,rjorie McLaugh!in -, Whittaker waste manifest activities · 2012. 11. 30. · ANALYTICAL. REPORT PROJECT NO. 23535 Whittaker, Transfer, PA Lot #: F5G070301 Rich Moss Scientech Inc

,rjorie McLaugh!in -, Whittaker waste manifest activities "Ip a g e 1 ý

From: "Kevin Taylor" <[email protected]>To: <[email protected]>Date: Mon, Nov 14, 2005 2:44 PMSubject: Whittaker waste manifest activities

Marjorie:

To address the last open issue from your site inspection, I haveattached a copy of the spreadsheet and laboratory report used tocalculate the activity values placed on the Whittaker waste manifests.However, minor mathematical errors were identified and the calculationsshow activity values slightly higher than what were on the manifest.The correct thorium value is 85.1 comparedto 83.9 pCi/g and the correcturanium activity is 16.7 compared to 16.2 pCi/g.

The methodology for determining the activity estimate for the manifestswas as follows:

1 - Eight representative slag samples (high, medium, and low activitysamples) were collected and pulverized on-site using the excavatorbucket.

2 - Samples were analyzed by STL for thorium and uranium isotopes usingalphaspectroscopy. See attached data report..

3 - The sums of the reported concentrations plus the 2-sigma analyticalerror were used to determine the average activity of the data set. Seeattached spreadsheet.

4 - To provide a level of conservatism, the average value was increasedby the standard deviation of the data set. This value (mean + 1 sigma)was placed on the waste manifest. See attached spreadsheet.

It is important to note that while only 8 samples were used for thedetermining the values to put on the manifest, the range of the data isconsistent with surveys of large (1.7 cubic yard) composite samples,including on-site gamma spectroscopy analyses.

We are sending out our reply to your comments on the Section 2 FFSP thisweek.

Information in this record was deletedin accordance with the Freedom of InformlatonAct, exemptions ti n . ..'FOIA - . . ,= -00 6 J ..

3rjorie McLaughlin - Whittaker waste manifest activities .Page 21

Pat is demobilizing from the site this week. I will include a copy forthe final fenceline survey with the groundwater sample results. Let meknow if you have any additional questions.

Kevin E. Taylor, PE, CHPSr. Health PhysicistEnvirocare of Utah, LLC17 College St., Suite D

p Greenville, SC 29601, 864-235-3695 - office

Ktaylorg)Denvllccom

CC: "Kenneth Kasper" <[email protected]>, "Richard Moss" <[email protected]>,"Stewart Smith" <[email protected]>, "Lee Penney" <[email protected]>,<[email protected]>

\temp\GW)OOOO1 .TMP - - Pagell\temp\GW)0000J.TMP Page 11

Mail Envelope Properties (4378E8E3.16B :7 :8555)

Subject:Creation DateFrom:

Created By:

Whittaker waste manifest activitiesMon, Nov 14, 2005 2:41 PM"Kevin Taylor" <ktaylorpenvllc.com>

ktaylor(&)envllc.com

Recipientsnrc.govkplpo.KPDOMMM3 (Marjorie McLaughlin)

scientech.comphorkman CC

envllc.comlpenney CC (Lee Penney)ssmith CC (Stewart Smith)rmoss CC (Richard Moss).kkasper CC (Kenneth Kasper)

Post Officekpl po.KPDO

FilesMESSAGETEXT.htmalpha spec-I .pdfmanifest activities.xlsMime.822

OptionsExpiration Date:Priority:ReplyRequested:Return Notification:

Concealed Subject:Security:

Routenrc.govscientech.comenvllc.com

Size19645773745887266241067728

NoneStandardNoNone

NoStandard

Date & TimeMonday, November 14, 2005 2:41 PM

SEVERN

--T-R'E STLI

STL St. Louls13715 Rider Trail NorthEarth City, MO 63045

Tel; 314 298 8566 Fax: 314 298 8757www,stl-inucom

ANALYTICAL. REPORT

PROJECT NO. 23535

Whittaker, Transfer, PA

Lot #: F5G070301

Rich Moss

Scientech Inc143 West Street

New Milford, CT 06776

SEVERN TRENT LABORATORIES, INC.

Chet ScheibelProject Manager

July 20, 2005

ro a e ting.-Ud ers.in Emi' iirý 5 Severn Trent Laboratorle4, Inc.

Case NarrativeLOT NUMBER: F5G070301

This report contains the analytical results for the eight samples received under chain of custody bySTL St. Louis on July 7, 2005. These samples are associated with your Whittaker, Transfer, PAproject.

The analytical results included in this report meet all applicable quality control procedurerequirements except as noted on the following page.

The test results in this report meet all NELAP requirements for parameters in which accreditationsare held by STL St. Louis. Any exceptions to NELAP requirements are noted in the case narrative.The case narrative is an integral part of this report.

All chemical analysis results are based upon sample as received, wet weight, unless noted otherwise.All radiochemistry results are based upon sample as dried and ground with the exception of tritium,unless requested wet weight by the client.

Observations/Nonconformances

Reference the chain of custody and condition upon receipt report for any variations on receiptconditions and temperature of samples on receipt.

Iso topic Thorium by A-01-R MOD

The Thorium spectrum are smeared due to a matrix interference. Samples to re-extract with areduced aliquot to minimize this interference. The re-extract results provided better qualityspectrnur and will be reported, F5G070301-007 and -007X were stopped during counting to mrnimizetailing.

Affected Samples:F5G070301 (1): 6-30-05 S-1F5(070301 (2): 6-30-05 S-2F5070301 (3):-6-30-05S-3F5G070301 (4): 6-30-05 S-4F5G070301 (5): 6-30-05 S-5F5G070301 (6): 6-30-05 S-6F5G070301 (7): 6-30-05 S-7F5G070301 (8): 6-30-05 S-8

METHODS SUMMARY

FSG070301

ANALYTICAL PREPARATIONMETHOD METHODPARAMETER

Inductively Coupled Plasma (ICP) MetalsIsotopic Thorium by Alpha SpectroscopyIsotopic Uranium by Alpha SpectroscopyMercury in Liquid Waste (Manual Cold-Vapor)

SW846 6010BEML A-01-R MODEML A-01-R MODSW846 7470A

SW846 1311/3010

SW846 1311/7470

References;

EML "ENVIRONMENTAL MEASUREMENTS LABORATORY PROCEDURES MANUAL"HASL-300 28TH EDITION, VOLUME I and II DEPARTMENT OF ENERGY

SW846 "Test Methods for Evaluating Solid Waste, Physical/ChemicalMethods"' Third Edition, November 1986 and its updates.

