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REQUEST FOR PROPOSALS
BENEFICIAL REUSE BIOSOLIDS INCINERATOR ASH
REGULATORY APPROVAL PROJECT
JULY 2016
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 1 of 10
This Request for Proposal (RFP) is being sent to interested parties for developing and implementing a Project for obtaining Regulatory Approval for the Beneficial Reuse of Biosolids Incinerator Ash generated at the Southerly Wastewater Treatment Center (WWTC) and Westerly WWTC for the Northeast Ohio Regional Sewer District (NEORSD). Proposals for providing these services will be received until the close of business (4:30 P.M.) on Friday, July 29, 2016. Proposals shall be no more than 25 printed pages and the font size shall be equivalent to Times New Roman 12 pt or larger (See Section 3.0). Proposals are to be delivered to: Julius Ciaccia, Chief Executive Officer Northeast Ohio Regional Sewer District 3900 Euclid Avenue Cleveland, OH 44115-2504 Attn: Robin Halperin, Manager of Regulatory Compliance Late submittals will not be considered. Questions regarding this RFP shall be directed to Robin Halperin by calling (216) 881-6600, ext. 6465 or at [email protected]. This RFP is organized as follows:
SECTION 1.0 INTRODUCTION SECTION 2.0 SCOPE OF SERVICES SECTION 3.0 PROPOSAL CONTENT & FORMAT SECTION 4.0 EVALUATION & SELECTION PROCESS
Various supporting and informational documents are referenced throughout this RFP. Unless otherwise noted, these documents are available on the Consultant and Contractor Resource Page on the District’s internet site (www.neorsd.org). Any future addenda related to this project will be posted to the NEORSD website under the “Bids and Proposals” section and within the NEORSD Sharefile system. ATTACHMENTS Attachment 1 Southerly WWTC Ash Analytical Report Attachment 2 Westerly WWTC Ash Analytical Report
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 2 of 10
SECTION 1.0 INTRODUCTION 1.1 BACKGROUND INFORMATION The Northeast Ohio Regional Sewer District (District) is a political subdivision of the State of Ohio and organized under Chapter 6119 of the Ohio Revised Code. Originally named the Cleveland Regional Sewer District, it was created in 1972 to assume the ownership, operation and maintenance of wastewater collection, treatment and disposal facilities servicing the member communities in the Cleveland metropolitan area. The District currently operates three wastewater treatment plant facilities and a wastewater collection system. The District’s mission is to serve the public by providing cost-effective wastewater collection and treatment services that protect health and the environment. Southerly Wastewater Treatment Center The largest of the District’s wastewater treatment plans is the Southerly Wastewater Treatment Center (WWTC) located at 6000 Canal Road, Cuyahoga Heights, Ohio. Southerly serves a population of more than 601,000 in the Greater Cleveland area with an average daily flow of 125 million gallons per day (mgd). The facility can provide complete treatment to a maximum of 400 mgd, and an additional 335 mgd of storm water can receive primary treatment only. The plant receives wastewater 24 hours per day, seven days a week. The plant also receives and processes biosolids from the Easterly Wastewater Treatment Plant (WWTP). The wastewater contains solid materials which are dewatered into a more concentrated sewage sludge cake and incinerated on site in three (3) Fluidized Bed Incinerators (FBIs). Ash from the FBIs is mixed with water and conveyed as a slurry to one of three (3) ash lagoons. The ash lagoons are located at the southern end of the property, south of Canal Road between the Ohio Canal and the Cuyahoga River. In the lagoons, the ash is allowed to settle by gravity and the carrier water is returned to the WWTC for processing. A copy of the most recent analytical results for Southerly ash is found in Attachment 1. Ash is generated year round. After a period of time, the accumulated ash in the lagoons must be removed to allow room for new ash. Each lagoon holds approximately 30,000 cubic yards of ash. The Southerly WWTC generates approximately 25,000 – 30,000 cubic yards of ash each year. Previous ash lagoon cleaning projects entailed cleaning of the lagoons and placing the ash on-site in the South Fill Area and North Fill Area. The District no longer has space to store the ash removed from the lagoons due to the closure of the South Fill Area in 2007. Westerly Wastewater Treatment Center The Westerly WWTC sits on a 14-acre triangular site directly east of Edgewater State Park on the shore of Lake Erie. Westerly serves approximately 103,000 residents from Cleveland's west side. This treatment plant processes an average flow of 26 mgd of wastewater, and has a Combined Sewer Overflow Treatment Facility, which provides storage for 6 million gallons and preliminary treatment and settling for up to 300 mgd during wet weather flows. The plant
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 3 of 10
receives wastewater 24 hours per day, seven days a week. Sludge removed from the wastewater treatment process is incinerated on-site in two (2) Multiple Hearth Incinerators (MHIs). Since Westerly lacks storage space for ash, the ash is removed from the MHIs and placed directly into hauling trucks for disposal. Westerly generates approximately 5,000 dry tons a year of ash. Approximately 330 truckloads of ash each year are removed from the Westerly WWTC. A copy of the most recent analytical results for Westerly ash is found in Attachment 2. 1.2 PROJECT PUPROSE The District is soliciting proposals for innovative, environmentally-friendly, sustainable and cost-effective approaches to reuse of the ash material from the Westerly and Southerly WWTCs. It is the District’s intent to hire one or more firms (Consultant) for Professional Services to identify viable reuse options for the ash and obtain the necessary regulatory approval for the identified reuse options. Consultants with beneficial reuse options for the District’s biosolids incinerator ash that are successful in obtaining the necessary regulatory approval will be eligible to submit proposals for the subsequent work which includes management of the Southerly Ash Lagoons and reuse of the District’s ash from Southerly and Westerly WWTCs.
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 4 of 10
SECTION 2.0 SCOPE OF SERVICES
2.1 REQUESTED SERVICES The District is seeking consulting services for the following tasks: Task 1 – Reuse Options Identify innovative, environmentally responsible, cost-effective and sustainable solutions for the reuse of the ash material generated at Southerly and Westerly WWTCs. The District, in consultation with the Consultant, will select the most promising solutions for which to pursue regulatory approval.
Task 2 – Regulatory Approval Obtain Regulatory approval for the selected reuse options. Consultant shall conduct any required research, testing or other analyses needed to obtain regulatory approval for the reuse options. Consultant shall provide draft permit/regulatory approval applications for District review and approval prior to submission to the appropriate regulatory agency. Consultant shall respond to inquiries from regulatory agencies relating to the regulatory approval process for the selected beneficial reuse options.
Task 3 – Summary Report Prepare a Summary Report detailing the approved ash reuse option(s), implementation considerations, and estimation of the environmental benefit for each reuse option(s).
2.2 PROJECT MANAGEMENT Project Management is a critical activity to be included within the execution of all tasks identified above. Utilize procedures related to cost estimating, scheduling, project documentation, risk management, QA/QC and others as necessary to enhance budget, scope and time management. In order to ensure that tasks authorized under this contract are successfully completed in a timely manner and to the satisfaction of the District, the selected Consultant(s) shall provide Monthly Project Summary Reports, conduct Project Meetings as required and prepare Monthly Invoices. 2.3 DELIVERY OF SERVICES The selected Consultant(s) shall deliver all services under this RFP in a timely and effective manner to meet the District’s needs. The specific schedule for each task will be agreed upon between the District and the Consultant(s) at the time of contract award. The selected Consultant(s) shall begin work immediately upon authorization to proceed and shall adhere to the schedule mutually agreed upon by the District and the Consultant for said task. Adequate time shall be built into the schedule for each task to allow for sufficient review time of any data
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 5 of 10
reports, permit applications, documents, etc. by District staff. All of these elements shall be discussed in a kickoff meeting to clarify the services requested. The selected Consultant(s) shall prepare and deliver all reports and deliverables in a professional, timely and efficient manner to the District. The exact deliverables and their associated timeframe will be determined jointly by the District and the Consultant(s) at the time of contract award. All reports shall include essential photographs, laboratory analyses, diagrams, maps, etc. 2.4 TRANSFER OF RECORDS It is the intent of the District that the work effort be conducted in a manner that maximizes the District’s flexibility regarding follow-up studies or compliance related efforts and other District projects. Software and software programs that would be necessary to achieve this shall be made available to the District. Utilization of proprietary software which cannot be made available to the District at the end of this project will not be allowed, unless it is essential for the project and unavoidable (e.g., air modeling). All records (project reports, meeting notes, data files, project data, original tracings, maps, field sketches, lab reports, data, graphic originals, electronic files, etc.) generated shall be the property of the District and shall be turned over to the District upon completion or as directed. All deliverables are required to be delivered to the District in hardcopy and electronic (original software and PDF) format. Depending on the size of the electronic deliverables, the Consultant may be required to provide and utilize portable hard drive(s) for delivery.
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 6 of 10
SECTION 3.0 PROPOSAL CONTENT & FORMAT Each Consultant shall submit one original and four (4) copies of the proposal, as well as an electronic version, in .pdf format with bookmarks, on either a CD or USB drive. The font size on all submitted materials shall be equivalent to Times New Roman 12 pt or larger. Proposals shall be no more than 25 printed pages, with hard copies printed on sheets of double-sided recycled paper. All pages will be counted (i.e., each side of a sheet will count as a unique page, so one double-sided sheet will be counted as two pages) unless indicated otherwise in this RFP. Sheets that are 11”x17” shall be counted as two pages per side, or four pages if double sided. The following information shall be included in the proposal: 3.1 EXECUTIVE SUMMARY Include a concise synopsis of the proposal focused on how the Consultant will address the District’s key issues with the Consultant’s approach to the requested services as described in Section 2.0. 3.2 QUALIFICATIONS Because of the time sensitivity and critical nature of the work described within this RFP, the District seeks services from highly experienced and qualified Consultants. The Consultants must be able to staff this project with qualified individuals, experienced in the key technical disciplines needed, who shall remain committed to this work from inception through completion. A clear and comprehensive organization chart must be presented to illustrate the organization of the team and key team members, including subconsultants. The District is looking for Consultants that will provide excellent service and deliver quality work for the District. The District expects this quality service to extend through the entire duration of the Project. In this section of the Proposal, present the capabilities, skills, and experience of your firm/team, project manager and key technical staff. These factors will be strongly considered in selecting the successful Consultant for this Project. Consultant Qualifications Provide a statement of the firm’s/team’s qualifications, including brief resumes of key staff members (excluding the proposed project manager, who should be addressed as noted in below) and/or subconsultants proposed to work on the project. The information should be focused on experience on similar and/or complementary projects. The roles proposed for each subconsultant as well as their qualifications in that area shall also be identified in the Proposal. Your ability to identify and highlight key staff in the Proposal will be considered when evaluating your understanding of the Project.
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 7 of 10
Include a description of three (3) of the most recent projects/programs/efforts that included similar scope of work. The following information shall be included for each project:
• Client • Client contact information • Project Description • Start and end dates of project • Key staff member’s role • Consultant fees and overall project budget • Consultant’s role in project – highlight roles of staff • Contact information of reference person for project Owner
It is expected that the Consultant will honor its proposed project staffing and proposed key individuals indicated as assigned to the project. Substitutions will not be allowed for the convenience of the Consultant. In the event a proposed individual becomes unavailable the firm must propose, in advance and in writing, a substitution. The District reserves the right to accept or reject any and all proposed substitutions. Proposed Project Manager The District expects the proposed project manager to lead the Consultant project team, be the single point of accountability for project delivery, and provide the primary point of communication between the District and project team. Describe the proposed project manager’s experience on similar projects, experience on other District projects, and skills and results supporting the ability to serve the District. The project manager is considered the most important key team member, and will be committed for the Project’s duration. Any change in project manager, or any other key team member, will require prior approval by the District. The Consultant’s proposed project manager must be experienced in projects of the magnitude and complexity of the services the Consultant is proposing to provide. It is expected that the Consultant’s proposed project manager will be available for frequent personal interaction with the District. In addition, the project manager must meet the following requirements:
• Must be experienced in multi-disciplined projects of the nature outlined in this RFP. • Must have had a key role in projects of similar or complementary nature. • Must have managed projects of a similar or greater complexity and/or size.
Previous Performance on District Projects Summarize your firm’s/team’s experience on District Projects. List the District staff that you worked with and would be most familiar with your work. Your prior performance on District projects is an important consideration in the selection process. The successful Consultant’s performance will be formally evaluated on this Project for use in subsequent procurements.
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 8 of 10
Consultants that do not have prior experience working for the District will receive a neutral rating for this evaluation criterion. Business Opportunity Program Participation The District encourages MBE/WBE and SBE participation on this project; however, no specific subcontracting goals have been established. All certified firms will receive notification of the RFP and have the opportunity to submit individually or as a part of a team. While there are not specified goals, teaming with District-certified MBE/WBE and SBE firms will be considered as part of the proposal evaluation. The Consultant shall provide a summary of the proposed percentage of Minority and Women Business Enterprises (MBE/WBE) and Small Business Enterprises (SBE) participation in the project. 3.3 TECHNICAL APPROACH The Consultant’s technical approach to the project is a very important component of the selection. In the Proposal, the Consultant(s) is requested to demonstrate their project understanding, provide a summary of the critical issues, and describe the Consultant’s proposed sequence of activities to meet the District’s objectives. Project Understanding The Consultant should concisely demonstrate its understanding of the services for which they are submitting a proposal in this section of the Proposal. Key activities and approaches that improve the chances of success should be presented, along with key issues/challenges and how they will be addressed. Reuse Options The Consultant shall detail the proposed reuse options to be explored under this contract. For each proposed reuse option include, at a minimum, the following:
• Volume of ash on an annual basis • Material Processing Description • End Use/Users • Regulatory Approval Process • Challenges/Concerns
Critical Issues The Consultant should include a description of what they view as the critical issues associated with the contract and the attainment of regulatory approval in this section of the Proposal. Regulatory Approval Process The Consultant shall provide a detailed description of the process to be used to obtain regulatory approval for each proposed reuse option. This includes identifying the need for
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 9 of 10
additional testing, analysis or other data gathering. Consultant shall demonstrate a thorough understanding of the process that is required to obtain regulatory approval for each proposed reuse option. Project Schedule The Consultant shall provide a schedule for the work to be performed including key milestones. 3.4 FEE PROPOSAL The Consultant shall provide a Fee Proposal which includes all costs associated with obtaining regulatory approval for each beneficial reuse option proposed. 3.4 STATEMENTS The Consultant(s) shall include a statement confirming that no personal or organizational conflicts of interest are known to exist. 3.5 DETAILED RESUMES Detailed resumes for key team members may be included as an appendix. No more than two pages per resume. Pages in this appendix are not included toward the total page count.
BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT
REQUEST FOR PROPOSAL JULY 2016
© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION
Page 10 of 10
SECTION 4.0 EVALUATION & SELECTION PROCESS 4.1 WRITTEN PROPOSALS The written Proposals will be evaluated and scored by a District Selection Committee utilizing the following criteria:
Written Qualifications - 30% of Total Score • Firm/Team Qualifications – 15% • Proposed Project Manager – 15%
Technical Approach - 70% of Total Score
• Project Understanding – 10% • Reuse Options – 20% • Critical Issues – 10% • Regulatory Approval Process -20% • Project Schedule – 10%
4.2 INTERVIEWS Upon completion of the scoring and ranking of the written submittals, the District may select the top ranked firms to deliver a presentation and provide further clarification of their approach. The District may prepare and submit a list of questions to each of the short-listed firms to address during their interview. Upon completion of interviews, the District Selection Committee will score each firm according to the following criteria:
Presentation & Interview (50 additional points) • Quality and clarity of presentation – 10 points • Project Manager’s ability to communicate project understanding – 15 points • Team Support on Project Understanding and Questions – 10 points • Adequacy of Response to District Questions – 15 points
For evaluations taken to the presentation stage, the scores for the Presentation and Interview will be combined with the scores from the evaluation of the written submittals to determine the overall ranking of the short-listed firms.
END OF RFP
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Canton4101 Shuffel Street NWNorth Canton, OH 44720Tel: (330)497-9396
TestAmerica Job ID: 240-65485-1Client Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
For:Northeast Ohio Regional Sewer District3900 Euclid AvenueCleveland, Ohio 44115
Attn: Ms. Sarah Rehner
Authorized for release by:6/14/2016 3:21:21 PM
Nathan Pietras, Project Manager II(330)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Northeast Ohio Regional Sewer DistrictProject/Site: SOUTHERLY WWTC-ASH (SWWTC)
TestAmerica Job ID: 240-65485-1
Page 2 of 54TestAmerica Canton
6/14/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
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Definitions/GlossaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Qualifiers
GC/MS VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
* LCS or LCSD is outside acceptance limits.
GC/MS Semi VOA
Qualifier Description
* LCS or LCSD is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F1 MS and/or MSD Recovery is outside acceptance limits.
GC Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
Metals
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Canton
Page 3 of 54 6/14/2016
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Case NarrativeClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Job ID: 240-65485-1
Laboratory: TestAmerica Canton
Narrative
Job Narrative240-65485-1
Comments
No additional comments.
Receipt
The sample was received on 6/1/2016 10:20 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2.3º C.
GC/MS VOA Method(s) 8260B: The laboratory control sample (LCS) for preparation batch 240-233606 and analytical batch 240-233711 recovered
outside control limits for 1,1,1-trichloroethane. This analyte was biased high in the LCS and was not detected in the associated samples;
therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method(s) 8270C: The laboratory control sample (LCS) for 233013 associated with sample SOUTHERLY WWTC-ASH (SWWTC) (240-65485-1), recovered outside control limits for the following analyte: N-Nitrosodiphenylamine. This analyte was biased high in the LCS and was not detected in the associated sample; therefore, the data have been reported.
Method(s) 8270C: The laboratory control sample (LCS) for 233761 recovered outside control limits for Caprolactam. The associated
sample, SOUTHERLY WWTC-ASH (SWWTC) (240-65485-1), was re-prepared and re-analyzed with the Caprolactam recovery in the LCS (prep batch 234253) again failing to meet acceptance criteria. The initial results have been reported as has Caprolactam from the reextracted results.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica CantonPage 4 of 54 6/14/2016
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Method SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method Method Description LaboratoryProtocol
SW8468260B Volatile Organic Compounds (GC/MS) TAL CAN
SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CAN
SW8468081B Organochlorine Pesticides (GC) TAL CAN
SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CAN
SW8466020A Metals (ICP/MS) TAL CAN
SW8467470A Mercury (CVAA) TAL CAN
SW8467471A Mercury (CVAA) TAL CAN
SW8467196A Chromium, Hexavalent TAL CAN
EPAMoisture Percent Moisture TAL CAN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396
TestAmerica Canton
Page 5 of 54 6/14/2016
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Sample SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Solid 05/31/16 13:25 06/01/16 10:20
TestAmerica Canton
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Detection SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1
☼Acetone
RL
20 ug/Kg
MDL
5.7
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J B6.2 8260B
☼2-Butanone (MEK) 20 ug/Kg1.1 Total/NA12.8 J B 8260B
☼Toluene 5.0 ug/Kg0.27 Total/NA10.69 J 8260B
Chloroform 1.0 ug/L0.25 SPLP11.3 B 8260B
Methylene Chloride 1.0 ug/L0.33 SPLP13.0 B 8260B
☼Naphthalene 6.6 ug/Kg0.81 Total/NA14.0 J 8270C
Naphthalene 0.19 ug/L0.060 ASTM Leach10.31 8270C
☼Silver 0.19 mg/Kg0.0014 Total/NA22.8 B 6020A
☼Aluminum 9.6 mg/Kg0.60 Total/NA27800 B 6020A
☼Arsenic 0.96 mg/Kg0.025 Total/NA25.9 B 6020A
☼Barium 0.96 mg/Kg0.21 Total/NA2120 6020A
☼Beryllium 0.19 mg/Kg0.011 Total/NA20.28 B 6020A
☼Cadmium 0.19 mg/Kg0.0036 Total/NA21.2 B 6020A
☼Cobalt 0.19 mg/Kg0.0016 Total/NA235 B 6020A
☼Chromium 0.39 mg/Kg0.058 Total/NA248 B 6020A
☼Copper 0.39 mg/Kg0.094 Total/NA2100 B 6020A
☼Iron 19 mg/Kg3.1 Total/NA219000 B 6020A
☼Manganese 0.96 mg/Kg0.12 Total/NA21000 B 6020A
☼Nickel 0.39 mg/Kg0.038 Total/NA2750 B 6020A
☼Lead 0.19 mg/Kg0.043 Total/NA224 B 6020A
☼Antimony 0.39 mg/Kg0.014 Total/NA20.39 6020A
☼Selenium 0.96 mg/Kg0.039 Total/NA21.0 B 6020A
☼Thallium 0.39 mg/Kg0.018 Total/NA20.11 J 6020A
☼Vanadium 0.96 mg/Kg0.036 Total/NA214 6020A
☼Zinc 3.9 mg/Kg0.48 Total/NA294 B 6020A
☼Calcium 190 mg/Kg21 Total/NA212000 B 6020A
☼Potassium 190 mg/Kg4.7 Total/NA22000 B 6020A
☼Magnesium 190 mg/Kg3.9 Total/NA282000 B 6020A
☼Sodium 190 mg/Kg8.4 Total/NA2410 B 6020A
Aluminum 50 ug/L9.0 ASTM Leach111000 6020A
Arsenic 5.0 ug/L0.49 ASTM Leach110 6020A
Barium 5.0 ug/L1.1 ASTM Leach129 6020A
Beryllium 1.0 ug/L0.053 ASTM Leach10.33 J 6020A
Cadmium 1.0 ug/L0.061 ASTM Leach10.44 J 6020A
Cobalt 1.0 ug/L0.021 ASTM Leach10.45 J B 6020A
Chromium 2.0 ug/L0.60 ASTM Leach13.9 6020A
Nickel 2.0 ug/L0.23 ASTM Leach10.33 J B 6020A
Lead 1.0 ug/L0.11 ASTM Leach10.17 J 6020A
Antimony 2.0 ug/L0.16 ASTM Leach13.4 6020A
Selenium 5.0 ug/L0.25 ASTM Leach123 B 6020A
Thallium 1.0 ug/L0.074 ASTM Leach10.27 J 6020A
Vanadium 5.0 ug/L0.23 ASTM Leach181 6020A
Calcium 1000 ug/L240 ASTM Leach178000 6020A
Potassium 1000 ug/L30 ASTM Leach14200 6020A
Magnesium 1000 ug/L48 ASTM Leach11100 6020A
Sodium 1000 ug/L68 ASTM Leach11700 B 6020A
Mercury 0.20 ug/L0.090 ASTM Leach10.093 J B 7470A
Cr (VI) 0.020 mg/L0.0021 ASTM Leach10.0058 J 7196A
TestAmerica Canton
This Detection Summary does not include radiochemical test results.
