. Job ID: 310-172445-1Project/Site: Warehouse Property SDG: 19631.01

Client Sample ID: EB-1 (0-1) Lab Sample ID: 310-172445-1Matrix: SoilDate Collected: 12/16/19 10:30


Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Prep 3546 266074 12/27/19 10:21 EAM TAL CFTotal/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260D 1 265370 12/20/19 08:51 DLK TAL CFTotal/NA


Analysis 8082A 1 265623 12/23/19 14:23 BBW TAL CFTotal/NA

Prep 3050B 265445 12/23/19 09:46 DLS TAL CFTotal/NA

Analysis 6010C 3 266336 12/30/19 13:03 CTB TAL CFTotal/NA

Prep 7471B 265487 12/20/19 12:11 HIS TAL CFTotal/NA

Analysis 7471B 1 265722 12/23/19 13:43 HIS TAL CFTotal/NA



Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











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Prep 3050B 12/23/19 09:46 DLS265445 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3546 12/20/19 12:30 EAM265491 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



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Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3050B 12/23/19 09:46 DLS265445 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/30/19 05:26 TCH266150 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260D 1 266187 12/30/19 16:12 TCH TAL CFTotal/NA


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Prep 3546 12/20/19 12:30 EAM265491 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



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Prep 3050B 12/23/19 09:46 DLS265445 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA






Prep 3546 12/20/19 12:30 EAM265491 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3546 12/20/19 12:30 EAM265491 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA







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Prep 3546 12/30/19 12:59 EAM266264 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA




Prep 3546 12/20/19 12:30 EAM265491 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA








Prep 3546 12/27/19 10:21 EAM266074 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



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Prep 5035 12/20/19 05:43 TCH265360 TAL CF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











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Accreditation/Certification SummaryClient: Thiele Geotech Inc. Job ID: 310-172445-1Project/Site: Warehouse Property SDG: 19631.01

Laboratory: Eurofins TestAmerica, Cedar FallsUnless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.

Authority Program Identification Number Expiration Date

Oregon IA100001NELAP 09-29-20

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which

the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

OA-2 3546 Soil Total Extractable Hydrocarbons


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Method SummaryJob ID: 310-172445-1Client: Thiele Geotech Inc.


Method Method Description LaboratoryProtocol

SW8468260D Volatile Organic Compounds by GC/MS TAL CF

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CF

Iowa DNROA-2 Iowa - Extractable Petroleum Hydrocarbons (GC) TAL CF

SW8466010C Metals (ICP) TAL CF

SW8467471B Mercury (CVAA) TAL CF

SW8463050B Preparation, Metals TAL CF

SW8463546 Microwave Extraction TAL CF

SW8465035 Purge and Trap for Methanol Extractions TAL CF

SW8465035 Purge and Trap for Solids TAL CF

SW8467471B Preparation, Mercury TAL CF

Protocol References:

Iowa DNR = Iowa Department of Natural Resources

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.




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-:~ eurofins Environment Testing TestAmerica 11111 Ii I ll Ill l Ill II lll l ll

310-172445 Chain of Custody

Cooler/Sample Receipt and Temperature Log r-onn

Project:

Received By:

Delivery Type: 0 UPS ~ FedEx O FedEx Ground D Spee-Dee

D Lab Courier tJ Lab Field Services D Client Drop-off

0 US Mail

D Other: --------Condition of Cooler/Containers

Sample(s) received in Cooler? If yes: Cooler ID:

Multiple Coolers? If yes: Cooler # of

Cooler Custody Seals Present? If yes: Cooler custody seals intact? □ No

Sample Custody Seals Present? If yes: Sample custody seals intact?□ Yes □ No

Trip Blank Present? D Yes If yes: Which VOA samples are in cooler? l

D Blue ice D Dry ice D Other: ------ □ NONE

Thermometer ID: Correction Factor (°C):

erature - If no temp blank, or temp blank temperature above criteria, proceed to Sample Container Temperature

Uncorrected Temp (°C): Corrected Temp (°C):

• Sam le Container Tem CONTAINER 2

Container(s) used:

Uncorrected Temp (0 C):

Corrected Temp (°C):

Exce tions Noted

1) If temperature exceeds criteria, was sample(s) received same day of sampling?

a) If yes: Is there evidence that the chilling process began? □ Yes □ Yes

□ No □ No

2) If temperature is <0°C, are there obvious signs that the integrity of sample containers is compromised? (e.g ., bulging septa, broken/cracked bottles, frozen solid?) D Yes D No

NOTE: If es, contact PM before Additional Comments

Document: CF-LG-Wl-002 Revision : 25 Date: 06/17/2019 Eurofins TestAmerica, Cedar Falls

General temperature criteria is Oto 6°C Bacteria temperature criteria is Oto 10°C

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123456789101112131415


Cedar Fa lls, IA 5061 3

phone 3 19.277.240 1 fax 319.277.2425

Client Contact


13478 Chandler Road

Omaha , NE 68138

402.556.2171

402.556.7831


7502 Crown Point Ave , Omaha , NE

PO#


EB-I (0- 1)

EB-2 (0-1)

EB-3 (0- 1)

EB-3 (5-6)

EB-4 (0- 1)

EB-4 (35-36)

EB-5 (0- 1)

EB-5 (1 -2)

EB-6 (0- 1)

EB-6 ( 1-2)

EB-7 (0-1)

EB-8 (0-1)

Test America Chain of Custody Record THE LEADER IN ENVIRONMENT AL TESTING

TestAmerica Laboratories, Inc. Project Manager: Robert Miller Site Contact: Jeremy Kendle Date: 12/ 18 / 19 COC No:

Tel/Fax : Lab Contact: Carrier: I of 2 COCs

Analysis Turnaround Time Job No. 19631.01

Calendar ( C) or Work Days (W)

w;eo;ceceo.C-s, •• ~..,~ "' ,,, " ..