I,

SAMPLE SUMMARY

PSG070301

SAMPLED SAMP

WO # SAMPLE# CLIENT SAMPLE iD DATE TIME

HE2LG 001 6-30-05 S-I 06/30/05 13:00HE2L4 002 6-30-05 S-2 06/30/05 13:05HE2L6 003 6-30-05 S-3 06/30/05 13:10HE2LB 004 6-30-05 S-4 06/30/05 13:15HE2MC 005 6-30-05 S-5 06/30/05 i3:20HE2MG 006 6-30-05 S-6 06/30/05 13:25HE2Mfl 007 6-30-05 S-7 06/30/05 13:30HE2MJ 008 6-30-05 S-8 06/30/05 13:35

NOTE(S)--The analytical results of the samples listed above are presented on the following pages.

- All calculations art performed before rounding to avoid round-off errors in calculated results.

- Resulit noted as 'ND' were not detected at or above the stated limit.

* This report must not be reproduced, except In full, without the written approval of the laboratory.

- Results for the following parameters are never teporEed on a dry weight basis: color, corrossviry, density, flsxpoim, ignitabIlity, layers, odor,

palin, Ailte test, pH, porosity pressure, reactivity. redox potential, specific gravity, spot tests, solids, solubltity, temperature, viscosity, and weight.

SCIEITECH INC

Client Sawple ID: 6-30-05 S-I

TCLP Metals

Lot-Sample #. : F5G070301-001

Date Sampled. .: 06/30/05 13:00 Date Received..:. 07/07/05

Leach Date ....... 07/11/05 Leach Batch #..: P519204

REPORTINGPARAMETER RESULT LIMIT UNITS METHOD

Matrix ....... : SOLID

Prep Batch #...: 5193423

Arsenic

Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

zinc

ND

4650 J

ND

ND

ND

ND

ND

ND

ND

124 B

ND

11.8 B,J

500Dilution

500Dilution

25.0

Dilution

50.0Dilution

250Dilution

50.0Dilution

500Dilution

375Dilution

62.5Dilution

250Dilution

1250

Dilution

150Dilution

ug/LFactor: 2.5

ug/LFactor: 2.5

ug/L

Factor: 2.5

Factor: 2.5

ug/LFactor: 2.5

ug/LFactor: 2.5

ug/LFactor: 2.5

uq/LFactor: 2.5

ug/LFactor: 2.5

ug/L

Factor: 2.5

ug/L

Factor: 2.5

SW846 6010B

Analysis Time..

SW846 6010BAnalysis Time.:

SW846 6010BAnalysis Time..

SW846 6010BAnalysis Time.

SW846 6010BAnalysis Time...,

SW846 6010BAnalysis Time...


SW846 6010BAnalysis Time..:

SW846 6010B.AnalyaAs. Time,.:

SW846 60103Analysis Time..


SW846 60103Analysis Time..

13 :56

13:56

13:56

13-,56

13 55

13 56

13:56

13;56

)j1: 56

13:56

13:56

13; :6

PREPARATION-

ANALYSIS DATE

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/OS

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

WORKORDER #

HE2LG1AA

EZ2LGIAC

HE2LG1AD

HE2LGIAE

HE2LGIAF

HE2LGiAG

HE2LGIAH

HE2LG1AJ

HE2LGIAK

H•2LGIAL

H{E2 LGlAM

HE2LGIAN>

Prep Batch #...: 5194097

Mercury ND 10.0 ug/L SW846 7470A

Analysis Time..: 14:2707/15/O5 "HE2LGIAP

Dilution Factor: 5

((Continued on next page)

SCIENTECH INC

Client Sample ID: 6-30-05 S-i

TCLP Metals

Lot-Sample #...: F5G070301-001 Matrix ......... : SOLID

NOTE (S) :

Analysis performned In accordance wirh USEPA Toxicity Charactcristic Leachrir Procedure Method 1311

I Method blank contamination. The alsoclaled method blamnk con(arns thre arget analyie at a reportable level.

B EgImaled rMlL •e•rlt Is lets than RL.

SCIENTECH INC

Client Sample ID: 6-30-05 S-2

TCLP Metals

Lot-Sample #...: F5G070301-002

Date Sampled...: 06/30/05 13:05 Date Received..: 07/07/05Leach Date......: 07/11/05 Leach Batch #..: P519204



PREPARATION- WORKANALYSIS DATE ORDER #

07/12-07/13/05 HE2L41AAPrep Batch #...: 5193423Arsenic

Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

Zinc

ND

4740 J

ND

ND

ND

ND

ND

ND

ND

1170

ND

11.3 B,J

5194097ND

500 ug/LDilution Factor: 2.5


25.0 ug/LDilution Factor: 2.5

50.0 ug/LDilution Factor: 2,5





62.5 ug/LDilutaon _act.or 2.5 5



15O ug/LDilution Factor: 2.5

1010 uq/LDilution Factor: 5


SW846 6010B

Analysis Time..

SW846 6010B

Analysis Time..

SW846 6010BAnalysis Time.-

SW846 GO1OB

Analysis Time,.

SW846 6010B

Analysis Time..


SW846 6010B

Analysis Time..:

SW846 6010B_.... An~a.!ysi!s Tim• ,.


SW846 6010B

Analysis Time..:

SW84S 6010BAnalysis Time,.:

14:20

14:20

14.20

14:20

14z20

14:20

14:20

14 :20

14:20

14,20

14120

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/o5

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/os

07/12-07/13/05

07/12-07/13/OS

BE2LA1AC

HE21,41AD

HE2L41AE

HE2L41AF

HE2L4 lAG

HE2L41AH

HE2L41AJ

HE2L,41AK

BER2L4IAL

HB2L4lAM

HE2L41AN

Prep Batch #.