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS) - SPLPRL MDL
Acetone ND 10 0.94 ug/L 06/08/16 20:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.35 ug/L 06/08/16 20:25 1Benzene ND
1.0 0.29 ug/L 06/08/16 20:25 1Dichlorobromomethane ND
1.0 0.56 ug/L 06/08/16 20:25 1Bromoform ND
1.0 0.44 ug/L 06/08/16 20:25 1Bromomethane ND
10 0.53 ug/L 06/08/16 20:25 12-Butanone (MEK) ND
1.0 0.38 ug/L 06/08/16 20:25 1Carbon disulfide ND
1.0 0.43 ug/L 06/08/16 20:25 1Carbon tetrachloride ND
1.0 0.25 ug/L 06/08/16 20:25 1Chlorobenzene ND
1.0 0.32 ug/L 06/08/16 20:25 1Chloroethane ND
1.0 0.25 ug/L 06/08/16 20:25 1Chloroform 1.3 B
1.0 0.44 ug/L 06/08/16 20:25 1Chloromethane ND
1.0 0.30 ug/L 06/08/16 20:25 11,1-Dichloroethane ND
1.0 0.23 ug/L 06/08/16 20:25 11,2-Dichloroethane ND
1.0 0.45 ug/L 06/08/16 20:25 11,1-Dichloroethene ND
1.0 0.25 ug/L 06/08/16 20:25 11,2-Dichloropropane ND
1.0 0.46 ug/L 06/08/16 20:25 1cis-1,3-Dichloropropene ND
1.0 0.56 ug/L 06/08/16 20:25 1trans-1,3-Dichloropropene ND
1.0 0.25 ug/L 06/08/16 20:25 1Ethylbenzene ND
10 0.48 ug/L 06/08/16 20:25 12-Hexanone ND
1.0 0.33 ug/L 06/08/16 20:25 1Methylene Chloride 3.0 B
10 0.99 ug/L 06/08/16 20:25 14-Methyl-2-pentanone (MIBK) ND
1.0 0.45 ug/L 06/08/16 20:25 1Styrene ND
1.0 0.22 ug/L 06/08/16 20:25 11,1,2,2-Tetrachloroethane ND
1.0 0.31 ug/L 06/08/16 20:25 1Tetrachloroethene ND
1.0 0.23 ug/L 06/08/16 20:25 1Toluene ND
1.0 0.22 ug/L 06/08/16 20:25 1Trichloroethene ND
1.0 0.29 ug/L 06/08/16 20:25 1Vinyl chloride ND
2.0 0.52 ug/L 06/08/16 20:25 1Xylenes, Total ND
1.0 0.44 ug/L 06/08/16 20:25 11,1,1-Trichloroethane ND *
1.0 0.24 ug/L 06/08/16 20:25 11,1,2-Trichloroethane ND
1.0 0.45 ug/L 06/08/16 20:25 1Cyclohexane ND
2.0 0.82 ug/L 06/08/16 20:25 11,2-Dibromo-3-Chloropropane ND
1.0 0.32 ug/L 06/08/16 20:25 1Ethylene Dibromide ND
1.0 0.32 ug/L 06/08/16 20:25 1Dichlorodifluoromethane ND
1.0 0.26 ug/L 06/08/16 20:25 1cis-1,2-Dichloroethene ND
1.0 0.30 ug/L 06/08/16 20:25 1trans-1,2-Dichloroethene ND
1.0 0.35 ug/L 06/08/16 20:25 1Isopropylbenzene ND
10 2.3 ug/L 06/08/16 20:25 1Methyl acetate ND
1.0 0.20 ug/L 06/08/16 20:25 1Methyl tert-butyl ether ND
1.0 0.45 ug/L 06/08/16 20:25 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.0 0.32 ug/L 06/08/16 20:25 11,2,4-Trichlorobenzene ND
1.0 0.25 ug/L 06/08/16 20:25 11,2-Dichlorobenzene ND
1.0 0.19 ug/L 06/08/16 20:25 11,3-Dichlorobenzene ND
1.0 0.27 ug/L 06/08/16 20:25 11,4-Dichlorobenzene ND
1.0 0.49 ug/L 06/08/16 20:25 1Trichlorofluoromethane ND
1.0 0.43 ug/L 06/08/16 20:25 1Chlorodibromomethane ND
1.0 0.43 ug/L 06/08/16 20:25 1Methylcyclohexane ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
1,2-Dichloroethane-d4 (Surr) 100 78 - 125 06/08/16 20:25 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 83 06/08/16 20:25 161 - 120
Toluene-d8 (Surr) 92 06/08/16 20:25 180 - 120
Dibromofluoromethane (Surr) 102 06/08/16 20:25 179 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM LeachRL MDL
Acenaphthene ND 0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.19 0.046 ug/L 06/09/16 07:34 06/09/16 20:29 1Acenaphthylene ND
0.95 0.32 ug/L 06/09/16 07:34 06/09/16 20:29 1Acetophenone ND
0.19 0.084 ug/L 06/09/16 07:34 06/09/16 20:29 1Anthracene ND
0.95 0.32 ug/L 06/09/16 07:34 06/09/16 20:29 1Atrazine ND
0.95 0.37 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzaldehyde ND
0.19 0.028 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[a]anthracene ND
0.19 0.038 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[b]fluoranthene ND
0.19 0.043 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[k]fluoranthene ND
0.19 0.044 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[g,h,i]perylene ND
0.19 0.049 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[a]pyrene ND
1.9 0.25 ug/L 06/09/16 07:34 06/09/16 20:29 1Butyl benzyl phthalate ND
0.95 0.12 ug/L 06/09/16 07:34 06/09/16 20:29 11,1'-Biphenyl ND
0.95 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-chloroethoxy)methane ND
0.95 0.095 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-chloroethyl)ether ND
4.8 1.6 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-ethylhexyl) phthalate ND
1.9 0.21 ug/L 06/09/16 07:34 06/09/16 20:29 14-Bromophenyl phenyl ether ND
4.8 0.19 ug/L 06/09/16 07:34 06/09/16 20:29 1Caprolactam ND F1 *
0.95 0.27 ug/L 06/09/16 07:34 06/09/16 20:29 1Carbazole ND
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chloroaniline ND
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chloro-3-methylphenol ND
0.95 0.095 ug/L 06/09/16 07:34 06/09/16 20:29 12-Chloronaphthalene ND
0.95 0.28 ug/L 06/09/16 07:34 06/09/16 20:29 12-Chlorophenol ND
1.9 0.29 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chlorophenyl phenyl ether ND
0.19 0.048 ug/L 06/09/16 07:34 06/09/16 20:29 1Chrysene ND
0.19 0.086 ug/L 06/09/16 07:34 06/09/16 20:29 12-Methylnaphthalene ND
1.9 0.76 ug/L 06/09/16 07:34 06/09/16 20:29 13 & 4 Methylphenol ND
0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1Dibenz(a,h)anthracene ND
0.95 0.019 ug/L 06/09/16 07:34 06/09/16 20:29 1Dibenzofuran ND
4.8 0.35 ug/L 06/09/16 07:34 06/09/16 20:29 13,3'-Dichlorobenzidine ND
1.9 0.18 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dichlorophenol ND
1.9 0.57 ug/L 06/09/16 07:34 06/09/16 20:29 1Diethyl phthalate ND
1.9 0.24 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dimethylphenol ND
1.9 0.28 ug/L 06/09/16 07:34 06/09/16 20:29 1Dimethyl phthalate ND
4.8 2.3 ug/L 06/09/16 07:34 06/09/16 20:29 14,6-Dinitro-2-methylphenol ND
4.8 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dinitrophenol ND
4.8 0.24 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dinitrotoluene ND
4.8 1.6 ug/L 06/09/16 07:34 06/09/16 20:29 1Di-n-butyl phthalate ND
1.9 0.22 ug/L 06/09/16 07:34 06/09/16 20:29 1Di-n-octyl phthalate ND
0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1Fluoranthene ND
0.19 0.039 ug/L 06/09/16 07:34 06/09/16 20:29 1Fluorene ND
0.19 0.081 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachlorobenzene ND
0.95 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachlorobutadiene ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach (Continued)RL MDL
Hexachlorocyclopentadiene ND 9.5 0.23 ug/L 06/09/16 07:34 06/09/16 20:29 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.95 0.18 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachloroethane ND
0.19 0.041 ug/L 06/09/16 07:34 06/09/16 20:29 1Indeno[1,2,3-cd]pyrene ND
0.95 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Isophorone ND
0.95 0.16 ug/L 06/09/16 07:34 06/09/16 20:29 12-Methylphenol ND
0.19 0.060 ug/L 06/09/16 07:34 06/09/16 20:29 1Naphthalene 0.31
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 12-Nitroaniline ND
1.9 0.27 ug/L 06/09/16 07:34 06/09/16 20:29 13-Nitroaniline ND
1.9 0.21 ug/L 06/09/16 07:34 06/09/16 20:29 14-Nitroaniline ND
0.95 0.038 ug/L 06/09/16 07:34 06/09/16 20:29 1Nitrobenzene ND
1.9 0.27 ug/L 06/09/16 07:34 06/09/16 20:29 12-Nitrophenol ND
4.8 0.28 ug/L 06/09/16 07:34 06/09/16 20:29 14-Nitrophenol ND
0.95 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 1N-Nitrosodiphenylamine ND
0.95 0.23 ug/L 06/09/16 07:34 06/09/16 20:29 1N-Nitrosodi-n-propylamine ND
0.95 0.38 ug/L 06/09/16 07:34 06/09/16 20:29 1bis (2-chloroisopropyl) ether ND
4.8 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Pentachlorophenol ND
0.19 0.059 ug/L 06/09/16 07:34 06/09/16 20:29 1Phenanthrene ND
0.95 0.57 ug/L 06/09/16 07:34 06/09/16 20:29 1Phenol ND
0.19 0.040 ug/L 06/09/16 07:34 06/09/16 20:29 1Pyrene ND
4.8 0.29 ug/L 06/09/16 07:34 06/09/16 20:29 12,4,5-Trichlorophenol ND
4.8 0.23 ug/L 06/09/16 07:34 06/09/16 20:29 12,4,6-Trichlorophenol ND
4.8 0.76 ug/L 06/09/16 07:34 06/09/16 20:29 12,6-Dinitrotoluene ND
2-Fluorobiphenyl (Surr) 79 42 - 120 06/09/16 07:34 06/09/16 20:29 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 36 06/09/16 07:34 06/09/16 20:29 110 - 120
2,4,6-Tribromophenol (Surr) 67 06/09/16 07:34 06/09/16 20:29 135 - 125
Nitrobenzene-d5 (Surr) 76 06/09/16 07:34 06/09/16 20:29 136 - 120
Phenol-d5 (Surr) 21 06/09/16 07:34 06/09/16 20:29 110 - 120
Terphenyl-d14 (Surr) 69 06/09/16 07:34 06/09/16 20:29 117 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach - RERL MDL
Caprolactam ND * 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 09:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2-Fluorobiphenyl (Surr) 77 42 - 120 06/13/16 11:40 06/14/16 09:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 35 06/13/16 11:40 06/14/16 09:49 110 - 120
2,4,6-Tribromophenol (Surr) 88 06/13/16 11:40 06/14/16 09:49 135 - 125
Nitrobenzene-d5 (Surr) 80 06/13/16 11:40 06/14/16 09:49 136 - 120
Phenol-d5 (Surr) 22 06/13/16 11:40 06/14/16 09:49 110 - 120
Terphenyl-d14 (Surr) 65 06/13/16 11:40 06/14/16 09:49 117 - 120
Method: 8081B - Organochlorine Pesticides (GC) - ASTM LeachRL MDL
4,4'-DDD ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.011 ug/L 06/09/16 06:31 06/13/16 14:40 14,4'-DDE ND
0.048 0.016 ug/L 06/09/16 06:31 06/13/16 14:40 14,4'-DDT ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Aldrin ND
0.048 0.013 ug/L 06/09/16 06:31 06/13/16 14:40 1alpha-BHC ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
Method: 8081B - Organochlorine Pesticides (GC) - ASTM Leach (Continued)RL MDL
beta-BHC ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.011 ug/L 06/09/16 06:31 06/13/16 14:40 1alpha-Chlordane ND
0.048 0.028 ug/L 06/09/16 06:31 06/13/16 14:40 1delta-BHC ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1gamma-BHC (Lindane) ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1gamma-Chlordane ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Dieldrin ND
0.048 0.015 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan I ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan II ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan sulfate ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin ND
0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin aldehyde ND
0.048 0.015 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin ketone ND
0.048 0.013 ug/L 06/09/16 06:31 06/13/16 14:40 1Heptachlor ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Heptachlor epoxide ND
0.095 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Methoxychlor ND
1.9 0.19 ug/L 06/09/16 06:31 06/13/16 14:40 1Toxaphene ND
DCB Decachlorobiphenyl 52 30 - 128 06/09/16 06:31 06/13/16 14:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 51 06/09/16 06:31 06/13/16 14:40 130 - 128
Tetrachloro-m-xylene 81 06/09/16 06:31 06/13/16 14:40 136 - 124
Tetrachloro-m-xylene 37 06/09/16 06:31 06/13/16 14:40 136 - 124
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography - ASTM LeachRL MDL
Aroclor-1016 ND 0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.095 0.086 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1221 ND
0.095 0.067 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1232 ND
0.095 0.057 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1242 ND
0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1248 ND
0.095 0.029 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1254 ND
0.095 0.038 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1260 ND
Tetrachloro-m-xylene 53 21 - 120 06/09/16 06:29 06/13/16 09:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 15 06/09/16 06:29 06/13/16 09:21 110 - 120
Method: 6020A - Metals (ICP/MS) - ASTM LeachRL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 14:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
50 9.0 ug/L 06/08/16 13:00 06/09/16 14:08 1Aluminum 11000
5.0 0.49 ug/L 06/08/16 13:00 06/09/16 14:08 1Arsenic 10
5.0 1.1 ug/L 06/08/16 13:00 06/09/16 14:08 1Barium 29
1.0 0.053 ug/L 06/08/16 13:00 06/09/16 14:08 1Beryllium 0.33 J
1.0 0.061 ug/L 06/08/16 13:00 06/09/16 14:08 1Cadmium 0.44 J
1.0 0.021 ug/L 06/08/16 13:00 06/09/16 14:08 1Cobalt 0.45 J B
2.0 0.60 ug/L 06/08/16 13:00 06/09/16 14:08 1Chromium 3.9
2.0 0.75 ug/L 06/08/16 13:00 06/09/16 14:08 1Copper ND
100 16 ug/L 06/08/16 13:00 06/09/16 14:08 1Iron ND
5.0 1.1 ug/L 06/08/16 13:00 06/09/16 14:08 1Manganese ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
Method: 6020A - Metals (ICP/MS) - ASTM Leach (Continued)RL MDL
Nickel 0.33 J B 2.0 0.23 ug/L 06/08/16 13:00 06/09/16 14:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.11 ug/L 06/08/16 13:00 06/09/16 14:08 1Lead 0.17 J
2.0 0.16 ug/L 06/08/16 13:00 06/09/16 14:08 1Antimony 3.4
5.0 0.25 ug/L 06/08/16 13:00 06/09/16 14:08 1Selenium 23 B
1.0 0.074 ug/L 06/08/16 13:00 06/09/16 14:08 1Thallium 0.27 J
5.0 0.23 ug/L 06/08/16 13:00 06/09/16 14:08 1Vanadium 81
20 7.3 ug/L 06/08/16 13:00 06/09/16 14:08 1Zinc ND
1000 240 ug/L 06/08/16 13:00 06/09/16 14:08 1Calcium 78000
1000 30 ug/L 06/08/16 13:00 06/09/16 14:08 1Potassium 4200
1000 48 ug/L 06/08/16 13:00 06/09/16 14:08 1Magnesium 1100
1000 68 ug/L 06/08/16 13:00 06/09/16 14:08 1Sodium 1700 B
Method: 7470A - Mercury (CVAA) - ASTM LeachRL MDL
Mercury 0.093 J B 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
Percent Solids 99.7 0.1 0.1 % 06/02/16 10:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.1 0.1 % 06/02/16 10:25 1Percent Moisture 0.3
General Chemistry - ASTM LeachRL MDL
Cr (VI) 0.0058 J 0.020 0.0021 mg/L 06/08/16 13:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 6.2 J B 20 5.7 ug/Kg ☼ 06/03/16 10:36 06/03/16 18:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
5.0 0.90 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Benzene ND
5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Dichlorobromomethane ND
5.0 0.24 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Bromoform ND
5.0 0.42 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Bromomethane ND
20 1.1 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼2-Butanone (MEK) 2.8 J B
5.0 0.59 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Carbon disulfide ND
5.0 0.65 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Carbon tetrachloride ND
5.0 0.53 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chlorobenzene ND
5.0 0.44 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloroethane ND
5.0 0.36 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloroform ND
5.0 0.79 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloromethane ND
5.0 0.34 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1-Dichloroethane ND
5.0 0.46 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dichloroethane ND
5.0 0.80 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1-Dichloroethene ND
5.0 0.14 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dichloropropane ND
5.0 0.71 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼cis-1,3-Dichloropropene ND
5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼trans-1,3-Dichloropropene ND
5.0 0.32 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Ethylbenzene ND
20 0.68 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼2-Hexanone ND
5.0 0.74 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methylene Chloride ND
20 1.2 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼4-Methyl-2-pentanone (MIBK) ND
5.0 0.40 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Styrene ND
5.0 0.31 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,2,2-Tetrachloroethane ND
5.0 0.80 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Tetrachloroethene ND
5.0 0.27 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Toluene 0.69 J
5.0 0.38 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Trichloroethene ND
5.0 0.30 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Vinyl chloride ND
10 0.54 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Xylenes, Total ND
5.0 0.65 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,1-Trichloroethane ND
5.0 0.37 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,2-Trichloroethane ND
10 0.48 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Cyclohexane ND
10 2.7 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dibromo-3-Chloropropane ND
5.0 0.53 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Ethylene Dibromide ND
5.0 0.28 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Dichlorodifluoromethane ND
5.0 0.28 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼cis-1,2-Dichloroethene ND
5.0 0.32 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼trans-1,2-Dichloroethene ND
5.0 0.20 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Isopropylbenzene ND
10 2.0 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methyl acetate ND
5.0 0.43 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methyl tert-butyl ether ND
5.0 0.42 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
5.0 0.38 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2,4-Trichlorobenzene ND
5.0 0.34 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dichlorobenzene ND
5.0 0.69 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,3-Dichlorobenzene ND
5.0 0.28 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,4-Dichlorobenzene ND
5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Trichlorofluoromethane ND
5.0 0.37 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chlorodibromomethane ND
10 0.58 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methylcyclohexane ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
1,2-Dichloroethane-d4 (Surr) 100 58 - 123 06/03/16 10:36 06/03/16 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 97 06/03/16 10:36 06/03/16 18:41 152 - 136
Toluene-d8 (Surr) 104 06/03/16 10:36 06/03/16 18:41 167 - 125
Dibromofluoromethane (Surr) 97 06/03/16 10:36 06/03/16 18:41 137 - 132
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
bis (2-chloroisopropyl) ether ND 99 9.4 ug/Kg ☼ 06/03/16 08:23 06/07/16 11:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
150 25 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4,5-Trichlorophenol ND
150 8.8 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4,6-Trichlorophenol ND
150 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dichlorophenol ND
150 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dimethylphenol ND
330 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dinitrophenol ND
200 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dinitrotoluene ND
200 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,6-Dinitrotoluene ND
49 0.44 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Chloronaphthalene ND
49 8.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Chlorophenol ND
6.6 0.49 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Methylnaphthalene ND
200 11 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Methylphenol ND
200 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Nitroaniline ND
49 8.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Nitrophenol ND
99 18 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3,3'-Dichlorobenzidine ND
200 16 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3-Nitroaniline ND
150 9.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4,6-Dinitro-2-methylphenol ND
49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Bromophenyl phenyl ether ND
150 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chloro-3-methylphenol ND
150 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chloroaniline ND
49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chlorophenyl phenyl ether ND
200 26 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Nitroaniline ND
330 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Nitrophenol ND
6.6 0.75 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acenaphthene ND
6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acenaphthylene ND
99 9.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acetophenone ND
6.6 0.77 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Anthracene ND
200 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Atrazine ND
6.6 0.62 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[a]anthracene ND
6.6 0.63 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[a]pyrene ND
6.6 0.58 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[b]fluoranthene ND
6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[g,h,i]perylene ND
6.6 0.67 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[k]fluoranthene ND
99 22 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-chloroethoxy)methane ND
99 2.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-chloroethyl)ether ND
69 19 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-ethylhexyl) phthalate ND
69 9.9 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Butyl benzyl phthalate ND
6.6 1.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Chrysene ND
6.6 0.65 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dibenz(a,h)anthracene ND
49 0.65 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dibenzofuran ND
69 16 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Diethyl phthalate ND
69 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dimethyl phthalate ND
69 15 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Di-n-butyl phthalate ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Di-n-octyl phthalate ND 69 7.8 ug/Kg ☼ 06/03/16 08:23 06/07/16 11:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
6.6 0.54 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Fluoranthene ND
6.6 0.52 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Fluorene ND
6.6 2.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorobenzene ND
49 5.5 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorobutadiene ND
330 8.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorocyclopentadiene ND
49 8.9 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachloroethane ND
6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Indeno[1,2,3-cd]pyrene ND
49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Isophorone ND
6.6 0.81 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Naphthalene 4.0 J
99 2.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Nitrobenzene ND
49 6.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼N-Nitrosodi-n-propylamine ND
49 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼N-Nitrosodiphenylamine ND *
150 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Pentachlorophenol ND
49 7.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Phenol ND
6.6 0.72 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Phenanthrene ND
6.6 0.43 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Pyrene ND
400 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3 & 4 Methylphenol ND
2-Fluorobiphenyl (Surr) 91 39 - 120 06/03/16 08:23 06/07/16 11:12 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 74 06/03/16 08:23 06/07/16 11:12 133 - 120
2,4,6-Tribromophenol (Surr) 41 06/03/16 08:23 06/07/16 11:12 110 - 120
Nitrobenzene-d5 (Surr) 80 06/03/16 08:23 06/07/16 11:12 132 - 120
Phenol-d5 (Surr) 74 06/03/16 08:23 06/07/16 11:12 132 - 120
Terphenyl-d14 (Surr) 111 06/03/16 08:23 06/07/16 11:12 147 - 120
Method: 8081B - Organochlorine Pesticides (GC)RL MDL
4,4'-DDD ND 1.7 0.20 ug/Kg ☼ 06/03/16 07:28 06/10/16 16:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.7 0.27 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼4,4'-DDE ND
1.7 0.31 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼4,4'-DDT ND
1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Aldrin ND
1.7 0.60 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼alpha-BHC ND
1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼alpha-Chlordane ND
1.7 0.36 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼beta-BHC ND
1.7 0.22 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼delta-BHC ND
1.7 0.16 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Dieldrin ND
1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan I ND
1.7 0.38 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan II ND
1.7 0.34 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan sulfate ND
1.7 0.21 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin ND
1.7 0.32 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin aldehyde ND
1.7 0.42 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin ketone ND
1.7 0.46 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼gamma-BHC (Lindane) ND
1.7 0.86 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼gamma-Chlordane ND
1.7 0.70 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Heptachlor ND
1.7 0.40 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Heptachlor epoxide ND
67 9.9 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Toxaphene ND
3.3 0.54 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Methoxychlor ND
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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
DCB Decachlorobiphenyl 59 42 - 138 06/03/16 07:28 06/10/16 16:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 83 06/03/16 07:28 06/10/16 16:02 142 - 138
Tetrachloro-m-xylene 68 06/03/16 07:28 06/10/16 16:02 131 - 159
Tetrachloro-m-xylene 56 06/03/16 07:28 06/10/16 16:02 131 - 159
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL
Aroclor-1016 ND 33 12 ug/Kg ☼ 06/03/16 07:23 06/06/16 14:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
33 16 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1221 ND
33 20 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1232 ND
33 11 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1242 ND
33 8.0 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1248 ND
33 14 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1254 ND
33 9.0 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1260 ND
Tetrachloro-m-xylene 60 14 - 128 06/03/16 07:23 06/06/16 14:28 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 63 06/03/16 07:23 06/06/16 14:28 110 - 132
Method: 6020A - Metals (ICP/MS)RL MDL
Silver 2.8 B 0.19 0.0014 mg/Kg ☼ 06/02/16 11:09 06/03/16 21:54 2
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.6 0.60 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Aluminum 7800 B
0.96 0.025 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Arsenic 5.9 B
0.96 0.21 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Barium 120
0.19 0.011 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Beryllium 0.28 B
0.19 0.0036 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Cadmium 1.2 B
0.19 0.0016 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Cobalt 35 B
0.39 0.058 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Chromium 48 B
0.39 0.094 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Copper 100 B
19 3.1 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Iron 19000 B
0.96 0.12 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Manganese 1000 B
0.39 0.038 mg/Kg 06/02/16 11:09 06/06/16 14:26 2☼Nickel 750 B
0.19 0.043 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Lead 24 B
0.39 0.014 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Antimony 0.39
0.96 0.039 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Selenium 1.0 B
0.39 0.018 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Thallium 0.11 J
0.96 0.036 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Vanadium 14
3.9 0.48 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Zinc 94 B
190 21 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Calcium 12000 B
190 4.7 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Potassium 2000 B
190 3.9 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Magnesium 82000 B
190 8.4 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Sodium 410 B
Method: 7471A - Mercury (CVAA)RL MDL
Mercury ND 0.11 0.015 mg/Kg ☼ 06/02/16 15:00 06/03/16 07:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
Cr (VI) ND 0.79 0.15 mg/Kg ☼ 06/09/16 09:04 06/09/16 13:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Surrogate SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (58-123) (52-136) (67-125) (37-132)
12DCE BFB TOL DBFM
100 97 104 97240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
90 94 103 96LCS 240-233030/5 Lab Control Sample
91 93 101 96MB 240-233030/6 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (78-125) (61-120) (80-120) (79-120)
12DCE BFB TOL DBFM
96 88 93 103LCS 240-233711/6
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: SPLPMatrix: Solid
Lab Sample ID Client Sample ID (78-125) (61-120) (80-120) (79-120)
12DCE BFB TOL DBFM
100 83 92 102240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
101 84 89 102LB 240-233606/1-A MB Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (39-120) (33-120) (10-120) (32-120) (32-120) (47-120)
FBP 2FP TBP NBZ PHL TPH
91 74 41 80 74 111240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
94 82 75 8384 113LCS 240-233013/18-A Lab Control Sample
92 77 59 7991 103MB 240-233013/17-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
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Surrogate SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (42-120) (10-120) (35-125) (36-120) (10-120) (17-120)
FBP 2FP TBP NBZ PHL TPH
87 41 87 94 24 78LCS 240-233761/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
72 30 101 1981 31LCS 240-234253/4-A Lab Control Sample
74 39 68 2473 76MB 240-233761/4-A Method Blank
80 37 96 2284 82MB 240-234253/3-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (42-120) (10-120) (35-125) (36-120) (10-120) (17-120)
FBP 2FP TBP NBZ PHL TPH
79 36 67 76 21 69240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
77 35 88 2280 65240-65485-1 - RE SOUTHERLY WWTC-ASH
(SWWTC)81 27 82 1584 60240-65485-1 MS SOUTHERLY WWTC-ASH
(SWWTC)
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-128) (30-128) (36-124) (36-124)
DCB1 DCB2 TCX1 TCX2
66 56 90 83LCS 240-233753/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
48 48 90 85MB 240-233753/4-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
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Surrogate SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (42-138) (42-138) (31-159) (31-159)
DCB1 DCB2 TCX1 TCX2
59 83 68 56240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
79 74 70 60LCS 240-233006/6-A Lab Control Sample
81 85 77 64MB 240-233006/5-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (30-128) (30-128) (36-124) (36-124)
DCB1 DCB2 TCX1 TCX2
52 51 81 37240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
30 29 X 80 80240-65485-1 MS SOUTHERLY WWTC-ASH
(SWWTC)
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (14-128) (10-132)
TCX2 DCB2
60 63240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
66 80LCS 240-233005/13-A Lab Control Sample
64 79MB 240-233005/12-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-120) (10-120)
TCX2 DCB2
60 36LCS 240-233752/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
59 33MB 240-233752/4-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
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Surrogate SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (21-120) (10-120)
TCX2 DCB2
53 15240-65485-1
Percent Surrogate Recovery (Acceptance Limits)
SOUTHERLY WWTC-ASH (SWWTC)
59 11240-65485-1 MS SOUTHERLY WWTC-ASH
(SWWTC)
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-233030/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
RL MDL
Acetone 7.04 J 20 5.7 ug/Kg 06/03/16 11:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.905.0 ug/Kg 06/03/16 11:24 1Benzene
ND 0.295.0 ug/Kg 06/03/16 11:24 1Dichlorobromomethane
ND 0.245.0 ug/Kg 06/03/16 11:24 1Bromoform
ND 0.425.0 ug/Kg 06/03/16 11:24 1Bromomethane
1.22 J 1.120 ug/Kg 06/03/16 11:24 12-Butanone (MEK)
ND 0.595.0 ug/Kg 06/03/16 11:24 1Carbon disulfide
ND 0.655.0 ug/Kg 06/03/16 11:24 1Carbon tetrachloride
ND 0.535.0 ug/Kg 06/03/16 11:24 1Chlorobenzene
ND 0.445.0 ug/Kg 06/03/16 11:24 1Chloroethane
ND 0.365.0 ug/Kg 06/03/16 11:24 1Chloroform
ND 0.795.0 ug/Kg 06/03/16 11:24 1Chloromethane
ND 0.345.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethane
ND 0.465.0 ug/Kg 06/03/16 11:24 11,2-Dichloroethane
ND 0.805.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethene
ND 0.145.0 ug/Kg 06/03/16 11:24 11,2-Dichloropropane
ND 0.715.0 ug/Kg 06/03/16 11:24 1cis-1,3-Dichloropropene
ND 0.295.0 ug/Kg 06/03/16 11:24 1trans-1,3-Dichloropropene