D 2weeks · / :; SDG No. 00

D I week < ~

D 2 days u u ~ .. 0 "'

D 'li. Q:) < I day >- u E .. r-.. :i:: Q:) ..,. "' "" 0 ,... r-

"' 00 oll 1l ,... ,... e Sample Sample Sa mple .. ,... 00 00 Q:)

# or .. ' < < 0

Date Time Type Matrix Cont ~ cS C. .. ;; Sample Speci fi e Notes: "" "' "'

12/ 16/20 19 10:30 Grab so 2 X X X X

I 2/ 16/2019 12:30 Grab so 2 X X X X

12/16/20 19 13:45 Grab so I X

12/16/2019 13:50 Grab so I X X

12/ 16/2019 14:30 Grab so I X X

12/1 6/2019 15 :15 Grab so I X X

I 2/17/2019 8:45 Grab so I X

12/17/20 I 9 8:45 Grab so I X X

12/17/ 19 9:00 Grab so I X X

12/17/1 9 9:00 Grab so I X X

12/17/1 9 10:00 Grab so 2 X X X X

12/ 17/ 19 11 : IO Grab so I X X

Preservation Use¥!= 1i;). 2= HCI; 3= H2S04; 4=HN03; S=NaOH; 6= Other

Possible Hazard ldentificatio11

~ Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)

D Non-Ha=ard □Flammable □Skin Irritant Poison B D Unknown D Return To Client ~posa/ By Lab D Archive For Months

Special Instructions/QC Requirements & Comments:

,,,,--,/1 -Relinqui(//4 ~ /1/' ~ ci,:_~lk.. C-z eD\e.G~ Dat~rrime: 14/(5 Received by: I~ Comi"Ultl ltq I Date/Time:

~\.;;;::,,_ I'-,;, :~o ht'C"" Relinquishif ( Company: Dateffime: Received by: Company: Date/Time:

Relinquished by: Company: Date/Time: Received by: Company: Date/Time:

Page 80 of 81

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Cedar Falls, IA 506 13

phone 3 19.277.240 I fax 3 I 9.277.2425

Client Contact


13478 Chandler Road

Omaha , NE 68138

402.556.2171

402.556.7831


7502 Crown Point Ave, Omaha, NE

PO#


EB-8 (1 0-11 )

EB-9 (0-1 )

EB-9 (1-2)

EB-10 (0-1)

EB-1 0 (12-13)

EB-I I (15-16)

EB- I I ( 1 6-1 7)

EB-1 2 (20-2 1)

TestAmerica Chain of Custody Record THE LEADER IN ENVIRONMENTAL TESTING

TestAmerica Laboratories, .Inc. Project Manager: Robert Miller Site Contact: Jerem y Kendle Date: 12/ 18 / 19 COC No:

Tel/Fax: Lab Contact: Carrier: _2_ of _2_ COCs

Analysis Turnaround Time Job No. 19631 .01

Calendar ( C) or Work Days (W)

TATifdifTerentfromBcluw ---~ "' " ;:;

D '"'°'~ :E SDG No. 00

D I week <: a: D 2days u u .. a:

D C. 0 o:l <: I day e > u ;:::

" :i: CQ ... ... rJJ 0 N r--~ "' "' 00 ~ f- N 0

Sample Sample Sample j '"I 00 00 CQ

Hor <: <: 0

Date Time Type Matrix Cont. i: < ... ... 0 0 "' "' "' Sample Specific Notes:

12/17/20 19 11 :20 Grab so I X

I 2/ 17/201 9 12:30 Grab so 1 X X

12/17/20 19 12:30 Grab so J X X

12/18/20 19 12:40 Grab so J X X

12/18/20 19 13:00 Grab so J X X

12/ 17/2019 14: 10 Grab so J X X

12/17/20 19 14:10 Grab so I X X

12/17/20 19 14:40 Grab so 2 X X X X

Preservation Use,V I= lee~= HCI; 3= H2S04; 4=HN03; S=NaOI-I ; 6= Other

Possible Ht1zard ~n P5Q

Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month)

D No n-1-fa=ard D Flammable D Skin Irritant Poison B D Unknown ./ D Return To Client Aisposal By Lab D Archive For Months Special Instructions/QC Requirements & Comments:

/ /)

Relinq/ #~ ~ Company: '..t /--'l.-- (., -lee Date/Tirne1l/,8 . Rece ived by:\~ Cornp7:1--J ( 4 I l ,,; Datfoeo~ ·v \ , 'fen · l /0)::____0

Relin~by: ( Company: Date/Time: Received by: v Company: Date/Time:

Relinquished by: Company: Date/Time: Received by: Company: Date/Time:

Login Sample Receipt Checklist

Client: Thiele Geotech Inc. Job Number: 310-172445-1

SDG Number: 19631.01

Login Number: 172445

Question Answer Comment

Creator: Homolar, Dana J

List Source: Eurofins TestAmerica, Cedar Falls

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

FalseThere are no discrepancies between the containers received and the COC. Label has EB-6 (5-6) and COC has EB-6 (1-2) logged per container, time matches

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Documents

RE: PHASE II ENVIRONMENTAL SITE ASSESSMENT WAREHOUSE