Mercury

K

SW846 7470A

Analysis Time.. % 14:3507/15/05 HE2L41AP

(Continued on next page)

SCIENTECH INC


TCLP Metals

Lot-Sample # .. : F5G070301-002 Matrix .......... : SOLID

NOTE (S):Analysis performed in accordance with USEPA Toxicity Charactcristic Leaching Procedurc Method 1311

J Method blank contamination. The associated mechod blank contains the targeo ana(yte at a reportable level.

8 Fstimated reult. Rensul Is less than RL

SCIENTECH INC


TCLP Metals

Lot-Sample #...: F5G070301-003Date Sampled... 06/30/05 13:10 Date Received..: 07/07/05Leach Date ..... .. 07/11/05 Leach Batch #..: P519204




07/12-07/13/0S HE2L61AA

Prep Batch #...; 5193423Arsenic ND

Barium 7740 J

Cadmium ND

Chromium ND

Lead ND

Silver ND

Selenium ND

Antimony ND

Beryllium ND

Nickel 6550

Thallium ND

Zinc 19.6 B,J

500 ug/LDilution Factori 2.5





50.0 ug/LDilution Factor. 2.5



62.5 ug/L_Dilution Factor .. 2..5


1250 ug/LDilution Factor, 2.5


SW846 6010B 'Analysis Time.

,SW846 6010BAnalysis Time..

SW846 6010BAnalysis Time..-

SW846 60108Analysis Time..:

SW846 6010BAnalysis Time.,.

SW846 6010BAnalysis Time,.:

SW846 6010BAnalysis Time.. i


SW846 6010BAnalysis-Time...



SW846 6010BAnalysis Time..-

14:25

14:25

14t25

14:25

14:25

14:25

14:25

14 :25

14.t25

14:25

14:25

14:25

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/O5

07/12-07/13/05

07/12-07/13/05

HE2L61AC

HE2L61AD

HE2L61AE

HE2L61AF

HE2L61AG

HE2L61AH

HE2L61AJ

HE2L61AK

IM2L61AL

HE2L61AM

BE2L61AN

Prep Batch #...: 5194097Mercury ND 10.0 ug/L SW846 7470A

Analysis Time.., 14:38

07/15/05 HE2L61APDilution Factor: 5


SCIENTECH INC


TCLP Metals

Lot-Sample #...: FSG070301-003 Matrix .......... .SOLID

NOTE (S) :Analysls performed in accordance with USEPA Toxicity Charcteristic Leach•ng Procedur Method 13.1

J MVIIod blank contamsnallon. The associated method blank contains the jorget analyte at a reporable level.

B Elsimated esult. Result Is loss than RL.

SCIENTECH INC

Client Sample ID; 6-30-05 S-4

TCLP Metals

Lot-Sample # ... : F5G070301-004

Date Sampled...: 06/30/05 13:15 Date Received..: 07/07/05

Leach Date ..... : 07/11/05 Leach Batch #..: P519204

REPORTING


PREPARATION-PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE

Prep Batch #....: 5193423

Arsenic

Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

Zinc

ND 500 usg/L SW846 6010B

Dilution Factor: 2.5

5590 J 5o0 ug/LDilution Factor: 2.5

ND 25.0 ý ug/LDilution Factor: 2,5

ND 50.0 ug/LDilution Factor: 2,5

ND 250 ug/LDilution Factor: 2.5

ND 50.0 ug/LDilution Factor: 2.5

ND 500 ug/LDilution Factor: 2.5

ND 375 ug/LDilution Factor; 2.5

ND 62.5 ug/L- Dilution FactOr: 2.5

1780 250 ug/LDilution Factor: 2.5

ND 1250 ug/LDilution FactOr: 2.5

25,0 B,J 150 ug/LDilution Factor: 2.5

Analysis

SW846Analysis

SW846

Analysis

SW846

Analysis

SW846

Analysis

SW846

Analysis

SW846Analysis

SW646

Analysis

SW846AnaiySis

SW846

Analysis

SWB46Analysis

SW846Analysis

Time.. 14:41

6010B

Time..: 14:41

6010B

Time,, 14:41

6010BTime,. 14:41

6010BTime. - 14:41

6010B

Time..: 14:41

6010B

Time..: 14:41

6010B

Time..: 14:41

6010BTime..:_14:4l

GOlOB

Time..: 14:41

6010B

Time..: 14:41

6010B

Time-..: 14:41

0'7/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07113/05

07/12-07/13/05

07/12-07/13/OS

WORKORDER #

HE2L81AA

IIE21,8XAC

HE2LBIAD

HE2L8 lAE

RE2LB1AF

}IE2L81AG

HE2L81AH

HE2L81AJ

IiE2LS1AX

BB2LBIAL

1E2LB1AM

8B2L83AN

Prep Batch #...: 5194097Mercury ND 10 .0 ug/L SW846 7470A

Analysis Time..: 14:4007/15/05 HE2LS1AP

Dilution Factor: S


SCIENECH INC


TCLP Metals

Lot-Sample # ... : F5G070301-004 Matrix ......... ; SOLID

NOTE (S) :Ana)ysis performeu In accordance with USEPA Toxicity Charactristic LeachIng Procedure Method 1311

I Method blank contamination. The associated method blank contains tht targOt analytc at a reportable level.