ND 0.325.0 ug/Kg 06/03/16 11:24 1Ethylbenzene
ND 0.6820 ug/Kg 06/03/16 11:24 12-Hexanone
ND 0.745.0 ug/Kg 06/03/16 11:24 1Methylene Chloride
ND 1.220 ug/Kg 06/03/16 11:24 14-Methyl-2-pentanone (MIBK)
ND 0.405.0 ug/Kg 06/03/16 11:24 1Styrene
ND 0.315.0 ug/Kg 06/03/16 11:24 11,1,2,2-Tetrachloroethane
ND 0.805.0 ug/Kg 06/03/16 11:24 1Tetrachloroethene
ND 0.275.0 ug/Kg 06/03/16 11:24 1Toluene
ND 0.385.0 ug/Kg 06/03/16 11:24 1Trichloroethene
ND 0.305.0 ug/Kg 06/03/16 11:24 1Vinyl chloride
ND 0.5410 ug/Kg 06/03/16 11:24 1Xylenes, Total
ND 0.655.0 ug/Kg 06/03/16 11:24 11,1,1-Trichloroethane
ND 0.375.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloroethane
ND 0.4810 ug/Kg 06/03/16 11:24 1Cyclohexane
ND 2.710 ug/Kg 06/03/16 11:24 11,2-Dibromo-3-Chloropropane
ND 0.535.0 ug/Kg 06/03/16 11:24 1Ethylene Dibromide
ND 0.285.0 ug/Kg 06/03/16 11:24 1Dichlorodifluoromethane
ND 0.285.0 ug/Kg 06/03/16 11:24 1cis-1,2-Dichloroethene
ND 0.325.0 ug/Kg 06/03/16 11:24 1trans-1,2-Dichloroethene
ND 0.205.0 ug/Kg 06/03/16 11:24 1Isopropylbenzene
ND 2.010 ug/Kg 06/03/16 11:24 1Methyl acetate
ND 0.435.0 ug/Kg 06/03/16 11:24 1Methyl tert-butyl ether
ND 0.425.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.385.0 ug/Kg 06/03/16 11:24 11,2,4-Trichlorobenzene
ND 0.345.0 ug/Kg 06/03/16 11:24 11,2-Dichlorobenzene
ND 0.695.0 ug/Kg 06/03/16 11:24 11,3-Dichlorobenzene
ND 0.285.0 ug/Kg 06/03/16 11:24 11,4-Dichlorobenzene
ND 0.295.0 ug/Kg 06/03/16 11:24 1Trichlorofluoromethane
ND 0.375.0 ug/Kg 06/03/16 11:24 1Chlorodibromomethane
ND 0.5810 ug/Kg 06/03/16 11:24 1Methylcyclohexane
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
1,2-Dichloroethane-d4 (Surr) 91 58 - 123 06/03/16 11:24 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
93 06/03/16 11:24 14-Bromofluorobenzene (Surr) 52 - 136
101 06/03/16 11:24 1Toluene-d8 (Surr) 67 - 125
96 06/03/16 11:24 1Dibromofluoromethane (Surr) 37 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233030/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
Acetone 100 107 ug/Kg 107 41 - 137
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 51.6 ug/Kg 103 79 - 120
Dichlorobromomethane 50.0 54.1 ug/Kg 108 80 - 122
Bromoform 50.0 53.3 ug/Kg 107 62 - 133
Bromomethane 20.0 14.1 ug/Kg 71 42 - 136
2-Butanone (MEK) 100 110 ug/Kg 110 52 - 131
Carbon disulfide 50.0 60.8 ug/Kg 122 62 - 146
Carbon tetrachloride 50.0 51.9 ug/Kg 104 71 - 129
Chlorobenzene 50.0 51.0 ug/Kg 102 78 - 120
Chloroethane 20.0 16.9 ug/Kg 85 58 - 120
Chloroform 50.0 51.3 ug/Kg 103 77 - 120
Chloromethane 20.0 14.8 ug/Kg 74 50 - 120
1,1-Dichloroethane 50.0 50.1 ug/Kg 100 76 - 120
1,2-Dichloroethane 50.0 51.6 ug/Kg 103 72 - 120
1,1-Dichloroethene 50.0 53.9 ug/Kg 108 75 - 135
1,2-Dichloropropane 50.0 52.1 ug/Kg 104 80 - 120
cis-1,3-Dichloropropene 50.0 55.8 ug/Kg 112 74 - 128
trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 73 - 131
Ethylbenzene 50.0 52.7 ug/Kg 105 79 - 120
2-Hexanone 100 118 ug/Kg 118 64 - 136
Methylene Chloride 50.0 49.5 ug/Kg 99 75 - 120
4-Methyl-2-pentanone (MIBK) 100 123 ug/Kg 123 67 - 135
Styrene 50.0 54.1 ug/Kg 108 80 - 120
1,1,2,2-Tetrachloroethane 50.0 56.1 ug/Kg 112 77 - 123
Tetrachloroethene 50.0 53.0 ug/Kg 106 79 - 120
Toluene 50.0 50.9 ug/Kg 102 75 - 120
Trichloroethene 50.0 54.9 ug/Kg 110 79 - 120
Vinyl chloride 20.0 14.5 ug/Kg 73 57 - 120
Xylenes, Total 100 106 ug/Kg 106 80 - 120
1,1,1-Trichloroethane 50.0 52.3 ug/Kg 105 77 - 126
1,1,2-Trichloroethane 50.0 54.2 ug/Kg 108 80 - 120
Cyclohexane 50.0 52.1 ug/Kg 104 66 - 120
1,2-Dibromo-3-Chloropropane 50.0 57.9 ug/Kg 116 61 - 132
Ethylene Dibromide 50.0 57.6 ug/Kg 115 80 - 120
Dichlorodifluoromethane 20.0 9.78 ug/Kg 49 26 - 120
cis-1,2-Dichloroethene 50.0 52.2 ug/Kg 104 76 - 120
trans-1,2-Dichloroethene 50.0 55.2 ug/Kg 110 78 - 120
Isopropylbenzene 50.0 56.0 ug/Kg 112 76 - 122
Methyl acetate 250 300 ug/Kg 120 57 - 130
Methyl tert-butyl ether 50.0 50.5 ug/Kg 101 49 - 165
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 52.7 ug/Kg 105 80 - 138
1,2,4-Trichlorobenzene 50.0 49.4 ug/Kg 99 64 - 124
1,2-Dichlorobenzene 50.0 50.3 ug/Kg 101 76 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233030/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
1,3-Dichlorobenzene 50.0 50.3 ug/Kg 101 78 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,4-Dichlorobenzene 50.0 49.3 ug/Kg 99 75 - 120
Trichlorofluoromethane 20.0 17.2 ug/Kg 86 57 - 146
Methylcyclohexane 50.0 51.2 ug/Kg 102 70 - 126
m-Xylene & p-Xylene 50.0 52.9 ug/Kg 106 80 - 120
o-Xylene 50.0 52.7 ug/Kg 105 80 - 120
1,2-Dichloroethane-d4 (Surr) 58 - 123
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr) 52 - 136
103Toluene-d8 (Surr) 67 - 125
96Dibromofluoromethane (Surr) 37 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233711/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233711
Acetone 40.0 35.6 ug/L 89 34 - 148
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 20.0 22.6 ug/L 113 80 - 120
Dichlorobromomethane 20.0 21.9 ug/L 109 80 - 120
Bromoform 20.0 24.3 ug/L 122 56 - 122
Bromomethane 20.0 23.5 ug/L 118 38 - 132
2-Butanone (MEK) 40.0 43.2 ug/L 108 56 - 138
Carbon disulfide 20.0 26.5 ug/L 132 65 - 144
Carbon tetrachloride 20.0 23.6 ug/L 118 77 - 131
Chlorobenzene 20.0 21.2 ug/L 106 80 - 120
Chloroethane 20.0 24.0 ug/L 120 36 - 126
Chloroform 20.0 23.0 ug/L 115 80 - 120
Chloromethane 20.0 23.8 ug/L 119 48 - 133
1,1-Dichloroethane 20.0 22.0 ug/L 110 79 - 125
1,2-Dichloroethane 20.0 22.3 ug/L 111 80 - 120
1,1-Dichloroethene 20.0 24.8 ug/L 124 76 - 124
1,2-Dichloropropane 20.0 22.3 ug/L 111 78 - 124
cis-1,3-Dichloropropene 20.0 23.4 ug/L 117 74 - 126
trans-1,3-Dichloropropene 20.0 18.4 ug/L 92 75 - 131
Ethylbenzene 20.0 19.9 ug/L 99 80 - 120
2-Hexanone 40.0 42.8 ug/L 107 55 - 141
Methylene Chloride 20.0 22.2 ug/L 111 77 - 129
4-Methyl-2-pentanone (MIBK) 40.0 44.2 ug/L 111 64 - 135
Styrene 20.0 20.6 ug/L 103 76 - 122
1,1,2,2-Tetrachloroethane 20.0 19.7 ug/L 99 71 - 123
Tetrachloroethene 20.0 20.9 ug/L 104 78 - 121
Toluene 20.0 22.4 ug/L 112 80 - 120
Trichloroethene 20.0 24.1 ug/L 121 80 - 121
Vinyl chloride 20.0 23.6 ug/L 118 52 - 121
Xylenes, Total 40.0 42.0 ug/L 105 80 - 120
1,1,1-Trichloroethane 20.0 25.6 * ug/L 128 77 - 123
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233711/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233711
1,1,2-Trichloroethane 20.0 21.9 ug/L 110 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Cyclohexane 20.0 21.0 ug/L 105 60 - 140
1,2-Dibromo-3-Chloropropane 20.0 22.6 ug/L 113 50 - 132
Ethylene Dibromide 20.0 22.2 ug/L 111 80 - 120
Dichlorodifluoromethane 20.0 23.1 ug/L 115 23 - 136
cis-1,2-Dichloroethene 20.0 22.1 ug/L 111 79 - 120
trans-1,2-Dichloroethene 20.0 22.8 ug/L 114 80 - 124
Isopropylbenzene 20.0 20.3 ug/L 102 77 - 120
Methyl acetate 100 113 ug/L 113 67 - 131
Methyl tert-butyl ether 20.0 23.0 ug/L 115 69 - 121
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
20.0 23.4 ug/L 117 67 - 138
1,2,4-Trichlorobenzene 20.0 20.1 ug/L 100 61 - 120
1,2-Dichlorobenzene 20.0 19.6 ug/L 98 79 - 120
1,3-Dichlorobenzene 20.0 19.7 ug/L 98 79 - 120
1,4-Dichlorobenzene 20.0 20.2 ug/L 101 79 - 120
Trichlorofluoromethane 20.0 21.8 ug/L 109 61 - 133
Methylcyclohexane 20.0 19.9 ug/L 100 61 - 134
m-Xylene & p-Xylene 20.0 21.4 ug/L 107 80 - 120
o-Xylene 20.0 20.6 ug/L 103 80 - 120
1,2-Dichloroethane-d4 (Surr) 78 - 125
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
884-Bromofluorobenzene (Surr) 61 - 120
93Toluene-d8 (Surr) 80 - 120
103Dibromofluoromethane (Surr) 79 - 120
Client Sample ID: Method BlankLab Sample ID: LB 240-233606/1-A MBMatrix: Solid Prep Type: SPLPAnalysis Batch: 233711
RL MDL
Acetone 1.76 J 10 0.94 ug/L 06/08/16 20:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.351.0 ug/L 06/08/16 20:01 1Benzene
ND 0.291.0 ug/L 06/08/16 20:01 1Dichlorobromomethane
ND 0.561.0 ug/L 06/08/16 20:01 1Bromoform
ND 0.441.0 ug/L 06/08/16 20:01 1Bromomethane
ND 0.5310 ug/L 06/08/16 20:01 12-Butanone (MEK)
ND 0.381.0 ug/L 06/08/16 20:01 1Carbon disulfide
ND 0.431.0 ug/L 06/08/16 20:01 1Carbon tetrachloride
ND 0.251.0 ug/L 06/08/16 20:01 1Chlorobenzene
ND 0.321.0 ug/L 06/08/16 20:01 1Chloroethane
1.24 0.251.0 ug/L 06/08/16 20:01 1Chloroform
ND 0.441.0 ug/L 06/08/16 20:01 1Chloromethane
ND 0.301.0 ug/L 06/08/16 20:01 11,1-Dichloroethane
ND 0.231.0 ug/L 06/08/16 20:01 11,2-Dichloroethane
ND 0.451.0 ug/L 06/08/16 20:01 11,1-Dichloroethene
ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichloropropane
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 240-233606/1-A MBMatrix: Solid Prep Type: SPLPAnalysis Batch: 233711
RL MDL
cis-1,3-Dichloropropene ND 1.0 0.46 ug/L 06/08/16 20:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.561.0 ug/L 06/08/16 20:01 1trans-1,3-Dichloropropene
ND 0.251.0 ug/L 06/08/16 20:01 1Ethylbenzene
ND 0.4810 ug/L 06/08/16 20:01 12-Hexanone
2.74 0.331.0 ug/L 06/08/16 20:01 1Methylene Chloride
ND 0.9910 ug/L 06/08/16 20:01 14-Methyl-2-pentanone (MIBK)
ND 0.451.0 ug/L 06/08/16 20:01 1Styrene
ND 0.221.0 ug/L 06/08/16 20:01 11,1,2,2-Tetrachloroethane
ND 0.311.0 ug/L 06/08/16 20:01 1Tetrachloroethene
ND 0.231.0 ug/L 06/08/16 20:01 1Toluene
ND 0.221.0 ug/L 06/08/16 20:01 1Trichloroethene
ND 0.291.0 ug/L 06/08/16 20:01 1Vinyl chloride
ND 0.522.0 ug/L 06/08/16 20:01 1Xylenes, Total
ND 0.441.0 ug/L 06/08/16 20:01 11,1,1-Trichloroethane
ND 0.241.0 ug/L 06/08/16 20:01 11,1,2-Trichloroethane
ND 0.451.0 ug/L 06/08/16 20:01 1Cyclohexane
ND 0.822.0 ug/L 06/08/16 20:01 11,2-Dibromo-3-Chloropropane
ND 0.321.0 ug/L 06/08/16 20:01 1Ethylene Dibromide
ND 0.321.0 ug/L 06/08/16 20:01 1Dichlorodifluoromethane
ND 0.261.0 ug/L 06/08/16 20:01 1cis-1,2-Dichloroethene
ND 0.301.0 ug/L 06/08/16 20:01 1trans-1,2-Dichloroethene
ND 0.351.0 ug/L 06/08/16 20:01 1Isopropylbenzene
ND 2.310 ug/L 06/08/16 20:01 1Methyl acetate
ND 0.201.0 ug/L 06/08/16 20:01 1Methyl tert-butyl ether
ND 0.451.0 ug/L 06/08/16 20:01 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.321.0 ug/L 06/08/16 20:01 11,2,4-Trichlorobenzene
ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichlorobenzene
ND 0.191.0 ug/L 06/08/16 20:01 11,3-Dichlorobenzene
ND 0.271.0 ug/L 06/08/16 20:01 11,4-Dichlorobenzene
ND 0.491.0 ug/L 06/08/16 20:01 1Trichlorofluoromethane
ND 0.431.0 ug/L 06/08/16 20:01 1Chlorodibromomethane
ND 0.431.0 ug/L 06/08/16 20:01 1Methylcyclohexane
1,2-Dichloroethane-d4 (Surr) 101 78 - 125 06/08/16 20:01 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
84 06/08/16 20:01 14-Bromofluorobenzene (Surr) 61 - 120
89 06/08/16 20:01 1Toluene-d8 (Surr) 80 - 120
102 06/08/16 20:01 1Dibromofluoromethane (Surr) 79 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
2-Chloronaphthalene ND 50 0.45 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 8.250 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Chlorophenol
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
4-Bromophenyl phenyl ether ND 50 13 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 21150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloro-3-methylphenol
ND 0.506.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylnaphthalene
ND 17150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloroaniline
ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chlorophenyl phenyl ether
ND 18100 ug/Kg 06/03/16 08:23 06/07/16 10:25 13,3'-Dichlorobenzidine
ND 0.766.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthene
ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dichlorophenol
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthylene
ND 9.2100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acetophenone
ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dimethylphenol
ND 0.786.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Anthracene
ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Atrazine
ND 9.2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14,6-Dinitro-2-methylphenol
ND 0.636.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]anthracene
ND 21330 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrophenol
ND 0.646.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]pyrene
ND 17200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrotoluene
ND 0.596.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[b]fluoranthene
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[g,h,i]perylene
ND 0.686.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[k]fluoranthene
ND 22100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethoxy)methane
ND 2.0100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethyl)ether
ND 1970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-ethylhexyl) phthalate
ND 1070 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Butyl benzyl phthalate
ND 1.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Chrysene
ND 0.666.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenz(a,h)anthracene
ND 0.6650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenzofuran
ND 1670 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Diethyl phthalate
ND 11200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylphenol
ND 1770 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dimethyl phthalate
27.9 J 1570 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-butyl phthalate
ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitroaniline
ND 7.970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-octyl phthalate
ND 16200 ug/Kg 06/03/16 08:23 06/07/16 10:25 13-Nitroaniline
ND 0.556.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluoranthene
ND 26200 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitroaniline
ND 0.536.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluorene
ND 2.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobenzene
ND 8.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitrophenol
ND 5.650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobutadiene
ND 17330 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitrophenol
ND 8.1330 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorocyclopentadiene
ND 9.050 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachloroethane
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Indeno[1,2,3-cd]pyrene
ND 9.5100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1bis (2-chloroisopropyl) ether
ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Isophorone
ND 0.826.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Naphthalene
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
Nitrobenzene ND 100 2.2 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 6.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodi-n-propylamine
ND 2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodiphenylamine
ND 25150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,5-Trichlorophenol
ND 9.1150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pentachlorophenol
ND 8.9150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,6-Trichlorophenol
ND 7.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenol
ND 0.736.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenanthrene
ND 0.446.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pyrene
ND 20400 ug/Kg 06/03/16 08:23 06/07/16 10:25 13 & 4 Methylphenol
ND 21200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,6-Dinitrotoluene
2-Fluorobiphenyl (Surr) 92 39 - 120 06/07/16 10:25 1
MB MB
Surrogate
06/03/16 08:23
Dil FacPrepared AnalyzedQualifier Limits%Recovery
77 06/03/16 08:23 06/07/16 10:25 12-Fluorophenol (Surr) 33 - 120
59 06/03/16 08:23 06/07/16 10:25 12,4,6-Tribromophenol (Surr) 10 - 120
91 06/03/16 08:23 06/07/16 10:25 1Nitrobenzene-d5 (Surr) 32 - 120
79 06/03/16 08:23 06/07/16 10:25 1Phenol-d5 (Surr) 32 - 120
103 06/03/16 08:23 06/07/16 10:25 1Terphenyl-d14 (Surr) 47 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233013/18-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
2-Chloronaphthalene 667 612 ug/Kg 92 54 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Chlorophenol 667 624 ug/Kg 94 50 - 120
4-Bromophenyl phenyl ether 667 770 ug/Kg 116 48 - 120
4-Chloro-3-methylphenol 667 523 ug/Kg 78 52 - 120
2-Methylnaphthalene 667 644 ug/Kg 97 53 - 120
4-Chloroaniline 667 387 ug/Kg 58 41 - 120
4-Chlorophenyl phenyl ether 667 712 ug/Kg 107 56 - 120
3,3'-Dichlorobenzidine 1330 1000 ug/Kg 75 39 - 120
Acenaphthene 667 602 ug/Kg 90 55 - 120
2,4-Dichlorophenol 667 612 ug/Kg 92 51 - 120
Acenaphthylene 667 632 ug/Kg 95 54 - 120
Acetophenone 667 589 ug/Kg 88 49 - 120
2,4-Dimethylphenol 667 448 ug/Kg 67 34 - 120
Anthracene 667 620 ug/Kg 93 59 - 120
Atrazine 1330 1460 ug/Kg 110 56 - 120
4,6-Dinitro-2-methylphenol 1330 849 ug/Kg 64 23 - 120
Benzo[a]anthracene 667 648 ug/Kg 97 60 - 120
2,4-Dinitrophenol 1330 503 ug/Kg 38 10 - 120
Benzo[a]pyrene 667 745 ug/Kg 112 61 - 120
2,4-Dinitrotoluene 667 716 ug/Kg 107 57 - 120
Benzo[b]fluoranthene 667 736 ug/Kg 110 60 - 120
Benzo[g,h,i]perylene 667 686 ug/Kg 103 60 - 120
Benzo[k]fluoranthene 667 759 ug/Kg 114 61 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233013/18-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
Bis(2-chloroethoxy)methane 667 569 ug/Kg 85 53 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Bis(2-chloroethyl)ether 667 548 ug/Kg 82 45 - 120
Bis(2-ethylhexyl) phthalate 667 665 ug/Kg 100 57 - 120
Butyl benzyl phthalate 667 653 ug/Kg 98 58 - 120
Chrysene 667 637 ug/Kg 96 62 - 120
Dibenz(a,h)anthracene 667 736 ug/Kg 110 59 - 120
Dibenzofuran 667 658 ug/Kg 99 57 - 120
Diethyl phthalate 667 665 ug/Kg 100 58 - 120
2-Methylphenol 667 617 ug/Kg 93 48 - 120
Dimethyl phthalate 667 708 ug/Kg 106 59 - 120
Di-n-butyl phthalate 667 669 ug/Kg 100 54 - 120
2-Nitroaniline 667 641 ug/Kg 96 50 - 120
Di-n-octyl phthalate 667 703 ug/Kg 105 54 - 120
3-Nitroaniline 667 574 ug/Kg 86 51 - 120
Fluoranthene 667 624 ug/Kg 94 57 - 120
4-Nitroaniline 667 552 ug/Kg 83 52 - 120
Fluorene 667 674 ug/Kg 101 56 - 120
Hexachlorobenzene 667 770 ug/Kg 115 43 - 120
2-Nitrophenol 667 609 ug/Kg 91 49 - 120
Hexachlorobutadiene 667 597 ug/Kg 90 48 - 120
4-Nitrophenol 1330 1230 ug/Kg 93 37 - 120
Hexachlorocyclopentadiene 667 352 ug/Kg 53 23 - 120
Hexachloroethane 667 576 ug/Kg 86 46 - 120
Indeno[1,2,3-cd]pyrene 667 710 ug/Kg 106 62 - 120
bis (2-chloroisopropyl) ether 667 556 ug/Kg 83 34 - 120
Isophorone 667 552 ug/Kg 83 54 - 120
Naphthalene 667 601 ug/Kg 90 53 - 120
Nitrobenzene 667 554 ug/Kg 83 50 - 120
N-Nitrosodi-n-propylamine 667 595 ug/Kg 89 49 - 120
N-Nitrosodiphenylamine 667 812 * ug/Kg 122 52 - 120
2,4,5-Trichlorophenol 667 566 ug/Kg 85 31 - 120
Pentachlorophenol 1330 676 ug/Kg 51 23 - 120
2,4,6-Trichlorophenol 667 471 ug/Kg 71 18 - 120
Phenol 667 567 ug/Kg 85 49 - 120
Phenanthrene 667 619 ug/Kg 93 58 - 120
Pyrene 667 639 ug/Kg 96 57 - 120
3 & 4 Methylphenol 667 594 ug/Kg 89 49 - 120
2,6-Dinitrotoluene 667 706 ug/Kg 106 61 - 120
2-Fluorobiphenyl (Surr) 39 - 120
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
822-Fluorophenol (Surr) 33 - 120
752,4,6-Tribromophenol (Surr) 10 - 120
84Nitrobenzene-d5 (Surr) 32 - 120
83Phenol-d5 (Surr) 32 - 120
113Terphenyl-d14 (Surr) 47 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233761/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
RL MDL
Benzaldehyde ND 1.0 0.39 ug/L 06/09/16 07:34 06/10/16 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.131.0 ug/L 06/09/16 07:34 06/10/16 09:52 11,1'-Biphenyl
0.977 J 0.205.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Caprolactam
ND 0.281.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Carbazole
ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chloronaphthalene
ND 0.291.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chlorophenol
ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Bromophenyl phenyl ether
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloro-3-methylphenol
ND 0.0900.20 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylnaphthalene
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloroaniline
ND 0.302.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chlorophenyl phenyl ether
ND 0.375.0 ug/L 06/09/16 07:34 06/10/16 09:52 13,3'-Dichlorobenzidine
ND 0.0440.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthene
ND 0.192.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dichlorophenol
ND 0.0480.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthylene
ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Acetophenone
ND 0.252.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dimethylphenol
ND 0.0880.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Anthracene
ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Atrazine
ND 2.45.0 ug/L 06/09/16 07:34 06/10/16 09:52 14,6-Dinitro-2-methylphenol
ND 0.0300.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]anthracene
ND 0.325.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrophenol
ND 0.0510.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]pyrene
ND 0.255.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrotoluene
ND 0.0390.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[b]fluoranthene
ND 0.0460.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[g,h,i]perylene
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[k]fluoranthene
ND 0.321.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethoxy)methane
ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethyl)ether
ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-ethylhexyl) phthalate
ND 0.262.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Butyl benzyl phthalate
ND 0.0500.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Chrysene
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenz(a,h)anthracene
ND 0.0201.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenzofuran
ND 0.602.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Diethyl phthalate
ND 0.171.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylphenol
ND 0.292.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dimethyl phthalate
ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-butyl phthalate
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitroaniline
ND 0.232.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-octyl phthalate
ND 0.282.0 ug/L 06/09/16 07:34 06/10/16 09:52 13-Nitroaniline
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluoranthene
ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Nitroaniline
ND 0.0410.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluorene
ND 0.0850.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobenzene
ND 0.282.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitrophenol
ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobutadiene
ND 0.295.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Nitrophenol
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233761/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
RL MDL
Hexachlorocyclopentadiene ND 10 0.24 ug/L 06/09/16 07:34 06/10/16 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.191.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachloroethane
ND 0.0430.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Indeno[1,2,3-cd]pyrene
ND 0.401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1bis (2-chloroisopropyl) ether
ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Isophorone
ND 0.0630.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Naphthalene
ND 0.0401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene
ND 0.241.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodi-n-propylamine
ND 0.311.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodiphenylamine
ND 0.305.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4,5-Trichlorophenol
ND 0.275.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Pentachlorophenol
ND 0.245.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4,6-Trichlorophenol
ND 0.601.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenol
ND 0.0620.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenanthrene
ND 0.0420.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Pyrene
ND 0.802.0 ug/L 06/09/16 07:34 06/10/16 09:52 13 & 4 Methylphenol
ND 0.805.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,6-Dinitrotoluene
2-Fluorobiphenyl (Surr) 74 42 - 120 06/10/16 09:52 1
MB MB
Surrogate
06/09/16 07:34
Dil FacPrepared AnalyzedQualifier Limits%Recovery
39 06/09/16 07:34 06/10/16 09:52 12-Fluorophenol (Surr) 10 - 120
68 06/09/16 07:34 06/10/16 09:52 12,4,6-Tribromophenol (Surr) 35 - 125
73 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene-d5 (Surr) 36 - 120
24 06/09/16 07:34 06/10/16 09:52 1Phenol-d5 (Surr) 10 - 120
76 06/09/16 07:34 06/10/16 09:52 1Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
Benzaldehyde 40.0 37.0 ug/L 93 60 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1'-Biphenyl 20.0 17.6 ug/L 88 58 - 120
Caprolactam 40.0 3.29 J * ug/L 8 10 - 120
Carbazole 20.0 20.0 ug/L 100 60 - 126
2-Chloronaphthalene 20.0 17.9 ug/L 89 56 - 120
2-Chlorophenol 20.0 15.9 ug/L 79 57 - 120
4-Bromophenyl phenyl ether 20.0 19.3 ug/L 97 52 - 128
4-Chloro-3-methylphenol 20.0 17.7 ug/L 89 59 - 120
2-Methylnaphthalene 20.0 18.0 ug/L 90 58 - 120
4-Chloroaniline 20.0 4.65 ug/L 23 10 - 120
4-Chlorophenyl phenyl ether 20.0 18.1 ug/L 91 58 - 120
3,3'-Dichlorobenzidine 40.0 31.8 ug/L 80 10 - 134
Acenaphthene 20.0 17.9 ug/L 89 57 - 120
2,4-Dichlorophenol 20.0 18.3 ug/L 92 57 - 120
Acenaphthylene 20.0 18.7 ug/L 94 55 - 120
Acetophenone 20.0 18.1 ug/L 90 60 - 120
2,4-Dimethylphenol 20.0 17.6 ug/L 88 55 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
Anthracene 20.0 19.9 ug/L 99 58 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Atrazine 40.0 39.5 ug/L 99 61 - 132
4,6-Dinitro-2-methylphenol 40.0 35.5 ug/L 89 35 - 140
Benzo[a]anthracene 20.0 17.1 ug/L 86 59 - 120
2,4-Dinitrophenol 40.0 30.0 ug/L 75 18 - 127
Benzo[a]pyrene 20.0 16.6 ug/L 83 60 - 120
2,4-Dinitrotoluene 20.0 18.7 ug/L 93 65 - 120
Benzo[b]fluoranthene 20.0 17.0 ug/L 85 62 - 120
Benzo[g,h,i]perylene 20.0 17.7 ug/L 88 59 - 120
Benzo[k]fluoranthene 20.0 18.1 ug/L 90 57 - 120
Bis(2-chloroethoxy)methane 20.0 18.7 ug/L 94 61 - 120
Bis(2-chloroethyl)ether 20.0 17.6 ug/L 88 55 - 120
Bis(2-ethylhexyl) phthalate 20.0 14.4 ug/L 72 62 - 123
Butyl benzyl phthalate 20.0 16.7 ug/L 83 61 - 120
Chrysene 20.0 16.9 ug/L 84 61 - 120
Dibenz(a,h)anthracene 20.0 14.8 ug/L 74 61 - 120
Dibenzofuran 20.0 18.1 ug/L 91 58 - 120
Diethyl phthalate 20.0 19.0 ug/L 95 62 - 120
2-Methylphenol 20.0 13.1 ug/L 65 52 - 120
Dimethyl phthalate 20.0 19.2 ug/L 96 62 - 120
Di-n-butyl phthalate 20.0 19.9 ug/L 99 59 - 128
2-Nitroaniline 20.0 20.1 ug/L 100 56 - 123
Di-n-octyl phthalate 20.0 13.7 ug/L 68 58 - 120
3-Nitroaniline 20.0 17.4 ug/L 87 36 - 120
Fluoranthene 20.0 19.5 ug/L 97 57 - 123
4-Nitroaniline 20.0 19.0 ug/L 95 51 - 122
Fluorene 20.0 18.9 ug/L 94 56 - 120
Hexachlorobenzene 20.0 18.5 ug/L 92 47 - 127
2-Nitrophenol 20.0 17.2 ug/L 86 62 - 120
Hexachlorobutadiene 20.0 17.0 ug/L 85 50 - 120
4-Nitrophenol 40.0 12.1 ug/L 30 16 - 120
Hexachlorocyclopentadiene 20.0 16.3 ug/L 82 25 - 120
Hexachloroethane 20.0 16.6 ug/L 83 50 - 120
Indeno[1,2,3-cd]pyrene 20.0 15.4 ug/L 77 61 - 120
bis (2-chloroisopropyl) ether 20.0 18.0 ug/L 90 46 - 120
Isophorone 20.0 18.9 ug/L 95 61 - 120
Naphthalene 20.0 17.4 ug/L 87 54 - 120
Nitrobenzene 20.0 18.8 ug/L 94 58 - 120
N-Nitrosodi-n-propylamine 20.0 18.3 ug/L 91 60 - 120
N-Nitrosodiphenylamine 20.0 19.2 ug/L 96 54 - 122
2,4,5-Trichlorophenol 20.0 19.2 ug/L 96 57 - 120
Pentachlorophenol 40.0 37.2 ug/L 93 35 - 121
2,4,6-Trichlorophenol 20.0 19.2 ug/L 96 60 - 120
Phenol 20.0 5.06 ug/L 25 16 - 120
Phenanthrene 20.0 18.5 ug/L 93 58 - 120
Pyrene 20.0 19.3 ug/L 97 60 - 120
3 & 4 Methylphenol 20.0 11.7 ug/L 58 46 - 120
2,6-Dinitrotoluene 20.0 19.8 ug/L 99 65 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
2-Fluorobiphenyl (Surr) 42 - 120
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
412-Fluorophenol (Surr) 10 - 120
872,4,6-Tribromophenol (Surr) 35 - 125
94Nitrobenzene-d5 (Surr) 36 - 120
24Phenol-d5 (Surr) 10 - 120
78Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Method BlankLab Sample ID: MB 240-234253/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234362 Prep Batch: 234253
RL MDL
Caprolactam ND 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 08:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2-Fluorobiphenyl (Surr) 80 42 - 120 06/14/16 08:11 1
MB MB
Surrogate
06/13/16 11:40
Dil FacPrepared AnalyzedQualifier Limits%Recovery
37 06/13/16 11:40 06/14/16 08:11 12-Fluorophenol (Surr) 10 - 120
96 06/13/16 11:40 06/14/16 08:11 12,4,6-Tribromophenol (Surr) 35 - 125
84 06/13/16 11:40 06/14/16 08:11 1Nitrobenzene-d5 (Surr) 36 - 120
22 06/13/16 11:40 06/14/16 08:11 1Phenol-d5 (Surr) 10 - 120
82 06/13/16 11:40 06/14/16 08:11 1Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-234253/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234362 Prep Batch: 234253
Caprolactam 40.0 2.99 J * ug/L 7 10 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Fluorobiphenyl (Surr) 42 - 120
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
302-Fluorophenol (Surr) 10 - 120
1012,4,6-Tribromophenol (Surr) 35 - 125
81Nitrobenzene-d5 (Surr) 36 - 120
19Phenol-d5 (Surr) 10 - 120
31Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233811 Prep Batch: 233761
Benzaldehyde ND 38.1 32.6 ug/L 86 42 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1'-Biphenyl ND 19.0 15.4 ug/L 81 45 - 120
Caprolactam ND F1 * 38.1 2.36 J F1 ug/L 6 10 - 120
Carbazole ND 19.0 17.6 ug/L 93 55 - 120
2-Chloronaphthalene ND 19.0 15.6 ug/L 82 43 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233811 Prep Batch: 233761
2-Chlorophenol ND 19.0 12.7 ug/L 67 43 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Bromophenyl phenyl ether ND 19.0 16.1 ug/L 85 32 - 120
4-Chloro-3-methylphenol ND 19.0 13.8 ug/L 73 49 - 120
2-Methylnaphthalene ND 19.0 15.8 ug/L 83 42 - 120
4-Chloroaniline ND 19.0 2.75 ug/L 14 10 - 120
4-Chlorophenyl phenyl ether ND 19.0 15.9 ug/L 83 41 - 120
3,3'-Dichlorobenzidine ND 38.1 26.4 ug/L 69 10 - 120
Acenaphthene ND 19.0 15.2 ug/L 80 37 - 120
2,4-Dichlorophenol ND 19.0 15.2 ug/L 80 44 - 120
Acenaphthylene ND 19.0 16.4 ug/L 86 40 - 120
Acetophenone ND 19.0 15.9 ug/L 83 43 - 120
2,4-Dimethylphenol ND 19.0 13.6 ug/L 71 38 - 120
Anthracene ND 19.0 17.1 ug/L 90 36 - 120
Atrazine ND 38.1 34.5 ug/L 90 50 - 122
4,6-Dinitro-2-methylphenol ND 38.1 21.9 ug/L 57 10 - 135
Benzo[a]anthracene ND 19.0 12.2 ug/L 64 18 - 120
2,4-Dinitrophenol ND 38.1 15.6 ug/L 41 10 - 122
Benzo[a]pyrene ND 19.0 10.5 ug/L 55 13 - 120
2,4-Dinitrotoluene ND 19.0 15.8 ug/L 83 50 - 120
Benzo[b]fluoranthene ND 19.0 11.5 ug/L 60 14 - 120
Benzo[g,h,i]perylene ND 19.0 10.6 ug/L 56 10 - 120
Benzo[k]fluoranthene ND 19.0 11.0 ug/L 58 13 - 120
Bis(2-chloroethoxy)methane ND 19.0 16.1 ug/L 85 50 - 120
Bis(2-chloroethyl)ether ND 19.0 15.2 ug/L 80 45 - 120
Bis(2-ethylhexyl) phthalate ND 19.0 9.57 ug/L 50 10 - 120
Butyl benzyl phthalate ND 19.0 14.3 ug/L 75 28 - 120
Chrysene ND 19.0 11.7 ug/L 61 17 - 120
Dibenz(a,h)anthracene ND 19.0 9.66 ug/L 51 10 - 120
Dibenzofuran ND 19.0 15.6 ug/L 82 44 - 120
Diethyl phthalate ND 19.0 16.8 ug/L 88 51 - 120
2-Methylphenol ND 19.0 9.49 ug/L 50 34 - 120
Dimethyl phthalate ND 19.0 16.6 ug/L 87 54 - 120
Di-n-butyl phthalate ND 19.0 16.8 ug/L 88 34 - 120
2-Nitroaniline ND 19.0 16.9 ug/L 89 49 - 120
Di-n-octyl phthalate ND 19.0 9.38 ug/L 49 10 - 120
3-Nitroaniline ND 19.0 13.4 ug/L 70 10 - 120
Fluoranthene ND 19.0 16.3 ug/L 86 28 - 120
4-Nitroaniline ND 19.0 14.7 ug/L 77 29 - 120
Fluorene ND 19.0 16.3 ug/L 85 38 - 120
Hexachlorobenzene ND 19.0 14.7 ug/L 77 17 - 120
2-Nitrophenol ND 19.0 14.7 ug/L 77 47 - 120
Hexachlorobutadiene ND 19.0 14.8 ug/L 77 32 - 120
4-Nitrophenol ND 38.1 6.93 ug/L 18 10 - 120
Hexachlorocyclopentadiene ND 19.0 9.31 J ug/L 49 10 - 120
Hexachloroethane ND 19.0 14.7 ug/L 77 10 - 120
Indeno[1,2,3-cd]pyrene ND 19.0 9.51 ug/L 50 10 - 120
bis (2-chloroisopropyl) ether ND 19.0 15.9 ug/L 84 39 - 120
Isophorone ND 19.0 16.3 ug/L 85 52 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233811 Prep Batch: 233761
Naphthalene 0.31 19.0 15.2 ug/L 78 37 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Nitrobenzene ND 19.0 15.9 ug/L 83 47 - 120
N-Nitrosodi-n-propylamine ND 19.0 16.5 ug/L 87 49 - 120
N-Nitrosodiphenylamine ND 19.0 16.9 ug/L 89 46 - 120
2,4,5-Trichlorophenol ND 19.0 16.4 ug/L 86 49 - 120
Pentachlorophenol ND 38.1 31.4 ug/L 83 32 - 120
2,4,6-Trichlorophenol ND 19.0 16.3 ug/L 86 51 - 120
Phenol ND 19.0 3.05 ug/L 16 10 - 120
Phenanthrene ND 19.0 15.9 ug/L 83 38 - 120
Pyrene ND 19.0 16.2 ug/L 85 26 - 120
3 & 4 Methylphenol ND 19.0 7.86 ug/L 41 26 - 120
2,6-Dinitrotoluene ND 19.0 17.6 ug/L 92 54 - 120
2-Fluorobiphenyl (Surr) 42 - 120
Surrogate
81
MS MS
Qualifier Limits%Recovery
272-Fluorophenol (Surr) 10 - 120
822,4,6-Tribromophenol (Surr) 35 - 125
84Nitrobenzene-d5 (Surr) 36 - 120
15Phenol-d5 (Surr) 10 - 120
60Terphenyl-d14 (Surr) 17 - 120
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 240-233006/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
RL MDL
4,4'-DDD ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.271.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDE
ND 0.311.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDT
ND 0.201.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Aldrin
ND 0.601.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-BHC
ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-Chlordane
ND 0.361.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1beta-BHC
ND 0.221.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1delta-BHC
ND 0.161.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Dieldrin
ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan I
ND 0.381.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan II
ND 0.341.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan sulfate
ND 0.211.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin
ND 0.321.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin aldehyde
ND 0.421.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin ketone
ND 0.461.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-BHC (Lindane)
ND 0.861.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-Chlordane
ND 0.701.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor
ND 0.401.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor epoxide
ND 9.867 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Toxaphene
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233006/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
RL MDL
Methoxychlor ND 3.3 0.54 ug/Kg 06/03/16 07:28 06/10/16 17:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
DCB Decachlorobiphenyl 81 42 - 138 06/10/16 17:39 1
MB MB
Surrogate
06/03/16 07:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
85 06/03/16 07:28 06/10/16 17:39 1DCB Decachlorobiphenyl 42 - 138
77 06/03/16 07:28 06/10/16 17:39 1Tetrachloro-m-xylene 31 - 159
64 06/03/16 07:28 06/10/16 17:39 1Tetrachloro-m-xylene 31 - 159
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233006/6-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
4,4'-DDD 33.3 26.5 ug/Kg 80 47 - 157
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4,4'-DDE 33.3 26.2 ug/Kg 79 56 - 125
4,4'-DDT 33.3 26.3 ug/Kg 79 57 - 142
Aldrin 33.3 23.5 ug/Kg 70 37 - 129
alpha-BHC 33.3 25.6 ug/Kg 77 50 - 125
alpha-Chlordane 33.3 24.8 ug/Kg 74 53 - 120
beta-BHC 33.3 24.7 ug/Kg 74 41 - 125
delta-BHC 33.3 21.6 ug/Kg 65 52 - 124
Dieldrin 33.3 25.9 ug/Kg 78 55 - 124
Endosulfan I 33.3 17.6 ug/Kg 53 18 - 120
Endosulfan II 33.3 20.8 ug/Kg 62 19 - 120
Endosulfan sulfate 33.3 24.6 ug/Kg 74 54 - 128
Endrin 33.3 27.5 ug/Kg 83 53 - 151
Endrin aldehyde 33.3 22.7 ug/Kg 68 44 - 130
Endrin ketone 33.3 24.3 ug/Kg 73 49 - 120
gamma-BHC (Lindane) 33.3 25.4 ug/Kg 76 50 - 123
gamma-Chlordane 33.3 25.2 ug/Kg 76 53 - 120
Heptachlor 33.3 27.0 ug/Kg 81 48 - 129
Heptachlor epoxide 33.3 25.4 ug/Kg 76 54 - 120
Methoxychlor 33.3 25.7 ug/Kg 77 52 - 147
DCB Decachlorobiphenyl 42 - 138
Surrogate
79
LCS LCS
Qualifier Limits%Recovery
74DCB Decachlorobiphenyl 42 - 138
70Tetrachloro-m-xylene 31 - 159
60Tetrachloro-m-xylene 31 - 159
Client Sample ID: Method BlankLab Sample ID: MB 240-233753/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
RL MDL
4,4'-DDD ND 0.050 0.018 ug/L 06/09/16 06:31 06/13/16 13:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDE
ND 0.0170.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDT
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233753/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
RL MDL
Aldrin ND 0.050 0.013 ug/L 06/09/16 06:31 06/13/16 13:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-BHC
ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-Chlordane
ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1beta-BHC
ND 0.0290.050 ug/L 06/09/16 06:31 06/13/16 13:51 1delta-BHC
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Dieldrin
ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan I
ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan II
ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan sulfate
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin
ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin aldehyde
ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin ketone
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-BHC (Lindane)
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-Chlordane
ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor
ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor epoxide
ND 0.202.0 ug/L 06/09/16 06:31 06/13/16 13:51 1Toxaphene
ND 0.0130.10 ug/L 06/09/16 06:31 06/13/16 13:51 1Methoxychlor
DCB Decachlorobiphenyl 48 30 - 128 06/13/16 13:51 1
MB MB
Surrogate
06/09/16 06:31
Dil FacPrepared AnalyzedQualifier Limits%Recovery
48 06/09/16 06:31 06/13/16 13:51 1DCB Decachlorobiphenyl 30 - 128
90 06/09/16 06:31 06/13/16 13:51 1Tetrachloro-m-xylene 36 - 124
85 06/09/16 06:31 06/13/16 13:51 1Tetrachloro-m-xylene 36 - 124
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233753/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
4,4'-DDD 0.500 0.492 ug/L 98 54 - 163
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4,4'-DDE 0.500 0.472 ug/L 94 60 - 146
4,4'-DDT 0.500 0.489 ug/L 98 56 - 160
Aldrin 0.500 0.439 ug/L 88 44 - 145
alpha-BHC 0.500 0.461 ug/L 92 53 - 148
alpha-Chlordane 0.500 0.475 ug/L 95 55 - 141
beta-BHC 0.500 0.469 ug/L 94 55 - 139
delta-BHC 0.500 0.409 ug/L 82 60 - 145
Dieldrin 0.500 0.485 ug/L 97 57 - 145
Endosulfan I 0.500 0.428 ug/L 86 26 - 120
Endosulfan II 0.500 0.460 ug/L 92 25 - 123
Endosulfan sulfate 0.500 0.471 ug/L 94 60 - 137
Endrin 0.500 0.462 ug/L 92 66 - 142
Endrin aldehyde 0.500 0.462 ug/L 92 59 - 120
Endrin ketone 0.500 0.481 ug/L 96 64 - 120
gamma-BHC (Lindane) 0.500 0.459 ug/L 92 53 - 144
gamma-Chlordane 0.500 0.483 ug/L 97 57 - 140
Heptachlor 0.500 0.441 ug/L 88 56 - 123
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233753/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
Heptachlor epoxide 0.500 0.477 ug/L 95 44 - 151
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Methoxychlor 0.500 0.465 ug/L 93 56 - 153
DCB Decachlorobiphenyl 30 - 128
Surrogate
66
LCS LCS
Qualifier Limits%Recovery
56DCB Decachlorobiphenyl 30 - 128
90Tetrachloro-m-xylene 36 - 124
83Tetrachloro-m-xylene 36 - 124
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 234206 Prep Batch: 233753
4,4'-DDD ND 0.476 0.410 ug/L 86 56 - 155
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4,4'-DDE ND 0.476 0.388 ug/L 81 47 - 137
4,4'-DDT ND 0.476 0.399 ug/L 84 37 - 134
Aldrin ND 0.476 0.348 ug/L 73 51 - 120
alpha-BHC ND 0.476 0.447 ug/L 94 53 - 160
alpha-Chlordane ND 0.476 0.382 ug/L 80 42 - 153
beta-BHC ND 0.476 0.420 ug/L 88 42 - 160
delta-BHC ND 0.476 0.366 ug/L 77 49 - 160
Dieldrin ND 0.476 0.422 ug/L 89 48 - 160
Endosulfan I ND 0.476 0.395 ug/L 83 29 - 159
Endosulfan II ND 0.476 0.383 ug/L 81 35 - 142
Endosulfan sulfate ND 0.476 0.425 ug/L 89 47 - 150
Endrin ND 0.476 0.423 ug/L 89 50 - 149
Endrin aldehyde ND 0.476 0.414 ug/L 87 42 - 149
Endrin ketone ND 0.476 0.443 ug/L 93 39 - 138
gamma-BHC (Lindane) ND 0.476 0.437 ug/L 92 53 - 160
gamma-Chlordane ND 0.476 0.389 ug/L 82 45 - 153
Heptachlor ND 0.476 0.376 ug/L 79 36 - 128
Heptachlor epoxide ND 0.476 0.426 ug/L 89 35 - 160
Methoxychlor ND 0.476 0.397 ug/L 83 35 - 141
DCB Decachlorobiphenyl 30 - 128
Surrogate
30
MS MS
Qualifier Limits%Recovery
29 XDCB Decachlorobiphenyl 30 - 128
80Tetrachloro-m-xylene 36 - 124
80Tetrachloro-m-xylene 36 - 124
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 240-233005/12-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233178 Prep Batch: 233005
RL MDL
Aroclor-1016 ND 33 12 ug/Kg 06/03/16 07:23 06/06/16 15:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1633 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1221
ND 2033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1232
ND 1133 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1242
ND 8.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1248
ND 1433 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1254
ND 9.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1260
Tetrachloro-m-xylene 64 14 - 128 06/06/16 15:06 1
MB MB
Surrogate
06/03/16 07:23
Dil FacPrepared AnalyzedQualifier Limits%Recovery
79 06/03/16 07:23 06/06/16 15:06 1DCB Decachlorobiphenyl 10 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233005/13-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233178 Prep Batch: 233005
Aroclor-1016 333 246 ug/Kg 74 47 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aroclor-1260 333 277 ug/Kg 83 46 - 120
Tetrachloro-m-xylene 14 - 128
Surrogate
66
LCS LCS
Qualifier Limits%Recovery
80DCB Decachlorobiphenyl 10 - 132
Client Sample ID: Method BlankLab Sample ID: MB 240-233752/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
RL MDL
Aroclor-1016 ND 0.10 0.050 ug/L 06/09/16 06:29 06/13/16 10:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0900.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1221
ND 0.0700.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1232
ND 0.0600.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1242
ND 0.0500.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1248
ND 0.0300.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1254
ND 0.0400.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1260
Tetrachloro-m-xylene 59 21 - 120 06/13/16 10:16 1
MB MB
Surrogate
06/09/16 06:29
Dil FacPrepared AnalyzedQualifier Limits%Recovery
33 06/09/16 06:29 06/13/16 10:16 1DCB Decachlorobiphenyl 10 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233752/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
Aroclor-1016 2.50 1.60 ug/L 64 32 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233752/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
Aroclor-1260 2.50 1.52 ug/L 61 36 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Tetrachloro-m-xylene 21 - 120
Surrogate
60
LCS LCS
Qualifier Limits%Recovery
36DCB Decachlorobiphenyl 10 - 120
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 234149 Prep Batch: 233752
Aroclor-1016 ND 2.38 1.40 ug/L 59 24 - 121
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Aroclor-1260 ND 2.38 0.990 ug/L 42 10 - 120
Tetrachloro-m-xylene 21 - 120
Surrogate
59
MS MS
Qualifier Limits%Recovery
11DCB Decachlorobiphenyl 10 - 120
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-232891/1-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891
RL MDL
Silver 0.00180 J 0.20 0.0014 mg/Kg 06/02/16 11:09 06/03/16 20:41 2
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.64 J 0.6210 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Aluminum
0.0354 J 0.0261.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Arsenic
ND 0.221.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Barium
0.0228 J 0.0110.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Beryllium
0.00780 J 0.00370.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cadmium
0.0170 J 0.00170.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cobalt
0.347 J 0.0600.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Chromium
0.243 J 0.0970.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Copper
281 3.220 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Iron
1.73 0.121.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Manganese
0.0688 J 0.0450.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Lead
ND 0.0140.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Antimony
0.0472 J 0.0401.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Selenium
ND 0.0190.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Thallium
ND 0.0371.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Vanadium
1.17 J 0.504.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Zinc
34.7 J 22200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Calcium
8.60 J 4.9200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Potassium
7.73 J 4.0200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Magnesium
26.5 J 8.7200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Sodium
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-232891/1-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233381 Prep Batch: 232891
RL MDL
Nickel 0.0802 J 0.40 0.039 mg/Kg 06/02/16 11:09 06/06/16 14:18 2
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891
Silver 10.0 9.61 mg/Kg 96 60 - 114
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aluminum 1000 964 mg/Kg 96 80 - 120
Arsenic 100 92.4 mg/Kg 92 73 - 110
Barium 100 95.2 mg/Kg 95 70 - 110
Beryllium 100 104 mg/Kg 104 79 - 110
Cadmium 100 92.8 mg/Kg 93 74 - 110
Cobalt 100 101 mg/Kg 101 74 - 110
Chromium 100 96.8 mg/Kg 97 70 - 110
Copper 100 98.5 mg/Kg 99 73 - 110
Iron 1000 982 mg/Kg 98 80 - 120
Manganese 100 98.4 mg/Kg 98 80 - 120
Lead 100 108 mg/Kg 108 75 - 110
Antimony 10.0 9.42 mg/Kg 94 68 - 113
Selenium 100 89.0 mg/Kg 89 65 - 110
Thallium 25.0 26.0 mg/Kg 104 71 - 110
Vanadium 100 96.6 mg/Kg 97 72 - 110
Zinc 100 95.9 mg/Kg 96 72 - 113
Calcium 1000 973 mg/Kg 97 80 - 120
Potassium 1000 1000 mg/Kg 100 80 - 120
Magnesium 1000 1000 mg/Kg 100 80 - 120
Sodium 1000 1010 mg/Kg 101 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233381 Prep Batch: 232891
Nickel 100 99.0 mg/Kg 99 75 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 240-233672/2-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:40 1Aluminum
ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Arsenic
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Barium
ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Beryllium
ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cadmium
ND 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cobalt
ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Chromium
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233672/2-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Copper ND 2.0 0.75 ug/L 06/08/16 13:00 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 16100 ug/L 06/08/16 13:00 06/09/16 13:40 1Iron
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Manganese
ND 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Nickel
ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Lead
ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Antimony
0.288 J 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Selenium
ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Thallium
ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Vanadium
ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:40 1Zinc
ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:40 1Calcium
ND 301000 ug/L 06/08/16 13:00 06/09/16 13:40 1Potassium
ND 481000 ug/L 06/08/16 13:00 06/09/16 13:40 1Magnesium
ND 681000 ug/L 06/08/16 13:00 06/09/16 13:40 1Sodium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233672/3-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
Silver 100 94.5 ug/L 95 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aluminum 10000 10400 ug/L 104 80 - 120
Arsenic 1000 913 ug/L 91 80 - 120
Barium 1000 931 ug/L 93 80 - 120
Beryllium 1000 1140 ug/L 114 80 - 120
Cadmium 1000 927 ug/L 93 80 - 120
Cobalt 1000 952 ug/L 95 80 - 120
Chromium 1000 973 ug/L 97 80 - 120
Copper 1000 931 ug/L 93 80 - 120
Iron 10000 9370 ug/L 94 80 - 120
Manganese 1000 997 ug/L 100 80 - 120
Nickel 1000 966 ug/L 97 80 - 120
Lead 1000 823 ug/L 82 80 - 120
Antimony 100 94.0 ug/L 94 80 - 120
Selenium 1000 904 ug/L 90 80 - 120
Thallium 250 209 ug/L 84 80 - 120
Vanadium 1000 1010 ug/L 101 80 - 120
Zinc 1000 959 ug/L 96 80 - 120
Calcium 10000 10700 ug/L 107 80 - 120
Potassium 10000 9350 ug/L 93 80 - 120
Magnesium 10000 9570 ug/L 96 80 - 120
Sodium 10000 9620 ug/L 96 80 - 120
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-CMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:36 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-CMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Aluminum ND 50 9.0 ug/L 06/08/16 13:00 06/09/16 13:36 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Arsenic
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Barium
ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Beryllium
ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cadmium
0.115 J 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cobalt
ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Chromium
1.96 J 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Copper
ND 16100 ug/L 06/08/16 13:00 06/09/16 13:36 1Iron
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Manganese
0.232 J 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Nickel
ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Lead
ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Antimony
ND 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Selenium
ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Thallium
ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Vanadium
ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:36 1Zinc
ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:36 1Calcium
ND 301000 ug/L 06/08/16 13:00 06/09/16 13:36 1Potassium
ND 481000 ug/L 06/08/16 13:00 06/09/16 13:36 1Magnesium
184 J 681000 ug/L 06/08/16 13:00 06/09/16 13:36 1Sodium
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 240-233673/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233843 Prep Batch: 233673
RL MDL
Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233673/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233843 Prep Batch: 233673
Mercury 5.00 4.82 ug/L 96 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-DMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673
RL MDL
Mercury 0.0925 J 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 11:58 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 240-232940/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233026 Prep Batch: 232940
RL MDL
Mercury ND 0.10 0.014 mg/Kg 06/02/16 15:00 06/03/16 07:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232940/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233026 Prep Batch: 232940
Mercury 0.833 0.865 mg/Kg 104 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 240-233791/9-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
RL MDL
Cr (VI) 0.358 J 0.80 0.15 mg/Kg 06/09/16 09:04 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 240-233791/11-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
Cr (VI) 643 582 mg/Kg 90 75 - 125
Analyte
LCSI LCSI
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 240-233791/10-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
Cr (VI) 20.0 18.5 mg/Kg 93 90 - 110
Analyte
LCSS LCSS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-AMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233639
RL MDL
Cr (VI) ND 0.020 0.0021 mg/L 06/08/16 11:47 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
GC/MS VOA
Analysis Batch: 233030
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 233052240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 8260BLCS 240-233030/5 Lab Control Sample Total/NA
Solid 8260BMB 240-233030/6 Method Blank Total/NA
Prep Batch: 233052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5030A240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Leach Batch: 233606
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1312240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) SPLP
Solid 1312LB 240-233606/1-A MB Method Blank SPLP
Analysis Batch: 233711
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 233606240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) SPLP
Solid 8260B 233606LB 240-233606/1-A MB Method Blank SPLP
Solid 8260BLCS 240-233711/6 Lab Control Sample Total/NA
GC/MS Semi VOA
Prep Batch: 233013
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 3540CLCS 240-233013/18-A Lab Control Sample Total/NA
Solid 3540CMB 240-233013/17-A Method Blank Total/NA
Analysis Batch: 233383
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233013240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 8270C 233013LCS 240-233013/18-A Lab Control Sample Total/NA
Solid 8270C 233013MB 240-233013/17-A Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid D3987-85240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Prep Batch: 233761
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3510C 233529240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3510CLCS 240-233761/5-A Lab Control Sample Total/NA
Solid 3510CMB 240-233761/4-A Method Blank Total/NA
Analysis Batch: 233811
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233761240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8270C 233761240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
GC/MS Semi VOA (Continued)
Analysis Batch: 233974
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233761LCS 240-233761/5-A Lab Control Sample Total/NA
Solid 8270C 233761MB 240-233761/4-A Method Blank Total/NA
Leach Batch: 234140
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Prep Batch: 234253
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 234140240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3510CLCS 240-234253/4-A Lab Control Sample Total/NA
Solid 3510CMB 240-234253/3-A Method Blank Total/NA
Analysis Batch: 234362
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 234253240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8270C 234253LCS 240-234253/4-A Lab Control Sample Total/NA
Solid 8270C 234253MB 240-234253/3-A Method Blank Total/NA
GC Semi VOA
Prep Batch: 233005
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 3540CLCS 240-233005/13-A Lab Control Sample Total/NA
Solid 3540CMB 240-233005/12-A Method Blank Total/NA
Prep Batch: 233006
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 3540CLCS 240-233006/6-A Lab Control Sample Total/NA
Solid 3540CMB 240-233006/5-A Method Blank Total/NA
Analysis Batch: 233178
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8082A 233005240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 8082A 233005LCS 240-233005/13-A Lab Control Sample Total/NA
Solid 8082A 233005MB 240-233005/12-A Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid D3987-85240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Prep Batch: 233752
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3520C 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3520C 233529240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3520CLCS 240-233752/5-A Lab Control Sample Total/NA
Solid 3520CMB 240-233752/4-A Method Blank Total/NA
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
GC Semi VOA (Continued)
Prep Batch: 233753
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3520C 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3520C 233529240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3520CLCS 240-233753/5-A Lab Control Sample Total/NA
Solid 3520CMB 240-233753/4-A Method Blank Total/NA
Analysis Batch: 233996
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 233006240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 8081B 233006LCS 240-233006/6-A Lab Control Sample Total/NA
Solid 8081B 233006MB 240-233006/5-A Method Blank Total/NA
Analysis Batch: 234149
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8082A 233752240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8082A 233752240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8082A 233752LCS 240-233752/5-A Lab Control Sample Total/NA
Solid 8082A 233752MB 240-233752/4-A Method Blank Total/NA
Analysis Batch: 234206
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 233753240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8081B 233753240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 8081B 233753LCS 240-233753/5-A Lab Control Sample Total/NA
Solid 8081B 233753MB 240-233753/4-A Method Blank Total/NA
Metals
Prep Batch: 232891
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 3050BLCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 3050BMB 240-232891/1-A ^2 Method Blank Total/NA
Prep Batch: 232940
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 7471ALCS 240-232940/2-A Lab Control Sample Total/NA
Solid 7471AMB 240-232940/1-A Method Blank Total/NA
Analysis Batch: 233026
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 232940240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 7471A 232940LCS 240-232940/2-A Lab Control Sample Total/NA
Solid 7471A 232940MB 240-232940/1-A Method Blank Total/NA
Analysis Batch: 233211
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 232891240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 6020A 232891LCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 6020A 232891MB 240-232891/1-A ^2 Method Blank Total/NA
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Metals (Continued)
Analysis Batch: 233381
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 232891240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 6020A 232891LCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 6020A 232891MB 240-232891/1-A ^2 Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid D3987-85LB 240-233529/1-C Method Blank ASTM Leach
Solid D3987-85LB 240-233529/1-D Method Blank ASTM Leach
Prep Batch: 233672
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3005A 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 3005A 233529LB 240-233529/1-C Method Blank ASTM Leach
Solid 3005ALCS 240-233672/3-A Lab Control Sample Total Recoverable
Solid 3005AMB 240-233672/2-A Method Blank Total Recoverable
Prep Batch: 233673
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 7470A 233529LB 240-233529/1-D Method Blank ASTM Leach
Solid 7470ALCS 240-233673/3-A Lab Control Sample Total/NA
Solid 7470AMB 240-233673/2-A Method Blank Total/NA
Analysis Batch: 233843
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 233673240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 7470A 233673LB 240-233529/1-D Method Blank ASTM Leach
Solid 7470A 233673LCS 240-233673/3-A Lab Control Sample Total/NA
Solid 7470A 233673MB 240-233673/2-A Method Blank Total/NA
Analysis Batch: 233954
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 233672240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 6020A 233672LB 240-233529/1-C Method Blank ASTM Leach
Solid 6020A 233672LCS 240-233672/3-A Lab Control Sample Total Recoverable
Solid 6020A 233672MB 240-233672/2-A Method Blank Total Recoverable
General Chemistry
Analysis Batch: 232880
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid D3987-85LB 240-233529/1-A Method Blank ASTM Leach
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District
Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
General Chemistry (Continued)
Analysis Batch: 233639
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach
Solid 7196A 233529LB 240-233529/1-A Method Blank ASTM Leach
Prep Batch: 233791
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 3060ALCSI 240-233791/11-A Lab Control Sample Total/NA
Solid 3060ALCSS 240-233791/10-A Lab Control Sample Total/NA
Solid 3060AMB 240-233791/9-A Method Blank Total/NA
Analysis Batch: 233886
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 233791240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA
Solid 7196A 233791LCSI 240-233791/11-A Lab Control Sample Total/NA
Solid 7196A 233791LCSS 240-233791/10-A Lab Control Sample Total/NA
Solid 7196A 233791MB 240-233791/9-A Method Blank Total/NA
TestAmerica Canton
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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1Matrix: SolidDate Collected: 05/31/16 13:25
Date Received: 06/01/16 10:20
Leach 1312 06/07/16 20:15 DRJ233606 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP
Analysis 8260B 1 233711 06/08/16 20:25 TJL1 TAL CANSPLP
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3510C 233761 06/09/16 07:34 CSC TAL CANASTM Leach
Analysis 8270C 1 233811 06/09/16 20:29 JMG TAL CANASTM Leach
Leach D3987-85 RE 234140 06/12/16 16:25 DRJ TAL CANASTM Leach
Prep 3510C RE 234253 06/13/16 11:40 JDR TAL CANASTM Leach
Analysis 8270C RE 1 234362 06/14/16 09:49 MRU TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3520C 233753 06/09/16 06:31 CSC TAL CANASTM Leach
Analysis 8081B 1 234206 06/13/16 14:40 BPM TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3520C 233752 06/09/16 06:29 CSC TAL CANASTM Leach
Analysis 8082A 1 234149 06/13/16 09:21 SEM TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3005A 233672 06/08/16 13:00 AJC TAL CANASTM Leach
Analysis 6020A 1 233954 06/09/16 14:08 AS1 TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 7470A 233673 06/08/16 13:30 AJC TAL CANASTM Leach
Analysis 7470A 1 233843 06/09/16 12:18 WKD TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Analysis 7196A 1 233639 06/08/16 13:35 GNR TAL CANASTM Leach
Analysis Moisture 1 232880 06/02/16 10:25 LCN TAL CANTotal/NA
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
Prep 5030A 06/03/16 10:36 SAM233052 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 233030 06/03/16 18:41 SAM TAL CANTotal/NA
Prep 3540C 233013 06/03/16 08:23 DT TAL CANTotal/NA
Analysis 8270C 1 233383 06/07/16 11:12 JMG TAL CANTotal/NA
Prep 3540C 233006 06/03/16 07:28 DT TAL CANTotal/NA
Analysis 8081B 1 233996 06/10/16 16:02 BPM TAL CANTotal/NA
Prep 3540C 233005 06/03/16 07:23 DT TAL CANTotal/NA
Analysis 8082A 1 233178 06/06/16 14:28 HMB TAL CANTotal/NA
Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA
Analysis 6020A 2 233211 06/03/16 21:54 AS1 TAL CANTotal/NA
Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA
Analysis 6020A 2 233381 06/06/16 14:26 AS1 TAL CANTotal/NA
Prep 7471A 232940 06/02/16 15:00 DEE TAL CANTotal/NA
Analysis 7471A 1 233026 06/03/16 07:42 WKD TAL CANTotal/NA
Prep 3060A 233791 06/09/16 09:04 DTN TAL CANTotal/NA
TestAmerica Canton
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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1Matrix: SolidDate Collected: 05/31/16 13:25
Percent Solids: 99.7Date Received: 06/01/16 10:20
Analysis 7196A 06/09/16 13:44 DTN1 233886 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Laboratory References:
TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396
TestAmerica Canton
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Certification SummaryClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)
Laboratory: TestAmerica CantonAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
California 01144CA9NELAP 06-30-14 *
California State Program 9 2927 04-30-17
Connecticut State Program 1 PH-0590 12-31-17
Florida NELAP 4 E87225 06-30-16 *
Illinois NELAP 5 200004 07-31-16 *
Kansas NELAP 7 E-10336 07-31-16 *
Kentucky (UST) State Program 4 58 02-23-17
Kentucky (WW) State Program 4 98016 12-31-16
L-A-B DoD ELAP L2315 07-18-16
Minnesota NELAP 5 039-999-348 12-31-16
Nevada State Program 9 OH-000482008A 07-31-16 *
New Jersey NELAP 2 OH001 06-30-16 *
New York NELAP 2 10975 03-31-17
Ohio VAP State Program 5 CL0024 09-14-17
Oregon NELAP 10 4062 02-23-17
Pennsylvania NELAP 3 68-00340 08-31-16 *
Texas NELAP 6 T104704517-15-5 08-31-16 *
USDA Federal P330-13-00319 11-26-16
Virginia NELAP 3 460175 09-14-16
Washington State Program 10 C971 01-12-17
West Virginia DEP State Program 3 210 12-31-16
Wisconsin State Program 5 999518190 08-31-16 *
TestAmerica Canton
* Certification renewal pending - certification considered valid.