B Estimated result. Result is less than RL,

SCIENTECH LNC


TCLP Metals

Lot-Sample #...: FSG070301-005

Date Sampled...; 06/30/05 13:20 Date Received..: 07/07/05

Leach Date ..... .. 07/11/05 Leach Batch #..: P519204


Matrix ....... .SOLID

Prep Batch i...: 5193423Arsenic ND

Barium 4340 J

Cadmium ND

Chromium ND

Lead ND

Silver ND

Selenium ND

Antimony ND

Beryllium ND

Nickel 591

Thallium ND

Zinc 10.5 BJ



25.0 ug/L


o 50,0 ug/LDilution Factor: 2.5

250 ug/L

Dilution Factor: 2,5

50.0 ug/L


500 ug/L

Dilution Factor, 2.5

375 ug/L


62.5 ug/L


250 ug/LDilution Factor; 2.5

1250 ug/L

Dilution Factor; 2.5

150 ug/L


SW846 6010BAnalysis Time..: 14:46

SW846 6010B

Analysis Time..: 14:46

SW846 60103

Analysis Time..- 14.46

SW846 6010B

Analysis Time..; 14.46

SW846 6010B

Analysis Time..; 14:46

SW846 6010B

Analysis Time.. : 14:46

SW846 6010BAnalysis Time,.- 14:46

SW846 6010BAnalysis Time..: 14:46

SW046 6010B


SW846 6010B


SW846 6010B


SW846 6010B


SW846 7470A

Analysis Time,._ 14:43

PREPARATION-ANALYSIS DATE

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/os

071/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/OS

07/12-07/13/05

07/12-07/13/05

WORKORDER #

H82MCIAA

HE2MCIAC

HE 2MClAD

HE2MCIAE

HE82MCAF

HE2MCIAG

HE2MClAR

HE2MC1AJ

HE2MCIAK

HE2MCIAL

EE2MC1AM

HB2MC1AN

Prep Batch #...: 5194097Mercury ND 10,0 ug/L 07/15/05 HE2MCIAP

Dilution Factor: 5


I SCIENTECH INC


TCLP Metals

Lot-Sample #...: FSG070301-005 Matrix ......... : SOLID

NOTE (S):Analysls performed In ccordarnce with USEPA Toxlcity COarocleriStu I..Laching Procedure Method 1311

J• Method blank contamination. The associated method blank contains the target ana.lyce at a reportable level.

B Estimaterd rciuL Rea.lt Is les than RL.

k

I'

SCIENTECH INC


TCLP Metals

Lot-Sample #...: F5G070301-006

Date SamplJed...: 06/30/05 13:25 Date Received..: 07/07/05Leach Date._.: 07/11/05 Leach Batch j..: P519204


Prep Batch #...: 5193423

Arsenic

Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

Zinc

ND

4460 J

WD

ND

ND

ND

ND

ND

ND

1030

ND

6.8 B,J

500



25.0 uq/L


5o.0 ug/L


250 uS/L


50.0 ug/L


500 uq/L


375 ug/L


62.5 ug/L


250 Ug/LDilution Factor: 2.5

1250 ug/L


ISO ug/LDilution Factor; 2.5

ug/L SW846 6010B

Analysis Time..

SW846 6010B

Analysis Time..:

SW846 6010B

Analysis Time.-



SW846 6010B

Analysis Time..;

SW846 6010B"Analysis Time..t

SW846 6010B

Analysis Time..:


SW846 6010B

Analysis Time.

SW846 6010BAnalysis Time.:

SW846 6010B

Analysis Time..:

14:51

14:51

14:51

14:51

14:51

14:51

14,51

14:51

14:51

14:51

14:51.

14:51

Matrix ........ SOLID

PREPARATION- WORK

ANALYSIS DATE ORDER #

07/12-07/13/05 EE2MGIAA

07/12-07/13/05 HE2MG1AC

07/12-07/13/05 HE2MG1AD

07/12-07/13/05 HE2MG4IA

07/12-07/13/05 HE2MGIAF

07/12-07/13/05 HE2MG1AG

07/12-07/13/0S HE2MGIAH

07/12-07/13/05 HE2MGIAJ

07/12-07/13/05 HE2MG1AK

07/12-07/13/05 HE2MGIAL

07/12-07/13/05 HE2MGIAM

07/12-07/13/05 HE2MGIAN

Prep Batch #...: 5194097Mercury ND 10.0 ug/L SW846 7470A 07/15/05 HE2MG1AP

Dilution Factor: 5 Analysis T:


ime.,: 14:44

4

SCIENTECH INC


TCLP Metals

Lot-Sample #,...: FSG070301-006 Matrix ......... : SOLID

NOTE (S) :Analysis performed In accordance with I•SEPA Toxicity Characterislic Larhing Piocedure Method 1311

1 Method blank contamination. The assoctited method blank contains the target anatytc at a reportable level.

B Eslmatcd re-it. Reshlt is loss than RL.

SCIENTECH INC

Client Sample ID: 6-30-OS S-7

TCLP Metals

Lot-Sample #..: FSG070301-007

Date Sampled... : 06/30/05 13:30 Date Received..: 07/07/05

Leach Date ..... : 07/11/05 Leach Batch #..: P519204


Matrix ........ SOLID

Prep Batch i...: 5193423Arsenic ND

Barium J14600

Cadmium ND

Chromium ND

Lead ND

Silver ND

Selenium ND

Antimony ND

Beryllium ND

Nickel 8360

Thallium ND

Zinc 13.8 B,J

500 ug/L


500 ug/LDilution Factor: 2.S

25.0 ug/LDilut'ion Factor: 2.5


250 • ug/LDilution Factor: 2.5



375 ug/L

Dilution Factors 2.5





Analysis

SW846

Analysis

SW846

Analysis

SW846

Ahalysia

SW846

Analysis

SW846

Analysis

SW846

Analysis

SW846

Analysis

SW846

Analysis

SW846Analysis

SW846

Analysis

SW846

Analysis

Time..

6010B3

Time..

6010B3

Time..,6010BTime. .601013Time..:

6010BTime..:

6010BTime..:

6010BTime..:

6010BTime. .:

6010BTime,..:

601013Time..

60101BTime..:

601DBTime. .

14:56

14:56

14:56

14:56

14:56

14:56

14:56

14:56

14:56

14:56

14:56

14:"56

SW846 6010B

PREPARATION-ANALYSIS DATE

07/12-07/13/05

07/12-07/13/os

07/12-07/13/OS

07/12-07/13/o5

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/1.2-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

WORKORDER #

HE2MHIAA'

HE2MHIAC

HE2MH1AD

HE2MH1AR

HE2MHIAF

HE2MH1AG

HE2MH1AH

HE2MHIAJ

HE2MH1AK

EE2MH13AL

HE2MH1AM

BE2MHIAN

Prep Batch #...: 5194097

Mercury ND 10,0 SW846 7470A 07/15/05 HE2MHlAPDilution Factor: S Analysis T:


iCe, , : 14:47

1.-.