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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Canton4101 Shuffel Street NWNorth Canton, OH 44720Tel: (330)497-9396
TestAmerica Job ID: 240-65486-1Client Project/Site: WESTERLY WWTC-ASH (WWWTC)
For:Northeast Ohio Regional Sewer District3900 Euclid AvenueCleveland, Ohio 44115
Attn: Ms. Sarah Rehner
Authorized for release by:6/14/2016 3:31:56 PM
Nathan Pietras, Project Manager II(330)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Northeast Ohio Regional Sewer DistrictProject/Site: WESTERLY WWTC-ASH (WWWTC)
TestAmerica Job ID: 240-65486-1
Page 2 of 55TestAmerica Canton
6/14/2016
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
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Definitions/GlossaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Qualifiers
GC/MS VOA
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
* LCS or LCSD is outside acceptance limits.
GC/MS Semi VOA
Qualifier Description
* LCS or LCSD is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
General Chemistry
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Canton
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Case NarrativeClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)
Job ID: 240-65486-1
Laboratory: TestAmerica Canton
Narrative
Job Narrative240-65486-1
Comments
No additional comments.
Receipt
The sample was received on 6/1/2016 10:20 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.1º C.
GC/MS VOA Method(s) 8260B: Additional 5 mL of water added due to absorption of the soil for sample WESTERLY WWTC-ASH (WWWTC)
(240-65486-1)
Method(s) 8260B: The laboratory control sample (LCS) for preparation batch 240-233606 and analytical batch 240-233711 recovered outside control limits for 1,1,1-trichloroethane. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA Method(s) 8270C: The following sample was diluted due to the nature of the sample matrix: WESTERLY WWTC-ASH (WWWTC) (240-65486-1). Elevated reporting limits (RLs) are provided.
Method(s) 8270C: The laboratory control sample (LCS) for 233013 associated with sample WESTERLY WWTC-ASH (WWWTC) (240-65486-1), recovered outside control limits for the following analyte: N-Nitrosodiphenylamine. This analyte was biased high in the LCS and was not detected in the associated sample; therefore, the data have been reported.
Method(s) 8270C: The laboratory control sample (LCS) for 233761 recovered outside control limits for Caprolactam. The associated sample, WESTERLY WWTC-ASH (WWWTC) (240-65486-1), was re-prepared and re-analyzed with the Caprolactam recovery in the LCS (prep batch 234253) again failing to meet acceptance criteria. The initial results have been reported as has Caprolactam from the reextracted results.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Method SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method Method Description LaboratoryProtocol
SW8468260B Volatile Organic Compounds (GC/MS) TAL CAN
SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CAN
SW8468081B Organochlorine Pesticides (GC) TAL CAN
SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CAN
SW8466020A Metals (ICP/MS) TAL CAN
SW8467470A Mercury (CVAA) TAL CAN
SW8467471A Mercury (CVAA) TAL CAN
SW8467196A Chromium, Hexavalent TAL CAN
EPAMoisture Percent Moisture TAL CAN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396
TestAmerica Canton
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Sample SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
240-65486-1 WESTERLY WWTC-ASH (WWWTC) Solid 05/31/16 14:10 06/01/16 10:20
TestAmerica Canton
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Detection SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1
☼Acetone
RL
19 ug/Kg
MDL
5.3
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J B7.8 8260B
☼Styrene 4.7 ug/Kg0.38 Total/NA11.1 J 8260B
☼Toluene 4.7 ug/Kg0.25 Total/NA10.34 J 8260B
Acetone 10 ug/L0.94 SPLP15.1 J B 8260B
Chloroform 1.0 ug/L0.25 SPLP11.1 B 8260B
Methylene Chloride 1.0 ug/L0.33 SPLP13.1 B 8260B
Styrene 1.0 ug/L0.45 SPLP10.53 J 8260B
N-Nitrosodiphenylamine 0.95 ug/L0.30 ASTM Leach12.8 8270C
☼Silver 0.19 mg/Kg0.0013 Total/NA24.0 B 6020A
☼Aluminum 9.4 mg/Kg0.58 Total/NA220000 B 6020A
☼Arsenic 0.94 mg/Kg0.024 Total/NA220 B 6020A
☼Barium 0.94 mg/Kg0.21 Total/NA2660 6020A
☼Beryllium 0.19 mg/Kg0.010 Total/NA21.1 B 6020A
☼Cadmium 0.19 mg/Kg0.0035 Total/NA27.1 B 6020A
☼Cobalt 0.19 mg/Kg0.0016 Total/NA213 B 6020A
☼Chromium 0.38 mg/Kg0.056 Total/NA2440 B 6020A
☼Copper 0.38 mg/Kg0.091 Total/NA2350 B 6020A
☼Iron 190 mg/Kg30 Total/NA2062000 B 6020A
☼Manganese 0.94 mg/Kg0.11 Total/NA2540 B 6020A
☼Nickel 0.38 mg/Kg0.037 Total/NA280 B 6020A
☼Lead 0.19 mg/Kg0.042 Total/NA2310 B 6020A
☼Antimony 0.38 mg/Kg0.013 Total/NA22.4 6020A
☼Selenium 0.94 mg/Kg0.038 Total/NA24.2 B 6020A
☼Thallium 0.38 mg/Kg0.018 Total/NA20.63 6020A
☼Vanadium 0.94 mg/Kg0.035 Total/NA260 6020A
☼Zinc 3.8 mg/Kg0.47 Total/NA2870 B 6020A
☼Calcium 190 mg/Kg21 Total/NA257000 B 6020A
☼Potassium 190 mg/Kg4.6 Total/NA26300 B 6020A
☼Magnesium 190 mg/Kg3.8 Total/NA215000 B 6020A
☼Sodium 190 mg/Kg8.2 Total/NA21300 B 6020A
Aluminum 50 ug/L9.0 ASTM Leach14100 6020A
Arsenic 5.0 ug/L0.49 ASTM Leach11.6 J 6020A
Barium 5.0 ug/L1.1 ASTM Leach1140 6020A
Beryllium 1.0 ug/L0.053 ASTM Leach10.16 J 6020A
Cadmium 1.0 ug/L0.061 ASTM Leach10.24 J 6020A
Cobalt 1.0 ug/L0.021 ASTM Leach10.19 J B 6020A
Chromium 2.0 ug/L0.60 ASTM Leach11500 6020A
Lead 1.0 ug/L0.11 ASTM Leach10.70 J 6020A
Antimony 2.0 ug/L0.16 ASTM Leach12.4 6020A
Selenium 5.0 ug/L0.25 ASTM Leach117 B 6020A
Thallium 1.0 ug/L0.074 ASTM Leach10.19 J 6020A
Vanadium 5.0 ug/L0.23 ASTM Leach198 6020A
Calcium 1000 ug/L240 ASTM Leach1250000 6020A
Potassium 1000 ug/L30 ASTM Leach111000 6020A
Magnesium 1000 ug/L48 ASTM Leach1140 J 6020A
Sodium 1000 ug/L68 ASTM Leach14200 B 6020A
☼Cr (VI) 0.79 mg/Kg0.15 Total/NA120 B 7196A
Cr (VI) 0.020 mg/L0.0021 ASTM Leach10.28 7196A
TestAmerica Canton
This Detection Summary does not include radiochemical test results.
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS) - SPLPRL MDL
Acetone 5.1 J B 10 0.94 ug/L 06/08/16 20:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.35 ug/L 06/08/16 20:49 1Benzene ND
1.0 0.29 ug/L 06/08/16 20:49 1Dichlorobromomethane ND
1.0 0.56 ug/L 06/08/16 20:49 1Bromoform ND
1.0 0.44 ug/L 06/08/16 20:49 1Bromomethane ND
10 0.53 ug/L 06/08/16 20:49 12-Butanone (MEK) ND
1.0 0.38 ug/L 06/08/16 20:49 1Carbon disulfide ND
1.0 0.43 ug/L 06/08/16 20:49 1Carbon tetrachloride ND
1.0 0.25 ug/L 06/08/16 20:49 1Chlorobenzene ND
1.0 0.32 ug/L 06/08/16 20:49 1Chloroethane ND
1.0 0.25 ug/L 06/08/16 20:49 1Chloroform 1.1 B
1.0 0.44 ug/L 06/08/16 20:49 1Chloromethane ND
1.0 0.30 ug/L 06/08/16 20:49 11,1-Dichloroethane ND
1.0 0.23 ug/L 06/08/16 20:49 11,2-Dichloroethane ND
1.0 0.45 ug/L 06/08/16 20:49 11,1-Dichloroethene ND
1.0 0.25 ug/L 06/08/16 20:49 11,2-Dichloropropane ND
1.0 0.46 ug/L 06/08/16 20:49 1cis-1,3-Dichloropropene ND
1.0 0.56 ug/L 06/08/16 20:49 1trans-1,3-Dichloropropene ND
1.0 0.25 ug/L 06/08/16 20:49 1Ethylbenzene ND
10 0.48 ug/L 06/08/16 20:49 12-Hexanone ND
1.0 0.33 ug/L 06/08/16 20:49 1Methylene Chloride 3.1 B
10 0.99 ug/L 06/08/16 20:49 14-Methyl-2-pentanone (MIBK) ND
1.0 0.45 ug/L 06/08/16 20:49 1Styrene 0.53 J
1.0 0.22 ug/L 06/08/16 20:49 11,1,2,2-Tetrachloroethane ND
1.0 0.31 ug/L 06/08/16 20:49 1Tetrachloroethene ND
1.0 0.23 ug/L 06/08/16 20:49 1Toluene ND
1.0 0.22 ug/L 06/08/16 20:49 1Trichloroethene ND
1.0 0.29 ug/L 06/08/16 20:49 1Vinyl chloride ND
2.0 0.52 ug/L 06/08/16 20:49 1Xylenes, Total ND
1.0 0.44 ug/L 06/08/16 20:49 11,1,1-Trichloroethane ND *
1.0 0.24 ug/L 06/08/16 20:49 11,1,2-Trichloroethane ND
1.0 0.45 ug/L 06/08/16 20:49 1Cyclohexane ND
2.0 0.82 ug/L 06/08/16 20:49 11,2-Dibromo-3-Chloropropane ND
1.0 0.32 ug/L 06/08/16 20:49 1Ethylene Dibromide ND
1.0 0.32 ug/L 06/08/16 20:49 1Dichlorodifluoromethane ND
1.0 0.26 ug/L 06/08/16 20:49 1cis-1,2-Dichloroethene ND
1.0 0.30 ug/L 06/08/16 20:49 1trans-1,2-Dichloroethene ND
1.0 0.35 ug/L 06/08/16 20:49 1Isopropylbenzene ND
10 2.3 ug/L 06/08/16 20:49 1Methyl acetate ND
1.0 0.20 ug/L 06/08/16 20:49 1Methyl tert-butyl ether ND
1.0 0.45 ug/L 06/08/16 20:49 11,1,2-Trichloro-1,2,2-trifluoroethane ND
1.0 0.32 ug/L 06/08/16 20:49 11,2,4-Trichlorobenzene ND
1.0 0.25 ug/L 06/08/16 20:49 11,2-Dichlorobenzene ND
1.0 0.19 ug/L 06/08/16 20:49 11,3-Dichlorobenzene ND
1.0 0.27 ug/L 06/08/16 20:49 11,4-Dichlorobenzene ND
1.0 0.49 ug/L 06/08/16 20:49 1Trichlorofluoromethane ND
1.0 0.43 ug/L 06/08/16 20:49 1Chlorodibromomethane ND
1.0 0.43 ug/L 06/08/16 20:49 1Methylcyclohexane ND
TestAmerica Canton
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
1,2-Dichloroethane-d4 (Surr) 97 78 - 125 06/08/16 20:49 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 86 06/08/16 20:49 161 - 120
Toluene-d8 (Surr) 94 06/08/16 20:49 180 - 120
Dibromofluoromethane (Surr) 87 06/08/16 20:49 179 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM LeachRL MDL
Acenaphthene ND 0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.19 0.046 ug/L 06/09/16 07:34 06/09/16 21:17 1Acenaphthylene ND
0.95 0.32 ug/L 06/09/16 07:34 06/09/16 21:17 1Acetophenone ND
0.19 0.084 ug/L 06/09/16 07:34 06/09/16 21:17 1Anthracene ND
0.95 0.32 ug/L 06/09/16 07:34 06/09/16 21:17 1Atrazine ND
0.95 0.37 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzaldehyde ND
0.19 0.028 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[a]anthracene ND
0.19 0.038 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[b]fluoranthene ND
0.19 0.043 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[k]fluoranthene ND
0.19 0.044 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[g,h,i]perylene ND
0.19 0.049 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[a]pyrene ND
1.9 0.25 ug/L 06/09/16 07:34 06/09/16 21:17 1Butyl benzyl phthalate ND
0.95 0.12 ug/L 06/09/16 07:34 06/09/16 21:17 11,1'-Biphenyl ND
0.95 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-chloroethoxy)methane ND
0.95 0.095 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-chloroethyl)ether ND
4.8 1.6 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-ethylhexyl) phthalate ND
1.9 0.21 ug/L 06/09/16 07:34 06/09/16 21:17 14-Bromophenyl phenyl ether ND
4.8 0.19 ug/L 06/09/16 07:34 06/09/16 21:17 1Caprolactam ND *
0.95 0.27 ug/L 06/09/16 07:34 06/09/16 21:17 1Carbazole ND
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chloroaniline ND
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chloro-3-methylphenol ND
0.95 0.095 ug/L 06/09/16 07:34 06/09/16 21:17 12-Chloronaphthalene ND
0.95 0.28 ug/L 06/09/16 07:34 06/09/16 21:17 12-Chlorophenol ND
1.9 0.29 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chlorophenyl phenyl ether ND
0.19 0.048 ug/L 06/09/16 07:34 06/09/16 21:17 1Chrysene ND
0.19 0.086 ug/L 06/09/16 07:34 06/09/16 21:17 12-Methylnaphthalene ND
1.9 0.76 ug/L 06/09/16 07:34 06/09/16 21:17 13 & 4 Methylphenol ND
0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1Dibenz(a,h)anthracene ND
0.95 0.019 ug/L 06/09/16 07:34 06/09/16 21:17 1Dibenzofuran ND
4.8 0.35 ug/L 06/09/16 07:34 06/09/16 21:17 13,3'-Dichlorobenzidine ND
1.9 0.18 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dichlorophenol ND
1.9 0.57 ug/L 06/09/16 07:34 06/09/16 21:17 1Diethyl phthalate ND
1.9 0.24 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dimethylphenol ND
1.9 0.28 ug/L 06/09/16 07:34 06/09/16 21:17 1Dimethyl phthalate ND
4.8 2.3 ug/L 06/09/16 07:34 06/09/16 21:17 14,6-Dinitro-2-methylphenol ND
4.8 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dinitrophenol ND
4.8 0.24 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dinitrotoluene ND
4.8 1.6 ug/L 06/09/16 07:34 06/09/16 21:17 1Di-n-butyl phthalate ND
1.9 0.22 ug/L 06/09/16 07:34 06/09/16 21:17 1Di-n-octyl phthalate ND
0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1Fluoranthene ND
0.19 0.039 ug/L 06/09/16 07:34 06/09/16 21:17 1Fluorene ND
0.19 0.081 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachlorobenzene ND
0.95 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachlorobutadiene ND
TestAmerica Canton
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach (Continued)RL MDL
Hexachlorocyclopentadiene ND 9.5 0.23 ug/L 06/09/16 07:34 06/09/16 21:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.95 0.18 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachloroethane ND
0.19 0.041 ug/L 06/09/16 07:34 06/09/16 21:17 1Indeno[1,2,3-cd]pyrene ND
0.95 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Isophorone ND
0.95 0.16 ug/L 06/09/16 07:34 06/09/16 21:17 12-Methylphenol ND
0.19 0.060 ug/L 06/09/16 07:34 06/09/16 21:17 1Naphthalene ND
1.9 0.20 ug/L 06/09/16 07:34 06/09/16 21:17 12-Nitroaniline ND
1.9 0.27 ug/L 06/09/16 07:34 06/09/16 21:17 13-Nitroaniline ND
1.9 0.21 ug/L 06/09/16 07:34 06/09/16 21:17 14-Nitroaniline ND
0.95 0.038 ug/L 06/09/16 07:34 06/09/16 21:17 1Nitrobenzene ND
1.9 0.27 ug/L 06/09/16 07:34 06/09/16 21:17 12-Nitrophenol ND
4.8 0.28 ug/L 06/09/16 07:34 06/09/16 21:17 14-Nitrophenol ND
0.95 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 1N-Nitrosodiphenylamine 2.8
0.95 0.23 ug/L 06/09/16 07:34 06/09/16 21:17 1N-Nitrosodi-n-propylamine ND
0.95 0.38 ug/L 06/09/16 07:34 06/09/16 21:17 1bis (2-chloroisopropyl) ether ND
4.8 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Pentachlorophenol ND
0.19 0.059 ug/L 06/09/16 07:34 06/09/16 21:17 1Phenanthrene ND
0.95 0.57 ug/L 06/09/16 07:34 06/09/16 21:17 1Phenol ND
0.19 0.040 ug/L 06/09/16 07:34 06/09/16 21:17 1Pyrene ND
4.8 0.29 ug/L 06/09/16 07:34 06/09/16 21:17 12,4,5-Trichlorophenol ND
4.8 0.23 ug/L 06/09/16 07:34 06/09/16 21:17 12,4,6-Trichlorophenol ND
4.8 0.76 ug/L 06/09/16 07:34 06/09/16 21:17 12,6-Dinitrotoluene ND
2-Fluorobiphenyl (Surr) 86 42 - 120 06/09/16 07:34 06/09/16 21:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 34 06/09/16 07:34 06/09/16 21:17 110 - 120
2,4,6-Tribromophenol (Surr) 78 06/09/16 07:34 06/09/16 21:17 135 - 125
Nitrobenzene-d5 (Surr) 82 06/09/16 07:34 06/09/16 21:17 136 - 120
Phenol-d5 (Surr) 19 06/09/16 07:34 06/09/16 21:17 110 - 120
Terphenyl-d14 (Surr) 89 06/09/16 07:34 06/09/16 21:17 117 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach - RERL MDL
Caprolactam ND * 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 10:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
2-Fluorobiphenyl (Surr) 74 42 - 120 06/13/16 11:40 06/14/16 10:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 41 06/13/16 11:40 06/14/16 10:13 110 - 120
2,4,6-Tribromophenol (Surr) 82 06/13/16 11:40 06/14/16 10:13 135 - 125
Nitrobenzene-d5 (Surr) 80 06/13/16 11:40 06/14/16 10:13 136 - 120
Phenol-d5 (Surr) 24 06/13/16 11:40 06/14/16 10:13 110 - 120
Terphenyl-d14 (Surr) 65 06/13/16 11:40 06/14/16 10:13 117 - 120
Method: 8081B - Organochlorine Pesticides (GC) - ASTM LeachRL MDL
4,4'-DDD ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.011 ug/L 06/09/16 06:31 06/13/16 15:28 14,4'-DDE ND
0.048 0.016 ug/L 06/09/16 06:31 06/13/16 15:28 14,4'-DDT ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Aldrin ND
0.048 0.013 ug/L 06/09/16 06:31 06/13/16 15:28 1alpha-BHC ND
TestAmerica Canton
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
Method: 8081B - Organochlorine Pesticides (GC) - ASTM Leach (Continued)RL MDL
beta-BHC ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.048 0.011 ug/L 06/09/16 06:31 06/13/16 15:28 1alpha-Chlordane ND
0.048 0.028 ug/L 06/09/16 06:31 06/13/16 15:28 1delta-BHC ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1gamma-BHC (Lindane) ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1gamma-Chlordane ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Dieldrin ND
0.048 0.015 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan I ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan II ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan sulfate ND
0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin ND
0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin aldehyde ND
0.048 0.015 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin ketone ND
0.048 0.013 ug/L 06/09/16 06:31 06/13/16 15:28 1Heptachlor ND
0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Heptachlor epoxide ND
0.095 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Methoxychlor ND
1.9 0.19 ug/L 06/09/16 06:31 06/13/16 15:28 1Toxaphene ND
DCB Decachlorobiphenyl 33 30 - 128 06/09/16 06:31 06/13/16 15:28 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 31 06/09/16 06:31 06/13/16 15:28 130 - 128
Tetrachloro-m-xylene 85 06/09/16 06:31 06/13/16 15:28 136 - 124
Tetrachloro-m-xylene 81 06/09/16 06:31 06/13/16 15:28 136 - 124
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography - ASTM LeachRL MDL
Aroclor-1016 ND 0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.095 0.086 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1221 ND
0.095 0.067 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1232 ND
0.095 0.057 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1242 ND
0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1248 ND
0.095 0.029 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1254 ND
0.095 0.038 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1260 ND
Tetrachloro-m-xylene 60 21 - 120 06/09/16 06:29 06/13/16 09:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 16 06/09/16 06:29 06/13/16 09:58 110 - 120
Method: 6020A - Metals (ICP/MS) - ASTM LeachRL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
50 9.0 ug/L 06/08/16 13:00 06/09/16 13:48 1Aluminum 4100
5.0 0.49 ug/L 06/08/16 13:00 06/09/16 13:48 1Arsenic 1.6 J
5.0 1.1 ug/L 06/08/16 13:00 06/09/16 13:48 1Barium 140
1.0 0.053 ug/L 06/08/16 13:00 06/09/16 13:48 1Beryllium 0.16 J
1.0 0.061 ug/L 06/08/16 13:00 06/09/16 13:48 1Cadmium 0.24 J
1.0 0.021 ug/L 06/08/16 13:00 06/09/16 13:48 1Cobalt 0.19 J B
2.0 0.60 ug/L 06/08/16 13:00 06/09/16 13:48 1Chromium 1500
2.0 0.75 ug/L 06/08/16 13:00 06/09/16 13:48 1Copper ND
100 16 ug/L 06/08/16 13:00 06/09/16 13:48 1Iron ND
5.0 1.1 ug/L 06/08/16 13:00 06/09/16 13:48 1Manganese ND
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
Method: 6020A - Metals (ICP/MS) - ASTM Leach (Continued)RL MDL
Nickel ND 2.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.0 0.11 ug/L 06/08/16 13:00 06/09/16 13:48 1Lead 0.70 J
2.0 0.16 ug/L 06/08/16 13:00 06/09/16 13:48 1Antimony 2.4
5.0 0.25 ug/L 06/08/16 13:00 06/09/16 13:48 1Selenium 17 B
1.0 0.074 ug/L 06/08/16 13:00 06/09/16 13:48 1Thallium 0.19 J
5.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:48 1Vanadium 98
20 7.3 ug/L 06/08/16 13:00 06/09/16 13:48 1Zinc ND
1000 240 ug/L 06/08/16 13:00 06/09/16 13:48 1Calcium 250000
1000 30 ug/L 06/08/16 13:00 06/09/16 13:48 1Potassium 11000
1000 48 ug/L 06/08/16 13:00 06/09/16 13:48 1Magnesium 140 J
1000 68 ug/L 06/08/16 13:00 06/09/16 13:48 1Sodium 4200 B
Method: 7470A - Mercury (CVAA) - ASTM LeachRL MDL
Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
Percent Solids 99.7 0.1 0.1 % 06/02/16 10:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.1 0.1 % 06/02/16 10:25 1Percent Moisture 0.3
General Chemistry - ASTM LeachRL MDL
Cr (VI) 0.28 0.020 0.0021 mg/L 06/08/16 13:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL
Acetone 7.8 J B 19 5.3 ug/Kg ☼ 06/03/16 10:36 06/03/16 19:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4.7 0.84 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Benzene ND
4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Dichlorobromomethane ND
4.7 0.23 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Bromoform ND
4.7 0.39 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Bromomethane ND
19 1.1 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼2-Butanone (MEK) ND
4.7 0.55 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Carbon disulfide ND
4.7 0.61 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Carbon tetrachloride ND
4.7 0.50 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chlorobenzene ND
4.7 0.41 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloroethane ND
4.7 0.34 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloroform ND
4.7 0.74 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloromethane ND
4.7 0.32 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1-Dichloroethane ND
4.7 0.43 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dichloroethane ND
4.7 0.75 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1-Dichloroethene ND
4.7 0.13 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dichloropropane ND
4.7 0.67 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼cis-1,3-Dichloropropene ND
4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼trans-1,3-Dichloropropene ND
4.7 0.30 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Ethylbenzene ND
19 0.64 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼2-Hexanone ND
4.7 0.69 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methylene Chloride ND
19 1.1 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼4-Methyl-2-pentanone (MIBK) ND
4.7 0.38 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Styrene 1.1 J
4.7 0.29 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,2,2-Tetrachloroethane ND
4.7 0.75 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Tetrachloroethene ND
4.7 0.25 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Toluene 0.34 J
4.7 0.36 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Trichloroethene ND
4.7 0.28 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Vinyl chloride ND
9.4 0.51 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Xylenes, Total ND
4.7 0.61 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,1-Trichloroethane ND
4.7 0.35 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,2-Trichloroethane ND
9.4 0.45 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Cyclohexane ND
9.4 2.5 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dibromo-3-Chloropropane ND
4.7 0.50 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Ethylene Dibromide ND
4.7 0.26 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Dichlorodifluoromethane ND
4.7 0.26 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼cis-1,2-Dichloroethene ND
4.7 0.30 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼trans-1,2-Dichloroethene ND
4.7 0.19 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Isopropylbenzene ND
9.4 1.9 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methyl acetate ND
4.7 0.40 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methyl tert-butyl ether ND
4.7 0.39 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND
4.7 0.36 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2,4-Trichlorobenzene ND
4.7 0.32 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dichlorobenzene ND
4.7 0.65 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,3-Dichlorobenzene ND
4.7 0.26 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,4-Dichlorobenzene ND
4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Trichlorofluoromethane ND
4.7 0.35 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chlorodibromomethane ND
9.4 0.54 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methylcyclohexane ND
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
1,2-Dichloroethane-d4 (Surr) 97 58 - 123 06/03/16 10:36 06/03/16 19:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 98 06/03/16 10:36 06/03/16 19:07 152 - 136
Toluene-d8 (Surr) 101 06/03/16 10:36 06/03/16 19:07 167 - 125
Dibromofluoromethane (Surr) 79 06/03/16 10:36 06/03/16 19:07 137 - 132
Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL
bis (2-chloroisopropyl) ether ND 400 38 ug/Kg ☼ 06/03/16 08:23 06/08/16 21:44 4
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
610 100 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4,5-Trichlorophenol ND
610 36 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4,6-Trichlorophenol ND
610 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dichlorophenol ND
610 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dimethylphenol ND
1300 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dinitrophenol ND
810 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dinitrotoluene ND
810 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,6-Dinitrotoluene ND
200 1.8 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Chloronaphthalene ND
200 33 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Chlorophenol ND
27 2.0 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Methylnaphthalene ND
810 44 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Methylphenol ND
810 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Nitroaniline ND
200 34 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Nitrophenol ND
400 73 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼3,3'-Dichlorobenzidine ND
810 65 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼3-Nitroaniline ND
610 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4,6-Dinitro-2-methylphenol ND
200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Bromophenyl phenyl ether ND
610 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chloro-3-methylphenol ND
610 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chloroaniline ND
200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chlorophenyl phenyl ether ND
810 110 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Nitroaniline ND
1300 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Nitrophenol ND
27 3.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acenaphthene ND
27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acenaphthylene ND
400 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acetophenone ND
27 3.2 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Anthracene ND
810 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Atrazine ND
27 2.5 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[a]anthracene ND
27 2.6 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[a]pyrene ND
27 2.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[b]fluoranthene ND
27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[g,h,i]perylene ND
27 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[k]fluoranthene ND
400 89 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-chloroethoxy)methane ND
400 8.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-chloroethyl)ether ND
280 77 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-ethylhexyl) phthalate ND
280 40 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Butyl benzyl phthalate ND
27 4.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Chrysene ND
27 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dibenz(a,h)anthracene ND
200 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dibenzofuran ND
280 65 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Diethyl phthalate ND
280 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dimethyl phthalate ND
280 61 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Di-n-butyl phthalate ND
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL
Di-n-octyl phthalate ND 280 32 ug/Kg ☼ 06/03/16 08:23 06/08/16 21:44 4
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
27 2.2 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Fluoranthene ND
27 2.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Fluorene ND
27 8.5 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorobenzene ND
200 23 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorobutadiene ND
1300 33 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorocyclopentadiene ND
200 36 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachloroethane ND
27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Indeno[1,2,3-cd]pyrene ND
200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Isophorone ND
27 3.3 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Naphthalene ND
400 8.9 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Nitrobenzene ND
200 25 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼N-Nitrosodi-n-propylamine ND
200 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼N-Nitrosodiphenylamine ND *
610 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Pentachlorophenol ND
200 30 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Phenol ND
27 3.0 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Phenanthrene ND
27 1.8 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Pyrene ND
1600 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼3 & 4 Methylphenol ND
2-Fluorobiphenyl (Surr) 60 39 - 120 06/03/16 08:23 06/08/16 21:44 4
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr) 44 06/03/16 08:23 06/08/16 21:44 433 - 120
2,4,6-Tribromophenol (Surr) 31 06/03/16 08:23 06/08/16 21:44 410 - 120
Nitrobenzene-d5 (Surr) 61 06/03/16 08:23 06/08/16 21:44 432 - 120
Phenol-d5 (Surr) 47 06/03/16 08:23 06/08/16 21:44 432 - 120
Terphenyl-d14 (Surr) 78 06/03/16 08:23 06/08/16 21:44 447 - 120
Method: 8081B - Organochlorine Pesticides (GC)RL MDL
4,4'-DDD ND 1.7 0.20 ug/Kg ☼ 06/03/16 07:28 06/10/16 16:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.7 0.28 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼4,4'-DDE ND
1.7 0.32 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼4,4'-DDT ND
1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Aldrin ND
1.7 0.61 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼alpha-BHC ND
1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼alpha-Chlordane ND
1.7 0.37 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼beta-BHC ND
1.7 0.22 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼delta-BHC ND
1.7 0.16 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Dieldrin ND
1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan I ND
1.7 0.39 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan II ND
1.7 0.35 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan sulfate ND
1.7 0.21 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin ND
1.7 0.33 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin aldehyde ND
1.7 0.43 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin ketone ND
1.7 0.47 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼gamma-BHC (Lindane) ND
1.7 0.88 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼gamma-Chlordane ND
1.7 0.71 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Heptachlor ND
1.7 0.41 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Heptachlor epoxide ND
68 10 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Toxaphene ND
3.4 0.55 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Methoxychlor ND
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Client Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
DCB Decachlorobiphenyl 87 42 - 138 06/03/16 07:28 06/10/16 16:27 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 80 06/03/16 07:28 06/10/16 16:27 142 - 138
Tetrachloro-m-xylene 87 06/03/16 07:28 06/10/16 16:27 131 - 159
Tetrachloro-m-xylene 77 06/03/16 07:28 06/10/16 16:27 131 - 159
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL
Aroclor-1016 ND 34 12 ug/Kg ☼ 06/03/16 07:23 06/06/16 14:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
34 16 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1221 ND
34 20 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1232 ND
34 11 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1242 ND
34 8.2 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1248 ND
34 14 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1254 ND
34 9.2 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1260 ND
Tetrachloro-m-xylene 76 14 - 128 06/03/16 07:23 06/06/16 14:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
DCB Decachlorobiphenyl 75 06/03/16 07:23 06/06/16 14:47 110 - 132
Method: 6020A - Metals (ICP/MS)RL MDL
Silver 4.0 B 0.19 0.0013 mg/Kg ☼ 06/02/16 11:09 06/03/16 21:58 2
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
9.4 0.58 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Aluminum 20000 B
0.94 0.024 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Arsenic 20 B
0.94 0.21 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Barium 660
0.19 0.010 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Beryllium 1.1 B
0.19 0.0035 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Cadmium 7.1 B
0.19 0.0016 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Cobalt 13 B
0.38 0.056 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Chromium 440 B
0.38 0.091 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Copper 350 B
190 30 mg/Kg 06/02/16 11:09 06/06/16 14:34 20☼Iron 62000 B
0.94 0.11 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Manganese 540 B
0.38 0.037 mg/Kg 06/02/16 11:09 06/06/16 14:30 2☼Nickel 80 B
0.19 0.042 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Lead 310 B
0.38 0.013 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Antimony 2.4
0.94 0.038 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Selenium 4.2 B
0.38 0.018 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Thallium 0.63
0.94 0.035 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Vanadium 60
3.8 0.47 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Zinc 870 B
190 21 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Calcium 57000 B
190 4.6 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Potassium 6300 B
190 3.8 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Magnesium 15000 B
190 8.2 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Sodium 1300 B
Method: 7471A - Mercury (CVAA)RL MDL
Mercury ND 0.11 0.016 mg/Kg ☼ 06/02/16 15:00 06/03/16 07:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General ChemistryRL MDL
Cr (VI) 20 B 0.79 0.15 mg/Kg ☼ 06/09/16 09:04 06/09/16 13:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Surrogate SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (58-123) (52-136) (67-125) (37-132)
12DCE BFB TOL DBFM
97 98 101 79240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
90 94 103 96LCS 240-233030/5 Lab Control Sample
91 93 101 96MB 240-233030/6 Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (78-125) (61-120) (80-120) (79-120)
12DCE BFB TOL DBFM
96 88 93 103LCS 240-233711/6
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: SPLPMatrix: Solid
Lab Sample ID Client Sample ID (78-125) (61-120) (80-120) (79-120)
12DCE BFB TOL DBFM
97 86 94 87240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
101 84 89 102LB 240-233606/1-A MB Method Blank
Surrogate Legend
12DCE = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
TOL = Toluene-d8 (Surr)
DBFM = Dibromofluoromethane (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (39-120) (33-120) (10-120) (32-120) (32-120) (47-120)
FBP 2FP TBP NBZ PHL TPH
60 44 31 61 47 78240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
94 82 75 8384 113LCS 240-233013/18-A Lab Control Sample
92 77 59 7991 103MB 240-233013/17-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
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Surrogate SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (42-120) (10-120) (35-125) (36-120) (10-120) (17-120)
FBP 2FP TBP NBZ PHL TPH
87 41 87 94 24 78LCS 240-233761/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
72 30 101 1981 31LCS 240-234253/4-A Lab Control Sample
74 39 68 2473 76MB 240-233761/4-A Method Blank
80 37 96 2284 82MB 240-234253/3-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (42-120) (10-120) (35-125) (36-120) (10-120) (17-120)
FBP 2FP TBP NBZ PHL TPH
86 34 78 82 19 89240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
74 41 82 2480 65240-65486-1 - RE WESTERLY WWTC-ASH
(WWWTC)
Surrogate Legend
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TBP = 2,4,6-Tribromophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPH = Terphenyl-d14 (Surr)
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-128) (30-128) (36-124) (36-124)
DCB1 DCB2 TCX1 TCX2
66 56 90 83LCS 240-233753/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
48 48 90 85MB 240-233753/4-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
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Surrogate SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (42-138) (42-138) (31-159) (31-159)
DCB1 DCB2 TCX1 TCX2
87 80 87 77240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
84 90 93 88240-65486-1 MS WESTERLY WWTC-ASH
(WWWTC)81 81 84 76240-65486-1 MSD WESTERLY WWTC-ASH
(WWWTC)79 74 70 60LCS 240-233006/6-A Lab Control Sample
81 85 77 64MB 240-233006/5-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081B - Organochlorine Pesticides (GC)Prep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (30-128) (30-128) (36-124) (36-124)
DCB1 DCB2 TCX1 TCX2
33 31 85 81240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
Surrogate Legend
DCB = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (14-128) (10-132)
TCX2 DCB2
76 75240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
66 80LCS 240-233005/13-A Lab Control Sample
64 79MB 240-233005/12-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (21-120) (10-120)
TCX2 DCB2
60 36LCS 240-233752/5-A
Percent Surrogate Recovery (Acceptance Limits)
Lab Control Sample
59 33MB 240-233752/4-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
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Surrogate SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: ASTM LeachMatrix: Solid
Lab Sample ID Client Sample ID (21-120) (10-120)
TCX2 DCB2
60 16240-65486-1
Percent Surrogate Recovery (Acceptance Limits)
WESTERLY WWTC-ASH (WWWTC)
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-233030/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
RL MDL
Acetone 7.04 J 20 5.7 ug/Kg 06/03/16 11:24 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.905.0 ug/Kg 06/03/16 11:24 1Benzene
ND 0.295.0 ug/Kg 06/03/16 11:24 1Dichlorobromomethane
ND 0.245.0 ug/Kg 06/03/16 11:24 1Bromoform
ND 0.425.0 ug/Kg 06/03/16 11:24 1Bromomethane
1.22 J 1.120 ug/Kg 06/03/16 11:24 12-Butanone (MEK)
ND 0.595.0 ug/Kg 06/03/16 11:24 1Carbon disulfide
ND 0.655.0 ug/Kg 06/03/16 11:24 1Carbon tetrachloride
ND 0.535.0 ug/Kg 06/03/16 11:24 1Chlorobenzene
ND 0.445.0 ug/Kg 06/03/16 11:24 1Chloroethane
ND 0.365.0 ug/Kg 06/03/16 11:24 1Chloroform
ND 0.795.0 ug/Kg 06/03/16 11:24 1Chloromethane
ND 0.345.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethane
ND 0.465.0 ug/Kg 06/03/16 11:24 11,2-Dichloroethane
ND 0.805.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethene
ND 0.145.0 ug/Kg 06/03/16 11:24 11,2-Dichloropropane
ND 0.715.0 ug/Kg 06/03/16 11:24 1cis-1,3-Dichloropropene
ND 0.295.0 ug/Kg 06/03/16 11:24 1trans-1,3-Dichloropropene
ND 0.325.0 ug/Kg 06/03/16 11:24 1Ethylbenzene
ND 0.6820 ug/Kg 06/03/16 11:24 12-Hexanone
ND 0.745.0 ug/Kg 06/03/16 11:24 1Methylene Chloride
ND 1.220 ug/Kg 06/03/16 11:24 14-Methyl-2-pentanone (MIBK)
ND 0.405.0 ug/Kg 06/03/16 11:24 1Styrene
ND 0.315.0 ug/Kg 06/03/16 11:24 11,1,2,2-Tetrachloroethane
ND 0.805.0 ug/Kg 06/03/16 11:24 1Tetrachloroethene
ND 0.275.0 ug/Kg 06/03/16 11:24 1Toluene
ND 0.385.0 ug/Kg 06/03/16 11:24 1Trichloroethene
ND 0.305.0 ug/Kg 06/03/16 11:24 1Vinyl chloride
ND 0.5410 ug/Kg 06/03/16 11:24 1Xylenes, Total
ND 0.655.0 ug/Kg 06/03/16 11:24 11,1,1-Trichloroethane
ND 0.375.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloroethane
ND 0.4810 ug/Kg 06/03/16 11:24 1Cyclohexane
ND 2.710 ug/Kg 06/03/16 11:24 11,2-Dibromo-3-Chloropropane
ND 0.535.0 ug/Kg 06/03/16 11:24 1Ethylene Dibromide
ND 0.285.0 ug/Kg 06/03/16 11:24 1Dichlorodifluoromethane
ND 0.285.0 ug/Kg 06/03/16 11:24 1cis-1,2-Dichloroethene
ND 0.325.0 ug/Kg 06/03/16 11:24 1trans-1,2-Dichloroethene
ND 0.205.0 ug/Kg 06/03/16 11:24 1Isopropylbenzene
ND 2.010 ug/Kg 06/03/16 11:24 1Methyl acetate
ND 0.435.0 ug/Kg 06/03/16 11:24 1Methyl tert-butyl ether
ND 0.425.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.385.0 ug/Kg 06/03/16 11:24 11,2,4-Trichlorobenzene
ND 0.345.0 ug/Kg 06/03/16 11:24 11,2-Dichlorobenzene
ND 0.695.0 ug/Kg 06/03/16 11:24 11,3-Dichlorobenzene
ND 0.285.0 ug/Kg 06/03/16 11:24 11,4-Dichlorobenzene
ND 0.295.0 ug/Kg 06/03/16 11:24 1Trichlorofluoromethane
ND 0.375.0 ug/Kg 06/03/16 11:24 1Chlorodibromomethane
ND 0.5810 ug/Kg 06/03/16 11:24 1Methylcyclohexane
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
1,2-Dichloroethane-d4 (Surr) 91 58 - 123 06/03/16 11:24 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
93 06/03/16 11:24 14-Bromofluorobenzene (Surr) 52 - 136
101 06/03/16 11:24 1Toluene-d8 (Surr) 67 - 125
96 06/03/16 11:24 1Dibromofluoromethane (Surr) 37 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233030/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
Acetone 100 107 ug/Kg 107 41 - 137
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 51.6 ug/Kg 103 79 - 120
Dichlorobromomethane 50.0 54.1 ug/Kg 108 80 - 122
Bromoform 50.0 53.3 ug/Kg 107 62 - 133
Bromomethane 20.0 14.1 ug/Kg 71 42 - 136
2-Butanone (MEK) 100 110 ug/Kg 110 52 - 131
Carbon disulfide 50.0 60.8 ug/Kg 122 62 - 146
Carbon tetrachloride 50.0 51.9 ug/Kg 104 71 - 129
Chlorobenzene 50.0 51.0 ug/Kg 102 78 - 120
Chloroethane 20.0 16.9 ug/Kg 85 58 - 120
Chloroform 50.0 51.3 ug/Kg 103 77 - 120
Chloromethane 20.0 14.8 ug/Kg 74 50 - 120
1,1-Dichloroethane 50.0 50.1 ug/Kg 100 76 - 120
1,2-Dichloroethane 50.0 51.6 ug/Kg 103 72 - 120
1,1-Dichloroethene 50.0 53.9 ug/Kg 108 75 - 135
1,2-Dichloropropane 50.0 52.1 ug/Kg 104 80 - 120
cis-1,3-Dichloropropene 50.0 55.8 ug/Kg 112 74 - 128
trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 73 - 131
Ethylbenzene 50.0 52.7 ug/Kg 105 79 - 120
2-Hexanone 100 118 ug/Kg 118 64 - 136
Methylene Chloride 50.0 49.5 ug/Kg 99 75 - 120
4-Methyl-2-pentanone (MIBK) 100 123 ug/Kg 123 67 - 135
Styrene 50.0 54.1 ug/Kg 108 80 - 120
1,1,2,2-Tetrachloroethane 50.0 56.1 ug/Kg 112 77 - 123
Tetrachloroethene 50.0 53.0 ug/Kg 106 79 - 120
Toluene 50.0 50.9 ug/Kg 102 75 - 120
Trichloroethene 50.0 54.9 ug/Kg 110 79 - 120
Vinyl chloride 20.0 14.5 ug/Kg 73 57 - 120
Xylenes, Total 100 106 ug/Kg 106 80 - 120
1,1,1-Trichloroethane 50.0 52.3 ug/Kg 105 77 - 126
1,1,2-Trichloroethane 50.0 54.2 ug/Kg 108 80 - 120
Cyclohexane 50.0 52.1 ug/Kg 104 66 - 120
1,2-Dibromo-3-Chloropropane 50.0 57.9 ug/Kg 116 61 - 132
Ethylene Dibromide 50.0 57.6 ug/Kg 115 80 - 120
Dichlorodifluoromethane 20.0 9.78 ug/Kg 49 26 - 120
cis-1,2-Dichloroethene 50.0 52.2 ug/Kg 104 76 - 120
trans-1,2-Dichloroethene 50.0 55.2 ug/Kg 110 78 - 120
Isopropylbenzene 50.0 56.0 ug/Kg 112 76 - 122
Methyl acetate 250 300 ug/Kg 120 57 - 130
Methyl tert-butyl ether 50.0 50.5 ug/Kg 101 49 - 165
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
50.0 52.7 ug/Kg 105 80 - 138
1,2,4-Trichlorobenzene 50.0 49.4 ug/Kg 99 64 - 124
1,2-Dichlorobenzene 50.0 50.3 ug/Kg 101 76 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233030/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030
1,3-Dichlorobenzene 50.0 50.3 ug/Kg 101 78 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,4-Dichlorobenzene 50.0 49.3 ug/Kg 99 75 - 120
Trichlorofluoromethane 20.0 17.2 ug/Kg 86 57 - 146
Methylcyclohexane 50.0 51.2 ug/Kg 102 70 - 126
m-Xylene & p-Xylene 50.0 52.9 ug/Kg 106 80 - 120
o-Xylene 50.0 52.7 ug/Kg 105 80 - 120
1,2-Dichloroethane-d4 (Surr) 58 - 123
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
944-Bromofluorobenzene (Surr) 52 - 136
103Toluene-d8 (Surr) 67 - 125
96Dibromofluoromethane (Surr) 37 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233711/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233711
Acetone 40.0 35.6 ug/L 89 34 - 148
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 20.0 22.6 ug/L 113 80 - 120
Dichlorobromomethane 20.0 21.9 ug/L 109 80 - 120
Bromoform 20.0 24.3 ug/L 122 56 - 122
Bromomethane 20.0 23.5 ug/L 118 38 - 132
2-Butanone (MEK) 40.0 43.2 ug/L 108 56 - 138
Carbon disulfide 20.0 26.5 ug/L 132 65 - 144
Carbon tetrachloride 20.0 23.6 ug/L 118 77 - 131
Chlorobenzene 20.0 21.2 ug/L 106 80 - 120
Chloroethane 20.0 24.0 ug/L 120 36 - 126
Chloroform 20.0 23.0 ug/L 115 80 - 120
Chloromethane 20.0 23.8 ug/L 119 48 - 133
1,1-Dichloroethane 20.0 22.0 ug/L 110 79 - 125
1,2-Dichloroethane 20.0 22.3 ug/L 111 80 - 120
1,1-Dichloroethene 20.0 24.8 ug/L 124 76 - 124
1,2-Dichloropropane 20.0 22.3 ug/L 111 78 - 124
cis-1,3-Dichloropropene 20.0 23.4 ug/L 117 74 - 126
trans-1,3-Dichloropropene 20.0 18.4 ug/L 92 75 - 131
Ethylbenzene 20.0 19.9 ug/L 99 80 - 120
2-Hexanone 40.0 42.8 ug/L 107 55 - 141
Methylene Chloride 20.0 22.2 ug/L 111 77 - 129
4-Methyl-2-pentanone (MIBK) 40.0 44.2 ug/L 111 64 - 135
Styrene 20.0 20.6 ug/L 103 76 - 122
1,1,2,2-Tetrachloroethane 20.0 19.7 ug/L 99 71 - 123
Tetrachloroethene 20.0 20.9 ug/L 104 78 - 121
Toluene 20.0 22.4 ug/L 112 80 - 120
Trichloroethene 20.0 24.1 ug/L 121 80 - 121
Vinyl chloride 20.0 23.6 ug/L 118 52 - 121
Xylenes, Total 40.0 42.0 ug/L 105 80 - 120
1,1,1-Trichloroethane 20.0 25.6 * ug/L 128 77 - 123
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233711/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233711
1,1,2-Trichloroethane 20.0 21.9 ug/L 110 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Cyclohexane 20.0 21.0 ug/L 105 60 - 140
1,2-Dibromo-3-Chloropropane 20.0 22.6 ug/L 113 50 - 132
Ethylene Dibromide 20.0 22.2 ug/L 111 80 - 120
Dichlorodifluoromethane 20.0 23.1 ug/L 115 23 - 136
cis-1,2-Dichloroethene 20.0 22.1 ug/L 111 79 - 120
trans-1,2-Dichloroethene 20.0 22.8 ug/L 114 80 - 124
Isopropylbenzene 20.0 20.3 ug/L 102 77 - 120
Methyl acetate 100 113 ug/L 113 67 - 131
Methyl tert-butyl ether 20.0 23.0 ug/L 115 69 - 121
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
20.0 23.4 ug/L 117 67 - 138
1,2,4-Trichlorobenzene 20.0 20.1 ug/L 100 61 - 120
1,2-Dichlorobenzene 20.0 19.6 ug/L 98 79 - 120
1,3-Dichlorobenzene 20.0 19.7 ug/L 98 79 - 120
1,4-Dichlorobenzene 20.0 20.2 ug/L 101 79 - 120
Trichlorofluoromethane 20.0 21.8 ug/L 109 61 - 133
Methylcyclohexane 20.0 19.9 ug/L 100 61 - 134
m-Xylene & p-Xylene 20.0 21.4 ug/L 107 80 - 120
o-Xylene 20.0 20.6 ug/L 103 80 - 120
1,2-Dichloroethane-d4 (Surr) 78 - 125
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
884-Bromofluorobenzene (Surr) 61 - 120
93Toluene-d8 (Surr) 80 - 120
103Dibromofluoromethane (Surr) 79 - 120
Client Sample ID: Method BlankLab Sample ID: LB 240-233606/1-A MBMatrix: Solid Prep Type: SPLPAnalysis Batch: 233711
RL MDL
Acetone 1.76 J 10 0.94 ug/L 06/08/16 20:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.351.0 ug/L 06/08/16 20:01 1Benzene
ND 0.291.0 ug/L 06/08/16 20:01 1Dichlorobromomethane
ND 0.561.0 ug/L 06/08/16 20:01 1Bromoform
ND 0.441.0 ug/L 06/08/16 20:01 1Bromomethane
ND 0.5310 ug/L 06/08/16 20:01 12-Butanone (MEK)
ND 0.381.0 ug/L 06/08/16 20:01 1Carbon disulfide
ND 0.431.0 ug/L 06/08/16 20:01 1Carbon tetrachloride
ND 0.251.0 ug/L 06/08/16 20:01 1Chlorobenzene
ND 0.321.0 ug/L 06/08/16 20:01 1Chloroethane
1.24 0.251.0 ug/L 06/08/16 20:01 1Chloroform
ND 0.441.0 ug/L 06/08/16 20:01 1Chloromethane
ND 0.301.0 ug/L 06/08/16 20:01 11,1-Dichloroethane
ND 0.231.0 ug/L 06/08/16 20:01 11,2-Dichloroethane
ND 0.451.0 ug/L 06/08/16 20:01 11,1-Dichloroethene
ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichloropropane
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 240-233606/1-A MBMatrix: Solid Prep Type: SPLPAnalysis Batch: 233711
RL MDL
cis-1,3-Dichloropropene ND 1.0 0.46 ug/L 06/08/16 20:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.561.0 ug/L 06/08/16 20:01 1trans-1,3-Dichloropropene
ND 0.251.0 ug/L 06/08/16 20:01 1Ethylbenzene
ND 0.4810 ug/L 06/08/16 20:01 12-Hexanone
2.74 0.331.0 ug/L 06/08/16 20:01 1Methylene Chloride
ND 0.9910 ug/L 06/08/16 20:01 14-Methyl-2-pentanone (MIBK)
ND 0.451.0 ug/L 06/08/16 20:01 1Styrene
ND 0.221.0 ug/L 06/08/16 20:01 11,1,2,2-Tetrachloroethane
ND 0.311.0 ug/L 06/08/16 20:01 1Tetrachloroethene
ND 0.231.0 ug/L 06/08/16 20:01 1Toluene
ND 0.221.0 ug/L 06/08/16 20:01 1Trichloroethene
ND 0.291.0 ug/L 06/08/16 20:01 1Vinyl chloride
ND 0.522.0 ug/L 06/08/16 20:01 1Xylenes, Total
ND 0.441.0 ug/L 06/08/16 20:01 11,1,1-Trichloroethane
ND 0.241.0 ug/L 06/08/16 20:01 11,1,2-Trichloroethane
ND 0.451.0 ug/L 06/08/16 20:01 1Cyclohexane
ND 0.822.0 ug/L 06/08/16 20:01 11,2-Dibromo-3-Chloropropane
ND 0.321.0 ug/L 06/08/16 20:01 1Ethylene Dibromide
ND 0.321.0 ug/L 06/08/16 20:01 1Dichlorodifluoromethane
ND 0.261.0 ug/L 06/08/16 20:01 1cis-1,2-Dichloroethene
ND 0.301.0 ug/L 06/08/16 20:01 1trans-1,2-Dichloroethene
ND 0.351.0 ug/L 06/08/16 20:01 1Isopropylbenzene
ND 2.310 ug/L 06/08/16 20:01 1Methyl acetate
ND 0.201.0 ug/L 06/08/16 20:01 1Methyl tert-butyl ether
ND 0.451.0 ug/L 06/08/16 20:01 11,1,2-Trichloro-1,2,2-trifluoroethane
ND 0.321.0 ug/L 06/08/16 20:01 11,2,4-Trichlorobenzene
ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichlorobenzene
ND 0.191.0 ug/L 06/08/16 20:01 11,3-Dichlorobenzene
ND 0.271.0 ug/L 06/08/16 20:01 11,4-Dichlorobenzene
ND 0.491.0 ug/L 06/08/16 20:01 1Trichlorofluoromethane
ND 0.431.0 ug/L 06/08/16 20:01 1Chlorodibromomethane
ND 0.431.0 ug/L 06/08/16 20:01 1Methylcyclohexane
1,2-Dichloroethane-d4 (Surr) 101 78 - 125 06/08/16 20:01 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
84 06/08/16 20:01 14-Bromofluorobenzene (Surr) 61 - 120
89 06/08/16 20:01 1Toluene-d8 (Surr) 80 - 120
102 06/08/16 20:01 1Dibromofluoromethane (Surr) 79 - 120
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
2-Chloronaphthalene ND 50 0.45 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 8.250 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Chlorophenol
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
4-Bromophenyl phenyl ether ND 50 13 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 21150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloro-3-methylphenol
ND 0.506.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylnaphthalene
ND 17150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloroaniline
ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chlorophenyl phenyl ether
ND 18100 ug/Kg 06/03/16 08:23 06/07/16 10:25 13,3'-Dichlorobenzidine
ND 0.766.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthene
ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dichlorophenol
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthylene
ND 9.2100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acetophenone
ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dimethylphenol
ND 0.786.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Anthracene
ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Atrazine
ND 9.2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14,6-Dinitro-2-methylphenol
ND 0.636.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]anthracene
ND 21330 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrophenol
ND 0.646.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]pyrene
ND 17200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrotoluene
ND 0.596.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[b]fluoranthene
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[g,h,i]perylene
ND 0.686.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[k]fluoranthene
ND 22100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethoxy)methane
ND 2.0100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethyl)ether
ND 1970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-ethylhexyl) phthalate
ND 1070 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Butyl benzyl phthalate
ND 1.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Chrysene
ND 0.666.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenz(a,h)anthracene
ND 0.6650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenzofuran
ND 1670 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Diethyl phthalate
ND 11200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylphenol
ND 1770 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dimethyl phthalate
27.9 J 1570 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-butyl phthalate
ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitroaniline
ND 7.970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-octyl phthalate