SCIE=ThCH INC


TCLP Metals

Lot-Samuple # ... : F5G070301-007 Matrix ......... : SOLID

NOTE (S) :Analysis perforated In accordance with USSPA Toxicity Charcteristic Leaching Procedure Method )3] 1

J1 Method blankc contamination. The "elocated method blank contains the target analyte at a reportable level.B Estimateed resule. Reasutl is less Eln RL

7}

--..o

SCIENTECH INC


TCLP Metals

Lot-Sample I...: F5G070301-008Date Sampled...: 06/30/05 13:35 Date Received..: 07/07/05Leach Date_..: 07/11/05 Leach Batch #.-: P519204




07/12-07/13/05 HE2MJIAAPrep Batch #...: 5193423

Arsenic

BaXium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

Zinc

ND

11000 J

ND

ND

ND

NU

ND

ND

ND

3290

ND

8.0 B,J

500 ug/LDilution Factor7 2.5

500 uq/LDilution Factor: 2,5

25.0 uq/LDilution Factor: 2.5


250 uq/LDilution Factor: 2,5


500 ug/LDilution Factor, 2.5

375 ug/LDilution Factor% 2.5


250 . ug/LDilution Factor: 2.5


15O uq/L


Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW84GAnalysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

SW846Analysis

Time..: 15:02

6010B

Time..: 15:02

6010B

Time..: 25:02

6010B

Time..: 15:02

6010BTime..: 25:02

6010BTime..: 15:02

602.0B

Time..: 15:02

6010B

Time..; 15:02

6010BTime..: 15:02

Time..: 15:02

6010B

Time,.: 15:02

GOiOBTime.. 15:02

SW846 6010B

07/12-07/13/05

07/12-07/13/os

07/12-07/13/os

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/05

07/12-07/13/os

07/12-07/13/05

HE2MJIJAC

HE2MJIAD

HE2MJIAE

HE2MJIAF

HE2MJIAG

HE2MJIAH

HE2MJIAJ

HE2MJIAK

EF2MfJIAL

HE2MJ1AM

HE2MJ.AN

Prep Batch #...: 5194097

Mercury ND 10.0 ug/L SW846 7470AAnalysis Time..: 14:53

07/1•I5/ HE2MJIAPDilution Factor: 5


(..t

SCIE=TECH INC


TCLP Metals

Lot-Sample #...: F5G070301-008 Matrix ......... : SOLID

NOTE (S) :Analysis performed in accordance with USEPA T'oxilcity Characteritic Leliching Procedure Method 1311

1 Method blank contamination. The associated method blank contains the target analyle at a reportaibe level.

B .stnmated result. Result is less than RL.

,

M•-)EOD BLANK REPORT

TCLP Metals

Client Lot #...: FSG070301 Matrix ..........- SOLID

PREPARATION- WORKREPORTINGPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #

MB Lot-Sample #: F5Gll0000-412 Prep Batch #...: 5193423Leach Date.....;. 07/11/05 Leach Batch #..: P519204

Arsenic

Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

ND

18.2 B

ND

ND

ND

ND

ND

ND

ND

ND


Analysis Time.. 13:46


Analysis Time..; 13:46,



50.0 ug/LDilution Factor: 2,5

Analysia Time..: 13:46

25o uq/LDilution Factor: 2.5




5oo uqg/LDilution Factor: 2.5






250 ug/L

Dilution Factorz 2.5


SWB46

SK846

SW846

SW846

SW846

SW846

SW846

SWMS4 6

SW846

SW846

6010B

60103

6010B

6010B

6010B

6010B

6010B

6010B

60108

6010B

07/12-07/13/05 HE8FQIAA

07/12-07/13/05 81E8FQ1AC

07/12-07/13/05 HE8FQ1AD

07/12-07/13/05 HESFQIAE

07/12-07/13/05 HRBFQ1AF

07/12-07/13/05 HE8FQIAG

07/12-07/13/05 HEBFQlAH

07/12-07/13/05 HE8FQlAJ

07/12-07/13/05 HE8FQlAK

07/12-07/13/05 HE8FQ1AL


"( ...

METHOD BLANK REPORT

TCLP Metals

Client Lot #...: F5G070301 Matrix ......... : SOLID

REPORTING PREPARATION- WORKPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #

MB Lot-Sample #: F5GI10000-412 Prep Batch #...:Leach Date.....- 07/11/05 Leach Batch V..:Mercury ND 10.0 ug/L

Dilution Pactor: 5Analysis Time.. 14;18

5194097P519204

SW846 7470A 07/15/05 HE8FQIAP

MB Lot-Sample #. F5GII0000-412 Prep Batch #. . :

Leach Date ..... ; 07/11/05 Leach Batch #..:

Thallium ND 1250 ug/LDilution Factors 2.5


5193423P519204

SW846 6010B

SW846 6010B

07/12-07/13/05 HEBFQIAM

07/12-07/13/05 BEBFQlANZinc 11.6 B 150 ug/LDilution Factor: 2.5

Analysis Timre..: 13:46

NOTE (S):

Calculations are istrfortned before rounding to avoid round-off erors ift calculated r'enut.. E.stm ated resu'l. R s.ult Is len. than RL.

K.