ND 16200 ug/Kg 06/03/16 08:23 06/07/16 10:25 13-Nitroaniline
ND 0.556.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluoranthene
ND 26200 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitroaniline
ND 0.536.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluorene
ND 2.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobenzene
ND 8.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitrophenol
ND 5.650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobutadiene
ND 17330 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitrophenol
ND 8.1330 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorocyclopentadiene
ND 9.050 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachloroethane
ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Indeno[1,2,3-cd]pyrene
ND 9.5100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1bis (2-chloroisopropyl) ether
ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Isophorone
ND 0.826.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Naphthalene
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
RL MDL
Nitrobenzene ND 100 2.2 ug/Kg 06/03/16 08:23 06/07/16 10:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 6.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodi-n-propylamine
ND 2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodiphenylamine
ND 25150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,5-Trichlorophenol
ND 9.1150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pentachlorophenol
ND 8.9150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,6-Trichlorophenol
ND 7.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenol
ND 0.736.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenanthrene
ND 0.446.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pyrene
ND 20400 ug/Kg 06/03/16 08:23 06/07/16 10:25 13 & 4 Methylphenol
ND 21200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,6-Dinitrotoluene
2-Fluorobiphenyl (Surr) 92 39 - 120 06/07/16 10:25 1
MB MB
Surrogate
06/03/16 08:23
Dil FacPrepared AnalyzedQualifier Limits%Recovery
77 06/03/16 08:23 06/07/16 10:25 12-Fluorophenol (Surr) 33 - 120
59 06/03/16 08:23 06/07/16 10:25 12,4,6-Tribromophenol (Surr) 10 - 120
91 06/03/16 08:23 06/07/16 10:25 1Nitrobenzene-d5 (Surr) 32 - 120
79 06/03/16 08:23 06/07/16 10:25 1Phenol-d5 (Surr) 32 - 120
103 06/03/16 08:23 06/07/16 10:25 1Terphenyl-d14 (Surr) 47 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233013/18-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
2-Chloronaphthalene 667 612 ug/Kg 92 54 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Chlorophenol 667 624 ug/Kg 94 50 - 120
4-Bromophenyl phenyl ether 667 770 ug/Kg 116 48 - 120
4-Chloro-3-methylphenol 667 523 ug/Kg 78 52 - 120
2-Methylnaphthalene 667 644 ug/Kg 97 53 - 120
4-Chloroaniline 667 387 ug/Kg 58 41 - 120
4-Chlorophenyl phenyl ether 667 712 ug/Kg 107 56 - 120
3,3'-Dichlorobenzidine 1330 1000 ug/Kg 75 39 - 120
Acenaphthene 667 602 ug/Kg 90 55 - 120
2,4-Dichlorophenol 667 612 ug/Kg 92 51 - 120
Acenaphthylene 667 632 ug/Kg 95 54 - 120
Acetophenone 667 589 ug/Kg 88 49 - 120
2,4-Dimethylphenol 667 448 ug/Kg 67 34 - 120
Anthracene 667 620 ug/Kg 93 59 - 120
Atrazine 1330 1460 ug/Kg 110 56 - 120
4,6-Dinitro-2-methylphenol 1330 849 ug/Kg 64 23 - 120
Benzo[a]anthracene 667 648 ug/Kg 97 60 - 120
2,4-Dinitrophenol 1330 503 ug/Kg 38 10 - 120
Benzo[a]pyrene 667 745 ug/Kg 112 61 - 120
2,4-Dinitrotoluene 667 716 ug/Kg 107 57 - 120
Benzo[b]fluoranthene 667 736 ug/Kg 110 60 - 120
Benzo[g,h,i]perylene 667 686 ug/Kg 103 60 - 120
Benzo[k]fluoranthene 667 759 ug/Kg 114 61 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233013/18-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013
Bis(2-chloroethoxy)methane 667 569 ug/Kg 85 53 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Bis(2-chloroethyl)ether 667 548 ug/Kg 82 45 - 120
Bis(2-ethylhexyl) phthalate 667 665 ug/Kg 100 57 - 120
Butyl benzyl phthalate 667 653 ug/Kg 98 58 - 120
Chrysene 667 637 ug/Kg 96 62 - 120
Dibenz(a,h)anthracene 667 736 ug/Kg 110 59 - 120
Dibenzofuran 667 658 ug/Kg 99 57 - 120
Diethyl phthalate 667 665 ug/Kg 100 58 - 120
2-Methylphenol 667 617 ug/Kg 93 48 - 120
Dimethyl phthalate 667 708 ug/Kg 106 59 - 120
Di-n-butyl phthalate 667 669 ug/Kg 100 54 - 120
2-Nitroaniline 667 641 ug/Kg 96 50 - 120
Di-n-octyl phthalate 667 703 ug/Kg 105 54 - 120
3-Nitroaniline 667 574 ug/Kg 86 51 - 120
Fluoranthene 667 624 ug/Kg 94 57 - 120
4-Nitroaniline 667 552 ug/Kg 83 52 - 120
Fluorene 667 674 ug/Kg 101 56 - 120
Hexachlorobenzene 667 770 ug/Kg 115 43 - 120
2-Nitrophenol 667 609 ug/Kg 91 49 - 120
Hexachlorobutadiene 667 597 ug/Kg 90 48 - 120
4-Nitrophenol 1330 1230 ug/Kg 93 37 - 120
Hexachlorocyclopentadiene 667 352 ug/Kg 53 23 - 120
Hexachloroethane 667 576 ug/Kg 86 46 - 120
Indeno[1,2,3-cd]pyrene 667 710 ug/Kg 106 62 - 120
bis (2-chloroisopropyl) ether 667 556 ug/Kg 83 34 - 120
Isophorone 667 552 ug/Kg 83 54 - 120
Naphthalene 667 601 ug/Kg 90 53 - 120
Nitrobenzene 667 554 ug/Kg 83 50 - 120
N-Nitrosodi-n-propylamine 667 595 ug/Kg 89 49 - 120
N-Nitrosodiphenylamine 667 812 * ug/Kg 122 52 - 120
2,4,5-Trichlorophenol 667 566 ug/Kg 85 31 - 120
Pentachlorophenol 1330 676 ug/Kg 51 23 - 120
2,4,6-Trichlorophenol 667 471 ug/Kg 71 18 - 120
Phenol 667 567 ug/Kg 85 49 - 120
Phenanthrene 667 619 ug/Kg 93 58 - 120
Pyrene 667 639 ug/Kg 96 57 - 120
3 & 4 Methylphenol 667 594 ug/Kg 89 49 - 120
2,6-Dinitrotoluene 667 706 ug/Kg 106 61 - 120
2-Fluorobiphenyl (Surr) 39 - 120
Surrogate
94
LCS LCS
Qualifier Limits%Recovery
822-Fluorophenol (Surr) 33 - 120
752,4,6-Tribromophenol (Surr) 10 - 120
84Nitrobenzene-d5 (Surr) 32 - 120
83Phenol-d5 (Surr) 32 - 120
113Terphenyl-d14 (Surr) 47 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233761/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
RL MDL
Benzaldehyde ND 1.0 0.39 ug/L 06/09/16 07:34 06/10/16 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.131.0 ug/L 06/09/16 07:34 06/10/16 09:52 11,1'-Biphenyl
0.977 J 0.205.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Caprolactam
ND 0.281.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Carbazole
ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chloronaphthalene
ND 0.291.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chlorophenol
ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Bromophenyl phenyl ether
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloro-3-methylphenol
ND 0.0900.20 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylnaphthalene
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloroaniline
ND 0.302.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chlorophenyl phenyl ether
ND 0.375.0 ug/L 06/09/16 07:34 06/10/16 09:52 13,3'-Dichlorobenzidine
ND 0.0440.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthene
ND 0.192.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dichlorophenol
ND 0.0480.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthylene
ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Acetophenone
ND 0.252.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dimethylphenol
ND 0.0880.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Anthracene
ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Atrazine
ND 2.45.0 ug/L 06/09/16 07:34 06/10/16 09:52 14,6-Dinitro-2-methylphenol
ND 0.0300.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]anthracene
ND 0.325.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrophenol
ND 0.0510.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]pyrene
ND 0.255.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrotoluene
ND 0.0390.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[b]fluoranthene
ND 0.0460.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[g,h,i]perylene
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[k]fluoranthene
ND 0.321.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethoxy)methane
ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethyl)ether
ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-ethylhexyl) phthalate
ND 0.262.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Butyl benzyl phthalate
ND 0.0500.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Chrysene
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenz(a,h)anthracene
ND 0.0201.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenzofuran
ND 0.602.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Diethyl phthalate
ND 0.171.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylphenol
ND 0.292.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dimethyl phthalate
ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-butyl phthalate
ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitroaniline
ND 0.232.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-octyl phthalate
ND 0.282.0 ug/L 06/09/16 07:34 06/10/16 09:52 13-Nitroaniline
ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluoranthene
ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Nitroaniline
ND 0.0410.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluorene
ND 0.0850.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobenzene
ND 0.282.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitrophenol
ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobutadiene
ND 0.295.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Nitrophenol
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233761/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
RL MDL
Hexachlorocyclopentadiene ND 10 0.24 ug/L 06/09/16 07:34 06/10/16 09:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.191.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachloroethane
ND 0.0430.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Indeno[1,2,3-cd]pyrene
ND 0.401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1bis (2-chloroisopropyl) ether
ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Isophorone
ND 0.0630.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Naphthalene
ND 0.0401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene
ND 0.241.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodi-n-propylamine
ND 0.311.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodiphenylamine
ND 0.305.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4,5-Trichlorophenol
ND 0.275.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Pentachlorophenol
ND 0.245.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4,6-Trichlorophenol
ND 0.601.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenol
ND 0.0620.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenanthrene
ND 0.0420.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Pyrene
ND 0.802.0 ug/L 06/09/16 07:34 06/10/16 09:52 13 & 4 Methylphenol
ND 0.805.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,6-Dinitrotoluene
2-Fluorobiphenyl (Surr) 74 42 - 120 06/10/16 09:52 1
MB MB
Surrogate
06/09/16 07:34
Dil FacPrepared AnalyzedQualifier Limits%Recovery
39 06/09/16 07:34 06/10/16 09:52 12-Fluorophenol (Surr) 10 - 120
68 06/09/16 07:34 06/10/16 09:52 12,4,6-Tribromophenol (Surr) 35 - 125
73 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene-d5 (Surr) 36 - 120
24 06/09/16 07:34 06/10/16 09:52 1Phenol-d5 (Surr) 10 - 120
76 06/09/16 07:34 06/10/16 09:52 1Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
Benzaldehyde 40.0 37.0 ug/L 93 60 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,1'-Biphenyl 20.0 17.6 ug/L 88 58 - 120
Caprolactam 40.0 3.29 J * ug/L 8 10 - 120
Carbazole 20.0 20.0 ug/L 100 60 - 126
2-Chloronaphthalene 20.0 17.9 ug/L 89 56 - 120
2-Chlorophenol 20.0 15.9 ug/L 79 57 - 120
4-Bromophenyl phenyl ether 20.0 19.3 ug/L 97 52 - 128
4-Chloro-3-methylphenol 20.0 17.7 ug/L 89 59 - 120
2-Methylnaphthalene 20.0 18.0 ug/L 90 58 - 120
4-Chloroaniline 20.0 4.65 ug/L 23 10 - 120
4-Chlorophenyl phenyl ether 20.0 18.1 ug/L 91 58 - 120
3,3'-Dichlorobenzidine 40.0 31.8 ug/L 80 10 - 134
Acenaphthene 20.0 17.9 ug/L 89 57 - 120
2,4-Dichlorophenol 20.0 18.3 ug/L 92 57 - 120
Acenaphthylene 20.0 18.7 ug/L 94 55 - 120
Acetophenone 20.0 18.1 ug/L 90 60 - 120
2,4-Dimethylphenol 20.0 17.6 ug/L 88 55 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
Anthracene 20.0 19.9 ug/L 99 58 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Atrazine 40.0 39.5 ug/L 99 61 - 132
4,6-Dinitro-2-methylphenol 40.0 35.5 ug/L 89 35 - 140
Benzo[a]anthracene 20.0 17.1 ug/L 86 59 - 120
2,4-Dinitrophenol 40.0 30.0 ug/L 75 18 - 127
Benzo[a]pyrene 20.0 16.6 ug/L 83 60 - 120
2,4-Dinitrotoluene 20.0 18.7 ug/L 93 65 - 120
Benzo[b]fluoranthene 20.0 17.0 ug/L 85 62 - 120
Benzo[g,h,i]perylene 20.0 17.7 ug/L 88 59 - 120
Benzo[k]fluoranthene 20.0 18.1 ug/L 90 57 - 120
Bis(2-chloroethoxy)methane 20.0 18.7 ug/L 94 61 - 120
Bis(2-chloroethyl)ether 20.0 17.6 ug/L 88 55 - 120
Bis(2-ethylhexyl) phthalate 20.0 14.4 ug/L 72 62 - 123
Butyl benzyl phthalate 20.0 16.7 ug/L 83 61 - 120
Chrysene 20.0 16.9 ug/L 84 61 - 120
Dibenz(a,h)anthracene 20.0 14.8 ug/L 74 61 - 120
Dibenzofuran 20.0 18.1 ug/L 91 58 - 120
Diethyl phthalate 20.0 19.0 ug/L 95 62 - 120
2-Methylphenol 20.0 13.1 ug/L 65 52 - 120
Dimethyl phthalate 20.0 19.2 ug/L 96 62 - 120
Di-n-butyl phthalate 20.0 19.9 ug/L 99 59 - 128
2-Nitroaniline 20.0 20.1 ug/L 100 56 - 123
Di-n-octyl phthalate 20.0 13.7 ug/L 68 58 - 120
3-Nitroaniline 20.0 17.4 ug/L 87 36 - 120
Fluoranthene 20.0 19.5 ug/L 97 57 - 123
4-Nitroaniline 20.0 19.0 ug/L 95 51 - 122
Fluorene 20.0 18.9 ug/L 94 56 - 120
Hexachlorobenzene 20.0 18.5 ug/L 92 47 - 127
2-Nitrophenol 20.0 17.2 ug/L 86 62 - 120
Hexachlorobutadiene 20.0 17.0 ug/L 85 50 - 120
4-Nitrophenol 40.0 12.1 ug/L 30 16 - 120
Hexachlorocyclopentadiene 20.0 16.3 ug/L 82 25 - 120
Hexachloroethane 20.0 16.6 ug/L 83 50 - 120
Indeno[1,2,3-cd]pyrene 20.0 15.4 ug/L 77 61 - 120
bis (2-chloroisopropyl) ether 20.0 18.0 ug/L 90 46 - 120
Isophorone 20.0 18.9 ug/L 95 61 - 120
Naphthalene 20.0 17.4 ug/L 87 54 - 120
Nitrobenzene 20.0 18.8 ug/L 94 58 - 120
N-Nitrosodi-n-propylamine 20.0 18.3 ug/L 91 60 - 120
N-Nitrosodiphenylamine 20.0 19.2 ug/L 96 54 - 122
2,4,5-Trichlorophenol 20.0 19.2 ug/L 96 57 - 120
Pentachlorophenol 40.0 37.2 ug/L 93 35 - 121
2,4,6-Trichlorophenol 20.0 19.2 ug/L 96 60 - 120
Phenol 20.0 5.06 ug/L 25 16 - 120
Phenanthrene 20.0 18.5 ug/L 93 58 - 120
Pyrene 20.0 19.3 ug/L 97 60 - 120
3 & 4 Methylphenol 20.0 11.7 ug/L 58 46 - 120
2,6-Dinitrotoluene 20.0 19.8 ug/L 99 65 - 120
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233761/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233974 Prep Batch: 233761
2-Fluorobiphenyl (Surr) 42 - 120
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
412-Fluorophenol (Surr) 10 - 120
872,4,6-Tribromophenol (Surr) 35 - 125
94Nitrobenzene-d5 (Surr) 36 - 120
24Phenol-d5 (Surr) 10 - 120
78Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Method BlankLab Sample ID: MB 240-234253/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234362 Prep Batch: 234253
RL MDL
Caprolactam ND 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 08:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
2-Fluorobiphenyl (Surr) 80 42 - 120 06/14/16 08:11 1
MB MB
Surrogate
06/13/16 11:40
Dil FacPrepared AnalyzedQualifier Limits%Recovery
37 06/13/16 11:40 06/14/16 08:11 12-Fluorophenol (Surr) 10 - 120
96 06/13/16 11:40 06/14/16 08:11 12,4,6-Tribromophenol (Surr) 35 - 125
84 06/13/16 11:40 06/14/16 08:11 1Nitrobenzene-d5 (Surr) 36 - 120
22 06/13/16 11:40 06/14/16 08:11 1Phenol-d5 (Surr) 10 - 120
82 06/13/16 11:40 06/14/16 08:11 1Terphenyl-d14 (Surr) 17 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-234253/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234362 Prep Batch: 234253
Caprolactam 40.0 2.99 J * ug/L 7 10 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
2-Fluorobiphenyl (Surr) 42 - 120
Surrogate
72
LCS LCS
Qualifier Limits%Recovery
302-Fluorophenol (Surr) 10 - 120
1012,4,6-Tribromophenol (Surr) 35 - 125
81Nitrobenzene-d5 (Surr) 36 - 120
19Phenol-d5 (Surr) 10 - 120
31Terphenyl-d14 (Surr) 17 - 120
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 240-233006/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
RL MDL
4,4'-DDD ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.271.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDE
ND 0.311.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDT
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233006/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
RL MDL
Aldrin ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.601.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-BHC
ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-Chlordane
ND 0.361.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1beta-BHC
ND 0.221.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1delta-BHC
ND 0.161.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Dieldrin
ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan I
ND 0.381.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan II
ND 0.341.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan sulfate
ND 0.211.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin
ND 0.321.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin aldehyde
ND 0.421.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin ketone
ND 0.461.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-BHC (Lindane)
ND 0.861.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-Chlordane
ND 0.701.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor
ND 0.401.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor epoxide
ND 9.867 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Toxaphene
ND 0.543.3 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Methoxychlor
DCB Decachlorobiphenyl 81 42 - 138 06/10/16 17:39 1
MB MB
Surrogate
06/03/16 07:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
85 06/03/16 07:28 06/10/16 17:39 1DCB Decachlorobiphenyl 42 - 138
77 06/03/16 07:28 06/10/16 17:39 1Tetrachloro-m-xylene 31 - 159
64 06/03/16 07:28 06/10/16 17:39 1Tetrachloro-m-xylene 31 - 159
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233006/6-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
4,4'-DDD 33.3 26.5 ug/Kg 80 47 - 157
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4,4'-DDE 33.3 26.2 ug/Kg 79 56 - 125
4,4'-DDT 33.3 26.3 ug/Kg 79 57 - 142
Aldrin 33.3 23.5 ug/Kg 70 37 - 129
alpha-BHC 33.3 25.6 ug/Kg 77 50 - 125
alpha-Chlordane 33.3 24.8 ug/Kg 74 53 - 120
beta-BHC 33.3 24.7 ug/Kg 74 41 - 125
delta-BHC 33.3 21.6 ug/Kg 65 52 - 124
Dieldrin 33.3 25.9 ug/Kg 78 55 - 124
Endosulfan I 33.3 17.6 ug/Kg 53 18 - 120
Endosulfan II 33.3 20.8 ug/Kg 62 19 - 120
Endosulfan sulfate 33.3 24.6 ug/Kg 74 54 - 128
Endrin 33.3 27.5 ug/Kg 83 53 - 151
Endrin aldehyde 33.3 22.7 ug/Kg 68 44 - 130
Endrin ketone 33.3 24.3 ug/Kg 73 49 - 120
gamma-BHC (Lindane) 33.3 25.4 ug/Kg 76 50 - 123
gamma-Chlordane 33.3 25.2 ug/Kg 76 53 - 120
Heptachlor 33.3 27.0 ug/Kg 81 48 - 129
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233006/6-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
Heptachlor epoxide 33.3 25.4 ug/Kg 76 54 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Methoxychlor 33.3 25.7 ug/Kg 77 52 - 147
DCB Decachlorobiphenyl 42 - 138
Surrogate
79
LCS LCS
Qualifier Limits%Recovery
74DCB Decachlorobiphenyl 42 - 138
70Tetrachloro-m-xylene 31 - 159
60Tetrachloro-m-xylene 31 - 159
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
4,4'-DDD ND 33.8 29.5 ug/Kg 87 17 - 160☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4,4'-DDE ND 33.8 29.5 ug/Kg 87 26 - 136☼
4,4'-DDT ND 33.8 29.5 ug/Kg 88 22 - 151☼
Aldrin ND 33.8 26.6 ug/Kg 79 22 - 128☼
alpha-BHC ND 33.8 30.0 ug/Kg 89 21 - 141☼
alpha-Chlordane ND 33.8 27.9 ug/Kg 83 22 - 124☼
beta-BHC ND 33.8 29.9 ug/Kg 89 14 - 139☼
delta-BHC ND 33.8 24.5 ug/Kg 73 22 - 130☼
Dieldrin ND 33.8 29.2 ug/Kg 86 25 - 133☼
Endosulfan I ND 33.8 19.5 ug/Kg 58 10 - 120☼
Endosulfan II ND 33.8 23.2 ug/Kg 69 13 - 120☼
Endosulfan sulfate ND 33.8 27.6 ug/Kg 82 24 - 131☼
Endrin ND 33.8 31.3 ug/Kg 93 27 - 158☼
Endrin aldehyde ND 33.8 23.0 ug/Kg 68 22 - 119☼
Endrin ketone ND 33.8 27.1 ug/Kg 80 21 - 120☼
gamma-BHC (Lindane) ND 33.8 32.5 ug/Kg 96 21 - 134☼
gamma-Chlordane ND 33.8 28.7 ug/Kg 85 28 - 130☼
Heptachlor ND 33.8 31.1 ug/Kg 92 26 - 133☼
Heptachlor epoxide ND 33.8 28.8 ug/Kg 85 27 - 127☼
Methoxychlor ND 33.8 28.7 ug/Kg 85 24 - 150☼
DCB Decachlorobiphenyl 42 - 138
Surrogate
84
MS MS
Qualifier Limits%Recovery
90DCB Decachlorobiphenyl 42 - 138
93Tetrachloro-m-xylene 31 - 159
88Tetrachloro-m-xylene 31 - 159
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
4,4'-DDD ND 33.5 27.2 ug/Kg 81 17 - 160 8 40☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4,4'-DDE ND 33.5 26.8 ug/Kg 80 26 - 136 10 40☼
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006
4,4'-DDT ND 33.5 26.6 ug/Kg 79 22 - 151 11 40☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Aldrin ND 33.5 24.0 ug/Kg 72 22 - 128 11 40☼
alpha-BHC ND 33.5 26.7 ug/Kg 80 21 - 141 11 40☼
alpha-Chlordane ND 33.5 25.5 ug/Kg 76 22 - 124 9 40☼
beta-BHC ND 33.5 27.5 ug/Kg 82 14 - 139 8 40☼
delta-BHC ND 33.5 23.0 ug/Kg 69 22 - 130 7 40☼
Dieldrin ND 33.5 26.7 ug/Kg 80 25 - 133 9 40☼
Endosulfan I ND 33.5 18.2 ug/Kg 54 10 - 120 7 40☼
Endosulfan II ND 33.5 21.3 ug/Kg 64 13 - 120 8 40☼
Endosulfan sulfate ND 33.5 25.1 ug/Kg 75 24 - 131 9 40☼
Endrin ND 33.5 28.6 ug/Kg 85 27 - 158 9 40☼
Endrin aldehyde ND 33.5 21.4 ug/Kg 64 22 - 119 7 40☼
Endrin ketone ND 33.5 25.0 ug/Kg 75 21 - 120 8 40☼
gamma-BHC (Lindane) ND 33.5 28.4 ug/Kg 85 21 - 134 13 40☼
gamma-Chlordane ND 33.5 26.0 ug/Kg 78 28 - 130 10 40☼
Heptachlor ND 33.5 27.4 ug/Kg 82 26 - 133 13 40☼
Heptachlor epoxide ND 33.5 26.1 ug/Kg 78 27 - 127 10 40☼
Methoxychlor ND 33.5 26.0 ug/Kg 78 24 - 150 10 40☼
DCB Decachlorobiphenyl 42 - 138
Surrogate
81
MSD MSD
Qualifier Limits%Recovery
81DCB Decachlorobiphenyl 42 - 138
84Tetrachloro-m-xylene 31 - 159
76Tetrachloro-m-xylene 31 - 159
Client Sample ID: Method BlankLab Sample ID: MB 240-233753/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
RL MDL
4,4'-DDD ND 0.050 0.018 ug/L 06/09/16 06:31 06/13/16 13:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDE
ND 0.0170.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDT
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Aldrin
ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-BHC
ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-Chlordane
ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1beta-BHC
ND 0.0290.050 ug/L 06/09/16 06:31 06/13/16 13:51 1delta-BHC
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Dieldrin
ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan I
ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan II
ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan sulfate
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin
ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin aldehyde
ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin ketone
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-BHC (Lindane)
ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-Chlordane
ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233753/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
RL MDL
Heptachlor epoxide ND 0.050 0.015 ug/L 06/09/16 06:31 06/13/16 13:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.202.0 ug/L 06/09/16 06:31 06/13/16 13:51 1Toxaphene
ND 0.0130.10 ug/L 06/09/16 06:31 06/13/16 13:51 1Methoxychlor
DCB Decachlorobiphenyl 48 30 - 128 06/13/16 13:51 1
MB MB
Surrogate
06/09/16 06:31
Dil FacPrepared AnalyzedQualifier Limits%Recovery
48 06/09/16 06:31 06/13/16 13:51 1DCB Decachlorobiphenyl 30 - 128
90 06/09/16 06:31 06/13/16 13:51 1Tetrachloro-m-xylene 36 - 124
85 06/09/16 06:31 06/13/16 13:51 1Tetrachloro-m-xylene 36 - 124
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233753/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234206 Prep Batch: 233753
4,4'-DDD 0.500 0.492 ug/L 98 54 - 163
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4,4'-DDE 0.500 0.472 ug/L 94 60 - 146
4,4'-DDT 0.500 0.489 ug/L 98 56 - 160
Aldrin 0.500 0.439 ug/L 88 44 - 145
alpha-BHC 0.500 0.461 ug/L 92 53 - 148
alpha-Chlordane 0.500 0.475 ug/L 95 55 - 141
beta-BHC 0.500 0.469 ug/L 94 55 - 139
delta-BHC 0.500 0.409 ug/L 82 60 - 145
Dieldrin 0.500 0.485 ug/L 97 57 - 145
Endosulfan I 0.500 0.428 ug/L 86 26 - 120
Endosulfan II 0.500 0.460 ug/L 92 25 - 123
Endosulfan sulfate 0.500 0.471 ug/L 94 60 - 137
Endrin 0.500 0.462 ug/L 92 66 - 142
Endrin aldehyde 0.500 0.462 ug/L 92 59 - 120
Endrin ketone 0.500 0.481 ug/L 96 64 - 120
gamma-BHC (Lindane) 0.500 0.459 ug/L 92 53 - 144
gamma-Chlordane 0.500 0.483 ug/L 97 57 - 140
Heptachlor 0.500 0.441 ug/L 88 56 - 123
Heptachlor epoxide 0.500 0.477 ug/L 95 44 - 151
Methoxychlor 0.500 0.465 ug/L 93 56 - 153
DCB Decachlorobiphenyl 30 - 128
Surrogate
66
LCS LCS
Qualifier Limits%Recovery
56DCB Decachlorobiphenyl 30 - 128
90Tetrachloro-m-xylene 36 - 124
83Tetrachloro-m-xylene 36 - 124
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 240-233005/12-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233178 Prep Batch: 233005
RL MDL
Aroclor-1016 ND 33 12 ug/Kg 06/03/16 07:23 06/06/16 15:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1633 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1221
ND 2033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1232
ND 1133 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1242
ND 8.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1248
ND 1433 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1254
ND 9.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1260
Tetrachloro-m-xylene 64 14 - 128 06/06/16 15:06 1
MB MB
Surrogate
06/03/16 07:23
Dil FacPrepared AnalyzedQualifier Limits%Recovery
79 06/03/16 07:23 06/06/16 15:06 1DCB Decachlorobiphenyl 10 - 132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233005/13-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233178 Prep Batch: 233005
Aroclor-1016 333 246 ug/Kg 74 47 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aroclor-1260 333 277 ug/Kg 83 46 - 120
Tetrachloro-m-xylene 14 - 128