LABORATORY CONTROL SAMPLE EVALUATION REPORT

TCLP Metals

Client Lot #...:

PARAMETER

F5G070301

PERCENT RECOVERY

RECOVERY LIMITS METHOD

Matrix ........ .. SOLID

PREPARATION-ANALYSIS DATE WORK ORDER #

07/12-07/13/05 HFA251AALCS Lot-Sample#: F5G120000-423 Prep Batch #...: 5193423Arsenic

'Barium

Cadmium

Chromium

Lead

Silver

Selenium

Antimony

Beryllium

Nickel

Thallium

Zinc

106

103

99

95

96

100

109

101

105

95

96

104


(80 - 120) SW846 601;Dilution Factor: 2.5

(80 - 120) SW846 601Dilution Factor; 2.5

(80 - 120) SW846 601


i80 - 120) SW846 '601

Dilution Factor; 2.5



(80 - 120) SW846 601


(80 - 120) SW846 601


(80 - 120) SW846 601


(80 - 120) SW846 601


(80 - 120) SW846 601

C

C

C

C

C

(

(80 - 120) SW846 6010BAnalysis Time..: 13:5l

OB 07/12-07/13/05Analysis Time..: 13!51

OB 07/12-07/13/05

Analysis Time-. 13:51

0a 07/12-07/13/05

Analysis Time.-. 13:5S

0B 07/12-07/13/05Analysis Time..- 13,51

OB 07/12-07/13/05


0B 07/12-07/13/05

Analysis Time.- . 13:51

OB 07/12-07/13/OSAnalysis Time..: 13:51

OB 07/12-07/13/05

Analysis Time.. ; 13:51

0B 07/12-07/13/05

HFA251AC

HFA25!AD

HFA251AE

HFA251AF

HFA2S1AG

HFA251AH

HFA251AJ

HFA251AK

HFA251ALAnalysis Time..: 13:51

0B 07/12-07/13/05 HFA251AMAnalysis Time.. ; 13%51

0B 07/12-07/13/05 RFA251AN

Analysis Time..; 13:51Dilution Factor; 2.5

LCS Lot-Sample#:Mercury

F5G130000-097 Prep Batch # ... : 5194097

99 (82 - 125) SW846 7470A 07/15/05

Dilution Factor: 5 Analysis Time..; l4t20


HFCNMIAA

(s'.

LABORATORY CONTROL SAMPLE EVALUATION REPORT

TCLP Metals

Client Lot ... FSG070301 Matrix ......... .. SOLID

PERCENT RECOVERY PREPARATION-PARAMETER RECOVERY LIMITS METHOD ANALYSIS DATE WORK ORDER #

NOTE(S):Caik.lL3tiOS are performed before roundin, to avoid round-off errors in calculaled results.

(

MATRIX SPIKE SAMPLE EVALUATION REPORT

TCLP Metals

Client Lot #...: F50070301Date Sampled... 06/30/05 13:00.Date Received..: 07/07/05

Matrix ......... : SOLID

I PERCENT RECOVERY RPD PREPARATION- WORK

PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER #

MS Lot-Sample #: F5G070301-001 Prep Batch ... : 5193423Leach Date ..... : 07/11/05 Leach Batch *..: P519204

Arsenic

Barium

Cadmium

105104

(83(83

- 111)- 111) 1.0 (0-20)



9898

9594

(79 - 1.1)(79- 111) 0.18 (0-20)


Analysis Time.. 14:02

(65 - 122)

(65 - 122) 0.48 (0-20)Dilution Factor% 2.5

Analysis Time..Cl14:02

(74 - 114)

(74 - 114) 0.56 (0-20)

Dilution Factor; 2,5

Analysis Time.-. 14:02

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

Chromium 9292

07/12-07/13/05 HE2LGIAT07/12-07/13/05 HE2LGIAU

07/12-07/13/05 HE2LGIAV07/12-07/13/05 HE2LG1AW

07/12-07/13/05 HE2LGIAX07/12-07/13/05 HE2LG1A0

07/12-07/13/05 HE2LGIAI07/12-07/13/05 HE2LGIA2

07/12-07/13/05 HE2LGIA307/12-07/13/05 RE2LGIA4

07/12-07/13/05 HE2LGIA5

07/12-07/13/05 HE2LG1A6

07/12-07/13/05 HE2LGIA707/12-07/13/05 HE2LG1A8

07/12-07/13/05 HE2LGIA9

07/12-07/13/05 HE2LGICA

Lead 9191

9089

(65 - 121) SW846 6010B

(65 - 121) 0.25 (0-20) SW846 6010B


.Analysis Time-. 14:02

Silver (70 - 123)(70 -- 123) 1.6 (0-.20)

Dilution Factor; 2.5Analysis Time. 14:02

(76 - 124)(76 - 124) 0.74 (0-20)

Dilution Factor! 2.5Analysis Time.. 14:02

Selenium 107206

Antimony 9595

SW846 6010BSW846 60.10B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

(68(68

- 129)- 129) 0.38 (0-20)


Analysis Time..ý 14:02


MATRIX SPIKE SAMPLE EVALUATION REPORT

TCLP Metals

Client Lot #,...: F51070301Date Sampled...: 06/30/05 13:00 Date Received..: 07/07/05

Matrix ......... : SOLID

PARAMETERBeryllium

PERCENTRECOVERY104103

Nickel 91

90

RECOVERY RPDLIMITS RPD LIMITS(82 - 113)

(82 - 113) 0.34 (0-20)Dilution Factorz 2.5

Analysis Time-. 14:02

(75 - 109)

(75 - 109) 0.42 (0-20)


Analysis Time..: 14!02

(78 - 110)

(78 - 110) 0.23 (0-20)


Analysis Time-. 14i02

METHODSW846 6010BSW846 6010B

PREPARATION- WORKANALYSIS DATE ORDER #07/12-07/13/05 HE2LGICC07/12-07/13/05 HE2LGICD

07/12-07/13/05 HE2LGICE07/12-07/13/05 HE2LGICF

Thallium 9393

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

07/12-07/13/05 HE2LG1CG07/12-07/13/OS HE2LGIC{

07/12-07/13/05 HE2LG1CJ07/12-07/13/05 HE2LGICK

Zinc 101

101(10

(10- 15o)- 150) 0.18 (0-30)


Analysis Time.. 1 14 : 02

MS Lot-Sanple #:Leach Date ..... :Mercury 100

98

FSG070301-001 Prep Batch #...: 5194097

07/11/05 Leach Batch I..: P519204(64 - 122) SW846 7470A(64 - 122) 2.0 (0-20) SW846 7470A

Dilution Factort 5Analysis Time. : 14,29

07/15/05 HE2LGICL07/15/05 HE2LGICM

NOTE (S) :CalculaLions are performcd before rounding to avoid round-off erors In calculated remisui.

K-.

SCIENTECH INC

Client SamDle ID: 6-30-05 S-i

Severn Trent Laboratories - Radiochamistry

Lab Sample ID: F5G070301-001

Work Order: HE2LGDate Collected:Date Received:

06/30/05 130007/07/05 0900

Matrix: SOLID

TotalUncert. Prep Aaaly&ia

PaKa.tr aegult QuaL 12 +/) MDC Date Date Batch 4 lOd

Xeo URANIKU (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Uranium 23419.9 2'1 0.05 07/11/05 07/14/05 5192451 85Uranium 235 0.96 J 0.25 0.07 07/11/05 Q7/14/0S 5192451 85

Uranium 238 19.8 2.1 0.05 07111/05 07/14/05 5192451 85

ISO THORIUM (SHORT CT) DOE .- 01-R MOD pCi/p A-01-R MOD

Thorium 228 55.4 5.2 0.2 07/15/05 07/18/05 5196204 86

Thorium 230 12.8 1.5 0.09 07/15/05 07/18/05 5196204 .86Thorium 232 56.0 5.2 0.06 07/15/05 07/18/D5 5196204 85

NOTE(S)

Data are incomplete without the case narrative.

k iCia determined by instrument performance only.,,.jold results are greater than the MDC

J Result is greater than sample detection limit but leas than stated reporting limit.

SCIENTECH INC


Severn Trent Laboratories - Radiochemistry

Lab Sample ID:Work Order:;Matrix:

FSC070301-002HE2L4SOLID

Date Collected:Date Received:

06/30/05 130507/07/05 0900

TotalVncert. Prep Analysis

Parameter Result Qual (2 a+/-) mc Date Date Batch y Xld s

Iso. URANIUM (SHORT CT) DOE A-01-R M0D pCi/g A-01-R MOD

Uranium 234 8.09 0.93 0.08. 07/11/05 07/14/05 5192451 86

Uranium 235S 0.39 3 0.15 0.07 07/11/05 07/14/05 5192451 86

Uranium 238 9.0 1.0 0.09 07/11/05 07/14/05 5192451 86

ISO THORIUM (SHORT CT) DOEIA-01"x MOD pCi/g A-01-R MODThorium 228 4 1 400715 0 5 6

Thorium 228 43.3 4.0 0.2 07/15/05 07/18/05 5196204 92

Thorium 230 11.2 1.3 0.0 07/15/05 07/18/05 5196204 92Thorium 232 41.9 3.9 0.09 07/15/05 07/18/05 5196204 92

NOTE (S)Data are incouplete without the case narrative.

)C is determined by instrument performance only.

-4old results are greater than the HDC

J Result is greater than sample detection limit but less than stated reporting limit.

SCIENTECH INC



Lab Sample ID;Work Order:

Matrix:

F5G070301-003

HE2L6

SOLID


06/30/05 131007/07/05 0900

TotalUncert. prop Analysia

Parameter ResUlt QUal (2 0/-) MDC Date Dats Batch 0 Yld

Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODUranium 234 10.3 2 1.2 0.09 07/11/G5 07/14/05 5192451 81

Uranium 235 0.64 J 0.20 0.09 07/11/05 07/14/05 5192451 81

Uranium 238 9.9 1.1 0.05 07/11/05 07/14/05 5192451 81

Iso THORIUM (SHORT CT) DOEiA-01-R MOD pCi/g A-01-R MODThorium 228 40.7 3.8 0.1 07/15/05 07/18/05 5196204 91Thorium 230 11.8 -1.4 0.05 07/15/05 07/18/05 5196204 91

Thorium 232 39.2 3.7 0.1 07/15/05 07/18/05 5196204 91

('V

-i

NOTE (S)

Data are incomplete without the case narrative.

DC is determined by instrument performance only..- Sold results are greater than the PMC

J Result is 'greater than sample detection limit but loss than stated reporting limit.

SCIENTECH INC

Client SamnDle ID: 6-30-05 S-4


Lab Sample ID: F5G070301-004Work Order: HE2L8


06/30/05 131507/07/05 0900

Matrix: SOLID

Tot.aOncert. Prep Analysis

PRsamutlr AsQua1 (2 o0/-) ImC Date Date Batch Yld Is

Tao URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Uranium 234 9.29 1.0 0.04 07/11/05 07/14/05 5192451 83

Uranium 235 0.39k J 0.15 0.03 07/11/05 07/14/05 5192451 83

Uranium 238 9.5 1.0 0.03 07/11/05 07/14/05 S192L.51 83

Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Thorium 228 76.6 7.6 0.3 07/15/05 07/18/05 5196204 69

Thorium 230 16.9 2.0 0.2 07/15/05 07/18/05 5196204 69

Thorium 232 75.2 7.5 0.2 07/15/05 07/18/05 5196204 69

NOTE (S)Data are iecccplate without the case narrative,

1DC is determined by instrument performance only.told results are greater than the KDC

J Result is greeter than sample detection limit but lees than stated reporting limit.

SCIENTECH INC

Client SalnDle ID: 6-30-05 S-5


Lab Sample ID:Work Order:Matrix:

F5G070301-005HE2MCSOLID


06/30/05 132007/07/05 0900

TotalUncert. Prep Analysis

Parameter Iesult Qual (2 a+/-) MDc Date Data Batch # Yld %

Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD-Uranium 234 10.2- 1.2 0.09 07/11/05 07/14/05 5192451 87

Uranium 235 0.78 j 0.24 0.08 07/11/05 07/14/05 5192451 87

Uranium 238 10.3 1.2 0.07 07/11/05 07/14/05 5192451 87

Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/5 A-01-R MOD

Thorium 228 28.5f 2.9 0.2 07/15/05 07/18/05 5196204 89

Thorium 230 7.4 -' 1.0 0.06 07/15/05 07/18/05 5196204 89

Thorium 232 29.5 3.0 0.09 07/15/05 07/18/05 5196204 89

NOTH (S)

Data are incomplete without the case narrativo.

DC is determined by instrument performance only.ý"'-Bold reaults are greator than the 4DC

J Result is greator than sample detection limit but less than stated reporting limit.

SCIENTECH INC

Client Sainnle ID: 6-30-05 S-6


Lab Sample ID:Work Order:Matrix:

FSG070301-006

HE2MG

SOLID


06/30/05 132507/07/05 0900

Totaluncert.