Surrogate
66
LCS LCS
Qualifier Limits%Recovery
80DCB Decachlorobiphenyl 10 - 132
Client Sample ID: Method BlankLab Sample ID: MB 240-233752/4-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
RL MDL
Aroclor-1016 ND 0.10 0.050 ug/L 06/09/16 06:29 06/13/16 10:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0900.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1221
ND 0.0700.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1232
ND 0.0600.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1242
ND 0.0500.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1248
ND 0.0300.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1254
ND 0.0400.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1260
Tetrachloro-m-xylene 59 21 - 120 06/13/16 10:16 1
MB MB
Surrogate
06/09/16 06:29
Dil FacPrepared AnalyzedQualifier Limits%Recovery
33 06/09/16 06:29 06/13/16 10:16 1DCB Decachlorobiphenyl 10 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233752/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
Aroclor-1016 2.50 1.60 ug/L 64 32 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233752/5-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 234149 Prep Batch: 233752
Aroclor-1260 2.50 1.52 ug/L 61 36 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Tetrachloro-m-xylene 21 - 120
Surrogate
60
LCS LCS
Qualifier Limits%Recovery
36DCB Decachlorobiphenyl 10 - 120
Method: 6020A - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 240-232891/1-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891
RL MDL
Silver 0.00180 J 0.20 0.0014 mg/Kg 06/02/16 11:09 06/03/16 20:41 2
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
1.64 J 0.6210 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Aluminum
0.0354 J 0.0261.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Arsenic
ND 0.221.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Barium
0.0228 J 0.0110.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Beryllium
0.00780 J 0.00370.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cadmium
0.0170 J 0.00170.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cobalt
0.347 J 0.0600.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Chromium
0.243 J 0.0970.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Copper
281 3.220 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Iron
1.73 0.121.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Manganese
0.0688 J 0.0450.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Lead
ND 0.0140.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Antimony
0.0472 J 0.0401.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Selenium
ND 0.0190.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Thallium
ND 0.0371.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Vanadium
1.17 J 0.504.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Zinc
34.7 J 22200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Calcium
8.60 J 4.9200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Potassium
7.73 J 4.0200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Magnesium
26.5 J 8.7200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Sodium
Client Sample ID: Method BlankLab Sample ID: MB 240-232891/1-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233381 Prep Batch: 232891
RL MDL
Nickel 0.0802 J 0.40 0.039 mg/Kg 06/02/16 11:09 06/06/16 14:18 2
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891
Silver 10.0 9.61 mg/Kg 96 60 - 114
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891
Aluminum 1000 964 mg/Kg 96 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 100 92.4 mg/Kg 92 73 - 110
Barium 100 95.2 mg/Kg 95 70 - 110
Beryllium 100 104 mg/Kg 104 79 - 110
Cadmium 100 92.8 mg/Kg 93 74 - 110
Cobalt 100 101 mg/Kg 101 74 - 110
Chromium 100 96.8 mg/Kg 97 70 - 110
Copper 100 98.5 mg/Kg 99 73 - 110
Iron 1000 982 mg/Kg 98 80 - 120
Manganese 100 98.4 mg/Kg 98 80 - 120
Lead 100 108 mg/Kg 108 75 - 110
Antimony 10.0 9.42 mg/Kg 94 68 - 113
Selenium 100 89.0 mg/Kg 89 65 - 110
Thallium 25.0 26.0 mg/Kg 104 71 - 110
Vanadium 100 96.6 mg/Kg 97 72 - 110
Zinc 100 95.9 mg/Kg 96 72 - 113
Calcium 1000 973 mg/Kg 97 80 - 120
Potassium 1000 1000 mg/Kg 100 80 - 120
Magnesium 1000 1000 mg/Kg 100 80 - 120
Sodium 1000 1010 mg/Kg 101 80 - 120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233381 Prep Batch: 232891
Nickel 100 99.0 mg/Kg 99 75 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 240-233672/2-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:40 1Aluminum
ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Arsenic
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Barium
ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Beryllium
ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cadmium
ND 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cobalt
ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Chromium
ND 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Copper
ND 16100 ug/L 06/08/16 13:00 06/09/16 13:40 1Iron
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Manganese
ND 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Nickel
ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Lead
ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Antimony
0.288 J 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Selenium
ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Thallium
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 240-233672/2-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Vanadium ND 5.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:40 1Zinc
ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:40 1Calcium
ND 301000 ug/L 06/08/16 13:00 06/09/16 13:40 1Potassium
ND 481000 ug/L 06/08/16 13:00 06/09/16 13:40 1Magnesium
ND 681000 ug/L 06/08/16 13:00 06/09/16 13:40 1Sodium
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233672/3-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672
Silver 100 94.5 ug/L 95 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Aluminum 10000 10400 ug/L 104 80 - 120
Arsenic 1000 913 ug/L 91 80 - 120
Barium 1000 931 ug/L 93 80 - 120
Beryllium 1000 1140 ug/L 114 80 - 120
Cadmium 1000 927 ug/L 93 80 - 120
Cobalt 1000 952 ug/L 95 80 - 120
Chromium 1000 973 ug/L 97 80 - 120
Copper 1000 931 ug/L 93 80 - 120
Iron 10000 9370 ug/L 94 80 - 120
Manganese 1000 997 ug/L 100 80 - 120
Nickel 1000 966 ug/L 97 80 - 120
Lead 1000 823 ug/L 82 80 - 120
Antimony 100 94.0 ug/L 94 80 - 120
Selenium 1000 904 ug/L 90 80 - 120
Thallium 250 209 ug/L 84 80 - 120
Vanadium 1000 1010 ug/L 101 80 - 120
Zinc 1000 959 ug/L 96 80 - 120
Calcium 10000 10700 ug/L 107 80 - 120
Potassium 10000 9350 ug/L 93 80 - 120
Magnesium 10000 9570 ug/L 96 80 - 120
Sodium 10000 9620 ug/L 96 80 - 120
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-CMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:36 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:36 1Aluminum
ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Arsenic
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Barium
ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Beryllium
ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cadmium
0.115 J 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cobalt
ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Chromium
1.96 J 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Copper
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-CMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
RL MDL
Iron ND 100 16 ug/L 06/08/16 13:00 06/09/16 13:36 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Manganese
0.232 J 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Nickel
ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Lead
ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Antimony
ND 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Selenium
ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Thallium
ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Vanadium
ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:36 1Zinc
ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:36 1Calcium
ND 301000 ug/L 06/08/16 13:00 06/09/16 13:36 1Potassium
ND 481000 ug/L 06/08/16 13:00 06/09/16 13:36 1Magnesium
184 J 681000 ug/L 06/08/16 13:00 06/09/16 13:36 1Sodium
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
Silver ND 100 93.6 ug/L 94 75 - 125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Aluminum 4100 10000 15000 ug/L 109 75 - 125
Arsenic 1.6 J 1000 992 ug/L 99 75 - 125
Barium 140 1000 1120 ug/L 98 75 - 125
Beryllium 0.16 J 1000 1180 ug/L 118 75 - 125
Cadmium 0.24 J 1000 951 ug/L 95 75 - 125
Cobalt 0.19 J B 1000 973 ug/L 97 75 - 125
Chromium 1500 1000 2500 ug/L 99 75 - 125
Copper ND 1000 921 ug/L 92 75 - 125
Iron ND 10000 9500 ug/L 95 75 - 125
Manganese ND 1000 1010 ug/L 101 75 - 125
Nickel ND 1000 970 ug/L 97 75 - 125
Lead 0.70 J 1000 860 ug/L 86 75 - 125
Antimony 2.4 100 102 ug/L 100 75 - 125
Selenium 17 B 1000 986 ug/L 97 75 - 125
Thallium 0.19 J 250 222 ug/L 89 75 - 125
Vanadium 98 1000 1130 ug/L 103 75 - 125
Zinc ND 1000 950 ug/L 95 75 - 125
Calcium 250000 10000 259000 4 ug/L 99 75 - 125
Potassium 11000 10000 20400 ug/L 95 75 - 125
Magnesium 140 J 10000 9860 ug/L 97 75 - 125
Sodium 4200 B 10000 14100 ug/L 98 75 - 125
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
Silver ND 100 93.6 ug/L 94 75 - 125 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Aluminum 4100 10000 14800 ug/L 107 75 - 125 1 20
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 6020A - Metals (ICP/MS) (Continued)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672
Arsenic 1.6 J 1000 986 ug/L 98 75 - 125 1 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 140 1000 1100 ug/L 97 75 - 125 1 20
Beryllium 0.16 J 1000 1170 ug/L 117 75 - 125 1 20
Cadmium 0.24 J 1000 940 ug/L 94 75 - 125 1 20
Cobalt 0.19 J B 1000 941 ug/L 94 75 - 125 3 20
Chromium 1500 1000 2440 ug/L 93 75 - 125 3 20
Copper ND 1000 901 ug/L 90 75 - 125 2 20
Iron ND 10000 9260 ug/L 93 75 - 125 3 20
Manganese ND 1000 982 ug/L 98 75 - 125 2 20
Nickel ND 1000 957 ug/L 96 75 - 125 1 20
Lead 0.70 J 1000 842 ug/L 84 75 - 125 2 20
Antimony 2.4 100 101 ug/L 98 75 - 125 1 20
Selenium 17 B 1000 977 ug/L 96 75 - 125 1 20
Thallium 0.19 J 250 218 ug/L 87 75 - 125 2 20
Vanadium 98 1000 1130 ug/L 103 75 - 125 0 20
Zinc ND 1000 924 ug/L 92 75 - 125 3 20
Calcium 250000 10000 255000 4 ug/L 62 75 - 125 1 20
Potassium 11000 10000 20100 ug/L 92 75 - 125 1 20
Magnesium 140 J 10000 9710 ug/L 96 75 - 125 2 20
Sodium 4200 B 10000 13900 ug/L 96 75 - 125 1 20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 240-233673/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233843 Prep Batch: 233673
RL MDL
Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233673/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233843 Prep Batch: 233673
Mercury 5.00 4.82 ug/L 96 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-DMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673
RL MDL
Mercury 0.0925 J 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 11:58 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673
Mercury ND 5.00 5.02 ug/L 100 80 - 120
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673
Mercury ND 5.00 4.89 ug/L 98 80 - 120 3 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 240-232940/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233026 Prep Batch: 232940
RL MDL
Mercury ND 0.10 0.014 mg/Kg 06/02/16 15:00 06/03/16 07:27 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232940/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233026 Prep Batch: 232940
Mercury 0.833 0.865 mg/Kg 104 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 240-233791/9-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
RL MDL
Cr (VI) 0.358 J 0.80 0.15 mg/Kg 06/09/16 09:04 06/09/16 13:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 240-233791/11-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
Cr (VI) 643 582 mg/Kg 90 75 - 125
Analyte
LCSI LCSI
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 240-233791/10-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791
Cr (VI) 20.0 18.5 mg/Kg 93 90 - 110
Analyte
LCSS LCSS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample ResultsTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-AMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233639
RL MDL
Cr (VI) ND 0.020 0.0021 mg/L 06/08/16 11:47 1
LB LB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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QC Association SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
GC/MS VOA
Analysis Batch: 233030
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 233052240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 8260BLCS 240-233030/5 Lab Control Sample Total/NA
Solid 8260BMB 240-233030/6 Method Blank Total/NA
Prep Batch: 233052
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5030A240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Leach Batch: 233606
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 1312240-65486-1 WESTERLY WWTC-ASH (WWWTC) SPLP
Solid 1312LB 240-233606/1-A MB Method Blank SPLP
Analysis Batch: 233711
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 233606240-65486-1 WESTERLY WWTC-ASH (WWWTC) SPLP
Solid 8260B 233606LB 240-233606/1-A MB Method Blank SPLP
Solid 8260BLCS 240-233711/6 Lab Control Sample Total/NA
GC/MS Semi VOA
Prep Batch: 233013
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3540CLCS 240-233013/18-A Lab Control Sample Total/NA
Solid 3540CMB 240-233013/17-A Method Blank Total/NA
Analysis Batch: 233383
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233013LCS 240-233013/18-A Lab Control Sample Total/NA
Solid 8270C 233013MB 240-233013/17-A Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Analysis Batch: 233573
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233013240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Prep Batch: 233761
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3510CLCS 240-233761/5-A Lab Control Sample Total/NA
Solid 3510CMB 240-233761/4-A Method Blank Total/NA
Analysis Batch: 233811
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233761240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
GC/MS Semi VOA (Continued)
Analysis Batch: 233974
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 233761LCS 240-233761/5-A Lab Control Sample Total/NA
Solid 8270C 233761MB 240-233761/4-A Method Blank Total/NA
Leach Batch: 234140
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Prep Batch: 234253
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3510C 234140240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3510CLCS 240-234253/4-A Lab Control Sample Total/NA
Solid 3510CMB 240-234253/3-A Method Blank Total/NA
Analysis Batch: 234362
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270C 234253240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 8270C 234253LCS 240-234253/4-A Lab Control Sample Total/NA
Solid 8270C 234253MB 240-234253/3-A Method Blank Total/NA
GC Semi VOA
Prep Batch: 233005
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3540CLCS 240-233005/13-A Lab Control Sample Total/NA
Solid 3540CMB 240-233005/12-A Method Blank Total/NA
Prep Batch: 233006
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3540C240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3540C240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3540C240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3540CLCS 240-233006/6-A Lab Control Sample Total/NA
Solid 3540CMB 240-233006/5-A Method Blank Total/NA
Analysis Batch: 233178
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8082A 233005240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 8082A 233005LCS 240-233005/13-A Lab Control Sample Total/NA
Solid 8082A 233005MB 240-233005/12-A Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Prep Batch: 233752
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3520C 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3520CLCS 240-233752/5-A Lab Control Sample Total/NA
Solid 3520CMB 240-233752/4-A Method Blank Total/NA
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
GC Semi VOA (Continued)
Prep Batch: 233753
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3520C 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3520CLCS 240-233753/5-A Lab Control Sample Total/NA
Solid 3520CMB 240-233753/4-A Method Blank Total/NA
Analysis Batch: 233996
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 233006240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 8081B 233006240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 8081B 233006240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 8081B 233006LCS 240-233006/6-A Lab Control Sample Total/NA
Solid 8081B 233006MB 240-233006/5-A Method Blank Total/NA
Analysis Batch: 234149
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8082A 233752240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 8082A 233752LCS 240-233752/5-A Lab Control Sample Total/NA
Solid 8082A 233752MB 240-233752/4-A Method Blank Total/NA
Analysis Batch: 234206
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8081B 233753240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 8081B 233753LCS 240-233753/5-A Lab Control Sample Total/NA
Solid 8081B 233753MB 240-233753/4-A Method Blank Total/NA
Metals
Prep Batch: 232891
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3050BLCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 3050BMB 240-232891/1-A ^2 Method Blank Total/NA
Prep Batch: 232940
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 7471ALCS 240-232940/2-A Lab Control Sample Total/NA
Solid 7471AMB 240-232940/1-A Method Blank Total/NA
Analysis Batch: 233026
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471A 232940240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 7471A 232940LCS 240-232940/2-A Lab Control Sample Total/NA
Solid 7471A 232940MB 240-232940/1-A Method Blank Total/NA
Analysis Batch: 233211
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 232891240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 6020A 232891LCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 6020A 232891MB 240-232891/1-A ^2 Method Blank Total/NA
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
Metals (Continued)
Analysis Batch: 233381
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 232891240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 6020A 232891240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 6020A 232891LCS 240-232891/3-A ^2 Lab Control Sample Total/NA
Solid 6020A 232891MB 240-232891/1-A ^2 Method Blank Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid D3987-85240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid D3987-85240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid D3987-85LB 240-233529/1-C Method Blank ASTM Leach
Solid D3987-85LB 240-233529/1-D Method Blank ASTM Leach
Prep Batch: 233672
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3005A 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3005A 233529240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3005A 233529240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 3005A 233529LB 240-233529/1-C Method Blank ASTM Leach
Solid 3005ALCS 240-233672/3-A Lab Control Sample Total Recoverable
Solid 3005AMB 240-233672/2-A Method Blank Total Recoverable
Prep Batch: 233673
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233529240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233529240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233529LB 240-233529/1-D Method Blank ASTM Leach
Solid 7470ALCS 240-233673/3-A Lab Control Sample Total/NA
Solid 7470AMB 240-233673/2-A Method Blank Total/NA
Analysis Batch: 233843
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7470A 233673240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233673240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233673240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7470A 233673LB 240-233529/1-D Method Blank ASTM Leach
Solid 7470A 233673LCS 240-233673/3-A Lab Control Sample Total/NA
Solid 7470A 233673MB 240-233673/2-A Method Blank Total/NA
Analysis Batch: 233954
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020A 233672240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 6020A 233672240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 6020A 233672240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 6020A 233672LB 240-233529/1-C Method Blank ASTM Leach
Solid 6020A 233672LCS 240-233672/3-A Lab Control Sample Total Recoverable
Solid 6020A 233672MB 240-233672/2-A Method Blank Total Recoverable
TestAmerica Canton
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QC Association SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District
Project/Site: WESTERLY WWTC-ASH (WWWTC)
General Chemistry
Analysis Batch: 232880
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Leach Batch: 233529
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D3987-85240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid D3987-85LB 240-233529/1-A Method Blank ASTM Leach
Analysis Batch: 233639
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach
Solid 7196A 233529LB 240-233529/1-A Method Blank ASTM Leach
Prep Batch: 233791
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 3060ALCSI 240-233791/11-A Lab Control Sample Total/NA
Solid 3060ALCSS 240-233791/10-A Lab Control Sample Total/NA
Solid 3060AMB 240-233791/9-A Method Blank Total/NA
Analysis Batch: 233886
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 233791240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA
Solid 7196A 233791LCSI 240-233791/11-A Lab Control Sample Total/NA
Solid 7196A 233791LCSS 240-233791/10-A Lab Control Sample Total/NA
Solid 7196A 233791MB 240-233791/9-A Method Blank Total/NA
TestAmerica Canton
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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1Matrix: SolidDate Collected: 05/31/16 14:10
Date Received: 06/01/16 10:20
Leach 1312 06/07/16 20:15 DRJ233606 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP
Analysis 8260B 1 233711 06/08/16 20:49 TJL1 TAL CANSPLP
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3510C 233761 06/09/16 07:34 CSC TAL CANASTM Leach
Analysis 8270C 1 233811 06/09/16 21:17 JMG TAL CANASTM Leach
Leach D3987-85 RE 234140 06/12/16 16:25 DRJ TAL CANASTM Leach
Prep 3510C RE 234253 06/13/16 11:40 JDR TAL CANASTM Leach
Analysis 8270C RE 1 234362 06/14/16 10:13 MRU TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3520C 233753 06/09/16 06:31 CSC TAL CANASTM Leach
Analysis 8081B 1 234206 06/13/16 15:28 BPM TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3520C 233752 06/09/16 06:29 CSC TAL CANASTM Leach
Analysis 8082A 1 234149 06/13/16 09:58 SEM TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 3005A 233672 06/08/16 13:00 AJC TAL CANASTM Leach
Analysis 6020A 1 233954 06/09/16 13:48 AS1 TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Prep 7470A 233673 06/08/16 13:30 AJC TAL CANASTM Leach
Analysis 7470A 1 233843 06/09/16 12:05 WKD TAL CANASTM Leach
Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach
Analysis 7196A 1 233639 06/08/16 13:35 GNR TAL CANASTM Leach
Analysis Moisture 1 232880 06/02/16 10:25 LCN TAL CANTotal/NA
Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
Prep 5030A 06/03/16 10:36 SAM233052 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8260B 1 233030 06/03/16 19:07 SAM TAL CANTotal/NA
Prep 3540C 233013 06/03/16 08:23 DT TAL CANTotal/NA
Analysis 8270C 4 233573 06/08/16 21:44 JMG TAL CANTotal/NA
Prep 3540C 233006 06/03/16 07:28 DT TAL CANTotal/NA
Analysis 8081B 1 233996 06/10/16 16:27 BPM TAL CANTotal/NA
Prep 3540C 233005 06/03/16 07:23 DT TAL CANTotal/NA
Analysis 8082A 1 233178 06/06/16 14:47 HMB TAL CANTotal/NA
Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA
Analysis 6020A 2 233211 06/03/16 21:58 AS1 TAL CANTotal/NA
Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA
Analysis 6020A 2 233381 06/06/16 14:30 AS1 TAL CANTotal/NA
Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA
Analysis 6020A 20 233381 06/06/16 14:34 AS1 TAL CANTotal/NA
Prep 7471A 232940 06/02/16 15:00 DEE TAL CANTotal/NA
TestAmerica Canton
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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)
Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1Matrix: SolidDate Collected: 05/31/16 14:10
Percent Solids: 99.7Date Received: 06/01/16 10:20
Analysis 7471A 06/03/16 07:44 WKD1 233026 TAL CAN
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Prep 3060A 233791 06/09/16 09:04 DTN TAL CANTotal/NA
Analysis 7196A 1 233886 06/09/16 13:45 DTN TAL CANTotal/NA
Laboratory References:
TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396
TestAmerica Canton
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Certification SummaryClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)
Laboratory: TestAmerica CantonAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
California 01144CA9NELAP 06-30-14 *
California State Program 9 2927 04-30-17
Connecticut State Program 1 PH-0590 12-31-17
Florida NELAP 4 E87225 06-30-16 *
Illinois NELAP 5 200004 07-31-16 *
Kansas NELAP 7 E-10336 07-31-16 *
Kentucky (UST) State Program 4 58 02-23-17
Kentucky (WW) State Program 4 98016 12-31-16
L-A-B DoD ELAP L2315 07-18-16
Minnesota NELAP 5 039-999-348 12-31-16
Nevada State Program 9 OH-000482008A 07-31-16 *
New Jersey NELAP 2 OH001 06-30-16 *
New York NELAP 2 10975 03-31-17
Ohio VAP State Program 5 CL0024 09-14-17
Oregon NELAP 10 4062 02-23-17
Pennsylvania NELAP 3 68-00340 08-31-16 *
Texas NELAP 6 T104704517-15-5 08-31-16 *
USDA Federal P330-13-00319 11-26-16
Virginia NELAP 3 460175 09-14-16
Washington State Program 10 C971 01-12-17
West Virginia DEP State Program 3 210 12-31-16
Wisconsin State Program 5 999518190 08-31-16 *
TestAmerica Canton
* Certification renewal pending - certification considered valid.
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