Prop Analysis

Parameter Result ual (2 a+/-) 1DC vat. Date Batch # Yld %

Iso URANIUTM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODGranium% 234 9.'2 1.0 0.05 07/11/05 07/14/05 5192451 88Uranium 23S 0.41 1 0.15 0.06 07/11/05 07/14/05 S192451 so

Uranium 238 9.4• 1.0 0.05 07/11/05 07/14/05 5192451 88

Iso THORIU M (SHORT CT) D0 A-01-R MOD pCi/g A-01R MODThorium 228 37.9 3.6 0.2 07/15/05 07/18/05 5196204 "90Thorium 230 1 0_5. 1.3 0.1 07/15/05 07/18/05 S196204 90

Thorium. 232 37.8 3.5 0.1 07/15/05 07/18/05 5196204 90

* NOTE(S)

Data are incomplete without thn case narrative.

( DC is determined by instrument performance only.( 8old results ara greater than the MDC

J Result is greater than sample deto•tion limit but less than stated reporting limit.

SCIENTECH INC



Lab Sample ID: F5G070301-007

Work Order: HE2MH

Matrix; SOLID


06/30/05 133007/07/05 0o00

TotalUneart, Prep Analysis

Parameter Result Qual (2 o+/-) MDC Date Data Batch 0 Yld %

ISO URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Uranium 234 14.3 | 1.6 0.08 07/11/05 07/14/05 5192451 88

Uranium 235 0.70 J 0.21 0.06 07/11/05 07/14/05 5192451 88

Uranium 238 14.4 1.6 0.06 07/11/05 07/14/05 5192451 88

ISO THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Thorium 228 90 16 0.4 07/15/05 07/19/05 5196204 84

Thorium 230 17.3 3.6 0.4 07/15/05 07/19/05 5196204 84

Thorium 232 83 14 0.4 07/15/05 07/19/05 5196204 84

NOTE (S)

Data are incomplete without the caae narrative.

DC in determined by instrument performance only.

results are greater Chan the MDC

J Result is greater than sample detection limit but less than stated reporting limit.

SCIENTECH INC

Client, Samole ID: 6-30-05 S-7 DUP

Severn Trent Laboratories -. Radiochemistry

Lab Sample ID:

Work Order:

Matrix;

F5G070301-007X

HE2MH

SOLID


06/30/05 133007/07/05 0900

TotalUncert. Prep Analysis

Parameter Result Qual (2 a+/-) MDC Date Date Batch # Yld %

ISo URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MOD

Uranium 234 12.7 1.5 0.1 07/11/05 07/14/05 5192451 77

Uranium 235 0.613 J 0.21 0.09 07/11/05 07/14/05 5192451 77

Uranium 238 12.6 1.5 0.07 07/11/05 07/14/05 5192451 77

Iso THORIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODThorium 228 77 14 0.5 07/15/05 07/19/05 5196204 84

Thorium 230 14.8 3.3 0.4 07/15/05 07/19/05 5196204 84

Thorium 232 74 13 0.3 07/15/05 07/19/05 5196204 84

NOTE (S)

Data are inoemplete without the cave narrative.

)C is determined by instrument performance only..... old results are greater than the MDC

iJ Result is greater than Sample detection limit but less than stated reporting limit.

SCIENTECH INC



Lab Sample ID:

Work Order;

Matrix:

FSG070301-008HE2MJSOLID


06/30/05 133507/07/05 0900

TotalVacert. Prop Analysis

Parameter Reauit Qual (2 o+/-) XDC Date Date Batch # Yld .

Iso URANIUM (SHORT CT) DOE A-01-R MOD pCi/g A-01-R MODUranium 23,4 9.2 1.I1 0.1 07/11/05 07 /14/05 5192451 90Uranium 235 0.41• J 0.16 0.09 07/11/05 07/14/05 5192451 90

Uranium 23 8 9.0I 1.0 0.08 07/11/05 07/14/05 5192451 90

ISO THORIUM (SHORT CT) DO A-01-R MOD pCi/g A-01-R MOD

Thorium 222 309.9 3.3 0.2 07/15/05 07/18/05 5196204 69Thorium 230 7.3 12 .1 0.1 07/15/05 07/18/D5 5196204 69

Thoritum 232 29.9 3.3 0.i 07/15/05 07/18/D5 5196204 69

NOTE(S)

Data are iucompletO without the case narrative.

(\ 'iDC is determined by instrument performance only..Bold results are greater than the MDC

J Result is greater than sample detection lim:it but less than stated reporting limit.

Uranium Decay Chain

28U t, 234Th :

100%

Thorium Decay Chain

234pa * 234u

234 u 230Th * 226Ra * 222Rn *'

218po * 214

pb C 214Bi

232Th r> 22Ra * 22Ac -

2 28Th • 2 24

Ra *2 2 0

Rn c* 2 16

po =:> 212 Pb * 2 1 2Bi

Note: All sample values include stated +2a lab variance. No background was subtracted.

Sample#S-1S-2S-3S-4S-5S-6S-7

S-7[Dup]S-8

Average =

232Th

61.245.842.982.732.541.4

9787

33.2

2 8Th

60.647.344.584.231.441.5106

9133.9

ThE60.9046.5543.7083.4531.9541.45

101.5089.0033.55

238u

21.91011

10.511.510.4

1614.1

10

234u 230Th

pCi< DJm

22 14.39.02 12.511.5 13.210.2 18.911.4 8.410.2 11.815.9 20.914.2 18.110.3 8.4

2 35U

1.21 19.400.54 10.510.84 11.900.54 13.201.02 10.430.56 10.800.91 17.600.82 15.470.57 9.57

13.21 pCl"'gu

3.51 pCi'9m u

16.7 pCi 9'mu

Standard deviation of data set =59.12 pCi"gn Th

25.94 pCiO Tn

85.1 pCi-'mT

Documents

,rjorie McLaugh!in -, Whittaker waste manifest activities · 2012. 11. 30. · ANALYTICAL. REPORT PROJECT NO. 23535 Whittaker, Transfer, PA Lot #: F5G070301 Rich Moss Scientech Inc